#------------------------------------------------------------------------------ #$Date: 2019-11-25 23:48:59 +0200 (Mon, 25 Nov 2019) $ #$Revision: 242092 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/20/4132050.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132050 loop_ _publ_author_name 'Spanopoulos, Ioannis' 'Ke, Weijun' 'Stoumpos, Constantinos C.' 'Schueller, Emily C.' 'Kontsevoi, Oleg Y.' 'Seshadri, Ram' 'Kanatzidis, Mercouri G.' _publ_section_title ; Unraveling the Chemical Nature of the 3D "Hollow" Hybrid Halide Perovskites. ; _journal_issue 17 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 5728 _journal_page_last 5742 _journal_paper_doi 10.1021/jacs.8b01034 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety (H3NCH2CH2NH3)I2 _chemical_formula_sum 'C2 H10 I2 N2' _chemical_formula_weight 315.9 _chemical_name_common 'ethylenediamonium iodide' _space_group_IT_number 12 _space_group_name_Hall '-I 2y' _space_group_name_H-M_alt 'I 1 2/m 1' _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 12 _symmetry_space_group_name_Hall '-I 2y' _symmetry_space_group_name_H-M 'I 1 2/m 1' _cell_angle_alpha 90 _cell_angle_beta 96.032(11) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 15.540(2) _cell_length_b 5.0795(6) _cell_length_c 5.0964(7) _cell_measurement_reflns_used 2409 _cell_measurement_temperature 293 _cell_measurement_theta_max 29.01 _cell_measurement_theta_min 2.64 _cell_volume 400.06(9) _diffrn_ambient_temperature 293 _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 0.99 _diffrn_measured_fraction_theta_max 0.99 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'IPDS Stoe' _diffrn_measurement_method 'rotation method' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0623 _diffrn_reflns_av_unetI/netI 0.0145 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 6 _diffrn_reflns_limit_l_min -6 _diffrn_reflns_number 1850 _diffrn_reflns_theta_full 29.12 _diffrn_reflns_theta_max 29.12 _diffrn_reflns_theta_min 2.64 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _diffrn_source_current 40 _diffrn_source_power 2.00 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 7.763 _exptl_absorpt_correction_T_max 0.4024 _exptl_absorpt_correction_T_min 0.2314 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details X-Shape _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 2.6226 _exptl_crystal_description 'colorless plate' _exptl_crystal_F_000 282 _exptl_crystal_size_max 0.1172 _exptl_crystal_size_mid 0.0611 _exptl_crystal_size_min 0.0520 _refine_diff_density_max 1.94 _refine_diff_density_min -1.77 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_gt 3.38 _refine_ls_goodness_of_fit_ref 3.24 _refine_ls_hydrogen_treatment constr _refine_ls_number_constraints 20 _refine_ls_number_parameters 20 _refine_ls_number_reflns 589 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0518 _refine_ls_R_factor_gt 0.0450 _refine_ls_shift/su_max 0.0381 _refine_ls_shift/su_mean 0.0039 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details w=1/(\s^2^(I)+0.0004I^2^) _refine_ls_weighting_scheme sigma _refine_ls_wR_factor_gt 0.1061 _refine_ls_wR_factor_ref 0.1071 _reflns_number_gt 533 _reflns_number_total 589 _reflns_threshold_expression I>2\s(I) _cod_data_source_file ja8b01034_si_006.cif _cod_data_source_block I _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas ; _cod_original_sg_symbol_Hall -I _cod_original_sg_symbol_H-M I2/m _cod_database_code 4132050 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y,-z 3 -x,-y,-z 4 x,-y,z 5 x+1/2,y+1/2,z+1/2 6 -x+1/2,y+1/2,-z+1/2 7 -x+1/2,-y+1/2,-z+1/2 8 x+1/2,-y+1/2,z+1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag I1 I 0.85012(6) 0 0.02190(17) Uani 0.0387(2) 4 1 d N1 N 0.3784(7) 0 0.022(2) Uani 0.040(3) 4 1 d C2 C 0.4719(8) 0 0.109(2) Uani 0.047(4) 4 1 d H1n1 H 0.367283 -0.11562 -0.102456 Uiso 0.0478 8 0.25 d H2n1 H 0.349865 -0.039818 0.155047 Uiso 0.0478 8 0.5 d H3n1 H 0.362821 0.155438 -0.036493 Uiso 0.0478 8 0.5 d H1c2 H 0.485875 -0.148974 0.221715 Uiso 0.057 8 0.5 d H2c2 H 0.485875 0.148974 0.221715 Uiso 0.057 8 0.5 d loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 I1 I 0.0365(4) 0.0379(4) 0.0414(4) 0 0.0031(3) 0 N1 N 0.036(5) 0.038(5) 0.045(5) 0 0.002(4) 0 C2 C 0.026(6) 0.081(10) 0.036(6) 0 0.008(5) 0 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C 0.0033 0.0016 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' I -0.4742 1.8119 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' N 0.0061 0.0033 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -30 -1 29 0.1043 -16 -10 -30 0.0976 -10 30 0 0.1029 9 -30 -2 0.1172 30 -1 0 0.0520 -30 0 1 0.0611 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle N1 I1 N1 5_544 5_545 89.35(17) N1 I1 N1 5_544 5_554 88.04(17) N1 I1 N1 5_544 5_555 166.1(2) N1 I1 N1 5_544 2_655 98.6(2) N1 I1 N1 5_545 5_554 166.1(2) N1 I1 N1 5_545 5_555 89.93(17) N1 I1 N1 5_545 2_655 95.3(2) N1 I1 N1 5_554 5_555 89.35(17) N1 I1 N1 5_554 2_655 98.6(2) N1 I1 N1 5_555 2_655 95.3(2) I1 N1 I1 5_444 5_445 89.35(4) I1 N1 I1 5_444 5_454 89.9(2) I1 N1 I1 5_444 5_455 166.1(3) I1 N1 I1 5_444 2_655 84.69(19) I1 N1 C2 5_444 . 104.9(5) I1 N1 H1n1 5_444 . 4.77 I1 N1 H1n1 5_444 4_555 87.57 I1 N1 H2n1 5_444 . 110.66 I1 N1 H2n1 5_444 4_555 132.95 I1 N1 H3n1 5_444 . 112.79 I1 N1 H3n1 5_444 4_555 26.45 I1 N1 I1 5_445 5_454 166.1(3) I1 N1 I1 5_445 5_455 88.0(2) I1 N1 I1 5_445 2_655 81.4(2) I1 N1 C2 5_445 . 88.7(5) I1 N1 H1n1 5_445 . 90.65 I1 N1 H1n1 5_445 4_555 161.74 I1 N1 H2n1 5_445 . 35.83 I1 N1 H2n1 5_445 4_555 60.81 I1 N1 H3n1 5_445 . 145.26 I1 N1 H3n1 5_445 4_555 63.92 I1 N1 I1 5_454 5_455 89.35(4) I1 N1 I1 5_454 2_655 84.69(19) I1 N1 C2 5_454 . 104.9(5) I1 N1 H1n1 5_454 . 87.57 I1 N1 H1n1 5_454 4_555 4.77 I1 N1 H2n1 5_454 . 132.95 I1 N1 H2n1 5_454 4_555 110.66 I1 N1 H3n1 5_454 . 26.45 I1 N1 H3n1 5_454 4_555 112.79 I1 N1 I1 5_455 2_655 81.4(2) I1 N1 C2 5_455 . 88.7(5) I1 N1 H1n1 5_455 . 161.74 I1 N1 H1n1 5_455 4_555 90.65 I1 N1 H2n1 5_455 . 60.81 I1 N1 H2n1 5_455 4_555 35.83 I1 N1 H3n1 5_455 . 63.92 I1 N1 H3n1 5_455 4_555 145.26 I1 N1 C2 2_655 . 166.3(8) I1 N1 H1n1 2_655 . 80.36 I1 N1 H1n1 2_655 4_555 80.36 I1 N1 H2n1 2_655 . 57.26 I1 N1 H2n1 2_655 4_555 57.26 I1 N1 H3n1 2_655 . 74.74 I1 N1 H3n1 2_655 4_555 74.74 C2 N1 H1n1 . . 109.47 C2 N1 H1n1 . 4_555 109.47 C2 N1 H2n1 . . 