#------------------------------------------------------------------------------ #$Date: 2017-09-04 16:43:19 +0300 (Mon, 04 Sep 2017) $ #$Revision: 200152 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/34/59/4345979.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4345979 loop_ _publ_author_name 'Yang, Mengxi' 'Gabba\"i, Fran\,cois P' _publ_section_title ; Synthesis and Properties of Triarylhalostibonium Cations. ; _journal_issue 15 _journal_name_full 'Inorganic chemistry' _journal_page_first 8644 _journal_page_last 8650 _journal_paper_doi 10.1021/acs.inorgchem.7b00293 _journal_volume 56 _journal_year 2017 _chemical_formula_sum 'C27 H33 F2 Sb' _chemical_formula_weight 517.28 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 104.478(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.2678(8) _cell_length_b 12.7918(10) _cell_length_c 18.0561(17) _cell_measurement_reflns_used 9924 _cell_measurement_temperature 110(2) _cell_measurement_theta_max 27.49 _cell_measurement_theta_min 2.33 _cell_volume 2296.2(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 110(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0370 _diffrn_reflns_av_unetI/netI 0.0203 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 21340 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.526 _diffrn_reflns_theta_min 2.330 _exptl_absorpt_coefficient_mu 1.229 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6569 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour colorless _exptl_crystal_description block _exptl_crystal_F_000 1056 _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.423 _refine_diff_density_min -0.516 _refine_diff_density_rms 0.065 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.098 _refine_ls_hydrogen_treatment riding _refine_ls_matrix_type full _refine_ls_number_parameters 143 _refine_ls_number_reflns 2639 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.098 _refine_ls_R_factor_all 0.0190 _refine_ls_R_factor_gt 0.0183 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0188P)^2^+3.9774P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0485 _refine_ls_wR_factor_ref 0.0489 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2555 _reflns_number_total 2639 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ic7b00293_si_003.cif _cod_data_source_block Mes3SbF2 _cod_database_code 4345979 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.757 _shelx_estimated_absorpt_t_max 0.887 _shelx_res_file ; y.res created by SHELXL-2014/7 TITL y in Cc New: C2/c CELL 0.71073 10.2678 12.7918 18.0561 90.000 104.478 90.000 ZERR 4 0.0008 0.0010 0.0017 0.000 0.003 0.000 LATT 7 SYMM - X , Y , 0.50000 - Z SFAC C H F Sb UNIT 108 132 8 4 LIST 4 L.S. 5 FMAP 2 PLAN 20 ACTA TEMP -163.15 SIZE 0.24 0.15 0.10 BOND $H CONF WGHT 