#------------------------------------------------------------------------------ #$Date: 2012-02-04 18:30:22 +0200 (Sat, 04 Feb 2012) $ #$Revision: 32116 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/4300182.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4300182 _journal_name_full 'Inorganic Chemistry' _journal_year 2000 _publ_section_title ; Trimerization of NaC2N3 to Na3C6N9 in the Solid: Ab Initio Crystal Structure Determination of two Polymorphs of NaC2N3 and of Na3C6N9 from X-ray Powder Diffractometry ; _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' loop_ _publ_author_name 'Barbara Juergens' 'Elisabeth Irran' 'Julius Schneider' 'Wolfgang Schnick' _chemical_formula_sum 'C2 N3 Na' _cell_length_a 11.0482(1) _cell_length_b 23.3806(3) _cell_length_c 3.51616(3) _cell_angle_alpha 90.0 _cell_angle_beta 97.9131(9) _cell_angle_gamma 90.0 _symmetry_cell_setting monoclinic loop_ _symmetry_equiv_pos_as_xyz +x,+y,+z -x+1/2,+y+1/2,-z+1/2 -x,-y,-z +x+1/2,-y+1/2,+z+1/2 _pd_phase_block_id PHASE_1 _pd_instr_radiation_probe x-ray _diffrn_radiation_polarisn_ratio .5 _diffrn_radiation_wavelength .59733 _diffrn_radiation_type 'synchrotron radiation' _pd_proc_ls_prof_R_factor "0.059" _pd_proc_ls_prof_wR_factor "0.080" _pd_proc_ls_prof_wR_expected "" _pd_proc_info_datetime "11:15:30 07-OCT-1999" _pd_calc_method "Rietveld Refinement" _pd_meas_2theta_range_min 2.5 _pd_meas_2theta_range_max 35.995 _pd_meas_2theta_range_inc .005 _pd_proc_2theta_range_min 2.5 _pd_proc_2theta_range_max 35.995 _pd_proc_2theta_range_inc .005 _pd_meas_number_of_points 6700 _pd_proc_number_of_points 6700 loop_ _pd_refln_index_h _pd_refln_index_k _pd_refln_index_l _pd_refln_phase_id _refln_observed_status _refln_F_squared_calc _refln_F_squared_meas _refln_phase_calc _pd_refln_i100_meas 0 2 0 1 o 332.162 313.169 180.00 11.56 1 1 0 1 o 24.133 2.115 .00 1.21 1 2 0 1 o 3074.000 3054.046 .00 100.00 1 3 0 1 o 71.956 .382 .00 1.48 0 4 0 1 o 117.920 12.884 .00 1.03 2 0 0 1 o 17.610 2.046 .00 .14 2 1 0 1 o 85.741 58.242 .00 1.25 1 4 0 1 o 65.168 13.507 180.00 .88 2 2 0 1 o 556.899 637.746 .00 6.91 2 3 0 1 o -1.345 44.502 .00 .00 1 5 0 1 o 551.633 505.331 .00 5.28 2 4 0 1 o 1321.243 1333.303 180.00 10.77 0 6 0 1 o 60.172 5.972 .00 .23 1 6 0 1 o 137.941 194.719 180.00 .94 3 1 0 1 o 1331.242 1482.202 .00 8.80 2 5 0 1 o 3254.186 3602.396 180.00 21.05 1 0 -1 1 o 4511.284 4047.441 .00 13.79 3 2 0 1 o 433.436 553.036 180.00 2.72 0 1 1 1 o 340.762 326.018 .00 2.07 1 1 -1 1 o 1599.837 1362.656 180.00 9.57 0 2 1 1 o 2878.917 2709.364 .00 16.35 1 2 -1 1 o 185.475 139.319 .00 1.03 3 3 0 1 o 1918.345 2041.852 180.00 10.77 1 0 1 1 o 325.966 360.505 .00 .85 1 1 1 1 o 2499.867 2508.219 180.00 12.85 0 3 1 1 o 4041.455 3746.816 .00 20.89 1 7 0 1 o 33.340 38.700 180.00 .17 1 3 -1 1 o 289.769 309.713 180.00 1.51 2 6 0 1 o 3893.535 3896.458 180.00 20.17 1 2 1 1 o 5058.373 4718.938 180.00 24.57 2 1 -1 1 o 27.726 120.361 180.00 .15 3 4 0 1 o 1270.221 1409.592 180.00 6.24 2 2 -1 1 o 5387.682 5014.220 .00 25.43 0 4 1 1 o 1950.956 2086.025 180.00 8.96 1 3 1 1 o 21.247 52.371 .00 .10 1 4 -1 1 o 15068.600 14706.740 180.00 68.46 2 3 -1 1 o 15754.040 14202.010 180.00 68.53 0 8 0 1 o 3854.281 4130.464 .00 8.50 3 5 0 1 o 5.166 7.628 .00 .02 1 4 1 1 o 1878.522 1870.004 .00 7.61 2 7 0 1 o 349.141 344.680 .00 1.45 0 5 1 1 o 2953.775 2785.861 180.00 11.83 1 5 -1 1 o 7002.795 6616.700 .00 27.83 1 8 0 1 o .043 .473 .00 .00 2 1 1 1 o 6104.958 6048.750 .00 23.77 2 4 -1 1 o 47.308 41.881 .00 .19 2 2 1 1 o 891.039 799.778 180.00 3.33 4 0 0 1 o 1457.542 1754.417 180.00 2.80 3 0 -1 1 o 14429.640 14436.380 .00 27.26 4 1 0 1 o 191.022 182.441 180.00 .72 3 1 -1 1 o 464.521 436.137 .00 1.74 1 5 1 1 o 6794.958 7418.081 180.00 24.32 4 2 0 1 o 5020.597 5722.781 180.00 18.35 3 6 0 1 o 978.100 1116.799 .00 3.58 3 2 -1 1 o 736.205 816.710 .00 2.63 2 3 1 1 o 131.667 136.684 .00 .46 2 5 -1 1 o 78.638 82.541 .00 .27 0 6 1 1 o 314.135 324.769 180.00 1.09 1 6 -1 1 o 2477.603 2483.974 180.00 8.54 4 3 0 1 o 844.573 962.951 180.00 2.87 3 3 -1 1 o 6016.421 5495.098 180.00 20.32 2 8 0 1 o 617.791 700.113 .00 2.12 2 4 1 1 o 177.731 198.342 .00 .57 1 9 0 1 o 32.164 56.625 .00 .11 1 6 1 1 o 815.130 538.082 .00 2.56 3 4 -1 1 o 894.420 501.062 .00 2.77 2 6 -1 1 o 561.390 166.155 180.00 1.72 4 4 0 1 o 2.365 1.169 180.00 .01 3 7 0 1 o 40.515 22.992 180.00 .13 0 7 1 1 o 751.024 724.352 .00 2.24 1 7 -1 1 o 142.257 216.334 .00 .42 2 5 1 1 o 7.491 5.522 180.00 .02 3 0 1 1 o 3780.225 3348.180 180.00 5.42 3 1 1 1 o 2795.456 2827.428 180.00 7.96 3 5 -1 1 o 3002.865 3103.107 .00 8.51 4 5 0 1 o 1484.201 1361.449 180.00 4.26 3 2 1 1 o 778.371 800.675 .00 2.14 2 9 0 1 o 31.442 33.796 .00 .09 1 7 1 1 o 1110.476 969.659 180.00 3.04 0 10 0 1 o 1002.801 1092.344 .00 1.41 4 1 -1 1 o 93.600 85.452 .00 .25 2 7 -1 1 o 1224.231 1328.521 180.00 3.31 4 2 -1 1 o 62.091 63.120 .00 .16 3 8 0 1 o 1721.951 1818.855 .00 4.62 3 3 1 1 o 366.179 355.514 .00 .97 2 6 1 1 o 731.782 720.865 180.00 1.92 1 10 0 1 o 10.816 