#------------------------------------------------------------------------------ #$Date: 2019-05-15 01:36:15 +0300 (Wed, 15 May 2019) $ #$Revision: 215145 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/12/72/4127264.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4127264 loop_ _publ_author_name 'Shanahan, James P.' 'Szymczak, Nathaniel K.' _publ_section_title ; Hydrogen Bonding to a Dinitrogen Complex at Room Temperature: Impacts on N2 Activation ; _journal_name_full 'Journal of the American Chemical Society' _journal_paper_doi 10.1021/jacs.9b02288 _journal_year 2019 _chemical_formula_moiety 'C20 H48 N2 P4 Re, Br' _chemical_formula_sum 'C20 H48 Br N2 P4 Re' _chemical_formula_weight 706.59 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-02-12 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 94.734(3) _cell_angle_beta 99.553(3) _cell_angle_gamma 102.843(3) _cell_formula_units_Z 1 _cell_length_a 7.9408(3) _cell_length_b 8.7181(3) _cell_length_c 10.1314(3) _cell_measurement_reflns_used 7521 _cell_measurement_temperature 85(2) _cell_measurement_theta_max 68.6690 _cell_measurement_theta_min 4.4490 _cell_volume 669.13(4) _computing_cell_refinement 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 85(2) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.978 _diffrn_measured_fraction_theta_max 0.968 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -110.00 70.00 1.00 1.00 -- -20.00 0.00-180.00 180 2 \w -45.00 0.00 1.00 1.00 -- -20.00 72.00 0.00 45 3 \w -45.00 0.00 1.00 1.00 -- -20.00 72.00 0.00 45 4 \w -25.00 43.00 1.00 1.00 -- -20.00 36.00 120.00 68 5 \w -45.00 0.00 1.00 1.00 -- -20.00 72.00-180.00 45 6 \w -173.00-128.00 1.00 3.00 -- -92.00 -36.00 120.00 45 7 \w -133.00 -88.00 1.00 3.00 -- -92.00 -36.00 -60.00 45 8 \w -104.00 -59.00 1.00 3.00 -- -92.00 36.00 60.00 45 9 \w -122.00 -77.00 1.00 3.00 -- -92.00 -72.00 60.00 45 10 \w -174.00 -78.00 1.00 3.00 -- -92.00 -72.00-120.00 96 11 \w -93.00 -35.00 1.00 3.00 -- -92.00 36.00-120.00 58 12 \w -176.00 -77.00 1.00 3.00 -- -92.00 -72.00 -60.00 99 13 \w -147.00 -75.00 1.00 3.00 -- -92.00 -72.00-180.00 72 14 \w -176.00 -77.00 1.00 3.00 -- -92.00 -72.00 120.00 99 15 \w -177.00-116.00 1.00 3.00 -- -92.00 -36.00 60.00 61 16 \w -87.00 -9.00 1.00 3.00 -- -92.00 36.00 -60.00 78 17 \w -102.00 -14.00 1.00 3.00 -- -92.00 36.00 0.00 88 18 \w -102.00 -21.00 1.00 3.00 -- -92.00 72.00 120.00 81 19 \w -175.00-104.00 1.00 3.00 -- -92.00 -36.00 0.00 71 20 \w -104.00 -52.00 1.00 3.00 -- -92.00 72.00 60.00 52 21 \w -109.00 -14.00 1.00 3.00 -- -92.00 72.00-120.00 95 22 \w -105.00 -24.00 1.00 3.00 -- -92.00 36.00-120.00 81 23 \w -105.00 -2.00 1.00 3.00 -- -92.00 36.00-180.00 103 24 \w -106.00 -2.00 1.00 3.00 -- -92.00 72.00 -60.00 104 25 \w -106.00 -2.00 1.00 3.00 -- -92.00 72.00 -60.00 104 26 \w -107.00 -29.00 1.00 3.00 -- -92.00 72.00 0.00 78 27 \w -117.00 -72.00 1.00 3.00 -- -92.00 72.00 180.00 45 ; _diffrn_measurement_device 'abstract diffractometer' _diffrn_measurement_device_type 'dtrek-CrysAlisPro-abstract goniometer imported rigaku-d*trek images' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0444389000 _diffrn_orient_matrix_UB_12 0.0179098000 _diffrn_orient_matrix_UB_13 0.1419590000 _diffrn_orient_matrix_UB_21 0.1499204000 _diffrn_orient_matrix_UB_22 -0.0770035000 _diffrn_orient_matrix_UB_23 0.0547680000 _diffrn_orient_matrix_UB_31 0.1289251000 _diffrn_orient_matrix_UB_32 0.1646616000 _diffrn_orient_matrix_UB_33 0.0315823000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0598 _diffrn_reflns_av_unetI/netI 0.0358 _diffrn_reflns_Laue_measured_fraction_full 0.978 _diffrn_reflns_Laue_measured_fraction_max 0.968 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 9468 _diffrn_reflns_point_group_measured_fraction_full 0.978 _diffrn_reflns_point_group_measured_fraction_max 0.968 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 69.142 _diffrn_reflns_theta_min 4.460 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 12.956 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.45195 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'pale yellow' _exptl_crystal_density_diffrn 1.754 _exptl_crystal_description block _exptl_crystal_F_000 352 _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.04 _refine_diff_density_max 2.314 _refine_diff_density_min -1.664 _refine_diff_density_rms 0.229 _refine_ls_extinction_coef 0.0109(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.124 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 135 _refine_ls_number_reflns 2426 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.124 _refine_ls_R_factor_all 0.0389 _refine_ls_R_factor_gt 0.0389 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0733P)^2^+2.3296P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1087 _refine_ls_wR_factor_ref 0.1087 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2424 _reflns_number_total 2426 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja9b02288_si_001.cif _cod_data_source_block jps3296b _cod_database_code 4127264 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula C20H48N2P4BrRe _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.625 _shelx_estimated_absorpt_t_min 0.264 _reflns_odcompleteness_completeness 96.85 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 69.02 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints Uanis(Br1) = Uanis(N1) = Uanis(N2) 3. Others Fixed Sof: Br1(0.5) N1(0.5) N2(0.5) 4.a Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C2(H2A,H2B), C7(H7A,H7B), C6(H6A,H6B), C5(H5A,H5B), C9(H9A,H9B) 4.b Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C10(H10A,H10B,H10C), C1(H1A,H1B,H1C), C4(H4A,H4B,H4C) ; _shelx_res_file ; TITL jps3296b.res created by SHELXL-2016/6 at 10:51:04 on 12-Feb-2019 CELL 1.54184 7.9408 8.7181 10.1314 94.734 99.553 102.843 ZERR 1 0.0003 0.0003 0.0003 0.003 0.003 0.003 LATT 1 SFAC C H N P Br Re UNIT 20 48 2 4 1 1 EADP Br1 N1 N2 L.S. 4 0 0 PLAN 20 SIZE 0.04 0.04 0.14 BOND $H list 4 fmap 2 53 acta REM REM REM WGHT 0.073300 2.329600 EXTI 0.010867 FVAR 0.82976 PART 1 RE1 6 0.500000 0.500000 0.500000 10.50000 0.01685 0.00668 = 0.01227 0.00122 -0.00020 0.00401 P1 4 0.350688 0.342158 0.646821 11.00000 0.02063 0.01071 = 0.01410 0.00178 0.00051 0.00342 P2 4 0.315788 0.292145 0.335182 11.00000 0.01894 0.00896 = 0.01353 0.00043 -0.00055 0.00241 C3 1 0.471067 0.234261 0.763076 11.00000 0.02778 0.01830 = 0.01692 -0.00144 -0.00164 0.00899 AFIX 23 H3A 2 0.387333 0.163867 0.803841 11.00000 -1.20000 H3B 2 0.528004 0.169224 0.711637 11.00000 -1.20000 AFIX 0 C8 1 0.299403 0.059430 0.110710 11.00000 0.03117 0.01444 = 0.02071 -0.00384 0.00489 0.00706 AFIX 137 H8A 2 0.366902 0.023108 0.049784 11.00000 -1.50000 H8B 2 0.195863 0.081314 0.060057 11.00000 -1.50000 H8C 2 0.265755 -0.021019 0.166983 11.00000 -1.50000 AFIX 0 C2 1 0.220531 0.430130 0.751323 11.00000 0.03057 0.01760 = 0.01841 0.00016 0.00690 0.01047 AFIX 23 H2A 2 0.301053 0.512852 0.816467 11.00000 -1.20000 H2B 2 0.145344 0.481022 0.693518 11.00000 -1.20000 AFIX 0 C7 1 0.410070 0.210116 0.198539 11.00000 0.02837 0.01613 = 0.02016 -0.00339 0.00468 0.00141 AFIX 23 H7A 2 0.436249 0.291403 0.140077 11.00000 -1.20000 H7B 2 0.521051 0.189166 0.238794 11.00000 -1.20000 AFIX 0 C10 1 -0.056494 0.190981 0.212660 11.00000 0.02539 0.02107 = 0.03737 -0.00477 -0.00419 0.00450 AFIX 137 H10A 2 -0.147401 0.224600 0.155920 11.00000 -1.50000 H10B 2 -0.094983 0.163047 0.294337 11.00000 -1.50000 H10C 2 -0.031470 0.100540 0.166267 11.00000 -1.50000 AFIX 0 C6 1 0.246793 0.117410 0.421940 11.00000 0.02146 0.01283 = 0.01782 0.00443 -0.00009 0.00405 AFIX 23 H6A 2 0.152737 0.039067 0.362749 11.00000 -1.20000 H6B 2 0.344900 0.069616 0.446936 11.00000 -1.20000 AFIX 0 C1 1 0.104981 0.321116 0.828250 11.00000 0.03237 0.02600 = 0.02473 0.00627 0.00985 0.00790 AFIX 137 H1A 2 0.020347 0.240757 0.765543 11.00000 -1.50000 H1B 2 0.044820 0.381913 0.878906 11.00000 -1.50000 H1C 2 0.177019 0.272038 0.888739 11.00000 -1.50000 AFIX 0 C5 1 0.183888 0.171837 0.546649 11.00000 0.02198 0.01404 = 0.02159 0.00635 0.00138 -0.00220 AFIX 23 H5A 2 0.162745 0.085416 0.600916 11.00000 -1.20000 H5B 2 0.074057 0.202497 0.520504 11.00000 -1.20000 AFIX 0 C9 1 0.106688 0.323496 0.246207 11.00000 0.02595 0.01907 = 0.04096 0.00656 -0.01018 0.00263 AFIX 23 H9A 2 0.079274 0.408873 0.299811 11.00000 -1.20000 H9B 2 0.128395 0.362112 0.162022 11.00000 -1.20000 AFIX 0 C4 1 0.609540 0.341801 0.874714 11.00000 0.03140 0.01669 = 0.02222 0.00438 -0.00180 0.00718 AFIX 137 H4A 2 0.696214 0.408626 0.835505 11.00000 -1.50000 H4B 2 0.665235 0.278174 0.932395 11.00000 -1.50000 H4C 2 0.554423 0.406365 0.926585 11.00000 -1.50000 