Crystallography Open Database

Information card for entry 4320345

4320344 << 4320345 >> 4320346

Preview

Coordinates	4320345.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66.25 H45.5 Au2 Cl0.5 F10 P3 Pt S
Calculated formula	C66.25 H45.5 Au2 Cl0.5 F10 P3 Pt S
Title of publication	Synthesis and Reactivity of Bridging and Terminal Hydrosulfido Palladium and Platinum Complexes. Crystal Structures of [NBu4]2[{Pt(C6F5)2(μ-SH)}2], [Pt(C6F5)2(PPh3){S(H)AgPPh3}], and [Pt(C6F5)2(PPh3){S(AuPPh3)2}]
Authors of publication	José Ruiz; Venancio Rodríguez; Consuelo Vicente; José M. Martí; Gregorio López; José Pérez
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5354 - 5360
a	62.6035 ± 0.0009 Å
b	13.0329 ± 0.0002 Å
c	32.0828 ± 0.0005 Å
α	90°
β	104.703 ± 0.001°
γ	90°
Cell volume	25319.4 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1079
Residual factor for significantly intense reflections	0.0619
Weighted residual factors for significantly intense reflections	0.1374
Weighted residual factors for all reflections included in the refinement	0.1594
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4320345.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320345.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320345.cif
17249	2011-04-06	../uploads/cif-deposit/cod/cif Adding structures of 4320345 via cif-deposit CGI script.	4320345.cif