#------------------------------------------------------------------------------ #$Date: 2016-04-07 01:59:18 +0300 (Thu, 07 Apr 2016) $ #$Revision: 181931 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/32/48/4324884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4324884 _pd_meas_number_of_points 1629 _pd_proc_number_of_points 1629 _cod_data_source_file ic102546w_si_001_2.hkl _cod_data_source_block Wet_Umbite loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 0.0 0.0 1158792511225856.00 . 86.0 0.0 1087188292861952.00 . 91.0 0.0 1019858573590528.00 . 100.0 0.0 956556929662976.000 . 107.0 0.0 897050828865536.000 . 107.0 0.0 841120556777472.000 . 102.0 0.0 788559216771072.000 . 99.0 0.0 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660.0 0.001515 665.95721 668.85663 662.0 0.001511 667.13409 669.33081 665.0 0.001504 668.30341 670.17810 669.0 0.001495 669.46808 671.52411 675.0 0.001481 670.62994 675.98413 686.0 0.001458 671.79163 689.29291 705.0 0.001418 672.95587 715.88013 738.0 0.001355 674.12585 756.61487 776.0 0.001289 675.30432 799.10718 802.0 0.001247 676.49451 808.27667 805.0 0.001242 677.69965 798.38257 792.0 0.001263 678.92322 767.28503 797.0 0.001255 680.16827 751.34912 869.0 0.001151 681.43976 809.34729 1060.0 0.000943 682.73981 1001.17871 1377.0 0.000726 684.07312 1329.41943 1718.0 0.000582 685.44299 1673.25842 1902.0 0.000526 686.85364 1846.76392 1814.0 0.000551 688.30865 1763.20618 1516.0 0.000660 689.81183 1478.51086 1184.0 0.000845 691.36731 1167.95093 948.0 0.001055 692.97833 974.59729 827.0 0.001209 694.64880 905.60168 783.0 0.001277 696.38263 890.93579 779.0 0.001284 698.18304 871.47589 794.0 0.001259 700.05347 833.13910 812.0 0.001232 701.99768 788.32355 821.0 0.001218 704.01782 750.98914 814.0 0.001229 706.11768 727.15649 797.0 0.001255 708.29956 715.50763 777.0 0.001287 710.56647 711.69507 760.0 0.001316 712.92035 711.83508 749.0 0.001335 715.36322 713.63379 742.0 0.001348 717.89722 716.05884 738.0 0.001355 720.52313 719.13916 737.0 0.001357 723.24329 721.99988 736.0 0.001359 726.05804 725.04700 737.0 0.001357 728.96735 728.11841 738.0 0.001355 731.97235 731.29474 740.0 0.001351 735.07257 734.57886 743.0 0.001346 738.26740 737.97546 748.0 0.001337 741.55676 741.49390 754.0 0.001326 744.93811 746.17584 759.0 0.001318 748.41095 751.56586 767.0 0.001304 751.97241 756.01367 777.0 0.001287 755.62067 761.34503 789.0 0.001267 759.35309 768.54144 800.0 0.001250 763.16565 779.36957 810.0 0.001235 767.05585 796.58771 821.0 0.001218 771.01831 824.01691 839.0 0.001192 775.05005 866.69354 873.0 0.001145 779.14520 930.11884 941.0 0.001063 783.29877 1016.47778 1055.0 0.000948 787.50531 1118.57227 1193.0 0.000838 791.75854 1215.26965 1293.0 0.000773 796.05322 1272.38733 1296.0 0.000772 800.38202 1259.93335 1197.0 0.000835 804.73724 1180.62317 1056.0 0.000947 809.11261 1070.17957 933.0 0.001072 813.50006 968.33282 855.0 0.001170 817.89197 897.28906 816.0 0.001225 822.28040 858.68671 801.0 0.001248 826.65619 842.81372 795.0 0.001258 831.01166 838.96979 796.0 0.001256 835.33698 831.41571 803.0 0.001245 839.62457 836.09155 819.0 0.001221 843.86456 852.87250 863.0 0.001159 848.04742 901.60870 970.0 0.001031 852.16498 1018.23462 1184.0 0.000845 856.20648 1233.90747 1505.0 0.000664 860.16412 1530.53564 1839.0 0.000544 864.02747 1810.28870 2017.0 0.000496 867.78717 1944.03943 1938.0 0.000516 871.43439 1872.82068 1656.0 0.000604 874.95923 1627.07373 1330.0 