11.912 .00 .03 0 8 1 1 o 3.130 3.429 .00 .01 1 8 -1 1 o 17.984 27.385 180.00 .05 3 6 -1 1 o 945.341 1050.789 180.00 2.42 4 6 0 1 o 7181.204 7327.614 180.00 18.56 4 3 -1 1 o 136.446 119.279 .00 .35 3 4 1 1 o 1502.532 1338.099 .00 3.72 5 1 0 1 o 1997.297 1976.633 .00 4.89 1 8 1 1 o 55.437 50.546 180.00 .13 4 4 -1 1 o 579.929 665.943 180.00 1.38 2 8 -1 1 o 1567.253 1780.540 180.00 3.71 5 2 0 1 o 2927.501 3091.392 180.00 6.98 2 10 0 1 o 3754.647 4229.269 180.00 8.94 2 7 1 1 o 351.210 348.934 .00 .83 3 5 1 1 o 1769.922 1816.602 180.00 4.06 3 7 -1 1 o 1745.740 1740.781 180.00 3.99 4 7 0 1 o 3927.509 4169.039 180.00 9.08 3 9 0 1 o 877.145 926.130 180.00 2.03 5 3 0 1 o 75.949 74.763 180.00 .18 0 9 1 1 o 788.184 800.771 .00 1.76 1 9 -1 1 o 110.148 137.363 .00 .25 4 5 -1 1 o 742.443 594.926 .00 1.66 1 11 0 1 o 1588.237 1637.662 180.00 3.56 5 4 0 1 o 155.427 22.712 180.00 .34 3 6 1 1 o 634.110 529.029 .00 1.34 1 9 1 1 o 3.603 3.163 .00 .01 4 1 1 1 o 305.866 292.399 .00 .64 2 8 1 1 o 2757.612 2836.857 .00 5.75 2 9 -1 1 o 1752.705 1939.100 180.00 3.63 4 2 1 1 o 3.730 15.859 180.00 .01 3 8 -1 1 o 73.265 116.496 .00 .15 4 6 -1 1 o 110.396 172.711 .00 .23 4 8 0 1 o 18.514 33.981 .00 .04 5 0 -1 1 o 6611.712 7351.380 .00 6.71 5 1 -1 1 o 283.065 358.029 .00 .57 5 5 0 1 o 1199.937 1210.939 180.00 2.43 2 11 0 1 o 4358.238 4460.631 .00 8.85 4 3 1 1 o 6981.037 7513.056 180.00 13.79 3 10 0 1 o 607.416 590.409 180.00 1.22 5 2 -1 1 o 241.507 331.162 .00 .48 0 10 1 1 o 1027.101 1006.643 180.00 2.01 1 10 -1 1 o 431.198 524.373 180.00 .84 0 12 0 1 o 512.431 754.116 .00 .51 3 7 1 1 o 2777.751 3132.573 .00 5.35 5 3 -1 1 o 971.696 1233.772 180.00 1.85 4 4 1 1 o 9.559 34.301 180.00 .02 1 12 0 1 o 419.731 540.516 .00 .80 4 7 -1 1 o 554.549 678.845 .00 1.04 5 6 0 1 o .236 2.641 .00 .00 2 9 1 1 o 4240.073 5254.605 .00 7.89 1 10 1 1 o 668.357 659.477 180.00 1.23 3 9 -1 1 o 94.603 143.591 .00 .17 2 10 -1 1 o 738.642 1082.053 .00 1.35 5 4 -1 1 o 11.231 16.402 .00 .02 4 9 0 1 o 789.970 770.461 .00 1.44 4 5 1 1 o 1333.972 1630.092 180.00 2.38 3 8 1 1 o 522.218 650.237 .00 .91 3 11 0 1 o 798.086 932.279 180.00 1.40 2 12 0 1 o 304.806 425.719 .00 .53 5 5 -1 1 o 434.792 426.769 180.00 .74 5 7 0 1 o 12.103 21.621 180.00 .02 0 11 1 1 o 547.266 757.978 180.00 .93 4 8 -1 1 o .716 .973 180.00 .00 6 0 0 1 o 3654.175 3425.718 .00 3.14 1 11 -1 1 o 2692.886 3038.695 180.00 4.58 6 1 0 1 o 191.183 248.422 180.00 .33 4 6 1 1 o 160.362 168.402 180.00 .27 6 2 0 1 o 774.984 736.453 180.00 1.30 2 10 1 1 o 177.073 113.998 180.00 .29 3 10 -1 1 o 1.181 2.770 180.00 .00 1 11 1 1 o 7.775 14.495 .00 .01 4 10 0 1 o 256.426 251.855 180.00 .42 1 1 -2 1 o 266.281 231.059 .00 .42 5 6 -1 1 o 564.158 744.171 180.00 .91 6 3 0 1 o 156.940 168.244 .00 .26 1 13 0 1 o 1868.336 2171.588 .00 3.06 2 11 -1 1 o 420.076 401.983 180.00 .68 0 0 2 1 o 7295.603 6802.130 180.00 5.74 1 2 -2 1 o 768.594 765.683 180.00 1.20 0 1 2 1 o 1516.974 1477.038 180.00 2.37 5 0 1 1 o 137.622 141.117 180.00 .11 3 9 1 1 o 11.137 11.306 .00 .02 5 1 1 1 o 258.401 233.847 180.00 .41 2 0 -2 1 o 824.651 1020.878 180.00 .64 5 8 0 1 o 11.565 8.935 .00 .02 2 1 -2 1 o 68.783 98.170 180.00 .10 0 2 2 1 o 57.175 82.960 180.00 .09 6 4 0 1 o 2637.840 2392.093 .00 4.16 4 7 1 1 o 89.836 112.159 180.00 .14 5 2 1 1 o 1016.231 1260.186 180.00 1.58 1 3 -2 1 o 31.423 56.241 180.00 .05 4 9 -1 1 o 496.796 606.065 180.00 .77 2 2 -2 1 o 536.823 672.056 .00 .82 0 3 2 1 o 84.049 92.699 180.00 .13 6 1 -1 1 o 820.943 973.344 .00 1.24 3 12 0 1 o 497.339 558.066 180.00 .76 5 3 1 1 o 108.931 169.360 .00 .16 5 7 -1 1 o 12.136 17.125 .00 .02 2 3 -2 1 o 154.839 238.977 180.00 .23 0 12 1 1 o 59.134 59.218 180.00 .09 2 13 0 1 o 170.008 223.792 .00 .26 1 12 -1 1 o 19.470 26.968 180.00 .03 6 2 -1 1 o 1033.941 1469.225 180.00 1.55 1 4 -2 1 o 2078.753 1982.424 180.00 3.05 1 1 2 1 o 894.899 897.937 180.00 1.31 6 5 0 1 o 649.081 624.823 180.00 .97 2 11 1 1 o 244.195 312.053 .00 .36 0 4 2 1 o 478.915 482.584 180.00 .69 1 2 2 1 o 816.920 815.810 .00 1.18 6 3 -1 1 o 1624.732 1952.637 .00 2.36 5 4 1 1 o 299.504 322.531 180.00 .44 3 11 -1 1 o 1174.284 1126.161 180.00 1.71 3 1 -2 1 o 2986.849 3237.683 .00 4.27 2 4 -2 1 o 411.589 447.657 180.00 .58 4 11 0 1 o 104.616 107.625 .00 .15 5 9 0 1 o 852.079 818.822 .00 1.24 1 12 1 1 o 2874.971 2851.581 .00 4.13 4 8 1 1 o 6.622 6.948 .00 .01 3 10 1 1 o 159.015 169.690 .00 .23 0 14 0 1 o 909.481 990.799 180.00 .66 3 2 -2 1 o 189.748 220.905 .00 .27 1 3 2 1 o 273.822 319.946 180.00 .39 1 5 -2 1 o 348.386 413.802 180.00 .49 2 12 -1 1 o 50.204 57.190 .00 .07 6 4 -1 1 o 46.034 53.037 .00 .06 4 10 -1 1 o 396.084 517.636 180.00 .55 0 5 2 1 o 39.215 46.626 180.00 .05 6 6 0 1 o 1329.062 1441.778 .00 1.88 1 14 0 1 o .910 1.053 .00 .00 5 8 -1 1 o 1898.610 1821.633 .00 2.66 3 3 -2 1 o 145.171 195.921 .00 .20 5 5 1 1 o 98.522 88.809 .00 .14 2 5 -2 1 o 6209.939 6016.511 .00 8.46 1 4 2 1 o 1227.778 1294.495 180.00 1.66 1 6 -2 1 o 2839.998 2556.790 .00 3.77 6 5 -1 1 o 169.670 363.593 .00 .23 3 4 -2 1 o 