Crystallography Open Database

Information card for entry 4312000

4311999 << 4312000 >> 4312001

Preview

Coordinates	4312000.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Ar'*Pb(p-t-BuPhenyl)0.25n-hexane
Formula	C41.5 H53.5 Pb
Calculated formula	C41.5 H53.5 Pb
Title of publication	Terphenyl Ligand Stabilized Lead(II) Derivatives: Steric Effects and Lead-Lead Bonding in Diplumbenes
Authors of publication	Shirley Hino; Marilyn Olmstead; Andrew D. Phillips; Robert J. Wright; Philip P. Power
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	7346 - 7352
a	13.477 ± 0.003 Å
b	16.148 ± 0.003 Å
c	19.017 ± 0.004 Å
α	105.856 ± 0.003°
β	106.89 ± 0.003°
γ	101.503 ± 0.003°
Cell volume	3630.5 ± 1.3 Å³
Cell temperature	86 ± 2 K
Ambient diffraction temperature	86 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0627
Residual factor for significantly intense reflections	0.0385
Weighted residual factors for significantly intense reflections	0.0901
Weighted residual factors for all reflections included in the refinement	0.0997
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4312000.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4312000.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4312000.cif
3502	2010-11-16	../uploads/cif-deposit/cod/cif Adding structures of 4312000 via cif-deposit CGI script.	4312000.cif