data_4335469 _audit_creation_date 2013-06-03 _audit_creation_method ; Olex2 1.2 (compiled Apr 23 2013 17:59:47, GUI svn.r4466) ; loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 -2 0 67.28 2.48 0 -3 0 -1.18 0.89 0 -3 0 -1 0.33 0 -4 0 121.33 4.24 0 -4 0 106.05 6.43 0 -5 0 -0.06 0.63 0 -5 0 -0.34 0.45 0 -5 0 -0.11 1.07 0 -6 0 32.15 1.57 0 -6 0 29.29 1.81 0 -6 0 28.8 2.57 0 -7 0 -0.01 0.9 0 -7 0 0.33 0.6 0 -7 0 -0.53 1.47 0 -8 0 22.67 1.45 0 -8 0 18.66 2.69 0 -9 0 2.89 1.87 0 -10 0 4.72 1.94 1 -1 0 157.47 6.58 1 1 0 135.74 8.06 -1 1 0 157.89 6.62 -1 -1 0 145.19 8.08 -1 1 0 145.14 5.43 -1 1 0 156.55 5.33 1 -1 0 154.96 5.32 1 -1 0 141.58 5.41 -1 -1 0 153.67 6.73 1 -2 0 6.68 0.68 1 -2 0 7.02 0.49 1 2 0 5.66 0.96 -1 -2 0 5.11 0.92 1 -3 0 1.55 0.58 1 -3 0 1.96 0.42 -1 -3 0 0.63 1 1 -4 0 47.32 1.86 -1 -4 0 44.06 1.86 -1 -4 0 39.18 2.91 -1 -5 0 5.51 1.35 1 -5 0 6.02 0.87 1 -5 0 6.97 0.71 1 -5 0 6.42 1.32 -1 -5 0 7.67 0.73 1 -6 0 0.45 1.23 1 -6 0 0.82 0.53 1 -6 0 0.43 0.74 -1 -6 0 0.92 0.54 -1 -6 0 0.65 1.28 -1 -7 0 26.15 2.72 -1 -7 0 23.82 1.5 1 -7 0 27.93 1.53 -1 -7 0 23.74 1.83 1 -7 0 26.59 2.68 1 -7 0 23.54 1.84 1 -8 0 4.39 1.85 1 -8 0 4.29 0.85 -1 -8 0 4.63 0.83 -1 -8 0 7.17 2.03 -1 -9 0 9.5 2.17 1 -9 0 12.47 2.29 1 -10 0 7.63 2.02 -1 -10 0 7.15 2.09 2 0 0 160.87 6.62 -2 0 0 157.96 6.6 -2 -1 0 184.99 7.54 -2 1 0 182.82 6.57 2 1 0 167.23 9.73 -2 1 0 187.38 7.52 -2 1 0 180.77 6.45 2 -1 0 182.33 6.44 2 -1 0 187.01 7.54 2 -1 0 182.19 6.55 2 2 0 147.87 6.44 -2 2 0 150.62 6.37 2 -2 0 160.53 6.36 -2 -2 0 158.45 6.37 -2 -2 0 140.38 8.28 -2 2 0 157.49 5.4 -2 2 0 152.97 5.61 2 -2 0 154.82 5.39 2 -2 0 146.47 5.58 2 2 0 143.19 8.3 -2 2 0 162.69 6.37 2 -3 0 12 0.98 -2 -3 0 10.17 1.41 2 -3 0 13.28 0.76 2 -3 0 13.42 0.76 2 3 0 10.43 1.53 -2 -3 0 12.08 0.69 2 -4 0 19.45 1.25 2 4 0 17.99 1.85 -2 -4 0 18.87 1.89 2 -4 0 20.97 1.05 -2 -5 0 21.27 1.2 -2 -5 0 17.93 2.07 2 -5 0 18.73 1.35 2 -5 0 23.13 1.19 -2 -6 0 4.75 0.71 2 -6 0 3.82 0.86 2 -6 0 5.67 0.71 -2 -6 0 3.37 1.47 2 -7 0 28.23 