0.018800 3.977400 FVAR 0.07881 SB1 4 0.000000 0.409510 0.250000 10.50000 0.01239 0.01030 = 0.01557 0.00000 0.00558 0.00000 C1 1 0.029154 0.323389 0.353508 11.00000 0.01413 0.01401 = 0.01655 0.00030 0.00462 -0.00050 F1 3 -0.196462 0.410138 0.240735 11.00000 0.01321 0.01933 = 0.02384 0.00019 0.00684 -0.00063 C2 1 -0.032228 0.356874 0.410529 11.00000 0.01452 0.01443 = 0.01906 -0.00218 0.00469 -0.00007 C3 1 -0.019167 0.294613 0.475463 11.00000 0.02039 0.01956 = 0.01688 -0.00173 0.00734 0.00099 AFIX 43 H3 2 -0.059734 0.317097 0.514590 11.00000 -1.20000 AFIX 0 C4 1 0.051478 0.200527 0.484730 11.00000 0.02141 0.01987 = 0.01825 0.00240 0.00417 0.00151 C7 1 -0.113534 0.456515 0.405575 11.00000 0.02040 0.01648 = 0.02040 -0.00229 0.00891 0.00354 AFIX 137 H7A 2 -0.066921 0.513247 0.386285 11.00000 -1.50000 H7B 2 -0.123856 0.474841 0.456500 11.00000 -1.50000 H7C 2 -0.202454 0.445953 0.370734 11.00000 -1.50000 AFIX 0 C6 1 0.104011 0.229667 0.362372 11.00000 0.01583 0.01532 = 0.02062 -0.00085 0.00619 0.00046 C5 1 0.112569 0.170385 0.428021 11.00000 0.02056 0.01636 = 0.02309 0.00221 0.00600 0.00429 AFIX 43 H5 2 0.162167 0.106920 0.434100 11.00000 -1.20000 AFIX 0 C8 1 0.061295 0.133959 0.554560 11.00000 0.04111 0.02999 = 0.02142 0.00777 0.01156 0.01163 AFIX 137 H8A 2 0.084498 0.062183 0.543826 11.00000 -1.50000 H8B 2 -0.025323 0.134210 0.568154 11.00000 -1.50000 H8C 2 0.131108 0.162102 0.597207 11.00000 -1.50000 AFIX 0 C10 1 0.000000 0.575691 0.250000 10.50000 0.01571 0.01222 = 0.01715 0.00000 0.00731 0.00000 C9 1 0.175482 0.188516 0.304655 11.00000 0.02601 0.01667 = 0.02701 0.00245 0.01409 0.00809 AFIX 137 H9A 2 0.117943 0.197980 0.252918 11.00000 -1.50000 H9B 2 0.195012 0.114003 0.314028 11.00000 -1.50000 H9C 2 0.259838 0.226882 0.309592 11.00000 -1.50000 AFIX 0 C11 1 0.095681 0.630512 0.305994 11.00000 0.01396 0.01589 = 0.01769 0.00024 0.00755 -0.00022 C12 1 0.093000 0.739751 0.304721 11.00000 0.01588 0.01522 = 0.02132 -0.00363 0.00896 -0.00292 AFIX 43 H12 2 0.157116 0.776856 0.342663 11.00000 -1.20000 AFIX 0 C13 1 0.000000 0.796349 0.250000 10.50000 0.01677 0.01297 = 0.02534 0.00000 0.01327 0.00000 C14 1 0.203908 0.578519 0.367173 11.00000 0.01735 0.01863 = 0.02001 -0.00074 0.00146 -0.00035 AFIX 137 H14A 2 0.276537 0.554656 0.344927 11.00000 -1.50000 H14B 2 0.165592 0.518496 0.388041 11.00000 -1.50000 H14C 2 0.239782 0.628686 0.408224 11.00000 -1.50000 AFIX 0 C15 1 0.000000 0.913915 0.250000 10.50000 0.01989 0.01308 = 0.03289 0.00000 0.01102 0.00000 AFIX 137 H15A 2 0.026334 0.939452 0.204670 10.50000 -1.50000 H15B 2 0.064020 0.939452 0.296196 10.50000 -1.50000 H15C 2 -0.090354 0.939452 0.249134 10.50000 -1.50000 AFIX 0 HKLF 4 REM y in Cc New: C2/c REM R1 = 0.0183 for 2555 Fo > 4sig(Fo) and 0.0190 for all 2639 data REM 143 parameters refined using 