Crystallography Open Database

Information card for entry 4316561

Preview

Coordinates	4316561.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C128 N8 O74 Si2 W20 Zn4
Calculated formula	C128.016 N8 O74 Si2 W20 Zn4
Title of publication	Sandwich-Type Zinc-Containing Polyoxometalates with a Hexaprismane Core [{Zn2W(O)O3}2]4+ Synthesized by Thermally Induced Isomerization of a Metastable Polyoxometalate
Authors of publication	Yuji Kikukawa; Kazuya Yamaguchi; Noritaka Mizuno
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	8194 - 8196
a	34.7252 ± 0.0004 Å
b	26.3949 ± 0.0005 Å
c	27.7763 ± 0.0006 Å
α	90°
β	119.036 ± 0.001°
γ	90°
Cell volume	22259.1 ± 0.7 Å³
Cell temperature	153 K
Ambient diffraction temperature	153 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0777
Weighted residual factors for all reflections included in the refinement	0.2444
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179245 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/65.	4316561.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4316561.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4316561.cif
9772	2011-02-10	../uploads/cif-deposit/cod/cif Adding structures of 4316561 via cif-deposit CGI script.	4316561.cif