Crystallography Open Database

Information card for entry 4333312

Preview

Coordinates	4333312.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H16 N3 O6 Pb S
Calculated formula	C22 H16 N3 O6 Pb S
Title of publication	Syntheses, structures, and characterizations of four new lead(II) 5-sulfosalicylate complexes with both chelating and bridging neutral ligands.
Authors of publication	Fan, Sai-Rong; Zhu, Long-Guan
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	16
Pages of publication	6785 - 6793
a	10.0888 ± 0.0005 Å
b	10.3628 ± 0.0005 Å
c	10.7442 ± 0.0006 Å
α	88.834 ± 0.001°
β	88.418 ± 0.001°
γ	67.372 ± 0.001°
Cell volume	1036.37 ± 0.09 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0341
Residual factor for significantly intense reflections	0.0319
Weighted residual factors for significantly intense reflections	0.0692
Weighted residual factors for all reflections included in the refinement	0.07
Goodness-of-fit parameter for all reflections included in the refinement	1.111
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179436 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/33.	4333312.cif
116741	2014-06-13	cif/ Updating files of 4333312, 4333313, 4333314, 4333315 Original log message: Adding full bibliography for 4333312--4333315.cif.	4333312.cif
98923	2014-01-30	cif/ Adding structures of 4333312 via cif-deposit CGI script.	4333312.cif