#------------------------------------------------------------------------------ #$Date: 2019-11-04 18:06:11 +0200 (Mon, 04 Nov 2019) $ #$Revision: 223204 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/12/72/4127269.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4127269 loop_ _publ_author_name 'Hu, Xiangquan' 'Chai, Jie' 'Zhang, Chen' 'Lang, Jinxin' 'Kelley, Steven P.' 'Feng, Sisi' 'Liu, Bin' 'Atwood, David A.' 'Atwood, Jerry L.' _publ_section_title ; Biomimetic Self-Assembly of CoII-Seamed Hexameric Metal-Organic Nanocapsules. ; _journal_issue 23 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 9151 _journal_page_last 9154 _journal_paper_doi 10.1021/jacs.9b02857 _journal_volume 141 _journal_year 2019 _chemical_formula_moiety '0.5(C576 H132 Co36 N16 O196), 5(O)' _chemical_formula_sum 'C288 H378 Co18 N8 O103' _chemical_formula_weight 6660.70 _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_Hall '-C 2y' _space_group_name_H-M_alt 'C 1 2/m 1' _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2019-03-14 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 116.955(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 27.458(3) _cell_length_b 36.623(4) _cell_length_c 21.558(3) _cell_measurement_reflns_used 9192 _cell_measurement_temperature 100 _cell_measurement_theta_max 24.80 _cell_measurement_theta_min 2.29 _cell_volume 19324(4) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker APEX II area detector' _diffrn_measurement_method 'omega and phi scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1064 _diffrn_reflns_av_unetI/netI 0.0431 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 33 _diffrn_reflns_limit_k_min -33 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 96177 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 18.914 _diffrn_reflns_theta_max 18.914 _diffrn_reflns_theta_min 2.224 _diffrn_source 'Sealed Source Mo with TRIUMPH optics' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.820 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6155 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Bruker AXScale' _exptl_crystal_colour 'clear reddish violet' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier reddish _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.145 _exptl_crystal_description needle _exptl_crystal_F_000 6944 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.08 _refine_diff_density_max 1.395 _refine_diff_density_min -0.610 _refine_diff_density_rms 0.114 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.627 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 807 _refine_ls_number_reflns 7820 _refine_ls_number_restraints 737 _refine_ls_restrained_S_all 1.567 _refine_ls_R_factor_all 0.1530 _refine_ls_R_factor_gt 0.1176 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3582 _refine_ls_wR_factor_ref 0.3891 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5505 _reflns_number_total 7820 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja9b02857_si_002.cif _cod_data_source_block s1_a_sq _cod_depositor_comments 'Adding full bibliography for 4127269.cif.' _cod_database_code 4127269 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.937 _shelx_estimated_absorpt_t_min 0.866 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Restrained distances N2S-C5S 1.4 with sigma of 0.02 C4S-N2S 1.4 with sigma of 0.02 C4S-O2S 1.2 with sigma of 0.02 C1AA-C7AA = C7AA-C5AA = C5AA-C3AA = C54-C53 = C53-C52 = C52-C51 = C3AA-C60 = C30-C29 = C31-C30 = C32-C31 = C32-C33 = C41-C40 = C42-C41 = C43-C42 = C44-C43 = C8-C7 = C9-C8 = C10-C9 = C11-C10 = C19-C18 = C20-C19 = C21-C20 = C22-C21 1.54 with sigma of 0.02 C16-C17 \\sim C16-C15 \\sim C15-C14 \\sim C17-C12 \\sim C13-C12 \\sim C14-C13 with sigma of 0.02 3. Rigid body (RIGU) restrains All non-hydrogen atoms with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 4. Others Fixed Sof: Co4A(0.8) Co1B(0.2) Co2'(0.25) Co1'(0.125) O5(0.91) O8(0.92) O2(0.92) Co1A(0.175) Co2(0.75) Co4B(0.2) O12(0.25) C55(0.5) C55'(0.5) 5.a Ternary CH refined with riding coordinates: C7(H7), C29(H29), C40(H40) 5.b Secondary CH2 refined with riding coordinates: C8(H8A,H8B), C19(H19A,H19B), C30(H30A,H30B), C3AA(H3AA,H3AB) 5.c Aromatic/amide H refined with riding coordinates: C49(H49), C28(H28), C5(H5), C39(H39), C64(H64), C17(H17) ; _shelx_res_file ; TITL s1_a.res in C2/m s1_a_sq.res created by SHELXL-2017/1 at 14:56:58 on 14-Mar-2019 REM Old TITL s1 in C2/m REM SHELXT solution in C2/m REM R1 0.288, Rweak 0.038, Alpha 0.080, Orientation as input REM Formula found by SHELXT: C289 Co18 N40 O58 CELL 0.71073 27.4582 36.6231 21.5579 90 116.955 90 ZERR 2 0.0025 0.0035 0.0034 0 0.002 0 LATT 7 SYMM -X,+Y,-Z SFAC C H Co N O UNIT 576 756 36 16 206 DFIX 1.4 N2S C5S DFIX 1.4 C4S N2S DFIX 1.2 C4S O2S DFIX 1.54 C1AA C7AA C7AA C5AA C5AA C3AA C54 C53 C53 C52 C52 C51 C3AA C60 = C30 C29 C31 C30 C32 C31 C32 C33 C41 C40 C42 C41 C43 C42 C44 C43 C8 C7 C9 C8 = C10 C9 C11 C10 C19 C18 C20 C19 C21 C20 C22 C21 SADI C16 C17 C16 C15 C15 C14 C17 C12 C13 C12 C14 C13 RIGU L.S. 50 0 191 PLAN 40 SIZE 0.18 0.11 0.08 TEMP -173.15 BOND $H ABIN fmap 2 acta REM REM REM WGHT 0.200000 FVAR 0.12041 CO5 3 0.589904 0.293821 0.502208 11.00000 0.07420 0.09639 = 0.07620 0.00651 0.03521 -0.00579 CO3 3 0.643994 0.351937 0.404236 11.00000 0.07699 0.10135 = 0.08499 0.00457 0.03372 -0.01832 CO4A 3 0.706114 0.359382 0.597312 10.80000 0.08361 0.06916 = 0.07465 0.00249 0.03781 -0.00381 PART 1 CO1B 3 0.553911 0.500000 0.865789 10.20000 0.04910 0.05770 = 0.04709 0.00000 0.02924 0.00000 PART 0 PART 2 CO2' 3 0.786640 0.552099 0.776651 10.25000 0.12453 0.04710 = 0.09517 -0.01386 0.09125 -0.00672 CO1' 3 0.725787 0.500000 0.872450 10.12500 0.12651 0.06051 = 0.08470 0.00000 0.07922 0.00000 PART 0 O7 5 0.576756 0.275110 0.580624 11.00000 0.07599 0.09217 = 0.07516 -0.00289 0.03605 -0.00368 O4 5 0.412567 0.346500 0.696495 11.00000 0.05585 0.08923 = 0.08727 0.00752 0.02963 0.00671 O6 5 0.485893 0.275265 0.578547 11.00000 0.06943 0.09008 = 0.06906 -0.01000 0.02724 -0.00963 O15 5 0.691123 0.386341 0.378991 11.00000 0.08002 0.08196 = 0.07850 -0.00287 0.03151 -0.00966 O5 5 0.408771 0.319896 0.578450 10.91000 0.06185 0.06384 = 0.06736 -0.00711 0.01820 0.00345 O16 5 0.657393 0.435592 0.292061 11.00000 0.06188 0.07056 = 0.10790 -0.00465 0.02198 -0.00379 O8 5 0.657968 0.315675 0.582352 10.92000 0.08017 0.08836 = 0.07371 0.00660 0.04586 0.00240 O9 5 0.743465 0.336674 0.699750 11.00000 0.06621 0.12042 = 0.08010 0.01843 0.03312 -0.00136 O3 5 0.448267 0.395997 0.781767 11.00000 0.07082 0.06979 = 0.11220 0.00302 0.02671 0.01697 O14 5 0.697935 0.365770 0.500813 11.00000 0.11961 0.09660 = 0.09693 0.00054 0.05572 -0.03117 O17 5 0.603666 0.500000 0.257838 10.50000 0.08328 0.06932 = 0.12786 0.00000 0.02014 0.00000 O13 5 0.780344 0.385864 0.624189 11.00000 0.12662 0.08729 = 0.08579 0.00954 0.05127 -0.01309 O2 5 0.507368 0.457606 0.819905 10.92000 0.07047 0.06881 = 0.12234 -0.00116 0.01593 -0.00537 O1 5 0.613240 0.458509 0.906391 11.00000 0.09364 0.06201 = 0.13683 -0.00102 0.03399 0.00033 C12 1 0.492323 0.310496 0.765188 11.00000 0.06471 0.05648 = 0.07376 0.00563 0.03635 -0.00176 C59 1 0.773266 0.500000 0.365199 10.50000 0.08060 0.06099 = 0.05317 0.00000 0.03000 0.00000 C23 1 0.623158 0.269781 0.706892 11.00000 0.06804 0.06804 = 0.07573 0.00176 0.03637 0.00770 C7 1 0.494733 0.325518 0.833095 11.00000 0.08158 0.06982 = 0.08523 0.00465 0.04573 0.01011 AFIX 13 H7 2 0.456542 0.332666 0.822193 11.00000 -1.20000 AFIX 0 C48 1 0.779407 0.418786 0.437273 11.00000 0.06193 0.05615 = 0.06641 0.00858 0.02519 0.00797 C24 1 0.619741 0.282286 0.643551 11.00000 0.07132 0.06740 = 0.07895 0.00480 0.03478 0.00582 C47 1 0.735884 0.397324 0.438043 11.00000 0.07556 0.06630 = 0.07794 -0.00288 0.03480 -0.00304 C56 1 0.745012 0.466524 0.346188 11.00000 0.06584 0.06035 = 0.06478 -0.00425 0.02999 -0.00143 C4 1 0.527595 0.359423 0.853879 11.00000 0.08263 0.06393 = 0.08743 -0.00307 0.04085 0.01173 C15 1 0.490159 0.285356 0.641952 11.00000 0.06786 0.04483 = 0.06811 -0.00412 0.02560 -0.00499 C58 1 0.659355 0.500000 0.289842 10.50000 0.07492 0.07175 = 0.06864 0.00000 0.01926 0.00000 C13 1 0.452760 0.321186 0.702000 11.00000 0.05524 0.06155 = 0.07310 -0.00116 0.02443 0.00215 C27 1 0.709900 0.302420 0.770794 11.00000 0.05629 0.09076 = 0.07456 0.01872 0.02934 0.01520 C18 1 0.576749 0.247676 0.706050 11.00000 0.07474 0.06047 = 0.10756 0.01147 0.05006 0.00798 C49 1 0.820367 0.428860 0.502161 11.00000 0.06262 0.06279 = 0.07832 0.00349 0.02758 0.00222 AFIX 43 H49 2 0.848378 0.444359 0.502926 11.00000 -1.20000 AFIX 0 O11 5 0.712708 0.454124 0.915845 11.00000 0.20296 0.08301 = 0.15539 -0.00887 0.09706 -0.03102 C28 1 0.668483 0.281161 0.766953 11.00000 0.06430 0.08159 = 0.08574 0.00422 0.03521 0.01024 AFIX 43 H28 2 0.670470 0.273080 0.809914 11.00000 -1.20000 AFIX 0 C14 1 0.450412 0.309095 0.640525 11.00000 0.06408 0.05670 = 0.06961 0.00363 0.02158 -0.00016 C51 1 0.775143 0.429980 0.368616 11.00000 0.08816 0.07088 = 0.07610 0.00017 0.05103 0.01329 C5 1 0.584567 0.360727 0.898527 11.00000 0.07841 0.05915 = 0.09055 0.01318 0.04670 0.01641 AFIX 43 H5 2 0.603543 0.338285 0.914401 11.00000 -1.20000 AFIX 0 C45 1 0.782187 0.397848 0.564182 11.00000 0.11384 0.05856 = 0.07630 0.00712 0.03710 -0.01011 C57 1 0.688397 0.467145 0.310543 11.00000 0.06796 0.07111 = 0.07977 -0.00804 0.03062 -0.00384 C26 1 0.705010 0.313764 0.705007 11.00000 0.06750 0.09471 = 0.07178 0.01142 0.03201 0.00992 C29 1 0.757681 0.314236 0.837402 11.00000 0.06948 0.09983 = 0.07651 0.00777 0.03452 -0.00786 AFIX 13 H29 2 0.788639 0.317762 0.825603 11.00000 -1.20000 AFIX 0 O4AA 5 0.814313 0.435324 0.716399 11.00000 0.20996 0.10002 = 0.09670 0.00999 0.07911 -0.01021 C60 1 0.871726 0.429897 0.634413 11.00000 0.11231 0.06998 = 0.07746 0.01710 0.01585 -0.00026 C61 1 0.855626 0.466594 0.655717 11.00000 0.11746 0.07874 = 0.05457 0.01052 0.00738 -0.00052 C34 1 0.746962 0.352736 0.860519 11.00000 0.07799 0.10919 = 0.08788 0.00465 0.03443 -0.01251 C50 1 0.823845 0.418716 0.563383 11.00000 0.09389 0.05190 = 0.07403 0.00450 0.02972 0.00280 C3 1 0.502003 0.392949 0.825212 11.00000 0.06702 0.06913 = 0.09949 -0.00369 0.02681 0.00566 C8 1 0.512798 0.296582 0.892180 11.00000 0.09247 0.08618 = 0.07546 0.00934 0.03748 0.00802 AFIX 23 H8A 2 0.551010 0.289380 0.905459 11.00000 -1.20000 H8B 2 0.512040 0.307916 0.933425 11.00000 -1.20000 AFIX 0 O10 5 0.789714 0.382738 0.799162 11.00000 0.13684 0.17840 = 0.13325 -0.01691 0.08314 -0.06249 C46 1 0.738737 0.387025 0.500737 11.00000 0.10353 0.06055 = 0.08388 -0.00796 0.04713 -0.01447 C25 1 0.661072 0.303205 0.642124 11.00000 0.07041 0.08583 = 0.06966 0.00684 0.03576 0.00263 C6 1 0.613344 0.392011 0.919736 11.00000 0.08428 0.07275 = 0.09101 0.00074 0.02810 0.00509 C52 1 0.830883 0.431604 0.368788 11.00000 0.09220 0.08732 = 0.08100 0.02154 0.05443 0.02730 C38 1 0.708828 0.388330 0.920451 11.00000 0.07148 0.08098 = 0.07695 -0.00295 0.01339 -0.00596 C39 1 0.719106 0.356106 0.901071 11.00000 0.07044 0.08452 = 0.08498 0.00780 0.02984 -0.00051 AFIX 43 H39 2 0.707280 0.334640 0.915022 11.00000 -1.20000 AFIX 0 C19 1 0.593985 0.219931 0.764808 11.00000 0.07064 0.07570 = 0.10295 0.01323 0.04291 0.00965 AFIX 23 H19A 2 0.607752 0.233207 0.809580 11.00000 -1.20000 H19B 2 0.624537 0.205211 0.765701 11.00000 -1.20000 AFIX 0 C2 1 0.532772 0.424999 0.845929 11.00000 0.08141 0.06434 = 0.11574 0.00748 0.03454 0.00289 C1 1 0.586309 0.424725 0.890567 11.00000 0.07757 0.06511 = 0.09900 -0.00063 0.02249 -0.00418 C64 1 0.867610 0.500000 0.637040 10.50000 0.09730 0.07301 = 0.06889 0.00000 0.00908 0.00000 AFIX 43 H64 2 0.885828 0.500001 0.608646 10.50000 -1.20000 AFIX 0 C40 1 0.676852 0.392344 0.964886 11.00000 0.08592 0.10340 = 0.08326 -0.00513 0.01898 0.01136 AFIX 13 H40 2 0.686872 0.416599 0.988683 11.00000 -1.20000 AFIX 0 C30 1 0.777116 0.286515 0.894307 11.00000 0.07569 0.12494 = 0.07806 0.02133 0.02081 -0.01341 AFIX 23 H30A 2 0.782502 0.263049 0.875456 11.00000 -1.20000 H30B 2 0.748125 0.282740 0.908944 11.00000 -1.20000 AFIX 0 C62 1 0.828598 0.468240 0.698813 11.00000 0.15999 0.08604 = 0.08333 0.00670 0.04671 -0.00311 C41 1 0.693896 0.362701 1.022703 11.00000 0.09825 C9 1 0.477211 0.262210 0.872649 11.00000 0.12700 C3AA 1 0.926412 0.430083 0.631774 11.00000 0.09305 0.08805 = 0.08212 0.01648 -0.00279 0.00575 AFIX 23 H3AA 2 0.925869 0.449375 0.599300 11.00000 -1.20000 H3AB 2 0.931572 0.406317 0.613670 11.00000 -1.20000 AFIX 0 C35 1 0.763309 0.384302 0.839413 11.00000 0.10885 0.10961 = 0.10460 -0.00671 0.05156 -0.03788 C37 1 0.724695 0.420394 0.900614 11.00000 0.11961 0.09010 = 0.11184 -0.01514 0.03673 -0.03079 O7W 5 0.656393 0.392745 0.615962 11.00000 0.19258 C33 1 0.826854 0.243385 1.031499 11.00000 0.12527 C31 1 0.829482 0.296197 0.957730 11.00000 0.10148 C36 1 0.750666 0.418318 0.858534 11.00000 0.15143 0.11180 = 0.12226 -0.01630 0.06043 -0.04552 C32 1 0.859890 0.262749 1.002500 11.00000 0.15015 C63 1 0.811863 0.500000 0.721674 10.50000 0.15768 0.07106 = 0.10635 0.00000 0.03385 0.00000 C20 1 0.548105 0.193994 0.758909 11.00000 0.13644 PART 2 CO1A 3 0.561854 0.500000 0.846561 10.17500 0.04122 0.03960 = 0.08743 0.00000 0.04387 0.00000 PART 0 O1W 5 0.538063 0.500000 0.944795 10.50000 0.22957 O3W 5 0.566472 0.453209 0.346425 11.00000 0.25051 C5AA 1 0.974991 0.436933 0.704440 11.00000 0.17660 C53 1 0.862221 0.394980 0.387379 11.00000 0.14457 O4W 5 0.579405 0.451513 0.131534 11.00000 0.25034 C7AA 1 1.030442 0.433195 0.702077 11.00000 0.23272 C54 1 0.829728 0.364265 0.340081 11.00000 0.20356 C42 1 0.671450 0.372400 1.075516 11.00000 0.20235 O1S 5 0.627189 0.245536 0.493300 11.00000 0.09122 O2S 5 0.687600 0.304444 0.396471 11.00000 0.13691 PART 2 CO2 3 0.574067 0.448947 0.243040 10.75000 0.04186 0.03666 = 0.12242 -0.00072 -0.00305 -0.00323 CO4B 3 0.728616 0.345713 0.603791 10.20000 0.08911 0.08638 = 0.10439 0.02493 0.05569 0.01075 PART 0 N1S 4 0.629537 0.197201 0.428609 11.00000 0.16717 C1S 1 0.613990 0.233725 0.436201 11.00000 0.15049 C3S 1 0.619808 0.184447 0.358531 11.00000 0.21714 C2S 1 0.663339 0.172744 0.492858 11.00000 0.20647 O8W 5 1.000000 0.500000 0.500000 10.25000 0.26276 N2S 4 0.726738 0.272274 0.339209 11.00000 0.34109 C6S 1 0.773981 0.289610 0.319019 11.00000 0.36167 O9W 5 0.549058 0.346916 0.511375 11.00000 0.25114 O5W 5 0.593948 0.402565 0.408735 11.00000 0.27848 C5S 1 0.731965 0.241777 0.382983 11.00000 0.24534 O2W 5 0.578568 0.500000 0.774264 10.50000 0.22595 C44 1 0.662075 0.357755 1.186769 11.00000 0.18781 C10 1 0.416460 0.269813 0.845815 11.00000 0.20127 C21 1 0.567741 0.164349 0.819206 11.00000 0.21023 C43 1 0.687714 0.346355 1.138194 11.00000 0.29684 C22 1 0.512380 0.154042 0.815439 11.00000 0.28279 C11 1 0.374961 0.238155 0.811777 11.00000 0.43373 O12 5 0.751047 0.544785 0.833862 10.25000 0.06692 O0AA 5 0.768637 0.301044 0.595756 11.00000 0.47120 C1AA 1 1.082109 0.445252 0.770338 11.00000 0.35580 C4S 1 0.709425 0.305255 0.358332 11.00000 0.31059 C55 1 0.862383 0.324366 0.360020 10.50000 0.18539 C55' 1 0.828059 0.436568 0.302382 10.50000 0.23039 C16 1 0.531238 0.273640 0.704575 11.00000 0.06407 0.04912 = 0.07418 0.00604 0.03344 -0.00544 C17 1 0.532083 0.287551 0.764372 11.00000 0.05765 0.06175 = 0.06846 0.01019 0.02525 0.00309 AFIX 43 H17 2 0.561729 0.281011 0.807673 11.00000 -1.20000 AFIX 0 HKLF 4 REM s1_a.res in C2/m REM R1 = 0.1176 for 5505 Fo > 4sig(Fo) and 0.1530 for all 7820 data REM 807 parameters refined using 737 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 1.395, deepest hole -0.610, 1-sigma level 0.114 Q1 1 0.9497 0.5000 0.4905 10.50000 0.05 1.40 Q2 1 0.7828 0.5000 0.9082 10.50000 0.05 1.21 Q3 1 0.7959 0.5000 0.7631 10.50000 0.05 1.20 Q4 1 0.7694 0.5000 0.9495 10.50000 0.05 1.10 Q5 1 0.7568 0.3671 1.0722 11.00000 0.05 1.00 Q6 1 0.4887 0.2399 0.9365 11.00000 0.05 0.76 Q7 1 0.7560 0.5488 0.7514 11.00000 0.05 0.74 Q8 1 0.6406 0.3854 0.6573 11.00000 0.05 0.64 Q9 1 0.5714 0.4457 0.3271 11.00000 0.05 0.58 Q10 1 0.6413 0.5000 0.7804 10.50000 0.05 0.58 Q11 1 0.8401 0.2711 1.0387 11.00000 0.05 0.54 Q12 1 0.8389 0.5490 0.8411 11.00000 0.05 0.52 Q13 1 0.7086 0.2615 0.4188 11.00000 0.05 0.51 Q14 1 0.6805 0.4082 0.5898 11.00000 0.05 0.50 Q15 1 0.7329 0.2729 0.2675 11.00000 0.05 0.49 Q16 1 0.7506 0.4085 0.3327 11.00000 0.05 0.49 Q17 1 0.3918 0.2237 0.8392 11.00000 0.05 0.48 Q18 1 0.6325 0.1882 