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Information card for entry 4127308
Preview
| Coordinates | 4127308.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23.5 H42.5 B I1.5 N5 O2 |
|---|---|
| Calculated formula | C23.5 H42.5 B I1.5 N5 O2 |
| Title of publication | A Versatile NHC-Parent Silyliumylidene Cation for Catalytic Chemo- and Regioselective Hydroboration. |
| Authors of publication | Leong, Bi-Xiang; Lee, Jiawen; Li, Yan; Yang, Ming-Chung; Siu, Chi-Kit; Su, Ming-Der; So, Cheuk-Wai |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2019 |
| a | 13.0847 ± 0.0006 Å |
| b | 32.8113 ± 0.0016 Å |
| c | 13.7965 ± 0.0007 Å |
| α | 90° |
| β | 106.296 ± 0.0018° |
| γ | 90° |
| Cell volume | 5685.2 ± 0.5 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0868 |
| Residual factor for significantly intense reflections | 0.0451 |
| Weighted residual factors for significantly intense reflections | 0.0799 |
| Weighted residual factors for all reflections included in the refinement | 0.0967 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 219577 (current) | 2019-10-28 | cif/ Adding structures of 4127308 via cif-deposit CGI script. |
4127308.cif |
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