AFIX 0 PART 0 PART -1 BR1 5 0.731061 0.322517 0.517324 10.50000 0.01946 0.01330 = 0.01799 0.00172 0.00135 0.00897 PART 0 PART 1 N1 3 0.670954 0.375667 0.511452 10.50000 0.01946 0.01330 = 0.01799 0.00172 0.00135 0.00897 N2 3 0.773872 0.303011 0.518856 10.50000 0.01946 0.01330 = 0.01799 0.00172 0.00135 0.00897 HKLF 4 REM REM R1 = 0.0389 for 2424 Fo > 4sig(Fo) and 0.0389 for all 2426 data REM 135 parameters refined using 0 restraints END WGHT 0.0732 2.3394 REM Highest difference peak 2.314, deepest hole -1.664, 1-sigma level 0.229 Q1 1 0.6470 0.4818 0.4995 11.00000 0.05 2.31 Q2 1 0.5724 0.3542 0.5437 11.00000 0.05 1.59 Q3 1 0.4792 0.5757 0.3942 11.00000 0.05 1.27 Q4 1 0.5073 0.4965 0.5829 11.00000 0.05 1.08 Q5 1 0.5599 0.1237 0.3521 11.00000 0.05 0.93 Q6 1 0.1819 0.1424 0.4605 11.00000 0.05 0.84 Q7 1 0.8985 0.4914 0.5091 11.00000 0.05 0.68 Q8 1 0.5363 0.5843 0.6144 11.00000 0.05 0.64 Q9 1 0.5829 0.1772 0.6587 11.00000 0.05 0.64 Q10 1 0.4224 0.1410 0.7249 11.00000 0.05 0.63 Q11 1 0.2930 0.0846 0.4295 11.00000 0.05 0.61 Q12 1 -0.0153 0.3079 0.7200 11.00000 0.05 0.61 Q13 1 0.7717 0.1774 0.5624 11.00000 0.05 0.60 Q14 1 0.3089 -0.0058 0.8146 11.00000 0.05 0.59 Q15 1 0.1376 0.0786 0.1362 11.00000 0.05 0.58 Q16 1 0.3238 -0.0368 0.4756 11.00000 0.05 0.56 Q17 1 -0.0599 0.2039 0.1434 11.00000 0.05 0.56 Q18 1 0.2471 0.0615 0.4206 11.00000 0.05 0.56 Q19 1 0.7980 0.5479 0.4795 11.00000 0.05 0.56 Q20 1 -0.0257 0.1014 0.7524 11.00000 0.05 0.55 ; _shelx_res_checksum 45548 _shelx_hkl_file ; -9 -1 2 145.14 6.37 -9 -1 3 153.33 6.59 -9 0 0 218.90 7.49 -9 0 1 90.04 5.32 -9 0 2 465.48 11.33 -9 0 3 778.36 14.30 -9 0 4 318.54 10.81 -9 0 5 488.33 10.48 -9 1 0 102.23 5.90 -9 1 1 194.02 8.01 -9 1 2 346.94 10.29 -9 1 3 330.34 10.09 -9 1 4 217.57 8.26 -9 1 5 190.65 7.90 -9 2 -1 61.87 4.81 -9 2 0 338.27 10.22 -9 2 1 563.52 13.08 -9 2 2 242.55 8.98 -9 2 3 14.87 3.48 -9 2 4 2.67 2.96 -9 2 5 54.34 4.92 -9 3 -1 374.41 10.78 -9 3 0 904.72 16.59 -9 3 1 769.44 15.31 -9 3 1 887.21 13.98 -9 3 2 259.05 9.21 -9 3 3 98.64 6.05 -9 3 4 26.07 3.95 -9 4 -1 759.32 15.55 -9 4 0 673.00 14.76 -9 4 0 732.49 12.59 -9 4 1 252.50 9.33 -9 4 1 319.43 8.72 -9 4 2 369.71 11.20 -9 4 3 356.37 11.66 -9 5 -1 538.40 12.91 -9 5 0 184.14 8.44 -9 5 0 226.18 7.19 -9 5 1 427.84 9.83 -9 5 1 334.06 10.83 -9 5 2 655.24 14.60 -9 5 2 964.11 14.47 -9 5 3 1183.92 15.72 -8 -2 0 44.35 4.01 -8 -1 -1 696.60 12.67 -8 -1 0 118.19 6.35 -8 0 -1 1355.03 19.56 -8 0 0 654.49 14.65 -8 1 -2 537.28 12.20 -8 1 -1 839.49 16.35 -8 1 0 2531.21 29.88 -8 1 1 1924.51 26.73 -8 1 6 497.02 11.96 -8 1 7 974.58 12.19 -8 2 -4 207.46 6.89 -8 2 -3 33.06 4.51 -8 2 -2 57.82 5.02 -8 2 -1 656.75 15.10 -8 2 0 2465.40 30.48 -8 2 1 2324.73 29.89 -8 2 2 939.73 19.48 -8 2 3 537.69 14.73 -8 2 4 428.71 12.56 -8 2 5 373.13 10.79 -8 2 6 830.90 12.35 -8 2 6 632.28 13.15 -8 2 7 1361.40 14.64 -8 3 -3 4.65 3.44 -8 3 -2 307.41 10.64 -8 3 -1 429.65 12.64 -8 3 -1 414.80 10.54 -8 3 0 289.57 10.88 -8 3 1 498.77 14.21 -8 3 2 291.11 11.19 -8 3 3 346.68 11.65 -8 3 4 262.84 9.66 -8 3 5 153.39 7.39 -8 3 6 313.55 8.05 -8 3 7 196.78 6.08 -8 4 -4 423.37 10.93 -8 4 -3 720.05 16.02 -8 4 -2 548.81 14.99 -8 4 -2 591.91 12.29 -8 4 -1 236.55 9.96 -8 4 -1 250.60 8.40 -8 4 0 24.61 4.29 -8 4 1 34.07 4.82 -8 4 2 337.91 11.49 -8 4 3 425.19 12.60 -8 4 4 644.59 14.14 -8 4 5 292.44 8.07 -8 4 6 9.48 2.71 -8 4 7 4.73 2.40 -8 5 -3 1934.52 20.12 -8 5 -3 1708.49 23.51 -8 5 -2 788.74 17.99 -8 5 -2 911.77 15.14 -8 5 -1 432.87 13.70 -8 5 -1 433.48 11.01 -8 5 -1 398.27 12.14 -8 5 0 270.03 10.98 -8 5 0 314.87 9.66 -8 5 1 524.46 14.69 -8 5 2 665.17 16.12 -8 5 3 719.02 17.06 -8 5 3 752.40 17.47 -8 5 4 881.92 18.74 -8 5 4 837.23 18.34 -8 5 5 252.36 10.01 -8 5 5 226.39 9.57 -8 5 6 19.21 3.75 -8 5 6 18.48 3.72 -8 6 -3 1312.44 18.16 -8 6 -3 1556.00 17.33 -8 6 -2 833.13 13.91 -8 6 -2 791.13 16.07 -8 6 -1 824.41 14.52 -8 6 -1 796.05 16.55 -8 6 0 1278.12 22.80 -8 6 0 1427.52 19.25 -8 6 1 760.06 17.70 -8 6 1 914.49 15.50 -8 6 2 652.03 15.72 -8 6 2 908.99 15.29 -8 6 3 377.56 12.21 -8 6 3 377.10 12.19 -8 6 4 267.78 10.57 -8 6 4 291.97 10.53 -8 6 5 633.16 14.29 -8 6 5 618.43 14.11 -8 7 -2 558.86 11.15 -8 7 -2 599.65 10.83 -8 7 -1 1241.97 17.81 -8 7 -1 1299.45 19.53 -8 7 0 1780.00 20.06 -8 7 0 1671.52 22.95 -8 7 1 1250.42 16.79 -8 7 1 964.55 16.09 -8 7 2 454.82 10.00 -8 7 3 228.71 6.91 -7 -3 7 298.63 6.57 -7 -2 -1 636.60 12.86 -7 -2 6 430.81 9.10 -7 -2 7 159.97 5.49 -7 -2 8 335.94 6.99 -7 -1 5 278.19 8.09 -7 -1 6 170.41 6.46 -7 -1 7 346.84 8.21 -7 -1 8 195.59 5.83 -7 -1 9 332.45 6.50 -7 0 -6 489.11 8.95 -7 0 -2 226.89 8.65 -7 0 -1 947.99 17.49 -7 0 5 19.54 3.21 -7 0 6 247.16 7.70 -7 0 7 805.55 12.78 -7 0 8 422.37 8.67 -7 0 9 105.24 4.02 -7 1 -6 1797.40 17.86 -7 1 -3 278.33 9.24 -7 1 -2 436.88 11.99 -7 1 -1 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15.39 0 2 11 668.27 8.75 0 3 -11 813.16 15.65 0 3 -11 838.30 12.30 0 3 -10 1589.56 20.99 0 3 -10 1337.52 22.06 0 3 -9 805.40 16.03 0 3 -9 768.80 18.67 0 3 -9 822.51 15.91 0 3 -8 101.43 5.97 0 3 -8 94.11 7.01 0 3 -8 92.86 5.83 0 3 -8 93.99 7.11 0 3 -7 58.45 6.25 0 3 -7 62.31 4.70 0 3 -7 42.48 5.40 0 3 -7 77.85 5.11 0 3 -7 42.03 5.37 0 3 -7 68.70 6.14 0 3 -7 65.34 4.67 0 3 -6 130.01 6.03 0 3 -6 129.58 8.27 0 3 -6 131.26 5.78 0 3 -6 128.25 7.56 0 3 -6 125.33 5.89 0 3 -6 105.46 6.90 0 3 -6 107.81 7.06 0 3 -5 657.80 12.61 0 3 -5 618.43 11.09 0 3 -5 697.20 15.93 0 3 -5 687.49 12.45 0 3 -5 636.98 14.46 0 3 -5 647.73 14.48 0 3 -4 3859.89 27.43 0 3 -4 3992.73 35.14 0 3 -2 458.11 11.13 0 3 -1 83.79 3.38 0 3 -1 84.45 3.73 0 3 0 67.96 3.25 0 3 1 1176.88 18.35 0 3 1 1159.08 18.04 0 3 2 1325.35 20.68 0 3 2 1340.63 20.79 0 3 3 949.89 19.58 0 3 3 963.94 19.80 0 3 4 1333.49 26.16 0 3 4 1383.74 18.73 0 3 4 1381.52 13.38 0 3 5 14.76 4.61 0 3 5 18.83 3.39 0 3 5 15.67 4.71 0 3 5 17.56 2.16 0 3 6 46.51 4.59 0 3 6 49.98 3.51 0 3 7 238.09 9.52 0 3 7 225.08 7.02 0 3 8 350.16 10.78 0 3 8 300.96 8.12 0 3 9 822.00 14.26 0 3 9 645.83 11.03 0 3 10 630.08 9.54 0 3 11 190.56 4.44 0 4 -11 1459.77 20.15 0 4 -11 1602.80 16.03 0 4 -10 1972.36 26.94 0 4 -10 2094.08 22.46 0 4 -9 1170.76 23.16 0 4 -9 1209.98 18.69 0 4 -8 938.36 20.95 0 4 -8 896.16 20.97 0 4 -8 863.75 16.33 0 4 -8 909.09 16.33 0 4 -7 2065.38 32.41 0 4 -7 1977.49 24.20 0 4 -7 1973.39 23.61 0 4 -7 1628.06 26.84 0 4 -7 1639.43 27.06 0 4 -7 1985.09 30.81 0 4 -7 1999.12 24.40 0 4 -6 1002.85 17.05 0 4 -6 1050.48 22.94 0 4 -6 952.84 20.86 0 4 -6 979.06 15.80 0 4 -6 1092.81 22.58 0 4 -6 1023.94 21.58 0 4 -6 972.63 16.16 0 4 -6 939.74 20.61 0 4 -5 1100.45 17.62 0 4 -5 1087.24 21.32 0 4 -5 1102.69 23.34 0 4 -5 1056.70 15.28 0 4 -5 1083.11 20.73 0 4 -5 1068.97 15.56 0 4 -5 1058.34 19.71 0 4 -5 1068.36 19.84 0 4 -4 4142.54 32.98 0 4 -4 4398.35 38.57 0 4 -4 4255.88 34.29 0 4 -4 3758.22 31.96 0 4 -4 3989.34 27.67 0 4 -4 4404.61 38.66 0 4 -4 4163.60 34.45 0 4 -4 4208.11 39.27 0 4 -3 2085.62 26.17 0 4 -3 2041.76 21.10 0 4 -3 1995.51 19.50 0 4 -3 2060.04 25.34 0 4 -3 2016.73 25.06 0 4 -3 2053.44 22.59 0 4 -2 471.64 10.45 0 4 -1 778.44 11.58 0 4 -1 714.26 12.58 0 4 1 925.04 19.37 0 4 1 941.27 19.90 0 4 2 893.33 20.30 0 4 2 893.73 20.05 0 4 2 899.41 10.50 0 4 3 809.10 11.30 0 4 3 820.32 14.37 0 4 3 755.65 13.85 0 4 3 707.48 19.59 0 4 3 730.75 20.00 0 4 3 705.78 9.82 0 4 4 585.54 13.14 0 4 4 573.86 13.05 0 4 4 545.94 9.20 0 4 4 567.77 19.44 0 4 4 552.70 19.18 0 4 5 1090.78 19.04 0 4 5 1106.45 18.79 0 4 6 1089.63 19.79 0 4 6 1085.02 19.95 0 4 7 355.02 8.87 0 4 7 379.82 11.43 0 4 8 254.80 8.88 0 4 8 228.84 7.04 0 4 9 186.65 6.46 0 4 9 160.49 5.36 0 4 10 31.04 3.33 0 4 10 76.50 3.25 0 5 -11 775.88 13.36 0 5 -11 910.01 11.15 0 5 -10 804.32 16.57 0 5 -10 782.23 12.30 0 5 -9 1379.20 24.57 0 5 -9 1390.98 19.16 0 5 -8 2528.25 34.61 0 5 -8 1686.27 27.43 0 5 -8 2500.70 26.47 0 5 -8 1768.31 28.04 0 5 -8 2557.38 35.60 0 5 -8 2485.14 27.56 0 5 -7 2873.06 36.96 0 5 -7 3355.80 42.13 0 5 -7 3369.31 33.20 0 5 -7 3131.36 29.37 0 5 -7 2905.27 36.96 0 5 -7 3315.99 41.12 0 5 -6 3809.28 35.85 0 5 -6 3837.07 45.72 0 5 -6 3821.96 43.20 0 5 -6 3704.90 30.89 0 5 -6 3886.69 43.76 0 5 -6 3774.26 43.19 0 5 -6 3753.65 43.78 0 5 -5 1362.85 26.73 0 5 -5 1281.10 20.70 0 5 -5 1336.59 17.60 0 5 -5 1297.71 22.95 0 5 -5 1293.72 24.15 0 5 -5 1331.64 24.41 0 5 -5 1377.83 25.54 0 5 -4 841.32 16.20 0 5 -4 832.88 20.70 0 5 -4 824.37 19.09 0 5 -4 801.09 16.32 0 5 -4 781.79 15.58 0 5 -4 826.90 19.03 0 5 -4 797.21 12.52 0 5 -4 832.42 19.00 0 5 -3 3034.42 29.63 0 5 -3 3049.59 36.82 0 5 -3 3077.97 29.17 0 5 -3 3020.22 26.81 0 5 -3 3095.66 35.14 0 5 -3 3126.53 35.32 0 5 -2 3569.34 30.79 0 5 -2 4143.27 41.03 0 5 -2 3791.53 28.82 0 5 -2 3784.00 28.64 0 5 -2 3955.86 38.85 0 5 -2 3882.99 38.52 0 5 -2 3824.79 31.89 