0.7661 11.00000 0.05 0.46 Q19 1 0.6921 0.1858 0.4884 11.00000 0.05 0.46 Q20 1 0.5511 0.2347 0.6444 11.00000 0.05 0.45 Q21 1 1.0399 0.4544 0.6716 11.00000 0.05 0.44 Q22 1 0.8169 0.2316 0.9900 11.00000 0.05 0.44 Q23 1 0.8219 0.5000 0.4060 10.50000 0.05 0.43 Q24 1 0.7009 0.4351 0.6867 11.00000 0.05 0.42 Q25 1 0.5235 0.1778 0.6998 11.00000 0.05 0.40 Q26 1 0.6061 0.1699 0.3636 11.00000 0.05 0.40 Q27 1 0.6807 0.3318 1.0031 11.00000 0.05 0.38 Q28 1 0.9626 0.4398 0.7315 11.00000 0.05 0.37 Q29 1 0.6106 0.1433 0.8298 11.00000 0.05 0.37 Q30 1 0.3431 0.2370 0.7340 11.00000 0.05 0.36 Q31 1 0.6855 0.2146 0.4511 11.00000 0.05 0.36 Q32 1 0.8639 0.4541 0.4069 11.00000 0.05 0.36 Q33 1 0.7168 0.5423 0.8015 11.00000 0.05 0.35 Q34 1 0.7641 0.2971 0.4871 11.00000 0.05 0.35 Q35 1 0.7572 0.4002 0.7826 11.00000 0.05 0.35 Q36 1 0.9101 0.3907 0.3777 11.00000 0.05 0.35 Q37 1 0.5571 0.4397 0.0781 11.00000 0.05 0.35 Q38 1 0.4599 0.5000 0.9219 10.50000 0.05 0.34 Q39 1 0.4890 0.4767 0.9301 11.00000 0.05 0.34 Q40 1 0.5077 0.2110 0.7613 11.00000 0.05 0.34 ; _shelx_res_checksum 99492 _shelx_hkl_file ; -4 0 4 1375.26 46.40 -4 0 4 1375.26 48.20 4 0 -4 1259.47 48.00 4 0 -4 1441.26 46.50 -4 0 4 1396.56 46.50 4 0 -4 1433.76 46.60 6 0 -6 1218.88 42.80 6 0 -6 1083.29 44.30 6 0 -6 1178.88 42.40 -6 0 6 1162.18 42.50 -6 0 6 1162.18 44.80 -6 0 6 1188.38 42.60 8 0 -8 103.89 15.00 -8 0 8 121.79 16.40 8 0 -8 93.09 16.10 -8 0 8 109.29 16.10 -8 0 8 89.09 13.50 8 0 -8 106.99 15.50 -10 0 10 1682.73 61.39 -10 0 10 1681.03 63.89 10 0 -10 1674.23 61.09 -10 0 10 1588.14 60.79 10 0 -10 1542.75 63.99 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27.00 9.00 2 14 -3 33.80 14.10 -2 -14 3 43.80 10.90 -2 -14 3 40.90 10.20 2 -14 -3 28.80 11.20 2 -14 -3 30.70 10.80 2 -14 -3 29.50 9.00 -2 -14 3 33.80 10.70 -4 14 5 1360.96 48.30 -4 14 5 1360.56 52.39 -4 14 5 1319.77 50.09 4 14 -5 1378.16 48.90 4 14 -5 1269.17 47.70 -4 14 5 1351.66 50.59 4 14 -5 1293.27 54.09 4 -14 -5 1365.76 51.29 -4 -14 5 1345.27 53.29 -4 -14 5 1332.67 53.99 -4 -14 5 1285.47 47.60 4 -14 -5 1463.55 52.19 4 -14 -5 1326.67 49.20 4 -14 -5 1363.36 50.49 -4 -14 5 1368.46 53.39 -6 14 7 1402.66 58.49 6 14 -7 1531.85 62.09 -6 14 7 1542.15 56.69 -6 14 7 1478.45 55.89 6 14 -7 1603.74 53.59 -6 14 7 1459.95 58.19 -6 -14 7 1469.85 58.49 6 -14 -7 1499.55 57.19 -6 -14 7 1544.25 55.69 6 -14 -7 1449.85 56.09 6 -14 -7 1491.75 55.49 -6 -14 7 1587.04 60.59 6 -14 -7 1516.25 57.69 -6 -14 7 1516.55 59.99 -6 -14 7 1452.25 53.89 -8 14 9 3.70 12.30 8 14 -9 1.60 14.40 8 14 -9 -9.00 7.90 -8 14 9 1.00 11.50 -8 14 9 -5.10 10.60 -8 14 9 10.60 13.00 8 14 -9 9.20 16.00 8 -14 -9 -14.60 14.90 -8 -14 9 15.20 14.90 -8 -14 9 3.80 10.90 8 -14 -9 13.70 11.50 -8 -14 9 -16.80 11.00 -8 -14 9 2.80 12.60 8 -14 -9 0.10 10.40 8 -14 -9 11.50 13.60 10 14 -11 72.89 21.20 10 14 -11 116.49 24.00 10 14 -11 112.69 14.50 -10 14 11 93.59 18.90 -10 14 11 106.89 18.00 -10 14 11 128.69 19.60 -10 -14 11 113.49 21.00 10 -14 -11 145.49 20.80 10 -14 -11 112.69 16.10 -10 -14 11 146.29 16.40 -10 -14 11 87.59 18.60 10 -14 -11 113.19 21.10 10 -14 -11 118.89 17.00 12 14 -13 219.58 29.80 -12 14 13 240.18 27.40 12 14 -13 213.58 28.80 -12 14 13 157.38 24.90 -12 14 13 161.08 22.80 12 -14 -13 198.08 24.70 12 -14 -13 241.98 25.50 12 -14 -13 200.78 24.80 -12 -14 13 169.48 25.50 -12 -14 13 151.38 23.70 12 -14 -13 176.48 26.80 12 -14 -13 213.28 26.50 -14 14 15 39.00 18.90 14 14 -15 67.39 27.10 -14 14 15 50.99 21.80 14 -14 -15 62.79 19.40 -14 -14 15 44.70 20.20 -14 -14 15 0.50 20.80 14 -14 -15 48.80 17.30 -14 -14 15 41.20 26.00 14 -14 -15 9.80 19.20 -14 -14 15 37.30 20.20 14 -14 -15 65.19 24.30 17 15 -16 19.70 32.60 -17 15 16 -7.70 22.00 -17 15 16 8.70 21.60 17 -15 -16 3.50 26.90 17 -15 -16 -26.40 22.20 -17 -15 16 -18.80 20.50 17 -15 -16 7.00 19.80 -17 -15 16 -10.30 20.40 17 -15 -16 6.80 20.90 -15 15 14 40.00 24.60 15 15 -14 69.59 27.30 -15 15 14 -6.70 20.40 -15 15 14 22.10 20.30 15 -15 -14 7.70 19.50 -15 -15 14 66.89 22.80 -15 -15 14 32.70 22.00 -15 -15 14 30.70 20.30 15 -15 -14 8.20 17.90 15 -15 -14 60.19 25.00 -13 15 12 240.28 23.50 -13 15 12 200.88 27.50 -13 15 12 254.87 38.50 -13 15 12 224.78 30.80 13 15 -12 292.47 36.60 13 -15 -12 242.38 28.10 -13 -15 12 253.47 31.20 13 -15 -12 261.97 33.40 13 -15 -12 309.17 28.10 -13 -15 12 232.48 29.00 -13 -15 12 219.58 31.20 13 -15 -12 214.58 31.60 11 15 -10 10.50 18.60 -11 15 10 12.00 14.50 -11 15 10 21.80 14.90 11 15 -10 10.70 15.90 11 15 -10 7.20 9.20 -11 15 10 2.10 15.20 11 -15 -10 -0.80 16.60 -11 -15 10 3.60 11.00 11 -15 -10 27.70 15.50 -11 -15 10 32.90 15.70 -11 -15 10 10.10 15.00 -11 -15 10 9.50 15.80 11 -15 -10 21.90 13.20 11 -15 -10 27.20 14.80 -9 15 8 341.17 28.30 9 15 -8 362.56 20.00 9 15 -8 367.16 29.00 -9 15 8 371.56 27.70 9 15 -8 372.26 32.90 -9 15 8 368.36 24.70 -9 15 8 347.47 29.20 -9 -15 8 330.67 28.30 9 -15 -8 353.26 28.20 -9 -15 8 351.86 29.80 9 -15 -8 370.36 27.30 -9 -15 8 372.56 30.30 9 -15 -8 381.76 26.60 -9 -15 8 400.56 26.80 9 -15 -8 331.77 26.60 -7 15 6 -2.80 10.30 -7 15 6 -12.70 11.10 -7 15 6 -0.20 12.40 7 15 -6 19.30 15.20 7 15 -6 23.30 9.00 -7 15 6 6.00 11.80 7 -15 -6 2.40 11.20 -7 -15 6 -10.90 11.80 -7 -15 6 15.50 11.20 -7 -15 6 -1.80 11.90 7 -15 -6 4.90 11.70 7 -15 -6 -0.20 11.20 -7 -15 6 8.80 10.50 -7 -15 6 9.10 12.70 -5 15 4 385.86 26.80 -5 15 4 431.96 21.60 -5 15 4 427.36 25.40 5 15 -4 381.96 22.40 5 15 -4 390.96 29.30 -5 15 4 404.66 26.00 5 15 -4 388.16 23.30 5 -15 -4 383.36 25.80 5 -15 -4 414.56 22.00 5 -15 -4 438.76 24.10 -5 -15 4 374.26 22.00 -5 -15 4 437.66 26.40 -5 -15 4 398.66 26.30 -5 -15 4 368.06 23.00 5 -15 -4 433.36 25.30 3 15 -2 122.59 16.60 -3 15 2 114.39 16.40 -3 15 2 130.69 16.80 3 15 -2 142.19 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-1 -7 107.29 21.10 -7 1 5 839.12 36.40 7 1 -5 943.81 34.90 -7 1 5 887.51 34.10 -7 1 5 903.41 33.50 7 1 -5 765.02 35.90 7 1 -5 930.31 33.80 -7 -1 5 855.41 34.40 7 -1 -5 829.62 36.20 -7 -1 5 807.42 35.90 7 -1 -5 921.71 33.60 7 -1 -5 905.01 34.40 -7 -1 5 896.71 33.40 5 1 -3 395.26 20.80 -5 1 3 401.56 20.90 5 1 -3 416.96 17.80 5 1 -3 417.96 19.00 -5 1 3 426.86 15.30 -5 1 3 420.06 17.80 -5 1 3 415.46 18.80 5 -1 -3 399.96 15.50 -5 -1 3 403.16 18.90 -5 -1 3 402.96 18.00 5 -1 -3 443.76 21.10 -5 -1 3 403.86 20.50 5 -1 -3 432.56 18.90 5 -1 -3 431.66 17.70 -3 1 1 2803.42 88.09 3 1 -1 2622.14 87.39 3 1 -1 2888.71 87.89 3 1 -1 2861.81 88.99 -3 1 1 2885.01 88.89 -3 -1 1 2779.12 88.19 3 -1 -1 2836.62 88.09 3 -1 -1 2900.01 88.69 3 -1 -1 2685.73 87.29 1 1 -3 2066.39 64.29 -1 1 3 1977.00 64.09 -1 1 3 2039.10 63.19 1 1 -3 2060.19 64.19 -1 1 3 2081.29 63.89 1 1 -3 2083.19 63.49 1 1 -3 1983.00 64.99 -1 1 3 2007.10 64.99 -1 -1 3 2102.39 64.39 1 -1 -3 2035.70 64.09 -1 -1 3 2072.69 63.49 1 -1 -3 1934.31 64.89 1 -1 -3 2063.29 63.79 -1 -1 3 2018.00 64.79 -1 -1 3 2013.00 64.09 -3 1 5 4699.43 151.18 -3 1 5 4960.70 149.69 3 1 -5 4735.43 152.68 -3 1 5 4811.02 150.38 -3 1 5 5012.10 152.78 3 1 -5 4764.42 148.79 3 1 -5 4903.61 151.38 3 -1 -5 4779.72 152.78 3 -1 -5 4940.61 151.38 -3 -1 5 4824.72 151.48 -3 -1 5 4838.32 148.89 -3 -1 5 5060.89 152.68 -3 -1 5 4800.02 151.28 3 -1 -5 4902.61 150.48 3 -1 -5 4810.12 149.29 5 1 -7 130.29 9.80 -5 1 7 174.48 19.10 -5 1 7 158.18 13.60 -5 1 7 152.48 18.60 5 1 -7 163.88 15.30 -5 1 7 136.89 11.40 5 -1 -7 141.99 14.00 -5 -1 7 144.29 14.30 5 -1 -7 162.28 15.20 -5 -1 7 146.19 17.70 5 -1 -7 131.69 10.90 -5 -1 7 152.98 18.90 -5 -1 7 128.89 15.30 -7 1 9 97.59 16.90 7 1 -9 97.59 13.70 7 1 -9 83.89 16.80 -7 1 9 86.49 13.70 7 -1 -9 98.89 13.20 7 -1 -9 94.39 10.90 -7 -1 9 123.99 17.90 -7 -1 9 97.69 16.10 7 -1 -9 62.29 15.10 -7 -1 9 68.59 12.20 -7 -1 9 74.99 13.50 -9 1 11 434.86 28.20 9 1 -11 469.45 28.30 9 1 -11 398.96 32.80 -9 1 11 432.56 27.40 -9 1 11 452.15 33.10 -9 -1 11 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111.79 13.20 -6 -4 4 109.49 15.10 6 -4 -4 129.89 13.30 6 -4 -4 110.29 15.70 6 -4 -4 112.99 10.70 -6 -4 4 134.79 14.50 -6 -4 4 110.69 14.00 -6 -4 4 104.89 13.20 -4 4 2 112.69 9.80 -4 4 2 94.19 11.70 -4 4 2 121.79 11.00 4 4 -2 101.29 12.30 4 4 -2 110.89 10.20 -4 4 2 124.49 9.70 4 4 -2 103.69 12.50 -4 -4 2 127.09 12.00 4 -4 -2 101.09 11.60 -4 -4 2 96.19 11.90 -4 -4 2 118.09 8.30 -4 -4 2 116.09 10.70 4 -4 -2 119.79 10.60 4 -4 -2 123.59 10.60 4 -4 -2 114.99 9.90 -2 4 0 3478.25 102.99 -2 4 0 3409.56 103.69 2 4 0 3235.88 104.09 -2 4 0 3304.87 103.79 -2 4 0 3331.77 104.29 2 4 0 3316.07 104.29 2 -4 0 3226.18 103.79 2 -4 0 3478.95 102.99 -2 -4 0 3297.07 103.89 2 -4 0 3391.56 104.29 2 -4 0 3406.46 103.59 0 4 -2 1052.99 33.80 0 4 -2 1022.10 34.90 0 4 2 1018.90 34.10 0 4 -2 986.40 33.10 0 4 2 1010.90 32.50 0 4 2 1031.30 33.90 0 -4 2 1008.70 33.70 0 -4 -2 1020.10 33.80 0 -4 2 1038.80 34.60 0 -4 -2 1020.60 34.40 0 -4 -2 1058.29 33.90 0 -4 -2 996.90 32.30 0 -4 2 1049.59 34.60 0 -4 2 917.91 32.80 -2 4 4 41.00 6.40 2 4 -4 34.00 7.20 2 4 -4 45.20 10.30 -2 4 4 38.00 7.80 -2 4 4 50.09 9.10 2 4 -4 39.70 7.40 2 4 -4 35.30 8.90 2 -4 -4 49.50 10.70 -2 -4 4 32.50 7.30 2 -4 -4 29.70 7.10 -2 -4 4 31.60 8.40 2 -4 -4 40.90 6.20 -2 -4 4 52.49 10.10 2 -4 -4 42.50 8.30 -2 -4 4 34.30 7.40 4 4 -6 498.55 22.60 4 4 -6 457.75 24.50 4 4 -6 442.36 23.30 -4 4 6 415.56 19.70 4 4 -6 480.15 17.90 -4 4 6 426.06 22.20 -4 4 6 410.86 24.30 4 -4 -6 447.36 19.70 4 -4 -6 451.65 22.40 4 -4 -6 423.96 19.90 -4 -4 6 458.25 22.10 4 -4 -6 406.66 24.90 -4 -4 6 500.75 23.70 -4 -4 6 489.85 24.60 4 -4 -6 404.76 19.80 -4 -4 6 488.65 17.80 -6 4 8 -0.50 7.10 6 4 -8 5.00 5.40 -6 4 8 -2.70 8.80 -6 4 8 5.30 12.70 6 4 -8 10.80 9.30 6 4 -8 3.40 12.20 -6 -4 8 -5.80 8.10 6 -4 -8 7.30 11.60 -6 -4 8 4.10 9.20 6 -4 -8 0.10 7.40 6 -4 -8 5.00 8.40 6 -4 -8 7.90 6.70 6 -4 -8 -6.70 8.10 -8 4 10 61.79 13.90 8 4 -10 69.49 14.00 8 4 -10 67.69 17.20 -8 4 10 78.59 13.50 -8 4 10 84.39 18.70 -8 -4 10 46.30 12.60 8 -4 -10 68.39 9.80 -8 -4 10 85.29 15.00 -8 -4 10 65.09 13.80 8 -4 -10 66.39 16.80 -8 -4 10 69.39 16.20 8 -4 -10 51.19 10.40 -10 4 12 -6.10 12.30 -10 4 12 -20.40 17.90 10 4 -12 16.20 12.30 -10 4 12 -6.90 11.30 10 4 -12 -18.60 16.20 10 -4 -12 -1.40 7.80 -10 -4 12 1.50 11.40 -10 -4 12 -1.10 12.40 -10 -4 12 3.30 13.00 10 -4 -12 -7.00 7.40 -10 -4 12 6.70 17.30 10 -4 -12 -6.70 11.50 10 -4 -12 -37.00 16.50 10 -4 -12 -3.80 10.80 -12 4 14 95.59 23.20 12 4 -14 75.59 20.90 -12 4 14 84.29 17.90 -12 4 14 109.99 17.80 12 4 -14 113.89 18.20 12 -4 -14 105.79 22.60 12 -4 -14 86.89 17.00 -12 -4 14 79.29 19.50 -12 -4 14 90.39 22.10 12 -4 -14 98.49 11.80 -12 -4 14 84.99 19.40 12 -4 -14 107.29 18.40 12 -4 -14 91.89 11.00 -12 -4 14 115.09 19.50 -14 4 16 59.59 18.00 -14 4 16 90.99 20.70 -14 4 16 48.40 23.40 14 4 -16 82.29 21.60 14 4 -16 84.59 26.80 14 -4 -16 97.59 26.90 14 -4 -16 20.50 17.90 -14 -4 16 93.39 28.70 -14 -4 16 103.59 22.00 -14 -4 16 68.09 19.80 -14 -4 16 63.29 20.60 -16 4 18 17.20 18.70 16 4 -18 -8.30 27.00 -16 4 18 -13.10 20.90 -16 -4 18 11.30 18.20 -16 -4 18 1.90 24.40 -16 -4 18 22.80 22.60 16 -4 -18 33.30 23.40 19 5 -17 -13.70 29.60 -19 5 17 4.10 21.50 -19 5 17 -3.40 19.50 -19 -5 17 12.10 20.40 -19 -5 17 -7.80 20.50 19 -5 -17 4.30 25.10 -17 5 15 151.18 27.80 -17 5 15 176.58 24.50 -17 5 15 216.58 31.50 17 5 -15 162.98 24.80 17 5 -15 182.28 30.20 17 -5 -15 141.19 26.40 17 -5 -15 119.29 21.20 -17 -5 15 230.28 32.80 17 -5 -15 143.79 24.90 -17 -5 15 160.18 27.10 -17 -5 15 158.98 26.70 -17 -5 15 160.58 24.90 15 5 -13 -13.90 18.80 -15 5 13 3.30 15.00 15 5 -13 -3.30 14.80 -15 5 13 24.30 17.80 -15 5 13 -7.40 13.60 -15 -5 13 19.40 14.60 15 -5 -13 19.20 15.40 -15 -5 13 8.40 15.30 15 -5 -13 27.80 17.70 -15 -5 13 7.80 15.50 -15 -5 13 42.70 19.50 15 -5 -13 0.00 15.90 -13 5 11 273.77 25.10 13 5 -11 298.27 30.90 -13 5 11 270.37 30.30 -13 5 11 328.47 26.10 13 5 -11 271.97 25.20 13 -5 -11 370.86 27.70 13 -5 -11 305.67 30.30 -13 -5 11 276.17 27.00 13 -5 -11 293.17 17.20 -13 -5 11 263.47 27.00 -13 -5 11 314.07 29.30 13 -5 -11 298.27 25.90 -13 -5 11 322.57 26.10 11 5 -9 143.99 21.80 -11 5 9 196.58 20.90 11 5 -9 157.18 21.00 -11 5 9 171.18 20.40 -11 5 9 175.48 13.50 -11 5 9 232.78 25.30 11 -5 -9 211.58 15.10 -11 -5 9 175.08 20.50 11 -5 -9 191.58 19.50 -11 -5 9 185.28 21.00 11 -5 -9 166.98 24.50 -11 -5 9 139.49 19.10 -11 -5 9 157.18 22.20 11 -5 -9 178.18 20.10 -9 5 7 117.39 11.60 9 5 -7 96.49 15.10 -9 5 7 121.69 15.80 -9 5 7 113.29 16.40 9 5 -7 109.59 13.10 -9 5 7 103.09 14.00 -9 -5 7 100.09 13.80 9 -5 -7 109.69 11.70 -9 -5 7 91.19 13.80 -9 -5 7 130.29 19.00 9 -5 -7 94.79 15.40 9 -5 -7 100.39 12.80 -9 -5 7 93.79 12.90 -7 5 5 70.29 10.30 7 5 -5 87.49 12.50 -7 5 5 84.19 12.50 -7 5 5 88.09 10.90 7 5 -5 50.69 12.10 -7 5 5 86.49 11.50 7 -5 -5 94.59 11.30 -7 -5 5 79.99 11.90 -7 -5 5 82.79 12.40 7 -5 -5 86.49 13.20 7 -5 -5 78.39 10.70 -7 -5 5 69.09 12.70 -7 -5 5 75.89 10.70 7 -5 -5 63.49 12.10 5 5 -3 175.78 16.30 -5 5 3 177.48 13.60 -5 5 3 172.28 14.30 5 5 -3 171.18 14.00 -5 5 3 195.68 12.90 5 5 -3 170.38 16.80 -5 5 3 177.38 16.50 -5 -5 3 198.38 10.60 5 -5 -3 193.08 13.50 5 -5 -3 169.78 13.60 5 -5 -3 187.58 14.40 -5 -5 3 148.59 15.80 -5 -5 3 170.88 16.00 -5 -5 3 154.58 14.50 -5 -5 3 201.68 11.20 5 -5 -3 177.58 16.20 -3 5 1 508.95 19.50 -3 5 1 516.65 20.10 -3 5 1 524.95 20.80 3 5 -1 487.45 21.40 -3 5 1 520.35 19.90 3 5 -1 499.45 21.40 3 5 -1 483.15 20.40 3 -5 -1 496.75 20.50 -3 -5 1 505.35 21.00 3 -5 -1 508.85 19.50 -3 -5 1 483.55 21.00 -3 -5 1 522.65 20.00 -3 -5 1 529.95 19.60 3 -5 -1 532.55 20.30 3 -5 -1 527.55 19.80 -1 5 -1 721.33 24.50 -1 5 -1 695.63 24.80 -1 5 -1 696.53 25.10 1 5 1 645.94 23.60 1 5 1 649.43 23.40 1 5 1 643.74 24.50 1 -5 1 659.63 24.50 1 -5 1 696.93 24.40 -1 -5 -1 646.04 23.10 1 -5 1 722.53 25.00 -1 -5 -1 645.74 23.30 -1 -5 -1 666.83 24.40 -1 5 3 30.50 5.40 -1 5 3 36.00 7.50 1 5 -3 31.50 7.50 1 5 -3 29.70 7.90 -1 5 3 17.30 7.00 1 5 -3 20.00 8.30 -1 -5 3 26.30 7.00 -1 -5 3 37.80 7.30 1 -5 -3 27.00 6.70 1 -5 -3 23.60 7.00 -1 -5 3 24.00 7.50 1 -5 -3 17.30 6.30 1 -5 -3 37.90 8.00 1 -5 -3 31.10 5.30 -1 -5 3 21.80 6.80 3 5 -5 44.20 10.90 -3 5 5 47.20 9.10 -3 5 5 52.69 7.60 3 5 -5 59.19 10.40 3 5 -5 82.99 12.20 3 -5 -5 42.70 9.00 3 -5 -5 49.99 8.40 3 -5 -5 44.30 7.50 -3 -5 5 45.70 7.60 -3 -5 5 59.19 10.20 3 -5 -5 41.50 8.20 -3 -5 5 74.29 11.00 3 -5 -5 62.69 11.30 -3 -5 5 62.19 9.40 5 5 -7 199.48 11.70 -5 5 7 150.68 13.10 5 5 -7 178.28 16.70 -5 5 7 199.28 19.00 5 5 -7 185.48 15.50 -5 5 7 164.58 16.10 5 5 -7 176.78 20.90 -5 -5 7 188.68 11.10 5 -5 -7 172.38 12.90 -5 -5 7 207.18 19.00 5 -5 -7 156.28 15.70 -5 -5 7 195.68 17.30 -5 -5 7 192.48 16.10 5 -5 -7 193.08 13.90 5 -5 -7 162.98 14.10 -7 5 9 0.60 11.40 7 5 -9 36.70 11.30 -7 5 9 14.30 12.50 7 5 -9 -8.40 13.00 7 -5 -9 15.20 9.50 7 -5 -9 5.30 8.50 7 -5 -9 18.20 8.00 -7 -5 9 13.80 13.50 7 -5 -9 8.30 10.20 -7 -5 9 16.70 11.20 7 -5 -9 5.20 15.30 -7 -5 9 26.50 11.20 9 5 -11 37.70 15.70 -9 5 11 53.99 16.60 -9 5 11 26.70 11.80 -9 5 11 26.40 14.20 9 5 -11 74.69 14.00 -9 -5 11 35.90 12.80 9 -5 -11 26.60 12.70 9 -5 -11 41.50 9.20 -9 -5 11 26.10 13.10 9 -5 -11 56.69 13.00 9 -5 -11 43.70 17.70 -9 -5 11 35.40 14.30 9 -5 -11 47.30 9.60 -9 -5 11 34.80 16.10 11 5 -13 126.09 29.50 11 5 -13 83.89 21.50 -11 5 13 101.19 18.50 -11 5 13 105.19 16.60 -11 5 13 80.69 22.90 11 -5 -13 97.99 11.70 -11 -5 13 92.99 18.10 11 -5 -13 116.69 14.60 11 -5 -13 82.19 27.60 11 -5 -13 79.59 21.40 11 -5 -13 86.19 16.70 -11 -5 13 84.69 19.30 -11 -5 13 86.19 17.80 -11 -5 13 99.29 16.80 -13 5 15 -10.50 13.00 13 5 -15 17.30 16.60 -13 5 15 -4.60 19.40 -13 5 15 -19.10 15.00 13 5 -15 -7.00 19.40 13 -5 -15 -1.30 10.10 13 -5 -15 -26.20 14.20 13 -5 -15 -16.20 8.80 -13 -5 15 -0.30 16.00 13 -5 -15 -15.70 14.90 -13 -5 15 12.00 15.60 -13 -5 15 -10.80 17.30 13 -5 -15 -13.80 18.10 -13 -5 15 3.50 20.50 -15 5 17 14.60 17.30 -15 5 17 -12.50 18.70 15 5 -17 -25.90 22.80 -15 -5 17 -21.80 16.40 -15 -5 17 -1.10 18.90 -15 -5 17 -1.00 23.40 15 -5 -17 9.30 21.70 -18 6 16 -28.10 19.60 -18 6 16 -12.90 16.30 18 6 -16 28.60 30.50 -18 -6 16 -6.00 21.00 18 -6 -16 27.70 25.80 18 -6 -16 3.40 20.70 -18 -6 16 2.30 20.00 16 6 -14 12.40 14.40 -16 6 14 -10.80 14.70 -16 6 14 18.60 20.90 -16 6 14 -20.00 16.20 16 6 -14 2.60 23.10 -16 -6 14 5.00 15.50 -16 -6 14 -12.60 14.60 16 -6 -14 -0.20 17.30 -16 -6 14 -1.30 21.20 16 -6 -14 21.90 20.50 -16 -6 14 1.50 17.60 16 -6 -14 28.30 17.70 -14 6 12 -18.20 10.70 14 6 -12 -3.90 14.40 -14 6 12 -15.80 13.60 -14 6 12 9.40 18.60 14 6 -12 2.00 16.50 14 -6 -12 3.00 13.60 -14 -6 12 -15.80 13.90 14 -6 -12 -11.80 8.80 -14 -6 12 9.80 16.00 14 -6 -12 16.20 18.70 -14 -6 