109.47 C2 N1 H2n1 . 4_555 109.47 C2 N1 H3n1 . . 109.47 C2 N1 H3n1 . 4_555 109.47 H1n1 N1 H1n1 . 4_555 84.92 H1n1 N1 H2n1 . . 109.47 H1n1 N1 H2n1 . 4_555 130.33 H1n1 N1 H3n1 . . 109.47 H1n1 N1 H3n1 . 4_555 26.89 H1n1 N1 H2n1 4_555 . 130.33 H1n1 N1 H2n1 4_555 4_555 109.47 H1n1 N1 H3n1 4_555 . 26.89 H1n1 N1 H3n1 4_555 4_555 109.47 H2n1 N1 H2n1 . 4_555 26.89 H2n1 N1 H3n1 . . 109.47 H2n1 N1 H3n1 . 4_555 84.92 H2n1 N1 H3n1 4_555 . 84.92 H2n1 N1 H3n1 4_555 4_555 109.47 H3n1 N1 H3n1 . 4_555 130.33 N1 C2 C2 . 2_655 114.4(10) N1 C2 H1c2 . . 109.47 N1 C2 H1c2 . 4_555 109.47 C2 C2 H1c2 2_655 . 109.47 C2 C2 H1c2 2_655 4_555 109.47 H1c2 C2 H1c2 . 4_555 104.04 N1 H1n1 H3n1 . 4_555 76.56 N1 H2n1 H2n1 . 4_555 76.56 N1 H3n1 H1n1 . 4_555 76.56 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance I1 N1 5_544 3.655(8) I1 N1 5_545 3.594(8) I1 N1 5_554 3.655(8) I1 N1 5_555 3.594(8) I1 N1 2_655 3.534(11) N1 C2 . 1.474(16) N1 H1n1 . 0.87 N1 H1n1 4_555 0.87 N1 H2n1 . 0.87 N1 H2n1 4_555 0.87 N1 H3n1 . 0.87 N1 H3n1 4_555 0.87 C2 C2 2_655 1.487(18) C2 H1c2 . 0.96 C2 H1c2 4_555 0.96 H1n1 H3n1 4_555 0.4045 H2n1 H2n1 4_555 0.4045 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1175.58 1344.46 87.24 o 4 0 0 23550.50 29333.80 167.84 o 6 0 0 17349.40 23995.30 126.21 o 8 0 0 3224.83 4846.45 58.46 o 10 0 0 10479.40 14188.20 78.83 o 12 0 0 237.49 364.02 31.88 o 14 0 0 2239.59 3057.37 46.06 o 16 0 0 1509.13 2053.90 46.06 o 18 0 0 178.92 178.02 42.51 o 20 0 0 506.60 568.16 96.10 o 1 1 0 4490.12 6649.25 54.47 o 3 1 0 27033.70 32451.80 123.55 o 5 1 0 11.76 40.74 33.66 < 7 1 0 12007.80 11582.90 76.61 o 9 1 0 5042.12 6512.42 67.75 o 11 1 0 2104.84 2545.45 46.06 o 13 1 0 5299.62 7298.46 52.26 o 15 1 0 4.61 41.18 28.78 < 17 1 0 1441.10 1951.60 37.20 o 19 1 0 396.44 496.42 37.20 o 0 2 0 31630.30 40103.20 110.27 o 2 2 0 1255.59 1577.40 27.01 o 4 2 0 13754.00 16212.00 54.91 o 6 2 0 9624.67 11344.30 50.93 o 8 2 0 1710.34 1962.67 38.08 o 10 2 0 7140.98 8762.05 48.71 o 12 2 0 182.49 278.99 25.24 o 14 2 0 1592.59 2210.22 35.43 o 16 2 0 1075.65 1466.69 34.10 o 18 2 0 122.26 89.45 34.98 o 20 2 0 385.20 337.89 40.30 o 1 3 0 3047.36 3740.68 28.78 o 3 3 0 9874.66 12248.10 41.18 o 5 3 0 15.77 17.71 19.93 < 7 3 0 6184.04 7164.72 41.18 o 9 3 0 2242.61 2607.45 31.44 o 11 3 0 1102.28 1468.02 32.77 o 13 3 0 2668.44 3598.97 35.43 o 15 3 0 1.58 17.27 31.00 < 17 3 0 811.85 991.52 34.54 o 19 3 0 206.97 173.15 37.20 o 0 4 0 7899.98 9223.93 49.16 o 2 4 0 485.50 517.68 21.70 o 4 4 0 4156.58 4740.61 28.78 o 6 4 0 2986.97 3350.98 28.34 o 8 4 0 525.76 599.16 26.13 o 10 4 0 2506.71 3055.60 32.33 o 12 4 0 76.76 59.78 27.01 o 14 4 0 634.41 770.10 33.66 o 16 4 0 405.65 392.80 34.54 o 1 5 0 781.87 887.01 21.70 o 3 5 0 2363.70 2715.94 26.13 o 5 5 0 3.45 28.78 21.26 < 7 5 0 1584.27 1526.91 31.00 o 9 5 0 605.09 668.25 24.80 o 11 5 0 314.57 388.81 29.67 o 13 5 0 751.53 764.79 37.20 o 0 6 0 1488.31 1398.05 38.53 o 2 6 0 98.57 131.97 24.80 o 4 6 0 824.34 859.55 25.24 o 6 6 0 596.99 644.33 27.90 o 8 6 0 112.60 80.15 32.77 o 10 6 0 530.24 545.14 31.88 o -17 0 1 1382.91 1371.92 54.03 o -15 0 1 26.70 42.51 50.04 < -13 0 1 6363.70 6482.30 87.24 o -11 0 1 975.42 452.58 33.21 o -9 0 1 5963.02 4194.59 50.93 o -7 0 1 12780.20 12636.00 113.37 o -5 0 1 1211.98 1063.26 38.08 o -3 0 1 25033.80 22876.30 144.81 o -1 0 1 3246.15 2959.06 50.93 o 1 0 1 7529.94 7478.70 66.43 o 3 0 1 24515.20 24043.20 100.08 o 5 0 1 407.05 419.37 31.44 o 7 0 1 11394.80 9204.89 64.21 o 9 0 1 3847.87 3975.82 44.28 o 11 0 1 3387.64 3048.07 43.40 o 13 0 1 4065.10 4185.29 47.38 o 15 0 1 62.33 52.26 33.21 < 17 0 1 1484.33 1533.11 45.17 o 19 0 1 227.96 203.26 41.63 o -20 1 1 498.74 395.01 60.67 o -18 1 1 60.36 63.33 35.87 < -16 1 1 1649.93 1672.61 37.20 o -14 1 1 1490.02 1388.31 34.54 o -12 1 1 492.23 409.63 27.46 o -10 1 1 9994.68 8728.83 54.47 o -8 1 1 704.98 761.69 33.66 o -6 1 1 14162.70 13762.60 79.71 o -4 1 1 16570.90 15100.90 62.44 o -2 1 1 4918.63 4471.81 39.86 o 0 1 1 43804.90 42081.40 103.18 o 2 1 1 70.77 117.35 27.90 o 4 1 1 19057.10 16068.00 53.58 o 6 1 1 9920.92 9380.25 42.96 o 8 1 1 4284.26 4001.51 31.88 o 10 1 1 7035.23 6375.14 37.20 o 12 1 1 52.44 85.03 23.03 o 14 1 1 2259.06 2413.48 30.11 o 16 1 1 856.71 898.08 30.11 o 18 1 1 227.88 154.11 35.43 o 20 1 1 394.86 289.17 41.18 o -19 2 1 406.99 355.16 37.20 o -17 2 1 1042.29 1056.18 33.66 o -15 2 1 23.89 53.58 29.23 < -13 2 1 4362.42 3734.03 35.87 o -11 2 1 808.54 803.31 27.46 o -9 2 1 4193.39 3906.30 40.30 o -7 2 1 8484.77 8147.83 48.27 o -5 2 1 566.55 557.54 22.58 o -3 2 1 15485.80 14977.30 49.16 o -1 2 1 2584.36 2461.31 27.46 o 1 2 1 5753.61 4641.86 31.88 o 3 2 1 14160.20 12396.40 42.96 o 5 2 1 194.08 182.45 19.93 o 7 2 1 8570.49 7861.75 36.76 o 9 2 1 2386.08 2267.79 26.13 o 11 2 1 2365.58 2400.20 27.90 o 13 2 1 2947.85 2855.44 35.43 o 15 2 1 49.36 24.80 27.46 < 17 2 1 1102.17 1153.16 33.66 o 19 2 1 164.27 100.08 38.97 o -18 3 1 27.50 18.16 33.21 < -16 3 1 837.84 786.04 32.33 o -14 3 1 818.64 753.27 32.33 o -12 3 1 305.15 254.19 26.57 o -10 3 1 4565.09 4397.41 38.97 o -8 3 1 321.56 331.69 22.58 o -6 3 1 6261.86 6074.00 33.21 o -4 3 1 6069.50 6231.21 32.33 o -2 3 1 2022.34 1993.67 25.68 o 0 3 1 13968.10 13393.30 42.07 o 2 3 1 119.11 109.38 21.26 o 4 3 1 7973.23 7416.70 40.74 o 6 3 1 3936.05 3544.05 27.46 o 8 3 1 1665.39 1568.10 24.80 o 10 3 1 3537.36 3502.43 29.67 o 12 3 1 25.60 45.17 23.91 < 14 3 1 1154.86 1157.59 32.77 o 16 3 1 453.34 452.14 31.00 o 18 3 1 117.07 69.08 36.76 < -17 4 1 444.18 393.24 37.64 o -15 4 1 13.95 -4.43 34.10 < -13 4 1 1587.38 1299.74 33.21 o -11 4 1 328.49 287.40 30.56 o -9 4 1 1514.81 1322.77 25.68 o -7 4 1 2859.66 2974.12 27.46 o -5 4 1 161.68 138.61 21.70 o -3 4 1 4900.02 5007.20 28.78 o -1 4 1 960.21 1001.26 21.26 o 1 4 1 2151.31 2043.27 24.80 o 3 4 1 4254.22 4321.68 29.67 o 5 4 1 55.81 72.18 27.90 o 7 4 1 3119.65 3125.13 27.90 o 9 4 1 784.59 840.07 25.24 o 11 4 1 868.73 933.07 26.57 o 13 4 1 1127.96 1016.76 38.53 o 15 4 1 18.15 36.31 34.10 < -14 5 1 256.68 209.46 35.43 o -12 5 1 92.49 75.28 32.33 o -10 5 1 1217.47 1089.83 31.88 o -8 5 1 90.44 74.84 23.03 o -6 5 1 1584.51 1520.27 24.80 o -4 5 1 1501.95 1519.83 23.91 o -2 5 1 505.82 501.74 22.58 o 0 5 1 3205.03 3037.89 25.24 o 2 5 1 44.83 45.17 21.26 o 4 5 1 2019.41 1861.26 33.21 o 6 5 1 987.88 928.19 24.80 o 8 5 1 424.67 430.88 23.91 o 10 5 1 986.67 923.77 27.46 o 12 