1.56 -2 -7 0 25.46 2.76 2 -7 0 27.71 1.9 2 -7 0 24.28 2.73 -2 -7 0 27.24 1.58 -2 -8 0 0.18 0.62 2 -8 0 -0.63 1.66 -2 -8 0 1.18 1.82 2 -8 0 -0.69 0.63 2 -9 0 26.68 3.02 -2 -9 0 26.9 3.08 -2 -10 0 5.21 2.01 2 -10 0 6.15 1.97 -3 0 0 0.07 0.24 3 0 0 0.04 0.26 3 -1 0 19.2 1.02 -3 1 0 18.62 0.88 -3 -1 0 18.56 0.98 -3 1 0 18.93 0.73 3 1 0 18.11 0.98 -3 1 0 17.73 0.98 -3 -2 0 981.62 38.81 3 -2 0 1000 38.82 3 2 0 913.47 50.34 -3 -2 0 904.64 50.31 3 -2 0 962.4 33.85 -3 2 0 916.7 33.87 -3 2 0 993.61 38.76 3 -2 0 968.63 33.12 -3 2 0 973.41 33.15 -3 3 0 1.56 0.36 -3 3 0 2.33 0.33 -3 -3 0 1.81 1.08 -3 3 0 2.03 0.58 3 3 0 0.74 1.03 3 -3 0 2.51 0.43 3 -3 0 1.71 0.55 -3 3 0 2.42 0.4 -3 -3 0 1.99 0.36 3 -3 0 1.74 0.38 3 -4 0 23 1.14 -3 -4 0 24.08 1.14 3 -4 0 20.52 1.34 3 4 0 21.68 2.09 -3 -4 0 20.19 2.05 3 -4 0 22.84 1.21 3 -5 0 8.59 0.96 -3 -5 0 8.33 0.67 3 5 0 7.67 1.53 3 -5 0 9.57 0.8 3 -5 0 8.59 0.76 -3 -5 0 8.16 0.79 -3 -5 0 7.22 1.5 3 -6 0 59.66 2.58 -3 -6 0 53.82 3.94 -3 -6 0 56.34 2.47 3 -6 0 55.67 2.72 3 -6 0 59.22 2.46 -3 -7 0 7.1 1.82 3 -7 0 6.12 1.12 -3 -7 0 5.17 0.83 3 -7 0 5.95 0.86 3 -8 0 3.37 0.84 -3 -8 0 4.86 0.85 -3 -8 0 4.8 1.98 3 -8 0 4.68 1.88 -3 -9 0 2.14 1.77 3 -9 0 0.42 1.69 3 -10 0 3.56 1.74 4 0 0 140.32 6.01 -4 0 0 147.08 6 4 -1 0 188.51 8.08 -4 1 0 194.74 8.06 -4 -1 0 202.73 8.08 4 1 0 195.17 8.08 -4 2 0 40.41 1.86 -4 2 0 36.22 1.7 -4 -2 0 39.84 1.87 4 -2 0 39.74 1.92 -4 2 0 39.77 1.51 4 -3 0 1.03 0.53 -4 3 0 1.19 0.42 -4 3 0 1.35 0.34 -4 -3 0 1.57 1.03 4 -3 0 0.47 0.43 4 3 0 0.91 1.05 -4 3 0 1.2 0.54 -4 -3 0 0.83 0.38 -4 3 0 1.13 0.34 4 -3 0 1.13 0.35 4 3 0 0.7 0.35 -4 -4 0 153.73 9.16 4 -4 0 170.66 5.94 -4 4 0 160.37 6.24 -4 4 0 160.01 6.81 4 -4 0 166.21 6.89 -4 4 0 179.68 6.82 -4 -4 0 172.83 6.85 4 -4 0 157.1 6.2 4 4 0 160.54 9.23 4 -5 0 16.76 1.32 -4 -5 0 12.86 2.02 4 -5 0 16.11 1.08 4 -5 0 17.6 1.03 4 5 0 14.83 1.99 -4 -5 0 15.94 1 4 -6 0 5.61 0.99 -4 -6 0 7.87 1.7 4 6 0 7.62 1.68 -4 -6 0 6.5 0.82 4 -6 0 6.76 0.71 4 -6 0 5.44 0.8 -4 -6 0 6.6 0.72 4 -7 0 