12 -11.10 13.60 -12 6 10 73.89 17.20 -12 6 10 76.39 16.20 12 6 -10 69.09 14.80 12 6 -10 61.39 17.90 -12 6 10 62.29 9.90 -12 6 10 76.09 14.80 12 -6 -10 74.19 10.80 12 -6 -10 44.60 18.00 12 -6 -10 92.79 16.00 -12 -6 10 68.79 15.00 -12 -6 10 51.39 16.50 -12 -6 10 85.29 16.90 12 -6 -10 90.29 15.20 -12 -6 10 83.49 19.50 -10 6 8 14.60 10.10 -10 6 8 0.60 10.30 -10 6 8 2.20 7.30 -10 6 8 10.60 12.80 10 6 -8 20.30 10.10 10 6 -8 -11.30 13.40 10 -6 -8 10.20 8.40 -10 -6 8 13.20 12.00 10 -6 -8 6.70 9.40 -10 -6 8 3.20 12.60 -10 -6 8 2.30 10.70 -10 -6 8 7.50 11.10 10 -6 -8 -3.20 12.60 10 -6 -8 -0.70 9.30 8 6 -6 2.60 13.20 -8 6 6 -8.40 8.00 8 6 -6 7.70 11.70 -8 6 6 -9.70 7.80 -8 6 6 1.30 10.70 -8 6 6 -0.90 6.70 -8 -6 6 3.80 8.90 8 -6 -6 -2.70 8.10 8 -6 -6 -11.20 7.50 -8 -6 6 -6.70 10.40 8 -6 -6 6.80 6.70 -8 -6 6 -3.10 8.40 -6 6 4 100.29 11.40 -6 6 4 111.29 13.00 6 6 -4 98.69 15.50 6 6 -4 98.39 13.30 -6 6 4 92.39 12.80 -6 6 4 107.59 13.40 6 6 -4 109.59 13.00 -6 -6 4 94.99 13.70 6 -6 -4 98.49 11.60 6 -6 -4 96.19 12.70 -6 -6 4 102.69 14.80 6 -6 -4 107.49 13.50 -6 -6 4 111.49 13.30 -6 -6 4 103.19 9.20 -6 -6 4 98.09 9.00 6 -6 -4 104.09 12.60 4 6 -2 2215.28 77.79 -4 6 2 2408.46 75.79 -4 6 2 2383.36 75.59 -4 6 2 2397.46 76.19 4 6 -2 2328.77 76.39 -4 6 2 2402.86 76.69 4 -6 -2 2438.26 76.49 -4 -6 2 2368.36 76.29 4 -6 -2 2360.16 75.99 -4 -6 2 2332.27 74.79 -4 -6 2 2300.37 77.79 -4 -6 2 2256.27 77.29 4 -6 -2 2430.96 75.89 4 -6 -2 2455.85 76.09 -2 6 0 205.48 12.80 -2 6 0 196.38 13.20 2 6 0 213.78 13.40 2 6 0 202.68 13.80 -2 6 0 198.48 12.50 -2 -6 0 210.28 12.30 -2 -6 0 214.28 11.40 -2 -6 0 209.28 12.30 2 -6 0 214.48 12.90 2 -6 0 210.58 13.50 -2 -6 0 214.58 13.60 2 -6 0 219.48 12.70 -2 -6 0 214.28 11.90 0 6 -2 18.30 7.00 0 6 -2 27.30 6.00 0 6 -2 16.00 7.40 0 6 2 13.20 7.00 0 6 2 19.30 5.80 0 6 2 19.20 6.10 0 6 -2 22.30 7.70 0 -6 2 29.00 7.60 0 -6 -2 15.00 5.30 0 -6 2 9.50 7.00 0 -6 -2 24.20 6.90 0 -6 2 20.20 7.20 0 -6 -2 17.90 6.70 0 -6 -2 22.30 6.00 2 6 -4 1956.80 62.79 -2 6 4 1917.11 62.69 2 6 -4 1940.41 64.29 2 6 -4 1918.21 66.09 -2 6 4 1911.11 64.59 -2 6 4 1902.41 64.79 2 6 -4 2084.79 65.29 -2 -6 4 1912.71 62.79 2 -6 -4 1910.51 62.59 2 -6 -4 1979.70 64.69 2 -6 -4 1896.71 65.19 -2 -6 4 2044.40 66.19 -2 -6 4 1978.50 65.19 -2 -6 4 2030.10 64.29 2 -6 -4 1979.00 64.49 4 6 -6 64.49 11.90 4 6 -6 54.89 11.80 -4 6 6 50.49 10.60 4 6 -6 67.29 10.50 4 6 -6 76.29 10.00 -4 6 6 63.99 11.10 -4 6 6 62.39 8.30 -4 -6 6 69.19 11.50 4 -6 -6 59.89 8.90 4 -6 -6 47.70 8.40 4 -6 -6 60.69 12.40 4 -6 -6 68.79 10.40 -4 -6 6 73.79 8.10 -4 -6 6 59.79 9.60 -4 -6 6 63.59 12.50 4 -6 -6 68.29 9.70 -6 6 8 144.19 14.00 6 6 -8 169.98 16.00 6 6 -8 158.08 19.70 6 6 -8 167.38 11.30 -6 6 8 133.89 17.60 -6 6 8 132.59 19.70 6 6 -8 166.88 18.60 -6 -6 8 164.38 11.10 6 -6 -8 146.49 13.10 -6 -6 8 167.68 17.10 6 -6 -8 124.19 14.80 6 -6 -8 115.79 14.00 6 -6 -8 158.98 16.80 6 -6 -8 128.19 20.40 -8 6 10 64.39 15.90 8 6 -10 53.49 12.40 -8 6 10 49.50 12.00 8 6 -10 46.20 15.70 -8 6 10 63.19 13.70 8 -6 -10 40.50 20.30 8 -6 -10 51.29 12.30 8 -6 -10 52.09 16.50 -8 -6 10 37.80 13.20 8 -6 -10 66.39 11.10 -8 -6 10 78.99 15.30 8 -6 -10 59.59 9.80 -8 -6 10 70.89 16.70 -10 6 12 6.90 11.30 -10 6 12 -24.00 12.50 10 6 -12 -12.40 16.80 10 6 -12 28.60 13.30 -10 6 12 9.50 17.40 10 -6 -12 7.10 12.60 10 -6 -12 -0.20 9.30 -10 -6 12 -8.30 16.60 -10 -6 12 7.40 12.60 10 -6 -12 -8.90 16.10 10 -6 -12 7.90 12.10 -10 -6 12 27.80 14.70 10 -6 -12 10.30 9.00 -10 -6 12 18.70 13.50 -12 6 14 143.79 22.50 12 6 -14 148.89 24.70 -12 6 14 120.09 22.30 -12 6 14 158.68 20.30 12 6 -14 172.78 25.40 12 -6 -14 140.29 20.00 -12 -6 14 115.19 22.30 12 -6 -14 155.38 17.10 -12 -6 14 100.79 21.10 12 -6 -14 133.89 24.20 -12 -6 14 122.69 19.30 12 -6 -14 206.78 24.20 12 -6 -14 171.48 25.70 -12 -6 14 122.99 22.70 -14 6 16 53.79 18.10 -14 6 16 57.69 23.80 14 6 -16 18.30 24.20 14 6 -16 48.40 19.50 -14 6 16 10.30 17.90 14 -6 -16 9.10 17.50 -14 -6 16 81.29 21.40 -14 -6 16 9.60 22.40 -14 -6 16 25.70 21.60 -14 -6 16 36.60 20.10 14 -6 -16 51.29 22.70 -16 6 18 -7.50 22.60 16 6 -18 45.40 27.80 -16 6 18 -0.70 18.00 -16 -6 18 -15.10 18.60 -16 -6 18 23.40 23.30 -16 -6 18 -8.70 29.60 16 -6 -18 16.60 24.70 19 7 -17 42.50 29.40 -19 7 17 40.70 21.10 -19 7 17 0.30 18.90 19 -7 -17 5.70 24.80 -19 -7 17 9.80 20.50 -19 -7 17 18.40 22.10 17 7 -15 234.08 36.40 -17 7 15 321.67 33.60 -17 7 15 272.07 30.80 -17 7 15 244.58 38.30 -17 -7 15 251.17 37.10 17 -7 -15 212.08 32.40 17 -7 -15 217.88 32.00 -17 -7 15 197.18 29.10 17 -7 -15 222.78 28.60 -17 -7 15 305.77 33.70 -17 -7 15 271.87 33.60 15 7 -13 -26.10 13.20 -15 7 13 -10.40 13.80 -15 7 13 -24.60 19.10 15 7 -13 -4.70 18.50 -15 7 13 28.70 15.00 -15 -7 13 -10.70 12.90 15 -7 -13 7.40 10.70 15 -7 -13 9.50 19.70 -15 -7 13 -6.60 16.30 -15 -7 13 -0.40 16.20 -15 -7 13 24.70 16.90 15 -7 -13 -12.40 24.10 15 -7 -13 12.40 16.60 13 7 -11 46.80 13.70 -13 7 11 16.50 13.00 -13 7 11 46.60 14.40 13 7 -11 28.80 18.70 -13 7 11 42.70 18.00 13 -7 -11 18.80 9.80 -13 -7 11 24.30 15.30 -13 -7 11 16.60 15.60 13 -7 -11 8.60 15.90 13 -7 -11 48.30 14.30 -13 -7 11 35.80 15.80 13 -7 -11 32.60 14.80 -13 -7 11 16.70 13.30 -11 7 9 894.11 40.70 11 7 -9 925.01 40.30 -11 7 9 861.41 34.60 -11 7 9 884.81 40.30 11 7 -9 957.00 45.10 -11 7 9 924.41 43.20 11 -7 -9 948.31 40.90 11 -7 -9 911.11 40.30 11 -7 -9 906.31 35.10 -11 -7 9 906.71 43.00 -11 -7 9 952.60 44.00 11 -7 -9 889.01 43.60 -11 -7 9 954.10 43.90 -11 -7 9 911.11 41.10 -9 7 7 612.24 25.40 9 7 -7 594.64 31.90 -9 7 7 591.54 29.10 9 7 -7 567.54 28.10 -9 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27.50 14.50 -10 14 8 23.10 14.30 10 14 -8 16.00 16.30 -10 14 8 26.40 12.30 10 14 -8 20.00 15.50 -10 -14 8 33.80 15.00 -10 -14 8 -3.00 10.60 10 -14 -8 34.70 13.50 10 -14 -8 -4.10 13.00 10 -14 -8 25.00 12.70 10 -14 -8 38.20 15.80 -10 -14 8 32.40 14.90 -10 -14 8 32.90 14.10 -8 14 6 -7.10 12.20 8 14 -6 -10.90 13.20 -8 14 6 0.10 11.50 -8 14 6 -0.30 12.70 8 14 -6 -2.90 8.30 -8 14 6 -1.70 11.90 8 14 -6 -8.70 12.30 8 -14 -6 7.50 11.50 -8 -14 6 -4.00 9.00 -8 -14 6 8.60 11.90 -8 -14 6 -5.10 12.30 8 -14 -6 12.30 10.60 -8 -14 6 13.30 12.90 8 -14 -6 -4.40 11.50 -8 -14 6 -8.70 11.90 -6 14 4 900.51 39.70 6 14 -4 937.11 36.40 -6 14 4 931.01 36.80 6 14 -4 891.81 42.60 6 14 -4 957.10 37.40 -6 14 4 948.01 38.90 -6 14 4 853.91 40.00 6 -14 -4 889.71 36.30 -6 -14 4 998.30 42.30 -6 -14 4 918.31 36.70 -6 -14 4 955.70 41.00 6 -14 -4 964.40 39.50 6 -14 -4 923.91 39.30 6 -14 -4 951.80 38.80 4 14 -2 188.18 14.90 4 14 -2 200.28 22.10 -4 14 2 153.68 19.10 4 14 -2 164.88 20.20 -4 14 2 136.39 18.40 -4 14 2 182.48 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13.20 -10 -14 12 47.40 19.80 -10 -14 12 33.30 17.60 -10 -14 12 52.49 18.00 10 -14 -12 41.30 14.60 -10 -14 12 65.09 12.60 10 -14 -12 19.40 13.90 10 -14 -12 2.40 19.80 -12 14 14 223.38 31.50 12 14 -14 303.47 39.50 -12 14 14 234.48 35.40 -12 14 14 261.77 29.00 -12 -14 14 250.77 32.60 -12 -14 14 231.98 35.20 12 -14 -14 233.98 27.60 12 -14 -14 249.48 26.50 12 -14 -14 239.28 30.90 12 -14 -14 307.47 27.50 12 -14 -14 260.57 35.40 -12 -14 14 279.37 37.70 -14 14 16 6.40 27.20 -14 14 16 49.30 21.70 -14 14 16 42.40 20.60 14 14 -16 11.70 27.60 -14 -14 16 38.40 22.10 -14 -14 16 -18.10 25.40 14 -14 -16 35.80 19.00 -14 -14 16 -9.60 18.60 14 -14 -16 8.30 19.20 14 -14 -16 0.20 15.90 14 -14 -16 59.99 27.30 -17 15 15 73.29 23.30 -17 15 15 53.69 31.00 17 15 -15 74.19 32.80 -17 15 15 59.89 23.50 -17 -15 15 47.80 26.90 17 -15 -15 60.89 21.00 17 -15 -15 54.99 21.70 -17 -15 15 49.70 23.80 17 -15 -15 52.09 26.90 -17 -15 15 67.39 22.10 15 15 -13 55.49 23.40 -15 15 13 32.30 15.10 -15 15 13 55.79 20.00 -15 15 13 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17 13 16.10 24.10 15 17 -13 47.90 27.20 -15 17 13 42.60 20.80 -15 17 13 52.19 18.80 15 -17 -13 14.70 23.90 15 -17 -13 5.20 18.30 -15 -17 13 26.60 21.70 -15 -17 13 17.50 21.80 15 -17 -13 7.90 20.20 13 17 -11 -1.20 20.70 -13 17 11 30.60 15.70 -13 17 11 20.40 18.00 -13 17 11 3.70 19.60 -13 17 11 -15.50 16.90 -13 -17 11 0.80 19.20 13 -17 -11 -17.40 15.70 -13 -17 11 -11.50 16.10 13 -17 -11 -8.00 19.10 -13 -17 11 12.10 13.90 -13 -17 11 24.30 17.70 13 -17 -11 -6.20 16.50 13 -17 -11 -5.90 15.90 11 17 -9 11.20 16.50 -11 17 9 16.40 16.20 -11 17 9 7.50 12.40 -11 17 9 5.10 14.10 11 17 -9 -11.30 15.50 -11 17 9 36.60 17.00 11 -17 -9 5.40 16.20 11 -17 -9 11.30 14.50 -11 -17 9 18.40 15.10 -11 -17 9 22.00 15.30 11 -17 -9 26.40 14.30 11 -17 -9 -9.10 15.60 -11 -17 9 -7.60 12.40 -11 -17 9 23.30 17.50 -11 -17 9 39.30 16.20 -9 17 7 495.85 29.50 -9 17 7 437.96 32.00 9 17 -7 498.75 30.50 -9 17 7 498.55 32.10 -9 17 7 495.85 30.70 9 17 -7 449.86 37.00 9 17 -7 462.15 24.90 9 -17 -7 493.95 30.80 -9 -17 7 511.95 31.70 -9 -17 7 442.46 31.90 -9 -17 7 474.15 26.00 9 -17 -7 477.15 30.20 -9 -17 7 517.65 29.60 9 -17 -7 409.26 30.10 -9 -17 7 423.46 32.60 9 -17 -7 498.95 30.50 -7 17 5 103.09 16.50 7 17 -5 108.19 14.30 -7 17 5 89.09 17.20 -7 17 5 99.69 13.90 7 17 -5 96.29 13.80 -7 17 5 84.49 16.20 7 17 -5 86.49 18.10 -7 -17 5 86.99 14.10 -7 -17 5 92.99 14.30 7 -17 -5 87.29 16.00 7 -17 -5 69.79 14.10 7 -17 -5 90.89 16.70 -7 -17 5 109.39 18.10 7 -17 -5 94.69 13.80 -7 -17 5 101.39 17.20 5 17 -3 9.90 14.20 5 17 -3 -1.40 9.70 -5 17 3 -3.00 9.90 5 17 -3 -27.10 13.50 5 17 -3 10.80 9.70 -5 17 3 14.30 11.90 -5 17 3 -2.40 11.70 -5 -17 3 1.80 11.00 5 -17 -3 -8.00 10.90 5 -17 -3 -6.20 9.10 5 -17 -3 -3.10 11.40 -5 -17 3 -7.30 9.20 -5 -17 3 -17.20 11.50 3 17 -1 32.40 15.50 -3 17 1 38.00 13.10 3 17 -1 64.19 12.10 -3 17 1 35.80 13.30 -3 17 1 51.39 12.20 -3 -17 1 27.00 12.70 3 -17 -1 29.40 11.70 3 -17 -1 52.49 13.40 3 -17 -1 35.90 11.60 -3 -17 1 43.90 14.00 -3 -17 1 50.39 12.00 1 17 1 760.02 37.70 1 17 1 712.03 33.90 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7 767.92 39.20 5 -17 -7 752.82 34.80 -5 -17 7 838.42 35.10 5 -17 -7 737.83 37.00 7 17 -9 172.08 26.70 -7 17 9 140.59 18.30 7 17 -9 192.28 26.50 7 17 -9 204.68 18.20 -7 17 9 173.98 21.70 -7 17 9 173.28 23.90 7 -17 -9 182.88 22.50 -7 -17 9 168.18 25.40 7 -17 -9 176.18 21.90 -7 -17 9 171.88 25.80 7 -17 -9 194.88 20.90 -7 -17 9 145.79 21.60 -7 -17 9 198.78 21.70 7 -17 -9 207.38 23.90 -7 -17 9 192.28 24.90 9 17 -11 44.10 12.30 9 17 -11 21.10 20.30 -9 17 11 51.09 16.40 -9 17 11 56.09 18.80 9 17 -11 41.60 20.60 -9 17 11 19.80 15.70 9 -17 -11 44.40 15.40 9 -17 -11 56.79 18.30 9 -17 -11 35.60 15.70 -9 -17 11 67.19 14.20 9 -17 -11 26.20 18.10 -9 -17 11 18.00 18.40 -9 -17 11 16.80 15.20 -9 -17 11 33.00 16.40 11 17 -13 460.65 43.20 11 17 -13 398.76 23.80 -11 17 13 447.86 37.20 11 17 -13 338.87 43.00 -11 17 13 373.66 37.60 -11 17 13 494.35 35.20 11 -17 -13 471.65 40.60 11 -17 -13 446.16 32.70 -11 -17 13 460.95 38.90 -11 -17 13 487.25 28.60 11 -17 -13 451.45 34.40 -11 -17 13 374.26 36.60 11 -17 -13 424.06 36.20 11 -17 -13 409.86 32.50 -11 -17 13 378.66 36.40 -13 17 15 -11.10 19.10 13 17 -15 50.19 30.00 -13 17 15 35.90 19.70 -13 17 15 3.40 23.70 13 -17 -15 63.19 19.80 -13 -17 15 36.80 20.30 13 -17 -15 6.80 19.20 13 -17 -15 32.90 24.80 -13 -17 15 -12.70 24.90 13 -17 -15 37.40 35.00 16 18 -14 -15.80 27.00 -16 18 14 -55.49 24.60 -16 18 14 -6.50 18.80 -16 18 14 5.20 20.70 16 -18 -14 15.50 22.80 16 -18 -14 -21.60 26.50 16 -18 -14 19.50 21.30 -16 -18 14 -15.50 21.80 -16 -18 14 -3.20 20.90 -14 18 12 89.39 18.80 14 18 -12 61.49 26.10 -14 18 12 67.29 21.00 -14 18 12 51.19 25.70 -14 18 12 88.69 20.50 14 -18 -12 57.29 20.20 14 -18 -12 70.79 21.80 14 -18 -12 51.19 25.00 -14 -18 12 89.59 24.10 -14 -18 12 69.49 20.70 14 -18 -12 100.59 21.80 -14 -18 12 70.79 14.80 -14 -18 12 87.39 22.90 -14 -18 12 105.39 21.70 -12 18 10 3.50 17.80 -12 18 10 9.40 18.30 12 18 -10 -1.20 18.30 12 18 -10 -1.90 19.00 -12 18 10 8.80 13.90 -12 18 10 7.60 17.20 12 -18 -10 18.60 16.40 12 -18 -10 -27.50 16.70 -12 -18 10 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19.30 18.90 10 18 -12 40.90 21.70 -10 18 12 39.90 19.60 10 18 -12 1.10 11.60 10 -18 -12 23.60 17.10 -10 -18 12 49.00 16.20 -10 -18 12 9.10 18.30 -10 -18 12 6.00 17.90 10 -18 -12 12.10 16.50 -10 -18 12 -28.10 19.40 -10 -18 12 16.60 18.50 10 -18 -12 26.30 22.10 10 -18 -12 33.70 15.20 -12 18 14 163.28 28.50 -12 18 14 147.59 27.70 12 18 -14 231.28 21.10 12 18 -14 198.78 35.90 12 18 -14 318.17 42.20 12 -18 -14 155.58 27.90 12 -18 -14 235.48 31.60 12 -18 -14 214.78 43.60 -12 -18 14 157.88 27.90 -12 -18 14 214.28 25.00 -12 -18 14 175.08 30.00 12 -18 -14 279.97 32.60 14 -18 -16 -4.00 22.60 15 19 -13 73.29 28.40 -15 19 13 60.69 21.30 -15 19 13 47.70 23.00 -15 19 13 46.70 21.90 15 -19 -13 33.50 25.70 15 -19 -13 78.59 23.30 -15 -19 13 33.90 20.30 -15 -19 13 49.10 24.40 15 -19 -13 -7.80 22.40 13 19 -11 169.68 29.90 -13 19 11 148.49 25.00 13 19 -11 171.58 29.20 -13 19 11 104.49 24.00 -13 19 11 157.48 25.50 -13 -19 11 150.28 26.50 13 -19 -11 146.89 23.70 -13 -19 11 151.58 24.00 -13 -19 11 149.09 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14.80 8 20 -6 7.40 10.80 8 20 -6 29.60 19.40 8 20 -6 36.70 13.40 -8 20 6 29.50 16.30 8 -20 -6 28.30 15.40 8 -20 -6 25.90 15.00 -8 -20 6 36.20 13.80 -8 -20 6 17.90 20.40 -8 -20 6 28.20 13.30 -8 -20 6 24.20 14.20 8 -20 -6 10.10 14.00 -6 20 4 427.56 30.20 -6 20 4 539.95 31.10 6 20 -4 470.65 27.40 6 20 -4 478.35 36.70 -6 20 4 420.36 32.20 -6 -20 4 458.95 31.90 6 -20 -4 520.05 31.10 6 -20 -4 487.15 31.50 -6 -20 4 441.96 28.40 -6 -20 4 481.35 32.00 6 -20 -4 545.85 31.20 -4 20 2 43.70 13.60 4 20 -2 34.70 18.40 4 20 -2 40.30 17.60 -4 20 2 36.80 15.90 4 20 -2 42.00 12.40 -4 20 2 74.59 17.70 4 -20 -2 47.20 13.60 -4 -20 2 54.19 15.30 4 -20 -2 62.89 16.00 -4 -20 2 47.30 15.20 -4 -20 2 47.60 13.70 4 -20 -2 59.79 14.70 2 20 0 12.10 14.50 -2 20 0 51.59 17.20 -2 20 0 26.00 15.40 2 20 0 14.50 12.30 -2 20 0 15.50 12.50 2 20 0 33.40 16.00 2 -20 0 19.40 11.90 2 -20 0 24.90 14.10 -2 -20 0 16.70 13.90 -2 -20 0 25.20 14.50 2 -20 0 -7.40 12.30 -2 -20 0 40.70 15.00 0 20 -2 -5.10 14.70 0 20 2 12.40 12.90 0 20 2 10.30 10.70 0 20 -2 -11.50 11.00 0 20 -2 4.60 15.10 0 20 2 -5.70 14.70 0 -20 -2 17.90 13.00 0 -20 2 -3.30 13.30 0 -20 -2 5.00 11.70 0 -20 2 8.10 12.80 0 -20 -2 12.10 11.90 0 -20 2 1.00 13.30 2 20 -4 66.69 18.50 -2 20 4 80.19 14.50 2 20 -4 83.49 14.60 2 20 -4 71.59 19.50 -2 20 4 92.29 16.30 -2 20 4 55.99 14.90 2 -20 -4 68.69 14.50 2 -20 -4 74.29 14.40 -2 -20 4 79.69 17.90 -2 -20 4 83.39 17.70 -2 -20 4 77.79 15.60 2 -20 -4 72.39 15.80 4 20 -6 0.60 15.60 -4 20 6 17.40 10.20 -4 20 6 18.50 14.70 -4 20 6 18.00 12.80 4 20 -6 3.50 12.10 -4 20 6 14.20 12.80 -4 -20 6 19.90 14.90 -4 -20 6 3.20 14.50 4 -20 -6 19.30 13.30 4 -20 -6 18.00 11.40 4 -20 -6 1.80 12.90 -4 -20 6 15.50 14.50 -6 20 8 519.45 34.50 6 20 -8 566.24 41.20 -6 20 8 540.95 33.20 6 20 -8 555.74 30.80 -6 20 8 538.75 36.20 6 20 -8 560.94 29.40 -6 20 8 532.75 31.00 -6 -20 8 604.34 33.10 -6 -20 8 565.84 36.10 6 -20 -8 543.45 31.50 6 -20 -8 545.35 34.90 -6 -20 8 502.75 30.80 -6 -20 8 589.64 36.20 6 -20 -8 515.85 34.00 6 -20 -8 535.95 33.20 -6 -20 8 496.45 34.60 -8 20 10 32.90 16.50 8 20 -10 64.69 19.40 -8 20 10 48.80 18.80 -8 20 10 29.30 17.60 8 20 -10 71.59 22.50 8 20 -10 62.79 13.20 -8 -20 10 90.59 18.40 -8 -20 10 41.70 19.80 8 -20 -10 60.49 16.10 8 -20 -10 66.09 18.80 8 -20 -10 52.19 20.10 -8 -20 10 38.10 18.30 -8 -20 10 41.80 18.80 8 -20 -10 45.60 17.40 -8 -20 10 47.30 18.90 10 20 -12 23.40 23.90 -10 20 12 -17.10 17.00 10 20 -12 15.20 12.20 -10 20 12 14.50 20.10 10 20 -12 56.39 21.90 -10 20 12 -27.10 19.10 -10 -20 12 49.20 20.90 10 -20 -12 18.70 16.80 -10 -20 12 23.50 17.20 10 -20 -12 9.60 21.90 10 -20 -12 -3.80 20.30 -10 -20 12 -17.30 16.00 10 -20 -12 18.30 17.30 -10 -20 12 1.50 20.60 -10 -20 12 38.40 20.60 12 20 -14 2.40 27.40 12 20 -14 48.90 29.10 12 20 -14 18.90 12.60 -12 20 14 -28.00 21.40 -12 20 14 3.50 21.30 -12 20 14 -43.70 21.40 12 -20 -14 20.00 24.60 -12 -20 14 -27.40 18.70 12 -20 -14 -20.40 18.70 12 -20 -14 11.90 21.90 -12 -20 14 -19.10 25.50 12 -20 -14 40.70 21.90 -12 -20 14 34.60 18.20 -15 21 13 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25.00 16.00 9 -21 -7 4.50 14.30 -9 -21 7 10.50 17.20 -9 -21 7 1.10 14.20 -9 -21 7 15.00 15.10 -9 -21 7 31.70 14.70 9 -21 -7 -10.70 14.30 -9 -21 7 18.00 14.20 9 -21 -7 31.60 17.80 9 -21 -7 -3.50 13.70 -7 21 5 18.90 15.20 -7 21 5 17.60 14.90 7 21 -5 28.00 17.50 7 21 -5 12.80 11.40 -7 21 5 19.30 13.80 7 21 -5 5.90 11.60 7 -21 -5 32.40 16.00 7 -21 -5 22.30 14.90 7 -21 -5 32.10 14.20 -7 -21 5 12.20 13.70 -7 -21 5 31.50 14.70 -5 21 3 324.47 