0.000752 878.35413 1331.21655 1086.0 0.000921 881.60870 1099.50732 957.0 0.001045 884.71478 953.39386 910.0 0.001099 887.66370 905.52362 914.0 0.001094 890.44727 904.19470 961.0 0.001041 893.05774 959.33685 1080.0 0.000926 895.48688 1081.54810 1307.0 0.000765 897.72736 1315.94727 1633.0 0.000612 899.77252 1643.06152 1975.0 0.000506 901.61517 1955.31274 2197.0 0.000455 903.24969 2134.43896 2230.0 0.000448 904.66974 2153.40625 2136.0 0.000468 905.86951 2066.07642 2038.0 0.000491 906.84497 2003.89355 2028.0 0.000493 907.59106 2039.48474 2137.0 0.000468 908.10425 2156.21973 2349.0 0.000426 908.38062 2305.94189 2617.0 0.000382 908.41766 2464.73413 2858.0 0.0003499 908.21271 2631.45508 2987.0 0.0003348 907.76416 2780.85547 2945.0 0.0003396 907.07062 2857.08276 2745.0 0.000364 906.13147 2799.70581 2457.0 0.000407 904.94653 2577.10303 2154.0 0.000464 903.51648 2226.77197 1865.0 0.000536 901.84222 1840.70618 1601.0 0.000625 899.92566 1500.49634 1369.0 0.000730 897.76837 1249.95874 1182.0 0.000846 895.37396 1086.96313 1046.0 0.000956 892.74481 994.98138 963.0 0.001038 889.88568 950.09808 921.0 0.001086 886.80060 934.20898 915.0 0.001093 883.49445 945.34113 956.0 0.001046 879.97308 1001.71967 1088.0 0.000919 876.24152 1151.17224 1381.0 0.000724 872.30762 1445.01794 1886.0 0.000530 868.17676 1912.57703 2543.0 0.000393 863.85754 2486.87549 3134.0 0.0003191 859.35736 2995.92261 3393.0 0.0002947 854.68365 3230.11157 3188.0 0.0003137 849.84613 3077.76709 2631.0 0.000380 844.85187 2603.41406 1981.0 0.000505 839.71191 2016.89856 1445.0 0.000692 834.43445 1504.79407 1107.0 0.000903 829.02930 1159.47449 936.0 0.001068 823.50677 975.76770 867.0 0.001153 817.87616 901.12213 852.0 0.001174 812.14801 888.62592 865.0 0.001156 806.33344 909.92645 893.0 0.001120 800.44141 949.75598 936.0 0.001068 794.48334 1001.23279 997.0 0.001003 788.46863 1055.06274 1087.0 0.000920 782.40839 1106.95789 1212.0 0.000825 776.31348 1167.08167 1371.0 0.000729 770.19287 1264.64307 1551.0 0.000645 764.05847 1427.31335 1729.0 0.000578 757.91791 1653.45618 1887.0 0.000530 751.78326 1902.12280 2013.0 0.000497 745.66357 2106.22900 2089.0 0.000479 739.56708 2203.48218 2092.0 0.000478 733.50439 2165.43188 1997.0 0.000501 727.48303 2000.41858 1796.0 0.000557 721.51245 1743.35791 1529.0 0.000654 715.60071 1446.75769 1255.0 0.000797 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597.58405 593.0 0.001686 588.67480 590.13519 586.0 0.001706 586.29980 585.78070 583.0 0.001715 584.02289 582.95941 581.0 0.001721 581.83966 580.76019 579.0 0.001727 579.74542 578.78900 577.0 0.001733 577.73669 577.43353 576.0 0.001736 575.80792 575.66406 575.0 0.001739 573.95557 574.66107 575.0 0.001739 572.17468 572.96844 574.0 0.001742 570.46100 571.36041 574.0 0.001742 568.81024 569.83850 576.0 0.001736 567.21826 568.40741 577.0 0.001733 565.68085 567.08240 581.0 0.001721 564.19305 563.78473 587.0 0.001704 562.75226 564.32819 597.0 0.001675 561.35388 569.30963 610.0 0.001639 559.99438 583.12451 628.0 0.001592 558.67047 610.32971 649.0 0.001541 557.37891 650.51379 670.0 0.001493 556.11633 695.22565 685.0 0.001460 554.88025 733.10895 691.0 0.001447 553.66803 756.91315 690.0 0.001449 552.47760 763.22961 685.0 0.001460 551.30597 754.20673 681.0 0.001468 550.15198 735.93268 678.0 0.001475 549.01373 714.47778 676.0 0.001479 547.88959 695.83594 674.0 0.001484 546.77917 684.00812 668.0 0.001497 545.68091 678.54187 661.0 0.001513 544.59399 674.59180 653.0 0.001531 