3.9 0.66 -4 -7 0 4.63 1.87 4 -7 0 5.28 0.81 -4 -7 0 5.33 0.82 4 -7 0 5.53 1.08 -4 -8 0 2.44 1.99 -4 -8 0 2.07 0.76 4 -8 0 0.82 0.76 4 -8 0 2.43 0.65 -4 -9 0 2 1.8 4 -9 0 1.3 1.7 4 -10 0 10.54 2.22 5 0 0 0.35 0.51 -5 0 0 0.64 0.45 -5 1 0 328.35 13.23 5 -1 0 321.84 13.26 5 1 0 325.07 13.25 -5 -1 0 317.96 13.22 -5 2 0 0.11 0.39 5 2 0 0.24 0.45 -5 -2 0 1.11 0.45 5 -2 0 0.46 0.51 5 2 0 1.69 1.06 -5 2 0 0.86 0.49 -5 2 0 0.97 0.27 5 3 0 162.23 9.43 5 -3 0 174.16 6.34 -5 -3 0 179.39 7.13 5 -3 0 171.37 6.04 -5 3 0 179.56 7.1 -5 3 0 168.68 6.36 5 3 0 153.17 7.07 5 -3 0 172.67 7.17 -5 3 0 174.27 6.07 -5 4 0 94.04 4 -5 4 0 88.86 3.77 -5 -4 0 88.02 5.53 -5 4 0 98.98 3.98 5 -4 0 91.04 3.47 5 -4 0 94.55 4.09 5 4 0 88.93 5.57 -5 -4 0 99.79 4.05 5 4 0 90.3 3.96 5 -4 0 93.6 3.73 5 -5 0 76.51 3.39 -5 -5 0 66.07 4.69 5 5 0 69.32 4.76 -5 5 0 74.07 3.26 -5 5 0 81.52 3.21 5 -5 0 75.05 2.94 -5 -5 0 77.31 3.31 5 -5 0 73.73 3.21 5 -6 0 13.06 1.14 5 -6 0 16.46 1.43 5 -6 0 14.81 1.1 -5 -6 0 13.45 1.08 -5 -6 0 14.3 1.05 -5 -6 0 14.55 2.1 5 6 0 15.5 2.22 5 -7 0 25.42 1.87 5 -7 0 26.96 1.57 5 -7 0 25.66 1.48 -5 -7 0 24.4 1.53 -5 -7 0 25.76 1.44 -5 -7 0 23.47 2.8 5 -8 0 12.23 1.21 5 -8 0 14.11 1.22 -5 -8 0 13.57 1.03 -5 -8 0 13.86 2.47 5 -9 0 -0.4 0.59 -5 -9 0 1.24 1.78 6 0 0 114.76 5.03 -6 0 0 117.14 5 6 -1 0 4.29 0.67 -6 1 0 4.31 0.58 -6 -1 0 4.69 0.62 6 1 0 3.86 0.64 6 -2 0 -0.35 0.47 6 2 0 0.2 0.47 -6 2 0 -0.02 0.46 -6 2 0 0.33 0.24 -6 2 0 -0.36 0.37 -6 -2 0 -0.14 0.41 -6 3 0 16.68 1.15 -6 3 0 17.91 1.17 6 -3 0 15.32 1.23 6 3 0 16.72 1.92 -6 3 0 17.44 0.85 -6 -3 0 16.26 1.15 6 -4 0 103.3 3.93 -6 4 0 110.72 4.65 6 4 0 109.65 4.6 -6 4 0 114.14 4.61 6 -4 0 99.87 4.19 6 -4 0 104.71 4.7 -6 4 0 105.55 4.28 -6 -4 0 110.17 4.65 6 4 0 104.4 6.36 -6 4 0 107.97 3.97 -6 5 0 55.17 2.52 6 -5 0 54.26 2.26 6 -5 0 51.73 2.66 -6 -5 0 55.27 3.85 -6 5 0 58.66 2.51 6 -5 0 52.47 2.51 -6 5 0 54 2.61 6 5 0 54.67 3.91 -6 -5 0 57.06 2.61 -6 -6 0 6.91 0.76 -6 -6 0 7.58 1.85 6 -6 0 5.85 0.84 6 -6 0 7.23 0.81 -6 -6 0 7.76 