Crystallography Open Database

Information card for entry 4306626

Preview

Coordinates	4306626.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H126 Ga7 N7 Ni2
Calculated formula	C63 H125.333 Ga7 N7 Ni2
Title of publication	2,2,6,6-Tetramethylpiperidinogallium as a Terminal and Bridging Ligand in Homo- and Heteroleptic Chromium, Nickel, and Cobalt Complexes
Authors of publication	Annekathrin Seifert; Gerald Linti
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11398 - 11404
a	61.281 ± 0.006 Å
b	13.164 ± 0.002 Å
c	31.559 ± 0.004 Å
α	90°
β	116.24 ± 0.03°
γ	90°
Cell volume	22835 ± 8 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0849
Residual factor for significantly intense reflections	0.049
Weighted residual factors for significantly intense reflections	0.1109
Weighted residual factors for all reflections included in the refinement	0.1233
Goodness-of-fit parameter for all reflections included in the refinement	0.842
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179104 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/66.	4306626.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306626.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306626.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306626.cif