#------------------------------------------------------------------------------ #$Date: 2016-03-23 16:56:26 +0200 (Wed, 23 Mar 2016) $ #$Revision: 179400 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/32/97/4329713.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4329713 loop_ _publ_author_name 'Volodymyr Smetana' 'Gordon J. Miller' 'John D. Corbett' _publ_section_title ; Three Alkali-Metal-Gold-Gallium Systems. Ternary Tunnel Structures and Some Problems with Poorly Ordered Cations ; _journal_name_full 'Inorganic Chemistry' _journal_page_first 7711 _journal_page_last 7721 _journal_paper_doi 10.1021/ic300740u _journal_volume 51 _journal_year 2012 _chemical_formula_sum 'Au3 Ga2 Rb' _chemical_formula_weight 815.81 _space_group_IT_number 62 _symmetry_cell_setting orthorhombic _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _audit_update_record ; 2011-07-07 # Formatted by publCIF ; _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_formula_units_Z 4 _cell_length_a 13.384(3) _cell_length_b 5.5770(11) _cell_length_c 7.0170(14) _cell_measurement_reflns_used 2595 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 26.35 _cell_measurement_theta_min 10.30 _cell_volume 523.77(19) _computing_structure_refinement 'SHELXL-97 (Sheldrick, 2008)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.955 _diffrn_measured_fraction_theta_max 0.955 _diffrn_measurement_device_type 'Bruker CCD' _diffrn_measurement_method 'w scan' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0786 _diffrn_reflns_av_sigmaI/netI 0.0584 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -7 _diffrn_reflns_number 2595 _diffrn_reflns_theta_full 26.35 _diffrn_reflns_theta_max 26.35 _diffrn_reflns_theta_min 10.30 _exptl_absorpt_coefficient_mu 102.947 _exptl_absorpt_correction_T_max 0.001 _exptl_absorpt_correction_T_min 0.000 _exptl_absorpt_correction_type empirical _exptl_crystal_colour silver _exptl_crystal_density_diffrn 10.346 _exptl_crystal_description 'irregular fragment' _exptl_crystal_F_000 1344 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.07 _refine_diff_density_max 4.054 _refine_diff_density_min -3.125 _refine_diff_density_rms 0.750 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.149 _refine_ls_matrix_type full _refine_ls_number_parameters 34 _refine_ls_number_reflns 545 