476.165 448.671 .00 .63 2 0 2 1 o 113.224 99.354 .00 .07 5 6 1 1 o 50.270 50.844 .00 .07 2 1 2 1 o 244.282 259.327 180.00 .32 3 13 0 1 o 5.275 11.112 .00 .01 0 6 2 1 o 1491.833 1597.712 .00 1.96 0 13 1 1 o 121.134 103.219 .00 .16 1 13 -1 1 o 289.566 263.435 .00 .38 1 5 2 1 o 3481.614 3760.999 180.00 4.54 4 9 1 1 o 107.186 107.261 180.00 .14 2 12 1 1 o 55.694 59.188 180.00 .07 2 2 2 1 o 19.244 23.438 180.00 .02 2 6 -2 1 o 79.456 102.567 180.00 .10 6 7 0 1 o 9.860 8.693 .00 .01 5 10 0 1 o 771.521 605.484 180.00 1.02 2 14 0 1 o 24.876 18.764 180.00 .03 3 12 -1 1 o 339.050 418.438 180.00 .44 4 0 -2 1 o 252.707 319.916 .00 .16 3 11 1 1 o 1445.096 1870.351 .00 1.88 4 12 0 1 o 308.059 290.604 180.00 .40 3 5 -2 1 o 61.891 63.123 180.00 .08 4 1 -2 1 o 103.631 105.832 180.00 .13 2 3 2 1 o 138.472 161.841 180.00 .18 5 9 -1 1 o 324.273 634.392 .00 .42 6 6 -1 1 o 1224.197 1577.178 .00 1.57 1 13 1 1 o 602.130 585.053 180.00 .77 4 2 -2 1 o 360.359 397.646 .00 .46 1 7 -2 1 o .334 .366 180.00 .00 4 11 -1 1 o 208.384 242.428 180.00 .26 2 13 -1 1 o 80.964 95.984 180.00 .10 5 7 1 1 o 1513.464 1478.222 .00 1.89 1 6 2 1 o 148.293 150.985 180.00 .19 0 7 2 1 o 361.724 366.116 .00 .45 7 1 0 1 o 335.932 389.626 .00 .43 2 4 2 1 o 66.900 62.665 180.00 .08 4 3 -2 1 o 41.231 42.433 180.00 .05 2 7 -2 1 o 588.108 445.139 180.00 .72 7 2 0 1 o 369.560 353.363 180.00 .46 3 6 -2 1 o 517.502 549.806 180.00 .63 4 10 1 1 o 50.454 54.124 180.00 .06 6 8 0 1 o 2231.629 2219.577 .00 2.78 6 1 1 1 o 587.178 642.120 180.00 .71 1 15 0 1 o 211.765 243.691 .00 .26 6 2 1 1 o 401.392 359.791 .00 .48 4 4 -2 1 o 34.648 40.207 .00 .04 6 7 -1 1 o 202.187 274.387 180.00 .24 7 3 0 1 o 854.061 638.945 180.00 1.04 2 5 2 1 o 101.996 195.239 .00 .12 5 11 0 1 o 16.728 35.728 .00 .02 1 8 -2 1 o 718.656 765.991 180.00 .85 1 7 2 1 o 462.800 500.403 180.00 .54 6 3 1 1 o 138.486 141.415 180.00 .16 3 1 2 1 o 386.615 405.752 .00 .45 5 10 -1 1 o 6.503 16.775 .00 .01 3 14 0 1 o 764.918 586.022 .00 .92 5 8 1 1 o 2.973 3.141 180.00 .00 2 13 1 1 o .002 .002 180.00 .00 0 14 1 1 o 72.110 71.784 180.00 .09 7 0 -1 1 o 102.898 99.958 180.00 .06 0 8 2 1 o 2820.711 2549.835 180.00 3.29 1 14 -1 1 o 163.217 181.792 180.00 .19 3 12 1 1 o 304.212 314.568 .00 .36 7 1 -1 1 o 143.790 144.353 .00 .17 3 2 2 1 o .034 .032 180.00 .00 7 4 0 1 o 6.644 25.766 180.00 .01 3 13 -1 1 o 134.217 135.778 180.00 .16 2 6 2 1 o 808.446 826.001 .00 .92 3 7 -2 1 o 2942.835 2871.168 .00 3.40 4 5 -2 1 o 1511.359 1472.387 .00 1.75 2 8 -2 1 o 273.850 267.266 .00 .31 4 13 0 1 o 346.090 344.415 180.00 .41 7 2 -1 1 o 555.276 628.553 180.00 .65 2 15 0 1 o 216.906 218.602 .00 .25 6 4 1 1 o 148.802 137.427 180.00 .17 4 12 -1 1 o 674.202 669.918 180.00 .78 3 3 2 1 o .924 1.311 .00 .00 6 9 0 1 o 170.958 213.768 180.00 .20 7 5 0 1 o 96.649 80.106 .00 .11 1 14 1 1 o 586.848 577.952 .00 .67 6 8 -1 1 o 136.238 134.648 180.00 .15 7 3 -1 1 o 187.750 199.696 180.00 .21 2 14 -1 1 o 4.211 8.528 .00 .00 4 11 1 1 o 828.643 1381.895 .00 .92 5 1 -2 1 o 124.796 196.252 180.00 .14 1 8 2 1 o 96.607 100.578 180.00 .11 3 4 2 1 o 2.855 3.039 .00 .00 4 6 -2 1 o 398.351 357.911 .00 .44 1 9 -2 1 o 139.008 121.158 .00 .15 6 5 1 1 o 257.204 214.880 180.00 .28 5 2 -2 1 o 59.826 47.742 .00 .07 2 7 2 1 o 768.483 829.444 .00 .83 5 9 1 1 o .020 .024 180.00 .00 7 4 -1 1 o 1524.869 1451.821 180.00 1.68 0 9 2 1 o 659.505 688.057 .00 .72 3 8 -2 1 o 8.531 9.337 180.00 .01 0 16 0 1 o 151.575 228.933 .00 .09 7 6 0 1 o 196.390 202.911 180.00 .22 5 11 -1 1 o 167.233 198.714 .00 .18 2 9 -2 1 o 1.269 1.356 180.00 .00 5 3 -2 1 o 997.412 1066.352 180.00 1.07 5 12 0 1 o 384.793 308.129 180.00 .43 3 5 2 1 o 192.194 167.126 .00 .20 1 16 0 1 o 803.964 933.543 .00 .88 3 13 1 1 o 522.765 481.672 180.00 .56 2 14 1 1 o 91.071 84.284 .00 .10 6 10 0 1 o 351.650 377.611 180.00 .38 6 6 1 1 o 718.990 547.208 180.00 .76 7 5 -1 1 o 8.050 9.150 180.00 .01 1 9 2 1 o 13.799 14.758 .00 .01 6 9 -1 1 o 312.697 306.194 .00 .33 4 7 -2 1 o 305.055 279.431 .00 .32 5 4 -2 1 o 336.196 305.508 .00 .35 3 15 0 1 o 1157.787 1319.905 180.00 1.24 0 15 1 1 o 467.894 414.303 180.00 .49 3 14 -1 1 o 171.384 153.028 .00 .18 1 15 -1 1 o 2.196 2.051 .00 .00 2 8 2 1 o 45.386 39.116 180.00 .05 4 13 -1 1 o 1784.585 1544.999 .00 1.88 4 14 0 1 o 51.988 40.018 .00 .05 7 7 0 1 o 22.713 21.781 180.00 .02 0 10 2 1 o 106.183 105.137 .00 .11 1 10 -2 1 o 515.462 359.203 180.00 .53 3 6 2 1 o 469.805 338.172 180.00 .48 4 12 1 1 o 618.764 484.587 .00 .64 1 15 1 1 o 28.312 25.653 180.00 .03 3 9 -2 1 o 721.509 672.687 .00 .74 5 10 1 1 o 32.260 33.196 .00 .03 5 5 -2 1 o 80.395 100.270 180.00 .08 2 16 0 1 o 15.108 8.776 .00 .02 7 6 -1 1 o 425.745 271.547 180.00 .44 4 0 2 1 o 83.692 74.553 180.00 .04 4 1 2 1 o 97.008 75.605 .00 .10 6 7 1 1 o 99.436 70.468 .00 .10 2 10 -2 1 o 225.400 190.799 .00 .23 2 15 -1 1 o 29.567 25.865 .00 .03 4 2 2 1 o 2661.731 2079.511 .00 2.63 4 8 -2 1 o 700.592 583.633 180.00 .70 5 13 0 1 o 329.873 356.475 .00 .33 5 12 -1 1 o 714.482 646.228 .00 .72 6 11 0 1 o 138.633 140.114 .00 .14 1 10 2 1 o 164.235 82.080 180.00 .16 6 10 -1 1 o 318.069 276.505 .00 .32 4 3 2 1 o 526.991 302.308 .00 .51 3 7 2 1 o 179.906 104.991 .00 .18 5 6 -2 1 o 567.019 488.983 .00 .55 7 8 0 1 o 248.138 205.708 180.00 .24 2 9 2 1 o 91.182 78.823 .00 .09 7 7 -1 1 o 795.682 610.652 180.00 .78 1 11 -2 1 o 734.173 677.194 .00 .70 3 14 1 1 o 106.150 59.336 .00 .10 8 0 0 1 o 154.756 85.382 .00 .08 2 15 1 1 o 5.561 5.629 .00 .01 7 0 1 1 o 46.279 44.401 .00 .02 8 1 0 1 o 137.369 74.150 180.00 .13 4 4 2 1 o 751.776 789.984 180.00 .71 6 8 1 1 o 2.180 2.037 180.00 .00 6 0 -2 1 o 264.083 246.842 .00 .13 0 11 2 1 o 41.595 43.561 180.00 .04 7 1 1 1 o 358.167 335.549 180.00 .35 3 10 -2 1 o 3.688 3.409 .00 .00 6 1 -2 1 o 183.239 171.868 .00 .18 8 2 0 1 o 324.817 354.305 180.00 .31 1 17 0 1 o 24.674 12.276 180.00 .02 5 11 1 1 o 20.189 18.654 .00 .02 7 2 1 1 o 13.114 12.850 180.00 .01 0 16 1 1 o 747.259 833.230 .00 .71 6 2 -2 1 o 752.926 802.149 .00 .71 4 15 0 1 o 1106.732 963.770 180.00 1.06 4 14 -1 1 o 9.486 9.037 .00 .01 4 9 -2 1 o .444 .328 .00 .00 3 15 -1 1 o 405.748 420.195 180.00 .39 4 13 1 1 o 46.640 35.570 180.00 .04 3 16 0 1 o 1981.784 1872.774 .00 1.91 2 11 -2 1 o 369.091 317.646 180.00 .35 5 7 -2 1 o 35.395 31.161 180.00 .03 8 3 0 1 o 54.355 62.874 180.00 .05 3 8 2 1 o 35.003 32.554 .00 .03 1 16 -1 1 o 297.008 305.940 180.00 .28 7 3 1 1 o 36.049 28.145 180.00 .03 4 5 2 1 o 165.502 157.924 180.00 .15 6 3 -2 1 o 1417.016 1145.806 180.00 1.32 7 9 0 1 o 2563.819 1988.637 .00 2.41 7 8 -1 1 o 16.853 12.925 .00 .02 1 16 1 1 o 25.032 28.081 .00 .02 1 11 2 1 o 147.049 149.329 .00 .13 8 1 -1 1 o 40.104 29.171 180.00 .04 6 11 -1 1 o 21.310 14.940 180.00 .02 2 10 2 1 o 802.428 745.481 .00 .73 8 4 0 1 o 737.533 503.237 .00 .69 6 12 0 1 o 2313.480 1624.228 .00 2.14 5 13 -1 1 o 30.037 22.050 .00 .03 7 4 1 1 o 532.469 479.009 180.00 .49 8 2 -1 1 o 969.990 1126.621 180.00 .90 6 4 -2 1 o 1214.176 1253.458 180.00 1.11 5 14 0 1 o 134.856 124.619 .00 .12 2 17 0 1 o 155.742 87.420 .00 .14 6 9 1 1 o 95.844 100.425 180.00 .09 2 16 -1 1 o 3512.003 2876.784 180.00 3.23 4 6 2 1 o 74.349 45.917 .00 .07 1 12 -2 1 o 406.402 253.760 180.00 .36 8 3 -1 1 o 279.252 248.623 180.00 .26 3 11 -2 1 o 817.253 426.854 .00 .73 5 8 -2 1 o 259.693 140.820 180.00 .23 0 12 2 1 o 114.297 76.561 180.00 .10 8 5 0 1 o 109.357 36.356 .00 .10 7 5 1 1 o 598.625 417.290 180.00 .53 4 10 -2 1 o 21.937 15.663 .00 .02 3 9 2 1 o 43.443 29.446 .00 .04 6 5 -2 1 o 1.037 .829 180.00 .00 2 12 -2 1 o 272.534 191.032 .00 .24 5 12 1 1 o 2300.278 1988.007 180.00 2.03 3 15 1 1 o 844.630 734.949 .00 .75 8 4 -1 1 o 8.676 6.304 .00 .01 7 9 -1 1 o 226.572 177.386 .00 .20 2 16 1 1 o 2190.578 1648.586 .00 1.91 7 10 0 1 o 166.560 134.909 .00 .15 4 7 2 1 o 1074.231 614.489 .00 .92 4 14 1 1 o 375.553 236.380 180.00 .33 0 18 0 1 o 104.764 71.853 180.00 .05 5 1 2 1 o 80.325 44.476 180.00 .07 4 15 -1 1 o 1.013 .791 180.00 .00 2 11 2 1 o 170.806 93.068 180.00 .15 8 6 0 1 o 1423.295 1190.569 .00 1.24 7 6 1 1 o 224.679 118.392 .00 .19 1 12 2 1 o 359.235 193.830 180.00 .30 4 16 0 1 o 52.629 31.580 180.00 .05 6 10 1 1 o 205.775 115.472 .00 .18 6 6 -2 1 o 11.124 6.185 180.00 .01 6 12 -1 1 o 24.799 14.803 180.00 .02 5 2 2 1 o 278.709 151.832 .00 .24 3 17 0 1 o .076 .048 .00 .00 3 16 -1 1 o 6.671 4.485 180.00 .01 0 17 1 1 o 405.712 237.611 180.00 .35 8 5 -1 1 o 546.727 376.334 180.00 .47 1 17 -1 1 o 52.759 29.398 .00 .05 1 18 0 1 o .957 .737 180.00 .00 5 9 -2 1 o 217.942 120.350 180.00 .19 6 13 0 1 o 203.784 116.053 .00 .17 3 12 -2 1 o 170.146 148.752 .00 .14 4 11 -2 1 o 102.168 77.623 180.00 .09 5 3 2 1 o 325.134 232.546 .00 .27 5 14 -1 1 o 541.687 292.891 180.00 .46 3 10 2 1 o 72.540 51.678 180.00 .06 1 13 -2 1 o 517.248 349.586 180.00 .43 1 17 1 1 o 755.023 614.822 180.00 .63 5 15 0 1 o 1718.715 1315.180 180.00 1.45 2 17 -1 1 o 615.991 407.630 180.00 .51 4 8 2 1 o 1986.922 1432.069 .00 1.63 7 10 -1 1 o 110.995 100.680 180.00 .09 8 7 0 1 o 3493.110 3162.286 .00 2.93 0 13 2 1 o 279.187 195.436 180.00 .23 8 6 -1 1 o .699 .647 180.00 .00 7 7 1 1 o 2304.194 1676.323 .00 1.91 5 4 2 1 o 21.016 13.123 .00 .02 2 18 0 1 o 45.169 40.733 180.00 .04 6 7 -2 1 o 743.599 502.066 .00 .61 2 13 -2 1 o 84.364 44.391 .00 .07 5 13 1 1 o 17.451 13.724 .00 .01 7 11 0 1 o 33.543 23.420 180.00 .03 7 1 -2 1 o 502.602 332.627 180.00 .41 7 2 -2 1 o .203 .100 180.00 .00 2 12 2 1 o .027 .014 180.00 .00 3 16 1 1 o 79.620 61.168 180.00 .06 6 11 1 1 o 643.698 488.138 180.00 .52 5 5 2 1 o 658.586 447.554 .00 .53 5 10 -2 1 o 1467.178 1007.339 .00 1.19 1 13 2 1 o 773.988 534.820 180.00 .61 7 3 -2 1 o 19.402 10.923 .00 .02 4 16 -1 1 o 414.980 298.821 180.00 .33 8 7 -1 1 o 115.381 83.607 180.00 .09 6 13 -1 1 o 371.451 266.595 .00 .30 4 15 1 1 o 289.335 197.629 180.00 .23 8 8 0 1 o 103.311 55.150 .00 .08 2 17 1 1 o 55.423 47.185 .00 .04 7 8 1 1 o 473.922 402.846 .00 .38 6 8 -2 1 o 1061.346 779.776 180.00 .84 4 12 -2 1 o 128.812 108.208 .00 .10 4 9 2 1 o 556.009 484.437 180.00 .43 3 11 2 1 o 706.945 633.787 .00 .56 3 13 -2 1 o 10.818 11.434 .00 .01 3 17 -1 1 o 32.486 21.027 .00 .03 6 14 0 1 o 250.000 237.319 180.00 .20 7 4 -2 1 o 49.514 45.015 .00 .04 5 6 2 1 o 229.724 128.943 .00 .18 4 17 0 1 o 152.823 97.966 180.00 .12 7 11 -1 1 o 71.005 44.535 .00 .06 5 15 -1 1 o 226.318 220.567 180.00 .18 1 14 -2 1 o 682.621 463.737 180.00 .52 3 18 0 1 o 198.924 174.964 .00 .16 0 18 1 1 o 777.188 416.357 180.00 .61 1 19 0 1 o 6.923 5.099 180.00 .01 1 18 -1 1 o 7.756 4.116 180.00 .01 8 1 1 1 o 256.542 141.745 .00 .20 5 11 -2 1 o 112.320 63.691 180.00 .09 7 12 0 1 o 214.417 179.238 .00 .17 0 14 2 1 o 67.258 36.116 .00 .05 8 2 1 1 o 2.373 1.661 180.00 .00 8 8 -1 1 o 1.035 .535 .00 .00 7 5 -2 1 o 339.012 221.426 180.00 .26 6 9 -2 1 o 759.036 526.082 .00 .58 5 16 0 1 o 6.424 3.691 .00 .00 2 14 -2 1 o 872.903 625.724 .00 .66 9 1 0 1 o 2.417 1.508 .00 .00 5 14 1 1 o 231.262 122.693 .00 .18 8 9 0 1 o 11.023 8.000 180.00 .01 6 12 1 1 o 163.454 100.564 .00 .12 7 9 1 1 o 756.518 499.829 180.00 .58 1 18 1 1 o 6.630 4.527 .00 .00 9 2 0 1 o 32.856 21.553 .00 .03 8 3 1 1 o 511.552 345.681 .00 .39 5 7 2 1 o 1365.733 1059.792 .00 1.02 2 13 2 1 o 528.199 383.047 180.00 .40 2 18 -1 1 o 45.911 34.372 .00 .03 4 10 2 1 o 275.450 225.899 .00 .21 9 3 0 1 o 724.697 516.802 180.00 .55 2 19 0 1 o 83.099 59.589 .00 .06 9 0 -1 1 o 43.750 32.118 .00 .02 9 1 -1 1 o 6.173 8.615 180.00 .00 1 14 2 1 o 1082.624 810.997 180.00 .80 3 12 2 1 o .445 .323 180.00 .00 7 6 -2 1 o 21.532 17.162 .00 .02 8 4 1 1 o 262.873 218.701 .00 .20 6 14 -1 1 o 270.519 217.009 .00 .20 4 13 -2 1 o .138 .119 .00 .00 3 17 1 1 o 29.883 30.380 .00 .02 9 2 -1 1 o 1673.447 1207.606 180.00 1.25 6 0 2 1 o 8.302 7.805 180.00 .00 6 1 2 1 o 55.848 50.829 180.00 .04 1 0 -3 1 o 8.086 9.263 .00 .00 7 12 -1 1 o 61.543 53.494 180.00 .05 3 14 -2 1 o 76.183 69.883 .00 .06 1 1 -3 1 o 275.513 285.145 180.00 .20 9 4 0 1 o 214.559 182.346 180.00 .16 4 16 1 1 o 58.137 43.222 .00 .04 8 9 -1 1 o 306.906 339.641 180.00 .23 4 17 -1 1 o 789.917 749.085 .00 .58 2 1 -3 1 o 29.199 24.560 180.00 .02 6 2 2 1 o 81.608 77.994 .00 .06 9 3 -1 1 o 931.222 849.741 180.00 .69 1 2 -3 1 o 279.270 232.144 .00 .20 6 10 -2 1 o 70.971 84.791 .00 .05 7 7 -2 1 o 332.641 420.840 180.00 .24 6 15 0 1 o 70.487 44.109 180.00 .05 5 8 2 1 o 907.689 1115.098 .00 .66 8 5 1 1 o 154.426 140.848 .00 .11 2 2 -3 1 o 397.864 335.886 180.00 .28 5 12 -2 1 o 20.278 21.985 .00 .01 2 18 1 1 o 11.387 11.184 .00 .01 5 16 -1 1 o 225.030 216.694 .00 .16 8 10 0 1 o 303.454 294.202 180.00 .22 6 3 2 1 o 47.604 39.754 .00 .03 7 10 1 1 o 1121.985 1098.587 180.00 .81 7 13 0 1 o 266.819 245.728 .00 .20 0 1 3 1 o 2.788 2.598 .00 .00 1 15 -2 1 o 61.315 51.794 180.00 .04 1 3 -3 1 o 365.499 334.761 .00 .26 3 18 -1 1 o 1212.407 1486.703 180.00 .87 9 5 0 1 o 1403.426 1353.344 180.00 1.02 9 4 -1 1 o 623.452 616.390 .00 .45 2 3 -3 1 o 27.276 25.497 .00 .02 0 2 3 1 o .189 .193 180.00 .00 0 15 2 1 o 925.595 800.029 .00 .66 4 18 0 1 o 79.596 98.594 180.00 .06 3 0 -3 1 o 199.694 230.662 180.00 .07 4 11 2 1 o .581 .534 180.00 .00 6 13 1 1 o 522.350 439.842 .00 .37 3 1 -3 1 o 18.235 19.836 180.00 .01 2 15 -2 1 o 226.218 203.504 180.00 .16 6 4 2 1 o 1095.819 954.410 180.00 .78 5 15 1 1 o 203.514 169.444 .00 .15 0 20 0 1 o 390.909 416.024 .00 .14 1 4 -3 1 o 354.372 388.224 .00 .25 0 3 3 1 o 134.335 149.408 .00 .09 8 6 1 1 o 107.405 88.892 180.00 .08 3 2 -3 1 o 28.977 33.642 .00 .02 8 1 -2 1 o 46.406 53.541 .00 .03 2 14 2 1 o 244.553 280.892 180.00 .17 3 19 0 1 o 397.700 337.227 180.00 .29 0 19 1 1 o 172.656 162.770 180.00 .12 2 4 -3 1 o 55.400 63.190 180.00 .04 1 19 -1 1 o 104.511 99.632 .00 .07 5 17 0 1 o 161.826 117.448 .00 .12 7 8 -2 1 o 212.067 222.855 180.00 .15 9 5 -1 1 o 739.866 644.623 .00 .53 1 20 0 1 o 49.167 41.432 .00 .04 8 2 -2 1 o 54.519 59.376 .00 .04 8 0 -2 1 o 265.575 249.872 .00 .09 3 13 2 1 o 327.183 354.646 .00 .23 8 10 -1 1 o 34.290 31.420 .00 .02 9 6 0 1 o .595 .555 180.00 .00 3 3 -3 1 o 76.124 89.679 .00 .05 7 13 -1 1 o 1336.500 1561.893 .00 .94 5 9 2 1 o 1504.873 1707.642 180.00 1.05 6 15 -1 1 o 12.290 15.422 180.00 .01 0 4 3 1 o 6.259 7.923 180.00 .00 1 0 3 1 o 58.466 81.865 180.00 .02 6 5 2 1 o 24.955 27.230 180.00 .02 1 1 3 1 o 1.673 3.308 180.00 .00 4 14 -2 1 o 779.997 858.019 .00 .54 1 15 2 1 o 191.699 211.213 .00 .13 1 5 -3 1 o 57.694 142.181 180.00 .04 6 11 -2 1 o 893.139 996.299 180.00 .62 8 3 -2 1 o 1411.855 1574.684 180.00 .97 1 19 1 1 o 214.663 233.708 180.00 .15 2 5 -3 1 o 39.726 69.679 .00 .03 1 2 3 1 o 94.870 132.457 .00 .06 2 19 -1 1 o 327.648 351.429 .00 .22 3 4 -3 1 o 329.263 337.207 180.00 .22 8 11 0 1 o 25.398 27.260 .00 .02 7 11 1 1 o 1214.009 1314.065 180.00 .84 8 7 1 1 o 385.150 425.933 .00 .27 3 15 -2 1 o 177.279 319.193 180.00 .12 5 13 -2 1 o 95.182 395.294 180.00 .07 9 6 -1 1 o 72.619 90.087 .00 .05 0 5 3 1 o 4.664 5.220 .00 .00 8 4 -2 1 o 160.128 274.450 180.00 .11 1 3 3 1 o 1.610 1.729 .00 .00 3 18 1 1 o 363.012 488.896 180.00 .25 4 1 -3 1 o 3.525 3.435 .00 .00 2 20 0 1 o .064 .074 .00 .00 9 7 0 1 o 