Crystallography Open Database

Information card for entry 4320343

4320342 << 4320343 >> 4320344

Preview

Coordinates	4320343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H74 F20 N2 Pt2 S2
Calculated formula	C56 H74 F20 N2 Pt2 S2
Title of publication	Synthesis and Reactivity of Bridging and Terminal Hydrosulfido Palladium and Platinum Complexes. Crystal Structures of [NBu4]2[{Pt(C6F5)2(μ-SH)}2], [Pt(C6F5)2(PPh3){S(H)AgPPh3}], and [Pt(C6F5)2(PPh3){S(AuPPh3)2}]
Authors of publication	José Ruiz; Venancio Rodríguez; Consuelo Vicente; José M. Martí; Gregorio López; José Pérez
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5354 - 5360
a	12.7811 ± 0.0009 Å
b	12.4547 ± 0.0008 Å
c	19.5582 ± 0.0016 Å
α	90°
β	103.706 ± 0.005°
γ	90°
Cell volume	3024.7 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.043
Residual factor for significantly intense reflections	0.0343
Weighted residual factors for significantly intense reflections	0.088
Weighted residual factors for all reflections included in the refinement	0.0927
Goodness-of-fit parameter for all reflections included in the refinement	0.995
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179306 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/03.	4320343.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320343.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320343.cif
17247	2011-04-06	../uploads/cif-deposit/cod/cif Adding structures of 4320343 via cif-deposit CGI script.	4320343.cif