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.149 _refine_ls_R_factor_all 0.0513 _refine_ls_R_factor_gt 0.0384 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0216P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0734 _refine_ls_wR_factor_ref 0.0785 _reflns_number_gt 444 _reflns_number_total 545 _reflns_threshold_expression >2\s(I) _cod_data_source_file ic300740u_si_002_4.cif _cod_data_source_block RbAu3Ga2 _cod_original_cell_volume 523.77(18) _cod_database_code 4329713 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags Au1 Au 0.28395(8) 0.2500 0.39109(12) 0.0076(3) Uani 1 2 d S Au2 Au 0.28849(8) 0.2500 0.80165(12) 0.0090(3) Uani 1 2 d S Au3 Au 0.49332(8) 0.2500 0.92453(13) 0.0086(3) Uani 1 2 d S Rb4 Rb 0.5720(2) 0.2500 0.4017(3) 0.0139(6) Uani 1 2 d S Ga5 Ga 0.15331(15) -0.0017(3) 0.6053(2) 0.0067(4) Uani 1 1 d . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.0045(6) 0.0113(4) 0.0068(5) 0.000 0.0017(4) 0.000 Au2 0.0041(6) 0.0145(5) 0.0083(5) 0.000 -0.0032(4) 0.000 Au3 0.0032(5) 0.0113(5) 0.0141(5) 0.000 0.0014(4) 0.000 Rb4 0.0059(14) 0.0212(11) 0.0145(12) 0.000 -0.0014(10) 0.000 Ga5 0.0025(11) 0.0077(8) 0.0098(9) 0.0009(6) -0.0016(8) 0.0005(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Ga5 Au1 Ga5 65.00(8) 2_554 8_665 Ga5 Au1 Ga5 111.40(4) 2_554 . Ga5 Au1 Ga5 157.46(6) 8_665 . Ga5 Au1 Ga5 157.46(6) 2_554 7_565 Ga5 Au1 Ga5 111.40(4) 8_665 7_565 Ga5 Au1 Ga5 62.66(8) . 7_565 Ga5 Au1 Au2 140.43(5) 2_554 . Ga5 Au1 Au2 140.43(5) 8_665 . Ga5 Au1 Au2 57.10(4) . . Ga5 Au1 Au2 57.10(4) 7_565 . Ga5 Au1 Au2 56.39(4) 2_554 2_554 Ga5 Au1 Au2 116.06(5) 8_665 2_554 Ga5 Au1 Au2 55.07(4) . 2_554 Ga5 Au1 Au2 112.84(6) 7_565 2_554 Au2 Au1 Au2 102.40(2) . 2_554 Ga5 Au1 Au2 116.06(5) 2_554 2_564 Ga5 Au1 Au2 56.39(4) 8_665 2_564 Ga5 Au1 Au2 112.84(6) . 2_564 Ga5 Au1 Au2 55.07(4) 7_565 2_564 Au2 Au1 Au2 102.40(2) . 2_564 Au2 Au1 Au2 135.00(5) 2_554 2_564 Ga5 Au1 Rb4 78.91(6) 2_554 6_556 Ga5 Au1 Rb4 78.91(6) 8_665 6_556 Ga5 Au1 Rb4 78.58(6) . 6_556 Ga5 Au1 Rb4 78.58(6) 7_565 6_556 Au2 Au1 Rb4 127.12(6) . 6_556 Au2 Au1 Rb4 67.53(3) 2_554 6_556 Au2 Au1 Rb4 67.53(3) 2_564 6_556 Ga5 Au1 Rb4 122.85(7) 2_554 5_666 Ga5 Au1 Rb4 74.35(5) 8_665 5_666 Ga5 Au1 Rb4 120.80(6) . 5_666 Ga5 Au1 Rb4 74.10(6) 7_565 5_666 Au2 Au1 Rb4 66.10(4) . 