26.30 -5 21 3 309.17 28.40 -5 21 3 307.57 29.70 5 21 -3 255.87 31.70 5 21 -3 340.97 24.30 5 21 -3 338.67 31.70 -5 -21 3 311.47 28.60 5 -21 -3 293.47 25.80 -5 -21 3 357.26 25.60 5 -21 -3 287.27 27.10 -5 -21 3 326.57 27.90 5 -21 -3 334.67 27.40 -3 21 1 1505.35 64.79 3 21 -1 1503.65 65.49 3 21 -1 1613.24 60.69 -3 21 1 1590.64 61.39 3 21 -1 1593.24 65.89 -3 21 1 1567.64 64.59 3 -21 -1 1588.24 61.59 3 -21 -1 1548.35 61.89 -3 -21 1 1610.54 63.29 -3 -21 1 1588.74 61.29 -3 -21 1 1569.24 62.59 3 -21 -1 1653.73 63.19 -1 21 -1 49.00 18.30 1 21 1 47.60 13.10 -1 21 -1 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18.80 -7 21 9 -2.50 15.10 7 -21 -9 -15.50 13.60 -7 -21 9 4.20 17.80 -7 -21 9 27.20 16.30 -7 -21 9 -24.30 16.30 7 -21 -9 12.70 18.50 -7 -21 9 4.90 14.10 -7 -21 9 -24.40 15.00 7 -21 -9 4.20 16.30 7 -21 -9 20.50 17.50 -9 21 11 34.70 20.90 9 21 -11 97.19 23.40 -9 21 11 54.39 21.60 -9 21 11 50.49 18.20 9 21 -11 94.59 24.70 9 21 -11 91.59 15.90 -9 -21 11 70.99 19.50 9 -21 -11 75.99 17.90 9 -21 -11 88.79 20.90 -9 -21 11 44.60 20.80 9 -21 -11 100.99 22.80 -9 -21 11 60.49 19.20 9 -21 -11 87.49 24.20 -9 -21 11 75.49 21.50 -9 -21 11 72.39 20.90 11 21 -13 10.50 13.80 11 21 -13 2.40 24.70 -11 21 13 -17.00 20.70 11 21 -13 30.40 25.50 -11 21 13 -22.30 20.30 11 -21 -13 8.30 23.10 -11 -21 13 38.00 17.60 11 -21 -13 20.40 21.40 -11 -21 13 -36.50 23.90 11 -21 -13 -4.90 18.80 -11 -21 13 1.80 19.40 -14 22 12 -33.20 21.80 -14 22 12 -11.30 23.00 -14 22 12 26.60 22.20 14 22 -12 -53.79 23.70 -14 22 12 63.39 21.80 14 22 -12 -16.70 26.70 -14 -22 12 2.20 22.40 -14 -22 12 -0.60 18.20 14 -22 -12 -25.20 23.70 14 -22 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21.10 17.30 -6 22 4 222.48 27.60 6 22 -4 267.57 21.90 -6 22 4 257.87 28.60 6 22 -4 258.67 33.20 6 22 -4 206.08 32.40 -6 -22 4 309.47 28.40 -6 -22 4 269.47 25.10 6 -22 -4 251.67 25.60 6 -22 -4 222.78 31.70 -6 -22 4 243.38 32.60 6 -22 -4 235.28 27.80 -4 22 2 79.69 19.20 4 22 -2 90.19 21.10 -4 22 2 75.29 14.40 4 22 -2 94.29 20.80 -4 22 2 69.09 18.00 4 22 -2 133.29 20.20 4 -22 -2 92.29 17.60 -4 -22 2 104.99 17.00 -4 -22 2 119.99 18.40 4 -22 -2 89.69 16.80 -4 -22 2 98.79 18.30 4 -22 -2 83.99 16.20 -2 22 0 37.70 13.40 -2 22 0 33.30 17.80 2 22 0 29.90 17.10 2 22 0 75.79 14.30 -2 22 0 59.69 18.20 2 22 0 47.80 16.50 -2 -22 0 26.80 13.90 2 -22 0 40.80 13.80 2 -22 0 49.50 16.40 2 -22 0 36.70 13.90 -2 -22 0 81.59 17.40 -2 -22 0 54.89 15.40 0 22 2 180.78 22.00 0 22 -2 205.08 29.60 0 22 2 212.68 27.80 0 22 -2 235.08 23.20 0 22 2 206.38 26.90 0 22 -2 203.48 29.10 0 -22 -2 206.38 24.40 0 -22 2 187.08 24.30 0 -22 2 158.58 24.00 0 -22 2 206.28 25.10 0 -22 -2 222.18 24.90 0 -22 -2 212.88 23.10 -2 22 4 4.70 15.10 2 22 -4 10.30 17.20 -2 22 4 14.00 12.40 -2 22 4 7.40 14.60 2 22 -4 5.50 17.10 2 22 -4 5.00 11.80 2 -22 -4 18.60 12.20 -2 -22 4 12.90 15.70 -2 -22 4 44.30 14.20 2 -22 -4 9.60 12.80 2 -22 -4 17.70 15.40 -2 -22 4 25.20 15.70 4 22 -6 114.79 17.10 -4 22 6 119.39 14.60 -4 22 6 91.99 19.20 4 22 -6 87.79 23.50 -4 22 6 102.59 20.00 -4 22 6 139.09 19.10 4 -22 -6 102.19 21.00 -4 -22 6 176.88 26.00 -4 -22 6 80.29 16.60 4 -22 -6 99.99 17.10 -4 -22 6 115.09 19.40 4 -22 -6 125.59 20.10 6 22 -8 166.58 21.80 -6 22 8 140.39 23.60 6 22 -8 181.48 19.40 -6 22 8 154.38 21.10 -6 22 8 125.89 16.80 6 22 -8 129.29 25.80 -6 22 8 140.19 23.10 6 -22 -8 139.29 21.40 -6 -22 8 154.98 21.90 -6 -22 8 148.59 22.50 6 -22 -8 155.78 21.80 -6 -22 8 111.19 21.30 6 -22 -8 147.09 18.90 6 -22 -8 141.99 21.80 -6 -22 8 134.39 23.40 -8 22 10 1.60 15.20 8 22 -10 45.30 21.40 8 22 -10 14.10 13.60 -8 22 10 -7.10 17.70 8 22 -10 -18.50 18.30 -8 22 10 18.10 19.60 8 -22 -10 -7.90 19.40 -8 -22 10 -24.00 17.50 8 -22 -10 23.50 18.90 8 -22 -10 16.30 19.20 -8 -22 10 1.00 18.80 -8 -22 10 -3.10 18.60 -8 -22 10 13.50 16.00 8 -22 -10 -1.90 14.00 -8 -22 10 26.70 18.80 10 22 -12 -9.30 25.20 10 22 -12 31.10 15.20 -10 22 12 -16.70 20.70 10 22 -12 -4.50 24.50 -10 22 12 -40.70 20.10 -10 22 12 -39.90 19.50 -10 -22 12 -6.90 17.60 -10 -22 12 6.10 18.10 -10 -22 12 -29.60 19.60 10 -22 -12 2.90 20.50 10 -22 -12 4.10 20.70 10 -22 -12 7.60 18.70 12 22 -14 64.99 30.30 -12 22 14 -36.90 23.00 -12 22 14 36.90 24.30 12 22 -14 21.30 28.70 -12 22 14 -7.80 22.00 12 22 -14 10.00 12.40 12 -22 -14 6.30 23.10 -12 -22 14 -27.40 26.60 12 -22 -14 2.10 23.80 -12 -22 14 18.70 19.40 12 -22 -14 66.09 27.00 12 -22 -14 -17.80 20.90 -12 -22 14 21.70 19.30 -13 23 11 16.70 22.20 -13 23 11 34.10 23.20 13 23 -11 29.60 26.20 13 23 -11 42.70 23.90 -13 23 11 -7.00 21.20 -13 23 11 -2.80 21.00 -13 -23 11 49.10 21.50 -13 -23 11 13.50 19.80 13 -23 -11 35.70 23.00 13 -23 -11 13.10 22.20 13 -23 -11 12.40 19.70 -13 -23 11 56.99 20.70 -11 23 9 51.49 22.90 -11 23 9 57.59 18.50 11 23 -9 127.19 25.40 11 23 -9 90.69 26.80 -11 23 9 53.79 23.90 -11 23 9 87.59 20.10 11 -23 -9 45.30 20.90 11 -23 -9 119.89 23.90 11 -23 -9 106.29 23.10 -11 -23 9 59.39 18.00 11 -23 -9 102.69 21.30 -11 -23 9 82.49 19.50 -11 -23 9 90.39 21.70 -11 -23 9 98.09 26.00 -11 -23 9 57.89 20.80 9 23 -7 34.10 13.90 9 23 -7 31.30 21.80 -9 23 7 -31.10 13.60 -9 23 7 3.90 17.20 -9 23 7 23.10 18.10 9 23 -7 -9.20 15.20 -9 23 7 5.60 17.30 9 -23 -7 13.00 16.40 9 -23 -7 -11.90 16.10 9 -23 -7 33.40 18.30 9 -23 -7 -8.90 15.60 -9 -23 7 -11.10 15.30 -9 -23 7 11.60 14.60 -9 -23 7 32.20 16.10 -9 -23 7 15.30 19.10 -9 -23 7 11.70 15.40 7 23 -5 28.00 18.70 -7 23 5 2.00 15.70 -7 23 5 -3.40 15.00 -7 23 5 -13.30 15.00 7 23 -5 11.30 11.90 -7 -23 5 5.10 15.00 7 -23 -5 24.70 16.70 -7 -23 5 4.10 14.10 7 -23 -5 -9.50 13.40 -7 -23 5 50.39 17.60 7 -23 -5 -7.60 18.30 -5 23 3 22.60 16.70 5 23 -3 27.00 18.40 -5 23 3 -3.20 16.00 5 23 -3 33.50 19.20 -5 23 3 25.90 16.10 5 23 -3 39.90 12.80 5 -23 -3 0.20 14.40 -5 -23 3 22.60 15.20 5 -23 -3 36.10 17.60 -5 -23 3 41.40 16.20 5 -23 -3 23.80 15.00 -5 -23 3 28.50 15.00 3 23 -1 39.20 16.90 -3 23 1 13.10 16.80 3 23 -1 49.90 13.80 -3 23 1 46.90 17.90 3 23 -1 57.19 18.70 -3 -23 1 43.70 15.20 3 -23 -1 16.30 14.80 3 -23 -1 40.10 13.80 -3 -23 1 40.90 17.00 1 23 1 74.39 18.60 -1 23 -1 80.99 19.90 1 23 1 74.39 15.10 1 23 1 66.99 19.00 -1 23 -1 81.69 16.00 -1 23 -1 81.59 20.50 -1 -23 -1 93.09 18.40 -1 -23 -1 80.49 19.30 1 -23 1 98.69 20.80 1 -23 1 81.29 17.80 1 -23 1 95.19 18.20 -1 -23 -1 92.39 17.10 1 23 -3 150.68 25.00 1 23 -3 135.69 23.40 -1 23 3 150.08 23.10 -1 23 3 196.88 27.10 -1 23 3 187.68 28.40 1 23 -3 144.09 22.10 1 -23 -3 162.38 24.30 -1 -23 3 206.28 37.10 -1 -23 3 133.59 23.60 1 -23 -3 155.88 22.20 1 -23 -3 156.08 25.10 -1 -23 3 184.88 25.20 3 23 -5 240.58 34.20 3 23 -5 292.27 25.80 -3 23 5 249.38 28.70 3 23 -5 239.68 33.10 -3 23 5 239.58 26.50 -3 23 5 241.68 26.80 3 -23 -5 185.08 26.80 3 -23 -5 258.47 24.70 -3 -23 5 286.67 29.20 3 -23 -5 264.27 29.30 -3 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34.70 19.20 0 24 2 40.90 15.40 0 24 2 46.10 18.60 0 24 2 71.49 19.50 0 -24 2 26.80 13.30 0 -24 -2 61.49 15.40 0 -24 -2 35.80 15.70 0 -24 2 8.30 16.60 0 -24 2 28.80 17.70 0 -24 -2 49.40 16.20 -2 24 4 -5.10 14.40 -2 24 4 -20.70 15.10 2 24 -4 23.40 14.40 2 24 -4 -17.50 18.80 2 24 -4 -3.80 18.20 -2 24 4 22.00 15.10 2 -24 -4 -14.90 14.40 -2 -24 4 -0.10 14.60 -2 -24 4 17.50 16.30 -2 -24 4 16.20 15.10 2 -24 -4 -12.80 13.90 2 -24 -4 -11.40 12.50 4 24 -6 85.59 16.00 -4 24 6 104.19 21.50 -4 24 6 96.49 18.80 4 24 -6 60.09 23.50 -4 24 6 81.29 21.00 4 -24 -6 61.09 17.30 4 -24 -6 102.89 20.30 -4 -24 6 110.89 22.10 -4 -24 6 97.79 20.90 -4 -24 6 129.19 20.80 4 -24 -6 70.69 16.60 -6 24 8 -8.30 13.40 -6 24 8 11.10 18.10 6 24 -8 20.20 21.40 6 24 -8 24.90 15.00 -6 24 8 -11.70 17.60 -6 24 8 14.90 17.60 -6 -24 8 -5.80 17.30 6 -24 -8 -8.50 13.80 -6 -24 8 -13.00 15.40 -6 -24 8 -12.70 16.80 -6 -24 8 -21.90 17.30 6 -24 -8 10.70 17.00 6 -24 -8 -3.80 18.00 6 -24 -8 -32.60 16.90 -8 24 10 -6.80 16.20 8 24 -10 0.30 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66.99 23.50 -16 -16 12 96.19 31.30 16 -16 -12 100.29 25.60 -16 -16 12 112.49 24.50 -14 16 10 24.80 18.40 -14 16 10 19.80 15.60 14 16 -10 4.10 19.90 -14 16 10 18.20 17.10 -14 16 10 12.80 15.20 14 -16 -10 34.60 19.60 -14 -16 10 12.10 10.80 -14 -16 10 8.60 15.40 -14 -16 10 6.30 12.60 -14 -16 10 29.70 18.90 -14 -16 10 29.50 19.40 14 -16 -10 -7.20 15.40 14 -16 -10 52.49 20.10 14 -16 -10 17.10 16.50 -12 16 8 5.50 13.60 -12 16 8 24.10 15.50 -12 16 8 0.30 13.60 -12 16 8 10.00 15.10 12 16 -8 12.30 17.50 12 16 -8 -10.10 15.40 12 -16 -8 6.60 13.50 -12 -16 8 5.30 13.70 12 -16 -8 -0.80 15.80 -12 -16 8 11.30 13.70 12 -16 -8 2.30 13.90 12 -16 -8 21.20 15.70 -12 -16 8 -16.70 14.60 -12 -16 8 -6.60 9.20 -12 -16 8 1.00 12.10 -10 16 6 262.57 26.20 -10 16 6 278.77 24.60 10 16 -6 252.37 29.40 -10 16 6 248.38 27.60 10 16 -6 305.27 26.20 10 -16 -6 271.77 25.60 10 -16 -6 257.57 23.70 -10 -16 6 290.07 24.30 -10 -16 6 260.77 19.70 -10 -16 6 266.47 27.50 -10 -16 6 280.47 25.40 -10 -16 6 268.97 27.70 10 -16 -6 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15 3 -10 70.89 19.80 -15 3 10 110.39 20.00 15 3 -10 96.29 16.80 -15 -3 10 103.59 19.80 -15 -3 10 84.39 16.70 15 -3 -10 90.39 20.60 15 -3 -10 123.89 17.10 15 -3 -10 116.49 19.50 -15 -3 10 97.59 18.10 -13 3 8 131.19 19.40 -13 3 8 135.39 20.10 -13 3 8 116.69 11.50 13 3 -8 133.99 18.50 13 3 -8 129.79 19.20 13 3 -8 118.99 21.10 -13 -3 8 165.18 25.30 13 -3 -8 151.78 19.00 13 -3 -8 105.29 12.60 -13 -3 8 139.79 18.80 -13 -3 8 131.09 18.30 13 -3 -8 125.79 20.30 11 3 -6 185.88 27.70 -11 3 6 206.38 19.40 -11 3 6 214.28 14.30 -11 3 6 216.38 17.70 11 3 -6 180.98 22.90 11 3 -6 235.08 19.90 -11 3 6 223.88 21.30 11 -3 -6 184.68 22.50 11 -3 -6 199.68 15.00 -11 -3 6 208.48 21.80 11 -3 -6 243.78 19.10 -11 -3 6 239.98 20.10 -11 -3 6 218.38 17.50 -9 3 4 28.30 10.40 9 3 -4 40.10 13.80 9 3 -4 41.10 8.60 -9 3 4 45.70 9.60 9 3 -4 54.19 7.50 -9 3 4 60.79 9.10 9 3 -4 50.99 11.00 -9 3 4 68.59 9.50 -9 -3 4 40.10 8.70 9 -3 -4 54.49 9.10 9 -3 -4 60.29 8.70 -9 -3 4 58.99 13.60 9 -3 -4 54.49 10.00 -9 -3 4 65.79 8.70 -9 -3 4 30.80 14.50 -7 3 2 618.14 23.50 7 3 -2 637.04 24.00 7 3 -2 634.24 24.20 -7 3 2 588.74 26.20 7 3 -2 616.44 28.40 -7 3 2 601.24 24.90 7 3 -2 656.43 26.50 -7 3 2 601.64 27.90 -7 -3 2 613.54 26.10 7 -3 -2 604.04 26.20 -7 -3 2 647.34 23.50 -7 -3 2 613.04 23.90 7 -3 -2 616.84 23.60 -7 -3 2 625.04 28.40 7 -3 -2 589.94 27.30 7 -3 -2 567.94 24.80 -5 3 0 1969.20 61.79 -5 3 0 1919.81 64.29 -5 3 0 1981.40 64.59 5 3 0 1922.31 64.29 5 3 0 2012.50 63.99 -5 3 0 1941.11 64.99 -5 -3 0 1984.10 63.99 -5 -3 0 2017.80 63.09 -5 -3 0 1986.00 63.69 5 -3 0 1978.00 65.19 5 -3 0 1965.40 64.49 5 -3 0 1977.70 61.59 -5 -3 0 1994.40 65.79 5 -3 0 1973.60 64.29 -3 3 -2 20.50 7.00 3 3 2 20.20 5.90 -3 3 -2 28.10 7.70 3 3 2 30.30 8.60 3 3 2 22.00 8.40 -3 3 -2 19.60 7.60 3 -3 2 18.50 6.60 -3 -3 -2 23.70 8.00 -3 -3 -2 29.20 4.70 -3 -3 -2 31.60 8.20 3 -3 2 29.60 8.60 -3 -3 -2 24.50 5.40 3 -3 2 21.50 5.10 3 -3 2 27.10 8.00 1 3 4 297.37 14.90 -1 3 -4 304.67 16.30 -1 3 -4 295.17 18.00 -1 3 -4 313.87 14.70 -1 3 -4 274.87 16.00 1 3 4 287.27 18.40 1 3 4 306.07 17.50 1 -3 4 281.57 17.50 1 -3 4 287.67 14.50 -1 -3 -4 302.27 19.10 1 -3 4 298.27 16.50 -1 -3 -4 300.67 14.90 1 -3 4 287.17 15.60 -1 -3 -4 319.27 17.00 -1 3 6 16.50 8.70 -1 3 6 12.30 8.50 -1 3 6 13.40 7.90 1 3 -6 8.70 9.80 1 3 -6 16.60 8.30 1 3 -6 25.50 7.50 1 3 -6 8.70 7.00 -1 3 6 10.80 4.50 -1 -3 6 15.60 7.40 -1 -3 6 16.40 7.70 -1 -3 6 6.00 7.00 1 -3 -6 11.40 7.30 1 -3 -6 10.60 7.60 1 -3 -6 5.40 10.30 -1 -3 6 14.60 9.00 3 3 -8 390.06 21.00 3 3 -8 379.36 17.80 -3 3 8 378.06 17.10 -3 3 8 360.56 20.20 3 3 -8 379.06 25.20 3 3 -8 364.76 20.50 -3 3 8 352.86 20.70 -3 3 8 361.76 23.20 3 -3 -8 354.86 20.30 -3 -3 8 398.56 19.30 -3 -3 8 401.36 21.20 -3 -3 8 358.76 21.00 3 -3 -8 358.06 25.40 3 -3 -8 363.56 19.20 5 3 -10 10.90 16.80 -5 3 10 27.50 10.20 5 3 -10 20.50 10.70 5 3 -10 -6.30 7.80 -5 3 10 6.00 11.00 -5 3 10 23.50 8.00 -5 3 10 15.00 12.60 -5 -3 10 11.60 11.50 -5 -3 10 14.00 14.10 5 -3 -10 17.60 16.00 5 -3 -10 10.50 10.00 -5 -3 10 17.30 10.60 -5 -3 10 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13.50 -11 5 6 70.79 12.40 -11 5 6 80.39 13.60 11 5 -6 93.59 12.80 11 5 -6 81.59 16.40 -11 5 6 85.09 10.20 -11 -5 6 91.49 13.20 -11 -5 6 62.89 13.50 11 -5 -6 73.09 17.10 11 -5 -6 92.89 12.40 11 -5 -6 92.79 13.40 -11 -5 6 74.19 15.60 11 -5 -6 86.09 11.30 9 5 -4 343.97 19.00 -9 5 4 361.46 20.80 9 5 -4 378.56 16.90 9 5 -4 345.27 23.90 -9 5 4 326.67 18.10 -9 5 4 339.47 18.80 -9 5 4 346.37 22.20 -9 -5 4 371.56 19.50 9 -5 -4 357.26 18.90 -9 -5 4 380.46 23.50 -9 -5 4 357.76 16.20 9 -5 -4 315.07 24.20 9 -5 -4 354.06 20.70 9 -5 -4 322.47 18.00 -9 -5 4 372.56 21.80 -7 5 2 2118.19 71.69 -7 5 2 2016.60 69.09 -7 5 2 2081.39 71.59 7 5 -2 2197.28 73.19 7 5 -2 2161.98 69.49 -7 5 2 2093.59 70.09 -7 -5 2 2188.68 69.29 7 -5 -2 2004.00 69.99 7 -5 -2 2164.18 69.29 7 -5 -2 2015.10 71.59 7 -5 -2 2144.39 71.69 -7 -5 2 2324.37 70.79 -7 -5 2 2273.97 71.99 -7 -5 2 2227.68 72.89 -5 5 0 182.68 11.90 -5 5 0 185.88 16.50 5 5 0 212.98 14.10 5 5 0 213.08 14.80 -5 5 0 161.08 15.20 -5 5 0 188.38 14.90 5 -5 0 147.19 16.50 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25.50 10.00 -1 13 -5 21.70 12.20 1 13 5 23.00 11.50 -1 13 -5 19.60 10.20 -1 13 -5 27.40 11.00 1 13 5 25.40 8.50 -1 -13 -5 11.70 11.20 -1 -13 -5 20.30 7.60 -1 -13 -5 18.50 11.80 1 -13 5 16.90 7.60 -1 -13 -5 5.30 10.20 1 -13 5 12.90 11.20 1 -13 5 17.40 11.00 -1 -13 -5 17.30 10.30 1 -13 5 11.20 12.00 -1 13 7 2610.94 89.49 1 13 -7 2618.74 86.69 -1 13 7 2529.45 83.89 1 13 -7 2551.04 91.99 1 13 -7 2512.85 86.49 -1 -13 7 2581.34 85.49 1 -13 -7 2604.04 89.49 -1 -13 7 2653.33 89.99 -1 -13 7 2596.44 87.39 -1 -13 7 2609.44 89.99 1 -13 -7 2538.05 88.19 1 -13 -7 2560.04 83.39 -1 -13 7 2475.85 88.19 1 -13 -7 2450.45 88.59 1 -13 -7 2710.33 88.59 -3 13 9 173.28 22.70 3 13 -9 169.48 18.30 -3 13 9 167.28 23.30 3 13 -9 118.69 20.30 -3 13 9 179.48 14.50 3 13 -9 187.28 24.90 -3 -13 9 189.38 20.50 3 -13 -9 184.08 15.30 3 -13 -9 159.08 20.70 -3 -13 9 180.28 21.00 3 -13 -9 176.38 21.20 3 -13 -9 177.98 21.30 -3 -13 9 169.38 20.90 -3 -13 9 213.88 22.00 3 -13 -9 157.08 20.10 -5 13 11 144.39 20.40 5 13 -11 120.09 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-24.90 18.60 11 -13 -17 30.90 17.70 11 -13 -17 -15.80 25.60 -11 -13 17 -8.10 19.10 11 -13 -17 -2.50 17.30 -11 -13 17 -9.40 26.20 -20 14 14 4.10 23.30 -20 14 14 32.40 22.60 20 14 -14 -18.10 28.60 -20 -14 14 0.00 21.50 20 -14 -14 -4.40 16.00 -20 -14 14 -14.00 20.20 20 -14 -14 -19.80 24.00 18 14 -12 87.09 28.50 -18 14 12 48.70 18.20 -18 14 12 57.99 23.00 -18 14 12 33.00 20.40 -18 14 12 36.50 22.90 18 -14 -12 40.50 18.30 -18 -14 12 111.59 25.10 -18 -14 12 50.69 20.90 18 -14 -12 29.10 24.80 -18 -14 12 92.69 23.40 18 -14 -12 38.30 21.10 18 -14 -12 45.20 21.10 -16 14 10 194.58 25.50 -16 14 10 160.28 23.60 16 14 -10 194.38 29.30 -16 14 10 224.88 24.40 -16 14 10 171.08 24.40 16 -14 -10 213.18 25.30 16 -14 -10 215.48 31.50 16 -14 -10 180.18 26.80 -16 -14 10 208.18 29.90 16 -14 -10 230.28 26.20 -16 -14 10 251.07 32.50 -16 -14 10 263.57 32.00 -16 -14 10 142.49 24.30 -14 14 8 132.19 19.30 14 14 -8 116.69 22.00 -14 14 8 162.78 25.20 -14 14 8 157.68 21.00 -14 14 8 140.49 20.80 14 -14 -8 104.29 18.70 -14 -14 8 136.19 21.00 -14 -14 8 144.29 21.40 -14 -14 8 147.59 21.50 -14 -14 8 125.49 20.40 14 -14 -8 96.59 20.30 -14 -14 8 136.09 15.90 14 -14 -8 137.89 20.20 -14 -14 8 120.49 14.80 -12 14 6 3.20 12.30 12 14 -6 -20.30 15.60 -12 14 6 -1.20 12.60 -12 14 6 3.10 13.40 -12 14 6 -11.50 12.20 12 -14 -6 -10.00 14.20 12 -14 -6 -9.50 11.60 -12 -14 6 -2.70 9.30 -12 -14 6 -14.60 13.60 -12 -14 6 -10.00 9.80 12 -14 -6 17.00 13.50 -12 -14 6 -18.10 12.60 -12 -14 6 7.10 14.40 12 -14 -6 2.00 14.70 -12 -14 6 -8.50 12.60 -10 14 4 413.86 29.70 10 14 -4 398.26 32.60 -10 14 4 405.46 24.80 10 14 -4 413.66 29.30 -10 14 4 418.26 27.30 -10 14 4 430.86 26.00 10 -14 -4 465.25 29.60 -10 -14 4 466.95 30.10 -10 -14 4 375.56 34.70 -10 -14 4 414.66 27.40 -10 -14 4 422.36 28.80 10 -14 -4 388.46 26.20 -10 -14 4 421.16 28.50 -10 -14 4 465.85 24.40 10 -14 -4 385.06 25.60 -8 14 2 2518.65 89.59 -8 14 2 2613.64 87.59 8 14 -2 2433.86 90.09 -8 14 2 2539.35 87.99 -8 14 2 2555.94 84.49 -8 -14 2 2589.84 87.09 8 -14 -2 2498.65 84.59 8 -14 -2 2618.74 86.69 8 -14 -2 2533.95 88.59 8 -14 -2 2694.53 89.19 -8 -14 2 2562.44 86.79 -8 -14 2 2513.55 89.29 -8 -14 2 2556.94 89.29 -8 -14 2 2492.95 87.19 -6 14 0 12.80 12.20 -6 14 0 22.50 12.50 6 14 0 59.89 13.50 6 14 0 32.10 14.90 -6 14 0 28.30 11.80 -6 -14 