Crystallography Open Database

Information card for entry 4338445

Preview

Coordinates	4338445.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H29 K3 Mn3 Na O50 Si W9
Calculated formula	K2.8 Mn3 Na1.25 O49 Si W9
Title of publication	Synthesis and characterization of multinuclear manganese-containing tungstosilicates.
Authors of publication	Al-Oweini, Rami; Bassil, Bassem S.; Friedl, Jochen; Kottisch, Veronika; Ibrahim, Masooma; Asano, Marie; Keita, Bineta; Novitchi, Ghenadie; Lan, Yanhua; Powell, Annie; Stimming, Ulrich; Kortz, Ulrich
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	11
Pages of publication	5663 - 5673
a	21.1404 ± 0.0014 Å
b	21.0962 ± 0.0012 Å
c	23.9958 ± 0.0014 Å
α	90°
β	105.286 ± 0.003°
γ	90°
Cell volume	10323.1 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0704
Residual factor for significantly intense reflections	0.057
Weighted residual factors for significantly intense reflections	0.1526
Weighted residual factors for all reflections included in the refinement	0.1603
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179487 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/84.	4338445.cif
115719	2014-06-05	cif/ Updating files of 4338445, 4338446, 4338447, 4338448, 4338449 Original log message: Adding full bibliography for 4338445--4338449.cif.	4338445.cif
113976	2014-05-20	cif/ Adding structures of 4338445 via cif-deposit CGI script.	4338445.cif