0 5 -2 4061.71 37.75 0 5 -1 5807.78 37.53 0 5 -1 6249.16 45.99 0 5 -1 5787.18 28.77 0 5 -1 5801.11 33.23 0 5 -1 5432.94 33.75 0 5 -1 5931.63 46.80 0 5 -1 5869.37 46.66 0 5 0 4718.82 31.88 0 5 0 4561.60 27.36 0 5 0 4551.62 28.08 0 5 0 4579.16 31.14 0 5 0 4766.96 42.02 0 5 0 4779.25 41.86 0 5 1 2329.24 21.13 0 5 1 2361.65 23.08 0 5 1 2625.88 31.23 0 5 1 2579.86 30.79 0 5 2 1550.57 31.56 0 5 2 1577.73 15.85 0 5 2 1620.02 19.84 0 5 2 1850.38 26.41 0 5 2 1539.15 19.47 0 5 2 1694.47 20.80 0 5 2 1552.80 32.25 0 5 2 1854.92 26.55 0 5 3 148.07 5.28 0 5 3 157.73 11.27 0 5 3 203.54 9.45 0 5 3 169.83 6.94 0 5 3 178.09 7.48 0 5 3 182.70 7.63 0 5 3 165.74 11.77 0 5 3 210.71 9.60 0 5 4 1024.89 17.51 0 5 4 1013.28 17.55 0 5 5 3872.74 35.69 0 5 5 3782.88 28.23 0 5 6 1890.49 24.90 0 5 6 1932.98 28.46 0 5 7 452.68 13.71 0 5 7 472.02 10.22 0 5 8 184.76 6.80 0 5 8 171.18 5.77 0 5 9 103.97 4.24 0 5 9 55.20 4.02 0 6 -10 54.00 4.43 0 6 -10 58.88 3.95 0 6 -10 55.98 4.58 0 6 -10 59.33 3.23 0 6 -9 769.95 17.09 0 6 -9 761.75 15.58 0 6 -9 751.33 12.06 0 6 -8 1676.11 27.42 0 6 -8 1181.36 22.80 0 6 -8 1590.13 26.88 0 6 -8 1215.82 23.09 0 6 -8 1583.37 18.93 0 6 -7 2204.57 32.50 0 6 -7 2501.51 36.05 0 6 -7 2200.56 32.67 0 6 -7 2313.05 24.10 0 6 -7 2436.67 28.92 0 6 -7 2333.67 34.58 0 6 -6 2833.68 39.86 0 6 -6 2907.36 26.90 0 6 -6 2720.72 31.11 0 6 -6 2686.37 38.71 0 6 -6 2815.15 38.34 0 6 -6 2792.40 38.44 0 6 -6 2803.13 38.33 0 6 -5 996.22 23.49 0 6 -5 985.33 19.14 0 6 -5 941.76 20.68 0 6 -5 911.79 21.63 0 6 -5 983.70 22.81 0 6 -5 948.32 22.24 0 6 -4 522.08 16.73 0 6 -4 524.83 13.72 0 6 -4 492.75 13.61 0 6 -4 489.36 13.23 0 6 -4 492.99 15.69 0 6 -4 531.21 17.09 0 6 -4 540.93 17.17 0 6 -3 2250.61 32.99 0 6 -3 2181.46 25.41 0 6 -3 2276.27 32.20 0 6 -3 2238.76 26.52 0 6 -3 2264.40 33.59 0 6 -3 2285.61 33.65 0 6 -2 4790.59 38.04 0 6 -2 4762.33 45.06 0 6 -2 4940.33 45.11 0 6 -2 4812.37 35.95 0 6 -2 4605.31 35.70 0 6 -2 4904.64 48.37 0 6 -2 4745.09 47.59 0 6 -1 4757.69 36.57 0 6 -1 4653.59 41.43 0 6 -1 4678.56 28.49 0 6 -1 4802.28 33.32 0 6 -1 4733.84 35.69 0 6 -1 4866.69 48.09 0 6 -1 4913.66 48.45 0 6 0 4679.74 30.50 0 6 0 4642.42 32.14 0 6 0 4651.67 35.69 0 6 0 4678.62 46.51 0 6 0 4567.87 46.00 0 6 1 2451.12 23.54 0 6 1 2483.14 26.53 0 6 1 2565.34 34.20 0 6 1 2555.91 33.97 0 6 2 686.36 12.97 0 6 2 759.25 18.69 0 6 2 688.90 14.44 0 6 2 747.21 18.64 0 6 3 1297.83 15.83 0 6 3 1341.16 19.15 0 6 3 1409.59 21.46 0 6 3 1571.06 26.27 0 6 3 1568.84 26.18 0 6 4 2038.43 24.48 0 6 4 2143.70 27.08 0 6 5 2463.61 27.13 0 6 5 2446.77 29.80 0 6 6 2330.02 25.65 0 6 6 2227.81 27.80 0 6 7 1196.61 16.63 0 6 7 1027.92 17.42 0 6 8 367.44 7.31 0 6 8 479.19 10.47 0 7 -9 273.17 8.30 0 7 -9 267.27 9.21 0 7 -8 771.30 16.74 0 7 -8 750.04 16.97 0 7 -8 537.37 14.23 0 7 -8 547.35 14.38 0 7 -7 423.32 11.87 0 7 -7 378.19 13.35 0 7 -7 454.50 14.61 0 7 -7 415.79 13.96 0 7 -7 375.50 13.30 0 7 -6 391.14 14.41 0 7 -6 383.55 11.95 0 7 -6 362.72 13.55 0 7 -6 386.87 14.98 0 7 -6 392.36 15.09 0 7 -5 709.84 19.45 0 7 -5 709.89 16.27 0 7 -5 713.77 18.65 0 7 -5 716.60 19.21 0 7 -5 730.95 20.47 0 7 -5 714.48 20.19 0 7 -4 370.51 12.25 0 7 -4 369.93 14.08 0 7 -4 378.14 11.88 0 7 -4 343.81 12.37 0 7 -4 346.22 13.47 0 7 -4 411.88 16.10 0 7 -4 390.48 15.49 0 7 -3 606.77 17.11 0 7 -3 647.08 15.26 0 7 -3 658.12 17.88 0 7 -3 641.40 15.07 0 7 -3 661.33 19.79 0 7 -3 687.96 20.09 0 7 -3 650.83 15.11 0 7 -2 667.92 16.91 0 7 -2 611.07 14.11 0 7 -2 630.88 14.36 0 7 -2 664.79 14.76 0 7 -2 629.59 19.01 0 7 -2 643.08 19.22 0 7 -1 810.82 15.44 0 7 -1 754.46 15.62 0 7 -1 796.40 21.03 0 7 -1 779.11 20.82 0 7 0 1468.75 17.61 0 7 0 1428.75 21.52 0 7 0 1482.03 27.98 0 7 0 1513.98 28.22 0 7 1 860.79 14.33 0 7 1 881.54 17.20 0 7 1 905.63 21.73 0 7 1 923.77 21.91 0 7 2 1796.93 22.22 0 7 2 1855.35 30.24 0 7 2 1856.53 30.21 0 7 3 2832.67 30.87 0 7 3 3018.97 29.75 0 7 4 1089.49 17.50 0 7 4 1099.20 19.09 0 7 5 536.37 11.90 0 7 5 517.78 12.65 0 7 6 942.29 14.83 0 7 6 909.68 15.43 0 7 7 1489.84 15.63 0 7 7 1207.45 15.88 0 8 -8 30.86 3.23 0 8 -8 24.80 3.69 0 8 -8 9.20 3.11 0 8 -8 8.38 3.08 0 8 -7 46.12 5.00 0 8 -7 56.88 4.74 0 8 -7 45.26 5.01 0 8 -7 49.84 5.06 0 8 -6 270.40 11.90 0 8 -6 245.99 10.21 0 8 -6 258.51 10.32 0 8 -6 265.46 11.77 0 8 -5 1162.01 22.57 0 8 -5 1215.36 20.04 0 8 -5 1186.20 25.18 0 8 -5 1168.36 24.89 0 8 -4 1154.52 19.55 0 8 -4 1164.49 22.77 0 8 -4 1126.79 21.93 0 8 -4 1149.64 21.05 0 8 -4 1178.21 25.64 0 8 -4 1211.74 25.86 0 8 -3 232.35 8.85 0 8 -3 234.93 9.98 0 8 -3 229.09 9.69 0 8 -3 254.39 13.06 0 8 -3 243.76 12.66 0 8 -2 154.67 7.71 0 8 -2 155.01 7.61 0 8 -2 168.30 10.73 0 8 -2 166.16 10.58 0 8 -1 37.78 4.16 0 8 -1 43.68 5.93 0 8 -1 43.06 5.96 0 8 0 39.39 4.12 0 8 0 48.11 6.12 0 8 0 44.33 6.01 0 8 1 1206.63 16.47 0 8 1 1179.57 24.36 0 8 1 1176.73 24.31 0 8 1 1125.26 19.23 0 8 2 1680.50 19.54 0 8 2 1686.44 23.25 0 8 2 1878.48 29.01 0 8 2 1855.70 28.75 0 8 3 659.25 12.27 0 8 3 696.22 14.65 0 8 4 64.35 3.97 0 8 4 70.35 4.67 0 8 5 9.87 1.90 0 8 5 9.60 2.25 0 8 6 133.66 4.43 0 8 6 132.90 5.16 0 9 -7 233.65 6.70 0 9 -6 725.04 15.51 0 9 -6 736.76 15.62 0 9 -5 1496.10 24.63 0 9 -5 1491.53 24.71 0 9 -4 946.38 16.76 0 9 -4 879.47 19.71 0 9 -4 896.91 19.82 0 9 -3 455.82 11.36 0 9 -3 458.94 14.76 0 9 -3 477.26 14.98 0 9 -3 447.52 12.14 0 9 -2 428.75 11.71 0 9 -2 416.66 14.53 0 9 -2 400.47 14.16 0 9 -1 81.73 7.03 0 9 -1 72.88 5.06 0 9 -1 78.55 6.89 0 9 0 138.07 6.44 0 9 0 143.00 8.59 0 9 0 149.41 8.72 0 9 1 922.19 19.02 0 9 1 958.53 19.49 0 9 2 842.68 14.30 0 9 3 207.19 6.82 0 9 4 102.87 4.54 0 10 -4 598.05 12.82 0 10 -4 596.07 12.85 0 10 -3 744.72 15.53 0 10 -3 760.59 15.62 0 10 -2 802.53 16.28 0 10 -2 788.61 16.10 0 10 -1 1366.86 17.09 0 10 -1 1381.72 20.66 0 10 -1 1392.91 20.64 0 10 0 691.89 11.88 1 -9 6 972.89 11.46 1 -9 7 301.46 5.89 1 -8 7 851.96 11.60 1 -8 8 584.65 8.47 1 -7 7 1412.15 16.72 1 -7 8 770.26 11.25 1 -7 9 141.07 4.27 1 -6 7 815.48 13.54 1 -6 8 627.12 11.19 1 -6 9 165.72 5.21 1 -6 10 59.07 2.98 1 -5 0 2538.70 27.29 1 -5 1 1660.69 24.69 1 -5 2 1787.74 28.83 1 -5 3 1811.64 31.01 1 -5 4 1343.21 29.77 1 -5 5 1291.15 30.14 1 -5 7 557.98 11.25 1 -5 8 672.03 11.97 1 -5 9 398.93 8.62 1 -5 10 947.20 11.63 1 -5 11 634.92 8.28 1 -4 -10 765.09 10.53 1 -4 -9 1358.97 17.39 1 -4 -8 1693.51 22.19 1 -4 -4 3629.32 42.46 1 -4 -3 3941.61 36.18 1 -4 -2 4136.06 34.60 1 -4 -1 4349.02 36.32 1 -4 0 1862.91 22.43 1 -4 1 1872.85 19.62 1 -4 1 1868.81 22.69 1 -4 2 2793.91 25.71 1 -4 2 2957.16 32.21 1 -4 3 6706.50 55.06 1 -4 4 8773.63 69.88 1 -4 5 3141.03 44.07 1 -4 7 422.17 9.62 1 -4 8 707.22 12.44 1 -4 9 1539.73 17.26 1 -4 10 1415.06 15.27 1 -4 11 1135.86 11.46 1 -3 -11 127.47 4.20 1 -3 -10 1019.28 15.34 1 -3 -6 74.13 10.48 1 -3 -5 44.36 6.99 1 -3 -4 2172.30 34.06 1 -3 -3 3966.63 39.42 1 -3 -2 2602.28 15.73 1 -3 -2 2548.06 26.04 1 -3 -1 583.67 11.00 1 -3 0 1406.28 16.75 1 -3 1 2024.97 20.87 1 -3 1 2154.14 19.31 1 -3 2 1429.54 17.90 1 -3 2 1584.66 21.24 1 -3 3 3466.48 36.49 1 -3 3 3417.26 34.91 1 -3 4 4170.93 44.64 1 -3 5 2797.80 39.25 1 -3 6 1201.06 27.97 1 -3 6 1012.72 13.40 1 -3 7 601.44 11.00 1 -3 8 1728.33 18.99 1 -3 9 2287.91 21.96 1 -3 10 1061.17 13.75 1 -3 11 908.81 10.68 1 -2 -11 279.85 7.15 1 -2 -6 787.78 26.48 1 -2 -5 337.69 15.33 1 -2 -4 722.28 19.22 1 -2 -3 965.53 19.29 1 -2 -2 12.38 2.54 1 -2 -2 17.18 2.04 1 -2 -1 357.92 7.80 1 -2 0 561.75 9.54 1 -2 0 550.85 9.45 1 -2 1 789.92 11.99 1 -2 1 787.32 11.04 1 -2 2 138.45 5.78 1 -2 2 144.87 6.01 1 -2 3 73.86 5.72 1 -2 3 62.64 4.95 1 -2 4 622.83 16.89 1 -2 5 767.45 19.51 1 -2 5 787.04 13.65 1 -2 6 1395.20 28.09 1 -2 6 1270.89 14.35 1 -2 7 1846.23 18.53 1 -2 8 783.88 12.98 1 -2 9 391.99 9.42 1 -2 10 123.94 5.10 1 -2 11 193.25 5.19 1 -1 -12 1244.19 11.87 1 -1 -11 626.89 11.70 1 -1 -9 412.91 11.35 1 -1 -9 367.77 9.67 1 -1 -8 1023.63 16.57 1 -1 -8 1021.41 16.94 1 -1 -7 1908.16 21.66 1 -1 -7 1972.15 22.08 1 -1 -6 2331.78 48.80 1 -1 -6 2230.22 21.91 1 -1 -6 2312.48 21.82 1 -1 -3 203.46 9.68 1 -1 -2 418.76 10.51 1 -1 -2 377.10 7.39 1 -1 -1 3431.11 23.08 1 -1 0 3617.48 16.72 1 -1 0 3529.91 16.55 1 -1 1 2883.71 20.01 1 -1 1 2766.70 20.92 1 -1 2 154.36 6.84 1 -1 2 148.89 5.94 1 -1 3 81.31 6.26 1 -1 3 72.67 5.06 1 -1 4 17.40 3.50 1 -1 5 175.68 9.12 1 -1 5 163.52 4.66 1 -1 6 1168.35 14.26 1 -1 6 1108.07 12.98 1 -1 7 1308.36 15.51 1 -1 8 146.31 5.87 1 -1 9 48.14 3.80 1 -1 10 10.00 2.24 1 -1 11 80.73 3.56 1 0 -12 1196.50 12.40 1 0 -11 1367.21 17.80 1 0 -11 1226.82 14.42 1 0 -10 444.78 10.53 1 0 -9 631.41 14.33 1 0 -9 608.16 13.41 1 0 -8 2720.28 28.01 1 0 -8 2794.39 28.56 1 0 -7 3936.14 31.78 1 0 -7 3923.02 31.60 1 0 -6 4737.52 31.60 1 0 -6 4694.85 32.37 1 0 -2 3134.50 20.72 1 0 -1 3069.37 20.35 1 0 -1 3018.08 16.37 1 0 