5 1 7.35 31.88 29.67 < 14 5 1 351.10 272.35 40.30 o -9 6 1 331.05 178.02 34.10 o -7 6 1 574.34 463.65 26.57 o -5 6 1 34.23 86.80 23.47 o -3 6 1 940.96 851.14 25.68 o -1 6 1 192.70 192.19 23.47 o 1 6 1 437.08 364.02 25.24 o 3 6 1 802.97 678.43 31.44 o 5 6 1 9.01 44.73 28.78 < 7 6 1 650.93 488.90 29.67 o 9 6 1 165.15 146.14 29.23 o -18 0 2 2.59 11.07 50.04 < -16 0 2 1584.14 1529.13 46.50 o -14 0 2 994.21 871.95 36.31 o -12 0 2 849.75 767.89 34.98 o -10 0 2 8634.36 7073.94 50.93 o -8 0 2 16.57 39.86 26.57 < -6 0 2 11628.80 9553.85 54.03 o -4 0 2 11399.20 10398.30 56.24 o -2 0 2 8503.58 7136.82 48.27 o 0 0 2 25014.80 23637.10 76.61 o 2 0 2 27.29 -11.07 27.90 < 4 0 2 16541.50 15668.60 65.54 o 6 0 2 5040.47 5031.56 42.96 o 8 0 2 4593.39 3904.97 39.86 o 10 0 2 4730.79 4546.65 41.63 o 12 0 2 0.01 17.71 28.78 < 14 0 2 2124.09 1900.67 34.10 o 16 0 2 421.14 382.61 35.43 o 18 0 2 240.39 183.34 39.86 o -19 1 2 506.80 465.43 38.53 o -17 1 2 998.04 875.94 36.31 o -15 1 2 162.96 97.87 37.20 o -13 1 2 4717.39 4881.88 65.10 o -11 1 2 277.45 315.74 32.33 o -9 1 2 4992.46 4674.18 41.63 o -7 1 2 8139.78 7140.36 43.40 o -5 1 2 2257.71 2060.98 24.36 o -3 1 2 13777.80 12732.10 42.51 o -1 1 2 1739.22 1687.67 27.01 o 1 1 2 8585.58 7998.15 34.10 o 3 1 2 11262.30 10679.10 38.08 o 5 1 2 826.38 702.34 20.81 o 7 1 2 8268.12 7482.68 33.66 o 9 1 2 1483.73 1478.20 22.58 o 11 1 2 3148.30 2906.36 26.57 o 13 1 2 2116.70 2039.28 26.57 o 15 1 2 124.95 95.21 22.58 o 17 1 2 1097.37 1044.66 28.34 o 19 1 2 68.27 83.25 30.11 o -18 2 2 1.59 41.63 50.04 < -16 2 2 1138.79 893.65 50.93 o -14 2 2 740.24 732.46 28.34 o -12 2 2 673.01 709.43 28.78 o -10 2 2 5707.23 4970.44 46.06 o -8 2 2 21.95 53.58 20.37 o -6 2 2 8282.37 7802.41 34.98 o -4 2 2 6189.91 6311.37 39.86 o -2 2 2 4761.96 4266.77 35.87 o 0 2 2 15439.70 14593.40 41.18 o 2 2 2 30.55 19.93 18.16 < 4 2 2 10245.90 9906.35 35.87 o 6 2 2 3341.64 3026.82 27.90 o 8 2 2 3024.33 2667.67 27.46 o 10 2 2 3323.12 3150.37 30.11 o 12 2 2 0.01 18.16 23.03 < 14 2 2 1512.52 1530.90 31.44 o 16 2 2 310.36 267.03 27.01 o 18 2 2 175.25 126.65 36.76 o -17 3 2 552.39 362.69 34.10 o -15 3 2 94.93 128.42 31.00 o -13 3 2 2334.91 2354.58 34.10 o -11 3 2 183.39 183.78 25.24 o -9 3 2 2592.43 2515.78 27.90 o -7 3 2 3625.80 3726.51 28.34 o -5 3 2 768.10 746.63 21.26 o -3 3 2 6874.74 6355.21 29.67 o -1 3 2 732.40 720.95 24.80 o 1 3 2 3940.10 3425.37 26.13 o 3 3 2 5241.02 4544.43 27.01 o 5 3 2 411.95 354.71 20.81 o 7 3 2 4190.43 3919.14 27.46 o 9 3 2 684.89 684.19 20.81 o 11 3 2 1598.12 1599.54 24.36 o 13 3 2 1134.48 1136.33 26.57 o 15 3 2 70.93 70.85 29.67 o 17 3 2 610.81 478.71 38.08 o -16 4 2 444.17 358.70 37.64 o -14 4 2 308.82 289.17 34.98 o -12 4 2 277.90 278.55 31.00 o -10 4 2 1997.14 1910.42 29.67 o -8 4 2 14.03 47.38 21.70 o -6 4 2 2941.89 3038.77 26.57 o -4 4 2 1917.72 2066.74 23.91 o -2 4 2 1490.71 1571.20 23.03 o 0 4 2 4827.94 4791.98 34.54 o 2 4 2 2.74 40.74 20.37 < 4 4 2 3502.14 3334.59 27.01 o 6 4 2 1112.61 1037.13 23.47 o 8 4 2 1011.24 1001.26 23.47 o 10 4 2 1284.96 1259.88 23.91 o 12 4 2 0.16 5.31 23.91 < 14 4 2 590.06 488.45 32.33 o -13 5 2 665.66 554.88 38.97 o -11 5 2 56.53 39.41 28.34 < -9 5 2 738.87 680.20 26.57 o -7 5 2 926.34 985.32 24.80 o -5 5 2 196.58 182.89 22.58 o -3 5 2 1737.79 1859.93 24.80 o -1 5 2 192.41 206.81 26.13 o 1 5 2 1064.78 1117.29 29.23 o 3 5 2 1258.02 1142.09 25.24 o 5 5 2 94.12 111.15 23.47 o 7 5 2 1174.57 1180.61 26.13 o 9 5 2 173.21 162.96 25.24 o 11 5 2 442.18 423.80 28.78 o -8 6 2 4.78 39.86 27.01 < -6 6 2 618.02 438.86 27.90 o -4 6 2 394.58 301.58 24.36 o -2 6 2 302.16 251.98 29.67 o 0 6 2 955.01 922.44 33.21 o 2 6 2 0.03 42.96 32.77 < 4 6 2 752.29 592.96 29.67 o 6 6 2 221.37 226.29 28.34 o 8 6 2 209.41 238.25 30.11 o -19 0 3 421.77 524.32 63.77 o -17 0 3 706.85 697.92 44.28 o -15 0 3 366.04 609.35 35.87 o -13 0 3 3178.33 3821.72 42.96 o -11 0 3 43.87 137.72 30.11 o -9 0 3 4329.94 5355.72 40.74 o -7 0 3 4500.58 4548.42 55.36 o -5 0 3 2725.81 3769.46 36.76 o -3 0 3 8452.45 9757.55 46.50 o -1 0 3 576.28 721.39 26.13 o 1 0 3 7853.52 9611.42 46.50 o 3 0 3 5242.12 5805.20 40.30 o 5 0 3 1113.22 2173.91 31.44 o 7 0 3 5689.83 6612.50 43.84 o 9 0 3 429.36 448.15 28.78 o 11 0 3 2582.59 3377.10 39.86 o 13 0 3 1040.18 1157.14 34.54 o 15 0 3 165.54 268.36 33.66 o 17 0 3 772.86 709.43 43.40 o -18 1 3 15.04 19.04 38.97 < -16 1 3 995.28 1240.40 36.76 o -14 1 3 499.45 517.68 26.57 o -12 1 3 1000.10 1323.65 24.80 o -10 1 3 4483.80 4636.10 31.00 o -8 1 3 65.79 427.78 21.26 o -6 1 3 7126.37 8743.45 34.10 o -4 1 3 3909.67 4078.56 32.77 o -2 1 3 6155.31 8170.85 38.08 o 0 1 3 9710.86 10896.10 34.10 o 2 1 3 207.90 1246.15 19.93 o 4 1 3 9023.82 10442.60 34.10 o 6 1 3 1520.53 1532.23 21.26 o 8 1 3 2988.96 3596.31 26.13 o 10 1 3 2231.46 2455.99 23.91 o 12 1 3 28.68 123.55 19.04 o 14 1 3 1332.33 1372.36 24.80 o 16 1 3 128.21 116.47 25.68 o -19 2 3 321.59 334.35 43.40 o -17 2 3 513.46 547.35 35.43 o -15 2 3 260.92 395.01 31.88 o -13 2 3 2279.08 2394.44 38.97 o -11 2 3 36.00 96.98 25.24 o -9 2 3 3047.08 3905.41 29.67 o -7 2 3 3086.45 3132.66 25.24 o -5 2 3 1695.89 2257.16 22.58 o -3 2 3 6073.87 6966.33 30.56 o -1 2 3 367.66 493.33 19.04 o 1 2 3 5228.67 6635.08 29.23 o 3 2 3 3781.82 4054.65 30.11 o 5 2 3 814.26 1503.44 25.24 o 7 2 3 4011.49 4299.54 31.44 o 9 2 3 307.39 344.97 23.03 o 11 2 3 1866.17 2131.84 28.34 o 13 2 3 768.11 797.56 27.46 o 15 2 3 125.13 189.09 28.78 o 17 2 3 576.60 333.46 30.11 o -16 3 3 549.09 662.49 34.10 o -14 3 3 266.74 310.87 48.27 o -12 3 3 538.76 804.20 45.17 o -10 3 3 2236.80 2450.68 33.21 o -8 3 3 28.01 242.23 23.91 o -6 3 3 3644.39 4532.03 28.78 o -4 3 3 1679.77 1815.65 21.26 o -2 3 3 2767.78 3614.47 25.68 o 0 3 3 4672.31 5113.93 28.34 o 2 3 3 115.44 610.68 20.81 o 4 3 3 4291.93 4808.37 27.90 o 6 3 3 754.78 677.99 21.70 o 8 3 3 1492.23 1721.76 23.47 o 10 3 3 1172.60 1224.90 23.47 o 12 3 3 17.63 55.36 22.14 o 14 3 3 706.38 756.37 28.34 o -15 4 3 107.07 91.23 52.70 < -13 4 3 879.22 875.94 50.04 o -11 4 3 16.67 46.06 29.67 < -9 4 3 1174.61 1478.20 31.88 o -7 4 3 1050.95 1146.51 28.34 o -5 4 3 547.06 853.80 27.46 o -3 4 3 2225.86 2546.78 25.24 o -1 4 3 112.29 178.91 19.49 o 1 4 3 1821.13 2171.69 24.80 o 3 4 3 1328.06 1361.74 23.03 o 5 4 3 287.59 461.00 22.58 o 7 4 3 1517.94 1651.35 25.24 o 9 4 3 105.83 111.15 21.26 o 11 4 3 704.28 759.03 25.68 o 13 4 3 325.43 328.59 27.90 