543.51868 665.71753 646.0 0.001548 542.45386 648.00439 641.0 0.001560 541.40021 623.97491 634.0 0.001577 540.35748 597.23694 623.0 0.001605 539.32617 574.16998 608.0 0.001645 538.30688 557.53656 590.0 0.001695 537.29999 547.21930 573.0 0.001745 536.30646 541.52386 559.0 0.001789 535.32745 538.55176 548.0 0.001825 534.36359 536.92804 543.0 0.001842 533.41626 535.89081 539.0 0.001855 532.48651 535.10065 535.0 0.001869 531.57581 534.43994 532.0 0.001880 530.68494 533.88165 531.0 0.001883 529.81555 533.44061 530.0 0.001887 528.96899 533.16315 530.0 0.001887 528.14600 533.16101 531.0 0.001883 527.34821 533.69208 534.0 0.001873 526.57678 535.20697 541.0 0.001848 525.83215 539.00903 551.0 0.001815 525.11572 545.75769 567.0 0.001764 524.42841 559.70868 590.0 0.001695 523.77039 582.93915 618.0 0.001618 523.14252 615.74518 649.0 0.001541 522.54486 657.23010 684.0 0.001462 521.97809 702.69342 718.0 0.001393 521.44153 744.68475 750.0 0.001333 520.93549 775.42633 780.0 0.001282 520.45917 792.02100 799.0 0.001252 520.01233 799.16193 804.0 0.001244 519.59381 801.96045 791.0 0.001264 519.20251 798.46320 766.0 0.001305 518.83752 782.60809 733.0 0.001364 518.49701 751.63293 699.0 0.001431 518.17920 712.57806 671.0 0.001490 517.88239 677.00446 660.0 0.001515 517.60431 661.58173 677.0 0.001477 517.34253 674.57971 722.0 0.001385 517.09485 711.05115 782.0 0.001279 516.85846 754.43781 825.0 0.001212 516.63013 783.79669 827.0 0.001209 516.40710 783.79022 780.0 0.001282 516.18652 752.41217 706.0 0.001416 515.96448 700.87854 633.0 0.001580 515.73804 646.15491 581.0 0.001721 515.50360 602.66602 558.0 0.001792 515.25787 578.23779 559.0 0.001789 514.99677 574.55566 579.0 0.001727 514.71759 583.76990 614.0 0.001629 514.41583 613.49835 661.0 0.001513 514.08844 654.76819 714.0 0.001401 513.73187 699.70306 768.0 0.001302 513.34265 756.79016 820.0 0.001220 512.91779 820.05750 862.0 0.001160 512.45367 886.84460 896.0 0.001116 511.94748 946.22424 924.0 0.001082 511.39627 985.48431 940.0 0.001064 510.79739 992.17072 932.0 0.001073 510.14850 954.01099 890.0 0.001124 509.44699 876.41394 812.0 0.001232 508.69122 780.40308 717.0 0.001395 507.87909 683.42224 630.0 0.001587 507.00970 601.85413 564.0 0.001773 506.08148 545.81720 525.0 0.001905 505.09381 514.61212 502.0 0.001992 504.04581 500.68152 491.0 0.002037 502.93768 495.80594 485.0 0.002062 501.76974 494.51691 482.0 0.002075 500.54190 494.19623 480.0 0.002083 499.25555 493.93073 480.0 0.002083 497.91147 493.53473 482.0 0.002075 496.51126 496.96484 487.0 0.002053 495.05704 495.97516 496.0 0.002016 493.55109 495.45447 508.0 0.001969 491.99548 494.73782 519.0 0.001927 490.39346 493.91550 527.0 0.001898 488.74808 492.76566 526.0 0.001901 487.06305 491.16248 520.0 0.001923 485.34198 489.13681 510.0 0.001961 483.58835 486.73331 501.0 0.001996 481.80731 484.48145 494.0 0.002024 480.00241 482.43851 489.0 0.002045 478.17929 480.70612 485.0 0.002062 476.34213 478.65079 485.0 0.002062 474.49573 477.68460 486.0 0.002058 472.64542 477.82916 490.0 0.002041 470.79672 480.43085 499.0 0.002004 468.95474 487.49509 512.0 0.001953 467.12427 501.38205 531.0 0.001883 465.31088 523.64417 553.0 0.001808 463.51978 553.86200 576.0 0.001736 461.75623 588.91254 595.0 0.001681 460.02527 623.33374 608.0 0.001645 458.33197 650.90039 611.0 0.001637 456.68054 665.13354 603.0 0.001658 455.07645 664.31665 586.0 0.001706 453.52356 650.68866 565.0 0.001770 452.02652 628.32062 545.0 0.001835 