0 2126.20 14.22 1 0 0 2059.84 14.16 1 0 1 2175.65 15.15 1 0 1 2304.27 19.53 1 0 2 2533.18 22.71 1 0 2 2906.29 29.23 1 0 3 209.55 8.06 1 0 4 958.57 18.19 1 0 5 1559.57 15.29 1 0 5 1500.29 24.27 1 0 6 726.18 11.21 1 0 6 727.82 12.73 1 0 6 692.76 10.54 1 0 7 940.05 13.22 1 0 7 924.90 14.89 1 0 7 896.89 13.01 1 0 8 587.39 11.33 1 0 9 339.39 8.73 1 0 10 502.99 9.68 1 0 11 167.87 4.79 1 1 -12 462.66 7.67 1 1 -11 1513.66 18.37 1 1 -11 1413.61 17.05 1 1 -10 2227.89 24.03 1 1 -10 2307.01 31.21 1 1 -9 1945.99 25.28 1 1 -9 2069.76 26.16 1 1 -8 2380.79 26.97 1 1 -8 2357.44 26.64 1 1 -7 4105.16 32.78 1 1 -7 4111.46 40.41 1 1 -6 3666.41 35.65 1 1 -6 3636.60 29.79 1 1 -5 3412.14 24.63 1 1 -5 3144.71 25.27 1 1 -2 8141.44 39.09 1 1 -1 1674.71 15.89 1 1 -1 1619.52 11.61 1 1 0 1068.75 11.52 1 1 0 1060.18 10.72 1 1 1 4676.89 21.39 1 1 1 4754.02 25.03 1 1 2 6799.27 32.95 1 1 3 5469.84 34.22 1 1 4 3099.85 29.16 1 1 5 2713.18 19.20 1 1 5 2700.66 30.85 1 1 5 2678.73 21.18 1 1 5 2924.69 26.63 1 1 5 2796.95 24.88 1 1 5 2856.17 27.44 1 1 6 858.25 12.73 1 1 6 857.31 11.94 1 1 6 831.85 20.18 1 1 7 334.07 8.16 1 1 7 366.24 8.68 1 1 7 346.13 9.70 1 1 8 1675.66 19.06 1 1 8 1899.94 23.71 1 1 9 2253.53 21.49 1 1 10 1134.15 13.79 1 1 11 464.82 7.26 1 2 -12 86.78 3.43 1 2 -11 679.92 14.09 1 2 -11 712.31 11.64 1 2 -10 2030.28 23.38 1 2 -10 2136.36 24.00 1 2 -9 1119.22 19.73 1 2 -9 987.14 21.74 1 2 -8 321.47 10.21 1 2 -8 321.70 10.60 1 2 -8 345.01 13.18 1 2 -7 201.35 9.57 1 2 -7 204.32 7.97 1 2 -7 115.87 7.77 1 2 -7 115.49 7.69 1 2 -7 184.70 9.60 1 2 -7 241.40 8.55 1 2 -6 508.08 14.24 1 2 -6 506.92 11.17 1 2 -6 477.40 11.28 1 2 -6 446.01 13.80 1 2 -6 447.65 13.77 1 2 -6 534.75 14.93 1 2 -6 517.53 11.67 1 2 -5 2249.72 21.05 1 2 -5 2616.83 29.89 1 2 -5 2225.06 21.99 1 2 -5 2696.37 28.43 1 2 -5 2627.48 28.01 1 2 -4 5595.07 45.22 1 2 -3 9662.91 43.78 1 2 -2 6319.29 35.61 1 2 -1 1747.52 16.93 1 2 0 2459.80 20.41 1 2 0 2387.41 20.41 1 2 1 3762.49 26.70 1 2 1 3606.20 26.29 1 2 2 8352.85 46.14 1 2 2 8444.48 46.68 1 2 3 8870.37 40.75 1 2 3 8810.93 56.08 1 2 4 2909.04 23.61 1 2 4 2917.83 36.85 1 2 4 2991.07 21.79 1 2 4 2987.94 37.37 1 2 4 2909.42 18.67 1 2 5 2375.17 23.82 1 2 5 2244.53 20.51 1 2 5 2379.21 25.87 1 2 5 2252.32 37.53 1 2 5 2226.02 37.02 1 2 5 2256.93 18.20 1 2 6 1007.07 16.91 1 2 6 914.56 27.70 1 2 6 1017.18 13.46 1 2 6 874.26 26.97 1 2 7 816.06 15.46 1 2 7 745.18 12.26 1 2 8 2125.88 25.87 1 2 8 1930.89 20.09 1 2 9 2501.22 26.29 1 2 9 2362.08 21.11 1 2 10 1456.68 15.95 1 2 10 1653.90 15.30 1 2 11 695.93 8.33 1 3 -12 131.16 4.00 1 3 -11 274.54 9.21 1 3 -11 276.22 7.52 1 3 -10 706.03 12.17 1 3 -10 735.64 13.85 1 3 -9 608.90 12.65 1 3 -9 634.88 18.06 1 3 -8 24.42 3.53 1 3 -8 21.57 4.80 1 3 -7 75.56 5.54 1 3 -7 75.20 6.64 1 3 -7 53.05 6.18 1 3 -7 76.24 6.85 1 3 -7 82.16 5.29 1 3 -7 55.94 6.30 1 3 -6 282.81 9.90 1 3 -6 313.81 11.92 1 3 -6 309.47 9.27 1 3 -6 351.11 12.07 1 3 -6 341.49 11.90 1 3 -6 315.58 12.27 1 3 -5 506.12 11.76 1 3 -5 532.71 15.11 1 3 -5 561.47 15.10 1 3 -5 530.94 11.09 1 3 -5 648.77 16.05 1 3 -5 629.72 15.73 1 3 -4 1595.51 19.98 1 3 -4 1478.85 23.99 1 3 -4 2004.86 26.50 1 3 -4 2156.07 26.47 1 3 -4 2211.21 26.64 1 3 -2 506.73 11.78 1 3 -2 549.28 10.09 1 3 -1 288.66 8.04 1 3 1 1922.06 23.75 1 3 1 1920.96 23.78 1 3 2 815.05 17.04 1 3 2 818.39 17.13 1 3 3 2038.95 29.47 1 3 3 2088.92 30.01 1 3 3 2076.65 15.32 1 3 4 2011.04 20.59 1 3 4 1920.48 32.33 1 3 4 2030.48 33.35 1 3 4 1957.00 16.37 1 3 5 1084.31 28.02 1 3 5 1085.24 27.85 1 3 5 1149.28 13.65 1 3 6 2745.34 29.04 1 3 6 2563.10 21.72 1 3 7 1824.93 23.99 1 3 7 1735.31 18.51 1 3 8 981.81 18.08 1 3 8 943.73 13.62 1 3 9 1146.11 13.85 1 3 9 1094.11 16.03 1 3 10 625.58 9.61 1 3 10 717.50 9.41 1 4 -11 236.67 7.94 1 4 -11 262.44 6.70 1 4 -10 314.79 11.42 1 4 -10 305.96 8.62 1 4 -9 511.48 13.83 1 4 -9 501.45 16.34 1 4 -9 471.47 11.77 1 4 -8 584.53 16.47 1 4 -8 873.15 20.61 1 4 -8 915.22 17.56 1 4 -8 880.74 21.68 1 4 -8 619.41 16.96 1 4 -7 1305.64 20.79 1 4 -7 1122.34 23.05 1 4 -7 1284.49 25.36 1 4 -7 1146.18 23.25 1 4 -7 1337.67 26.47 1 4 -7 1209.64 19.29 1 4 -6 625.96 14.77 1 4 -6 667.19 18.38 1 4 -6 600.33 12.70 1 4 -6 648.09 18.04 1 4 -6 657.66 17.88 1 4 -6 673.64 18.00 1 4 -5 132.22 6.89 1 4 -5 128.37 8.48 1 4 -5 127.95 5.57 1 4 -5 143.16 8.34 1 4 -5 146.36 8.70 1 4 -5 154.67 8.79 1 4 -5 149.19 8.59 1 4 -4 16.41 3.16 1 4 -4 19.83 4.68 1 4 -4 17.44 4.01 1 4 -4 13.29 2.63 1 4 -4 16.60 3.66 1 4 -4 19.94 4.10 1 4 -4 19.43 3.89 1 4 -4 18.23 2.43 1 4 -4 19.64 3.88 1 4 -3 52.67 4.95 1 4 -3 38.80 3.97 1 4 -3 52.66 5.34 1 4 -3 49.52 3.59 1 4 -3 55.69 5.30 1 4 -3 53.53 5.20 1 4 -2 429.28 10.53 1 4 -2 391.60 10.95 1 4 -2 477.55 12.96 1 4 -2 464.29 9.46 1 4 -2 534.88 14.15 1 4 -2 505.58 13.79 1 4 -1 926.75 16.15 1 4 1 201.14 6.31 1 4 1 225.90 6.60 1 4 2 60.97 5.99 1 4 2 56.91 4.99 1 4 2 57.59 5.87 1 4 2 64.42 4.24 1 4 2 52.32 2.89 1 4 2 51.12 3.89 1 4 3 57.11 4.89 1 4 3 39.27 5.84 1 4 3 51.54 4.24 1 4 3 38.97 5.84 1 4 3 34.94 2.69 1 4 4 441.87 11.92 1 4 4 443.95 18.67 1 4 4 449.37 18.78 1 4 4 416.95 8.30 1 4 5 1089.80 18.58 1 4 5 1115.77 19.81 1 4 6 1330.54 20.84 1 4 6 1319.50 16.23 1 4 7 655.44 15.33 1 4 7 616.22 11.26 1 4 8 42.28 3.98 1 4 8 42.56 3.36 1 4 9 9.61 1.97 1 4 9 8.55 1.98 1 4 9 8.39 2.54 1 5 -11 153.43 5.77 1 5 -11 168.44 4.77 1 5 -10 81.89 6.08 1 5 -10 83.13 6.00 1 5 -10 87.19 4.42 1 5 -9 913.64 18.08 1 5 -9 899.14 14.85 1 5 -8 1897.22 30.06 1 5 -8 1744.27 21.41 1 5 -8 1955.16 32.19 1 5 -8 1482.23 26.89 1 5 -8 1526.53 27.43 1 5 -7 1971.89 26.84 1 5 -7 1803.74 22.05 1 5 -7 1727.41 29.90 1 5 -7 1885.98 31.88 1 5 -7 2007.33 32.68 1 5 -7 1735.79 29.94 1 5 -6 2510.10 37.52 1 5 -6 2183.91 34.45 1 5 -6 2311.28 29.62 1 5 -6 2317.04 34.82 1 5 -6 2216.89 24.06 1 5 -6 2440.90 36.87 1 5 -5 531.60 16.99 1 5 -5 594.84 16.98 1 5 -5 595.36 17.50 1 5 -5 623.34 18.32 1 5 -5 583.11 11.40 1 5 -5 620.13 18.22 1 5 -5 550.63 14.24 1 5 -4 105.82 8.67 1 5 -4 128.54 8.60 1 5 -4 130.94 7.12 1 5 -4 139.69 7.99 1 5 -4 158.32 9.09 1 5 -4 131.72 7.01 1 5 -4 141.45 9.01 1 5 -4 135.26 8.79 1 5 -3 565.76 13.38 1 5 -3 556.21 16.34 1 5 -3 591.34 16.39 1 5 -3 623.58 14.38 1 5 -3 635.66 16.78 1 5 -3 608.27 12.80 1 5 -3 744.39 19.52 1 5 -3 695.66 18.78 1 5 -2 2584.85 27.55 1 5 -2 2455.47 31.59 1 5 -2 2816.72 32.94 1 5 -2 2419.12 30.64 1 5 -2 2745.86 25.37 1 5 -2 2763.76 35.54 1 5 -2 2775.18 35.50 1 5 -1 4533.79 26.14 1 5 -1 4624.43 32.13 1 5 -1 4579.19 44.99 1 5 -1 4604.34 45.01 1 5 -1 4560.69 35.03 1 5 0 1291.21 14.50 1 5 0 1328.80 17.38 1 5 0 1371.73 24.44 1 5 0 1349.08 24.16 1 5 1 416.78 9.48 1 5 1 428.80 10.51 1 5 1 441.16 10.37 1 5 1 452.09 14.09 1 5 1 454.31 14.14 1 5 2 145.19 6.22 1 5 2 146.91 6.84 1 5 2 149.63 6.54 1 5 3 42.12 3.89 1 5 3 49.30 4.59 1 5 3 45.75 4.05 1 5 4 414.75 11.58 1 5 4 441.06 11.84 1 5 4 453.60 12.65 1 5 4 391.65 8.85 1 5 5 565.78 13.59 1 5 5 579.77 13.76 1 5 6 593.16 13.87 1 5 6 608.19 14.35 1 5 6 540.86 14.45 1 5 6 542.17 10.56 1 5 7 331.77 9.76 1 5 7 334.14 8.10 1 5 8 15.94 2.42 1 5 8 5.42 2.27 1 5 9 26.75 2.25 1 6 -10 665.55 13.38 1 6 -10 653.43 9.45 1 6 -9 1595.47 24.07 1 6 -9 1456.37 21.01 1 6 -9 1558.39 24.59 1 6 -9 1465.84 16.32 1 6 -8 1905.15 30.17 1 6 -8 1970.75 28.59 1 6 -8 1459.56 26.33 1 6 -8 1806.73 20.15 1 6 -8 1522.15 26.95 1 6 -7 1584.38 28.55 1 6 -7 1515.65 28.43 1 6 -7 1506.64 18.70 1 6 -7 1536.14 28.64 1 6 -6 2186.34 29.20 1 6 -6 2182.20 34.99 1 6 -6 2279.66 37.37 1 6 -6 2247.62 37.26 1 6 -6 2134.08 33.54 1 6 -5 2263.54 29.81 1 6 -5 2195.93 34.96 1 6 -5 2254.71 34.29 1 6 -5 2406.46 37.68 1 6 -5 2421.29 37.58 1 6 -4 1061.23 23.55 1 6 -4 1103.60 20.15 1 6 -4 1105.13 20.45 1 6 -4 1052.25 21.60 1 6 -4 1100.80 23.45 1 6 -4 1163.81 26.26 1 6 -4 1156.12 26.03 1 6 -3 1232.92 24.23 1 6 -3 1245.89 21.08 1 6 -3 1245.61 23.76 1 6 -3 1259.87 19.97 1 6 -3 1371.85 28.87 1 6 -3 1385.21 28.76 1 6 -2 2575.29 28.88 1 6 -2 2631.80 27.10 1 6 -2 2658.57 38.29 1 6 -2 2618.07 37.80 1 6 -1 1883.35 25.00 1 6 -1 1859.52 22.71 1 6 -1 1815.73 30.93 1 6 -1 1860.55 23.98 1 6 -1 1835.56 31.08 1 6 0 1151.53 15.41 1 6 0 1164.82 18.10 1 6 0 1122.43 24.30 1 6 0 1115.54 24.22 1 6 1 1212.06 18.64 1 6 1 1219.17 24.65 1 6 1 1230.78 24.80 1 6 2 2136.36 22.84 1 6 2 2129.50 23.22 1 6 3 1724.47 21.71 1 6 3 1774.12 23.53 1 6 4 676.79 14.34 1 6 4 698.06 14.68 1 6 4 684.76 15.10 1 6 5 675.72 14.28 1 6 5 681.58 15.02 1 6 6 525.34 11.65 1 6 6 501.65 12.20 1 6 7 657.17 11.36 1 6 7 538.05 11.45 1 6 8 723.73 10.03 1 7 -9 557.24 11.17 1 7 -9 560.61 12.93 1 7 -8 433.82 11.38 1 7 -8 523.56 13.19 1 7 -8 397.28 12.73 1 7 -8 525.82 14.49 1 7 -8 393.40 12.61 1 7 -7 471.65 14.14 1 7 -7 454.99 15.15 1 7 -7 478.55 14.71 1 7 -7 459.98 15.25 1 7 -7 462.29 13.23 1 7 -6 1382.49 28.30 