Crystallography Open Database

Information card for entry 4332782

Preview

Coordinates	4332782.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Rh~2~(O~2~CR)~4~(H~2~O)~2~, R=CH~2~CH~2~Cl
Formula	C12 H18 Cl4 O10 Rh2
Calculated formula	C12 H18 Cl4 O10 Rh2
Title of publication	Substituent Effects in Five Oxo-Centered Trinuclear Rhodium(III) Clusters
Authors of publication	Houston, Jacqueline R.; Olmstead, Marilyn M.; Casey, William H.
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	19
Pages of publication	7799 - 7805
a	13.3174 ± 0.0017 Å
b	29.568 ± 0.004 Å
c	21.286 ± 0.003 Å
α	90°
β	90.295 ± 0.006°
γ	90°
Cell volume	8382 ± 2 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0709
Residual factor for significantly intense reflections	0.0587
Weighted residual factors for significantly intense reflections	0.1535
Weighted residual factors for all reflections included in the refinement	0.1653
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179430 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/27.	4332782.cif
98545	2014-01-30	cif/ Adding structures of 4332782 via cif-deposit CGI script.	4332782.cif