o -12 5 3 164.76 186.88 44.73 o -10 5 3 623.65 542.48 32.33 o -8 5 3 4.02 46.94 28.34 < -6 5 3 1045.06 1121.72 32.33 o -4 5 3 434.67 440.18 28.34 o -2 5 3 712.47 883.47 25.24 o 0 5 3 1271.99 1286.01 25.68 o 2 5 3 28.15 83.25 24.36 o 4 5 3 1206.94 1155.81 27.46 o 6 5 3 201.32 209.46 24.36 o 8 5 3 412.12 427.34 28.34 o 10 5 3 366.84 369.33 30.11 o -5 6 3 110.66 136.84 31.88 o -3 6 3 479.44 483.14 27.46 o -1 6 3 20.87 65.98 28.78 o 1 6 3 381.12 395.90 29.23 o 3 6 3 276.10 271.02 31.00 o -18 0 4 50.73 53.14 44.73 < -16 0 4 597.10 629.28 38.97 o -14 0 4 245.69 207.25 31.44 o -12 0 4 1003.77 957.42 28.34 o -10 0 4 2196.20 1820.08 32.77 o -8 0 4 179.76 139.49 40.74 o -6 0 4 4478.89 4184.40 34.98 o -4 0 4 1298.19 1363.95 28.34 o -2 0 4 4389.68 3967.41 33.21 o 0 0 4 4212.67 4344.27 34.10 o 2 0 4 352.89 247.99 27.46 o 4 0 4 5217.85 5403.99 38.97 o 6 0 4 371.83 369.33 28.34 o 8 0 4 1905.86 1687.67 30.11 o 10 0 4 1072.76 1123.93 30.56 o 12 0 4 74.31 37.64 29.67 < 14 0 4 790.95 648.32 37.20 o 16 0 4 30.69 43.84 38.08 < -17 1 4 341.88 329.03 35.43 o -15 1 4 396.00 362.24 27.01 o -13 1 4 1423.93 1473.33 25.68 o -11 1 4 0.06 9.74 19.93 < -9 1 4 2612.55 2529.51 28.78 o -7 1 4 1513.13 1498.13 21.26 o -5 1 4 1783.40 1638.51 23.91 o -3 1 4 3774.67 3886.81 28.78 o -1 1 4 55.04 96.10 17.71 o 1 1 4 4370.99 4267.66 25.24 o 3 1 4 1660.57 1691.21 20.81 o 5 1 4 853.70 769.66 19.93 o 7 1 4 2694.54 2575.56 23.47 o 9 1 4 41.19 62.00 19.93 o 11 1 4 1396.90 1371.92 24.36 o 13 1 4 363.58 367.56 23.47 o 15 1 4 141.23 110.71 25.68 o -16 2 4 454.82 457.90 37.64 o -14 2 4 172.69 179.35 26.57 o -12 2 4 723.41 658.50 25.68 o -10 2 4 1594.74 1616.37 22.58 o -8 2 4 138.21 86.35 18.16 o -6 2 4 3173.30 2989.62 25.68 o -4 2 4 890.07 988.42 19.93 o -2 2 4 3104.46 2969.25 23.47 o 0 2 4 2924.25 3105.64 27.90 o 2 2 4 254.87 277.66 22.14 o 4 2 4 3695.76 3840.32 28.34 o 6 2 4 256.54 298.48 23.03 o 8 2 4 1363.62 1226.23 23.03 o 10 2 4 785.33 728.92 22.14 o 12 2 4 57.79 47.38 27.01 < 14 2 4 577.27 405.20 30.56 o -15 3 4 206.81 221.42 34.10 o -13 3 4 779.32 673.12 31.44 o -11 3 4 0.03 34.54 23.47 < -9 3 4 1349.02 1313.47 23.47 o -7 3 4 771.54 804.64 21.70 o -5 3 4 868.50 807.30 21.70 o -3 3 4 1942.71 1826.72 22.58 o -1 3 4 26.61 50.04 19.04 o 1 3 4 2176.98 2246.97 22.14 o 3 3 4 861.20 907.82 21.26 o 5 3 4 434.87 380.40 21.70 o 7 3 4 1422.50 1320.55 25.24 o 9 3 4 20.70 60.23 22.58 o 11 3 4 741.55 642.56 25.24 o 13 3 4 210.55 188.65 26.57 o -12 4 4 286.13 244.45 30.11 o -10 4 4 621.68 627.06 26.13 o -8 4 4 47.58 23.91 22.58 < -6 4 4 1245.72 1184.60 26.13 o -4 4 4 309.16 371.10 22.14 o -2 4 4 1110.80 1029.60 23.91 o 0 4 4 1134.95 1070.35 23.47 o 2 4 4 104.61 120.90 21.70 o 4 4 4 1395.82 1370.15 25.24 o 6 4 4 98.86 98.31 23.47 o 8 4 4 534.51 439.30 27.46 o 10 4 4 325.46 313.53 27.46 o -9 5 4 412.70 364.02 29.67 o -7 5 4 206.86 177.14 27.46 o -5 5 4 232.02 216.11 24.36 o -3 5 4 576.14 596.51 26.13 o -1 5 4 4.15 -6.20 26.57 < 1 5 4 589.86 542.04 27.46 o 3 5 4 254.11 246.22 26.57 o 5 5 4 127.96 185.55 27.90 o 7 5 4 423.82 263.49 64.21 o -15 0 5 343.29 347.19 37.64 o -13 0 5 608.85 597.84 33.66 o -11 0 5 9.46 35.43 28.78 < -9 0 5 1570.55 1317.01 30.56 o -7 0 5 431.10 472.07 40.74 o -5 0 5 1114.45 1029.60 26.57 o -3 0 5 1685.72 1727.08 28.78 o -1 0 5 2.54 -6.64 26.13 < 1 0 5 2360.62 2348.83 31.00 o 3 0 5 470.02 583.66 29.67 o 5 0 5 566.99 553.99 30.56 o 7 0 5 1276.23 1460.49 33.66 o 9 0 5 1.98 -24.36 32.33 < 11 0 5 706.07 685.52 35.43 o 13 0 5 125.41 79.71 39.41 o -16 1 5 273.01 242.68 73.95 o -14 1 5 75.72 78.83 23.47 o -12 1 5 653.93 598.72 23.91 o -10 1 5 724.01 693.49 27.01 o -8 1 5 171.22 86.35 20.81 o -6 1 5 2025.23 2063.20 21.70 o -4 1 5 231.82 267.48 21.26 o -2 1 5 2140.68 2119.88 25.68 o 0 1 5 1291.37 1487.06 21.70 o 2 1 5 300.33 286.08 20.81 o 4 1 5 2165.12 2324.03 23.91 o 6 1 5 30.57 49.60 20.81 o 8 1 5 844.62 711.20 23.03 o 10 1 5 384.04 364.02 25.68 o 12 1 5 83.08 65.98 25.68 o -15 2 5 248.25 214.34 35.87 o -13 2 5 459.62 493.33 27.90 o -11 2 5 7.50 17.27 28.34 < -9 2 5 1136.13 1197.88 24.36 o -7 2 5 316.42 344.97 20.81 o -5 2 5 793.42 776.74 21.70 o -3 2 5 1228.56 1290.88 21.26 o -1 2 5 1.72 -23.03 19.49 < 1 2 5 1692.63 1646.92 26.13 o 3 2 5 348.85 362.69 24.36 o 5 2 5 411.59 345.86 24.80 o 7 2 5 940.12 887.45 28.78 o 9 2 5 1.45 27.90 27.01 < 11 2 5 521.98 433.98 30.56 o -12 3 5 348.51 277.22 32.33 o -10 3 5 399.93 359.14 26.13 o -8 3 5 94.12 59.34 21.70 o -6 3 5 1084.56 1049.98 24.80 o -4 3 5 114.78 151.45 22.14 o -2 3 5 1111.58 1051.30 24.36 o 0 3 5 695.09 691.27 22.14 o 2 3 5 170.16 137.28 22.14 o 4 3 5 1140.20 1145.19 25.24 o 6 3 5 16.67 32.77 24.80 < 8 3 5 463.92 387.04 27.01 o 10 3 5 212.84 220.09 49.16 o -9 4 5 455.68 372.87 26.57 o -7 4 5 123.99 114.70 25.24 o -5 4 5 305.02 288.29 25.24 o -3 4 5 497.64 480.04 26.57 o -1 4 5 1.61 50.48 25.24 < 1 4 5 639.85 553.99 25.68 o 3 4 5 148.53 142.60 25.68 o 5 4 5 171.27 160.31 27.90 o -12 0 6 389.82 334.79 37.64 o -10 0 6 220.53 211.68 32.77 o -8 0 6 122.52 54.91 51.81 < -6 0 6 940.44 1162.90 50.93 o -4 0 6 17.22 -2.21 27.46 < -2 0 6 994.84 964.51 34.54 o 0 0 6 411.79 532.29 32.33 o 2 0 6 227.45 95.65 34.10 o 4 0 6 885.78 961.85 35.87 o 6 0 6 0.46 -4.87 34.98 < 8 0 6 376.16 322.83 39.86 o -11 1 6 16.51 54.47 24.80 o -9 1 6 677.69 611.12 29.23 o -7 1 6 65.39 46.50 22.58 o -5 1 6 466.70 384.39 27.46 o -3 1 6 573.16 624.85 26.57 o -1 1 6 31.05 31.88 26.57 < 1 1 6 875.86 864.87 24.36 o 3 1 6 90.07 106.28 23.91 o 5 1 6 269.64 214.78 25.24 o 7 1 6 437.53 356.93 27.46 o -10 2 6 167.82 125.77 31.00 o -8 2 6 93.47 50.48 23.91 o -6 2 6 694.14 664.70 25.24 o -4 2 6 11.72 16.83 23.91 < -2 2 6 726.47 653.63 23.91 o 0 2 6 308.49 231.16 23.91 o 2 2 6 175.19 170.49 29.23 o 4 2 6 644.70 647.43 29.67 o 6 2 6 0.23 44.73 29.67 < -7 3 6 38.00 76.61 27.46 o -5 3 6 255.58 209.02 27.01 o -3 3 6 318.97 357.82 26.57 o -1 3 6 18.46 36.31 26.57 < 1 3 6 467.69 390.14 26.57 o 3 3 6 55.08 99.64 26.57 o loop_ _twin_individual_id _twin_individual_mass_fraction_refined _twin_individual_twin_matrix_11 _twin_individual_twin_matrix_12 _twin_individual_twin_matrix_13 _twin_individual_twin_matrix_21 _twin_individual_twin_matrix_22 _twin_individual_twin_matrix_23 _twin_individual_twin_matrix_31 _twin_individual_twin_matrix_32 _twin_individual_twin_matrix_33 1 0.811(7) 1 0 0 0 1 0 0 0 1 2 0.189(7) 0.999 0 0.003 0 -1 0 0.666 0 -0.999 loop_ _twin_refln_datum_id _twin_refln_individual_id _twin_refln_index_h _twin_refln_index_k _twin_refln_index_l _twin_refln_f_squared_calc _twin_refln_f_squared_meas _twin_refln_f_squared_sigma _twin_refln_include_status 1 2 2 0 0 1190.62 1144.85 74.29 o 1 1 2 0 0 1190.62 1144.85 74.29 o 2 2 4 0 0 23582.40 24978.50 142.92 o 2 1 4 0 0 23582.40 24978.50 142.92 o 3 2 6 0 0 17699.80 20432.70 107.47 o 3 1 6 0 0 17699.80 20432.70 107.47 o 4 2 8 0 0 3294.66 4126.89 49.78 o 4 1 8 0 0 3294.66 4126.89 49.78 o 5 1 10 0 0 8764.06 12081.60 67.12 o 6 1 12 0 0 204.46 309.97 27.15 o 7 1 14 0 0 1930.98 2603.44 39.22 o 8 1 16 0 0 1324.50 1748.95 39.22 o 9 1 18 0 0 165.66 151.59 36.20 o 10 1 20 0 0 451.41 483.81 81.83 o 11 2 1 -1 0 4495.07 5662.02 46.38 o 11 1 1 1 0 4495.07 5662.02 46.38 o 12 2 3 -1 0 27026.50 27633.60 105.21 o 12 1 3 1 0 27026.50 27633.60 105.21 o 13 2 5 -1 0 9.15 34.69 28.66 < 13 1 5 1 0 9.15 34.69 28.66 < 14 2 7 -1 0 12071.50 9863.20 65.24 o 14 1 7 1 0 12071.50 9863.20 65.24 o 15 1 9 1 0 4172.05 5545.50 57.69 o 16 1 11 1 0 1755.69 2167.52 39.22 o 17 1 13 1 0 4485.96 6214.84 44.50 o 18 1 15 1 0 3.60 35.07 24.51 < 19 1 17 1 0 1250.15 1661.84 31.68 o 20 1 19 1 0 367.29 422.72 31.68 o 21 2 0 -2 0 31550.00 34149.00 93.90 o 21 1 0 2 0 31550.00 34149.00 93.90 o 22 2 2 -2 0 1269.33 1343.20 23.00 o 22 1 2 2 0 1269.33 1343.20 23.00 o 23 2 4 -2 0 13751.20 13804.90 46.76 o 23 1 4 2 0 13751.20 13804.90 46.76 o 24 2 6 -2 0 9794.01 9659.95 43.37 o 24 1 6 2 0 9794.01 9659.95 43.37 o 25 2 8 -2 0 1732.08 1671.27 32.43 o 25 1 8 2 0 1732.08 1671.27 32.43 o 26 1 10 2 0 5971.87 7461.13 41.48 o 27 1 12 2 0 156.49 237.57 21.49 o 28 1 14 2 0 1368.53 1882.06 30.17 o 29 1 16 2 0 944.10 1248.93 29.04 o 30 1 18 2 0 113.41 76.17 29.79 o 31 1 20 2 0 342.81 287.72 34.32 o 32 2 1 -3 0 3022.51 3185.29 24.51 o 32 1 1 3 0 3022.51 3185.29 24.51 o 33 2 3 -3 0 9815.66 10429.60 35.07 o 33 1 3 3 0 9815.66 10429.60 35.07 o 34 2 5 -3 0 13.47 15.08 16.97 < 34 1 5 3 0 13.47 15.08 16.97 < 35 2 7 -3 0 6187.00 6100.96 35.07 o 35 1 7 3 0 6187.00 6100.96 35.07 o 36 1 9 3 0 1832.99 2220.31 26.77 o 37 1 11 3 0 911.04 1250.06 27.90 o 38 1 13 3 0 2242.22 3064.62 30.17 o 39 1 15 3 0 1.29 14.71 26.40 < 40 1 17 3 0 697.11 844.31 29.41 o 41 1 19 3 0 190.46 147.44 31.68 o 42 2 0 -4 0 7812.87 7854.43 41.86 o 42 1 0 4 0 7812.87 7854.43 41.86 o 43 2 2 -4 0 478.56 440.82 18.48 o 43 1 2 4 0 478.56 440.82 18.48 o 44 2 4 -4 0 4095.94 4036.76 24.51 o 44 1 4 4 0 4095.94 4036.76 24.51 o 45 2 6 -4 0 3011.34 2853.45 24.13 o 45 1 6 4 0 3011.34 2853.45 24.13 o 46 2 8 -4 0 525.17 510.20 22.25 o 46 1 8 4 0 525.17 510.20 22.25 o 47 1 10 4 0 2078.10 2601.93 27.53 o 48 1 12 4 0 65.25 50.91 23.00 o 49 1 14 4 0 539.43 655.76 28.66 o 50 1 16 4 0 354.24 334.48 29.41 o 51 2 1 -5 0 762.48 755.31 18.48 o 51 1 1 5 0 762.48 755.31 18.48 o 52 2 3 -5 0 2331.49 2312.70 22.25 o 52 1 3 5 0 2331.49 2312.70 22.25 o 53 2 5 -5 0 2.67 24.51 18.10 < 53 1 5 5 0 2.67 24.51 18.10 < 54 2 7 -5 0 1565.18 1300.21 26.40 o 54 1 7 5 0 1565.18 1300.21 26.40 o 55 1 9 5 0 487.39 569.03 21.12 o 56 1 11 5 0 256.67 331.09 25.27 o 57 1 13 5 0 622.33 651.24 31.68 o 58 2 0 -6 0 1445.01 1190.48 32.81 o 58 1 0 6 0 1445.01 1190.48 32.81 o 59 2 2 -6 0 95.01 112.37 21.12 o 59 1 2 6 0 95.01 112.37 21.12 o 60 2 4 -6 0 795.25 731.93 21.49 o 60 1 4 6 0 795.25 731.93 21.49 o 61 2 6 -6 0 592.09 548.67 23.76 o 61 1 6 6 0 592.09 548.67 23.76 o 62 2 8 -6 0 109.89 68.25 27.90 o 62 1 8 6 0 109.89 68.25 27.90 o 63 1 10 6 0 432.91 464.20 27.15 o 64 1 -17 0 1 1200.88 1168.23 46.01 o 65 1 -15 0 1 20.29 36.20 42.61 < 66 1 -13 0 1 5399.57 5519.86 74.29 o 67 1 -11 0 1 830.91 385.39 28.28 o 68 1 -9 0 1 4883.52 3571.81 43.37 o 69 1 -7 0 1 10592.40 10759.90 96.54 o 70 1 -5 0 1 965.33 905.40 32.43 o 71 1 -3 0 1 20334.50 19479.80 123.31 o 72 1 -1 0 1 2684.40 2519.72 43.37 o 73 1 1 0 1 6100.30 6368.32 56.56 o 74 1 3 0 1 19855.20 20473.40 85.22 o 75 1 5 0 1 326.73 357.11 26.77 o 76 1 7 0 1 9198.13 7838.22 54.68 o 77 1 9 0 1 3265.87 3385.52 37.71 o 78 1 11 0 1 2811.34 2595.52 36.95 o 79 1 13 0 1 3447.50 3563.89 40.35 o 80 1 15 0 1 45.43 44.50 28.28 < 81 1 17 0 1 1305.44 1305.49 38.46 o 82 1 19 0 1 216.36 173.09 35.45 o 83 1 -20 1 1 448.47 336.36 51.66 o 84 1 -18 1 1 58.98 53.92 30.54 < 85 1 -16 1 1 1442.99 1424.27 31.68 o 86 1 -14 1 1 1283.34 1182.18 29.41 o 87 1 -12 1 1 404.22 348.81 23.38 o 88 1 -10 1 1 8351.75 7432.84 46.38 o 89 1 -8 1 1 593.17 648.60 28.66 o 90 1 -6 1 1 11508.80 11719.20 67.88 o 91 1 -4 1 1 13591.00 12858.80 53.17 o 92 1 -2 1 1 3903.40 3807.87 33.94 o 93 1 0 1 1 35525.10 35833.50 87.86 o 94 1 2 1 1 77.88 99.93 23.76 o 95 1 4 1 1 15475.20 13682.40 45.63 o 96 1 6 1 1 8339.87 7987.55 36.58 o 97 1 8 1 1 3538.41 3407.40 27.15 o 98 1 10 1 1 5892.27 5428.60 31.68 o 99 1 12 1 1 50.85 72.40 19.61 o 100 1 14 1 1 1957.89 2055.15 25.64 o 101 1 16 1 1 749.02 764.74 25.64 o 102 1 18 1 1 203.26 131.23 30.17 o 103 1 20 1 1 352.69 246.24 35.07 o 104 1 -19 2 1 366.22 302.43 31.68 o 105 1 -17 2 1 899.82 899.36 28.66 o 106 1 -15 2 1 18.05 45.63 24.89 < 107 1 -13 2 1 3676.33 3179.63 30.54 o 108 1 -11 2 1 686.22 684.04 23.38 o 109 1 -9 2 1 3394.30 3326.32 34.32 o 110 1 -7 2 1 6988.60 6938.10 41.10 o 111 1 -5 2 1 427.91 474.76 19.23 o 112 1 -3 2 1 12488.10 12753.60 41.86 o 113 1 -1 2 1 2152.69 2095.87 23.38 o 114 1 1 2 1 4577.33 3952.67 27.15 o 115 1 3 2 1 11488.00 10555.90 36.58 o 116 1 5 2 1 147.77 155.36 16.97 o 117 1 7 2 1 6920.78 6694.50 31.30 o 118 1 9 2 1 2022.62 1931.08 22.25 o 119 1 11 2 1 1950.50 2043.83 23.76 o 120 1 13 2 1 2497.01 2431.48 30.17 o 121 1 15 2 1 36.46 21.12 23.38 < 122 1 17 2 1 963.81 981.95 28.66 o 123 1 19 2 1 155.95 85.22 33.18 o 124 1 -18 3 1 26.99 15.46 28.28 < 125 1 -16 3 1 731.88 669.34 27.53 o 126 1 -14 3 1 700.69 641.43 27.53 o 127 1 -12 3 1 252.37 216.45 22.63 o 128 1 -10 3 1 3805.00 3744.52 33.18 o 129 1 -8 3 1 263.18 282.44 19.23 o 130 1 -6 3 1 5090.21 5172.18 28.28 o 131 1 -4 3 1 4917.44 5306.05 27.53 o 132 1 -2 3 1 1615.03 1697.66 21.87 o 133 1 0 3 1 11262.40 11404.70 35.82 o 134 1 2 3 1 103.12 93.14 18.10 o 135 1 4 3 1 6422.43 6315.52 34.69 o 136 1 6 3 1 3272.48 3017.86 23.38 o 137 1 8 3 1 1364.67 1335.28 21.12 o 138 1 10 3 1 2944.75 2982.41 25.27 o 139 1 12 3 1 24.22 38.46 20.36 < 140 1 14 3 1 992.48 985.72 27.90 o 141 1 16 3 1 395.52 385.01 26.40 o 142 1 18 3 1 104.51 58.83 31.30 < 143 