1 7 -6 1261.41 24.37 1 7 -6 1371.33 28.24 1 7 -6 1248.17 24.32 1 7 -5 2645.37 36.62 1 7 -5 2740.37 36.55 1 7 -5 2964.66 43.73 1 7 -5 2925.32 43.41 1 7 -4 3307.16 39.93 1 7 -4 3183.93 35.05 1 7 -4 3245.35 38.79 1 7 -4 3482.84 46.68 1 7 -4 3477.26 46.46 1 7 -3 2369.41 29.19 1 7 -3 2400.95 38.25 1 7 -2 722.15 15.44 1 7 -2 767.09 22.42 1 7 -2 775.23 22.40 1 7 -1 922.23 17.23 1 7 -1 993.17 24.72 1 7 -1 976.99 24.34 1 7 0 1634.46 17.90 1 7 0 1599.12 22.39 1 7 0 1602.78 30.11 1 7 0 1611.96 30.01 1 7 1 2704.85 24.63 1 7 1 2777.70 29.57 1 7 1 2866.06 39.05 1 7 1 2925.08 39.22 1 7 2 4707.75 34.51 1 7 2 4469.03 37.69 1 7 3 2486.42 25.03 1 7 3 2560.29 27.80 1 7 4 747.71 13.45 1 7 4 779.39 15.19 1 7 5 240.93 7.45 1 7 5 242.01 8.17 1 7 6 284.98 7.42 1 7 6 250.32 7.44 1 7 7 971.99 11.31 1 8 -8 23.12 2.60 1 8 -8 20.61 3.41 1 8 -8 13.07 3.00 1 8 -8 12.78 3.06 1 8 -7 230.95 9.70 1 8 -7 249.88 8.61 1 8 -7 250.40 9.30 1 8 -7 236.68 9.82 1 8 -6 454.27 12.93 1 8 -6 454.26 13.06 1 8 -6 482.30 14.95 1 8 -6 481.23 14.90 1 8 -5 1852.71 31.94 1 8 -5 1859.96 31.97 1 8 -4 2474.95 37.63 1 8 -4 2506.90 37.63 1 8 -3 1060.69 19.41 1 8 -3 1100.53 20.43 1 8 -3 1140.65 25.56 1 8 -3 1090.22 24.93 1 8 -2 456.83 12.58 1 8 -2 450.14 16.21 1 8 -2 469.00 16.45 1 8 -1 380.39 11.11 1 8 -1 395.14 15.03 1 8 -1 407.44 15.22 1 8 0 1342.78 20.29 1 8 0 1379.88 26.86 1 8 0 1397.66 26.82 1 8 1 1968.40 19.58 1 8 1 1940.43 24.01 1 8 2 1431.21 16.68 1 8 2 1468.78 20.25 1 8 3 1507.37 16.75 1 8 3 1579.68 19.97 1 8 4 655.53 10.60 1 8 4 688.57 12.44 1 8 5 530.21 8.63 1 9 -6 159.07 5.64 1 9 -6 159.92 7.50 1 9 -6 161.30 7.54 1 9 -5 166.54 6.12 1 9 -5 178.05 8.34 1 9 -5 174.58 8.28 1 9 -4 94.56 4.88 1 9 -4 110.23 7.45 1 9 -4 101.21 7.16 1 9 -3 242.97 10.89 1 9 -3 243.63 10.89 1 9 -2 341.94 10.08 1 9 -2 335.14 12.72 1 9 -2 341.18 12.76 1 9 -1 474.03 11.44 1 9 -1 443.24 14.31 1 9 -1 428.13 13.95 1 9 0 497.26 11.19 1 9 1 256.69 7.81 1 9 2 204.38 6.58 2 -9 1 762.93 12.99 2 -9 6 528.95 8.43 2 -9 7 459.50 7.16 2 -8 2 1829.94 20.72 2 -8 7 2069.45 17.53 2 -8 8 1382.46 12.63 2 -7 2 1880.71 20.55 2 -7 7 1800.68 18.69 2 -7 8 1219.18 13.63 2 -7 9 607.96 8.21 2 -6 -1 477.21 8.94 2 -6 3 238.67 7.30 2 -6 7 56.30 4.08 2 -6 8 417.52 8.94 2 -6 9 637.16 9.42 2 -6 10 628.58 8.17 2 -5 -3 3342.79 42.53 2 -5 -2 2253.72 35.40 2 -5 -1 543.68 15.57 2 -5 0 226.97 9.55 2 -5 0 226.00 5.60 2 -5 0 240.78 10.35 2 -5 1 62.34 5.69 2 -5 1 70.27 6.13 2 -5 2 514.71 16.22 2 -5 3 1591.59 16.60 2 -5 3 1633.71 31.06 2 -5 4 1978.84 18.98 2 -5 4 1718.60 34.17 2 -5 7 33.61 3.47 2 -5 8 80.25 4.52 2 -5 9 338.21 7.65 2 -5 10 575.01 8.67 2 -4 -10 2128.88 18.38 2 -4 -9 2469.46 23.87 2 -4 -8 1790.81 22.63 2 -4 -7 1432.28 21.14 2 -4 -6 379.18 10.64 2 -4 -5 457.42 19.33 2 -4 -5 586.32 12.15 2 -4 -4 3840.00 26.79 2 -4 -4 2953.74 41.27 2 -4 -3 5074.18 47.18 2 -4 -2 3120.81 34.92 2 -4 -1 1339.35 23.04 2 -4 0 2119.09 27.03 2 -4 1 1359.75 21.84 2 -4 1 1428.29 21.72 2 -4 2 696.70 15.82 2 -4 2 660.76 15.99 2 -4 3 4126.11 24.63 2 -4 3 4154.28 43.64 2 -4 3 4234.91 44.86 2 -4 4 3354.84 23.56 2 -4 4 3271.69 44.41 2 -4 4 3275.29 44.02 2 -4 5 707.81 23.24 2 -4 5 785.10 14.66 2 -4 6 544.90 10.53 2 -4 7 262.02 7.75 2 -4 8 448.38 9.89 2 -4 9 605.79 10.75 2 -4 10 442.15 8.16 2 -4 11 442.33 6.63 2 -3 -11 754.52 10.34 2 -3 -10 1187.95 16.27 2 -3 -9 1100.74 18.65 2 -3 -8 2162.81 27.42 2 -3 -6 1827.00 43.11 2 -3 -5 3643.33 53.52 2 -3 -4 3443.06 46.05 2 -3 -3 4229.68 44.44 2 -3 -2 2545.30 9.16 2 -3 -2 3593.98 32.61 2 -3 -1 3639.24 32.44 2 -3 0 4358.77 36.21 2 -3 1 4125.40 35.43 2 -3 1 4254.96 34.77 2 -3 2 2560.79 28.38 2 -3 2 2513.45 28.71 2 -3 3 1669.36 26.88 2 -3 3 1567.22 25.32 2 -3 4 1408.73 19.84 2 -3 4 1404.06 14.36 2 -3 4 1453.29 28.58 2 -3 4 1467.58 27.27 2 -3 5 2102.79 36.87 2 -3 5 2079.41 24.54 2 -3 5 1968.57 18.36 2 -3 5 1986.58 17.78 2 -3 6 3268.92 31.06 2 -3 6 3038.25 23.53 2 -3 7 2521.35 22.40 2 -3 8 1281.16 16.25 2 -3 9 835.49 13.07 2 -3 10 421.32 8.29 2 -3 11 303.40 5.87 2 -2 -11 133.61 5.05 2 -2 -10 54.02 4.36 2 -2 -9 266.97 10.01 2 -2 -7 1444.72 17.87 2 -2 -6 2822.92 52.94 2 -2 -6 3197.57 25.21 2 -2 -5 2210.98 41.16 2 -2 -4 174.84 10.55 2 -2 -3 97.15 6.95 2 -2 -2 5300.71 29.99 2 -2 -2 5149.86 41.55 2 -2 -1 4815.55 20.72 2 -2 -1 4087.68 31.58 2 -2 0 1699.04 16.81 2 -2 0 1717.91 16.94 2 -2 1 8348.77 41.08 2 -2 1 8333.72 41.85 2 -2 1 8320.66 46.74 2 -2 2 6724.55 42.31 2 -2 2 5819.64 41.99 2 -2 3 215.45 10.11 2 -2 3 209.96 9.06 2 -2 4 1018.09 24.41 2 -2 4 1076.80 11.53 2 -2 4 1002.35 21.51 2 -2 5 2971.93 29.98 2 -2 5 2971.46 22.13 2 -2 5 2965.04 40.76 2 -2 5 2941.05 20.66 2 -2 6 4744.86 54.70 2 -2 6 4832.15 29.70 2 -2 6 4786.56 28.23 2 -2 7 3033.30 24.07 2 -2 7 3194.03 24.48 2 -2 8 1122.84 15.56 2 -2 9 591.52 10.98 2 -2 10 274.71 6.87 2 -2 11 462.44 7.28 2 -1 -12 385.32 6.74 2 -1 -11 49.83 3.61 2 -1 -10 24.36 3.57 2 -1 -10 16.53 2.63 2 -1 -9 16.00 2.83 2 -1 -8 74.38 5.87 2 -1 -8 93.15 5.41 2 -1 -7 1058.89 19.77 2 -1 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688.25 13.00 2 0 -6 744.92 13.76 2 0 -5 195.05 13.25 2 0 -5 204.16 6.62 2 0 -4 2619.48 40.55 2 0 -3 2548.83 32.61 2 0 -2 321.73 9.34 2 0 -2 303.23 9.58 2 0 -1 387.74 8.17 2 0 -1 412.26 8.75 2 0 0 20.89 2.23 2 0 0 22.41 2.58 2 0 0 24.92 2.26 2 0 1 318.61 7.27 2 0 1 304.83 8.78 2 0 2 868.59 17.91 2 0 2 850.96 14.07 2 0 3 718.81 19.31 2 0 3 764.37 15.58 2 0 4 665.49 13.50 2 0 4 680.56 16.50 2 0 4 652.63 10.07 2 0 5 156.03 7.39 2 0 5 150.95 5.50 2 0 5 166.07 7.65 2 0 5 154.33 8.59 2 0 5 151.86 6.16 2 0 5 162.38 5.08 2 0 6 6.59 2.74 2 0 6 12.98 4.29 2 0 6 9.93 2.51 2 0 6 10.88 3.21 2 0 7 77.73 4.57 2 0 7 75.15 4.93 2 0 7 76.02 4.28 2 0 8 383.63 9.09 2 0 8 383.47 8.86 2 0 8 383.76 9.95 2 0 9 1133.28 14.99 2 0 10 866.17 11.51 2 0 11 197.37 4.61 2 1 -12 575.95 8.17 2 1 -11 1539.78 17.46 2 1 -11 1541.39 17.57 2 1 -10 2883.05 29.07 2 1 -10 2928.29 29.17 2 1 -9 2778.58 37.87 2 1 -9 2798.44 30.56 2 1 -8 1159.78 23.58 2 1 -8 1131.10 19.09 2 1 -7 262.44 9.18 2 1 -7 242.78 11.73 2 1 -6 431.94 23.29 2 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2989.23 29.38 2 2 -9 3044.60 31.41 2 2 -8 1429.88 20.57 2 2 -8 1412.84 27.68 2 2 -7 425.27 12.72 2 2 -7 334.09 12.77 2 2 -7 425.66 15.12 2 2 -7 368.47 10.88 2 2 -7 332.20 12.93 2 2 -6 2780.71 32.56 2 2 -6 2264.33 53.80 2 2 -6 3146.44 38.00 2 2 -6 3041.77 36.44 2 2 -6 2977.21 35.97 2 2 -6 2572.65 27.23 2 2 -5 6204.14 47.48 2 2 -5 4540.91 40.42 2 2 -5 5371.86 46.22 2 2 -5 4896.50 34.45 2 2 -5 6120.53 47.18 2 2 -4 3704.47 35.00 2 2 -4 3668.79 35.02 2 2 -3 5736.37 50.43 2 2 -3 6305.06 52.03 2 2 -2 5728.80 35.68 2 2 -2 5751.94 33.51 2 2 -1 2237.21 18.11 2 2 -1 2004.02 11.67 2 2 0 3143.36 27.73 2 2 1 3188.35 26.42 2 2 1 3300.18 26.67 2 2 2 2687.02 26.91 2 2 2 2688.03 27.04 2 2 3 3267.88 22.70 2 2 3 3250.73 23.51 2 2 3 3244.05 22.67 2 2 3 3392.71 33.22 2 2 3 3176.64 34.24 2 2 3 3086.45 33.85 2 2 4 2337.23 20.58 2 2 4 2366.34 29.42 2 2 4 2328.21 34.25 2 2 4 2342.73 21.72 2 2 4 2281.54 33.95 2 2 4 2353.39 17.51 2 2 4 2343.62 25.10 2 2 5 1141.32 18.69 2 2 5 1165.38 15.55 2 2 5 1189.39 20.13 2 2 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3 -3 455.92 11.23 2 3 -3 505.13 13.59 2 3 -3 547.37 14.17 2 3 -3 690.64 16.70 2 3 -3 662.71 16.31 2 3 -2 3950.75 36.78 2 3 -2 3838.99 21.93 2 3 -1 5575.29 43.64 2 3 1 2431.06 28.62 2 3 1 2570.41 29.90 2 3 2 398.39 12.85 2 3 2 416.32 12.41 2 3 2 367.65 7.64 2 3 2 409.77 12.94 2 3 3 3205.68 34.94 2 3 3 3030.07 23.64 2 3 3 3191.06 23.49 2 3 3 3470.02 41.37 2 3 3 3459.46 41.51 2 3 3 3114.73 19.41 2 3 4 2897.78 32.45 2 3 4 2800.53 23.42 2 3 4 2588.73 40.29 2 3 4 2612.35 40.47 2 3 4 2737.73 19.83 2 3 4 2730.00 24.80 2 3 5 2414.04 28.56 2 3 5 2339.66 24.89 2 3 5 2379.99 19.79 2 3 6 4559.53 37.89 2 3 6 4300.93 27.97 2 3 7 2410.20 20.96 2 3 7 2443.60 26.85 2 3 8 476.76 12.21 2 3 8 500.55 9.42 2 3 9 137.42 5.45 2 3 9 158.15 4.92 2 4 -11 4.30 2.08 2 4 -11 6.11 2.12 2 4 -11 5.39 1.57 2 4 -10 8.45 3.11 2 4 -10 10.60 2.24 2 4 -9 93.49 7.79 2 4 -9 79.36 5.89 2 4 -9 85.99 7.70 2 4 -9 79.36 5.19 2 4 -8 1483.58 25.65 2 4 -8 1531.26 30.07 2 4 -8 1107.69 23.64 2 4 -8 1346.98 20.18 2 4 -8 1120.01 23.93 2 4 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3 596.60 11.28 2 4 3 650.57 21.67 2 4 3 643.27 10.14 2 4 4 1655.73 23.75 2 4 4 1678.88 20.45 2 4 4 1726.30 17.25 2 4 5 2582.80 29.03 2 4 5 2601.89 30.12 2 4 5 2553.06 21.60 2 4 6 2021.69 27.09 2 4 6 2014.69 25.10 2 4 7 1095.76 18.73 2 4 7 1103.98 14.24 2 4 8 446.06 10.34 2 4 8 483.02 8.66 2 4 9 409.04 7.90 2 5 -11 9.77 2.05 2 5 -11 13.83 2.18 2 5 -10 47.53 4.21 2 5 -10 44.13 3.49 2 5 -9 345.84 12.22 2 5 -9 359.12 11.04 2 5 -9 366.00 13.37 2 5 -9 339.76 8.83 2 5 -8 285.62 12.48 2 5 -8 277.34 11.43 2 5 -8 216.39 