Crystallography Open Database

Information card for entry 4115015

Preview

Coordinates	4115015.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C10 H18 Cl4 Pt Si2
Calculated formula	C10 H18 Cl4 Pt Si2
Title of publication	The First Alkene-Platinum-Silyl Complexes: Lifting the Hydrosilation Mechanism Shroud with Long-Lived Precatalytic Intermediates and True Pt Catalysts
Authors of publication	Aroop K. Roy; Richard B. Taylor
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	9510 - 9524
a	8.26 ± 0.002 Å
b	16.961 ± 0.003 Å
c	11.406 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	1598 ± 0.6 Å³
Cell temperature	153.2 K
Ambient diffraction temperature	153.2 K
Number of distinct elements	5
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.0371
Residual factor for significantly intense reflections	0.024
Weighted residual factors for all reflections	0.05
Weighted residual factors for all reflections included in the refinement	0.025
Goodness-of-fit parameter for all reflections	2.222
Goodness-of-fit parameter for all reflections included in the refinement	2.4
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4115015.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115015.cif
68401	2012-10-26	cif/ Adding structures of 4115015 via cif-deposit CGI script.	4115015.cif