1 -17 4 1 378.48 334.86 32.05 o 144 1 -15 4 1 10.38 -3.77 29.04 < 145 1 -13 4 1 1323.87 1106.76 28.28 o 146 1 -11 4 1 275.72 244.73 26.02 o 147 1 -9 4 1 1208.66 1126.37 21.87 o 148 1 -7 4 1 2339.13 2532.54 23.38 o 149 1 -5 4 1 119.31 118.03 18.48 o 150 1 -3 4 1 3926.84 4263.77 24.51 o 151 1 -1 4 1 789.30 852.60 18.10 o 152 1 1 4 1 1695.64 1739.90 21.12 o 153 1 3 4 1 3438.15 3680.03 25.27 o 154 1 5 4 1 43.05 61.47 23.76 o 155 1 7 4 1 2499.93 2661.13 23.76 o 156 1 9 4 1 657.56 715.34 21.49 o 157 1 11 4 1 709.13 794.53 22.63 o 158 1 13 4 1 945.90 865.80 32.81 o 159 1 15 4 1 13.38 30.92 29.04 < 160 1 -14 5 1 216.34 178.36 30.17 o 161 1 -12 5 1 75.44 64.11 27.53 o 162 1 -10 5 1 1002.09 928.02 27.15 o 163 1 -8 5 1 72.42 63.73 19.61 o 164 1 -6 5 1 1265.55 1294.55 21.12 o 165 1 -4 5 1 1198.61 1294.18 20.36 o 166 1 -2 5 1 393.50 427.24 19.23 o 167 1 0 5 1 2547.82 2586.85 21.49 o 168 1 2 5 1 38.11 38.46 18.10 o 169 1 4 5 1 1594.83 1584.91 28.28 o 170 1 6 5 1 814.35 790.38 21.12 o 171 1 8 5 1 341.50 366.91 20.36 o 172 1 10 5 1 812.00 786.61 23.38 o 173 1 12 5 1 6.99 27.15 25.27 < 174 1 14 5 1 298.00 231.91 34.32 o 175 1 -9 6 1 259.58 151.59 29.04 o 176 1 -7 6 1 463.53 394.81 22.63 o 177 1 -5 6 1 25.08 73.91 19.99 o 178 1 -3 6 1 745.30 724.77 21.87 o 179 1 -1 6 1 154.99 163.66 19.99 o 180 1 1 6 1 341.31 309.97 21.49 o 181 1 3 6 1 639.28 577.70 26.77 o 182 1 5 6 1 7.21 38.09 24.51 < 183 1 7 6 1 513.73 416.31 25.27 o 184 1 9 6 1 134.82 124.44 24.89 o 185 1 -18 0 2 3.47 9.43 42.61 < 186 1 -16 0 2 1372.06 1302.10 39.59 o 187 1 -14 0 2 866.85 742.49 30.92 o 188 1 -12 0 2 686.01 653.88 29.79 o 189 1 -10 0 2 7195.95 6023.65 43.37 o 190 1 -8 0 2 20.21 33.94 22.63 < 191 1 -6 0 2 9289.26 8135.37 46.01 o 192 1 -4 0 2 9549.18 8854.48 47.89 o 193 1 -2 0 2 6668.86 6077.20 41.10 o 194 1 0 0 2 20314.90 20127.60 65.24 o 195 1 2 0 2 5.15 -9.43 23.76 < 196 1 4 0 2 13529.40 13342.20 55.81 o 197 1 6 0 2 4311.04 4284.51 36.58 o 198 1 8 0 2 3773.22 3325.19 33.94 o 199 1 10 0 2 3985.60 3871.60 35.45 o 200 1 12 0 2 0.44 15.08 24.51 < 201 1 14 0 2 1851.79 1618.48 29.04 o 202 1 16 0 2 364.65 325.81 30.17 o 203 1 18 0 2 206.71 156.12 33.94 o 204 1 -19 1 2 446.31 396.32 32.81 o 205 1 -17 1 2 875.13 745.89 30.92 o 206 1 -15 1 2 129.55 83.34 31.68 o 207 1 -13 1 2 3991.35 4157.05 55.43 o 208 1 -11 1 2 250.76 268.87 27.53 o 209 1 -9 1 2 4062.21 3980.20 35.45 o 210 1 -7 1 2 6809.84 6080.22 36.95 o 211 1 -5 1 2 1795.66 1754.98 20.74 o 212 1 -3 1 2 11144.80 10841.70 36.20 o 213 1 -1 1 2 1487.89 1437.09 23.00 o 214 1 1 1 2 6908.61 6810.64 29.04 o 215 1 3 1 2 9117.39 9093.55 32.43 o 216 1 5 1 2 620.54 598.07 17.72 o 217 1 7 1 2 6691.34 6371.71 28.66 o 218 1 9 1 2 1306.44 1258.73 19.23 o 219 1 11 1 2 2597.48 2474.85 22.63 o 220 1 13 1 2 1811.05 1736.51 22.63 o 221 1 15 1 2 90.65 81.07 19.23 o 222 1 17 1 2 982.33 889.56 24.13 o 223 1 19 1 2 66.78 70.89 25.64 o 224 1 -18 2 2 2.22 35.45 42.61 < 225 1 -16 2 2 987.11 760.97 43.37 o 226 1 -14 2 2 644.67 623.71 24.13 o 227 1 -12 2 2 548.18 604.10 24.51 o 228 1 -10 2 2 4764.06 4232.47 39.22 o 229 1 -8 2 2 22.33 45.63 17.35 o 230 1 -6 2 2 6679.14 6643.97 29.79 o 231 1 -4 2 2 5137.01 5374.30 33.94 o 232 1 -2 2 2 3770.33 3633.27 30.54 o 233 1 0 2 2 12539.40 12426.70 35.07 o 234 1 2 2 2 14.31 16.97 15.46 < 235 1 4 2 2 8340.93 8435.53 30.54 o 236 1 6 2 2 2831.32 2577.42 23.76 o 237 1 8 2 2 2488.66 2271.60 23.38 o 238 1 10 2 2 2782.07 2682.63 25.64 o 239 1 12 2 2 0.22 15.46 19.61 < 240 1 14 2 2 1312.98 1303.60 26.77 o 241 1 16 2 2 268.10 227.39 23.00 o 242 1 18 2 2 150.83 107.85 31.30 o 243 1 -17 3 2 479.17 308.84 29.04 o 244 1 -15 3 2 74.18 109.36 26.40 o 245 1 -13 3 2 1956.00 2004.99 29.04 o 246 1 -11 3 2 163.56 156.49 21.49 o 247 1 -9 3 2 2073.65 2142.25 23.76 o 248 1 -7 3 2 3014.75 3173.22 24.13 o 249 1 -5 3 2 584.07 635.78 18.10 o 250 1 -3 3 2 5521.22 5411.64 25.27 o 251 1 -1 3 2 636.22 613.90 21.12 o 252 1 1 3 2 3108.43 2916.80 22.25 o 253 1 3 3 2 4271.39 3869.71 23.00 o 254 1 5 3 2 306.23 302.05 17.72 o 255 1 7 3 2 3376.05 3337.26 23.38 o 256 1 9 3 2 604.92 582.61 17.72 o 257 1 11 3 2 1309.99 1362.05 20.74 o 258 1 13 3 2 966.62 967.62 22.63 o 259 1 15 3 2 51.65 60.33 25.27 o 260 1 17 3 2 541.47 407.64 32.43 o 261 1 -16 4 2 383.17 305.44 32.05 o 262 1 -14 4 2 264.86 246.24 29.79 o 263 1 -12 4 2 225.20 237.19 26.40 o 264 1 -10 4 2 1653.47 1626.77 25.27 o 265 1 -8 4 2 12.35 40.35 18.48 o 266 1 -6 4 2 2344.75 2587.60 22.63 o 267 1 -4 4 2 1567.64 1759.88 20.36 o 268 1 -2 4 2 1166.92 1337.92 19.61 o 269 1 0 4 2 3868.41 4080.50 29.41 o 270 1 2 4 2 0.78 34.69 17.35 < 271 1 4 4 2 2803.42 2839.50 23.00 o 272 1 6 4 2 934.60 883.15 19.99 o 273 1 8 4 2 820.35 852.60 19.99 o 274 1 10 4 2 1065.25 1072.82 20.36 o 275 1 12 4 2 0.01 4.53 20.36 < 276 1 14 4 2 506.36 415.93 27.53 o 277 1 -13 5 2 551.03 472.49 33.18 o 278 1 -11 5 2 49.76 33.56 24.13 < 279 1 -9 5 2 582.52 579.21 22.63 o 280 1 -7 5 2 766.30 839.03 21.12 o 281 1 -5 5 2 149.14 155.74 19.23 o 282 1 -3 5 2 1384.61 1583.78 21.12 o 283 1 -1 5 2 163.96 176.10 22.25 o 284 1 1 5 2 837.54 951.40 24.89 o 285 1 3 5 2 1013.33 972.52 21.49 o 286 1 5 5 2 70.80 94.65 19.99 o 287 1 7 5 2 935.55 1005.33 22.25 o 288 1 9 5 2 149.45 138.77 21.49 o 289 1 11 5 2 357.37 360.88 24.51 o 290 1 -8 6 2 3.97 33.94 23.00 < 291 1 -6 6 2 482.36 373.70 23.76 o 292 1 -4 6 2 316.66 256.80 20.74 o 293 1 -2 6 2 230.36 214.57 25.27 o 294 1 0 6 2 751.07 785.48 28.28 o 295 1 2 6 2 0.04 36.58 27.90 < 296 1 4 6 2 589.44 504.92 25.27 o 297 1 6 6 2 184.61 192.69 24.13 o 298 1 8 6 2 165.60 202.88 25.64 o 299 1 -19 0 3 363.93 446.48 54.30 o 300 1 -17 0 3 633.06 594.30 37.71 o 301 1 -15 0 3 298.49 518.88 30.54 o 302 1 -13 0 3 2688.02 3254.30 36.58 o 303 1 -11 0 3 49.66 117.28 25.64 o 304 2 -7 0 -3 4637.55 4560.54 34.69 o 304 1 -9 0 3 4637.55 4560.54 34.69 o 305 2 -5 0 -3 3994.76 3873.10 47.14 o 305 1 -7 0 3 3994.76 3873.10 47.14 o 306 2 -3 0 -3 3158.95 3209.80 31.30 o 306 1 -5 0 3 3158.95 3209.80 31.30 o 307 2 -1 0 -3 8349.72 8308.83 39.59 o 307 1 -3 0 3 8349.72 8308.83 39.59 o 308 2 1 0 -3 640.00 614.28 22.25 o 308 1 -1 0 3 640.00 614.28 22.25 o 309 2 3 0 -3 7957.12 8184.39 39.59 o 309 1 1 0 3 7957.12 8184.39 39.59 o 310 2 5 0 -3 4751.61 4943.29 34.32 o 310 1 3 0 3 4751.61 4943.29 34.32 o 311 2 7 0 -3 1709.94 1851.14 26.77 o 311 1 5 0 3 1709.94 1851.14 26.77 o 312 2 9 0 -3 5497.14 5630.73 37.33 o 312 