11.13 2 5 -8 221.01 11.23 2 5 -8 294.02 13.24 2 5 -8 249.80 8.23 2 5 -7 619.78 18.22 2 5 -7 654.75 19.39 2 5 -7 679.04 20.34 2 5 -7 624.13 12.90 2 5 -7 678.58 20.34 2 5 -6 469.52 15.97 2 5 -6 516.90 17.13 2 5 -6 548.67 18.52 2 5 -6 501.31 11.30 2 5 -6 556.49 18.60 2 5 -5 54.82 6.39 2 5 -5 54.57 6.44 2 5 -5 72.48 7.97 2 5 -5 54.72 3.87 2 5 -5 65.03 7.61 2 5 -4 180.29 8.78 2 5 -4 143.73 8.95 2 5 -4 132.89 8.91 2 5 -4 148.28 7.45 2 5 -4 184.97 11.34 2 5 -4 182.79 11.18 2 5 -3 163.15 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731.81 21.84 2 6 -5 970.95 22.48 2 6 -5 956.23 22.46 2 6 -5 1230.19 29.75 2 6 -5 1193.62 29.29 2 6 -4 1391.19 26.20 2 6 -4 1289.79 24.66 2 6 -4 1424.20 22.48 2 6 -4 1636.82 33.51 2 6 -4 1626.46 33.31 2 6 -3 1055.34 21.59 2 6 -3 1146.48 19.56 2 6 -3 1129.18 26.78 2 6 -3 1069.22 25.91 2 6 -2 75.94 5.95 2 6 -2 54.09 4.44 2 6 -2 62.28 7.16 2 6 -2 63.87 7.25 2 6 -1 59.23 4.68 2 6 -1 37.99 3.84 2 6 -1 47.44 6.57 2 6 -1 50.07 6.65 2 6 0 433.84 15.98 2 6 0 439.35 15.93 2 6 1 565.14 10.94 2 6 1 686.82 14.24 2 6 2 1220.10 17.04 2 6 2 1180.31 17.93 2 6 3 834.70 14.97 2 6 3 822.38 15.02 2 6 4 124.87 6.19 2 6 4 129.85 6.33 2 6 5 23.03 3.10 2 6 5 31.25 4.01 2 6 5 26.03 3.62 2 6 6 24.47 2.66 2 6 7 303.70 6.74 2 7 -9 386.71 8.33 2 7 -8 343.61 9.53 2 7 -8 364.11 11.02 2 7 -8 291.05 10.56 2 7 -8 299.61 10.69 2 7 -7 327.70 10.90 2 7 -7 335.49 13.45 2 7 -7 363.07 12.49 2 7 -7 343.37 13.63 2 7 -6 999.74 20.91 2 7 -6 1040.46 21.46 2 7 -6 1135.36 25.40 2 7 -6 1114.22 25.13 2 7 -5 2769.37 41.45 2 7 -5 2760.75 41.15 2 7 -4 4162.44 52.30 2 7 -4 4300.30 53.06 2 7 -3 1602.52 24.64 2 7 -3 1670.50 24.32 2 7 -3 1841.46 34.56 2 7 -3 1836.60 34.35 2 7 -2 244.16 8.98 2 7 -2 259.82 9.49 2 7 -2 272.44 13.52 2 7 -1 751.77 21.46 2 7 -1 725.42 20.88 2 7 0 1395.32 27.75 2 7 0 1411.56 27.76 2 7 1 1299.87 16.21 2 7 1 1353.83 20.13 2 7 2 1372.84 17.59 2 7 2 1445.33 20.18 2 7 3 1099.94 15.36 2 7 3 1269.32 18.63 2 7 4 273.13 7.50 2 7 5 53.83 3.37 2 7 6 162.54 4.87 2 8 -8 743.28 10.66 2 8 -7 647.03 14.65 2 8 -7 675.09 12.10 2 8 -7 664.73 14.96 2 8 -6 882.61 19.13 2 8 -6 891.78 19.24 2 8 -5 1458.50 26.12 2 8 -5 1471.43 26.18 2 8 -4 854.08 21.48 2 8 -4 852.71 21.37 2 8 -3 1321.52 27.61 2 8 -3 1325.22 27.56 2 8 -2 1778.31 23.67 2 8 -2 1706.93 30.89 2 8 -1 1071.54 24.15 2 8 -1 992.39 23.07 2 8 0 1753.96 21.93 2 8 3 918.23 11.50 2 9 -5 100.70 6.16 2 9 -5 101.94 6.22 2 9 -4 140.77 7.66 2 9 -4 135.14 7.66 2 9 -3 986.81 18.49 2 9 -3 998.48 18.66 2 9 -2 1946.49 25.66 2 9 -2 1918.63 25.54 3 -10 -2 717.74 10.70 3 -10 -1 349.00 7.86 3 -10 0 100.24 4.82 3 -9 0 577.56 12.06 3 -9 1 1491.72 18.69 3 -9 6 300.86 6.29 3 -8 -6 1573.49 15.25 3 -8 -5 1596.66 16.91 3 -8 -4 1341.15 15.95 3 -8 1 2638.81 26.80 3 -8 2 1741.54 21.43 3 -8 3 692.50 12.98 3 -8 6 805.19 11.94 3 -8 7 1042.00 12.03 3 -7 -3 1231.10 17.22 3 -7 -2 1198.34 16.37 3 -7 -1 1741.46 18.64 3 -7 2 1672.97 20.93 3 -7 3 1018.59 16.08 3 -7 4 1473.45 18.75 3 -7 6 991.48 14.44 3 -7 7 473.55 9.31 3 -7 8 546.43 8.73 3 -6 -1 1056.95 14.54 3 -6 0 407.82 16.50 3 -6 0 427.43 8.72 3 -6 1 384.61 16.32 3 -6 1 397.35 8.41 3 -6 2 1244.48 17.06 3 -6 2 1232.81 14.85 3 -6 3 2327.68 23.33 3 -6 4 2915.53 26.20 3 -6 6 623.57 11.92 3 -6 7 307.95 8.13 3 -6 8 469.63 8.96 3 -6 9 1038.93 11.52 3 -5 -8 491.65 9.83 3 -5 -7 14.69 2.62 3 -5 -6 5.77 2.18 3 -5 -5 21.70 2.68 3 -5 -4 364.66 17.84 3 -5 -3 1278.75 29.83 3 -5 -2 1247.50 30.22 3 -5 -1 612.95 10.20 3 -5 -1 612.85 18.71 3 -5 0 40.07 5.90 3 -5 0 33.41 5.82 3 -5 0 34.57 2.69 3 -5 1 32.38 5.03 3 -5 1 32.31 6.06 3 -5 1 34.21 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3 2 -3 308.64 11.55 3 2 -2 1189.54 22.36 3 2 -2 1200.00 15.71 3 2 -1 2405.64 31.06 3 2 -1 2373.73 16.33 3 2 0 739.57 16.91 3 2 1 253.08 8.72 3 2 1 234.70 11.37 3 2 2 79.33 4.00 3 2 2 82.39 6.03 3 2 2 82.35 3.91 3 2 2 88.14 5.57 3 2 2 89.28 5.58 3 2 3 29.13 2.81 3 2 3 26.38 3.57 3 2 3 29.09 2.97 3 2 3 23.38 4.55 3 2 4 173.85 8.23 3 2 4 178.31 6.44 3 2 4 168.70 9.44 3 2 4 175.92 6.61 3 2 4 198.47 5.53 3 2 5 850.04 13.94 3 2 5 847.99 18.33 3 2 5 853.56 15.46 3 2 5 870.38 11.89 3 2 6 1195.76 16.60 3 2 6 1234.63 20.62 3 2 6 1188.89 19.18 3 2 6 1234.55 14.61 3 2 7 540.84 12.67 3 2 7 553.09 9.99 3 2 8 27.02 3.44 3 2 8 24.94 2.71 3 2 9 10.07 2.19 3 2 9 9.37 2.11 3 3 -11 323.32 8.75 3 3 -11 326.03 8.69 3 3 -10 525.10 14.02 3 3 -10 535.82 14.32 3 3 -10 573.71 12.02 3 3 -9 836.15 19.96 3 3 -9 819.21 15.80 3 3 -8 3141.19 34.18 3 3 -8 3224.81 32.13 3 3 -7 4202.35 49.29 3 3 -7 4245.84 42.76 3 3 -7 4237.45 36.69 3 3 -6 1426.71 27.56 3 3 -6 1546.40 27.52 3 3 -6 1742.35 31.23 3 3 -6 2109.43 36.05 3 3 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7.34 3 3 8 171.21 6.73 3 3 8 177.16 5.57 3 3 9 30.86 2.50 3 4 -11 269.05 7.14 3 4 -11 257.37 7.09 3 4 -10 232.27 8.73 3 4 -10 230.39 8.88 3 4 -9 601.65 15.84 3 4 -9 571.74 13.08 3 4 -9 604.60 12.58 3 4 -8 1763.41 29.43 3 4 -8 1719.67 25.90 3 4 -8 1702.63 21.95 3 4 -7 2433.10 34.76 3 4 -7 2570.04 36.08 3 4 -7 2868.04 41.33 3 4 -7 2661.71 40.10 3 4 -7 2452.12 26.31 3 4 -7 2758.71 41.10 3 4 -6 1543.16 27.45 3 4 -6 1401.96 27.57 3 4 -6 1517.09 29.71 3 4 -6 1923.20 35.86 3 4 -6 1526.94 19.94 3 4 -6 1810.47 35.04 3 4 -5 968.81 20.13 3 4 -5 628.49 18.23 3 4 -5 720.97 20.38 3 4 -5 1027.11 26.46 3 4 -5 946.28 15.22 3 4 -5 1028.12 26.55 3 4 -4 2474.70 28.58 3 4 -4 2501.43 39.26 3 4 -4 2462.63 38.68 3 4 -3 3035.84 27.68 3 4 -3 3113.80 47.28 3 4 -3 3293.71 37.08 3 4 -3 3137.27 28.15 3 4 -3 2899.54 42.44 3 4 -3 2925.07 42.26 3 4 -2 2159.13 36.79 3 4 -2 2382.72 27.74 3 4 -2 1563.32 31.01 3 4 -2 1603.39 31.09 3 4 -1 1671.20 30.03 3 4 -1 1710.82 30.15 3 4 0 3585.78 28.77 3 4 0 3552.94 37.18 3 4 1 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20.38 2.45 4 2 -10 20.62 3.37 4 2 -9 176.13 9.07 4 2 -9 173.06 6.05 4 2 -9 163.57 8.90 4 2 -8 388.74 14.23 4 2 -8 516.43 12.93 4 2 -8 474.30 10.09 4 2 -8 405.88 14.48 4 2 -8 400.71 12.11 4 2 -7 731.21 19.16 4 2 -7 1169.17 20.37 4 2 -7 1288.07 16.31 4 2 -7 740.65 19.41 4 2 -7 937.91 17.91 4 2 -6 452.64 14.48 4 2 -6 465.46 14.79 4 2 -5 20.74 3.85 4 2 -5 15.72 3.28 4 2 -5 23.95 2.41 4 2 -5 23.35 4.01 4 2 -5 25.48 5.84 4 2 -5 21.53 5.64 4 2 -4 88.09 5.66 4 2 -4 89.88 8.80 4 2 -4 84.31 5.74 4 2 -4 87.48 3.77 4 2 -4 93.29 5.81 4 2 -4 67.02 7.65 4 2 -4 72.75 7.90 4 2 -3 217.47 7.64 4 2 -3 226.74 13.01 4 2 -3 208.77 8.12 4 2 -3 209.56 5.40 4 2 -3 223.92 7.80 4 2 -3 162.91 10.17 4 2 -3 156.92 9.95 4 2 -3 217.36 7.07 4 2 -2 472.54 10.00 4 2 -2 480.33 17.17 4 2 -2 478.09 11.55 4 2 -2 457.13 7.65 4 2 -2 482.94 10.10 4 2 -2 409.70 13.41 4 2 -2 399.89 13.32 4 2 -2 466.71 9.61 4 2 -1 1147.76 14.23 4 2 -1 1079.77 22.41 4 2 -1 1195.44 18.19 4 2 -1 1128.44 14.14 4 2 -1 1137.51 14.51 4 2 0 2457.79 26.68 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243.59 7.68 4 3 -3 534.52 11.79 4 3 -3 572.89 21.90 4 3 -3 538.49 13.88 4 3 -3 539.21 11.84 4 3 -3 371.80 15.71 4 3 -3 367.29 15.69 4 3 -2 452.78 9.98 4 3 -2 427.40 17.72 4 3 -2 443.34 11.65 4 3 -2 451.81 12.07 4 3 -2 410.79 9.43 4 3 -2 283.98 13.57 4 3 -2 292.08 13.68 4 3 -1 810.63 15.25 4 3 -1 848.26 16.72 4 3 0 1358.78 18.41 4 3 0 1346.45 21.90 4 3 1 74.32 4.59 4 3 1 84.01 7.15 4 3 1 95.63 4.47 4 3 2 185.27 10.11 4 3 2 196.58 6.42 4 3 2 178.93 6.64 4 3 3 504.80 16.46 4 3 3 526.33 10.58 4 3 3 510.31 11.46 4 3 4 149.85 9.19 4 3 4 147.02 6.11 4 3 4 157.77 6.91 4 3 5 129.41 7.78 4 3 5 141.97 6.68 4 3 6 172.51 7.31 4 3 7 189.27 6.94 4 3 7 206.54 6.86 4 3 8 202.74 5.88 4 4 -10 1017.73 15.24 4 4 -10 1095.32 15.93 4 4 -9 1029.10 17.89 4 4 -9 1081.62 16.69 4 4 -9 1053.19 18.22 4 4 -8 991.63 18.47 4 4 -8 956.97 19.20 4 4 -7 794.63 17.87 4 4 -7 833.71 18.68 4 4 -7 769.81 17.91 4 4 -6 1256.18 21.91 4 4 -6 1297.89 22.35 4 4 -6 1478.96 32.17 4 4 -6 1540.55 32.93 4 4 -5 2543.39 29.37 4 4 -5 2549.43 29.56 4 4 -5 2806.65 43.69 4 4 -5 2765.48 43.38 4 4 -4 2430.75 26.72 4 4 -4 1882.15 28.16 4 4 -4 2509.77 27.12 4 4 -4 2136.04 38.07 4 4 -4 2070.96 37.56 4 4 -3 770.39 23.21 4 4 -3 762.26 23.13 4 4 -2 669.98 21.14 4 4 -2 664.76 21.16 4 4 -1 217.00 8.46 4 4 -1 213.53 10.05 4 4 0 236.23 8.22 4 4 0 238.54 10.83 4 4 1 1639.71 19.52 4 4 1 1761.96 28.69 4 4 2 1726.70 28.32 4 4 2 1701.79 20.56 4 4 3 1174.20 22.76 4 4 3 1075.19 16.66 4 4 4 329.17 9.72 4 4 4 338.63 11.09 4 4 5 63.09 4.96 4 4 5 72.16 4.78 4 4 6 104.69 5.30 4 4 6 113.86 5.32 4 4 7 206.85 6.00 4 4 7 248.39 6.74 4 5 -9 537.09 11.05 4 5 -9 526.55 10.96 4 5 -8 116.46 6.08 4 5 -8 106.05 5.97 4 5 -8 109.39 5.93 4 5 -7 422.40 11.52 4 5 -7 410.12 12.54 4 5 -7 400.41 11.40 4 5 -6 1483.03 21.50 4 5 -6 1376.23 24.19 4 5 -6 1565.22 22.17 4 5 -6 1755.52 33.67 4 5 -6 1756.76 33.88 4 5 -5 2680.00 27.26 4 5 -5 2307.97 