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Information card for entry 4323999
Preview
| Coordinates | 4323999.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | {N,N'-di-3-ethoxysalicylidene-(R,R)-2,4-pentanediamine}oxovanadium(IV) |
|---|---|
| Formula | C23 H30 N2 O6 V |
| Calculated formula | C23 H28 N2 O6 V |
| Title of publication | Interconversion between Polymeric and Monomeric Forms of Oxovanadium(IV) Complexes with Tetradentate Schiff Base Ligands Derived from (R,R)-2,4-Pentanediamine |
| Authors of publication | Ryuichi Kasahara; Masanobu Tsuchimoto; Shigeru Ohba; Kiyohiko Nakajima; Hiroyuki Ishida; Masaaki Kojima |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 1996 |
| Journal volume | 35 |
| Pages of publication | 7661 - 7665 |
| a | 13.764 ± 0.004 Å |
| b | 21.544 ± 0.004 Å |
| c | 7.682 ± 0.005 Å |
| α | 90 ± 0° |
| β | 90 ± 0° |
| γ | 90 ± 0° |
| Cell volume | 2278 ± 1.7 Å3 |
| Cell temperature | 299 K |
| Ambient diffraction temperature | 299 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for significantly intense reflections | 0.0643 |
| Weighted residual factors for significantly intense reflections | 0.0535 |
| Goodness-of-fit parameter for significantly intense reflections | 1.37 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4323999.cif |
| 131254 | 2015-02-06 | cif/4/32/ (antanas@tasmanijos-velnias) Changing _atom_site_thermal_displace_type tag values from Uij to Uani, splitting _refine_ls_weighting_scheme tag into two tags, fixing values of *_site_symmetry_* tags for CIF 4323999. |
4323999.cif |
| 120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4323999.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4323999.cif |
| 24251 | 2011-08-14 | ../uploads/cif-deposit/cod/cif Adding structures of 4323999 via cif-deposit CGI script. |
4323999.cif |
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