669.736 718.420 .00 .46 4 17 1 1 o .042 .079 180.00 .00 6 6 2 1 o 4.330 4.422 .00 .00 7 14 0 1 o 920.964 1063.056 180.00 .63 1 6 -3 1 o 347.642 326.053 .00 .23 4 12 2 1 o 267.554 279.185 180.00 .18 6 16 0 1 o 243.508 285.275 .00 .17 7 9 -2 1 o 590.463 608.730 180.00 .40 4 2 -3 1 o 223.607 203.435 180.00 .15 3 5 -3 1 o 123.690 117.038 .00 .08 2 6 -3 1 o 567.455 537.208 .00 .38 4 18 -1 1 o 227.846 309.090 .00 .15 8 11 -1 1 o 129.181 141.149 180.00 .09 1 4 3 1 o 1105.441 1111.766 180.00 .73 1 16 -2 1 o 459.563 453.071 180.00 .31 5 17 -1 1 o 50.484 54.740 .00 .03 6 14 1 1 o 2089.559 2139.166 180.00 1.41 5 10 2 1 o 1611.243 1522.898 .00 1.07 8 5 -2 1 o 316.139 294.860 .00 .21 4 3 -3 1 o 39.804 46.682 180.00 .03 0 6 3 1 o .840 1.114 .00 .00 0 16 2 1 o 532.800 504.148 180.00 .35 2 19 1 1 o 30.524 29.099 180.00 .02 9 7 -1 1 o 408.284 444.143 180.00 .28 8 8 1 1 o 1381.827 1374.339 .00 .92 2 16 -2 1 o 37.845 41.550 180.00 .02 2 15 2 1 o 16.550 18.975 180.00 .01 5 16 1 1 o 367.064 326.520 180.00 .24 3 19 -1 1 o 1953.758 1678.541 180.00 1.29 6 7 2 1 o .187 .228 .00 .00 3 14 2 1 o 488.069 596.198 180.00 .32 6 12 -2 1 o 231.950 288.607 180.00 .15 1 5 3 1 o 346.500 408.703 .00 .22 3 6 -3 1 o 3.052 3.539 180.00 .00 4 4 -3 1 o .058 .068 180.00 .00 1 7 -3 1 o 1404.609 1633.357 180.00 .90 7 14 -1 1 o 148.364 136.766 180.00 .10 9 8 0 1 o 674.799 627.024 .00 .45 4 19 0 1 o 9.359 8.651 .00 .01 2 1 3 1 o 114.899 143.232 180.00 .08 2 7 -3 1 o 160.515 209.189 180.00 .10 8 12 0 1 o 56.396 53.492 .00 .04 8 6 -2 1 o 285.726 352.568 180.00 .18 7 12 1 1 o 901.155 1040.387 .00 .59 2 2 3 1 o 42.966 56.168 .00 .03 6 16 -1 1 o 1085.750 1464.230 .00 .71 4 15 -2 1 o 167.168 200.950 .00 .11 5 18 0 1 o 3.761 3.526 .00 .00 7 10 -2 1 o .020 .027 .00 .00 1 16 2 1 o 94.937 121.287 180.00 .06 0 7 3 1 o 11.194 12.825 180.00 .01 0 20 1 1 o 269.866 326.698 180.00 .18 3 20 0 1 o 112.005 133.828 180.00 .07 1 20 -1 1 o 1.264 1.643 180.00 .00 4 5 -3 1 o 914.581 1006.342 180.00 .58 5 14 -2 1 o 23.894 30.948 180.00 .01 2 3 3 1 o 56.472 59.879 .00 .04 9 8 -1 1 o 3.953 6.438 .00 .00 1 6 3 1 o 13.629 13.315 .00 .01 3 16 -2 1 o 3462.925 3965.680 180.00 2.20 4 13 2 1 o 525.895 599.269 180.00 .33 8 12 -1 1 o 20.952 29.220 180.00 .01 3 7 -3 1 o 133.490 136.401 .00 .08 1 21 0 1 o 3549.130 4560.832 .00 2.30 8 9 1 1 o 367.123 489.135 .00 .24 5 0 -3 1 o 2503.719 2584.500 180.00 .79 5 11 2 1 o 13.388 15.638 .00 .01 9 0 1 1 o 760.076 979.140 .00 .24 5 1 -3 1 o 8.361 8.593 180.00 .01 6 8 2 1 o 468.476 534.395 180.00 .30 9 1 1 1 o 83.350 112.707 180.00 .05 1 8 -3 1 o 123.682 123.306 .00 .08 7 15 0 1 o 871.483 1131.782 .00 .56 2 4 3 1 o 376.237 364.115 180.00 .23 8 7 -2 1 o 183.051 176.892 180.00 .12 1 20 1 1 o 69.611 79.053 .00 .04 2 8 -3 1 o 1148.607 1145.808 .00 .72 5 2 -3 1 o 4.127 4.232 180.00 .00 9 2 1 1 o 98.869 111.684 .00 .06 9 9 0 1 o 20.980 26.818 .00 .01 7 1 2 1 o 151.921 155.705 180.00 .10 2 20 -1 1 o 220.559 268.611 .00 .14 4 6 -3 1 o 36.140 48.814 .00 .02 6 17 0 1 o 420.935 475.540 180.00 .27 4 18 1 1 o 25.911 24.448 180.00 .02 6 15 1 1 o 82.536 78.829 .00 .05 7 2 2 1 o 43.483 41.318 180.00 .03 5 3 -3 1 o 387.450 477.651 .00 .24 3 19 1 1 o 754.804 731.586 .00 .48 0 8 3 1 o 192.314 234.788 .00 .12 9 3 1 1 o 930.863 913.868 .00 .59 9 9 -1 1 o 23.456 23.976 .00 .01 1 7 3 1 o 44.651 52.706 180.00 .03 10 0 0 1 o 92.126 98.971 180.00 .03 1 17 -2 1 o 501.015 580.108 180.00 .31 6 13 -2 1 o 82.876 101.783 .00 .05 10 1 0 1 o 81.131 73.933 180.00 .05 2 5 3 1 o 332.177 391.105 180.00 .20 10 1 -1 1 o 290.299 266.758 .00 .18 7 3 2 1 o 26.293 35.449 180.00 .02 4 19 -1 1 o 94.384 86.971 180.00 .06 5 18 -1 1 o 419.647 384.693 .00 .26 2 21 0 1 o 483.425 462.095 .00 .31 0 17 2 1 o 3.259 4.132 .00 .00 3 8 -3 1 o .063 .070 180.00 .00 7 11 -2 1 o 18.736 22.654 .00 .01 10 2 0 1 o 403.638 419.407 180.00 .26 3 15 2 1 o 138.021 163.594 .00 .09 2 16 2 1 o 258.098 301.690 180.00 .16 8 13 0 1 o .141 .146 .00 .00 7 13 1 1 o 1883.775 2022.807 180.00 1.17 5 4 -3 1 o 410.314 458.060 180.00 .25 10 2 -1 1 o 152.126 181.596 180.00 .09 7 15 -1 1 o 286.265 345.210 180.00 .18 9 4 1 1 o 44.750 57.150 180.00 .03 2 17 -2 1 o 105.870 127.877 .00 .06 5 17 1 1 o 164.421 231.971 .00 .10 6 9 2 1 o 591.522 677.833 .00 .36 8 8 -2 1 o 71.902 80.228 .00 .04 1 9 -3 1 o 16.235 23.091 180.00 .01 8 10 1 1 o 277.861 367.861 .00 .17 4 7 -3 1 o 14.415 20.935 .00 .01 10 3 0 1 o 20.051 21.063 .00 .01 7 4 2 1 o 15.587 16.685 180.00 .01 2 9 -3 1 o .439 .621 180.00 .00 10 3 -1 1 o 1284.839 1500.518 180.00 .79 2 20 1 1 o 177.389 211.183 .00 .11 3 0 3 1 o 31.091 40.098 .00 .01 3 1 3 1 o 501.852 592.619 .00 .30 4 16 -2 1 o 32.482 45.433 180.00 .02 2 6 3 1 o 1026.968 1219.207 .00 .61 5 12 2 1 o 28.778 40.402 .00 .02 9 10 0 1 o 67.506 79.744 .00 .04 3 20 -1 1 o 185.236 196.501 .00 .11 8 13 -1 1 o 17.670 18.598 .00 .01 6 17 -1 1 o 598.292 631.823 180.00 .36 5 5 -3 1 o 33.388 43.346 .00 .02 5 15 -2 1 o 375.774 558.912 .00 .23 9 1 -2 1 o 185.395 277.359 .00 .11 1 8 3 1 o 75.047 93.296 180.00 .04 9 5 1 1 