450.58899 601.47668 530.0 0.001887 449.21457 574.01898 521.0 0.001919 447.90668 548.91010 516.0 0.001938 446.66837 527.96619 512.0 0.001953 445.50217 511.53778 509.0 0.001965 444.41086 498.79761 504.0 0.001984 443.39572 488.22171 499.0 0.002004 442.45865 479.17676 496.0 0.002016 441.60092 471.02631 494.0 0.002024 440.82321 464.16589 496.0 0.002016 440.12585 459.35846 501.0 0.001996 439.50858 457.20547 508.0 0.001969 438.97128 457.01843 517.0 0.001934 438.51248 463.42548 527.0 0.001898 438.13135 476.70096 540.0 0.001852 437.82623 500.32388 560.0 0.001786 437.59460 535.05945 585.0 0.001709 437.43411 577.60846 613.0 0.001631 437.34192 618.58563 632.0 0.001582 437.31470 646.86487 633.0 0.001580 437.34909 653.79095 613.0 0.001631 437.44092 636.71564 580.0 0.001724 437.58609 601.66412 547.0 0.001828 437.78049 561.27515 521.0 0.001919 438.01840 528.18805 504.0 0.001984 438.29562 508.65753 497.0 0.002012 438.60690 504.16483 495.0 0.002020 438.94666 511.76001 499.0 0.002004 439.30917 525.00122 505.0 0.001980 439.68936 536.78693 509.0 0.001965 440.08093 541.32178 509.0 0.001965 440.47812 536.10077 504.0 0.001984 440.87537 522.42969 495.0 0.002020 441.26669 504.40060 485.0 0.002062 441.64597 487.22134 478.0 0.002092 442.00760 475.50546 476.0 0.002101 442.34579 472.35669 484.0 0.002066 442.65509 479.34769 504.0 0.001984 442.93002 496.68219 536.0 0.001866 443.16476 522.89447 576.0 0.001736 443.35483 554.25177 612.0 0.001634 443.49503 584.59473 635.0 0.001575 443.58084 606.34790 639.0 0.001565 443.60770 612.99280 622.0 0.001608 443.57159 602.33813 591.0 0.001692 443.46902 577.85455 555.0 0.001802 443.29642 546.44495 521.0 0.001919 443.05099 515.06757 493.0 0.002028 442.72995 488.67599 474.0 0.002110 442.33130 469.38834 460.0 0.002174 441.85349 456.75208 451.0 0.002217 441.29498 449.40341 445.0 0.002247 440.65527 445.16028 439.0 0.002278 439.93439 442.69272 435.0 0.002299 439.13269 441.08472 432.0 0.002315 438.25107 439.82751 431.0 0.002320 437.29099 438.67969 431.0 0.002320 436.25504 437.54004 430.0 0.002326 435.14557 436.36966 430.0 0.002326 433.96649 435.15726 430.0 0.002326 432.72198 433.90311 429.0 0.002331 431.41647 432.11270 429.0 0.002331 430.05597 430.86127 429.0 0.002331 428.64624 429.62311 429.0 0.002331 427.19495 427.58646 431.0 0.002320 425.70947 426.90460 433.0 0.002309 424.19766 427.39542 436.0 0.002294 422.66931 429.87402 439.0 0.002278 421.13394 435.21793 441.0 0.002268 419.60242 443.38403 442.0 0.002262 418.08548 452.74078 441.0 0.002268 416.59503 460.49591 439.0 0.002278 415.14331 464.49026 438.0 0.002283 413.74393 463.97690 439.0 0.002278 412.40961 459.16757 442.0 0.002262 411.15466 452.05096 446.0 0.002242 409.99295 445.64673 451.0 0.002217 408.93942 441.70773 456.0 0.002193 408.00861 441.84207 462.0 0.002165 407.21533 445.76636 468.0 0.002137 406.57471 453.02252 476.0 0.002101 406.10104 463.16635 484.0 0.002066 405.80905 475.29526 494.0 0.002024 405.71268 488.13617 503.0 0.001988 405.82513 500.33667 514.0 0.001946 406.15924 511.11331 523.0 0.001912 406.72696 520.61005 530.0 0.001887 407.53873 528.92084 533.0 0.001876 408.60437 534.75745 531.0 0.001883 409.93146 535.69482 527.0 0.001898 411.52652 529.82397 520.0 0.001923 413.39404 516.88647 510.0 0.001961 415.53683 498.68918 499.0 0.002004 417.95462 478.92114 488.0 0.002049 420.64539 461.62009 478.0 0.002092 423.60495 449.64612 470.0 0.002128 426.82593 443.93430 464.0 0.002155 430.29819 443.97775 461.0 0.002169 434.00858 