5_666 Au2 Au1 Rb4 161.48(5) 2_554 5_666 Au2 Au1 Rb4 63.35(4) 2_564 5_666 Rb4 Au1 Rb4 130.89(3) 6_556 5_666 Ga5 Au1 Rb4 74.35(5) 2_554 5_656 Ga5 Au1 Rb4 122.85(7) 8_665 5_656 Ga5 Au1 Rb4 74.10(6) . 5_656 Ga5 Au1 Rb4 120.80(6) 7_565 5_656 Au2 Au1 Rb4 66.10(4) . 5_656 Au2 Au1 Rb4 63.35(4) 2_554 5_656 Au2 Au1 Rb4 161.48(5) 2_564 5_656 Rb4 Au1 Rb4 130.89(3) 6_556 5_656 Rb4 Au1 Rb4 98.20(7) 5_666 5_656 Ga5 Au1 Rb4 71.90(6) 2_554 . Ga5 Au1 Rb4 71.90(6) 8_665 . Ga5 Au1 Rb4 129.56(5) . . Ga5 Au1 Rb4 129.56(5) 7_565 . Au2 Au1 Rb4 87.69(5) . . Au2 Au1 Rb4 108.98(3) 2_554 . Au2 Au1 Rb4 108.98(3) 2_564 . Rb4 Au1 Rb4 145.20(4) 6_556 . Rb4 Au1 Rb4 57.98(5) 5_666 . Rb4 Au1 Rb4 57.98(5) 5_656 . Ga5 Au2 Ga5 62.80(7) 8_666 2 Ga5 Au2 Ga5 152.29(6) 8_666 . Ga5 Au2 Ga5 109.76(4) 2 . Ga5 Au2 Ga5 109.76(4) 8_666 7_565 Ga5 Au2 Ga5 152.29(6) 2 7_565 Ga5 Au2 Ga5 63.37(8) . 7_565 Ga5 Au2 Au3 58.66(5) 8_666 . Ga5 Au2 Au3 58.66(5) 2 . Ga5 Au2 Au3 143.18(5) . . Ga5 Au2 Au3 143.18(5) 7_565 . Ga5 Au2 Au1 143.87(4) 8_666 . Ga5 Au2 Au1 143.87(4) 2 . Ga5 Au2 Au1 58.02(4) . . Ga5 Au2 Au1 58.02(4) 7_565 . Au3 Au2 Au1 108.67(4) . . Ga5 Au2 Au1 114.13(5) 8_666 2 Ga5 Au2 Au1 56.36(4) 2 2 Ga5 Au2 Au1 53.45(4) . 2 Ga5 Au2 Au1 112.02(6) 7_565 2 Au3 Au2 Au1 104.13(3) . 2 Au1 Au2 Au1 101.60(2) . 2 Ga5 Au2 Au1 56.36(4) 8_666 2_565 Ga5 Au2 Au1 114.13(5) 2 2_565 Ga5 Au2 Au1 112.02(6) . 2_565 Ga5 Au2 Au1 53.45(4) 7_565 2_565 Au3 Au2 Au1 104.13(3) . 2_565 Au1 Au2 Au1 101.60(2) . 2_565 Au1 Au2 Au1 135.00(5) 2 2_565 Ga5 Au2 Rb4 76.72(6) 8_666 6_557 Ga5 Au2 Rb4 76.72(6) 2 6_557 Ga5 Au2 Rb4 75.58(6) . 6_557 Ga5 Au2 Rb4 75.58(6) 7_565 6_557 Au3 Au2 Rb4 126.85(5) . 6_557 Au1 Au2 Rb4 124.48(6) . 6_557 Au1 Au2 Rb4 67.53(3) 2 6_557 Au1 Au2 Rb4 67.53(3) 2_565 6_557 Ga5 Au2 Rb4 76.42(5) 8_666 5_666 Ga5 Au2 Rb4 124.19(7) 2 5_666 Ga5 Au2 Rb4 123.14(6) . 5_666 Ga5 Au2 Rb4 75.13(6) 7_565 5_666 Au3 Au2 Rb4 68.21(5) . 5_666 Au1 Au2 Rb4 67.65(4) . 5_666 Au1 Au2 Rb4 162.23(5) 2 5_666 Au1 Au2 Rb4 62.58(4) 2_565 5_666 Rb4 Au2 Rb4 130.10(4) 6_557 5_666 Ga5 Au2 Rb4 124.19(7) 8_666 5_656 Ga5 Au2 Rb4 76.42(5) 2 5_656 Ga5 Au2 Rb4 75.13(6) . 5_656 Ga5 Au2 Rb4 123.14(6) 7_565 5_656 Au3 Au2 Rb4 68.21(5) . 5_656 Au1 Au2 Rb4 67.65(4) . 