Crystallography Open Database

Information card for entry 4312003

4312002 << 4312003 >> 4312004

Preview

Coordinates	4312003.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Ar*PbSi(SiMe3)3.0.5n-hexane
Formula	C48 H83 Pb Si4
Calculated formula	C48 H83 Pb Si4
Title of publication	Terphenyl Ligand Stabilized Lead(II) Derivatives: Steric Effects and Lead-Lead Bonding in Diplumbenes
Authors of publication	Shirley Hino; Marilyn Olmstead; Andrew D. Phillips; Robert J. Wright; Philip P. Power
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	7346 - 7352
a	19.6824 ± 0.0012 Å
b	15.91 ± 0.0008 Å
c	16.9291 ± 0.001 Å
α	90°
β	101.041 ± 0.003°
γ	90°
Cell volume	5203.2 ± 0.5 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0479
Residual factor for significantly intense reflections	0.0331
Weighted residual factors for significantly intense reflections	0.0597
Weighted residual factors for all reflections included in the refinement	0.0644
Goodness-of-fit parameter for all reflections included in the refinement	1.131
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179159 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/20.	4312003.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4312003.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4312003.cif
3505	2010-11-16	../uploads/cif-deposit/cod/cif Adding structures of 4312003 via cif-deposit CGI script.	4312003.cif