448.63809 461.0 0.002169 437.94086 456.83102 463.0 0.002160 442.07571 467.22327 466.0 0.002146 446.39221 478.91309 469.0 0.002132 450.86386 490.55283 472.0 0.002119 455.46338 500.80240 474.0 0.002110 460.15817 508.62570 478.0 0.002092 464.91559 513.65131 481.0 0.002079 469.69989 516.31171 487.0 0.002053 474.47147 517.68237 494.0 0.002024 479.19034 518.84180 504.0 0.001984 483.81332 520.33569 514.0 0.001946 488.29791 522.13574 524.0 0.001908 492.60117 523.58301 533.0 0.001876 496.67816 524.17053 539.0 0.001855 500.48489 523.78583 541.0 0.001848 503.97906 522.82965 541.0 0.001848 507.12070 522.04297 537.0 0.001862 509.87119 522.28937 536.0 0.001866 512.19568 524.41431 538.0 0.001859 514.06287 527.57294 544.0 0.001838 515.44635 535.60663 552.0 0.001812 516.32520 547.71887 564.0 0.001773 516.68463 564.48425 579.0 0.001727 516.51617 586.09570 605.0 0.001653 515.81903 612.30371 648.0 0.001543 514.60010 642.20935 706.0 0.001416 512.87439 674.56903 769.0 0.001300 510.66479 707.95691 824.0 0.001214 508.00363 739.05786 849.0 0.001178 504.93063 763.49139 837.0 0.001195 501.49515 775.28137 789.0 0.001267 497.75241 769.54767 720.0 0.001389 493.76459 745.76233 648.0 0.001543 489.60110 707.48334 587.0 0.001704 485.33563 659.62927 542.0 0.001845 481.04498 609.84528 513.0 0.001949 476.80634 565.83209 497.0 0.002012 472.69785 532.34546 491.0 0.002037 468.79391 509.89404 488.0 0.002049 465.16492 495.99399 490.0 0.002041 461.87302 487.37869 493.0 0.002028 458.96964 481.60818 497.0 0.002012 456.49298 477.58362 500.0 0.002000 454.46603 475.30890 500.0 0.002000 452.89377 475.38440 501.0 0.001996 451.75992 478.45950 505.0 0.001980 451.02603 484.98584 511.0 0.001957 450.62949 494.77325 518.0 0.001931 450.48322 507.04004 525.0 0.001905 450.47586 520.49072 534.0 0.001873 450.47253 533.60327 541.0 0.001848 450.31693 545.40417 547.0 0.001828 449.83569 553.88995 553.0 0.001808 448.84293 559.12549 557.0 0.001795 447.14771 561.33252 556.0 0.001799 444.56161 561.46991 552.0 0.001812 440.90979 560.30347 545.0 0.001835 436.04254 554.60156 535.0 0.001869 429.84851 548.48096 525.0 0.001905 422.27173 537.68842 514.0 0.001946 413.32413 521.65967 502.0 0.001992 403.10333 502.12018 492.0 0.002033 391.80444 483.09900 484.0 0.002066 379.73611 470.05817 483.0 0.002070 367.32867 468.68658 493.0 0.002028 355.13736 483.05130 517.0 0.001934 343.82849 513.14362 549.0 0.001821 334.16522 552.98578 582.0 0.001718 326.97498 591.39514 606.0 0.001650 323.08087 616.41095 613.0 0.001631 323.21753 620.67847 598.0 0.001672 327.90085 601.67804 566.0 0.001767 337.25641 566.39557 527.0 0.001898 350.77802 520.73138 488.0 0.002049 367.02570 482.60767 460.0 0.002174 383.21451 457.37833 443.0 0.002257 394.71838 446.53815 439.0 . . . 448.0 . . . 472.0 . . . 508.0 . . . 560.0 . . . 625.0 . . . 695.0 . . . 759.0 . . . 801.0 . . . 807.0 . . . 777.0 . . . 719.0 . . . 650.0 . . . 519.0 . . . 413.0 . . . 350.0 . . . 304.0 . . . 265.0 . . . 233.0 . . . 199.0 . . . 167.0 . . . 130.0 . . . 82.0 . . . 28.0 . . . 2.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . 0.0 . . . loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_wavelength_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 0 1 1 1 o 7976.695 7946.141 180.00 8.23780 47.09 0 1 1 2 o 7976.695 7946.141 180.00 8.23780 47.09 1 0 0 1 o 411.875 399.401 180.00 7.28111 0.96 1 0 0 2 o 411.875 399.401 180.00 7.28111 0.96 0 0 2 2 o 24282.881 24427.363 180.00 6.72617 46.34 0 0 2 1 o 24282.881 24427.363 180.00 6.72617 46.34 1 1 0 1 o 33335.453 33743.813 0.00 5.96839 100.00 1 1 0 2 o 33335.453 33743.813 0.00 5.96839 100.00 0 1 2 1 o 68.514 198.930 0.00 5.65110 0.16 0 1 2 2 o 68.514 198.930 0.00 5.65110 0.16 1 1 -1 1 o 3876.710 3952.597 180.00 5.47083 9.85 1 1 -1 2 o 3876.710 3952.597 180.00 5.47083 9.85 1 1 1 1 o 3056.116 3075.848 0.00 5.44040 7.62 1 1 1 2 o 3056.116 3075.848 0.00 5.44040 7.62 0 2 0 1 o 23578.334 23334.879 180.00 5.21003 27.18 0 2 0 2 o 23578.334 23334.879 180.00 5.21003 27.18 1 0 -2 1 o 1661.228 2593.852 0.00 4.96343 1.61 1 0 -2 2 o 1661.228 2593.852 0.00 4.96343 1.61 1 0 2 1 o 2583.706 2232.942 180.00 4.91822 2.54 1 0 2 2 o 2583.706 2232.942 180.00 4.91822 2.54 0 2 1 2 o 728.581 600.893 0.00 4.85838 1.68 0 2 1 1 o 728.581 600.893 0.00 4.85838 1.68 1 1 -2 2 o 6283.660 6401.166 180.00 4.48104 10.43 1 1 -2 1 o 6283.660 6401.166 180.00 4.48104 10.43 1 1 2 2 o 4711.807 4935.667 180.00 4.44769 7.66 1 1 2 1 o 4711.807 4935.667 180.00 4.44769 7.66 1 2 0 1 o 852.327 634.572 180.00 4.23703 1.33 1 2 0 2 o 852.327 634.572 180.00 4.23703 1.33 0 1 3 2 o 18199.484 17609.674 0.00 4.11892 26.82 0 1 3 1 o 18199.484 17609.674 0.00 4.11892 26.82 0 2 2 1 o 1727.837 1711.935 0.00 4.11890 2.31 0 2 2 2 o 1727.837 1711.935 0.00 4.11890 2.31 1 2 -1 2 o 568.706 623.032 180.00 4.04751 0.78 1 2 -1 1 o 568.706 623.032 180.00 4.04751 0.78 1 2 1 1 o 35.426 30.399 180.00 4.03514 0.04 1 2 1 2 o 35.426 30.399 180.00 4.03514 0.04 2 0 0 2 o 17316.924 14212.983 180.00 3.64055 9.71 2 0 0 1 o 17316.924 14212.983 180.00 3.64055 9.71 1 1 -3 1 o 4351.110 4855.118 0.00 3.59806 4.91 1 1 -3 2 o 4351.110 4855.118 0.00 3.59806 4.91 1 2 -2 1 o 93.069 117.947 0.00 3.59369 0.15 1 2 -2 2 o 93.069 117.947 0.00 3.59369 0.15 1 1 3 1 o 2239.079 2445.622 180.00 3.57215 2.50 1 1 3 2 o 2239.079 2445.622 180.00 3.57215 2.50 1 2 2 2 o 281.844 276.835 0.00 3.57642 0.25 1 2 2 1 o 281.844 276.835 0.00 3.57642 0.25 2 1 0 1 o -3.155 60.204 180.00 3.43683 0.00 2 1 0 2 o -3.155 60.204 180.00 3.43683 0.00 0 0 4 2 o 272.933 229.277 180.00 3.36309 0.16 0 0 4 1 o 272.933 229.277 180.00 3.36309 0.16 0 2 3 1 o 2584.154 2523.988 0.00 3.39866 2.48 0 2 3 2 o 2584.154 2523.988 0.00 3.39866 2.48 2 1 -1 1 o 6203.796 4585.114 180.00 3.33682 5.98 2 1 -1 2 o 6203.796 4585.114 180.00 3.33682 5.98 0 3 1 1 o 17205.715 17591.342 0.00 3.36306 17.02 0 3 1 2 o 17205.715 17591.342 0.00 3.36306 17.02 2 1 1 2 o 142.761 24.275 0.00 3.32298 0.14 2 1 1 1 o 142.761 24.275 0.00 3.32298 0.14 2 0 -2 1 o 3627.151 3985.687 180.00 3.21404 1.78 2 0 -2 2 o 3627.151 3985.687 180.00 3.21404 1.78 0 1 4 2 o 9600.493 10698.842 180.00 3.20052 8.20 0 1 4 1 o 9600.493 10698.842 180.00 3.20052 8.20 2 0 2 1 o -14.405 0.254 180.00 3.18944 0.01 2 0 2 2 o -14.405 0.254 180.00 3.18944 0.01 1 3 0 1 o 22221.279 22145.510 180.00 3.13492 18.79 1 3 0 2 o 22221.279 22145.510 180.00 3.13492 18.79 1 2 -3 1 o 2285.293 2198.546 180.00 3.08792 2.00 1 2 -3 2 o 2285.293 2198.546 180.00 3.08792 2.00 2 1 -2 2 o 10135.307 9762.810 0.00 3.07126 8.27 2 1 -2 1 o 10135.307 9762.810 0.00 3.07126 8.27 1 0 -4 2 o 46857.15 44711.16 180.00 3.06386 18.96 1 0 -4 1 o 46857.15 44711.16 180.00 3.06386 18.96 0 3 2 2 o 18128.627 17649.273 180.00 3.08616 15.05 0 3 2 1 o 18128.627 17649.273 180.00 3.08616 15.05 1 0 4 2 o 72072.47 68867.93 0.00 3.04252 28.81 1 0 4 1 o 72072.47 68867.93 0.00 3.04252 28.81 1 3 -1 1 o 5110.347 4838.640 0.00 3.05578 3.96 1 3 -1 2 o 5110.347 4838.640 0.00 3.05578 3.96 