0 48.70 11.90 -6 -14 0 21.30 12.10 -6 -14 0 38.40 11.10 -6 -14 0 33.60 10.40 -6 -14 0 27.90 11.50 -6 -14 0 26.50 11.80 6 -14 0 34.80 14.30 6 -14 0 40.40 11.40 -4 14 -2 2004.00 71.39 -4 14 -2 2020.40 69.99 -4 14 -2 1974.90 72.49 4 14 2 1969.20 71.79 4 14 2 1978.50 69.29 -4 -14 -2 2058.39 71.29 4 -14 2 1974.40 70.59 -4 -14 -2 2039.90 68.69 4 -14 2 1843.72 72.79 -4 -14 -2 1960.50 70.49 -4 -14 -2 1939.71 67.89 -4 -14 -2 2105.89 70.99 4 -14 2 2055.89 71.19 2 14 4 162.18 17.10 2 14 4 176.78 16.30 2 14 4 177.38 20.60 -2 14 -4 142.19 20.70 -2 14 -4 176.98 21.90 -2 14 -4 185.18 18.60 -2 -14 -4 187.58 14.80 -2 -14 -4 194.78 19.30 2 -14 4 168.88 21.00 2 -14 4 194.48 19.40 2 -14 4 145.49 18.40 -2 -14 -4 204.98 19.80 -2 -14 -4 183.08 19.00 -2 -14 -4 144.69 18.90 0 14 -6 173.28 17.60 0 14 -6 166.18 23.50 0 14 6 154.78 22.40 0 14 6 168.68 16.20 0 14 -6 192.48 19.20 0 -14 6 203.58 21.50 0 -14 -6 174.78 20.80 0 -14 -6 213.58 20.90 0 -14 6 207.48 21.20 0 -14 -6 182.18 15.30 0 -14 -6 198.68 20.50 0 -14 6 205.98 20.40 0 -14 6 166.28 15.50 0 -14 -6 182.98 20.20 0 -14 6 165.08 18.30 2 14 -8 199.18 18.50 2 14 -8 193.78 23.30 2 14 -8 198.38 24.10 -2 14 8 183.78 23.70 -2 14 8 227.88 22.50 -2 14 8 212.58 15.80 -2 -14 8 202.08 21.50 -2 -14 8 188.58 19.80 -2 -14 8 216.28 22.90 2 -14 -8 222.98 27.80 -2 -14 8 215.28 23.00 2 -14 -8 177.98 21.00 -2 -14 8 214.18 22.20 2 -14 -8 229.48 16.50 2 -14 -8 214.08 22.10 2 -14 -8 208.68 21.10 -4 14 10 163.58 21.20 4 14 -10 152.08 17.10 -4 14 10 173.68 25.60 4 14 -10 193.98 26.60 -4 14 10 145.19 17.00 4 14 -10 172.18 23.40 4 -14 -10 171.98 22.20 -4 -14 10 172.48 22.10 -4 -14 10 147.79 19.00 -4 -14 10 129.29 19.00 4 -14 -10 145.29 20.90 4 -14 -10 144.89 19.40 4 -14 -10 165.28 17.00 -4 -14 10 150.48 22.10 4 -14 -10 166.18 21.40 -6 14 12 308.37 29.50 6 14 -12 277.77 20.70 6 14 -12 304.47 36.10 -6 14 12 299.47 22.80 6 14 -12 276.17 32.70 -6 14 12 280.17 31.70 6 -14 -12 304.87 25.80 6 -14 -12 304.27 34.90 6 -14 -12 266.07 27.20 -6 -14 12 314.07 24.60 6 -14 -12 264.67 24.30 -6 -14 12 240.98 30.40 -6 -14 12 303.67 30.10 -6 -14 12 264.47 27.80 6 -14 -12 268.07 24.80 8 14 -14 124.89 25.80 8 14 -14 132.39 26.00 -8 14 14 140.79 26.00 8 14 -14 106.39 13.90 8 14 -14 178.28 24.10 -8 14 14 160.68 22.60 -8 14 14 128.49 22.20 -8 -14 14 202.68 30.20 -8 -14 14 133.49 22.20 8 -14 -14 108.39 23.30 8 -14 -14 97.39 18.30 -8 -14 14 127.49 26.10 -8 -14 14 110.29 19.10 8 -14 -14 148.09 19.80 8 -14 -14 99.39 25.10 8 -14 -14 120.99 16.90 -10 14 16 -18.50 17.90 10 14 -16 -7.20 24.20 -10 14 16 -2.70 23.10 -10 14 16 -28.00 21.50 -10 -14 16 -9.70 24.00 -10 -14 16 -10.20 16.00 -10 -14 16 8.50 18.90 -10 -14 16 -26.90 19.40 10 -14 -16 -3.60 22.20 10 -14 -16 -19.60 14.50 10 -14 -16 -14.50 16.60 10 -14 -16 0.10 16.50 -19 15 13 -46.70 23.00 -19 15 13 11.20 20.30 -19 15 13 30.10 19.10 -19 15 13 -14.40 23.00 19 15 -13 20.00 29.80 -19 -15 13 -34.70 17.70 19 -15 -13 -27.30 16.50 19 -15 -13 -30.30 25.30 -19 -15 13 12.30 21.00 -19 -15 13 46.80 29.80 -17 15 11 27.20 20.30 -17 15 11 21.70 19.40 -17 15 11 35.10 19.60 17 15 -11 30.80 24.90 -17 15 11 0.60 16.00 17 -15 -11 84.29 20.70 -17 -15 11 -16.50 17.50 17 -15 -11 28.60 19.80 -17 -15 11 52.19 22.80 17 -15 -11 -17.90 23.10 17 -15 -11 -10.70 18.00 -17 -15 11 6.00 20.80 -17 -15 11 7.90 21.10 -15 15 9 14.20 15.60 -15 15 9 -3.60 15.70 -15 15 9 13.90 16.50 15 15 -9 -20.50 18.90 -15 15 9 -1.40 15.70 15 -15 -9 -11.70 17.90 -15 -15 9 3.50 15.60 -15 -15 9 29.80 16.90 15 -15 -9 -9.20 17.30 15 -15 -9 -4.20 14.60 -15 -15 9 17.50 9.50 -15 -15 9 -8.80 15.20 -15 -15 9 -12.00 15.50 15 -15 -9 13.60 14.10 -15 -15 9 -8.70 9.20 -13 15 7 47.50 15.20 -13 15 7 53.19 17.20 13 15 -7 60.39 17.90 -13 15 7 63.79 15.70 -13 15 7 40.30 13.80 13 -15 -7 59.99 17.80 -13 -15 7 32.40 15.50 13 -15 -7 41.10 16.60 13 -15 -7 32.70 13.00 -13 -15 7 23.10 10.40 -13 -15 7 28.50 16.30 -13 -15 7 22.50 11.00 13 -15 -7 43.40 16.10 -13 -15 7 44.60 15.60 -13 -15 7 31.50 16.20 11 15 -5 289.97 28.50 -11 15 5 324.87 28.00 -11 15 5 271.47 23.90 -11 15 5 259.37 25.80 -11 15 5 276.27 25.40 11 15 -5 301.87 32.30 -11 -15 5 265.47 27.10 -11 -15 5 283.87 26.10 -11 -15 5 332.27 26.40 -11 -15 5 286.27 27.50 -11 -15 5 248.58 21.50 -11 -15 5 258.87 21.00 11 -15 -5 286.47 24.40 11 -15 -5 301.37 27.20 11 -15 -5 262.07 23.90 11 -15 -5 294.27 23.10 -9 15 3 162.28 23.60 -9 15 3 141.49 18.60 9 15 -3 143.69 20.90 -9 15 3 144.09 17.60 9 15 -3 143.89 22.20 -9 15 3 148.09 17.30 9 -15 -3 142.69 18.40 -9 -15 3 123.69 18.90 9 -15 -3 160.98 19.70 -9 -15 3 155.28 18.30 9 -15 -3 186.18 21.10 -9 -15 3 149.59 19.80 9 -15 -3 204.08 20.90 -9 -15 3 185.88 22.70 -9 -15 3 162.28 22.50 -7 15 1 56.19 12.40 -7 15 1 41.70 15.30 7 15 -1 71.99 15.50 7 15 -1 68.99 16.50 -7 -15 1 40.10 12.90 7 -15 -1 56.49 16.60 7 -15 -1 45.10 13.40 -7 -15 1 64.99 14.90 -7 -15 1 59.29 12.90 7 -15 -1 18.30 12.40 -7 -15 1 52.29 13.40 -7 -15 1 62.09 13.80 5 15 1 642.84 35.30 -5 15 -1 693.53 32.00 -5 15 -1 627.74 34.00 -5 15 -1 677.13 33.40 5 15 1 675.03 32.90 -5 -15 -1 655.43 32.70 -5 -15 -1 636.74 29.40 -5 -15 -1 660.63 30.50 5 -15 1 669.03 32.90 5 -15 1 671.73 34.00 5 -15 1 606.84 31.10 -5 -15 -1 680.03 32.30 -5 -15 -1 667.93 33.40 -5 -15 -1 691.43 31.10 3 15 3 147.29 21.40 3 15 3 172.28 19.00 -3 15 -3 159.18 19.10 3 15 3 173.58 17.50 -3 15 -3 156.58 21.60 -3 15 -3 157.18 18.20 -3 -15 -3 128.69 16.30 -3 -15 -3 186.58 16.60 3 -15 3 168.68 19.00 -3 -15 -3 157.78 19.90 3 -15 3 179.38 21.50 3 -15 3 132.39 18.60 -3 -15 -3 165.38 19.50 -3 -15 -3 150.68 20.00 -1 15 -5 276.47 21.30 1 15 5 273.87 19.20 1 15 5 224.48 23.90 -1 15 -5 266.77 26.20 1 15 5 301.77 20.90 -1 -15 -5 275.67 23.20 -1 -15 -5 282.97 22.90 1 -15 5 310.37 22.00 -1 -15 -5 289.57 23.40 1 -15 5 299.87 24.00 1 -15 5 292.77 22.70 -1 -15 -5 268.77 21.10 -1 -15 -5 299.27 18.20 -1 15 7 5.10 9.20 1 15 -7 3.50 11.60 1 15 -7 2.90 14.60 -1 15 7 14.70 10.20 -1 15 7 -0.90 13.00 1 15 -7 5.70 10.90 1 -15 -7 11.90 11.70 1 -15 -7 12.70 11.80 -1 -15 7 -7.70 10.30 -1 -15 7 10.10 9.00 1 -15 -7 9.60 11.80 -1 -15 7 -2.40 11.10 1 -15 -7 20.60 14.30 -1 -15 7 -0.40 13.40 1 -15 -7 5.90 8.60 -1 -15 7 6.60 11.10 3 15 -9 -12.10 9.30 -3 15 9 8.60 14.50 3 15 -9 7.80 16.30 3 15 -9 -28.80 13.40 -3 15 9 -1.60 8.20 -3 -15 9 21.60 15.20 3 -15 -9 15.50 12.40 3 -15 -9 -7.10 11.00 3 -15 -9 -0.20 12.00 -3 -15 9 -16.70 12.30 -3 -15 9 -4.40 12.30 3 -15 -9 6.70 14.90 -3 -15 9 35.00 13.40 -3 -15 9 -0.30 11.60 3 -15 -9 17.80 9.70 5 15 -11 22.10 19.30 5 15 -11 19.40 17.80 -5 15 11 28.20 12.00 -5 15 11 10.60 13.70 -5 15 11 21.70 16.60 5 15 -11 24.80 10.60 5 -15 -11 9.90 13.60 -5 -15 11 33.50 14.90 -5 -15 11 3.30 15.10 5 -15 -11 30.60 13.40 -5 -15 11 -0.40 14.70 5 -15 -11 2.20 19.00 -5 -15 11 12.40 14.90 5 -15 -11 -10.70 11.80 -7 15 13 53.19 15.30 7 15 -13 -9.80 21.10 7 15 -13 37.60 21.60 -7 15 13 39.80 21.30 -7 15 13 75.09 20.50 7 15 -13 46.20 11.80 7 -15 -13 21.60 14.20 7 -15 -13 52.89 18.20 7 -15 -13 61.39 13.20 -7 -15 13 42.10 20.00 7 -15 -13 46.40 15.30 -7 -15 13 34.10 18.00 7 -15 -13 40.90 21.40 -7 -15 13 65.99 20.10 -7 -15 13 29.10 15.90 9 15 -15 40.40 27.90 9 15 -15 27.50 23.50 -9 15 15 28.30 22.50 -9 15 15 21.90 15.70 9 15 -15 18.10 12.00 9 15 -15 33.40 20.70 -9 15 15 4.30 21.30 9 -15 -15 22.30 17.20 9 -15 -15 9.60 16.00 9 -15 -15 10.10 14.60 9 -15 -15 14.70 23.30 9 -15 -15 34.20 24.90 -9 -15 15 -27.30 20.40 -9 -15 15 -19.00 16.00 -9 -15 15 29.80 21.40 -9 -15 15 29.80 18.10 -11 15 17 -5.90 24.50 -11 15 17 20.00 19.00 11 15 -17 43.50 31.40 11 -15 -17 -6.70 17.60 -11 -15 17 -14.00 20.00 -11 -15 17 -34.90 25.40 11 -15 -17 -20.90 25.70 11 -15 -17 18.60 17.60 -18 16 12 8.30 21.60 -18 16 12 62.49 25.30 -18 16 12 59.99 19.20 -18 16 12 30.90 20.80 18 16 -12 22.60 26.40 -18 -16 12 5.50 19.60 18 -16 -12 9.80 25.50 18 -16 -12 38.20 29.20 18 -16 -12 -8.90 19.00 -18 -16 12 -3.20 20.30 -18 -16 12 56.39 25.00 18 -16 -12 20.70 22.30 16 16 -10 94.79 26.90 -16 16 10 61.09 20.70 -16 16 10 76.49 17.70 -16 16 10 73.29 20.90 -16 16 10 89.69 21.90 -16 -16 10 85.59 22.20 -16 -16 10 57.49 19.00 16 -16 -10 62.69 22.90 -16 -16 10 78.69 13.10 16 -16 -10 58.89 20.60 -16 -16 10 45.20 18.40 16 -16 -10 88.59 21.10 -16 -16 10 70.89 21.20 16 -16 -10 29.60 18.20 -14 16 8 95.39 17.00 14 16 -8 114.69 22.10 -14 16 8 99.49 19.30 -14 16 8 73.09 20.10 -14 16 8 109.59 19.70 -14 -16 8 107.39 21.80 14 -16 -8 111.49 18.50 -14 -16 8 114.59 15.40 -14 -16 8 119.69 20.10 14 -16 -8 111.79 20.40 -14 -16 8 123.29 22.40 14 -16 -8 100.69 20.80 -14 -16 8 90.59 20.20 -14 -16 8 117.49 16.40 14 -16 -8 115.79 24.70 -12 16 6 51.69 16.90 -12 16 6 41.00 13.50 12 16 -6 71.89 17.20 -12 16 6 56.79 15.50 -12 16 6 32.60 17.10 -12 -16 6 13.60 13.70 -12 -16 6 21.90 15.60 -12 -16 6 58.39 15.70 12 -16 -6 42.90 18.30 -12 -16 6 47.00 13.20 -12 -16 6 28.60 17.60 12 -16 -6 19.00 13.70 -12 -16 6 38.90 12.20 12 -16 -6 31.80 14.50 12 -16 -6 47.10 15.90 -10 16 4 140.39 19.70 10 16 -4 158.08 22.80 -10 16 4 133.39 19.00 10 16 -4 160.28 22.50 -10 16 4 156.58 20.70 -10 16 4 167.38 19.60 10 -16 -4 169.78 21.20 -10 -16 4 146.59 19.00 10 -16 -4 167.68 25.30 -10 -16 4 140.99 22.30 -10 -16 4 169.58 21.60 -10 -16 4 138.79 17.20 -10 -16 4 153.18 21.10 -10 -16 4 143.99 19.70 10 -16 -4 164.38 20.50 -8 16 2 347.27 24.60 8 16 -2 320.07 28.50 -8 16 2 318.57 24.80 8 16 -2 348.37 29.50 -8 16 2 317.57 27.10 8 -16 -2 340.47 23.20 -8 -16 2 328.87 23.10 8 -16 -2 319.67 24.60 -8 -16 2 301.07 23.70 8 -16 -2 322.47 27.20 -8 -16 2 321.07 26.10 -8 -16 2 377.46 26.80 -8 -16 2 274.97 23.00 -6 16 0 9.20 11.40 6 16 0 6.40 14.10 -6 16 0 -14.60 12.10 6 16 0 8.90 12.70 -6 16 0 -14.70 10.20 6 -16 0 -12.20 8.90 -6 -16 0 19.00 12.10 6 -16 0 -12.10 13.90 -6 -16 0 -0.20 9.40 6 -16 0 -4.10 10.80 -6 -16 0 7.10 9.80 -6 -16 0 4.30 10.50 -6 -16 0 9.20 10.60 -6 -16 0 -0.40 8.70 -4 16 -2 300.37 25.30 -4 16 -2 343.27 23.70 4 16 2 367.26 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126.39 15.70 -2 -16 8 127.49 15.50 2 -16 -8 130.09 18.40 -2 -16 8 136.09 19.50 4 16 -10 119.69 23.00 -4 16 10 110.99 20.00 -4 16 10 94.09 14.10 -4 16 10 104.49 18.70 4 16 -10 93.59 19.90 4 16 -10 91.79 13.60 -4 -16 10 103.19 16.80 4 -16 -10 64.79 19.60 -4 -16 10 94.89 17.80 -4 -16 10 113.79 20.20 4 -16 -10 73.89 17.40 -4 -16 10 95.19 17.90 4 -16 -10 117.39 15.90 4 -16 -10 106.69 17.90 -4 -16 10 92.39 17.10 4 -16 -10 99.19 16.90 -6 16 12 45.00 16.30 6 16 -12 24.50 12.60 6 16 -12 29.20 19.60 -6 16 12 29.60 14.40 -6 16 12 36.10 19.00 6 16 -12 28.30 21.00 -6 -16 12 18.30 16.80 -6 -16 12 18.70 16.00 -6 -16 12 27.00 15.80 6 -16 -12 24.60 14.60 -6 -16 12 41.90 16.70 6 -16 -12 67.99 18.40 6 -16 -12 55.29 14.10 6 -16 -12 54.39 16.70 6 -16 -12 30.40 20.70 8 16 -14 26.80 24.60 -8 16 14 2.20 19.20 8 16 -14 1.50 11.50 -8 16 14 7.60 15.70 -8 16 14 -31.00 17.80 8 16 -14 10.70 22.00 8 -16 -14 28.90 19.40 -8 -16 14 17.70 19.20 8 -16 -14 4.20 14.20 -8 -16 14 7.50 17.00 -8 -16 14 -3.20 21.20 8 -16 -14 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6 30.60 16.30 13 15 -6 43.40 17.80 -13 15 6 26.40 15.40 -13 15 6 70.39 14.60 -13 15 6 32.40 13.70 13 -15 -6 18.50 14.90 -13 -15 6 20.70 17.20 -13 -15 6 25.70 15.40 13 -15 -6 30.30 18.40 13 -15 -6 18.30 14.00 -13 -15 6 44.10 16.90 -13 -15 6 10.50 11.80 -13 -15 6 41.10 12.20 -13 -15 6 22.50 15.70 13 -15 -6 5.40 13.50 -11 15 4 492.95 29.70 -11 15 4 490.15 33.50 11 15 -4 459.45 31.90 -11 15 4 455.65 28.60 -11 -15 4 477.35 31.80 11 -15 -4 491.35 28.50 -11 -15 4 451.15 32.10 11 -15 -4 490.05 28.40 -11 -15 4 442.16 29.90 -11 -15 4 463.15 26.60 -11 -15 4 431.46 30.30 11 -15 -4 498.15 31.00 11 -15 -4 550.94 30.80 -11 -15 4 474.85 26.50 -9 15 2 -19.60 11.60 9 15 -2 12.00 13.70 -9 15 2 2.70 10.10 -9 15 2 -3.20 10.60 -9 15 2 -1.00 12.50 9 -15 -2 -15.70 15.00 9 -15 -2 -4.40 10.40 -9 -15 2 7.70 13.20 -9 -15 2 3.00 11.80 9 -15 -2 -18.10 9.50 -9 -15 2 2.70 12.10 -9 -15 2 -17.40 10.90 -9 -15 2 -10.30 10.10 9 -15 -2 2.80 11.10 -7 15 0 178.68 20.00 7 15 0 196.88 23.50 -7 15 0 197.38 22.60 7 15 0 211.38 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53.79 17.70 -17 -13 8 60.39 13.30 -17 -13 8 72.99 22.80 17 -13 -8 35.90 18.10 -17 -13 8 74.79 19.70 -17 -13 8 44.50 19.00 -17 -13 8 79.09 11.80 17 -13 -8 57.49 16.60 -17 -13 8 62.19 19.50 17 -13 -8 69.19 20.60 17 -13 -8 41.60 21.10 -15 13 6 7.50 12.50 -15 13 6 3.90 13.90 -15 13 6 5.10 13.60 -15 13 6 -23.40 14.50 15 13 -6 3.50 16.90 15 -13 -6 16.50 13.40 15 -13 -6 -5.40 14.20 15 -13 -6 13.50 14.70 -15 -13 6 26.40 16.00 -15 -13 6 2.00 11.70 -15 -13 6 -16.80 15.70 -15 -13 6 7.20 11.40 -15 -13 6 21.20 15.00 -15 -13 6 11.20 15.90 -15 -13 6 26.10 16.20 15 -13 -6 -0.60 15.70 -13 13 4 244.78 26.60 -13 13 4 242.48 23.10 13 13 -4 273.37 29.50 -13 13 4 207.88 23.00 -13 13 4 218.38 23.00 -13 -13 4 217.48 25.10 -13 -13 4 272.67 20.10 -13 -13 4 206.98 24.20 13 -13 -4 222.88 23.90 -13 -13 4 239.88 25.60 13 -13 -4 232.18 25.40 13 -13 -4 240.48 24.60 -13 -13 4 237.98 27.40 13 -13 -4 239.18 21.10 -13 -13 4 298.57 29.50 -11 13 2 509.95 28.50 -11 13 2 548.45 33.20 -11 13 2 565.04 30.20 -11 -13 2 551.24 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-15 13 18.90 17.60 1 -15 -13 31.70 22.60 -1 -15 13 47.60 22.50 1 -15 -13 18.30 16.80 -1 -15 13 6.70 16.30 -1 -15 13 6.30 16.30 1 -15 -13 48.60 18.20 -3 15 15 17.10 22.40 3 15 -15 25.00 19.40 -3 15 15 -30.20 21.10 3 15 -15 51.09 28.50 3 15 -15 48.90 32.80 -3 -15 15 21.80 20.30 3 -15 -15 -30.00 19.90 -3 -15 15 5.60 17.80 3 -15 -15 2.10 20.50 -3 -15 15 12.90 17.60 -3 -15 15 2.90 22.00 3 -15 -15 4.50 26.00 5 15 -17 14.60 21.10 5 15 -17 79.59 33.60 -5 15 17 59.19 16.30 -5 -15 17 45.20 26.60 5 -15 -17 88.69 20.40 -5 -15 17 47.70 26.60 -20 16 8 90.79 20.00 -20 16 8 93.79 23.60 -20 16 8 84.29 22.70 -20 16 8 80.89 24.10 20 16 -8 73.89 29.70 -20 -16 8 81.79 26.80 20 -16 -8 88.49 22.10 -20 -16 8 114.89 26.80 20 -16 -8 106.49 25.60 -20 -16 8 56.49 22.50 -20 -16 8 50.39 22.00 -20 -16 8 69.59 18.70 20 -16 -8 47.30 20.30 -20 -16 8 46.00 15.80 -18 16 6 31.00 19.20 -18 16 6 51.79 19.20 -18 16 6 46.40 20.20 18 16 -6 27.00 24.20 -18 16 6 25.70 17.60 18 -16 -6 20.20 20.90 -18 -16 6 39.40 15.50 -18 -16 6 32.50 18.40 -18 -16 6 43.20 21.30 -18 -16 6 55.69 24.60 18 -16 -6 36.20 17.50 18 -16 -6 31.50 20.20 -18 -16 6 52.19 20.10 -18 -16 6 45.00 20.30 18 -16 -6 25.40 18.70 -18 -16 6 22.30 14.90 -16 16 4 3.00 15.60 16 16 -4 15.20 21.70 -16 16 4 -1.20 16.80 -16 16 4 26.00 15.60 -16 16 4 -37.80 16.70 16 -16 -4 23.20 13.50 16 -16 -4 -15.60 16.20 -16 -16 4 -7.50 16.50 16 -16 -4 24.90 21.60 -16 -16 4 -1.50 12.90 -16 -16 4 -4.60 16.80 -16 -16 4 4.90 15.70 -16 -16 4 16.10 19.00 16 -16 -4 -18.80 16.70 -14 16 2 7.80 16.60 -14 16 2 7.50 17.10 -14 16 2 2.80 14.20 -14 16 2 34.80 14.90 -14 -16 2 -1.40 13.10 14 -16 -2 9.10 22.50 -14 -16 2 22.60 16.00 -14 -16 2 19.70 15.10 -14 -16 2 -3.00 17.40 14 -16 -2 17.40 14.30 14 -16 -2 35.20 13.10 -14 -16 2 -3.70 16.40 -14 -16 2 -18.70 14.20 -12 16 0 52.69 15.00 -12 16 0 42.60 18.40 -12 16 0 50.59 18.40 -12 16 0 42.80 15.50 -12 16 0 70.49 16.50 12 -16 0 77.99 20.70 12 -16 0 89.39 20.20 -12 -16 0 55.99 16.30 12 -16 0 56.29 13.40 -12 -16 0 49.60 14.00 -12 -16 0 64.69 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18.20 19.00 -17 -17 5 1.90 17.10 17 -17 -5 4.30 18.50 -17 -17 5 38.10 23.20 17 -17 -5 -9.80 16.60 17 -17 -5 51.19 23.80 -17 -17 5 32.20 20.50 -17 -17 5 27.30 16.40 -15 17 3 112.19 18.90 -15 17 3 110.09 20.80 -15 17 3 135.59 22.70 -15 17 3 185.38 25.80 15 -17 -3 95.79 19.20 -15 -17 3 115.19 20.70 15 -17 -3 86.09 17.90 15 -17 -3 180.78 22.20 -15 -17 3 131.89 23.10 -15 -17 3 144.59 25.90 -15 -17 3 106.09 20.30 -15 -17 3 129.29 21.30 15 -17 -3 152.58 24.90 -15 -17 3 108.99 18.80 -13 17 1 101.89 17.30 -13 17 1 82.49 18.70 -13 17 1 97.69 17.00 -13 17 1 95.09 20.60 -13 -17 1 110.79 19.00 -13 -17 1 96.09 18.90 -13 -17 1 94.59 20.20 -13 -17 1 145.19 21.90 13 -17 -1 113.59 19.30 13 -17 -1 111.79 16.00 -13 -17 1 99.19 16.50 -13 -17 1 110.49 19.60 -11 17 -1 22.30 15.00 -11 17 -1 -16.70 15.00 -11 17 -1 -23.00 13.20 11 17 1 -19.60 14.70 -11 17 -1 14.20 12.50 -11 17 -1 -6.60 14.60 11 -17 1 0.70 11.40 11 -17 1 13.40 20.50 -11 -17 -1 -12.00 12.80 -11 -17 -1 -9.80 11.80 -11 -17 -1 3.80 14.40 -11 -17 -1 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-23.30 25.00 -3 -17 15 11.70 18.40 -3 -17 15 0.00 20.80 -3 -17 15 -26.60 16.90 3 -17 -15 7.20 20.70 -20 18 8 29.70 20.20 -20 18 8 77.69 25.20 -20 18 8 19.10 24.70 -20 18 8 -24.70 20.40 20 18 -8 16.70 26.60 -20 -18 8 21.30 20.50 -20 -18 8 -24.60 24.40 -20 -18 8 30.70 26.70 20 -18 -8 30.40 24.70 -20 -18 8 23.00 17.10 -20 -18 8 17.60 22.10 -20 -18 8 -30.30 17.50 20 -18 -8 3.00 22.20 20 -18 -8 35.00 23.10 18 18 -6 33.30 23.70 -18 18 6 48.10 20.40 -18 18 6 34.60 20.00 -18 18 6 33.80 22.50 -18 18 6 54.49 20.90 -18 -18 6 63.59 22.20 -18 -18 6 53.49 24.90 18 -18 -6 22.00 19.60 -18 -18 6 63.49 21.50 18 -18 -6 17.00 19.00 -18 -18 6 53.69 22.20 18 -18 -6 21.00 21.60 -18 -18 6 29.30 17.20 -18 -18 6 -0.10 15.40 -18 -18 6 -15.70 22.90 -16 18 4 15.80 17.40 -16 18 4 35.80 18.90 -16 18 4 1.90 18.70 -16 18 4 63.29 16.50 16 -18 -4 28.20 16.10 -16 -18 4 31.20 18.70 16 -18 -4 64.09 21.40 -16 -18 4 19.40 24.30 -16 -18 4 42.50 19.00 -16 -18 4 21.30 14.60 -16 -18 4 14.20 20.20 -16 -18 4 23.10 21.50 16 -18 -4 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68.29 24.60 -15 15 2 24.90 15.80 -15 15 2 -11.00 16.70 15 15 -2 6.30 19.10 -15 15 2 16.80 15.90 -15 15 2 -26.70 15.40 15 -15 -2 8.20 12.80 -15 -15 2 8.50 14.60 -15 -15 2 12.20 16.30 15 -15 -2 -29.20 13.80 -15 -15 2 2.00 15.70 -15 -15 2 -9.60 16.20 15 -15 -2 -3.30 17.80 -15 -15 2 21.90 14.10 -13 15 0 38.10 16.40 13 15 0 17.70 18.50 -13 15 0 11.50 16.20 -13 15 0 18.00 14.90 -13 15 0 -7.30 16.90 -13 15 0 1.30 14.50 -13 -15 0 18.50 14.50 13 -15 0 3.10 14.20 13 -15 0 31.10 12.00 -13 -15 0 24.50 14.80 -13 -15 0 21.80 14.00 -13 -15 0 -6.80 14.50 -13 -15 0 35.80 17.50 13 -15 0 33.10 19.50 -13 -15 0 12.90 16.80 -11 15 -2 54.89 15.20 -11 15 -2 61.79 16.70 11 15 2 88.99 18.90 11 15 2 51.29 21.10 -11 15 -2 64.09 18.80 -11 15 -2 74.69 15.90 -11 15 -2 36.60 17.50 -11 -15 -2 76.59 15.60 -11 -15 -2 85.99 17.60 -11 -15 -2 59.49 16.80 11 -15 2 43.10 14.50 -11 -15 -2 75.49 16.70 11 -15 2 63.09 20.10 -11 -15 -2 82.69 16.10 -11 -15 -2 89.19 19.30 -9 15 -4 96.19 17.40 -9 15 -4 88.39 16.00 -9 15 -4 68.19 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59.79 21.90 20 16 -7 -12.70 28.60 -20 16 7 28.70 21.90 -20 -16 7 29.70 20.60 -20 -16 7 65.09 25.60 20 -16 -7 14.00 20.80 20 -16 -7 24.70 20.60 -20 -16 7 16.70 26.20 20 -16 -7 33.30 24.50 -20 -16 7 35.30 22.60 -20 -16 7 21.40 16.80 -20 -16 7 17.20 38.50 -20 -16 7 56.39 19.00 -18 16 5 -19.70 18.50 -18 16 5 7.00 18.30 -18 16 5 26.70 21.00 18 16 -5 -1.50 24.50 -18 16 5 38.90 19.90 18 -16 -5 9.70 19.00 -18 -16 5 -3.40 18.90 -18 -16 5 -30.40 22.30 18 -16 -5 -0.80 19.00 -18 -16 5 -31.30 23.10 -18 -16 5 2.70 22.30 -18 -16 5 16.00 18.00 -18 -16 5 35.70 16.20 18 -16 -5 24.50 16.10 18 -16 -5 -8.60 16.30 -16 16 3 92.09 21.80 -16 16 3 84.39 19.80 -16 16 3 197.78 27.00 -16 16 3 100.99 18.60 -16 -16 3 124.19 21.20 16 -16 -3 123.89 19.20 -16 -16 3 134.29 21.40 -16 -16 3 139.29 22.30 -16 -16 3 108.39 22.70 -16 -16 3 98.99 17.80 16 -16 -3 131.39 23.60 16 -16 -3 113.49 21.00 -16 -16 3 127.29 29.90 16 -16 -3 61.29 19.20 -14 16 1 23.00 15.10 -14 16 1 37.70 15.70 -14 16 1 21.10 16.10 -14 16 1 28.10 17.60 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25.20 20.30 0 16 -13 -11.40 25.90 0 16 -13 -5.60 19.50 0 16 13 -13.50 20.20 0 -16 -13 2.60 19.80 0 -16 -13 -7.70 18.00 0 -16 13 37.90 19.40 0 -16 13 2.00 17.70 0 -16 13 14.90 18.10 0 -16 -13 20.00 24.90 0 -16 13 18.60 16.80 2 16 -15 32.60 20.40 -2 16 15 23.00 25.20 2 16 -15 11.60 27.80 2 16 -15 28.30 32.50 -2 -16 15 1.60 21.30 -2 -16 15 -12.40 23.70 2 -16 -15 -0.60 21.20 -2 -16 15 0.60 16.60 2 -16 -15 54.59 26.50 -2 -16 15 1.10 19.00 2 -16 -15 -2.50 20.70 -2 -16 15 42.40 21.80 -21 17 8 4.80 21.20 -21 17 8 48.10 22.10 21 17 -8 16.50 30.80 -21 17 8 2.00 21.60 -21 17 8 48.80 21.60 21 -17 -8 22.30 22.10 -21 -17 8 -29.20 21.90 21 -17 -8 22.30 26.50 -21 -17 8 -13.40 29.20 -21 -17 8 -29.40 16.80 21 -17 -8 -1.60 20.90 -21 -17 8 21.50 21.30 -21 -17 8 -9.60 16.00 -19 17 6 113.79 26.30 -19 17 6 134.59 24.30 19 17 -6 112.49 27.80 -19 17 6 109.99 22.50 -19 17 6 107.79 20.40 19 -17 -6 79.69 20.90 -19 -17 6 97.19 23.50 -19 -17 6 126.89 21.80 -19 -17 6 95.09 19.50 -19 -17 6 99.49 27.40 -19 -17 6 97.79 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10.50 19.20 -18 14 4 58.29 24.60 -18 14 4 57.39 17.40 18 14 -4 17.30 20.50 -18 14 4 27.40 20.70 -18 -14 4 46.50 20.30 -18 -14 4 47.30 19.00 -18 -14 4 42.30 23.90 18 -14 -4 46.00 21.60 18 -14 -4 32.10 19.20 -18 -14 4 47.60 22.30 -18 -14 4 1.10 17.00 18 -14 -4 76.49 19.40 -18 -14 4 38.00 15.60 18 -14 -4 64.19 17.00 -16 14 2 57.79 21.40 -16 14 2 33.10 15.10 -16 14 2 5.10 18.10 16 14 -2 27.70 19.50 -16 14 2 59.59 19.00 -16 -14 2 44.80 17.30 -16 -14 2 28.80 16.00 -16 -14 2 51.49 19.70 -16 -14 2 41.30 20.20 -16 -14 2 26.50 16.10 16 -14 -2 40.80 12.90 16 -14 -2 25.30 20.60 16 -14 -2 46.80 17.20 -16 -14 2 39.90 15.30 -14 14 0 41.90 17.60 -14 14 0 59.69 18.40 14 14 0 35.10 18.60 -14 14 0 46.70 18.90 -14 14 0 46.40 14.80 -14 14 0 55.99 17.30 14 -14 0 56.39 15.40 -14 -14 0 30.40 19.60 -14 -14 0 58.79 17.60 14 -14 0 17.20 19.80 -14 -14 0 53.79 15.00 -14 -14 0 54.99 15.40 -14 -14 0 34.60 14.80 -14 -14 0 39.80 15.20 12 14 2 84.09 19.80 -12 14 -2 88.59 19.80 -12 14 -2 86.59 22.50 -12 14 -2 83.89 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14 39.30 18.60 2 14 -16 35.00 36.10 2 14 -16 67.69 30.90 2 14 -16 81.89 22.00 -2 14 16 58.69 27.50 -2 -14 16 22.10 16.80 -2 -14 16 38.70 24.90 -2 -14 16 101.69 25.00 2 -14 -16 56.39 24.00 -2 -14 16 26.80 19.90 2 -14 -16 11.50 21.80 2 -14 -16 89.29 28.60 21 15 -7 6.40 28.50 -21 15 7 11.90 24.00 -21 15 7 16.40 21.00 -21 15 7 -2.60 20.60 -21 15 7 -14.90 18.90 21 -15 -7 -9.30 22.10 21 -15 -7 -23.60 23.60 -21 -15 7 -40.50 19.40 -21 -15 7 -20.90 26.30 -21 -15 7 -2.90 19.30 -21 -15 7 -35.30 20.60 21 -15 -7 27.80 19.70 19 15 -5 -20.10 24.40 -19 15 5 37.60 19.70 -19 15 5 -7.50 17.50 -19 15 5 -9.70 19.20 -19 15 5 -6.90 21.50 -19 -15 5 31.70 17.70 19 -15 -5 19.60 23.40 19 -15 -5 -11.60 20.70 -19 -15 5 -9.90 17.10 -19 -15 5 -1.30 22.70 -19 -15 5 45.70 25.50 19 -15 -5 -7.10 16.80 -19 -15 5 -16.70 16.60 17 15 -3 9.40 21.50 -17 15 3 6.00 16.30 -17 15 3 -30.50 18.10 -17 15 3 12.00 18.70 -17 15 3 49.20 19.10 -17 -15 3 -30.30 16.70 -17 -15 3 16.60 18.70 -17 -15 3 14.90 14.80 -17 -15 3 -3.60 21.20 17 -15 -3 11.40 18.30 17 -15 -3 -19.80 16.20 17 -15 -3 -8.50 12.50 -17 -15 3 -27.50 19.30 -17 -15 3 17.00 16.90 17 -15 -3 -17.30 21.90 15 15 -1 29.20 20.30 -15 15 1 27.80 17.40 -15 15 1 11.60 14.30 -15 15 1 0.20 19.10 -15 15 1 -1.40 16.80 -15 -15 1 9.50 16.40 -15 -15 1 21.20 16.10 -15 -15 1 13.50 18.70 -15 -15 1 8.10 16.00 -15 -15 1 7.10 14.80 15 -15 -1 14.00 14.70 -15 -15 1 44.60 17.70 -15 -15 1 28.30 19.20 15 -15 -1 23.00 21.00 15 -15 -1 18.70 12.20 -13 15 -1 5.80 17.20 -13 15 -1 -10.80 18.50 13 15 1 4.90 17.60 -13 15 -1 5.80 15.90 -13 15 -1 17.90 16.10 -13 15 -1 24.60 13.60 -13 -15 -1 21.10 13.70 -13 -15 -1 18.60 19.00 -13 -15 -1 -14.50 17.00 -13 -15 -1 11.10 15.50 -13 -15 -1 22.40 16.90 -13 -15 -1 32.60 15.60 13 -15 1 58.19 20.90 13 -15 1 12.80 14.40 13 -15 1 15.00 13.90 11 15 3 22.00 19.10 -11 15 -3 7.30 15.80 11 15 3 9.70 16.10 -11 15 -3 23.10 14.70 -11 15 -3 37.20 18.00 -11 15 -3 8.70 16.60 -11 15 -3 15.80 15.30 -11 -15 -3 17.80 13.30 -11 -15 -3 11.40 12.80 -11 -15 -3 10.10 12.90 11 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15 -11 97.79 24.00 3 15 11 74.89 19.10 -3 15 -11 47.50 24.70 3 15 11 43.50 21.90 -3 15 -11 50.79 21.60 3 -15 11 41.70 19.20 -3 -15 -11 53.99 21.10 3 -15 11 46.50 15.80 -3 -15 -11 35.80 17.10 -3 -15 -11 53.29 17.50 3 -15 11 37.90 15.80 3 -15 11 50.99 16.50 3 -15 11 42.70 15.50 -1 15 -13 -2.30 26.80 -1 15 -13 8.20 24.60 1 15 13 -29.20 18.10 1 15 13 9.40 21.90 1 -15 13 20.40 18.40 -1 -15 -13 4.60 22.40 1 -15 13 -8.70 15.70 1 -15 13 -32.50 16.70 1 -15 13 11.10 19.00 -1 -15 -13 1.60 18.00 -1 15 15 -4.30 23.50 1 15 -15 36.50 29.40 1 15 -15 40.10 21.30 1 15 -15 -25.30 30.40 1 -15 -15 17.40 21.60 1 -15 -15 -3.30 28.60 -1 -15 15 -5.80 16.30 -1 -15 15 -15.70 21.50 -1 -15 15 -16.10 17.80 1 -15 -15 -18.10 20.30 -1 -15 15 68.79 23.70 20 16 -6 -16.10 26.30 -20 16 6 15.60 21.80 -20 16 6 -3.90 20.30 -20 16 6 13.80 19.50 -20 16 6 -20.20 19.90 -20 -16 6 17.80 19.90 -20 -16 6 1.60 23.90 20 -16 -6 -12.60 23.60 20 -16 -6 -5.00 20.90 -20 -16 6 0.30 24.00 -20 -16 6 0.20 18.90 -20 -16 6 10.00 18.70 -20 -16 6 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-16 8 57.29 14.60 -6 -16 -8 23.60 16.70 6 -16 8 40.50 15.40 6 -16 8 40.10 15.30 -6 -16 -8 16.80 17.60 -6 -16 -8 42.80 16.10 6 -16 8 27.80 17.70 -4 16 -10 44.50 21.80 -4 16 -10 -39.60 20.30 -4 16 -10 -22.80 18.60 4 16 10 29.50 21.50 4 16 10 12.00 18.60 4 16 10 13.60 15.00 4 -16 10 7.30 18.00 -4 -16 -10 2.10 14.70 -4 -16 -10 12.50 18.20 4 -16 10 2.10 14.50 4 -16 10 32.20 15.80 4 -16 10 -23.50 13.10 -4 -16 -10 -16.70 17.10 2 16 12 23.40 18.00 2 16 12 -4.60 20.00 -2 16 -12 -13.80 21.20 -2 16 -12 39.20 24.50 -2 16 -12 20.50 27.00 -2 -16 -12 -19.10 21.60 2 -16 12 14.80 18.00 2 -16 12 52.49 18.70 -2 -16 -12 30.30 19.20 2 -16 12 24.80 17.80 2 -16 12 13.60 16.50 2 -16 12 -11.00 17.20 -2 -16 -12 15.20 19.70 0 16 -14 -2.30 27.60 0 16 -14 -16.70 29.50 0 16 14 32.70 23.90 0 16 14 32.20 24.80 0 16 -14 20.40 21.50 0 -16 -14 -13.80 25.20 0 -16 14 5.70 19.40 0 -16 14 34.00 19.50 0 -16 14 38.30 18.70 0 -16 -14 28.90 22.80 0 -16 -14 -17.60 19.50 0 -16 14 -11.20 15.50 0 -16 14 13.30 18.70 2 16 -16 4.10 22.90 -2 -16 16 41.30 25.10 -21 17 7 5.60 21.00 21 17 -7 -24.90 27.10 -21 17 7 46.20 25.30 -21 17 7 -12.40 20.80 21 -17 -7 -4.20 23.20 -21 -17 7 -11.70 22.10 21 -17 -7 29.70 22.20 -21 -17 7 -30.90 17.90 -21 -17 7 16.00 22.30 21 -17 -7 -11.30 18.90 -21 -17 7 -19.20 15.90 -21 -17 7 -5.30 25.00 -19 17 5 55.59 20.80 -19 17 5 25.50 23.10 -19 17 5 51.69 20.80 -19 17 5 -16.00 19.70 -19 -17 5 31.10 19.30 -19 -17 5 -0.70 18.40 -19 -17 5 13.20 19.30 19 -17 -5 19.30 23.10 19 -17 -5 9.10 17.00 -19 -17 5 61.59 24.10 -19 -17 5 62.29 24.90 19 -17 -5 1.80 18.70 -19 -17 5 43.20 24.50 -17 17 3 83.09 20.70 -17 17 3 93.29 25.10 -17 17 3 90.69 21.90 -17 17 3 68.59 20.50 -17 -17 3 114.29 22.40 17 -17 -3 112.79 22.20 -17 -17 3 69.19 21.60 -17 -17 3 105.29 23.80 17 -17 -3 142.19 25.30 -17 -17 3 65.69 23.80 17 -17 -3 91.29 18.90 -17 -17 3 94.19 18.90 -17 -17 3 79.19 22.50 -15 17 1 60.19 17.50 -15 17 1 30.50 20.50 -15 17 1 84.69 20.30 -15 17 1 64.59 20.40 -15 17 1 29.50 20.60 -15 -17 1 42.10 20.30 -15 -17 1 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-1 17 -13 1.00 27.70 -1 17 -13 -4.00 22.00 -1 17 -13 -8.40 26.80 1 17 13 18.80 22.80 1 -17 13 7.10 16.20 1 -17 13 57.49 19.40 -1 -17 -13 2.80 18.40 1 -17 13 3.70 24.40 -1 -17 -13 12.60 25.60 1 -17 13 -38.00 16.90 1 17 -15 23.80 31.70 1 17 -15 -10.50 33.80 -1 17 15 -51.89 24.50 1 17 -15 -4.50 21.70 -1 -17 15 34.60 23.10 -1 -17 15 8.60 21.70 -1 -17 15 7.00 19.70 -1 -17 15 -24.70 15.00 -1 -17 15 23.90 23.10 1 -17 -15 -6.50 21.40 1 -17 -15 8.20 28.20 -20 18 6 83.09 24.10 -20 18 6 154.48 28.20 -20 18 6 63.79 20.50 20 18 -6 126.29 30.90 -20 -18 6 75.69 19.90 -20 -18 6 94.19 21.90 20 -18 -6 108.79 24.60 -20 -18 6 64.69 24.40 20 -18 -6 96.39 27.00 20 -18 -6 90.09 23.60 -20 -18 6 75.59 27.70 -20 -18 6 102.89 23.60 -18 18 4 -13.90 18.60 -18 18 4 33.70 24.10 -18 18 4 28.10 20.60 -18 18 4 28.10 21.20 18 -18 -4 37.60 24.90 18 -18 -4 28.50 20.60 -18 -18 4 28.50 19.90 -18 -18 4 9.00 20.70 -18 -18 4 -0.60 24.30 -18 -18 4 16.60 22.30 -18 -18 4 20.10 20.40 -18 -18 4 -24.10 23.00 18 -18 -4 33.90 17.50 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20 -5.96 0.00 6 8 20 -0.98 0.00 8 8 20 -1.51 0.00 10 8 20 -2.48 0.00 -25 9 20 -6.47 0.00 -23 9 20 -8.93 0.00 -21 9 20 -6.15 0.00 -19 9 20 0.09 0.00 -17 9 20 -10.89 0.00 -15 9 20 2.04 0.00 -13 9 20 2.41 0.00 -11 9 20 0.38 0.00 -9 9 20 -4.42 0.00 -7 9 20 -1.75 0.00 -5 9 20 -1.40 0.00 -3 9 20 3.21 0.00 -1 9 20 5.37 0.00 1 9 20 12.21 0.00 3 9 20 2.30 0.00 5 9 20 0.45 0.00 7 9 20 -0.97 0.00 9 9 20 -3.31 0.00 -26 10 20 -0.02 0.00 -24 10 20 2.63 0.00 -22 10 20 -0.48 0.00 -20 10 20 6.23 0.00 -18 10 20 -4.69 0.00 -16 10 20 -2.46 0.00 -14 10 20 5.84 0.00 -12 10 20 11.28 0.00 -10 10 20 14.12 0.00 -8 10 20 3.70 0.00 -6 10 20 -4.48 0.00 -4 10 20 -2.14 0.00 -2 10 20 -3.27 0.00 0 10 20 9.63 0.00 2 10 20 1.09 0.00 4 10 20 -1.36 0.00 6 10 20 -3.00 0.00 8 10 20 0.50 0.00 -25 11 20 -0.69 0.00 -23 11 20 -1.18 0.00 -21 11 20 0.06 0.00 -19 11 20 2.55 0.00 -17 11 20 -8.14 0.00 -15 11 20 3.09 0.00 -13 11 20 -3.33 0.00 -11 11 20 -5.20 0.00 -9 11 20 -5.28 0.00 -7 11 20 6.92 0.00 -5 11 20 -6.16 0.00 -3 11 20 1.59 0.00 -1 11 20 0.84 0.00 1 11 20 5.38 0.00 3 11 20 -4.07 0.00 5 11 20 7.51 0.00 7 11 20 3.31 0.00 9 11 20 -2.22 0.00 -26 12 20 2.16 0.00 -24 12 20 3.32 0.00 -22 12 20 -4.71 0.00 -20 12 20 -2.24 0.00 -18 12 20 -6.03 0.00 -16 12 20 -7.19 0.00 -14 12 20 3.47 0.00 -12 12 20 11.69 0.00 -10 12 20 11.24 0.00 -8 12 20 6.33 0.00 -6 12 20 1.23 0.00 -4 12 20 8.92 0.00 -2 12 20 7.05 0.00 0 12 20 12.15 0.00 2 12 20 3.78 0.00 4 12 20 3.23 0.00 6 12 20 -5.60 0.00 8 12 20 4.04 0.00 -25 13 20 3.76 0.00 -23 13 20 0.49 0.00 -21 13 20 1.51 0.00 -19 13 20 4.03 0.00 -17 13 20 -1.66 0.00 -15 13 20 3.91 0.00 -13 13 20 -6.40 0.00 -11 13 20 -1.78 0.00 -9 13 20 4.58 0.00 -7 13 20 5.21 0.00 -5 13 20 -2.85 0.00 -3 13 20 -2.46 0.00 -1 13 20 -5.79 0.00 1 13 20 4.49 0.00 3 13 20 -1.86 0.00 5 13 20 6.49 0.00 7 13 20 -0.38 0.00 9 13 20 -5.21 0.00 -26 14 20 -0.61 0.00 -24 14 20 1.04 0.00 -22 14 20 -4.88 0.00 -20 14 20 -2.09 0.00 -18 14 20 -3.99 0.00 -16 14 20 -3.30 0.00 -14 14 20 2.02 0.00 -12 14 20 4.96 0.00 -10 14 20 -7.96 0.00 -8 14 20 -1.99 0.00 -6 14 20 -4.03 0.00 -4 14 20 1.62 0.00 -2 14 20 3.76 0.00 0 14 20 4.83 0.00 2 14 20 -4.81 0.00 4 14 20 3.00 0.00 6 14 20 1.24 0.00 8 14 20 5.15 0.00 -25 15 20 -2.70 0.00 -23 15 20 -3.36 0.00 -21 15 20 -3.46 0.00 -19 15 20 4.64 0.00 -17 15 20 -2.83 0.00 -15 15 20 3.80 0.00 -13 15 20 -3.94 0.00 -11 15 20 5.32 0.00 -9 15 20 5.00 0.00 -7 15 20 1.41 0.00 -5 15 20 -1.92 0.00 -3 15 20 -2.07 0.00 -1 15 20 -6.83 0.00 1 15 20 3.39 0.00 3 15 20 -0.70 0.00 5 15 20 -1.26 0.00 7 15 20 -1.83 0.00 -26 16 20 0.34 0.00 -24 16 20 -3.41 0.00 -22 16 20 -0.44 0.00 -20 16 20 -0.45 0.00 -18 16 20 -1.47 0.00 -16 16 20 -3.54 0.00 -14 16 20 -2.39 0.00 -12 16 20 0.78 0.00 -10 16 20 -8.48 0.00 -8 16 20 -4.26 0.00 -6 16 20 -6.65 0.00 -4 16 20 -1.24 0.00 -2 16 20 -1.43 0.00 0 16 20 4.32 0.00 2 16 20 -1.75 0.00 4 16 20 1.71 0.00 6 16 20 -1.11 0.00 8 16 20 1.73 0.00 -25 17 20 -4.53 0.00 -23 17 20 1.14 0.00 -21 17 20 4.76 0.00 -19 17 20 5.58 0.00 -17 17 20 -2.72 0.00 -15 17 20 5.04 0.00 -13 17 20 4.30 0.00 -11 17 20 -2.93 0.00 -9 17 20 -3.70 0.00 -7 17 20 -1.51 0.00 -5 17 20 -4.59 0.00 -3 17 20 -0.92 0.00 -1 17 20 -3.85 0.00 1 17 20 0.15 0.00 3 17 20 -2.18 0.00 5 17 20 0.53 0.00 7 17 20 1.30 0.00 -26 18 20 2.54 0.00 -24 18 20 -2.02 0.00 -22 18 20 -4.42 0.00 -20 18 20 -2.76 0.00 -18 18 20 -1.79 0.00 -16 18 20 -6.07 0.00 -14 18 20 -4.14 0.00 -12 18 20 7.33 0.00 -10 18 20 10.67 0.00 -8 18 20 4.32 0.00 -6 18 20 3.55 0.00 -4 18 20 -0.50 0.00 -2 18 20 -3.31 0.00 0 18 20 1.73 0.00 2 18 20 1.33 0.00 4 18 20 0.72 0.00 6 18 20 -2.28 0.00 -25 19 20 2.21 0.00 -23 19 20 9.29 0.00 -21 19 20 8.29 0.00 -19 19 20 3.95 0.00 -17 19 20 0.47 0.00 -15 19 20 -2.01 0.00 -13 19 20 4.64 0.00 -11 19 20 -5.64 0.00 -9 19 20 -1.65 0.00 -7 19 20 2.29 0.00 -5 19 20 -1.18 0.00 -3 19 20 1.69 0.00 -1 19 20 -3.33 0.00 1 19 20 3.19 0.00 3 19 20 2.27 0.00 5 19 20 -1.34 0.00 7 19 20 -0.53 0.00 -26 20 20 3.72 0.00 -24 20 20 2.19 0.00 -22 20 20 -3.66 0.00 -20 20 20 0.08 0.00 -18 20 20 -0.05 0.00 -16 20 20 -6.15 0.00 -14 20 20 -6.09 0.00 -12 20 20 1.60 0.00 -10 20 20 2.13 0.00 -8 20 20 1.41 0.00 -6 20 20 -0.86 0.00 -4 20 20 -5.67 0.00 -2 20 20 -3.10 0.00 0 20 20 3.81 0.00 2 20 20 1.48 0.00 4 20 20 3.07 0.00 6 20 20 1.61 0.00 -25 21 20 5.48 0.00 -23 21 20 4.48 0.00 -21 21 20 2.08 0.00 -19 21 20 2.02 0.00 -17 21 20 0.19 0.00 -15 21 20 -5.64 0.00 -13 21 20 3.10 0.00 -11 21 20 6.33 0.00 -9 21 20 5.42 0.00 -7 21 20 5.08 0.00 -5 21 20 2.82 0.00 -3 21 20 3.64 0.00 -1 21 20 -4.11 0.00 1 21 20 0.38 0.00 3 21 20 3.30 0.00 5 21 20 -2.52 0.00 -26 22 20 5.50 0.00 -24 22 20 1.52 0.00 -22 22 20 2.21 0.00 -20 22 20 3.20 0.00 -18 22 20 6.07 0.00 -16 22 20 -5.47 0.00 -14 22 20 -5.63 0.00 -12 22 20 -2.25 0.00 -10 22 20 -4.31 0.00 -8 22 20 5.29 0.00 -6 22 20 1.99 0.00 -4 22 20 -3.24 0.00 -2 22 20 -4.79 0.00 0 22 20 -1.01 0.00 2 22 20 -0.75 0.00 4 22 20 -1.95 0.00 -25 23 20 1.09 0.00 -23 23 20 -1.05 0.00 -21 23 20 3.77 0.00 -19 23 20 2.26 0.00 -17 23 20 -2.33 0.00 -15 23 20 -5.48 0.00 -13 23 20 -0.75 0.00 -11 23 20 -3.36 0.00 -9 