o 466.426 493.232 180.00 .28 3 2 3 1 o .018 .022 .00 .00 0 9 3 1 o .387 .444 .00 .00 4 14 2 1 o 142.120 205.833 .00 .09 1 17 2 1 o 75.504 106.182 180.00 .05 10 4 0 1 o 149.778 184.344 180.00 .09 4 20 0 1 o 841.149 969.846 .00 .51 9 2 -2 1 o 4.979 5.633 .00 .00 10 4 -1 1 o 1399.389 2065.190 180.00 .85 7 5 2 1 o 50.131 60.424 180.00 .03 9 10 -1 1 o 296.031 418.855 180.00 .18 5 19 0 1 o 366.639 402.275 180.00 .22 3 3 3 1 o 1.295 1.574 .00 .00 3 9 -3 1 o 1153.394 1322.109 180.00 .68 3 17 -2 1 o 1.330 1.533 .00 .00 9 3 -2 1 o 1165.965 1319.174 .00 .69 7 16 0 1 o 17.149 26.501 .00 .01 4 8 -3 1 o 156.928 197.155 180.00 .09 8 9 -2 1 o 23.664 30.163 180.00 .01 5 6 -3 1 o 4.998 5.933 180.00 .00 2 7 3 1 o 10.625 12.681 180.00 .01 10 5 0 1 o 8.852 12.838 .00 .01 0 21 1 1 o 235.871 297.867 .00 .14 9 6 1 1 o 34.490 40.381 .00 .02 3 21 0 1 o 317.295 483.652 180.00 .19 1 21 -1 1 o 270.038 300.284 180.00 .16 6 10 2 1 o 129.677 144.730 .00 .08 10 5 -1 1 o 90.025 100.865 180.00 .05 3 4 3 1 o 441.142 475.103 180.00 .26 1 10 -3 1 o 762.124 816.259 .00 .44 7 12 -2 1 o 120.081 143.392 180.00 .07 6 14 -2 1 o 50.388 76.602 180.00 .03 0 22 0 1 o 727.343 869.136 180.00 .22 6 1 -3 1 o 113.248 130.481 .00 .07 6 16 1 1 o 266.271 316.423 180.00 .16 2 10 -3 1 o 244.664 278.298 180.00 .14 8 11 1 1 o 63.719 77.850 180.00 .04 9 4 -2 1 o 71.679 94.403 180.00 .04 7 6 2 1 o 3.741 4.660 180.00 .00 6 2 -3 1 o 423.823 540.175 180.00 .24 1 9 3 1 o 123.427 158.569 .00 .07 7 14 1 1 o 56.618 61.266 180.00 .03 8 14 0 1 o 414.718 451.728 .00 .25 6 18 0 1 o 233.657 250.613 180.00 .14 1 22 0 1 o 41.918 44.931 .00 .03 1 21 1 1 o 31.092 46.674 180.00 .02 0 10 3 1 o 3.769 5.415 .00 .00 4 19 1 1 o 11.104 14.705 .00 .01 9 11 0 1 o 93.802 125.314 180.00 .06 1 18 -2 1 o 194.573 217.421 180.00 .11 3 16 2 1 o 406.341 461.075 180.00 .24 3 5 3 1 o .931 1.071 .00 .00 2 21 -1 1 o 841.966 1027.137 .00 .49 10 6 0 1 o 793.912 825.435 180.00 .47 6 3 -3 1 o 34.329 35.743 180.00 .02 7 16 -1 1 o 3.353 3.892 .00 .00 5 13 2 1 o 264.216 337.743 .00 .15 3 20 1 1 o 50.088 52.947 .00 .03 10 6 -1 1 o 248.919 263.044 .00 .14 2 17 2 1 o 254.357 333.051 .00 .15 5 7 -3 1 o 27.371 23.681 .00 .02 9 5 -2 1 o 252.669 344.127 .00 .15 0 18 2 1 o 21.118 28.927 180.00 .01 9 7 1 1 o 6.766 7.886 .00 .00 3 10 -3 1 o 819.280 741.127 .00 .46 9 11 -1 1 o 15.400 16.949 .00 .01 5 19 -1 1 o 294.243 315.676 .00 .17 2 8 3 1 o 423.429 388.670 .00 .24 4 9 -3 1 o 32.042 31.383 .00 .02 2 18 -2 1 o 11.703 14.672 .00 .01 8 14 -1 1 o 341.648 421.168 .00 .20 4 20 -1 1 o 625.200 785.125 180.00 .36 5 18 1 1 o 645.875 831.183 180.00 .37 7 7 2 1 o 192.365 177.224 180.00 .11 6 4 -3 1 o 76.993 109.641 .00 .04 8 10 -2 1 o 82.476 65.923 .00 .05 4 15 2 1 o 23.543 21.109 .00 .01 4 17 -2 1 o 25.311 22.802 180.00 .01 5 16 -2 1 o 236.735 210.836 .00 .13 2 22 0 1 o 362.275 453.512 .00 .21 3 6 3 1 o 74.199 89.811 180.00 .04 6 11 2 1 o 1224.732 1353.118 180.00 .69 1 11 -3 1 o 1.271 1.658 .00 .00 6 18 -1 1 o 68.773 60.291 .00 .04 9 6 -2 1 o 33.733 53.204 .00 .02 10 7 0 1 o 112.211 164.501 180.00 .06 2 11 -3 1 o 868.474 984.774 .00 .48 1 10 3 1 o 128.323 143.053 .00 .07 10 7 -1 1 o .445 .382 180.00 .00 1 18 2 1 o 21.276 21.929 180.00 .01 2 21 1 1 o 222.869 208.151 180.00 .13 7 13 -2 1 o 9.591 10.207 180.00 .01 6 5 -3 1 o 25.949 26.166 180.00 .01 8 12 1 1 o 26.977 29.281 180.00 .01 5 8 -3 1 o 733.603 731.152 180.00 .41 9 8 1 1 o 14.767 20.311 180.00 .01 3 21 -1 1 o 40.687 66.084 .00 .02 0 11 3 1 o 339.535 404.057 .00 .19 4 1 3 1 o 8.579 9.982 180.00 .00 3 18 -2 1 o 395.219 433.939 .00 .22 6 15 -2 1 o 402.958 452.870 180.00 .22 7 17 0 1 o 94.584 102.704 180.00 .05 2 9 3 1 o 136.505 156.996 180.00 .08 7 8 2 1 o 628.909 666.045 .00 .35 9 12 0 1 o 8.292 10.195 .00 .00 4 21 0 1 o 4.503 5.639 .00 .00 5 20 0 1 o 76.772 98.311 180.00 .04 4 2 3 1 o 206.049 238.371 180.00 .11 3 7 3 1 o 1044.546 1114.014 180.00 .57 4 10 -3 1 o .101 .109 180.00 .00 10 8 0 1 o 183.295 215.944 .00 .10 3 11 -3 1 o 1317.326 1343.630 .00 .72 7 15 1 1 o 99.804 108.901 .00 .06 8 15 0 1 o 561.082 484.889 .00 .32 6 17 1 1 o 277.688 310.533 180.00 .15 9 7 -2 1 o 16.903 17.718 .00 .01 9 12 -1 1 o 1.666 1.738 180.00 .00 6 6 -3 1 o .300 .406 180.00 .00 4 3 3 1 o .303 .400 180.00 .00 5 14 2 1 o 55.063 64.734 180.00 .03 8 11 -2 1 o 42.624 49.418 .00 .02 10 8 -1 1 o .000 .000 .00 .00 9 9 1 1 o 13.531 13.964 .00 .01 3 17 2 1 o 244.710 280.458 180.00 .13 0 22 1 1 o 293.194 379.060 180.00 .16 3 22 0 1 o 277.514 266.274 180.00 .15 1 22 -1 1 o 97.035 117.525 .00 .05 6 19 0 1 o 227.942 253.381 .00 .13 7 17 -1 1 o 137.650 162.595 180.00 .07 5 9 -3 1 o .411 .425 180.00 .00 8 0 2 1 o 17.452 25.155 .00 .00 8 15 -1 1 o 30.645 35.290 180.00 .02 4 4 3 1 o 18.297 19.326 .00 .01 6 12 2 1 o 302.618 422.731 180.00 .17 1 12 -3 1 o 2.224 2.372 180.00 .00 8 1 2 1 o 569.730 687.580 .00 .31 1 11 3 1 o 36.950 39.174 180.00 .02 1 19 -2 1 o 34.987 37.715 .00 .02 2 12 -3 1 o 363.419 368.173 .00 .19 2 18 2 1 o 36.688 37.339 180.00 .02 4 20 1 1 o 500.986 555.981 .00 .27 8 2 2 