Crystallography Open Database

Information card for entry 4323555

Preview

Coordinates	4323555.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H62 Cl4 Cu2 N10 O11
Calculated formula	C36 H56 Cl4 Cu2 N10 O11
Title of publication	Synthesis, Crystal Structures, and Catalytic Activity of Dicopper(II) Complexes with Dinucleating Tetraimidazole Ligands [Cu2(RO)(mbipl)](ClO4)2 (R = Me, Et, 2-Pr; Hmbipl = 1,5-Bis[bis[(1-methyl-4-imidazolyl)methyl]amino]-3-pentanol) and [Cu2(MeO)(pbipl)](ClO4)2 (Hpbipl = 1,5-Bis[bis[(1-isopropyl-4-imidazolyl)methyl]amino]-3-pentanol)
Authors of publication	Masahito Kodera; Norihisa Terasako; Toshio Kita; Yoshimitsu Tachi; Koji Kano; Mikio Yamazaki; Masayuki Koikawa; Tadashi Tokii
Journal of publication	Inorganic Chemistry
Year of publication	1997
Journal volume	36
Pages of publication	3861 - 3868
a	28.46 ± 0.01 Å
b	19.28 ± 0.005 Å
c	18.339 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	10063 ± 5 Å³
Cell temperature	293.2 K
Ambient diffraction temperature	293.2 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for significantly intense reflections	0.0644
Weighted residual factors for significantly intense reflections	0.0683
Goodness-of-fit parameter for significantly intense reflections	1.06
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4323555.cif
130086	2015-01-23	cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ \| xargs -i sh -c 'cif_fix_values {} \ \| cif_filter --add-cif-header {} \ \| sponge {}'	4323555.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4323555.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4323555.cif
23802	2011-08-10	../uploads/cif-deposit/cod/cif Adding structures of 4323555 via cif-deposit CGI script.	4323555.cif