Crystallography Open Database

Information card for entry 4303845

Preview

Coordinates	4303845.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H42 Cl I N4 U
Calculated formula	C26 H42 Cl I N4 U
SMILES	[U]1(I)(Cl)(=NC(C)(C)C)(=NC(C)(C)C)[n]2ccc(cc2c2[n]1ccc(c2)C(C)(C)C)C(C)(C)C
Title of publication	Oxidative Addition to U(V)-U(V) Dimers: Facile Routes to Uranium(VI) Bis(imido) Complexes
Authors of publication	Liam P. Spencer; Ping Yang; Brian L. Scott; Enrique R. Batista; James M. Boncella
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	11615 - 11623
a	19.096 ± 0.008 Å
b	14.268 ± 0.006 Å
c	22.477 ± 0.009 Å
α	90°
β	95.921 ± 0.005°
γ	90°
Cell volume	6091 ± 4 Å³
Cell temperature	120 ± 1 K
Ambient diffraction temperature	120 ± 1 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0718
Residual factor for significantly intense reflections	0.0474
Weighted residual factors for significantly intense reflections	0.1118
Weighted residual factors for all reflections included in the refinement	0.1216
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179076 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/38.	4303845.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303845.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303845.cif
1125	2010-04-25	cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition.	4303845.cif