23 20 -4.76 0.00 -7 23 20 -5.24 0.00 -5 23 20 -4.35 0.00 -3 23 20 3.35 0.00 -1 23 20 -0.07 0.00 1 23 20 -4.19 0.00 3 23 20 -0.66 0.00 -26 24 20 1.62 0.00 -24 24 20 -4.97 0.00 -22 24 20 -3.67 0.00 -20 24 20 4.18 0.00 -18 24 20 4.38 0.00 -16 24 20 0.34 0.00 -14 24 20 1.02 0.00 -12 24 20 6.76 0.00 -10 24 20 1.19 0.00 -8 24 20 4.80 0.00 -6 24 20 4.67 0.00 -4 24 20 2.10 0.00 -2 24 20 -3.41 0.00 0 24 20 -4.58 0.00 2 24 20 -2.78 0.00 4 24 20 -3.57 0.00 -25 25 20 -0.54 0.00 -23 25 20 -1.36 0.00 -21 25 20 3.32 0.00 -19 25 20 1.17 0.00 -17 25 20 0.48 0.00 -15 25 20 0.67 0.00 -13 25 20 5.10 0.00 -11 25 20 -1.25 0.00 -9 25 20 0.26 0.00 -7 25 20 4.72 0.00 -5 25 20 -1.50 0.00 -3 25 20 4.93 0.00 -1 25 20 -1.12 0.00 1 25 20 -4.50 0.00 3 25 20 -1.98 0.00 -24 26 20 -7.28 0.00 -22 26 20 -4.86 0.00 -20 26 20 3.20 0.00 -18 26 20 2.06 0.00 -16 26 20 -0.38 0.00 -14 26 20 0.00 0.00 -12 26 20 3.67 0.00 -10 26 20 -0.76 0.00 -8 26 20 -1.96 0.00 -6 26 20 -2.36 0.00 -4 26 20 1.57 0.00 -2 26 20 0.62 0.00 0 26 20 1.03 0.00 2 26 20 -3.10 0.00 -25 27 20 0.21 0.00 -23 27 20 -3.43 0.00 -21 27 20 -2.19 0.00 -19 27 20 -3.24 0.00 -17 27 20 0.09 0.00 -15 27 20 0.58 0.00 -13 27 20 2.70 0.00 -11 27 20 1.40 0.00 -9 27 20 -0.59 0.00 -7 27 20 6.40 0.00 -5 27 20 2.40 0.00 -3 27 20 6.15 0.00 -1 27 20 0.16 0.00 1 27 20 -0.77 0.00 -24 28 20 -1.96 0.00 -22 28 20 -1.23 0.00 -20 28 20 1.46 0.00 -18 28 20 4.19 0.00 -16 28 20 -0.89 0.00 -14 28 20 -3.66 0.00 -12 28 20 0.36 0.00 -10 28 20 1.33 0.00 -8 28 20 3.20 0.00 -6 28 20 0.75 0.00 -4 28 20 1.98 0.00 -2 28 20 1.53 0.00 0 28 20 0.68 0.00 -23 29 20 -1.65 0.00 -21 29 20 -0.62 0.00 -19 29 20 -3.70 0.00 -17 29 20 -0.86 0.00 -15 29 20 -4.09 0.00 -13 29 20 -4.84 0.00 -11 29 20 -1.47 0.00 -9 29 20 -3.24 0.00 -7 29 20 0.44 0.00 -5 29 20 0.75 0.00 -3 29 20 4.22 0.00 -1 29 20 3.35 0.00 -20 30 20 0.95 0.00 -18 30 20 2.36 0.00 -16 30 20 -1.11 0.00 -14 30 20 -6.76 0.00 -12 30 20 -3.88 0.00 -10 30 20 -3.85 0.00 -8 30 20 -2.94 0.00 -6 30 20 -2.97 0.00 -4 30 20 1.53 0.00 -2 30 20 0.23 0.00 -19 31 20 -2.76 0.00 -17 31 20 2.60 0.00 -15 31 20 -1.27 0.00 -13 31 20 -1.88 0.00 -11 31 20 0.00 0.00 -9 31 20 -1.80 0.00 -7 31 20 -1.81 0.00 -5 31 20 -2.90 0.00 -3 31 20 -1.17 0.00 -18 32 20 2.46 0.00 -16 32 20 -0.73 0.00 -14 32 20 -2.86 0.00 -12 32 20 -0.55 0.00 -10 32 20 0.77 0.00 -8 32 20 -2.26 0.00 -6 32 20 -2.82 0.00 -15 33 20 1.33 0.00 -13 33 20 -0.67 0.00 -11 33 20 1.00 0.00 -9 33 20 -3.15 0.00 -7 33 20 -2.58 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 30118) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.500 864 206 ' ' 2 -0.036 0.000 0.000 1723 395 ' ' 3 0.000 0.355 0.500 181 32 ' ' 4 -0.008 0.500 0.000 1723 395 ' ' 5 0.000 0.645 0.500 181 32 ' ' 6 0.023 0.500 0.386 7 0 ' ' 7 0.103 0.500 0.496 7 2 ' ' 8 0.230 0.293 0.869 16 2 ' ' 9 0.231 0.707 0.869 16 2 ' ' 10 0.500 0.500 0.500 864 206 ' ' 11 0.269 0.207 0.131 16 2 ' ' 12 0.269 0.793 0.131 16 2 ' ' 13 0.398 0.000 0.505 7 2 ' ' 14 0.500 0.145 0.500 181 32 ' ' 15 0.500 0.855 0.500 181 32 ' ' 16 0.477 0.000 0.614 7 0 ' ' 17 0.523 0.000 0.386 7 0 ' ' 18 0.603 0.000 0.496 7 2 ' ' 19 0.731 0.207 0.869 16 2 ' ' 20 0.730 0.793 0.869 16 2 ' ' 21 0.769 0.293 0.131 16 2 ' ' 22 0.769 0.707 0.131 16 2 ' ' 23 0.898 0.500 0.505 7 2 ' ' 24 0.977 0.500 0.614 7 0 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 2 0 0 1.664 1 1 0 1.001 0 2 0 1.112 2 2 0 2.002 1 3 0 1.864 -2 0 1 1.514 0 0 1 1.060 -1 1 1 1.151 1 1 1 1.710 -2 2 1 1.879 0 2 1 1.536 -1 3 1 1.949 -2 0 2 2.016 0 0 2 2.120 -1 1 2 1.974 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL s1_a.res in C2/m CELL 27.4580 36.6230 21.5580 90.00 116.96 90.00 SPGR C2/m # Solvent Accessible Volume = 6084 # Electrons Found in S.A.V. = 1350 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others Q101 0.808 0.502 0.969 ! 2.61 eA-3 C102 0.304 0.502 0.484 ! 2.51 eA-3 C103 0.282 0.499 0.516 ! 2.46 eA-3 C104 0.413 0.369 0.271 ! 2.43 eA-3 C105 0.430 0.389 0.302 ! 2.31 eA-3 C106 0.500 0.203 0.498 ! 2.28 eA-3 C107 0.733 0.499 0.133 ! 2.26 eA-3 Q108 0.069 0.502 0.492 ! 2.17 eA-3 C109 0.500 0.156 0.501 ! 2.16 eA-3 C110 1.000 0.094-0.001 ! 1.92 eA-3 Q111 0.820 0.501 0.922 ! 1.90 eA-3 Q112 0.627 0.056 0.122 ! 1.87 eA-3 Q113 1.000 0.445 0.499 ! 1.72 eA-3 C114 0.291 0.501 0.937 ! 1.64 eA-3 Q115 0.774 0.500 0.922 ! 1.56 eA-3 Q116 0.757 0.444 0.754 ! 1.55 eA-3 Q117 0.833 0.497 0.016 ! 1.50 eA-3 Q118 0.795 0.501 0.758 ! 1.45 eA-3 Q119 0.949 0.132 0.391 ! 1.43 eA-3 C120 0.500 0.094 0.496 ! 1.41 eA-3 C121 0.192 0.023 0.554 ! 1.40 eA-3 Q122 0.630 0.369 0.420 ! 1.39 eA-3 C123 0.173 0.041 0.528 ! 1.38 eA-3 Q124 0.526 0.437 0.046 ! 1.38 eA-3 C125 0.868 0.500 0.906 ! 1.33 eA-3 C126 0.342 0.502 0.883 ! 1.29 eA-3 C127 0.242 0.017 0.066 ! 1.26 eA-3 Q128 0.624 0.384 0.670 ! 1.25 eA-3 C129 0.298 0.500 0.828 ! 1.25 eA-3 Q130 0.188 0.453 0.192 ! 1.24 eA-3 Q131 0.775 0.359 0.147 ! 1.24 eA-3 C132 0.142 0.400 0.978 ! 1.24 eA-3 Q133 0.197 0.046 0.679 ! 1.21 eA-3 C134 0.049 0.498 0.172 ! 1.19 eA-3 Q135 0.488 0.437 0.011 ! 1.18 eA-3 C136 0.601 0.140 0.206 ! 1.13 eA-3 C137 0.605 0.069 0.961 ! 1.12 eA-3 Q138 0.554 0.398 0.063 ! 1.11 eA-3 Q139 0.393 0.040 0.910 ! 1.11 eA-3 C140 0.744 0.499 0.180 ! 1.11 eA-3 C141 0.020 0.347 0.448 ! 1.09 eA-3 C142 0.352 0.476 0.293 ! 1.08 eA-3 C143 1.000 0.346 0.424 ! 1.07 eA-3 C144 0.428 0.054 0.871 ! 1.07 eA-3 Q145 0.269 0.109 0.115 ! 1.05 eA-3 C146 0.600 0.095 0.115 ! 1.04 eA-3 Q147 0.513 0.447 0.674 ! 1.04 eA-3 Q148 0.355 0.156 0.172 ! 1.03 eA-3 C149 0.129 0.389 0.007 ! 1.03 eA-3 C150 0.984 0.125 0.971 ! 1.03 eA-3 C151 0.058 0.500 0.133 ! 1.01 eA-3 C152 0.905 0.388 0.019 ! 1.00 eA-3 C153 0.916 0.383 0.969 ! 1.00 eA-3 C154 0.657 0.061 0.987 ! 1.00 eA-3 C155 0.767 0.021 0.828 ! 1.00 eA-3 C156 0.803 0.500 0.094 ! 0.99 eA-3 Q157 0.954 0.044 0.594 ! 0.99 eA-3 C158 0.017 0.500 0.125 ! 0.99 eA-3 Q159 0.741 0.178 0.864 ! 0.98 eA-3 Q160 0.446 0.201 0.919 ! 0.98 eA-3 Q161 0.301 0.500 0.164 ! 0.96 eA-3 Q162 1.002 0.124 0.434 ! 0.95 eA-3 C163 0.077 0.081 0.709 ! 0.95 eA-3 C164 0.352 0.475 0.920 ! 0.94 eA-3 C165 0.462 0.039 0.887 ! 0.94 eA-3 C166 0.361 0.070 0.044 ! 0.93 eA-3 Q167 0.608 0.499 0.062 ! 0.92 eA-3 C168 0.203 0.047 0.584 ! 0.92 eA-3 Q169 0.623 0.501 0.711 ! 0.91 eA-3 C170 0.856 0.500 0.969 ! 0.91 eA-3 Q171 0.936 0.133 0.944 ! 0.90 eA-3 C172 0.020 0.368 0.479 ! 0.90 eA-3 C173 0.343 0.500 0.945 ! 0.89 eA-3 C174 0.490 0.025 0.833 ! 0.89 eA-3 C175 0.553 0.573 0.700 ! 0.89 eA-3 C176 0.053 0.073 0.700 ! 0.89 eA-3 C177 0.859 0.479 0.932 ! 0.89 eA-3 C178 0.789 0.500 0.047 ! 0.88 eA-3 Q179 0.867 0.328 0.357 ! 0.88 eA-3 C180 0.494 0.117 0.485 ! 0.87 eA-3 C181 0.328 0.141 0.191 ! 0.87 eA-3 Q182 0.243 0.368 0.932 ! 0.87 eA-3 C183 0.702 0.118 0.841 ! 0.86 eA-3 Q184 0.577 0.321 0.487 ! 0.86 eA-3 C185 0.647 0.047 0.952 ! 0.86 eA-3 C186 0.025 0.501 0.867 ! 0.86 eA-3 Q187 0.593 0.499 0.430 ! 0.85 eA-3 Q188 1.000 0.094 0.502 ! 0.85 eA-3 C189 0.063 0.499 0.648 ! 0.84 eA-3 C190 0.474 0.376 0.362 ! 0.84 eA-3 Q191 0.164 0.374 0.786 ! 0.83 eA-3 Q192 0.080 0.054 0.462 ! 0.82 eA-3 C193 0.187 0.648 0.825 ! 0.82 eA-3 C194 0.624 0.047 0.003 ! 0.82 eA-3 Q195 0.353 0.490 0.257 ! 0.82 eA-3 C196 0.420 0.125 0.896 ! 0.81 eA-3 Q197 0.789 0.344 0.194 ! 0.81 eA-3 C198 0.938 0.139 0.319 ! 0.80 eA-3 C199 0.327 0.483 0.942 ! 0.80 eA-3 ) ; _shelx_fab_checksum 85324 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co5 Co 0.58990(8) 0.29382(6) 0.50221(10) 0.0818(8) Uani 1 1 d . U . . . Co3 Co 0.64399(8) 0.35194(6) 0.40424(11) 0.0889(9) Uani 1 1 d . U . . . Co4A Co 0.70611(14) 0.35938(9) 0.59731(17) 0.0751(11) Uani 0.8 1 d . U . D . Co1B Co 0.5539(9) 0.500000 0.8658(10) 0.048(4) Uani 0.4 2 d S TU P A 1 Co2' Co 0.7866(4) 0.55210(19) 0.7767(4) 0.073(2) Uani 0.25 1 d . U . B 2 Co1' Co 0.7258(5) 0.500000 0.8725(6) 0.079(3) Uani 0.25 2 d S TU P B 2 O7 O 0.5768(4) 0.2751(3) 0.5806(5) 0.080(3) Uani 1 1 d . U . . . O4 O 0.4126(3) 0.3465(3) 0.6965(5) 0.079(3) Uani 1 1 d . U . . . O6 O 0.4859(4) 0.2753(3) 0.5785(5) 0.078(3) Uani 1 1 d . U . . . O15 O 0.6911(4) 0.3863(3) 0.3790(5) 0.082(3) Uani 1 1 d . U . . . O5 O 0.4088(4) 0.3199(2) 0.5785(5) 0.069(3) Uani 0.91 1 d . U . . . O16 O 0.6574(4) 0.4356(3) 0.2921(5) 0.086(3) Uani 1 1 d . U . . . O8 O 0.6580(4) 0.3157(3) 0.5824(5) 0.077(3) Uani 0.92 1 d . U . D . O9 O 0.7435(4) 0.3367(3) 0.6997(5) 0.089(3) Uani 1 1 d . U . . . O3 O 0.4483(4) 0.3960(3) 0.7818(5) 0.090(3) Uani 1 1 d . U . . . O14 O 0.6979(5) 0.3658(3) 0.5008(5) 0.102(3) Uani 1 1 d . U . . . O17 O 0.6037(6) 0.500000 0.2578(8) 0.104(5) Uani 1 2 d S TU P . . O13 O 0.7803(4) 0.3859(3) 0.6242(5) 0.099(3) Uani 1 1 d . U . . . O2 O 0.5074(4) 0.4576(3) 0.8199(6) 0.098(4) Uani 0.92 1 d . U . . . O1 O 0.6132(4) 0.4585(3) 0.9064(6) 0.104(3) Uani 1 1 d . U . . . C12 C 0.4923(5) 0.3105(3) 0.7652(6) 0.063(3) Uani 1 1 d D U . . . C59 C 0.7733(8) 0.500000 0.3652(9) 0.065(5) Uani 1 2 d S TU P . . C23 C 0.6232(6) 0.2698(4) 0.7069(7) 0.069(3) Uani 1 1 d . U . . . C7 C 0.4947(6) 0.3255(4) 0.8331(7) 0.076(3) Uani 1 1 d D U . . . H7 H 0.456542 0.332666 0.822193 0.091 Uiso 1 1 calc R . . . . C48 C 0.7794(5) 0.4188(3) 0.4373(7) 0.063(3) Uani 1 1 d . U . . . C24 C 0.6197(6) 0.2823(4) 0.6436(8) 0.072(3) Uani 1 1 d . U . . . C47 C 0.7359(6) 0.3973(4) 0.4380(8) 0.073(4) Uani 1 1 d . U . . . C56 C 0.7450(5) 0.4665(3) 0.3462(7) 0.064(3) Uani 1 1 d . U . . . C4 C 0.5276(6) 0.3594(4) 0.8539(8) 0.077(4) Uani 1 1 d . U . . . C15 C 0.4902(5) 0.2854(3) 0.6420(7) 0.062(3) Uani 1 1 d D U . . . C58 C 0.6594(9) 0.500000 0.2898(10) 0.077(5) Uani 1 2 d S TU P C . C13 C 0.4528(5) 0.3212(4) 0.7020(6) 0.065(3) Uani 1 1 d D U . . . C27 C 0.7099(6) 0.3024(4) 0.7708(7) 0.074(4) Uani 1 1 d . U . . . C18 C 0.5767(6) 0.2477(4) 0.7060(7) 0.078(4) Uani 1 1 d D U . . . C49 C 0.8204(5) 0.4289(4) 0.5022(7) 0.070(4) Uani 1 1 d . U . . . H49 H 0.848378 0.444359 0.502926 0.083 Uiso 1 1 calc R . . . . O11 O 0.7127(6) 0.4541(3) 0.9158(7) 0.141(5) Uani 1 1 d . U . . . C28 C 0.6685(6) 0.2812(4) 0.7670(8) 0.077(4) Uani 1 1 d . U . . . H28 H 0.670470 0.273080 0.809914 0.092 Uiso 1 1 calc R . . . . C14 C 0.4504(5) 0.3091(3) 0.6405(7) 0.067(3) Uani 1 1 d D U . . . C51 C 0.7751(5) 0.4300(4) 0.3686(7) 0.073(3) Uani 1 1 d D U . . . C5 C 0.5846(6) 0.3607(4) 0.8985(7) 0.073(4) Uani 1 1 d . U . . . H5 H 0.603543 0.338285 0.914401 0.087 Uiso 1 1 calc R . . . . C45 C 0.7822(7) 0.3978(4) 0.5642(8) 0.085(4) Uani 1 1 d . U . . . C57 C 0.6884(6) 0.4671(4) 0.3105(7) 0.074(4) Uani 1 1 d . U . . . C26 C 0.7050(6) 0.3138(4) 0.7050(8) 0.078(4) Uani 1 1 d . U . . . C29 C 0.7577(6) 0.3142(4) 0.8374(7) 0.081(4) Uani 1 1 d D U . . . H29 H 0.788639 0.317762 0.825603 0.098 Uiso 1 1 calc R . . . . O4AA O 0.8143(6) 0.4353(3) 0.7164(6) 0.132(5) Uani 1 1 d . U . . . C60 C 0.8717(7) 0.4299(4) 0.6344(8) 0.097(4) Uani 1 1 d D U . . . C61 C 0.8556(7) 0.4666(4) 0.6557(8) 0.096(4) Uani 1 1 d . U . . . C34 C 0.7470(6) 0.3527(5) 0.8605(8) 0.093(4) Uani 1 1 d . U . . . C50 C 0.8238(6) 0.4187(4) 0.5634(8) 0.076(4) Uani 1 1 d . U . . . C3 C 0.5020(6) 0.3929(4) 0.8252(8) 0.083(4) Uani 1 1 d . U . . . C8 C 0.5128(6) 0.2966(4) 0.8922(7) 0.085(4) Uani 1 1 d D U . . . H8A H 0.551010 0.289380 0.905459 0.102 Uiso 1 1 calc R . . . . H8B H 0.512040 0.307916 0.933425 0.102 Uiso 1 1 calc R . . . . O10 O 0.7897(5) 0.3827(4) 0.7992(7) 0.141(5) Uani 1 1 d . U . . . C46 C 0.7387(7) 0.3870(4) 0.5007(8) 0.081(4) Uani 1 1 d . U . . . C25 C 0.6611(6) 0.3032(4) 0.6421(8) 0.074(4) Uani 1 1 d . U . . . C6 C 0.6133(6) 0.3920(4) 0.9197(8) 0.087(4) Uani 1 1 d . U . . . C52 C 0.8309(6) 0.4316(4) 0.3688(8) 0.081(4) Uani 1 1 d D U . . . C38 C 0.7088(6) 0.3883(5) 0.9205(8) 0.084(4) Uani 1 1 d . U . . . C39 C 0.7191(6) 0.3561(4) 0.9011(8) 0.082(4) Uani 1 1 d . U . . . H39 H 0.707280 0.334640 0.915022 0.098 Uiso 1 1 calc R . . . . C19 C 0.5940(5) 0.2199(4) 0.7648(7) 0.082(4) Uani 1 1 d D U . . . H19A H 0.607752 0.233207 0.809580 0.098 Uiso 1 1 calc R . . . . H19B H 0.624537 0.205211 0.765701 0.098 Uiso 1 1 calc R . . . . C2 C 0.5328(7) 0.4250(4) 0.8459(9) 0.091(5) Uani 1 1 d . U . . . C1 C 0.5863(6) 0.4247(4) 0.8906(8) 0.087(4) Uani 1 1 d . U . . . C64 C 0.8676(9) 0.500000 0.6370(11) 0.091(6) Uani 1 2 d S TU P . . H64 H 0.885828 0.500001 0.608646 0.109 Uiso 1 2 calc RS T P . . C40 C 0.6769(6) 0.3923(4) 0.9649(8) 0.098(4) Uani 1 1 d D U . . . H40 H 0.686872 0.416599 0.988683 0.118 Uiso 1 1 calc R . . . . C30 C 0.7771(6) 0.2865(4) 0.8943(7) 0.098(5) Uani 1 1 d D U . . . H30A H 0.782502 0.263049 0.875456 0.118 Uiso 1 1 calc R . . . . H30B H 0.748125 0.282740 0.908944 0.118 Uiso 1 1 calc R . . . . C62 C 0.8286(9) 0.4682(5) 0.6988(9) 0.113(5) Uani 1 1 d . U . . . C41 C 0.6939(7) 0.3627(4) 1.0227(8) 0.098(5) Uiso 1 1 d D U . . . C9 C 0.4772(8) 0.2622(5) 0.8726(10) 0.127(6) Uiso 1 1 d D U . . . C3AA C 0.9264(6) 0.4301(5) 0.6318(8) 0.104(5) Uani 1 1 d D U . . . H3AA H 0.925869 0.449375 0.599300 0.125 Uiso 1 1 calc R . . . . H3AB H 0.931572 0.406317 0.613670 0.125 Uiso 1 1 calc R . . . . C35 C 0.7633(7) 0.3843(5) 0.8394(9) 0.106(5) Uani 1 1 d . U . . . C37 C 0.7247(8) 0.4204(5) 0.9006(10) 0.113(5) Uani 1 1 d . U . . . O7W O 0.6564(7) 0.3927(5) 0.6160(9) 0.193(7) Uiso 1 1 d . U . . . C33 C 0.8269(8) 0.2434(5) 1.0315(10) 0.125(6) Uiso 1 1 d D U . . . C31 C 0.8295(6) 0.2962(4) 0.9577(8) 0.101(5) Uiso 1 1 d D U . . . C36 C 0.7507(9) 0.4183(6) 0.8585(11) 0.129(6) Uani 1 1 d . U . . . C32 C 0.8599(9) 0.2627(5) 1.0025(11) 0.150(8) Uiso 1 1 d D U . . . C63 C 0.8119(12) 0.500000 0.7217(13) 0.122(8) Uani 1 2 d S TU P . . C20 C 0.5481(8) 0.1940(5) 0.7589(10) 0.136(7) Uiso 1 1 d D U . . . Co1A Co 0.5619(10) 0.500000 0.8466(12) 0.050(5) Uani 0.35 2 d S TU P A 2 O1W O 0.5381(12) 0.500000 0.9448(15) 0.230(12) Uiso 1 2 d S TU P . . O3W O 0.5665(9) 0.4532(6) 0.3464(12) 0.251(10) Uiso 1 1 d . U . . . C5AA C 0.9750(10) 0.4369(7) 0.7044(11) 0.177(9) Uiso 1 1 d D U . . . C53 C 0.8622(9) 0.3950(5) 0.3874(11) 0.145(7) Uiso 1 1 d D U . . . O4W O 0.5794(9) 0.4515(6) 0.1315(12) 0.250(9) Uiso 1 1 d . U . . . C7AA C 1.0304(13) 0.4332(10) 0.7021(18) 0.233(14) Uiso 1 1 d D U . . . C54 C 0.8297(12) 0.3643(8) 0.3401(15) 0.204(11) Uiso 1 1 d D U . . . C42 C 0.6714(12) 0.3724(8) 1.0755(14) 0.202(11) Uiso 1 1 d D U . . . O1S O 0.6272(4) 0.2455(3) 0.4933(6) 0.091(3) Uiso 1 1 d . U . . . O2S O 0.6876(6) 0.3044(4) 0.3965(7) 0.137(4) Uiso 1 1 d D U . . . Co2 Co 0.57407(9) 0.44895(6) 0.24304(15) 0.0823(10) Uani 0.75 1 d . U . C 2 Co4B Co 0.7286(7) 0.3457(5) 0.6038(10) 0.089(4) Uani 0.2 1 d . U . D 2 N1S N 0.6295(8) 0.1972(6) 0.4286(11) 0.167(7) Uiso 1 1 d . U . . . C1S C 0.6140(10) 0.2337(7) 0.4362(13) 0.150(8) Uiso 1 1 d . U . . . C3S C 0.6198(13) 0.1844(9) 0.3585(17) 0.217(12) Uiso 1 1 d . U . . . C2S C 0.6633(12) 0.1727(9) 0.4929(16) 0.206(12) Uiso 1 1 d . U . . . O8W O 1.000000 0.500000 0.500000 0.26(2) Uiso 1 4 d S TU P . . N2S N 0.7267(19) 0.2723(12) 0.339(2) 0.341(19) Uiso 1 1 d D U . . . C6S C 0.774(2) 0.2896(15) 0.319(3) 0.36(3) Uiso 1 1 d . U . . . O9W O 0.5491(10) 0.3469(6) 0.5114(12) 0.251(9) Uiso 1 1 d . U . . . O5W O 0.5939(10) 0.4026(7) 0.4087(13) 0.278(11) Uiso 1 1 d . U . . . C5S C 0.7320(16) 0.2418(12) 0.383(2) 0.245(15) Uiso 1 1 d D U . . . O2W O 0.5786(12) 0.500000 0.7743(15) 0.226(12) Uiso 1 2 d S TU P . . C44 C 0.6621(11) 0.3578(8) 1.1868(15) 0.188(10) Uiso 1 1 d D U . . . C10 C 0.4165(10) 0.2698(9) 0.8458(16) 0.201(11) Uiso 1 1 d D U . . . C21 C 0.5677(13) 0.1643(8) 0.8192(14) 0.210(12) Uiso 1 1 d D U . . . C43 C 0.6877(17) 0.3464(11) 1.1382(18) 0.297(19) Uiso 1 1 d D U . . . C22 C 0.5124(15) 0.1540(11) 0.815(2) 0.283(18) Uiso 1 1 d D U . . . C11 C 0.375(2) 0.2382(14) 0.812(3) 0.43(3) Uiso 1 1 d D U . . . O12 O 0.7510(13) 0.5448(9) 0.8339(17) 0.067(9) Uiso 0.25 1 d . U . . . O0AA O 0.769(2) 0.3010(15) 0.596(2) 0.47(2) Uiso 1 1 d . U . . . C1AA C 1.0821(18) 0.4453(14) 0.770(2) 0.36(2) Uiso 1 1 d D U . . . C4S C 0.7094(18) 0.3053(13) 0.358(2) 0.31(2) Uiso 1 1 d D U . . . C55 C 0.862(2) 0.3244(16) 0.360(3) 0.19(2) Uiso 0.5 1 d . U . . . C55' C 0.828(3) 0.4366(19) 0.302(4) 0.23(3) Uiso 0.5 1 d . U . . . C16 C 0.5312(5) 0.2736(3) 0.7046(6) 0.062(3) Uani 1 1 d D U . . . C17 C 0.5321(5) 0.2876(3) 0.7644(7) 0.064(3) Uani 1 1 d D U . . . H17 H 0.561729 0.281011 0.807673 0.077 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co5 0.0742(15) 0.0964(17) 0.0762(15) 0.0065(11) 0.0352(12) -0.0058(12) Co3 0.0770(16) 0.1013(18) 0.0850(16) 0.0046(12) 0.0337(13) -0.0183(12) Co4A 