1 7 0 3 5497.14 5630.73 37.33 o 313 1 9 0 3 399.52 381.62 24.51 o 314 1 11 0 3 2123.33 2875.70 33.94 o 315 1 13 0 3 910.51 985.34 29.41 o 316 1 15 0 3 122.43 228.52 28.66 o 317 1 17 0 3 706.86 604.10 36.95 o 318 1 -18 1 3 11.39 16.21 33.18 < 319 1 -16 1 3 852.80 1056.23 31.30 o 320 1 -14 1 3 447.55 440.82 22.63 o 321 1 -12 1 3 812.66 1127.13 21.12 o 322 1 -10 1 3 3732.43 3947.77 26.40 o 323 2 -6 -1 -3 344.38 364.27 18.10 o 323 1 -8 1 3 344.38 364.27 18.10 o 324 2 -4 -1 -3 7436.14 7445.29 29.04 o 324 1 -6 1 3 7436.14 7445.29 29.04 o 325 2 -2 -1 -3 3378.19 3473.01 27.90 o 325 1 -4 1 3 3378.19 3473.01 27.90 o 326 2 0 -1 -3 6676.44 6957.71 32.43 o 326 1 -2 1 3 6676.44 6957.71 32.43 o 327 2 2 -1 -3 9073.39 9278.33 29.04 o 327 1 0 1 3 9073.39 9278.33 29.04 o 328 2 4 -1 -3 901.01 1061.13 16.97 o 328 1 2 1 3 901.01 1061.13 16.97 o 329 2 6 -1 -3 8773.44 8892.19 29.04 o 329 1 4 1 3 8773.44 8892.19 29.04 o 330 2 8 -1 -3 1325.67 1304.74 18.10 o 330 1 6 1 3 1325.67 1304.74 18.10 o 331 1 8 1 3 2436.64 3062.36 22.25 o 332 1 10 1 3 1897.04 2091.35 20.36 o 333 1 12 1 3 19.29 105.21 16.21 o 334 1 14 1 3 1160.08 1168.61 21.12 o 335 1 16 1 3 109.92 99.18 21.87 o 336 1 -19 2 3 276.32 284.70 36.95 o 337 1 -17 2 3 456.50 466.08 30.17 o 338 1 -15 2 3 211.01 336.36 27.15 o 339 1 -13 2 3 1915.97 2038.93 33.18 o 340 1 -11 2 3 39.06 82.58 21.49 o 341 2 -7 -2 -3 3227.90 3325.57 25.27 o 341 1 -9 2 3 3227.90 3325.57 25.27 o 342 2 -5 -2 -3 2733.09 2667.54 21.49 o 342 1 -7 2 3 2733.09 2667.54 21.49 o 343 2 -3 -2 -3 2041.63 1922.03 19.23 o 343 1 -5 2 3 2041.63 1922.03 19.23 o 344 2 -1 -2 -3 5858.71 5932.02 26.02 o 344 1 -3 2 3 5858.71 5932.02 26.02 o 345 2 1 -2 -3 417.94 420.08 16.21 o 345 1 -1 2 3 417.94 420.08 16.21 o 346 2 3 -2 -3 5305.43 5649.96 24.89 o 346 1 1 2 3 5305.43 5649.96 24.89 o 347 2 5 -2 -3 3390.46 3452.65 25.64 o 347 1 3 2 3 3390.46 3452.65 25.64 o 348 2 7 -2 -3 1201.77 1280.22 21.49 o 348 1 5 2 3 1201.77 1280.22 21.49 o 349 2 9 -2 -3 3848.78 3661.18 26.77 o 349 1 7 2 3 3848.78 3661.18 26.77 o 350 1 9 2 3 289.89 293.75 19.61 o 351 1 11 2 3 1530.47 1815.32 24.13 o 352 1 13 2 3 670.85 679.14 23.38 o 353 1 15 2 3 92.18 161.02 24.51 o 354 1 17 2 3 525.22 283.95 25.64 o 355 1 -16 3 3 470.02 564.13 29.04 o 356 1 -14 3 3 237.19 264.72 41.10 o 357 1 -12 3 3 436.74 684.80 38.46 o 358 1 -10 3 3 1861.99 2086.82 28.28 o 359 2 -6 -3 -3 168.02 206.27 20.36 o 359 1 -8 3 3 168.02 206.27 20.36 o 360 2 -4 -3 -3 3729.91 3859.15 24.51 o 360 1 -6 3 3 3729.91 3859.15 24.51 o 361 2 -2 -3 -3 1442.46 1546.07 18.10 o 361 1 -4 3 3 1442.46 1546.07 18.10 o 362 2 0 -3 -3 3060.22 3077.82 21.87 o 362 1 -2 3 3 3060.22 3077.82 21.87 o 363 2 2 -3 -3 4305.95 4354.65 24.13 o 363 1 0 3 3 4305.95 4354.65 24.13 o 364 2 4 -3 -3 405.30 520.01 17.72 o 364 1 2 3 3 405.30 520.01 17.72 o 365 2 6 -3 -3 4181.92 4094.46 23.76 o 365 1 4 3 3 4181.92 4094.46 23.76 o 366 2 8 -3 -3 652.21 577.33 18.48 o 366 1 6 3 3 652.21 577.33 18.48 o 367 1 8 3 3 1214.20 1466.13 19.99 o 368 1 10 3 3 985.62 1043.03 19.99 o 369 1 12 3 3 12.02 47.14 18.85 o 370 1 14 3 3 610.76 644.07 24.13 o 371 1 -15 4 3 84.88 77.68 44.87 < 372 1 -13 4 3 732.21 745.89 42.61 o 373 1 -11 4 3 17.69 39.22 25.27 < 374 2 -7 -4 -3 1222.41 1258.73 27.15 o 374 1 -9 4 3 1222.41 1258.73 27.15 o 375 2 -5 -4 -3 932.37 976.29 24.13 o 375 1 -7 4 3 932.37 976.29 24.13 o 376 2 -3 -4 -3 672.28 727.03 23.38 o 376 1 -5 4 3 672.28 727.03 23.38 o 377 2 -1 -4 -3 2117.36 2168.65 21.49 o 377 1 -3 4 3 2117.36 2168.65 21.49 o 378 2 1 -4 -3 129.29 152.35 16.59 o 378 1 -1 4 3 129.29 152.35 16.59 o 379 2 3 -4 -3 1855.52 1849.26 21.12 o 379 1 1 4 3 1855.52 1849.26 21.12 o 380 2 5 -4 -3 1178.70 1159.56 19.61 o 380 1 3 4 3 1178.70 1159.56 19.61 o 381 2 7 -4 -3 417.52 392.55 19.23 o 381 1 5 4 3 417.52 392.55 19.23 o 382 2 9 -4 -3 1445.50 1406.17 21.49 o 382 1 7 4 3 1445.50 1406.17 21.49 o 383 1 9 4 3 99.27 94.65 18.10 o 384 1 11 4 3 572.59 646.33 21.87 o 385 1 13 4 3 281.20 279.80 23.76 o 386 1 -12 5 3 132.13 159.13 38.09 o 387 1 -10 5 3 511.11 461.94 27.53 o 388 2 -6 -5 -3 42.55 39.97 24.13 < 388 1 -8 5 3 42.55 39.97 24.13 < 389 2 -4 -5 -3 1044.24 955.17 27.53 o 389 1 -6 5 3 1044.24 955.17 27.53 o 390 2 -2 -5 -3 366.09 374.83 24.13 o 390 1 -4 5 3 366.09 374.83 24.13 o 391 2 0 -5 -3 784.48 752.30 21.49 o 391 1 -2 5 3 784.48 752.30 21.49 o 392 2 2 -5 -3 1143.36 1095.07 21.87 o 392 1 0 5 3 1143.36 1095.07 21.87 o 393 2 4 -5 -3 101.24 70.89 20.74 o 393 1 2 5 3 101.24 70.89 20.74 o 394 2 6 -5 -3 1155.56 984.21 23.38 o 394 1 4 5 3 1155.56 984.21 23.38 o 395 2 8 -5 -3 173.25 178.36 20.74 o 395 1 6 5 3 173.25 178.36 20.74 o 396 1 8 5 3 328.88 363.89 24.13 o 397 1 10 5 3 305.26 314.49 25.64 o 398 2 -3 -6 -3 135.37 116.52 27.15 o 398 1 -5 6 3 135.37 116.52 27.15 o 399 2 -1 -6 -3 449.56 411.41 23.38 o 399 1 -3 6 3 449.56 411.41 23.38 o 400 2 1 -6 -3 23.53 56.19 24.51 o 400 1 -1 6 3 23.53 56.19 24.51 o 401 2 3 -6 -3 386.85 337.12 24.89 o 401 1 1 6 3 386.85 337.12 24.89 o 402 2 5 -6 -3 240.70 230.78 26.40 o 402 1 3 6 3 240.70 230.78 26.40 o 403 1 -18 0 4 41.56 45.25 38.09 < 404 1 -16 0 4 507.83 535.85 33.18 o 405 1 -14 0 4 228.13 176.48 26.77 o 406 1 -12 0 4 821.34 815.27 24.13 o 407 1 -10 0 4 1822.26 1549.84 27.90 o 408 1 -8 0 4 115.25 118.78 34.69 o 409 1 -6 0 4 3617.14 3563.13 29.79 o 410 1 -4 0 4 1147.28 1161.44 24.13 o 411 1 -2 0 4 3418.65 3378.36 28.28 o 412 1 0 0 4 3502.87 3699.26 29.04 o 413 1 2 0 4 226.36 211.17 23.38 o 414 1 4 0 4 4338.94 4601.64 33.18 o 415 1 6 0 4 332.22 314.49 24.13 o 416 1 8 0 4 1538.23 1437.09 25.64 o 417 1 10 0 4 931.00 957.06 26.02 o 418 1 12 0 4 57.60 32.05 25.27 < 419 1 14 0 4 684.32 552.06 31.68 o 420 1 16 0 4 26.82 37.33 32.43 < 421 1 -17 1 4 311.98 280.18 30.17 o 422 1 -15 1 4 325.12 308.46 23.00 o 423 1 -13 1 4 1201.13 1254.58 21.87 o 424 1 -11 1 4 1.44 8.30 16.97 < 425 1 -9 1 4 2153.04 2153.94 24.51 o 426 1 -7 1 4 1285.10 1275.70 18.10 o 427 1 -5 1 4 1392.66 1395.24 20.36 o 428 1 -3 1 4 3079.30 3309.73 24.51 o 429 1 -1 1 4 59.97 81.83 15.08 o 430 1 1 1 4 3502.59 3634.03 21.49 o 431 1 3 1 4 1362.73 1440.11 17.72 o 432 1 5 1 4 619.46 655.39 16.97 o 433 1 7 1 4 2239.91 2193.16 19.99 o 434 1 9 1 4 46.06 52.79 16.97 o 435 1 11 1 4 1141.22 1168.23 20.74 o 436 1 13 1 4 332.32 312.99 19.99 o 437 1 15 1 4 108.29 94.27 21.87 o 438 1 -16 2 4 386.67 389.91 32.05 o 439 1 -14 2 4 160.85 152.72 22.63 o 440 1 -12 