Crystallography Open Database

Information card for entry 4335465

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Structure parameters

Formula	C50 H49 Co F24 N6 O9 Ru2
Calculated formula	C44 H35 Co F23.979 N6 O9 Ru2
Title of publication	Binuclear Ruthenium Complexes of a Neutral Radical Bridging Ligand. A New "Spin" on Mixed Valency
Authors of publication	Stephen D. J. McKinnon; Brian O. Patrick; A. B. P. Lever; Robin G. Hicks
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	8053 - 8066
a	14.2706 ± 0.0009 Å
b	23.201 ± 0.0017 Å
c	17.8901 ± 0.0013 Å
α	90°
β	102.025 ± 0.004°
γ	90°
Cell volume	5793.3 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1113
Residual factor for significantly intense reflections	0.0506
Weighted residual factors for significantly intense reflections	0.1183
Weighted residual factors for all reflections included in the refinement	0.1384
Goodness-of-fit parameter for all reflections included in the refinement	0.968
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181932 (current)	2016-04-07	hkl/4/ (antanas@echidna.ibt.lt) Adding svn headers to multiple entries in subrange 4/33.	4335465.cif 4335465.hkl
180708	2016-04-02	hkl/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4335465.cif 4335465.hkl
179457	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/54.	4335465.cif 4335465.hkl
101395	2014-02-13	cif/ hkl/ Adding structures of 4335465 via cif-deposit CGI script.	4335465.cif 4335465.hkl