Crystallography Open Database

Information card for entry 4324900

Preview

Coordinates	4324900.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24.99 H15.06 N0.33 O13.705 Zn4
Calculated formula	C24.99 H11.31 N0.33 O13.705 Zn4
Title of publication	Synthesis of Phase-Pure Interpenetrated MOF-5 and Its Gas Sorption Properties
Authors of publication	Hyunuk Kim; Sunirban Das; Min Gyu Kim; Danil N. Dybtsev; Yonghwi Kim; Kimoon Kim
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	3691 - 3696
a	18.388 ± 0.003 Å
b	18.388 ± 0.003 Å
c	43.916 ± 0.009 Å
α	90°
β	90°
γ	120°
Cell volume	12859 ± 4 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0891
Residual factor for significantly intense reflections	0.088
Weighted residual factors for significantly intense reflections	0.2691
Weighted residual factors for all reflections included in the refinement	0.2702
Goodness-of-fit parameter for all reflections included in the refinement	1.112
Diffraction radiation wavelength	0.9 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179352 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/49.	4324900.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324900.cif
43351	2012-03-14	../uploads/cif-deposit/cod/cif Adding structures of 4324900 via cif-deposit CGI script.	4324900.cif