1 o 7.541 6.446 .00 .00 3 8 3 1 o 10.722 9.526 180.00 .01 7 9 2 1 o .983 .882 180.00 .00 7 0 -3 1 o 291.469 257.122 .00 .08 4 16 2 1 o 3.774 3.668 .00 .00 0 19 2 1 o 154.261 155.099 180.00 .08 7 1 -3 1 o 7.059 6.004 .00 .00 2 10 3 1 o 270.697 228.585 .00 .14 6 7 -3 1 o 403.139 337.225 .00 .21 10 1 1 1 o 160.000 174.827 180.00 .09 10 9 0 1 o 24.587 28.211 .00 .01 1 22 1 1 o 172.346 195.233 .00 .09 9 8 -2 1 o 36.003 38.973 180.00 .02 8 13 1 1 o .392 .442 .00 .00 1 23 0 1 o 15.150 15.903 180.00 .01 0 12 3 1 o 13.525 11.402 180.00 .01 2 19 -2 1 o 73.289 77.144 180.00 .04 5 17 -2 1 o 88.250 91.947 180.00 .05 9 13 0 1 o 52.751 50.480 .00 .03 7 2 -3 1 o 264.391 230.705 .00 .14 3 21 1 1 o 26.334 24.040 180.00 .01 8 3 2 1 o 67.575 67.000 .00 .04 7 14 -2 1 o 6.854 6.809 180.00 .00 2 22 -1 1 o 28.289 22.611 .00 .02 5 20 -1 1 o 200.674 158.342 .00 .11 4 5 3 1 o 507.006 475.133 .00 .27 10 2 1 1 o 67.409 65.775 .00 .04 5 19 1 1 o 4.257 3.517 .00 .00 4 18 -2 1 o 621.303 573.855 180.00 .33 4 11 -3 1 o 87.590 79.427 .00 .05 10 9 -1 1 o 529.520 581.257 .00 .28 4 21 -1 1 o 753.410 819.783 .00 .40 3 12 -3 1 o 2.980 2.446 180.00 .00 7 3 -3 1 o 77.868 65.578 180.00 .04 10 3 1 1 o 35.085 30.188 .00 .02 9 10 1 1 o 949.704 817.165 .00 .50 8 4 2 1 o 101.808 107.283 180.00 .05 6 19 -1 1 o 2.153 1.834 .00 .00 6 16 -2 1 o 408.928 294.505 180.00 .21 8 12 -2 1 o 66.307 47.468 180.00 .03 9 13 -1 1 o 11.895 9.541 180.00 .01 1 19 2 1 o 73.220 55.800 180.00 .04 5 10 -3 1 o 7.453 9.766 180.00 .00 4 6 3 1 o 247.593 268.689 180.00 .13 7 4 -3 1 o 18.492 19.733 .00 .01 6 8 -3 1 o 36.792 39.122 180.00 .02 10 4 1 1 o 7.954 7.976 180.00 .00 3 9 3 1 o 43.743 46.429 .00 .02 2 23 0 1 o 957.720 778.537 .00 .51 7 18 0 1 o 8.598 7.201 180.00 .00 7 16 1 1 o 1.130 .984 180.00 .00 10 0 -2 1 o 86.920 110.219 180.00 .02 8 16 0 1 o 363.678 300.691 180.00 .19 3 19 -2 1 o 43.613 62.697 .00 .02 11 1 0 1 o 145.146 97.902 180.00 .08 10 1 -2 1 o 767.499 1125.516 180.00 .40 5 15 2 1 o 11.568 16.730 .00 .01 7 10 2 1 o 6.071 8.661 .00 .00 11 0 -1 1 o 205.428 158.236 .00 .05 1 12 3 1 o 42.713 38.814 180.00 .02 9 9 -2 1 o 5.206 7.332 180.00 .00 11 1 -1 1 o 1.979 1.475 .00 .00 2 22 1 1 o 662.568 525.617 180.00 .35 8 5 2 1 o 79.655 104.679 180.00 .04 6 13 2 1 o 165.315 204.848 180.00 .09 1 13 -3 1 o 1.499 1.198 .00 .00 11 2 0 1 o 269.415 257.749 .00 .14 10 2 -2 1 o 7.686 8.495 .00 .00 10 10 0 1 o 460.255 437.153 180.00 .24 2 11 3 1 o 114.832 84.405 180.00 .06 6 18 1 1 o 54.960 55.309 180.00 .03 2 13 -3 1 o 69.090 47.864 .00 .04 11 2 -1 1 o 17.800 26.239 .00 .01 3 22 -1 1 o 47.484 70.166 180.00 .03 8 14 1 1 o 147.090 155.192 180.00 .08 5 21 0 1 o 234.193 175.727 .00 .12 7 5 -3 1 o 18.450 8.714 .00 .01 10 5 1 1 o 492.020 465.536 .00 .25 11 3 0 1 o 73.043 84.741 180.00 .04 10 3 -2 1 o 73.309 55.190 180.00 .04 8 16 -1 1 o 292.515 323.698 180.00 .15 4 22 0 1 o 61.837 57.728 .00 .03 10 10 -1 1 o 292.759 310.143 180.00 .15 0 13 3 1 o 23.398 17.053 .00 .01 11 3 -1 1 o 66.815 72.984 .00 .03 4 7 3 1 o 1.031 .789 180.00 .00 4 12 -3 1 o 307.004 238.142 .00 .15 3 18 2 1 o 170.258 117.225 180.00 .09 7 18 -1 1 o 506.199 522.746 .00 .26 9 14 0 1 o 41.967 45.728 180.00 .02 9 11 1 1 o 12.080 5.328 180.00 .01 8 6 2 1 o 2.722 1.117 .00 .00 5 0 3 1 o 1.298 1.041 .00 .00 6 9 -3 1 o 86.703 69.363 .00 .04 7 15 -2 1 o 64.521 41.797 180.00 .03 5 1 3 1 o 148.431 119.281 .00 .08 10 4 -2 1 o 10.370 6.740 180.00 .01 11 4 0 1 o 6.993 5.403 .00 .00 4 17 2 1 o 2.505 1.666 180.00 .00 3 13 -3 1 o 76.402 61.910 180.00 .04 6 20 0 1 o 2.692 3.142 180.00 .00 5 11 -3 1 o 251.816 212.891 180.00 .13 2 19 2 1 o 26.154 20.407 180.00 .01 11 4 -1 1 o 204.013 155.191 .00 .11 3 10 3 1 o 64.293 55.451 180.00 .03 7 6 -3 1 o 28.530 24.647 .00 .01 5 2 3 1 o 310.972 263.951 .00 .16 1 20 -2 1 o 110.594 92.187 180.00 .06 10 6 1 1 o 40.196 33.817 .00 .02 8 13 -2 1 o 47.026 41.324 180.00 .02 8 7 2 1 o .253 .249 180.00 .00 5 18 -2 1 o 9.286 7.335 .00 .00 9 10 -2 1 o 44.780 35.451 180.00 .02 0 23 1 1 o 209.206 139.621 180.00 .11 1 23 -1 1 o 15.979 12.567 .00 .01 3 23 0 1 o 47.938 38.365 .00 .02 7 11 2 1 o 230.669 187.092 180.00 .12 0 20 2 1 o 323.708 262.703 180.00 .16 4 21 1 1 o 5.096 4.010 180.00 .00 9 14 -1 1 o 47.674 37.417 .00 .02 4 19 -2 1 o 17.940 15.740 .00 .01 2 20 -2 1 o 142.354 124.573 .00 .07 10 5 -2 1 o 111.278 97.824 .00 .06 11 5 0 1 o 1000.701 869.144 .00 .50 10 11 0 1 o 198.691 175.418 180.00 .10 5 20 1 1 o 9.149 7.205 .00 .00 11 5 -1 1 o .648 .503 180.00 .00 5 21 -1 1 o 64.897 53.090 .00 .03 0 24 0 1 o .947 .873 180.00 .00 8 17 0 1 o 864.656 720.843 .00 .43 3 22 1 1 o 474.933 414.092 .00 .24 1 23 1 1 o 145.447 131.029 .00 .07 10 11 -1 1 o 34.493 29.726 180.00 .02 2 23 -1 1 o 122.564 108.039 .00 .06 7 19 0 1 o 1.431 1.892 180.00 .00 1 24 0 1 o 13.543 11.173 180.00 .01 _reflns_number_observed 1059 _reflns_limit_h_min 0 _reflns_limit_h_max 11 _reflns_limit_k_min 0 _reflns_limit_k_max 24 _reflns_limit_l_min -3 _reflns_limit_l_max 3 _reflns_d_resolution_high .967 _reflns_d_resolution_low 11.690