0.89 6 6 0 6.54 1.86 6 -6 0 6.83 1.04 6 -7 0 2.54 0.75 6 7 0 3.73 1.89 6 -7 0 3.02 0.72 -6 -7 0 3.02 0.77 -6 -7 0 2.62 0.61 -6 -7 0 3.21 1.84 6 -8 0 0.76 0.7 -6 -8 0 0.23 1.91 -6 -8 0 0.49 0.52 6 -8 0 -1.15 0.66 6 -9 0 10.22 1.16 -6 -9 0 10.31 0.97 -6 -9 0 10.77 2.33 6 -10 0 0.72 0.71 -7 0 0 0.27 0.45 7 0 0 -0.52 0.51 7 -1 0 12.53 1.15 7 1 0 13.22 1.09 -7 -1 0 12.3 1.04 -7 1 0 12.31 1.04 -7 -2 0 85.57 3.75 -7 2 0 86.23 3.75 -7 2 0 85.09 3.01 7 2 0 78.11 3.73 7 -2 0 80.27 3.8 -7 2 0 84.59 3.29 -7 -3 0 21.46 1.38 -7 3 0 21.73 1.33 -7 3 0 21.91 1 7 -3 0 20.82 1.45 7 3 0 20.78 2.14 -7 3 0 22.1 1.37 7 3 0 20.89 1.37 -7 4 0 1.88 0.5 -7 4 0 2.25 0.45 -7 4 0 2.73 0.72 -7 -4 0 2.57 0.57 7 -4 0 2.19 0.66 7 -4 0 2.95 0.71 7 4 0 2.53 1.4 7 4 0 2.08 0.57 7 5 0 7.69 0.78 -7 5 0 7.34 0.81 7 -5 0 6.57 0.9 -7 -5 0 9.29 0.99 7 5 0 10.88 1.86 7 -5 0 8.08 0.99 -7 5 0 8.63 1.08 -7 5 0 10.04 0.92 -7 6 0 29.07 1.52 7 -6 0 26.4 1.76 7 6 0 27.8 2.87 7 -6 0 28.23 1.89 7 -6 0 26.87 1.44 -7 -6 0 27.77 1.67 -7 6 0 27.92 1.89 7 7 0 7.84 2.14 7 -7 0 7.33 1.01 -7 -7 0 8.92 1.06 -7 -7 0 8.19 2.17 7 -7 0 8.03 0.91 -7 -7 0 7.79 1.02 7 -8 0 -0.87 0.71 -7 -8 0 0.07 1.9 -7 -8 0 -0.01 0.53 7 -8 0 -0.57 0.66 7 8 0 1.92 1.78 -7 -9 0 7.24 2.31 7 -9 0 12.27 1.26 -7 -9 0 10.23 1.05 7 -10 0 4.1 0.88 8 0 0 1.65 0.64 -8 0 0 1.13 0.54 -8 -1 0 23.19 1.45 8 -1 0 20.55 1.49 -8 1 0 22.21 1.43 8 1 0 22.13 1.47 8 -2 0 62.59 3.13 -8 2 0 64.9 2.68 8 2 0 64.18 3.08 -8 2 0 65.18 2.37 -8 2 0 66.88 3.08 -8 -2 0 64.45 3.07 8 -3 0 65.8 3.29 8 3 0 66.5 3.22 -8 3 0 68.62 2.56 -8 3 0 69.38 2.91 8 3 0 67.1 4.42 -8 -3 0 70.36 3.23 -8 3 0 69.97 3.2 -8 4 0 3.14 0.48 -8 4 0 2.03 0.63 -8 4 0 2.56 0.74 8 4 0 2.65 1.51 -8 -4 0 2.38 0.63 -8 4 0 2.28 0.58 8 -4 0 2.2 0.73 8 5 0 17.61 1.35 -8 -5 0 21.51 1.44 8 -5 0 19.76 1.44 -8 5 0 20.9 1.34 8 5 0 19.65 2.57 -8 5 0 18.03 1.48 8 -5 0 20.81 1.56 -8 5 0 18.92 1.45 8 -6 0 15.02 1.41 8 6 0 15.79 2.38 -8 6 0 13.83 1.17 -8 -6 0 14.96 1.3 8 -6 0 15.01 1.4 -8 6 0 16.14 1.51 8 7 0 19.17 2.83 -8 -7 0 