Crystallography Open Database

Information card for entry 4324874

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Coordinates	4324874.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H61 O5 Os P4 Rh
Calculated formula	C62 H61 O5 Os P4 Rh
Title of publication	Unusual Ligand Transformations Initiated by dppm Deprotonation in Methylene-Bridged Rh/Os Complexes
Authors of publication	Kyle D. Wells; Robert McDonald; Michael J. Ferguson; Martin Cowie
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	3523 - 3538
a	13.6181 ± 0.0008 Å
b	19.2851 ± 0.0011 Å
c	21.612 ± 0.0012 Å
α	90°
β	97.6482 ± 0.0009°
γ	90°
Cell volume	5625.4 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0366
Residual factor for significantly intense reflections	0.0286
Weighted residual factors for significantly intense reflections	0.0707
Weighted residual factors for all reflections included in the refinement	0.0743
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179351 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/48.	4324874.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324874.cif
43325	2012-03-14	../uploads/cif-deposit/cod/cif Adding structures of 4324874 via cif-deposit CGI script.	4324874.cif