5_656 Au1 Au2 Rb4 62.58(4) 2 5_656 Au1 Au2 Rb4 162.23(5) 2_565 5_656 Rb4 Au2 Rb4 130.10(4) 6_557 5_656 Rb4 Au2 Rb4 99.75(7) 5_666 5_656 Ga5 Au3 Ga5 66.24(8) 4_556 6_657 Ga5 Au3 Ga5 156.76(4) 4_556 2 Ga5 Au3 Ga5 111.21(5) 6_657 2 Ga5 Au3 Ga5 111.21(5) 4_556 8_666 Ga5 Au3 Ga5 156.76(4) 6_657 8_666 Ga5 Au3 Ga5 61.31(8) 2 8_666 Ga5 Au3 Au2 140.42(4) 4_556 . Ga5 Au3 Au2 140.42(4) 6_657 . Ga5 Au3 Au2 56.70(5) 2 . Ga5 Au3 Au2 56.70(5) 8_666 . Ga5 Au3 Au3 57.94(5) 4_556 5_667 Ga5 Au3 Au3 119.26(6) 6_657 5_667 Ga5 Au3 Au3 110.70(6) 2 5_667 Ga5 Au3 Au3 53.27(5) 8_666 5_667 Au2 Au3 Au3 99.41(4) . 5_667 Ga5 Au3 Au3 119.26(6) 4_556 5_657 Ga5 Au3 Au3 57.94(5) 6_657 5_657 Ga5 Au3 Au3 53.27(5) 2 5_657 Ga5 Au3 Au3 110.70(6) 8_666 5_657 Au2 Au3 Au3 99.41(4) . 5_657 Au3 Au3 Au3 137.86(6) 5_667 5_657 Ga5 Au3 Rb4 80.08(6) 4_556 1_556 Ga5 Au3 Rb4 80.08(6) 6_657 1_556 Ga5 Au3 Rb4 76.77(6) 2 1_556 Ga5 Au3 Rb4 76.77(6) 8_666 1_556 Au2 Au3 Rb4 124.91(6) . 1_556 Au3 Au3 Rb4 69.14(3) 5_667 1_556 Au3 Au3 Rb4 69.14(3) 5_657 1_556 Ga5 Au3 Rb4 123.81(6) 4_556 5_656 Ga5 Au3 Rb4 74.66(6) 6_657 5_656 Ga5 Au3 Rb4 74.63(5) 2 5_656 Ga5 Au3 Rb4 120.06(7) 8_666 5_656 Au2 Au3 Rb4 65.82(5) . 5_656 Au3 Au3 Rb4 159.02(5) 5_667 5_656 Au3 Au3 Rb4 62.07(4) 5_657 5_656 Rb4 Au3 Rb4 131.21(3) 1_556 5_656 Ga5 Au3 Rb4 74.66(6) 4_556 5_666 Ga5 Au3 Rb4 123.81(6) 6_657 5_666 Ga5 Au3 Rb4 120.06(7) 2 5_666 Ga5 Au3 Rb4 74.63(5) 8_666 5_666 Au2 Au3 Rb4 65.82(5) . 5_666 Au3 Au3 Rb4 62.07(4) 5_667 5_666 Au3 Au3 Rb4 159.02(5) 5_657 5_666 Rb4 Au3 Rb4 131.21(3) 1_556 5_666 Rb4 Au3 Rb4 97.39(6) 5_656 5_666 Ga5 Au3 Rb4 72.05(5) 4_556 . Ga5 Au3 Rb4 72.05(5) 6_657 . Ga5 Au3 Rb4 130.40(5) 2 . Ga5 Au3 Rb4 130.40(5) 8_666 . Au2 Au3 Rb4 88.55(5) . . Au3 Au3 Rb4 108.92(3) 5_667 . Au3 Au3 Rb4 108.92(3) 5_657 . Rb4 Au3 Rb4 146.54(9) 1_556 . Rb4 Au3 Rb4 58.14(5) 5_656 . Rb4 Au3 Rb4 58.14(5) 5_666 . Au1 Rb4 Au3 71.55(5) 6_656 1_554 Au1 Rb4 Au2 71.60(6) 6_656 6_657 Au3 Rb4 Au2 143.14(9) 1_554 6_657 Au1 Rb4 Au2 49.89(4) 6_656 5_666 Au3 Rb4 Au2 77.31(4) 1_554 5_666 Au2 Rb4 Au2 79.18(5) 6_657 5_666 Au1 Rb4 Au2 49.89(4) 6_656 5_656 Au3 Rb4 Au2 77.31(4) 1_554 5_656 Au2 Rb4 Au2 79.18(5) 6_657 5_656 Au2 Rb4 Au2 99.75(7) 5_666 5_656 Au1 Rb4 Rb4 130.36(6) 6_656 5_656 Au3 Rb4 Rb4 101.65(9) 1_554 5_656 Au2 Rb4 Rb4 101.98(8) 6_657 5_656 Au2 Rb4 Rb4 178.84(12) 5_666 5_656 Au2 Rb4 Rb4 80.47(4) 5_656 5_656 Au1 Rb4 Rb4 130.36(6) 6_656 5_666 Au3 Rb4 Rb4 101.65(9) 1_554 5_666 Au2 Rb4 Rb4 101.98(8) 6_657 5_666 Au2 Rb4 Rb4 80.47(4) 5_666 5_666 Au2 Rb4 Rb4 178.84(12) 5_656 5_666 Rb4 Rb4 Rb4 99.29(13) 5_656 5_666 Au1 Rb4 Au1 78.92(5) 