Crystallography Open Database

Information card for entry 4337966

Preview

Coordinates	4337966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H33 Cl3 Ga P
Calculated formula	C18 H33 Cl3 Ga P
SMILES	[Ga](Cl)(Cl)(Cl)[P](C1CCCCC1)(C1CCCCC1)C1CCCCC1
Title of publication	Azidophosphenium Cations: Versatile Reagents in Inorganic Synthesis.
Authors of publication	Hering, Christian; Hertrich, Maximilian; Schulz, Axel; Villinger, Alexander
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	7
Pages of publication	3880
a	8.6326 ± 0.0004 Å
b	21.8911 ± 0.0009 Å
c	11.364 ± 0.0005 Å
α	90°
β	91.592 ± 0.001°
γ	90°
Cell volume	2146.71 ± 0.16 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0555
Residual factor for significantly intense reflections	0.0335
Weighted residual factors for significantly intense reflections	0.0669
Weighted residual factors for all reflections included in the refinement	0.0706
Goodness-of-fit parameter for all reflections included in the refinement	0.938
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179482 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/79.	4337966.cif
109930	2014-04-17	cif/ Updating files of 4337958, 4337959, 4337960, 4337961, 4337962, 4337963, 4337964, 4337965, 4337966, 4337967 Original log message: Adding full bibliography for 4337958--4337967.cif.	4337966.cif
108508	2014-04-02	cif/ Adding structures of 4337958, 4337959, 4337960, 4337961, 4337962, 4337963, 4337964, 4337965, 4337966, 4337967 via cif-deposit CGI script.	4337966.cif