1 2 3 1 o 287.663 277.429 180.00 3.07150 0.28 1 2 3 2 o 287.663 277.429 180.00 3.07150 0.28 2 1 2 2 o 9528.234 9136.028 180.00 3.04977 7.64 2 1 2 1 o 9528.234 9136.028 180.00 3.04977 7.64 1 3 1 2 o 6285.521 6028.655 180.00 3.05045 4.87 1 3 1 1 o 6285.521 6028.655 180.00 3.05045 4.87 1 1 -4 2 o 7945.943 9089.130 0.00 2.93943 5.99 1 1 -4 1 o 7945.943 9089.130 0.00 2.93943 5.99 2 2 0 1 o 63620.16 63341.54 0.00 2.98420 49.07 2 2 0 2 o 63620.16 63341.54 0.00 2.98420 49.07 2 2 -1 1 o 18287.357 18620.658 180.00 2.91802 13.49 2 2 -1 2 o 18287.357 18620.658 180.00 2.91802 13.49 1 1 4 1 o 12831.086 12798.912 0.00 2.92057 9.53 1 1 4 2 o 12831.086 12798.912 0.00 2.92057 9.53 2 2 1 2 o 20322.539 19088.141 0.00 2.90875 14.96 2 2 1 1 o 20322.539 19088.141 0.00 2.90875 14.96 1 3 -2 1 o 100.255 310.756 0.00 2.84576 0.06 1 3 -2 2 o 100.255 310.756 0.00 2.84576 0.06 0 2 4 1 o 3019.728 1999.945 180.00 2.82555 2.05 0 2 4 2 o 3019.728 1999.945 180.00 2.82555 2.05 1 3 2 1 o 2080.145 2177.753 0.00 2.83716 1.41 1 3 2 2 o 2080.145 2177.753 0.00 2.83716 1.41 2 1 -3 1 o 213.416 220.898 0.00 2.73927 0.16 2 1 -3 2 o 213.416 220.898 0.00 2.73927 0.16 2 2 -2 2 o 4987.089 5711.294 180.00 2.73542 3.12 2 2 -2 1 o 4987.089 5711.294 180.00 2.73542 3.12 0 3 3 2 o 2529.822 3136.600 180.00 2.74593 1.62 0 3 3 1 o 2529.822 3136.600 180.00 2.74593 1.62 2 2 2 1 o 1438.302 1427.965 180.00 2.72020 0.86 2 2 2 2 o 1438.302 1427.965 180.00 2.72020 0.86 2 1 3 1 o 3205.770 2381.545 0.00 2.71644 2.13 2 1 3 2 o 3205.770 2381.545 0.00 2.71644 2.13 1 2 -4 1 o 10755.829 10970.082 0.00 2.64104 6.48 1 2 -4 2 o 10755.829 10970.082 0.00 2.64104 6.48 1 2 4 2 o 6328.434 6605.429 180.00 2.62733 3.75 1 2 4 1 o 6328.434 6605.429 180.00 2.62733 3.75 0 1 5 1 o 10290.266 9794.015 180.00 2.60503 6.07 0 1 5 2 o 10290.266 9794.015 180.00 2.60503 6.07 0 4 0 1 o 2178.357 2012.867 180.00 2.60501 0.68 0 4 0 2 o 2178.357 2012.867 180.00 2.60501 0.68 1 3 -3 2 o 8247.971 8491.921 180.00 2.57407 4.79 1 3 -3 1 o 8247.971 8491.921 180.00 2.57407 4.79 1 3 3 1 o 8143.753 8586.096 0.00 2.56454 4.66 1 3 3 2 o 8143.753 8586.096 0.00 2.56454 4.66 0 4 1 1 o 7557.255 7075.242 0.00 2.55750 4.28 0 4 1 2 o 7557.255 7075.242 0.00 2.55750 4.28 2 2 -3 2 o 382.797 131.154 0.00 2.49300 0.20 2 2 -3 1 o 382.797 131.154 0.00 2.49300 0.20 2 0 -4 2 o 42.486 28.232 180.00 2.48172 0.01 2 0 -4 1 o 42.486 28.232 180.00 2.48172 0.01 2 3 0 2 o 935.787 142.776 180.00 2.51306 0.51 2 3 0 1 o 935.787 142.776 180.00 2.51306 0.51 1 1 -5 1 o 3328.979 3623.567 0.00 2.45972 1.79 1 1 -5 2 o 3328.979 3623.567 0.00 2.45972 1.79 2 2 3 1 o 1091.268 1220.940 180.00 2.47576 0.57 2 2 3 2 o 1091.268 1220.940 180.00 2.47576 0.57 2 0 4 2 o 1283.685 1535.855 0.00 2.45911 0.35 2 0 4 1 o 1283.685 1535.855 0.00 2.45911 0.35 2 3 -1 1 o 3207.475 3812.344 180.00 2.47316 1.74 2 3 -1 2 o 3207.475 3812.344 180.00 2.47316 1.74 2 3 1 1 o 2279.092 3359.672 180.00 2.46750 1.26 2 3 1 2 o 2279.092 3359.672 180.00 2.46750 1.26 1 1 5 1 o 1882.960 1131.932 180.00 2.44589 0.98 1 1 5 2 o 1882.960 1131.932 180.00 2.44589 0.98 1 4 0 1 o 41.455 41.650 0.00 2.45276 0.02 1 4 0 2 o 41.455 41.650 0.00 2.45276 0.02 2 1 -4 1 o 5880.064 5519.894 180.00 2.41419 2.95 2 1 -4 2 o 5880.064 5519.894 180.00 2.41419 2.95 3 0 0 2 o 84.185 40.453 180.00 2.42704 0.02 3 0 0 1 o 84.185 40.453 180.00 2.42704 0.02 0 4 2 2 o 708.869 251.144 0.00 2.42919 0.38 0 4 2 1 o 708.869 251.144 0.00 2.42919 0.38 1 4 -1 1 o 84.355 87.105 180.00 2.41429 0.04 