6_656 5_666 Au3 Rb4 Au1 122.20(4) 1_554 5_666 Au2 Rb4 Au1 49.12(3) 6_657 5_666 Au2 Rb4 Au1 46.25(3) 5_666 5_666 Au2 Rb4 Au1 117.68(8) 5_656 5_666 Rb4 Rb4 Au1 134.63(10) 5_656 5_666 Rb4 Rb4 Au1 63.29(5) 5_666 5_666 Au1 Rb4 Au1 78.92(5) 6_656 5_656 Au3 Rb4 Au1 122.20(4) 1_554 5_656 Au2 Rb4 Au1 49.12(3) 6_657 5_656 Au2 Rb4 Au1 117.68(8) 5_666 5_656 Au2 Rb4 Au1 46.25(3) 5_656 5_656 Rb4 Rb4 Au1 63.29(5) 5_656 5_656 Rb4 Rb4 Au1 134.63(10) 5_666 5_656 Au1 Rb4 Au1 98.20(7) 5_666 5_656 Au1 Rb4 Au3 80.15(5) 6_656 5_656 Au3 Rb4 Au3 48.79(3) 1_554 5_656 Au2 Rb4 Au3 123.43(5) 6_657 5_656 Au2 Rb4 Au3 116.98(7) 5_666 5_656 Au2 Rb4 Au3 45.96(3) 5_656 5_656 Rb4 Rb4 Au3 62.37(4) 5_656 5_656 Rb4 Rb4 Au3 132.93(12) 5_666 5_656 Au1 Rb4 Au3 159.06(8) 5_666 5_656 Au1 Rb4 Au3 78.36(2) 5_656 5_656 Au1 Rb4 Au3 80.15(5) 6_656 5_666 Au3 Rb4 Au3 48.79(3) 1_554 5_666 Au2 Rb4 Au3 123.43(5) 6_657 5_666 Au2 Rb4 Au3 45.96(3) 5_666 5_666 Au2 Rb4 Au3 116.98(7) 5_656 5_666 Rb4 Rb4 Au3 132.93(12) 5_656 5_666 Rb4 Rb4 Au3 62.37(4) 5_666 5_666 Au1 Rb4 Au3 78.36(2) 5_666 5_666 Au1 Rb4 Au3 159.06(8) 5_656 5_666 Au3 Rb4 Au3 97.39(6) 5_656 5_666 Au1 Rb4 Au3 141.92(8) 6_656 . Au3 Rb4 Au3 146.54(9) 1_554 . Au2 Rb4 Au3 70.32(5) 6_657 . Au2 Rb4 Au3 121.15(4) 5_666 . Au2 Rb4 Au3 121.15(4) 5_656 . Rb4 Rb4 Au3 59.49(6) 5_656 . Rb4 Rb4 Au3 59.49(6) 5_666 . Au1 Rb4 Au3 76.42(4) 5_666 . Au1 Rb4 Au3 76.42(4) 5_656 . Au3 Rb4 Au3 121.86(5) 5_656 . Au3 Rb4 Au3 121.86(5) 5_666 . Au3 Ga5 Au1 128.94(8) 6_557 2 Au3 Ga5 Au2 117.62(7) 6_557 2_554 Au1 Ga5 Au2 104.37(6) 2 2_554 Au3 Ga5 Au2 108.63(6) 6_557 . Au1 Ga5 Au2 70.16(5) 2 . Au2 Ga5 Au2 119.24(8) 2_554 . Au3 Ga5 Au1 102.15(6) 6_557 . Au1 Ga5 Au1 120.10(8) 2 . Au2 Ga5 Au1 68.57(5) 2_554 . Au2 Ga5 Au1 64.88(5) . . Au3 Ga5 Au3 68.79(5) 6_557 2_554 Au1 Ga5 Au3 108.95(6) 2 2_554 Au2 Ga5 Au3 64.64(5) 2_554 2_554 Au2 Ga5 Au3 176.09(9) . 2_554 Au1 Ga5 Au3 118.22(7) . 2_554 Au3 Ga5 Ga5 123.12(4) 6_557 7 Au1 Ga5 Ga5 57.50(4) 2 7 Au2 Ga5 Ga5 58.60(4) 2_554 7 Au2 Ga5 Ga5 121.68(4) . 7 Au1 Ga5 Ga5 121.33(4) . 7 Au3 Ga5 Ga5 59.35(4) 2_554 7 Au3 Ga5 Ga5 56.88(4) 6_557 7_565 Au1 Ga5 Ga5 122.50(4) 2 7_565 Au2 Ga5 Ga5 121.40(4) 2_554 7_565 Au2 Ga5 Ga5 58.32(4) . 7_565 Au1 Ga5 Ga5 58.67(4) . 7_565 Au3 Ga5 Ga5 120.65(4) 2_554 7_565 Ga5 Ga5 Ga5 180.00(8) 7 7_565 Au3 Ga5 Rb4 69.02(6) 6_557 6_557 Au1 Ga5 Rb4 65.99(5) 2 6_557 Au2 Ga5 Rb4 169.49(6) 2_554 6_557 Au2 Ga5 Rb4 62.70(5) . 