18.98 1.42 8 -7 0 15.08 1.49 -8 -7 0 16.61 1.33 8 8 0 3.09 1.92 -8 -8 0 0.45 0.62 8 -8 0 0.14 0.77 8 -9 0 12.01 1.35 -8 -9 0 9.54 1.11 8 -10 0 9.7 1.14 9 0 0 -0.02 0.62 -9 0 0 -0.52 0.46 9 1 0 20.41 1.54 9 -1 0 21.07 1.55 -9 1 0 20.82 1.5 -9 -1 0 22.37 1.51 -9 2 0 1.63 0.29 -9 -2 0 0.44 0.57 -9 2 0 1.15 0.58 9 2 0 0.12 0.67 9 -2 0 -0.01 0.71 -9 3 0 23.41 1.42 9 3 0 20.57 1.55 -9 -3 0 22.31 1.49 -9 3 0 22.82 1.01 -9 3 0 22.4 1.49 9 3 0 20.88 2.38 9 -3 0 19.83 1.57 9 4 0 11.5 1.93 9 -4 0 8.02 1.03 -9 -4 0 8.49 0.93 -9 4 0 8.98 0.7 -9 4 0 9.01 1.02 -9 4 0 10.34 1.07 -9 4 0 9.09 1.07 9 5 0 0.07 0.62 9 5 0 -1.71 1.59 9 -5 0 -0.56 0.74 -9 -5 0 0.08 0.58 -9 5 0 -0.2 0.66 -9 5 0 -0.5 0.79 -9 6 0 0.68 0.95 9 -6 0 -1.09 0.73 -9 6 0 -1.52 0.62 -9 -6 0 -0.39 0.6 9 6 0 -0.62 1.71 9 -6 0 -1.2 0.88 -9 -7 0 6.6 0.9 -9 7 0 6.76 1.29 9 -7 0 5.39 1.06 -9 -7 0 7.31 1 9 7 0 7.79 2.21 9 8 0 1.48 1.88 -9 -8 0 -0.06 0.61 9 -8 0 -0.41 0.78 9 -9 0 3.05 0.94 9 9 0 6.11 2.09 -10 0 0 125.32 5.4 10 0 0 115.61 5.43 -10 1 0 73.5 3.45 -10 -1 0 71.75 3.44 10 1 0 69.61 3.49 10 -1 0 70.04 3.52 -10 -2 0 6.03 0.83 -10 2 0 6.85 0.83 10 -2 0 5.53 0.96 10 2 0 6.44 0.92 -10 3 0 6.84 0.86 -10 3 0 8.8 0.94 -10 3 0 7.58 0.56 10 3 0 6.63 0.94 10 3 0 7.94 1.81 10 -3 0 8 1.05 -10 -3 0 6.96 0.88 -10 -4 0 38.82 2.21 -10 4 0 39.76 1.65 -10 4 0 38.01 2.08 -10 4 0 38.62 2.17 10 -4 0 36.45 2.32 10 4 0 37.86 2.26 10 4 0 40.13 3.41 -10 4 0 39.04 2.31 10 -5 0 29.65 2.06 -10 5 0 28.88 1.92 10 5 0 29.17 1.9 -10 -5 0 33.47 2 10 5 0 34.04 3.19 -10 6 0 -0.82 0.68 10 6 0 -0.28 1.88 -10 -6 0 0.51 0.66 -10 6 0 0.52 0.93 10 -6 0 -0.76 0.81 10 6 0 -1.13 0.65 10 7 0 5.27 2.19 10 -7 0 4.27 1.03 -10 -7 0 4.32 0.83 -10 7 0 4.42 1.18 -10 7 0 2.9 0.66 -10 -7 0 2.7 0.82 10 -8 0 5.83 1.09 -10 -8 0 5.78 0.91 10 8 0 9.59 2.26 10 9 0 12.3 2.51 10 -9 0 7.68 1.19 11 0 0 -0.26 0.71 -11 0 0 0.06 0.55 -11 1 0 2.3 0.69 -11 -1 0 1.53 0.67 11 1 0 0.69 0.76 11 -1 0 1.07 0.82 -11 -2 0 7.5 0.91 -11 2 0 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