Crystallography Open Database

Information card for entry 4303952

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Coordinates	4303952.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	bis(2,2'-bis(diphenylphosphino)-1,1'-biphenyl)palladium(0) tri(benzene)solvate
Formula	C90 H74 P4 Pd
Calculated formula	C90 P4 Pd
Title of publication	Strongly Luminescent Palladium(0) and Platinum(0) Diphosphine Complexes
Authors of publication	Taro Tsubomura; Yasuhiro Ito; Satoshi Inoue; Yu Tanaka; Kenji Matsumoto; Toshiaki Tsukuda
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	481 - 486
a	12.055 ± 0.002 Å
b	12.061 ± 0.003 Å
c	26.226 ± 0.007 Å
α	93.01 ± 0.02°
β	92.877 ± 0.019°
γ	107.417 ± 0.014°
Cell volume	3624.6 ± 1.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1979
Residual factor for significantly intense reflections	0.1174
Weighted residual factors for significantly intense reflections	0.3124
Weighted residual factors for all reflections included in the refinement	0.3626
Goodness-of-fit parameter for all reflections included in the refinement	1.191
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179077 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/39.	4303952.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303952.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303952.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4303952.cif