6_557 Au1 Ga5 Rb4 119.28(6) . 6_557 Au3 Ga5 Rb4 113.41(7) 2_554 6_557 Ga5 Ga5 Rb4 111.16(3) 7 6_557 Ga5 Ga5 Rb4 68.84(3) 7_565 6_557 Au3 Ga5 Rb4 66.09(5) 6_557 2 Au1 Ga5 Rb4 69.37(6) 2 2 Au2 Ga5 Rb4 117.84(6) 2_554 2 Au2 Ga5 Rb4 115.68(7) . 2 Au1 Ga5 Rb4 168.06(7) . 2 Au3 Ga5 Rb4 60.75(6) 2_554 2 Ga5 Ga5 Rb4 69.29(3) 7 2 Ga5 Ga5 Rb4 110.71(3) 7_565 2 Rb4 Ga5 Rb4 55.92(5) 6_557 2 Au3 Ga5 Rb4 166.30(7) 6_557 5_656 Au1 Ga5 Rb4 61.02(5) 2 5_656 Au2 Ga5 Rb4 62.10(5) 2_554 5_656 Au2 Ga5 Rb4 63.77(5) . 5_656 Au1 Ga5 Rb4 64.55(5) . 5_656 Au3 Ga5 Rb4 119.37(6) 2_554 5_656 Ga5 Ga5 Rb4 69.36(3) 7 5_656 Ga5 Ga5 Rb4 110.64(3) 7_565 5_656 Rb4 Ga5 Rb4 113.60(7) 6_557 5_656 Rb4 Ga5 Rb4 127.05(5) 2 5_656 Au3 Ga5 Rb4 60.39(5) 6_557 6_556 Au1 Ga5 Rb4 167.12(6) 2 6_556 Au2 Ga5 Rb4 63.06(4) 2_554 6_556 Au2 Ga5 Rb4 117.47(6) . 6_556 Au1 Ga5 Rb4 59.71(5) . 6_556 Au3 Ga5 Rb4 64.17(5) 2_554 6_556 Ga5 Ga5 Rb4 110.67(3) 7 6_556 Ga5 Ga5 Rb4 69.33(3) 7_565 6_556 Rb4 Ga5 Rb4 126.29(6) 6_557 6_556 Rb4 Ga5 Rb4 112.90(6) 2 6_556 Rb4 Ga5 Rb4 111.68(7) 5_656 6_556 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Au1 Ga5 2.5776(18) 2_554 Au1 Ga5 2.5776(18) 8_665 Au1 Ga5 2.699(2) . Au1 Ga5 2.699(2) 7_565 Au1 Au2 2.8816(13) . Au1 Au2 3.0182(8) 2_554 Au1 Au2 3.0182(8) 2_564 Au1 Rb4 3.503(3) 6_556 Au1 Rb4 3.6891(19) 5_666 Au1 Rb4 3.6891(19) 5_656 Au1 Rb4 3.856(3) . Au2 Ga5 2.6581(19) 8_666 Au2 Ga5 2.6581(19) 2 Au2 Ga5 2.672(2) . Au2 Ga5 2.672(2) 7_565 Au2 Au3 2.8738(16) . Au2 Au1 3.0182(8) 2 Au2 Au1 3.0182(8) 2_565 Au2 Rb4 3.568(3) 6_557 Au2 Rb4 3.6468(19) 5_666 Au2 Rb4 3.6468(19) 5_656 Au3 Ga5 2.569(2) 4_556 Au3 Ga5 2.569(2) 6_657 Au3 Ga5 2.716(2) 2 Au3 Ga5 2.716(2) 8_666 Au3 Au3 2.9883(8) 5_667 Au3 Au3 2.9883(8) 5_657 Au3 Rb4 3.510(3) 1_556 Au3 Rb4 3.7119(18) 5_656 Au3 Rb4 3.7119(18) 5_666 Au3 Rb4 3.817(3) . Rb4 Au1 3.503(3) 6_656 Rb4 Au3 3.510(3) 1_554 Rb4 Au2 3.568(3) 6_657 Rb4 Au2 3.6468(19) 5_666 Rb4 Au2 3.6468(19) 5_656 Rb4 Rb4 3.659(4) 5_656 Rb4 Rb4 3.659(4) 5_666 Rb4 Au1 3.6891(19) 5_666 Rb4 Au1 3.6891(19) 5_656 Rb4 Au3 3.7119(17) 5_656 Rb4 Au3 3.7119(17) 5_666 Ga5 Au3 2.569(2) 6_557 Ga5 Au1 2.5776(18) 2 Ga5 Au2 2.6581(19) 2_554 Ga5 Au3 2.716(2) 2_554 Ga5 Ga5 2.770(3) 7 Ga5 Ga5 2.807(3) 7_565 Ga5 Rb4 3.889(3) 6_557 Ga5 Rb4 3.916(3) 2 Ga5 Rb4 3.929(3) 5_656 Ga5 Rb4 3.976(3) 6_556