31.89 4 5 -5 2711.13 27.47 4 5 -5 3163.29 46.95 4 5 -5 3177.46 47.07 4 5 -4 2306.05 40.05 4 5 -4 2307.62 40.07 4 5 -3 1506.26 32.10 4 5 -3 1535.63 32.61 4 5 -2 1090.34 26.64 4 5 -2 1116.91 26.96 4 5 -1 513.01 12.63 4 5 0 1078.27 15.90 4 5 0 1069.74 16.85 4 5 0 1113.44 21.24 4 5 1 3547.52 36.03 4 5 1 3328.61 27.88 4 5 2 3246.96 26.42 4 5 2 3343.24 33.52 4 5 2 3289.58 27.86 4 5 3 1707.10 19.80 4 5 3 1728.92 22.89 4 5 3 1731.20 20.58 4 5 4 739.50 12.95 4 5 4 713.45 13.47 4 5 5 369.20 8.59 4 5 5 378.13 9.03 4 5 6 343.28 7.42 4 5 6 397.09 8.29 4 6 -8 79.66 4.61 4 6 -7 442.50 11.38 4 6 -6 758.53 20.40 4 6 -6 720.05 20.16 4 6 -5 653.82 20.16 4 6 -5 641.22 20.06 4 6 -4 1222.69 21.24 4 6 -4 1256.29 28.53 4 6 -4 1204.46 27.90 4 6 -3 674.32 21.02 4 6 -3 661.06 21.11 4 6 -2 704.29 20.65 4 6 -2 715.24 20.75 4 6 -1 1651.11 21.44 4 6 2 1125.77 15.77 4 6 3 1005.03 14.31 4 6 4 993.71 12.04 4 6 4 1166.18 14.21 4 7 -7 493.17 9.82 4 7 -6 87.57 4.87 4 7 -5 14.36 2.77 4 7 -5 10.23 4.03 4 7 -5 8.80 3.97 4 7 -4 69.77 4.69 4 7 -4 50.74 6.36 4 7 -4 50.88 6.40 4 7 -3 184.12 10.08 4 7 -3 189.67 10.26 5 -9 -4 252.34 7.28 5 -9 -3 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188.38 6.76 5 4 -8 22.68 3.20 5 4 -8 21.07 3.17 5 4 -8 22.05 3.10 5 4 -7 72.92 5.24 5 4 -7 69.63 5.65 5 4 -7 67.65 5.11 5 4 -6 270.39 9.51 5 4 -6 268.76 9.46 5 4 -5 949.20 17.22 5 4 -5 1022.87 17.78 5 4 -4 1076.61 17.17 5 4 -4 1041.48 16.83 5 4 -3 408.27 13.05 5 4 -2 68.68 5.50 5 4 -1 43.24 4.40 5 4 -1 27.24 5.63 5 4 0 117.89 6.30 5 4 0 127.58 8.77 5 4 0 123.91 5.90 5 4 1 813.31 19.67 5 4 1 824.81 14.66 5 4 2 1000.35 20.80 5 4 2 937.14 15.57 5 4 3 598.33 14.69 5 4 3 594.75 12.34 5 4 4 49.74 3.94 5 4 4 56.65 4.72 5 4 4 57.84 4.26 5 4 5 13.29 2.40 5 4 5 17.28 2.79 5 4 6 16.72 2.23 5 4 6 22.95 2.56 5 5 -8 243.25 7.29 5 5 -8 234.75 7.50 5 5 -8 251.83 7.32 5 5 -7 369.19 9.52 5 5 -7 370.98 9.61 5 5 -6 670.05 15.74 5 5 -5 758.52 17.24 5 5 -4 739.06 16.94 5 5 -3 815.00 17.13 5 5 -2 630.50 14.88 5 5 -1 661.24 13.83 5 5 -1 613.82 12.26 5 5 0 613.72 14.43 5 5 0 663.58 12.58 5 5 1 410.43 11.67 5 5 1 404.27 9.83 5 5 2 379.45 10.57 5 5 2 385.23 9.53 5 5 3 334.01 8.99 5 5 3 367.90 8.91 5 5 4 260.45 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7.93 7 2 -8 260.07 7.85 7 2 -8 263.96 8.03 7 2 -7 130.66 6.38 7 2 -7 136.45 6.56 7 2 -6 596.69 13.59 7 2 -6 562.18 13.11 7 2 -5 1497.45 21.61 7 2 -5 1451.27 22.67 7 2 -5 1481.25 21.36 7 2 -4 2181.33 25.78 7 2 -4 2123.03 28.68 7 2 -4 2098.04 24.97 7 2 -3 970.17 16.63 7 2 -3 995.67 21.05 7 2 -3 966.14 19.96 7 2 -3 979.41 16.63 7 2 -2 168.07 6.89 7 2 -2 172.23 9.49 7 2 -2 163.18 9.36 7 2 -2 180.03 7.67 7 2 -1 196.14 7.87 7 2 -1 184.07 10.00 7 2 -1 198.02 8.10 7 2 0 271.78 9.29 7 2 0 275.90 12.19 7 2 0 284.11 9.43 7 2 1 705.24 14.97 7 2 1 706.56 18.55 7 2 1 700.65 14.21 7 2 2 1151.79 22.59 7 2 2 1266.75 18.34 7 2 3 701.50 15.66 7 2 3 759.54 13.70 7 2 4 219.19 7.54 7 2 4 272.53 7.55 7 3 -7 327.86 8.67 7 3 -7 325.91 9.29 7 3 -7 314.42 8.31 7 3 -6 563.71 11.66 7 3 -6 568.30 11.62 7 3 -5 1150.50 16.86 7 3 -5 1105.80 16.31 7 3 -4 1188.94 16.71 7 3 -4 1203.88 16.76 7 3 -3 905.73 19.06 7 3 -3 940.37 18.99 7 3 -2 748.16 16.83 7 3 -2 792.06 18.01 7 3 -1 745.40 17.86 7 3 -1 753.19 14.27 7 3 0 1008.44 20.37 7 3 0 1077.47 16.86 7 3 1 1256.11 21.94 7 3 1 1327.84 17.91 7 3 2 754.37 15.29 7 3 2 836.37 13.55 7 3 3 645.19 12.15 7 3 3 727.61 12.00 7 4 -7 688.67 11.62 7 4 -6 501.50 11.18 7 4 -5 197.16 7.77 7 4 -4 224.27 8.39 7 4 -3 935.80 17.04 7 4 -2 1128.14 18.39 7 4 -2 1381.72 17.52 7 4 -1 1273.55 16.62 7 4 0 621.90 13.03 7 4 0 861.15 13.21 7 4 1 242.33 7.75 7 4 1 322.42 7.94 7 4 2 252.70 6.76 7 5 -4 33.63 3.35 7 5 -4 44.44 3.13 7 5 -3 373.07 7.95 7 5 -2 987.48 12.55 8 -7 -4 426.86 8.83 8 -7 -3 249.03 7.39 8 -7 -2 350.95 9.37 8 -7 -1 990.37 15.38 8 -7 0 1501.01 18.88 8 -7 1 1180.31 15.95 8 -7 2 504.79 9.79 8 -6 -5 801.93 12.70 8 -6 -4 392.14 9.64 8 -6 -3 369.21 10.06 8 -6 -3 449.90 10.86 8 -6 -2 533.99 12.33 8 -6 -2 749.17 14.38 8 -6 -1 652.63 13.81 8 -6 0 1098.51 17.47 8 -6 1 724.98 13.85 8 -6 2 699.35 12.75 8 -6 3 1217.67 14.94 8 -5 -6 24.56 3.10 8 -5 -5 251.02 7.94 8 -5 -4 968.01 15.86 8 -5 -4 857.23 15.20 8 -5 -3 691.92 14.22 8 -5 -3 897.87 15.93 8 -5 -2 459.63 11.86 8 -5 -2 560.72 13.03 8 -5 -1 298.26 9.67 8 -5 -1 265.73 10.97 8 -5 0 133.62 6.82 8 -5 0 213.74 8.65 8 -5 1 189.12 8.30 8 -5 1 330.41 10.30 8 -5 2 345.66 11.14 8 -5 2 724.08 13.79 8 -5 3 640.17 13.84 8 -5 3 1586.70 18.30 8 -5 4 1140.92 13.67 8 -4 -7 6.89 2.03 8 -4 -6 8.15 2.86 8 -4 -6 7.62 2.24 8 -4 -6 8.12 2.85 8 -4 -5 251.85 8.30 8 -4 -5 237.94 7.95 8 -4 -5 232.53 8.62 8 -4 -4 651.83 13.41 8 -4 -4 622.47 14.32 8 -4 -3 453.03 11.66 8 -4 -3 389.89 11.79 8 -4 -2 289.54 9.74 8 -4 -2 266.85 9.86 8 -4 -1 18.09 3.67 8 -4 -1 28.81 4.52 8 -4 -1 19.03 5.13 8 -4 0 3.70 2.85 8 -4 0 3.73 4.59 8 -4 1 144.89 7.42 8 -4 1 130.99 8.21 8 -4 2 339.77 11.07 8 -4 2 510.54 11.98 8 -4 3 392.34 12.15 8 -4 3 673.56 12.36 8 -4 4 245.76 8.19 8 -4 4 541.48 9.89 8 -3 -8 220.25 6.00 8 -3 -7 203.38 6.69 8 -3 -7 176.22 7.10 8 -3 -6 296.99 8.65 8 -3 -6 295.46 9.77 8 -3 -5 214.91 8.31 8 -3 -5 203.89 7.61 8 -3 -5 211.15 7.70 8 -3 -5 188.59 8.36 8 -3 -4 290.49 9.96 8 -3 -4 279.49 9.15 8 -3 -4 266.24 8.67 8 -3 -4 260.77 10.04 8 -3 -3 324.42 9.93 8 -3 -3 314.41 11.09 8 -3 -2 255.65 10.13 8 -3 -1 395.67 12.31 8 -3 -1 386.75 10.89 8 -3 -1 395.07 13.99 8 -3 0 232.27 9.46 8 -3 0 242.58 8.92 8 -3 0 224.94 10.88 8 -3 1 328.25 10.93 8 -3 1 365.94 10.52 8 -3 2 206.61 8.97 8 -3 2 213.73 10.23 8 -3 3 10.21 3.50 8 -3 3 9.85 2.91 8 -3 4 82.07 5.70 8 -3 4 130.40 5.32 8 -3 5 326.02 6.91 8 -2 -8 565.16 10.06 8 -2 -8 597.52 10.14 8 -2 -7 1281.71 17.78 8 -2 -7 904.59 13.84 8 -2 -7 1357.14 17.87 8 -2 -7 813.98 15.22 8 -2 -6 860.76 16.00 8 -2 -6 720.45 13.54 8 -2 -6 866.79 15.78 8 -2 -6 759.07 15.95 8 -2 -5 407.10 11.75 8 -2 -5 364.39 10.20 8 -2 -5 417.22 11.77 8 -2 -5 357.84 11.58 8 -2 -4 419.91 11.32 8 -2 -4 411.15 12.58 8 -2 -3 404.30 12.03 8 -2 -3 514.27 14.16 8 -2 -2 892.65 17.38 8 -2 -2 812.28 17.61 8 -2 -1 1833.49 29.38 8 -2 -1 1744.85 25.51 8 -2 0 1765.66 25.07 8 -2 0 1756.19 21.01 8 -2 1 516.25 13.43 8 -2 1 549.00 12.01 8 -2 1 530.52 15.67 8 -2 2 61.02 5.30 8 -2 2 61.22 4.57 8 -2 2 58.86 6.60 8 -2 2 70.40 5.09 8 -2 3 39.12 4.71 8 -2 3 45.69 3.93 8 -2 3 34.45 5.43 8 -2 4 142.96 7.00 8 -2 4 187.48 6.08 8 -1 -8 1064.44 14.46 8 -1 -8 1109.48 14.77 8 -1 -7 916.08 15.35 8 -1 -7 912.81 15.31 8 -1 -6 669.79 14.39 8 -1 -6 693.35 12.99 8 -1 -6 649.46 14.19 8 -1 -5 352.62 11.08 8 -1 -5 374.04 10.07 8 -1 -5 334.21 10.80 8 -1 -5 336.85 11.08 8 -1 -4 398.10 11.84 8 -1 -4 393.02 11.73 8 -1 -3 773.31 16.33 8 -1 -3 652.69 15.59 8 -1 -2 721.01 15.39 8 -1 -2 751.51 15.05 8 -1 -2 700.76 16.17 8 -1 -1 1596.32 27.45 8 -1 -1 1662.25 22.34 8 -1 0 2098.32 30.96 8 -1 0 2211.81 25.36 8 -1 1 603.76 14.31 8 -1 1 640.25 11.97 8 -1 1 651.06 17.16 8 -1 2 438.61 12.51 8 -1 2 438.09 14.40 8 -1 3 608.21 14.59 8 -1 3 582.78 14.98 8 -1 4 650.03 12.93 8 -1 4 563.80 12.17 8 0 -8 228.26 6.89 8 0 -8 224.20 6.75 8 0 -7 149.79 6.33 8 0 -7 148.44 6.29 8 0 -6 272.28 9.19 8 0 -6 279.16 9.24 8 0 -5 533.59 13.18 8 0 -5 501.29 14.46 8 0 -5 525.31 12.98 8 0 -5 522.85 13.09 8 0 -4 670.15 14.90 8 0 -4 644.95 16.86 8 0 -4 673.75 14.70 8 0 -3 900.37 16.82 8 0 -3 859.18 19.78 8 0 -3 834.56 16.89 8 0 -2 746.35 14.82 8 0 -2 744.72 18.67 8 0 -2 781.28 15.57 8 0 -2 725.71 15.80 8 0 -1 258.19 9.49 8 0 -1 267.93 11.71 8 0 -1 288.47 9.53 8 0 0 510.15 12.72 8 0 0 529.41 15.88 8 0 1 1103.92 18.89 8 0 1 1196.82 23.09 8 0 2 898.86 17.26 8 0 2 899.83 12.48 8 0 3 841.24 15.93 8 0 3 816.63 17.18 8 0 4 485.28 10.18 8 1 -7 11.45 2.40 8 1 -7 12.08 2.40 8 1 -7 16.88 2.98 8 1 -6 180.46 7.10 8 1 -6 178.18 7.01 8 1 -5 719.55 14.26 8 1 -5 695.39 15.39 8 1 -5 715.98 14.19 8 1 -4 700.77 13.82 8 1 -4 708.35 16.26 8 1 -3 670.72 13.31 8 1 -3 641.19 16.03 8 1 -3 650.96 13.94 8 1 -2 221.53 8.35 8 1 -2 231.40 7.76 8 1 -2 237.72 10.62 8 1 -2 236.48 8.65 8 1 -1 9.54 3.00 8 1 -1 13.56 4.71 8 1 -1 13.61 2.98 8 1 0 110.46 6.20 8 1 0 118.36 8.35 8 1 0 130.25 6.27 8 1 1 663.20 14.15 8 1 1 684.96 16.85 8 1 2 821.20 15.60 8 1 2 900.68 17.70 8 1 3 618.95 12.64 8 1 3 714.96 11.86 8 2 -6 84.36 4.59 8 2 -6 85.25 4.45 8 2 -5 256.70 7.62 8 2 -4 419.47 9.56 8 2 -4 347.04 11.40 8 2 -3 70.60 6.52 8 2 -3 75.13 4.84 8 2 -2 93.30 7.24 8 2 -2 95.51 5.28 8 2 -1 163.32 8.84 8 2 -1 186.91 7.03 8 2 0 57.10 5.83 8 2 0 63.68 4.24 8 2 1 289.85 10.36 8 2 1 333.21 8.49 8 2 2 385.26 10.19 8 2 2 465.90 9.53 8 3 -4 176.32 6.07 8 3 -3 347.65 8.48 8 3 -2 756.64 12.44 8 3 -1 508.06 12.49 8 3 -1 765.19 12.24 8 3 0 254.83 6.99 9 -4 -4 166.22 6.74 9 -4 -3 336.76 9.73 9 -4 -3 260.27 10.61 9 -4 -2 