Crystallography Open Database

Information card for entry 4324889

Preview

Coordinates	4324889.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H84 Cu9 N66
Calculated formula	C52 H84 Cu9 N66.24
Title of publication	Synthesis, Structures, and Magnetic Behavior of a Series of Copper(II) Azide Polymers of Cu4 Building Clusters and Isolation of a New Hemiaminal Ether as the Metal Complex
Authors of publication	Sandip Mukherjee; Bappaditya Gole; You Song; Partha Sarathi Mukherjee
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	3621 - 3631
a	10.92 ± 0.0003 Å
b	11.1292 ± 0.0003 Å
c	20.3016 ± 0.0005 Å
α	91.627 ± 0.001°
β	90.081 ± 0.001°
γ	115.39 ± 0.001°
Cell volume	2227.81 ± 0.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1005
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.0878
Weighted residual factors for all reflections included in the refinement	0.1031
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179351 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/48.	4324889.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324889.cif
43340	2012-03-14	../uploads/cif-deposit/cod/cif Adding structures of 4324889 via cif-deposit CGI script.	4324889.cif