2 4 589.80 560.73 21.87 o 441 1 -10 2 4 1330.07 1376.38 19.23 o 442 1 -8 2 4 90.81 73.53 15.46 o 443 1 -6 2 4 2563.39 2545.74 21.87 o 444 1 -4 2 4 791.24 841.67 16.97 o 445 1 -2 2 4 2435.44 2528.40 19.99 o 446 1 0 2 4 2428.42 2644.54 23.76 o 447 1 2 2 4 166.62 236.44 18.85 o 448 1 4 2 4 3071.40 3270.13 24.13 o 449 1 6 2 4 228.08 254.16 19.61 o 450 1 8 2 4 1102.80 1044.17 19.61 o 451 1 10 2 4 677.57 620.69 18.85 o 452 1 12 2 4 44.93 40.35 23.00 < 453 1 14 2 4 498.31 345.04 26.02 o 454 1 -15 3 4 168.09 188.55 29.04 o 455 1 -13 3 4 651.83 573.18 26.77 o 456 1 -11 3 4 0.55 29.41 19.99 < 457 1 -9 3 4 1094.53 1118.45 19.99 o 458 1 -7 3 4 652.90 685.17 18.48 o 459 1 -5 3 4 672.11 687.44 18.48 o 460 1 -3 3 4 1562.34 1555.50 19.23 o 461 1 -1 3 4 30.29 42.61 16.21 o 462 1 1 3 4 1726.06 1913.36 18.85 o 463 1 3 3 4 705.02 773.04 18.10 o 464 1 5 3 4 312.76 323.92 18.48 o 465 1 7 3 4 1171.15 1124.49 21.49 o 466 1 9 3 4 23.81 51.28 19.23 o 467 1 11 3 4 602.37 547.16 21.49 o 468 1 13 3 4 190.69 160.64 22.63 o 469 1 -12 4 4 231.14 208.15 25.64 o 470 1 -10 4 4 514.18 533.96 22.25 o 471 1 -8 4 4 31.60 20.36 19.23 < 472 1 -6 4 4 992.31 1008.72 22.25 o 473 1 -4 4 4 271.97 316.00 18.85 o 474 1 -2 4 4 862.28 876.74 20.36 o 475 1 0 4 4 928.90 911.43 19.99 o 476 1 2 4 4 68.71 102.95 18.48 o 477 1 4 4 4 1141.96 1166.72 21.49 o 478 1 6 4 4 88.15 83.71 19.99 o 479 1 8 4 4 428.68 374.07 23.38 o 480 1 10 4 4 277.11 266.98 23.38 o 481 1 -9 5 4 330.08 309.97 25.27 o 482 1 -7 5 4 175.47 150.84 23.38 o 483 1 -5 5 4 177.43 184.02 20.74 o 484 1 -3 5 4 461.03 507.94 22.25 o 485 1 -1 5 4 5.16 -5.28 22.63 < 486 1 1 5 4 463.91 461.56 23.38 o 487 1 3 5 4 206.70 209.66 22.63 o 488 1 5 5 4 92.91 158.00 23.76 o 489 1 7 5 4 343.35 224.37 54.68 o 490 1 -15 0 5 281.23 295.64 32.05 o 491 1 -13 0 5 518.38 509.07 28.66 o 492 1 -11 0 5 3.30 30.17 24.51 < 493 1 -9 0 5 1307.12 1121.47 26.02 o 494 1 -7 0 5 371.51 401.98 34.69 o 495 1 -5 0 5 856.75 876.74 22.63 o 496 1 -3 0 5 1399.77 1470.66 24.51 o 497 1 -1 0 5 0.40 -5.66 22.25 < 498 1 1 0 5 1880.71 2000.09 26.40 o 499 1 3 0 5 399.30 497.01 25.27 o 500 1 5 0 5 410.72 471.74 26.02 o 501 1 7 0 5 1081.03 1243.65 28.66 o 502 1 9 0 5 0.31 -20.74 27.53 < 503 1 11 0 5 574.02 583.74 30.17 o 504 1 13 0 5 123.41 67.88 33.56 o 505 1 -16 1 5 232.95 206.65 62.97 o 506 1 -14 1 5 73.66 67.12 19.99 o 507 1 -12 1 5 535.14 509.83 20.36 o 508 1 -10 1 5 604.90 590.53 23.00 o 509 1 -8 1 5 112.59 73.53 17.72 o 510 1 -6 1 5 1660.59 1756.87 18.48 o 511 1 -4 1 5 218.05 227.76 18.10 o 512 1 -2 1 5 1666.53 1805.14 21.87 o 513 1 0 1 5 1105.74 1266.27 18.48 o 514 1 2 1 5 208.65 243.60 17.72 o 515 1 4 1 5 1816.17 1978.97 20.36 o 516 1 6 1 5 30.41 42.23 17.72 o 517 1 8 1 5 678.86 605.61 19.61 o 518 1 10 1 5 341.24 309.97 21.87 o 519 1 12 1 5 68.41 56.19 21.87 o 520 1 -15 2 5 203.18 182.51 30.54 o 521 1 -13 2 5 388.47 420.08 23.76 o 522 1 -11 2 5 2.86 14.71 24.13 < 523 1 -9 2 5 938.57 1020.03 20.74 o 524 1 -7 2 5 270.25 293.75 17.72 o 525 1 -5 2 5 608.48 661.42 18.48 o 526 1 -3 2 5 1006.61 1099.22 18.10 o 527 1 -1 2 5 0.21 -19.61 16.59 < 528 1 1 2 5 1339.58 1402.40 22.25 o 529 1 3 2 5 293.45 308.84 20.74 o 530 1 5 2 5 295.08 294.51 21.12 o 531 1 7 2 5 791.20 755.69 24.51 o 532 1 9 2 5 0.19 23.76 23.00 < 533 1 11 2 5 422.55 369.55 26.02 o 534 1 -12 3 5 283.42 236.06 27.53 o 535 1 -10 3 5 334.31 305.82 22.25 o 536 1 -8 3 5 62.22 50.53 18.48 o 537 1 -6 3 5 883.67 894.08 21.12 o 538 1 -4 3 5 109.64 128.96 18.85 o 539 1 -2 3 5 865.85 895.21 20.74 o 540 1 0 3 5 591.15 588.64 18.85 o 541 1 2 3 5 118.14 116.90 18.85 o 542 1 4 3 5 953.05 975.16 21.49 o 543 1 6 3 5 16.60 27.90 21.12 < 544 1 8 3 5 372.62 329.58 23.00 o 545 1 10 3 5 187.33 187.41 41.86 o 546 1 -9 4 5 371.27 317.51 22.63 o 547 1 -7 4 5 106.22 97.67 21.49 o 548 1 -5 4 5 232.66 245.49 21.49 o 549 1 -3 4 5 402.87 408.77 22.63 o 550 1 -1 4 5 0.42 42.99 21.49 < 551 1 1 4 5 502.61 471.74 21.87 o 552 1 3 4 5 123.81 121.42 21.87 o 553 1 5 4 5 122.79 136.51 23.76 o 554 1 -12 0 6 316.87 285.08 32.05 o 555 2 -6 0 -6 188.13 180.25 27.90 o 555 1 -10 0 6 188.13 180.25 27.90 o 556 2 -4 0 -6 255.02 46.76 44.12 < 556 1 -8 0 6 255.02 46.76 44.12 < 557 2 -2 0 -6 822.45 990.24 43.37 o 557 1 -6 0 6 822.45 990.24 43.37 o 558 2 0 0 -6 105.93 -1.89 23.38 < 558 1 -4 0 6 105.93 -1.89 23.38 < 559 2 2 0 -6 950.82 821.30 29.41 o 559 1 -2 0 6 950.82 821.30 29.41 o 560 2 4 0 -6 373.81 453.26 27.53 o 560 1 0 0 6 373.81 453.26 27.53 o 561 2 6 0 -6 350.97 81.45 29.04 o 561 1 2 0 6 350.97 81.45 29.04 o 562 2 8 0 -6 765.58 819.04 30.54 o 562 1 4 0 6 765.58 819.04 30.54 o 563 2 10 0 -6 44.14 -4.15 29.79 < 563 1 6 0 6 44.14 -4.15 29.79 < 564 1 8 0 6 303.07 274.90 33.94 o 565 1 -11 1 6 9.30 46.38 21.12 o 566 2 -5 -1 -6 610.77 520.39 24.89 o 566 1 -9 1 6 610.77 520.39 24.89 o 567 2 -3 -1 -6 77.23 39.59 19.23 o 567 1 -7 1 6 77.23 39.59 19.23 o 568 2 -1 -1 -6 513.26 327.32 23.38 o 568 1 -5 1 6 513.26 327.32 23.38 o 569 2 1 -1 -6 487.42 532.08 22.63 o 569 1 -3 1 6 487.42 532.08 22.63 o 570 2 3 -1 -6 132.99 27.15 22.63 < 570 1 -1 1 6 132.99 27.15 22.63 < 571 2 5 -1 -6 770.07 736.46 20.74 o 571 1 1 1 6 770.07 736.46 20.74 o 572 2 7 -1 -6 95.97 90.50 20.36 o 572 1 3 1 6 95.97 90.50 20.36 o 573 2 9 -1 -6 328.43 182.89 21.49 o 573 1 5 1 6 328.43 182.89 21.49 o 574 1 7 1 6 375.70 303.93 23.38 o 575 2 -6 -2 -6 143.24 107.09 26.40 o 575 1 -10 2 6 143.24 107.09 26.40 o 576 2 -4 -2 -6 188.37 42.99 20.36 o 576 1 -8 2 6 188.37 42.99 20.36 o 577 2 -2 -2 -6 607.76 566.01 21.49 o 577 1 -6 2 6 607.76 566.01 21.49 o 578 2 0 -2 -6 78.54 14.33 20.36 < 578 1 -4 2 6 78.54 14.33 20.36 < 579 2 2 -2 -6 694.88 556.59 20.36 o 579 1 -2 2 6 694.88 556.59 20.36 o 580 2 4 -2 -6 279.75 196.84 20.36 o 580 1 0 2 6 279.75 196.84 20.36 o 581 2 6 -2 -6 264.06 145.18 24.89 o 581 1 2 2 6 264.06 145.18 24.89 o 582 2 8 -2 -6 558.44 551.31 25.27 o 582 1 4 2 6 558.44 551.31 25.27 o 583 2 10 -2 -6 33.56 38.09 25.27 < 583 1 6 2 6 33.56 38.09 25.27 < 584 2 -3 -3 -6 44.74 65.24 23.38 o 584 1 -7 3 6 44.74 65.24 23.38 o 585 2 -1 -3 -6 277.74 177.99 23.00 o 585 1 -5 3 6 277.74 177.99 23.00 o 586 2 1 -3 -6 267.11 304.69 22.63 o 586 1 -3 3 6 267.11 304.69 22.63 o 587 2 3 -3 -6 73.66 30.92 22.63 < 587 1 -1 3 6 73.66 30.92 22.63 < 588 2 5 -3 -6 409.39 332.22 22.63 o 588 1 1 3 6 409.39 332.22 22.63 o 589 2 7 -3 -6 56.99 84.85 22.63 o 589 1 3 3 6 56.99 84.85 22.63 o