0.084(3) 0.069(3) 0.075(2) 0.0025(17) 0.038(2) -0.0038(17) Co1B 0.049(9) 0.058(5) 0.047(8) 0.000 0.029(5) 0.000 Co2' 0.125(7) 0.047(5) 0.095(6) -0.014(4) 0.091(6) -0.007(4) Co1' 0.127(10) 0.061(7) 0.085(8) 0.000 0.079(8) 0.000 O7 0.076(6) 0.092(7) 0.075(5) -0.003(5) 0.036(5) -0.004(5) O4 0.056(6) 0.089(7) 0.087(7) 0.008(5) 0.030(5) 0.007(5) O6 0.069(6) 0.090(7) 0.069(5) -0.010(5) 0.027(5) -0.010(5) O15 0.080(6) 0.082(7) 0.079(6) -0.003(5) 0.032(5) -0.010(5) O5 0.062(6) 0.064(7) 0.067(5) -0.007(5) 0.018(5) 0.003(5) O16 0.062(6) 0.071(6) 0.108(7) -0.005(5) 0.022(6) -0.004(4) O8 0.080(6) 0.088(7) 0.074(5) 0.007(5) 0.046(5) 0.002(5) O9 0.066(6) 0.120(8) 0.080(6) 0.018(5) 0.033(5) -0.001(5) O3 0.071(6) 0.070(7) 0.112(8) 0.003(6) 0.027(5) 0.017(5) O14 0.120(8) 0.097(8) 0.097(6) 0.001(6) 0.056(6) -0.031(6) O17 0.083(8) 0.069(8) 0.128(12) 0.000 0.020(9) 0.000 O13 0.127(8) 0.087(7) 0.086(6) 0.010(5) 0.051(6) -0.013(6) O2 0.070(7) 0.069(6) 0.122(9) -0.001(6) 0.016(6) -0.005(5) O1 0.094(7) 0.062(6) 0.137(9) -0.001(6) 0.034(6) 0.000(5) C12 0.065(8) 0.056(8) 0.074(6) 0.006(6) 0.036(6) -0.002(6) C59 0.081(12) 0.061(9) 0.053(11) 0.000 0.030(10) 0.000 C23 0.068(7) 0.068(9) 0.076(7) 0.002(7) 0.036(6) 0.008(6) C7 0.082(9) 0.070(8) 0.085(7) 0.005(6) 0.046(8) 0.010(6) C48 0.062(8) 0.056(8) 0.066(6) 0.009(6) 0.025(6) 0.008(6) C24 0.071(8) 0.067(9) 0.079(6) 0.005(7) 0.035(6) 0.006(7) C47 0.076(8) 0.066(9) 0.078(7) -0.003(7) 0.035(6) -0.003(6) C56 0.066(6) 0.060(7) 0.065(8) -0.004(6) 0.030(7) -0.001(5) C4 0.083(7) 0.064(7) 0.087(10) -0.003(6) 0.041(7) 0.012(6) C15 0.068(8) 0.045(8) 0.068(6) -0.004(6) 0.026(6) -0.005(6) C58 0.075(9) 0.072(9) 0.069(13) 0.000 0.019(10) 0.000 C13 0.055(8) 0.062(9) 0.073(6) -0.001(7) 0.024(6) 0.002(6) C27 0.056(8) 0.091(10) 0.075(6) 0.019(7) 0.029(6) 0.015(6) C18 0.075(8) 0.060(9) 0.108(10) 0.011(7) 0.050(8) 0.008(5) C49 0.063(8) 0.063(9) 0.078(6) 0.003(7) 0.028(6) 0.002(7) O11 0.203(14) 0.083(7) 0.155(11) -0.009(8) 0.097(10) -0.031(9) C28 0.064(8) 0.082(10) 0.086(8) 0.004(8) 0.035(6) 0.010(6) C14 0.064(8) 0.057(9) 0.070(6) 0.004(6) 0.022(6) 0.000(6) C51 0.088(8) 0.071(8) 0.076(7) 0.000(7) 0.051(8) 0.013(7) C5 0.078(7) 0.059(8) 0.091(10) 0.013(7) 0.047(7) 0.016(6) C45 0.114(10) 0.059(10) 0.076(7) 0.007(7) 0.037(7) -0.010(7) C57 0.068(6) 0.071(8) 0.080(10) -0.008(7) 0.031(7) -0.004(5) C26 0.068(8) 0.095(11) 0.072(6) 0.011(7) 0.032(6) 0.010(7) C29 0.069(9) 0.100(9) 0.077(7) 0.008(6) 0.035(6) -0.008(7) O4AA 0.210(14) 0.100(8) 0.097(8) 0.010(7) 0.079(9) -0.010(9) C60 0.112(9) 0.070(9) 0.077(8) 0.017(7) 0.016(7) 0.000(8) C61 0.117(12) 0.079(9) 0.055(9) 0.011(7) 0.007(8) -0.001(8) C34 0.078(11) 0.109(8) 0.088(11) 0.005(8) 0.034(8) -0.013(8) C50 0.094(9) 0.052(9) 0.074(7) 0.004(6) 0.030(7) 0.003(7) C3 0.067(7) 0.069(7) 0.099(11) -0.004(7) 0.027(7) 0.006(6) C8 0.092(11) 0.086(10) 0.075(9) 0.009(7) 0.037(9) 0.008(9) O10 0.137(11) 0.178(13) 0.133(10) -0.017(9) 0.083(9) -0.062(9) C46 0.104(10) 0.061(10) 0.084(6) -0.008(7) 0.047(7) -0.014(7) C25 0.070(8) 0.086(10) 0.070(6) 0.007(7) 0.036(6) 0.003(7) C6 0.084(7) 0.073(8) 0.091(11) 0.001(8) 0.028(7) 0.005(6) C52 0.092(9) 0.087(11) 0.081(10) 0.022(8) 0.054(9) 0.027(8) C38 0.071(9) 0.081(8) 0.077(10) -0.003(8) 0.013(7) -0.006(8) C39 0.070(10) 0.085(9) 0.085(11) 0.008(8) 0.030(8) -0.001(8) C19 0.071(10) 0.076(10) 0.103(11) 0.013(7) 0.043(9) 0.010(7) C2 0.081(8) 0.064(7) 0.116(12) 0.007(8) 0.035(8) 0.003(6) C1 0.078(8) 0.065(7) 0.099(11) -0.001(7) 0.022(7) -0.004(6) C64 0.097(16) 0.073(10) 0.069(14) 0.000 0.009(11) 0.000 C40 0.086(8) 0.103(12) 0.083(11) -0.005(9) 0.019(7) 0.011(8) C30 0.076(10) 0.125(12) 0.078(9) 0.021(8) 0.021(9) -0.013(9) C62 0.160(17) 0.086(10) 0.083(12) 0.007(9) 0.047(10) -0.003(10) C3AA 0.093(9) 0.088(12) 0.082(11) 0.016(9) -0.003(9) 0.006(9) C35 0.109(13) 0.110(9) 0.105(13) -0.007(10) 0.052(10) -0.038(11) C37 0.120(15) 0.090(8) 0.112(14) -0.015(10) 0.037(10) -0.031(10) C36 0.151(18) 0.112(11) 0.122(15) -0.016(12) 0.060(12) -0.046(12) C63 0.16(2) 0.071(12) 0.106(19) 0.000 0.034(15) 0.000 Co1A 0.041(6) 0.040(5) 0.087(15) 0.000 0.044(8) 0.000 Co2 0.0419(16) 0.0367(16) 0.122(2) -0.0007(14) -0.0030(15) -0.0032(12) Co4B 0.089(7) 0.086(8) 0.104(8) 0.025(6) 0.056(6) 0.011(5) C16 0.064(7) 0.049(8) 0.074(6) 0.006(6) 0.033(6) -0.005(6) C17 0.058(8) 0.062(9) 0.068(7) 0.010(6) 0.025(7) 0.003(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O7 Co5 O6 95.6(4) . 2_656 O7 Co5 O8 82.3(4) . . O7 Co5 O1S 94.1(4) . . O7 Co5 O9W 86.3(6) . . O6 Co5 O9W 90.3(7) 2_656 . O5 Co5 O7 168.3(4) 2_656 . O5 Co5 O6 80.7(4) 2_656 2_656 O5 Co5 O8 100.2(4) 2_656 . O5 Co5 O1S 97.0(4) 2_656 . O5 Co5 O9W 82.7(7) 2_656 . O8 Co5 O6 173.8(4) . 2_656 O8 Co5 O1S 96.3(4) . . O8 Co5 O9W 83.7(7) . . O1S Co5 O6 89.6(4) . 2_656 O1S Co5 O9W 179.6(7) . . O4 Co3 O15 92.6(4) 2_656 . O4 Co3 O2S 91.2(5) 2_656 . O4 Co3 O5W 86.7(7) 2_656 . O15 Co3 O2S 92.0(5) . . O15 Co3 O5W 88.7(7) . . O5 Co3 O4 82.9(4) 2_656 2_656 O5 Co3 O15 174.6(4) 2_656 . O5 Co3 O2S 90.9(5) 2_656 . O5 Co3 O5W 88.2(7) 2_656 . O14 Co3 O4 170.9(4) . 2_656 O14 Co3 O15 82.0(4) . . O14 Co3 O5 102.1(4) . 2_656 O14 Co3 O2S 96.3(5) . . O14 Co3 O5W 85.8(7) . . O2S Co3 O5W 177.8(7) . . O8 Co4A O9 80.1(4) . . O8 Co4A O13 154.7(4) . . O14 Co4A O8 99.8(4) . . O14 Co4A O9 153.4(5) . . O14 Co4A O13 82.5(4) . . O14 Co4A O7W 111.8(6) . . O13 Co4A O9 86.7(4) . . O7W Co4A O8 93.4(6) . . O7W Co4A O9 94.7(6) . . O7W Co4A O13 109.2(6) . . Co4B Co4A O8 85.7(16) . . Co4B Co4A O9 65.4(15) . . Co4B Co4A O14 88.1(16) . . Co4B Co4A O13 69.1(16) . . Co4B Co4A O7W 159.9(17) . . O2 Co1B O2 104.1(12) 6_565 . O2 Co1B O1 81.0(4) 6_565 6_565 O2 Co1B O1 81.0(4) . . O2 Co1B O1 168.9(9) . 6_565 O2 Co1B O1 168.9(9) 6_565 . O2 Co1B O2W 87.0(8) 6_565 . O2 Co1B O2W 87.0(8) . . O1 Co1B O1 92.3(11) . 6_565 O1 Co1B O2W 83.5(8) 6_565 . O1 Co1B O2W 83.5(8) . . O1W Co1B O2 95.1(9) . . O1W Co1B O2 95.1(9) . 6_565 O1W Co1B O1 94.3(10) . 6_565 O1W Co1B O1 94.3(10) . . O1W Co1B O2W 176.7(17) . . O4AA Co2' C63 64.2(7) 6_565 . O4AA Co2' O12 171.9(12) 6_565 . O12 Co2' C63 122.1(12) . . O11 Co1' O11 111.5(9) . 6_565 O11 Co1' O12 72.2(10) . 6_565 O11 Co1' O12 72.2(10) 6_565 . O11 Co1' O12 171.7(12) 6_565 6_565 O11 Co1' O12 171.7(12) . . O12 Co1' O12 103.1(19) 6_565 . C24 O7 Co5 111.6(8) . . C13 O4 Co3 110.3(7) . 2_656 C15 O6 Co5 109.9(7) . 2_656 C47 O15 Co3 110.0(8) . . Co5 O5 Co3 137.2(5) 2_656 2_656 C14 O5 Co5 112.1(7) . 2_656 C14 O5 Co3 109.8(7) . 2_656 C57 O16 Co2 109.8(8) . . Co5 O8 Co4B 142.4(7) . . Co4A O8 Co5 136.9(5) . . Co4A O8 Co4B 21.2(4) . . C25 O8 Co5 108.4(9) . . C25 O8 Co4A 111.7(9) . . C25 O8 Co4B 108.7(10) . . C26 O9 Co4A 107.0(8) . . C26 O9 Co4B 112.8(10) . . Co4B O9 Co4A 20.7(4) . . C3 O3 Co2 111.5(9) . 2_656 Co3 O14 Co4A 137.2(6) . . Co3 O14 Co4B 139.4(7) . . Co4A O14 Co4B 20.9(4) . . C46 O14 Co3 111.4(9) . . C46 O14 Co4A 111.2(9) . . C46 O14 Co4B 105.2(10) . . C58 O17 Co2 111.2(4) . 6_565 C58 O17 Co2 111.2(4) . . Co2 O17 Co2 137.5(8) 6_565 . C45 O13 Co4A 109.4(9) . . C45 O13 Co4B 111.0(10) . . Co4B O13 Co4A 21.3(4) . . Co1B O2 Co2 136.1(8) . 2_656 C2 O2 Co1B 112.8(11) . . C2 O2 Co1A 112.0(11) . . C2 O2 Co2 109.7(9) . 2_656 Co2 O2 Co1A 137.9(8) 2_656 . C1 O1 Co1B 108.2(10) . . C1 O1 Co1A 111.1(10) . . C13 C12 C7 121.4(11) . . C13 C12 C17 116.0(12) . . C17 C12 C7 122.4(11) . . C56 C59 C56 121.0(18) 6_565 . C24 C23 C18 118.8(13) . . C28 C23 C24 116.4(13) . . C28 C23 C18 124.6(13) . . C12 C7 H7 106.4 . . C12 C7 C8 113.3(11) . . C4 C7 C12 110.2(11) . . C4 C7 H7 106.4 . . C4 C7 C8 113.5(12) . . C8 C7 H7 106.4 . . C47 C48 C51 118.1(12) . . C49 C48 C47 115.6(12) . . C49 C48 C51 126.2(12) . . O7 C24 C23 123.6(13) . . O7 C24 C25 115.8(13) . . C25 C24 C23 120.7(14) . . O15 C47 C48 123.4(13) . . O15 C47 C46 117.5(13) . . C46 C47 C48 119.1(14) . . C59 C56 C51 121.4(12) . . C57 C56 C59 118.5(13) . . C57 C56 C51 119.9(12) . . C5 C4 C7 124.6(13) . . C3 C4 C7 118.9(13) . . C3 C4 C5 116.4(14) . . O6 C15 C14 115.9(11) . . O6 C15 C16 123.8(11) . . C16 C15 C14 120.3(12) . . O17 C58 C57 120.5(10) . . O17 C58 C57 120.5(10) . 6_565 C57 C58 C57 118(2) 6_565 . C12 C13 O4 121.0(11) . . C12 C13 C14 122.8(12) . . C14 C13 O4 116.1(10) . . C28 C27 C26 114.2(14) . . C28 C27 C29 124.8(13) . . C26 C27 C29 121.0(13) . . C23 C18 C19 114.0(12) . . C23 C18 C16 109.8(11) . . C19 C18 C16 111.6(11) . . C48 C49 H49 117.1 . . C50 C49 C48 125.8(14) . . C50 C49 H49 117.1 . . C37 O11 Co1' 121.9(13) . . C23 C28 H28 116.5 . . C27 C28 C23 127.1(15) . . C27 C28 H28 116.5 . . O5 C14 C15 120.3(11) . . O5 C14 C13 120.3(11) . . C13 C14 C15 119.3(12) . . C48 C51 C56 110.0(10) . . C48 C51 C52 112.4(11) . . C52 C51 C56 111.3(11) . . C4 C5 H5 118.1 . . C6 C5 C4 123.7(14) . . C6 C5 H5 118.1 . . O13 C45 C46 116.4(14) . . C50 C45 O13 124.5(14) . . C50 C45 C46 119.1(14) . . O16 C57 C56 122.3(12) . . O16 C57 C58 116.0(13) . . C56 C57 C58 121.6(14) . . O9 C26 C27 121.6(13) . . O9 C26 C25 116.1(13) . . C25 C26 C27 122.3(14) . . C27 C29 H29 105.6 . . C27 C29 C34 110.7(12) . . C34 C29 H29 105.6 . . C30 C29 C27 114.9(12) . . C30 C29 H29 105.6 . . C30 C29 C34 113.5(13) . . C62 O4AA Co2' 103.7(12) . 6_565 C61 C60 C50 107.1(12) . . C3AA C60 C61 115.1(14) . . C3AA C60 C50 111.8(13) . . C64 C61 C60 123.2(18) . . C64 C61 C62 114.6(18) . . C62 C61 C60 122.1(15) . . C39 C34 C29 120.7(14) . . C35 C34 C29 120.6(16) . . C35 C34 C39 118.6(17) . . C49 C50 C45 118.6(14) . . C49 C50 C60 123.5(14) . . C45 C50 C60 117.9(14) . . O3 C3 C4 123.2(14) . . O3 C3 C2 117.8(13) . . C2 C3 C4 118.9(14) . . C7 C8 H8A 108.7 . . C7 C8 H8B 108.7 . . H8A C8 H8B 107.6 . . C9 C8 C7 114.1(13) . . C9 C8 H8A 108.7 . . C9 C8 H8B 108.7 . . O14 C46 C47 118.6(14) . . O14 C46 C45 119.7(14) . . C47 C46 C45 121.8(15) . . O8 C25 C24 121.2(14) . . O8 C25 C26 119.4(13) . . C24 C25 C26 119.2(14) . . C5 C6 C1 117.7(14) . . C5 C6 C40 122.3(14) . . C1 C6 C40 119.2(14) . . C51 C52 C53 113.9(13) . . C55' C52 C51 114(3) . . C55' C52 C53 98(3) . . C39 C38 C40 122.2(15) . . C39 C38 C37 121.1(18) . . C37 C38 C40 116.7(16) . . C34 C39 H39 119.0 . . C38 C39 C34 121.9(16) . . C38 C39 H39 119.0 . . C18 C19 H19A 108.7 . . C18 C19 H19B 108.7 . . C18 C19 C20 114.2(13) . . H19A C19 H19B 107.6 . . C20 C19 H19A 108.7 . . C20 C19 H19B 108.7 . . O2 C2 C3 118.7(14) . . C1 C2 O2 119.3(14) . . C1 C2 C3 122.0(15) . . C6 C1 O1 122.2(14) . . C2 C1 O1 116.9(14) . . C2 C1 C6 120.9(15) . . C61 C64 C61 126(3) . 6_565 C61 C64 H64 117.1 . . C61 C64 H64 117.1 6_565 . C6 C40 C38 113.1(12) . . C6 C40 H40 107.2 . . C38 C40 H40 107.2 . . C41 C40 C6 109.8(13) . . C41 C40 C38 112.0(13) . . C41 C40 H40 107.2 . . C29 C30 H30A 108.5 . . C29 C30 H30B 108.5 . . C29 C30 C31 115.1(13) . . H30A C30 H30B 107.5 . . C31 C30 H30A 108.5 . . C31 C30 H30B 108.5 . . O4AA C62 C61 116.1(16) . . O4AA C62 C63 116(2) . . C63 C62 C61 127(2) . . C40 C41 C42 110.5(17) . . C10 C9 C8 114.0(19) . . C60 C3AA H3AA 109.2 . . C60 C3AA H3AB 109.2 . . C60 C3AA C5AA 111.9(16) . . H3AA C3AA H3AB 107.9 . . C5AA C3AA H3AA 109.2 . . C5AA C3AA H3AB 109.2 . . C34 C35 C36 118.8(19) . . O10 C35 C34 121.2(18) . . O10 C35 C36 119.9(18) . . O11 C37 C38 123.5(19) . . O11 C37 C36 117.5(19) . . C38 C37 C36 118.8(19) . . C30 C31 C32 113.7(15) . . C35 C36 O12 132(2) . 6_565 C37 C36 C35 120.6(19) . . C37 C36 O12 106(2) . 6_565 C33 C32 C31 112.2(16) . . C62 C63 Co2' 172.7(17) . . C62 C63 Co2' 172.7(17) 6_565 6_565 C62 C63 Co2' 75.1(10) 6_565 . C62 C63 Co2' 75.1(10) . 6_565 C62 C63 C62 110(3) . 6_565 C19 C20 C21 113.2(18) . . O2 Co1A O2 98.5(12) 6_565 . O2 Co1A O1 79.9(4) . . O2 Co1A O1 158.8(11) . 6_565 O2 Co1A O1 158.8(11) 6_565 . O2 Co1A O1 79.9(4) 6_565 6_565 O1 Co1A O1 94.0(12) 6_565 . O2W Co1A O2 101.3(11) . . O2W Co1A O2 101.3(11) . 6_565 O2W Co1A O1 99.7(10) . . O2W Co1A O1 99.7(10) . 6_565 C3AA C5AA C7AA 111(2) . . C54 C53 C52 112.5(19) . . C5AA C7AA C1AA 115(3) . . C53 C54 C55 113(3) . . C43 C42 C41 116(2) . . C1S O1S Co5 117.8(14) . . C4S O2S Co3 119(3) . . O16 Co2 O3W 94.8(6) . . O3 Co2 O16 92.3(4) 2_656 . O3 Co2 O2 82.2(4) 2_656 2_656 O3 Co2 O3W 99.7(7) 2_656 . O17 Co2 O16 82.3(5) . . O17 Co2 O3 169.8(6) . 2_656 O17 Co2 O2 101.7(5) . 2_656 O17 Co2 O3W 89.5(8) . . O2 Co2 O16 169.9(5) 2_656 . O2 Co2 O3W 94.5(7) 2_656 . Co4A Co4B O8 73.1(15) . . Co4A Co4B O9 93.9(17) . . Co4A Co4B O14 71.0(14) . . Co4A Co4B O13 89.6(17) . . Co4A Co4B O0AA 162(3) . . O8 Co4B O14 93.6(8) . . O9 Co4B O8 82.6(7) . . O9 Co4B O14 164.9(10) . . O9 Co4B O13 96.2(9) . . O9 Co4B O0AA 95.4(15) . . O13 Co4B O8 162.5(9) . . O13 Co4B O14 83.0(7) . . O13 Co4B O0AA 105.1(16) . . O0AA Co4B O8 92.4(16) . . O0AA Co4B O14 99.5(16) . . C1S N1S C3S 119(2) . . C1S N1S C2S 122(2) . . C3S N1S C2S 119(2) . . O1S C1S N1S 119(2) . . C5S N2S C6S 128(4) . . C4S N2S C6S 99(4) . . C4S N2S C5S 115(5) . . N2S C5S O0AA 158(4) . 7_656 C9 C10 C11 119(3) . . C22 C21 C20 99(2) . . C42 C43 C44 112(3) . . Co2' O12 Co1' 136.5(19) . . C36 O12 Co2' 101(2) 6_565 . C36 O12 Co1' 122(2) 6_565 . C5S O0AA Co4B 133(3) 7_656 . O2S C4S N2S 120(4) . . C15 C16 C18 120.2(11) . . C17 C16 C15 117.5(12) . . C17 C16 C18 122.2(11) . . C12 C17 H17 118.0 . . C16 C17 C12 123.9(12) . . C16 C17 H17 118.0 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Co5 O7 2.003(9) . Co5 O6 2.131(9) 2_656 Co5 O5 1.999(9) 2_656 Co5 O8 2.047(10) . Co5 O1S 2.095(10) . Co5 O9W 2.30(2) . Co3 O4 2.027(9) 2_656 Co3 O15 2.049(9) . Co3 O5 2.026(9) 2_656 Co3 O14 1.997(11) . Co3 O2S 2.161(14) . Co3 O5W 2.34(3) . Co4A O8 2.007(11) . Co4A O9 2.137(10) . Co4A O14 2.002(10) . Co4A O13 2.088(11) . Co4A O7W 2.004(18) . Co4A Co4B 0.757(13) . Co1B O2 1.969(18) . Co1B O2 1.969(18) 6_565 Co1B O1 2.106(19) 6_565 Co1B O1 2.106(19) . Co1B O1W 1.94(3) . Co1B O2W 2.36(3) . Co2' O4AA 1.836(14) 6_565 Co2' C63 2.50(2) . Co2' O12 1.91(3) . Co1' O11 2.033(13) 6_565 Co1' O11 2.033(13) . Co1' O12 2.09(3) . Co1' O12 2.09(3) 6_565 O7 C24 1.360(16) . O4 C13 1.405(15) . O6 C15 1.369(15) . O15 C47 1.369(16) . O5 C14 1.367(14) . O16 C57 1.383(16) . O16 Co2 2.097(9) . O8 C25 1.333(15) . O8 Co4B 2.09(2) . O9 C26 1.393(17) . O9 Co4B 1.95(2) . O3 C3 1.347(16) . O3 Co2 2.031(9) 2_656 O14 C46 1.365(17) . O14 Co4B 2.12(2) . O17 C58 1.36(2) . O17 Co2 2.006(6) . O17 Co2 2.006(6) 6_565 O13 C45 1.389(17) . O13 Co4B 1.95(2) . O2 C2 1.368(17) . O2 Co1A 2.049(19) . O2 Co2 2.047(10) 2_656 O1 C1 1.402(17) . O1 Co1A 2.08(2) . C12 C7 1.537(17) . C12 C13 1.359(12) . C12 C17 1.384(12) . C59 C56 1.409(15) 6_565 C59 C56 1.409(15) . C23 C24 1.402(18) . C23 C18 1.503(19) . C23 C28 1.392(19) . C7 H7 1.0000 . C7 C4 1.480(19) . C7 C8 1.555(14) . C48 C47 1.437(18) . C48 C49 1.390(17) . C48 C51 1.488(18) . C24 C25 1.381(19) . C47 C46 1.371(19) . C56 C51 1.532(18) . C56 C57 1.387(18) . C4 C5 1.418(19) . C4 C3 1.411(19) . C15 C14 1.385(12) . C15 C16 1.378(12) . C58 C57 1.400(17) . C58 C57 1.400(17) 6_565 C13 C14 1.371(12) . C27 C28 1.349(19) . C27 C26 1.425(18) . C27 C29 1.504(19) . C18 C19 1.522(14) . C18 C16 1.559(18) . C49 H49 0.9500 . C49 C50 1.332(17) . O11 C37 1.36(2) . C28 H28 0.9500 . C51 C52 1.530(14) . C5 H5 0.9500 . C5 C6 1.349(19) . C45 C50 1.38(2) . C45 C46 1.40(2) . C26 C25 1.400(19) . C29 H29 1.0000 . C29 C34 1.57(2) . C29 C30 1.492(14) . O4AA C62 1.37(2) . C60 C61 1.55(2) . C60 C50 1.55(2) . C60 C3AA 1.528(16) . C61 C64 1.374(19) . C61 C62 1.43(2) . C34 C39 1.40(2) . C34 C35 1.39(2) . C3 C2 1.40(2) . C8 H8A 0.9900 . C8 H8B 0.9900 . C8 C9 1.531(16) . O10 C35 1.36(2) . C6 C1 1.40(2) . C6 C40 1.57(2) . C52 C53 1.545(16) . C52 C55' 1.41(7) . C38 C39 1.324(19) . C38 C40 1.57(2) . C38 C37 1.39(2) . C39 H39 0.9500 . C19 H19A 0.9900 . C19 H19B 0.9900 . C19 C20 1.536(16) . C2 C1 1.34(2) . C64 H64 0.9500 . C40 H40 1.0000 . C40 C41 1.556(15) . C30 H30A 0.9900 . C30 H30B 0.9900 . C30 C31 1.510(15) . C62 C63 1.42(2) . C41 C42 1.562(18) . C9 C10 1.523(18) . C3AA H3AA 0.9900 . C3AA H3AB 0.9900 . C3AA C5AA 1.550(17) . C35 C36 1.40(3) . C37 C36 1.39(3) . C33 C32 1.494(17) . C31 C32 1.549(16) . C36 O12 1.45(4) 6_565 C20 C21 1.589(18) . Co1A O2W 1.81(4) . O3W Co2 2.34(2) . C5AA C7AA 1.552(19) . C53 C54 1.509(18) . C7AA C1AA 1.57(2) . C54 C55 1.67(6) . C42 C43 1.545(19) . O1S C1S 1.20(2) . O2S C4S 1.218(19) . Co4B O0AA 2.02(5) . N1S C1S 1.44(3) . N1S C3S 1.49(3) . N1S C2S 1.55(3) . N2S C6S 1.67(6) . N2S C5S 1.43(2) . N2S C4S 1.43(2) . C5S O0AA 1.64(5) 7_656 C44 C43 1.560(19) . C10 C11 1.56(2) . C21 C22 1.532(19) . C16 C17 1.377(12) . C17 H17 0.9500 .