Crystallography Open Database

Information card for entry 4325921

Preview

Coordinates	4325921.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H102 Br2 Li6 N2 O10 Si6
Calculated formula	C52 H102 Br2 Li6 N2 O10 Si6
Title of publication	Synthesis and Structural Characterization of Alkaline-Earth-Metal Bis(amido)silane and Lithium Oxobis(aminolato)silane Complexes
Authors of publication	Dongming Yang; Yuqiang Ding; Haishun Wu; Wenjun Zheng
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	7698 - 7706
a	12.9987 ± 0.0012 Å
b	14.2883 ± 0.0013 Å
c	19.3868 ± 0.0018 Å
α	100.68 ± 0.001°
β	101.062 ± 0.001°
γ	96.146 ± 0.001°
Cell volume	3434.4 ± 0.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0377
Residual factor for significantly intense reflections	0.0282
Weighted residual factors for significantly intense reflections	0.0727
Weighted residual factors for all reflections included in the refinement	0.079
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179362 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/59.	4325921.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325921.cif
46957	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4325921 via cif-deposit CGI script.	4325921.cif