1 4 -1 2 o 84.355 87.105 180.00 2.41429 0.04 0 3 4 2 o 4357.952 4333.655 0.00 2.41610 2.26 0 3 4 1 o 4357.952 4333.655 0.00 2.41610 2.26 1 4 1 2 o 440.945 489.035 180.00 2.41166 0.23 1 4 1 1 o 440.945 489.035 180.00 2.41166 0.23 2 1 4 2 o 2259.218 2901.977 0.00 2.39337 1.12 2 1 4 1 o 2259.218 2901.977 0.00 2.39337 1.12 0 2 5 1 o 1716.707 2171.035 0.00 2.39054 0.84 0 2 5 2 o 1716.707 2171.035 0.00 2.39054 0.84 3 1 0 2 o 10654.914 9546.907 180.00 2.36376 5.10 3 1 0 1 o 10654.914 9546.907 180.00 2.36376 5.10 2 3 -2 1 o 133.567 119.224 0.00 2.35902 0.08 2 3 -2 2 o 133.567 119.224 0.00 2.35902 0.08 2 3 2 2 o 5.038 5.804 0.00 2.34924 0.00 2 3 2 1 o 5.038 5.804 0.00 2.34924 0.00 3 1 -1 2 o 1.573 2.502 0.00 2.33165 0.00 3 1 -1 1 o 1.573 2.502 0.00 2.33165 0.00 3 1 1 1 o 4.647 5.693 180.00 2.32456 0.00 3 1 1 2 o 4.647 5.693 180.00 2.32456 0.00 1 3 -4 2 o 914.572 1047.716 180.00 2.29768 0.41 1 3 -4 1 o 914.572 1047.716 180.00 2.29768 0.41 1 2 -5 1 o 4807.535 4450.300 180.00 2.27677 2.13 1 2 -5 2 o 4807.535 4450.300 180.00 2.27677 2.13 1 4 -2 1 o 77.786 67.137 0.00 2.30662 0.03 1 4 -2 2 o 77.786 67.137 0.00 2.30662 0.03 3 0 -2 2 o 999.691 897.297 0.00 2.28968 0.27 3 0 -2 1 o 999.691 897.297 0.00 2.28968 0.27 1 4 2 1 o 874.550 1347.416 180.00 2.30204 0.38 1 4 2 2 o 874.550 1347.416 180.00 2.30204 0.38 1 3 4 2 o 86.634 71.954 180.00 2.28864 0.04 1 3 4 1 o 86.634 71.954 180.00 2.28864 0.04 3 0 2 2 o 2428.031 2216.894 180.00 2.27630 0.60 3 0 2 1 o 2428.031 2216.894 180.00 2.27630 0.60 0 0 6 2 o 18.246 23.335 0.00 2.24206 0.01 0 0 6 1 o 18.246 23.335 0.00 2.24206 0.01 2 2 -4 1 o 786.130 1101.473 180.00 2.24052 0.37 2 2 -4 2 o 786.130 1101.473 180.00 2.24052 0.37 1 2 5 2 o 5966.669 5246.081 180.00 2.26579 2.63 1 2 5 1 o 5966.669 5246.081 180.00 2.26579 2.63 3 1 -2 2 o 1327.816 2341.708 0.00 2.23633 0.54 3 1 -2 1 o 1327.816 2341.708 0.00 2.23633 0.54 0 4 3 1 o 14.080 0.591 0.00 2.25250 0.01 0 4 3 2 o 14.080 0.591 0.00 2.25250 0.01 3 1 2 1 o 1751.460 1532.389 0.00 2.22385 0.73 3 1 2 2 o 1751.460 1532.389 0.00 2.22385 0.73 2 2 4 1 o 0.799 0.587 0.00 2.22384 0.00 2 2 4 2 o 0.799 0.587 0.00 2.22384 0.00 2 3 -3 1 o 3832.703 3326.100 0.00 2.19820 1.55 2 3 -3 2 o 3832.703 3326.100 0.00 2.19820 1.55 3 2 0 2 o 872.080 747.607 180.00 2.20004 0.37 3 2 0 1 o 872.080 747.607 180.00 2.20004 0.37 0 1 6 2 o 11353.720 10395.410 0.00 2.19189 4.53 0 1 6 1 o 11353.720 10395.410 0.00 2.19189 4.53 2 3 3 2 o 6904.750 7875.360 0.00 2.18635 2.80 2 3 3 1 o 6904.750 7875.360 0.00 2.18635 2.80 3 2 -1 1 o 1210.516 1213.963 180.00 2.17408 0.49 3 2 -1 2 o 1210.516 1213.963 180.00 2.17408 0.49 3 2 1 1 o 605.039 414.704 180.00 2.16832 0.25 3 2 1 2 o 605.039 414.704 180.00 2.16832 0.25 1 4 -3 2 o 2409.010 2017.144 180.00 2.15468 0.93 1 4 -3 1 o 2409.010 2017.144 180.00 2.15468 0.93 1 0 -6 2 o 12127.816 11906.549 0.00 2.14832 2.37 1 0 -6 1 o 12127.816 11906.549 0.00 2.14832 2.37 2 1 -5 1 o 873.932 845.136 180.00 2.12749 0.37 2 1 -5 2 o 873.932 845.136 180.00 2.12749 0.37 1 0 6 1 o 15384.730 15715.898 180.00 2.13726 2.98 1 0 6 2 o 15384.730 15715.898 180.00 2.13726 2.98 1 4 3 1 o 17.934 19.584 0.00 2.14908 0.02 1 4 3 2 o 17.934 19.584 0.00 2.14908 0.02 0 3 5 2 o 411.111 395.287 0.00 2.12700 0.14 0 3 5 1 o 411.111 395.287 0.00 2.12700 0.14 2 1 5 1 o 174.325 173.594 180.00 2.10967 0.08 2 1 5 2 o 174.325 173.594 180.00 2.10967 0.08 2 4 0 1 o 17780.129 17789.945 180.00 2.11851 6.99 2 4 0 2 o 17780.129 17789.945 180.00 2.11851 6.99