206.41 7.93 9 -4 -2 241.22 9.89 9 -4 -1 121.86 6.43 9 -4 -1 162.96 8.34 9 -4 0 326.47 10.11 9 -4 0 410.91 11.93 9 -4 1 353.42 10.63 9 -3 -5 7.99 2.87 9 -3 -4 16.00 4.61 9 -3 -4 22.31 3.48 9 -3 -3 76.97 5.36 9 -3 -3 73.51 6.68 9 -3 -2 167.02 7.50 9 -3 -2 166.94 9.17 9 -3 -1 484.38 12.12 9 -3 -1 597.49 15.07 9 -3 0 508.23 12.39 9 -3 0 652.79 15.24 9 -3 1 217.22 8.56 9 -3 1 271.38 10.40 9 -3 2 10.07 3.36 9 -2 -6 57.27 6.49 9 -2 -6 135.57 6.08 9 -2 -5 69.45 5.97 9 -2 -5 74.97 4.94 9 -2 -4 10.21 3.08 9 -2 -4 12.09 4.43 9 -2 -3 24.88 3.53 9 -2 -3 18.22 4.92 9 -2 -2 179.78 7.71 9 -2 -2 197.50 9.51 9 -2 -1 359.46 10.18 9 -2 -1 450.55 13.58 9 -2 0 227.34 8.31 9 -2 0 266.96 10.70 9 -2 1 45.66 4.33 9 -2 1 55.72 6.11 9 -2 2 49.16 4.63 9 -1 -6 241.45 6.99 9 -1 -6 262.60 7.85 9 -1 -5 153.19 9.20 9 -1 -5 268.89 8.47 9 -1 -4 240.14 9.81 9 -1 -4 231.67 8.28 9 -1 -3 342.02 9.97 9 -1 -3 362.11 11.91 9 -1 -2 279.21 9.00 9 -1 -2 295.01 11.10 9 -1 -1 189.76 9.14 9 -1 -1 215.29 7.29 9 -1 0 106.74 5.93 9 -1 0 113.49 7.64 9 -1 1 282.21 9.30 9 -1 1 326.48 11.12 9 0 -5 877.55 13.20 9 0 -5 867.51 13.93 9 0 -4 848.89 16.99 9 0 -4 768.91 12.50 9 0 -3 940.35 15.20 9 0 -3 977.86 14.57 9 0 -2 410.77 10.15 9 0 -2 500.70 13.47 9 0 -1 92.76 6.94 9 0 -1 106.89 5.24 9 0 0 281.38 10.26 9 0 0 324.70 8.34 9 0 1 654.43 14.26 9 1 -3 389.68 8.87 9 1 -2 258.25 9.87 9 1 -2 295.07 7.79 9 1 -1 227.10 9.81 9 1 -1 395.58 8.80 0 0 0 0.00 0.00 TITL jps3296b in P1 REM P1 (#1 in standard setting) CELL 1.54184 7.940793 8.718086 10.131366 94.7337 99.5535 102.8432 ZERR 1.00 0.000279 0.000280 0.000313 0.0026 0.0028 0.0029 LATT -1 SFAC C H N P Br Re UNIT 20.00 48.00 2.00 4.00 1.00 1.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 80284 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.366 _oxdiff_exptl_absorpt_empirical_full_min 0.477 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Re1 Re 0.500000 0.500000 0.500000 0.01209(19) Uani 1 2 d S T P A 1 P1 P 0.35069(18) 0.34216(16) 0.64682(14) 0.0155(3) Uani 1 1 d . . . A 1 P2 P 0.31579(18) 0.29214(15) 0.33518(13) 0.0144(3) Uani 1 1 d . . . A 1 C3 C 0.4711(8) 0.2343(7) 0.7631(6) 0.0214(12) Uani 1 1 d . . . A 1 H3A H 0.387333 0.163867 0.803841 0.026 Uiso 1 1 calc R . . A 1 H3B H 0.528004 0.169224 0.711637 0.026 Uiso 1 1 calc R . . A 1 C8 C 0.2994(8) 0.0594(7) 0.1107(6) 0.0222(12) Uani 1 1 d . . . A 1 H8A H 0.366902 0.023108 0.049784 0.033 Uiso 1 1 calc GR . . A 1 H8B H 0.195863 0.081314 0.060057 0.033 Uiso 1 1 calc GR . . A 1 H8C H 0.265755 -0.021019 0.166983 0.033 Uiso 1 1 calc GR . . A 1 C2 C 0.2205(9) 0.4301(7) 0.7513(6) 0.0213(12) Uani 1 1 d . . . A 1 H2A H 0.301053 0.512852 0.816467 0.026 Uiso 1 1 calc R . . A 1 H2B H 0.145344 0.481022 0.693518 0.026 Uiso 1 1 calc R . . A 1 C7 C 0.4101(8) 0.2101(7) 0.1985(6) 0.0225(12) Uani 1 1 d . . . A 1 H7A H 0.436249 0.291403 0.140077 0.027 Uiso 1 1 calc R . . A 1 H7B H 0.521051 0.189166 0.238794 0.027 Uiso 1 1 calc R . . A 1 C10 C -0.0565(9) 0.1910(8) 0.2127(7) 0.0298(14) Uani 1 1 d . . . A 1 H10A H -0.147401 0.224600 0.155920 0.045 Uiso 1 1 calc GR . . A 1 H10B H -0.094983 0.163047 0.294337 0.045 Uiso 1 1 calc GR . . A 1 H10C H -0.031470 0.100540 0.166267 0.045 Uiso 1 1 calc GR . . A 1 C6 C 0.2468(8) 0.1174(6) 0.4219(6) 0.0177(11) Uani 1 1 d . . . A 1 H6A H 0.152737 0.039067 0.362749 0.021 Uiso 1 1 calc R . . A 1 H6B H 0.344900 0.069616 0.446936 0.021 Uiso 1 1 calc R . . A 1 C1 C 0.1050(9) 0.3211(8) 0.8283(7) 0.0269(13) Uani 1 1 d . . . A 1 H1A H 0.020347 0.240757 0.765543 0.040 Uiso 1 1 calc GR . . A 1 H1B H 0.044820 0.381913 0.878906 0.040 Uiso 1 1 calc GR . . A 1 H1C H 0.177019 0.272038 0.888739 0.040 Uiso 1 1 calc GR . . A 1 C5 C 0.1839(8) 0.1718(7) 0.5466(6) 0.0203(12) Uani 1 1 d . . . A 1 H5A H 0.162745 0.085416 0.600916 0.024 Uiso 1 1 calc R . . A 1 H5B H 0.074057 0.202497 0.520504 0.024 Uiso 1 1 calc R . . A 1 C9 C 0.1067(9) 0.3235(8) 0.2462(8) 0.0309(15) Uani 1 1 d . . . A 1 H9A H 0.079274 0.408873 0.299811 0.037 Uiso 1 1 calc R . . A 1 H9B H 0.128395 0.362112 0.162022 0.037 Uiso 1 1 calc R . . A 1 C4 C 0.6095(8) 0.3418(7) 0.8747(6) 0.0239(13) Uani 1 1 d . . . A 1 H4A H 0.696214 0.408626 0.835505 0.036 Uiso 1 1 calc GR . . A 1 H4B H 0.665235 0.278174 0.932395 0.036 Uiso 1 1 calc GR . . A 1 H4C H 0.554423 0.406365 0.926585 0.036 Uiso 1 1 calc GR . . A 1 Br1 Br 0.7311(2) 0.32252(18) 0.51732(16) 0.0164(4) Uani 0.5 1 d . . . A -1 N1 N 0.6710(16) 0.3757(14) 0.5115(10) 0.0164(4) Uani 0.5 1 d . . . A 1 N2 N 0.774(2) 0.303(2) 0.519(2) 0.0164(4) Uani 0.5 1 d . . . A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Re1 0.0168(3) 0.0067(2) 0.0123(2) 0.00122(13) -0.00020(14) 0.00401(15) P1 0.0206(7) 0.0107(6) 0.0141(7) 0.0018(5) 0.0005(5) 0.0034(5) P2 0.0189(7) 0.0090(6) 0.0135(7) 0.0004(5) -0.0006(5) 0.0024(5) C3 0.028(3) 0.018(3) 0.017(3) -0.001(2) -0.002(2) 0.009(2) C8 0.031(3) 0.014(3) 0.021(3) -0.004(2) 0.005(2) 0.007(2) C2 0.031(3) 0.018(3) 0.018(3) 0.000(2) 0.007(2) 0.010(2) C7 0.028(3) 0.016(3) 0.020(3) -0.003(2) 0.005(2) 0.001(2) C10 0.025(3) 0.021(3) 0.037(4) -0.005(3) -0.004(3) 0.005(3) C6 0.021(3) 0.013(3) 0.018(3) 0.004(2) 0.000(2) 0.004(2) C1 0.032(3) 0.026(3) 0.025(3) 0.006(3) 0.010(3) 0.008(3) C5 0.022(3) 0.014(3) 0.022(3) 0.006(2) 0.001(2) -0.002(2) C9 0.026(3) 0.019(3) 0.041(4) 0.007(3) -0.010(3) 0.003(3) C4 0.031(3) 0.017(3) 0.022(3) 0.004(2) -0.002(2) 0.007(2) Br1 0.0195(9) 0.0133(7) 0.0180(6) 0.0017(5) 0.0013(7) 0.0090(6) N1 0.0195(9) 0.0133(7) 0.0180(6) 0.0017(5) 0.0013(7) 0.0090(6) N2 0.0195(9) 0.0133(7) 0.0180(6) 0.0017(5) 0.0013(7) 0.0090(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Re Re -5.2083 5.8923 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 P1 Re1 P1 180.00(6) 2_666 . P1 Re1 P2 81.10(5) 2_666 2_666 P1 Re1 P2 98.90(5) . 2_666 P1 Re1 P2 98.90(5) 2_666 . P1 Re1 P2 81.10(5) . . P1 Re1 Br1 91.45(5) 2_666 . P1 Re1 Br1 88.55(5) . . P2 Re1 P2 180.0 . 2_666 P2 Re1 Br1 93.87(5) 2_666 . P2 Re1 Br1 86.13(5) . . N1 Re1 P1 90.2(3) . 2_666 N1 Re1 P1 89.8(3) 2_666 2_666 N1 Re1 P1 89.8(3) . . N1 Re1 P1 90.2(3) 2_666 . N1 Re1 P2 86.8(3) . . N1 Re1 P2 86.8(3) 2_666 2_666 N1 Re1 P2 93.2(3) . 2_666 N1 Re1 P2 93.2(3) 2_666 . N1 Re1 Br1 178.7(3) 2_666 . N1 Re1 Br1 1.3(3) . . N1 Re1 N1 180.0 2_666 . C3 P1 Re1 120.0(2) . . C3 P1 C5 99.1(3) . . C2 P1 Re1 119.0(2) . . C2 P1 C3 103.7(3) . . C2 P1 C5 102.0(3) . . C5 P1 Re1 109.87(19) . . C7 P2 Re1 119.1(2) . . C6 P2 Re1 107.96(19) . . C6 P2 C7 102.4(3) . . C9 P2 Re1 118.2(2) . . C9 P2 C7 103.5(3) . . C9 P2 C6 103.6(3) . . P1 C3 H3A 108.8 . . P1 C3 H3B 108.8 . . H3A C3 H3B 107.7 . . C4 C3 P1 113.8(4) . . C4 C3 H3A 108.8 . . C4 C3 H3B 108.8 . . H8A C8 H8B 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . C7 C8 H8A 109.5 . . C7 C8 H8B 109.5 . . C7 C8 H8C 109.5 . . P1 C2 H2A 107.8 . . P1 C2 H2B 107.8 . . H2A C2 H2B 107.1 . . C1 C2 P1 118.0(4) . . C1 C2 H2A 107.8 . . C1 C2 H2B 107.8 . . P2 C7 H7A 107.9 . . P2 C7 H7B 107.9 . . C8 C7 P2 117.5(4) . . C8 C7 H7A 107.9 . . C8 C7 H7B 107.9 . . H7A C7 H7B 107.2 . . H10A C10 H10B 109.5 . . H10A C10 H10C 109.5 . . H10B C10 H10C 109.5 . . C9 C10 H10A 109.5 . . C9 C10 H10B 109.5 . . C9 C10 H10C 109.5 . . P2 C6 H6A 110.1 . . P2 C6 H6B 110.1 . . H6A C6 H6B 108.4 . . C5 C6 P2 108.0(4) . . C5 C6 H6A 110.1 . . C5 C6 H6B 110.1 . . C2 C1 H1A 109.5 . . C2 C1 H1B 109.5 . . C2 C1 H1C 109.5 . . H1A C1 H1B 109.5 . . H1A C1 H1C 109.5 . . H1B C1 H1C 109.5 . . P1 C5 H5A 109.6 . . P1 C5 H5B 109.6 . . C6 C5 P1 110.1(4) . . C6 C5 H5A 109.6 . . C6 C5 H5B 109.6 . . H5A C5 H5B 108.1 . . P2 C9 H9A 107.0 . . P2 C9 H9B 107.0 . . C10 C9 P2 121.1(5) . . C10 C9 H9A 107.0 . . C10 C9 H9B 107.0 . . H9A C9 H9B 106.8 . . C3 C4 H4A 109.5 . . C3 C4 H4B 109.5 . . C3 C4 H4C 109.5 . . H4A C4 H4B 109.5 . . H4A C4 H4C 109.5 . . H4B C4 H4C 109.5 . . N1 Br1 Re1 3.5(8) . . Br1 N1 Re1 175.2(11) . . Br1 N1 N2 5.3(10) . . N2 N1 Re1 179.3(15) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Re1 P1 2.3895(14) 2_666 Re1 P1 2.3896(14) . Re1 P2 2.3923(13) 2_666 Re1 P2 2.3923(13) . Re1 Br1 2.6442(14) . Re1 N1 1.911(14) 2_666 Re1 N1 1.912(14) . P1 C3 1.842(6) . P1 C2 1.833(6) . P1 C5 1.849(6) . P2 C7 1.846(6) . P2 C6 1.845(6) . P2 C9 1.841(6) . C3 H3A 0.9700 . C3 H3B 0.9700 . C3 C4 1.524(8) . C8 H8A 0.9600 . C8 H8B 0.9600 . C8 H8C 0.9600 . C8 C7 1.525(8) . C2 H2A 0.9700 . C2 H2B 0.9700 . C2 C1 1.525(9) . C7 H7A 0.9700 . C7 H7B 0.9700 . C10 H10A 0.9600 . C10 H10B 0.9600 . C10 H10C 0.9600 . C10 C9 1.501(9) . C6 H6A 0.9700 . C6 H6B 0.9700 . C6 C5 1.512(8) . C1 H1A 0.9600 . C1 H1B 0.9600 . C1 H1C 0.9600 . C5 H5A 0.9700 . C5 H5B 0.9700 . C9 H9A 0.9700 . C9 H9B 0.9700 . C4 H4A 0.9600 . C4 H4B 0.9600 . C4 H4C 0.9600 . Br1 N1 0.735(13) . N1 N2 1.137(17) .