Crystallography Open Database

Information card for entry 4310862

Preview

Coordinates	4310862.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H39 N4 Ni2 O11.7 Pb
Calculated formula	C38 H39 N4 Ni2 O11.806 Pb
Title of publication	Toward Rational Control of Metal Stoichiometry in Heterobimetallic Coordination Complexes: Synthesis and Characterization of Pb(Hsal)2(Cu(salen))2, [Pb(NO3)(Cu(salen))2](NO3), Pb(OAc)2(Cu(salen)), and [Pb(OAc)(Ni(salen))2](OAc)
Authors of publication	John H. Thurston; Christopher G.-Z. Tang; Daniel W. Trahan; Kenton H. Whitmire
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	2708 - 2713
a	18.688 ± 0.004 Å
b	26.355 ± 0.005 Å
c	13.377 ± 0.003 Å
α	90°
β	133.01 ± 0.03°
γ	90°
Cell volume	4818 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0758
Residual factor for significantly intense reflections	0.0533
Weighted residual factors for significantly intense reflections	0.1626
Weighted residual factors for all reflections included in the refinement	0.1769
Goodness-of-fit parameter for all reflections included in the refinement	1.139
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4310862.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310862.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310862.cif
2354	2010-11-10	../uploads/cif-deposit/cod/cif Adding structures of 4310862 via cif-deposit CGI script.	4310862.cif