Crystallography Open Database

Information card for entry 4135610

Preview

Coordinates	4135610.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44.5 H66 F3 N2 O3 S Sb
Calculated formula	C44.5 H66 F3 N2 O3 S Sb
Title of publication	Donor-Stabilized Antimony(I) and Bismuth(I) Ions: Heavier Valence Isoelectronic Analogues of Carbones.
Authors of publication	Siddiqui, Mujahuddin M.; Sarkar, Samir Kumar; Nazish, Mohd; Morganti, Massimiliano; Köhler, Christian; Cai, Jiali; Zhao, Lili; Herbst-Irmer, Regine; Stalke, Dietmar; Frenking, Gernot; Roesky, Herbert W.
Journal of publication	Journal of the American Chemical Society
Year of publication	2021
Journal volume	143
Journal issue	3
Pages of publication	1301 - 1306
a	9.189 ± 0.002 Å
b	15.33 ± 0.002 Å
c	32.284 ± 0.004 Å
α	90°
β	92.02 ± 0.02°
γ	90°
Cell volume	4544.9 ± 1.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0373
Residual factor for significantly intense reflections	0.0274
Weighted residual factors for significantly intense reflections	0.0598
Weighted residual factors for all reflections included in the refinement	0.0646
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
261475 (current)	2021-02-04	cif/ Adding structures of 4135610 via cif-deposit CGI script.	4135610.cif