Crystallography Open Database

Information card for entry 4314735

Preview

Coordinates	4314735.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H96 Cl7 Co2 N4 O6 Si2
Calculated formula	C69 H96 Cl7 Co2 N4 O6 Si2
Title of publication	Lewis-Base-Stabilized Dichlorosilylene: A Two-Electron σ-Donor Ligand
Authors of publication	Jianfeng Li; Sebastian Merkel; Julian Henn; Kathrin Meindl; Alexander Döring; Herbert W. Roesky; Rajendra S. Ghadwal; Dietmar Stalke
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	775 - 777
a	9.991 ± 0.0015 Å
b	29.253 ± 0.004 Å
c	25.866 ± 0.004 Å
α	90°
β	94.831 ± 0.002°
γ	90°
Cell volume	7532.9 ± 1.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0592
Residual factor for significantly intense reflections	0.0539
Weighted residual factors for significantly intense reflections	0.1244
Weighted residual factors for all reflections included in the refinement	0.1271
Goodness-of-fit parameter for all reflections included in the refinement	1.127
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179227 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/47.	4314735.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4314735.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4314735.cif
7878	2011-02-02	../uploads/cif-deposit/cod/cif Adding structures of 4314735 via cif-deposit CGI script.	4314735.cif