Crystallography Open Database

Information card for entry 4325917

Preview

Coordinates	4325917.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H87 Li2 Mg N4 Si2
Calculated formula	C55 H87 Li2 Mg N4 Si2
Title of publication	Synthesis and Structural Characterization of Alkaline-Earth-Metal Bis(amido)silane and Lithium Oxobis(aminolato)silane Complexes
Authors of publication	Dongming Yang; Yuqiang Ding; Haishun Wu; Wenjun Zheng
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	7698 - 7706
a	13.288 ± 0.01 Å
b	20.967 ± 0.017 Å
c	20.419 ± 0.016 Å
α	90°
β	99.613 ± 0.01°
γ	90°
Cell volume	5609 ± 8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1342
Residual factor for significantly intense reflections	0.0639
Weighted residual factors for significantly intense reflections	0.1629
Weighted residual factors for all reflections included in the refinement	0.192
Goodness-of-fit parameter for all reflections included in the refinement	0.92
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179362 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/59.	4325917.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325917.cif
46953	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4325917 via cif-deposit CGI script.	4325917.cif