Crystallography Open Database

Information card for entry 4321900

4321899 << 4321900 >> 4321901

Preview

Coordinates	4321900.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H49 N Os P2 S
Calculated formula	C23 H49 N Os P2 S
Title of publication	Thermally Activated Site Exchange and Quantum Exchange Coupling Processes in Unsymmetrical Trihydride Osmium Compounds
Authors of publication	Amaya Castillo; Guada Barea; Miguel A. Esteruelas; Fernando J. Lahoz; Agustí LLedós; Feliu Maseras; Javier Modrego; Enrique Oñate; Luis A. Oro; Natividad Ruiz; Eduardo Sola
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	1814 - 1824
a	8.832 ± 0.002 Å
b	21.124 ± 0.005 Å
c	14.923 ± 0.004 Å
α	90 ± 0°
β	98.23 ± 0.03°
γ	90 ± 0°
Cell volume	2755.5 ± 1.2 Å³
Cell temperature	230 ± 0.2 K
Ambient diffraction temperature	230 ± 0.2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0466
Residual factor for significantly intense reflections	0.0301
Weighted residual factors for all reflections	0.0452
Weighted residual factors for significantly intense reflections	0.0328
Goodness-of-fit parameter for significantly intense reflections	1.0892
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179322 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/19.	4321900.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321900.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321900.cif
19763	2011-05-25	../uploads/cif-deposit/cod/cif Adding structures of 4321900 via cif-deposit CGI script.	4321900.cif