Crystallography Open Database

Information card for entry 4314729

Preview

Coordinates	4314729.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	complex8
Formula	C60 H146 Li5 N15 Si10
Calculated formula	C59.49 H144.47 Li5 N15 Si10
Title of publication	Lithium Furyl and Pyridyl Amidinates as Building Blocks in Coordination Polymers, Ladder and Cage Structures
Authors of publication	Sinai Aharonovich; Mark Botoshanski; Ziv Rabinovich; Robert M. Waymouth; Moris S. Eisen
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	1220 - 1229
a	20.727 ± 0.004 Å
b	24.744 ± 0.005 Å
c	20.756 ± 0.004 Å
α	90°
β	114.09 ± 0.03°
γ	90°
Cell volume	9718 ± 4 Å³
Cell temperature	230 ± 0.1 K
Ambient diffraction temperature	230 ± 0.1 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1209
Residual factor for significantly intense reflections	0.0685
Weighted residual factors for significantly intense reflections	0.2007
Weighted residual factors for all reflections included in the refinement	0.229
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4314729.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4314729.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4314729.cif
7872	2011-02-02	../uploads/cif-deposit/cod/cif Adding structures of 4314729 via cif-deposit CGI script.	4314729.cif