0 restraints END WGHT 0.0188 3.9775 REM Highest difference peak 0.423, deepest hole -0.516, 1-sigma level 0.065 Q1 1 -0.0657 0.4039 0.4072 11.00000 0.05 0.42 Q2 1 -0.0036 0.0673 0.5504 11.00000 0.05 0.40 Q3 1 0.0257 0.2501 0.4808 11.00000 0.05 0.40 Q4 1 0.0413 0.1788 0.5972 11.00000 0.05 0.39 Q5 1 0.1455 0.6039 0.3353 11.00000 0.05 0.38 Q6 1 0.0066 0.3583 0.3062 11.00000 0.05 0.37 Q7 1 -0.0039 0.3367 0.3823 11.00000 0.05 0.36 Q8 1 0.1855 0.2373 0.2695 11.00000 0.05 0.36 Q9 1 0.1431 0.2173 0.3376 11.00000 0.05 0.34 Q10 1 0.0799 0.1876 0.4589 11.00000 0.05 0.33 Q11 1 -0.0050 0.3295 0.4507 11.00000 0.05 0.32 Q12 1 0.0578 0.1772 0.5202 11.00000 0.05 0.31 Q13 1 0.0000 0.8485 0.2500 10.50000 0.05 0.31 Q14 1 0.0792 0.6873 0.3120 11.00000 0.05 0.31 Q15 1 0.0655 0.2785 0.3588 11.00000 0.05 0.28 Q16 1 0.0620 0.7658 0.2710 11.00000 0.05 0.26 Q17 1 0.0406 0.6012 0.2968 11.00000 0.05 0.25 Q18 1 0.1168 0.2073 0.4039 11.00000 0.05 0.25 Q19 1 0.0356 0.7723 0.2879 11.00000 0.05 0.25 Q20 1 0.0740 0.1892 0.3901 11.00000 0.05 0.24 ; _shelx_res_checksum 19936 _shelx_hkl_file ; -2 0 2 225.80 10.23 -2 0 2 250.92 10.23 -2 0 2 228.40 10.21 -2 0 2 190.81 10.23 -2 0 2 213.21 10.24 -2 0 2 229.73 10.24 2 0 -2 254.74 10.25 2 0 -2 219.25 10.25 2 0 -2 219.82 10.23 2 0 -2 235.81 10.20 4 0 -4 483.40 20.73 4 0 -4 425.51 20.70 -4 0 4 499.37 20.77 -4 0 4 486.70 20.77 -4 0 4 441.72 20.79 4 0 -4 444.75 20.80 -4 0 4 451.69 20.77 -6 0 6 115.72 5.41 -6 0 6 114.04 5.42 -6 0 6 114.65 5.45 6 0 -6 119.73 5.32 6 0 -6 113.37 5.47 -6 0 6 122.60 5.26 -8 0 8 45.54 2.31 8 0 -8 44.84 2.09 -8 0 8 44.94 2.25 -8 0 8 42.82 2.22 8 0 -8 43.87 2.32 -10 0 10 61.57 3.15 -10 0 10 60.39 3.05 10 0 -10 59.70 3.17 -10 0 10 62.14 3.09 -12 0 12 44.96 2.45 -12 0 12 52.10 2.66 -12 0 12 41.17 2.45 -1 1 1 141.80 6.47 1 1 -1 150.92 6.48 1 1 -1 140.91 6.46 1 1 -1 143.46 6.46 -1 1 1 152.37 6.49 1 1 -1 134.12 6.45 -1 1 1 144.90 6.47 1 1 -1 134.00 6.48 -1 1 1 140.19 6.46 -1 1 1 152.31 6.46 1 -1 -1 144.87 6.49 1 -1 -1 145.81 6.47 -1 -1 1 154.84 6.49 -1 -1 1 124.11 6.46 -1 -1 1 147.47 6.48 1 -1 -1 150.84 6.47 -3 1 3 10.74 0.62 3 1 -3 11.28 0.63 3 1 -3 11.92 0.59 -3 1 3 11.74 0.61 3 1 -3 11.40 0.64 -3 1 3 12.82 0.64 3 1 -3 11.06 0.56 3 1 -3 11.63 0.56 -3 1 3 12.18 0.63 -3 1 3 12.14 0.58 -3 -1 3 11.23 0.61 -3 -1 3 13.14 0.62 3 -1 -3 11.79 0.57 -3 -1 3 11.85 0.64 3 -1 -3 11.40 0.62 -3 -1 3 12.85 0.56 3 -1 -3 11.86 0.58 -5 1 5 59.49 2.58 -5 1 5 58.86 2.71 5 1 -5 57.36 2.70 5 1 -5 56.95 2.55 5 1 -5 59.87 2.55 -5 1 5 57.52 2.67 5 1 -5 57.42 2.72 -5 1 5 56.54 2.69 5 1 -5 51.43 2.60 -5 -1 5 61.24 2.56 -5 -1 5 54.08 2.71 5 -1 -5 55.64 2.68 -5 -1 5 50.71 2.66 -5 -1 5 55.75 2.67 5 -1 -5 50.82 2.71 5 -1 -5 53.39 2.58 5 -1 -5 58.09 2.60 7 1 -7 7.03 0.42 -7 1 7 6.39 0.48 -7 1 7 6.95 0.52 7 1 -7 7.16 0.56 -7 1 7 7.09 0.54 -7 -1 7 7.29 0.51 -7 -1 7 7.61 0.52 7 -1 -7 7.25 0.56 -7 -1 7 7.29 0.55 9 1 -9 15.72 1.04 -9 1 9 15.36 0.95 -9 1 9 14.92 0.96 9 1 -9 15.20 0.81 -9 1 9 15.44 1.02 -9 -1 9 14.84 0.95 -9 -1 9 15.10 0.96 9 -1 -9 15.97 1.05 -9 -1 9 15.81 1.03 -11 1 11 26.36 1.50 11 1 -11 24.26 1.57 -11 1 11 22.63 1.42 -11 1 11 26.53 1.59 11 -1 -11 23.03 1.54 -11 -1 11 24.32 1.47 -11 -1 11 23.52 1.44 -11 -1 11 26.27 1.58 0 2 0 24.33 1.10 0 2 0 24.99 1.15 0 2 0 24.52 1.12 0 2 0 23.83 1.15 0 -2 0 24.76 1.13 0 -2 0 21.99 1.10 0 -2 0 24.66 1.11 0 -2 0 23.88 1.15 2 2 -2 0.12 0.04 -2 2 2 0.03 0.04 -2 2 2 0.08 0.04 2 2 -2 0.12 0.04 2 2 -2 0.06 0.03 2 2 -2 0.08 0.04 2 2 -2 0.11 0.06 -2 2 2 0.10 0.06 -2 2 2 0.09 0.05 -2 2 2 0.11 0.05 2 2 -2 0.04 0.05 -2 2 2 0.10 0.05 -2 -2 2 0.08 0.05 2 -2 -2 0.07 0.05 2 -2 -2 0.05 0.05 -2 -2 2 0.10 0.06 2 -2 -2 0.05 0.06 -2 -2 2 0.09 0.04 -2 -2 2 0.06 0.04 4 2 -4 11.44 0.56 -4 2 4 10.51 0.64 4 2 -4 11.51 0.56 4 2 -4 11.58 0.67 4 2 -4 11.47 0.59 -4 2 4 10.35 0.58 -4 2 4 11.38 0.65 4 2 -4 13.00 0.68 -4 2 4 12.33 0.66 -4 2 4 11.77 0.62 -4 -2 4 11.64 0.63 -4 -2 4 11.58 0.57 4 -2 -4 11.52 0.68 -4 -2 4 11.04 0.63 -4 -2 4 10.89 0.66 6 2 -6 17.20 0.87 -6 2 6 17.17 0.96 -6 2 6 16.56 0.91 6 2 -6 16.53 0.99 -6 2 6 15.69 0.95 6 2 -6 17.23 0.80 -6 2 6 17.09 0.84 -6 -2 6 16.49 0.98 -6 -2 6 16.45 0.93 -6 -2 6 16.72 0.94 6 -2 -6 17.88 1.01 -8 2 8 9.15 0.59 8 2 -8 8.23 0.65 -8 2 8 7.53 0.62 8 2 -8 8.65 0.50 -8 2 8 7.50 0.59 -8 -2 8 8.04 0.58 8 -2 -8 7.70 0.64 -8 -2 8 7.95 0.58 -8 -2 8 8.06 0.64 -10 2 10 12.37 0.87 -10 2 10 12.19 0.92 10 2 -10 10.80 0.89 -10 2 10 12.87 0.84 -10 -2 10 11.67 0.84 10 -2 -10 11.68 0.92 -10 -2 10 12.48 0.85 -10 -2 10 13.96 0.96 -12 2 12 4.49 0.56 -12 2 12 6.15 0.76 -12 2 12 5.63 0.68 -12 -2 12 3.75 0.54 -12 -2 12 4.99 0.63 1 3 -1 47.71 2.15 -1 3 1 46.75 2.17 -1 3 1 43.55 2.19 1 3 -1 47.28 2.18 1 3 -1 46.23 2.20 1 3 -1 46.95 2.13 -1 3 1 49.31 2.11 1 3 -1 47.87 2.19 -1 3 1 47.26 2.19 -1 3 1 48.56 2.18 -1 -3 1 44.61 2.14 -1 -3 1 46.93 2.17 -1 -3 1 45.62 2.19 -1 -3 1 44.90 2.14 3 3 -3 64.32 3.11 -3 3 3 66.14 3.04 -3 3 3 65.03 3.09 3 3 -3 69.54 3.01 3 3 -3 66.13 3.05 -3 3 3 67.27 3.09 -3 3 3 65.45 3.07 -3 3 3 64.19 3.13 3 3 -3 65.10 3.05 -3 3 3 66.36 3.10 -3 -3 3 65.32 3.11 -3 -3 3 71.07 3.08 3 -3 -3 65.50 3.13 3 -3 -3 69.21 3.10 -3 -3 3 61.55 3.06 -5 3 5 151.02 6.83 5 3 -5 148.13 6.86 -5 3 5 141.88 6.82 5 3 -5 148.10 6.75 -5 3 5 148.90 6.89 5 3 -5 138.22 6.83 5 3 -5 150.74 6.71 -5 3 5 145.21 6.75 -5 3 5 151.52 6.77 -5 -3 5 150.07 6.81 5 -3 -5 155.01 6.89 -5 -3 5 147.23 6.86 -5 -3 5 153.60 6.81 -7 3 7 58.44 2.83 -7 3 7 59.91 2.82 7 3 -7 52.35 2.83 7 3 -7 57.34 2.69 -7 3 7 58.08 2.75 -7 3 7 55.39 2.87 7 -3 -7 57.04 2.87 -7 -3 7 57.26 2.85 -7 -3 7 58.41 2.78 -7 -3 7 56.41 2.78 9 3 -9 20.09 1.29 9 3 -9 20.05 1.08 -9 3 9 20.85 1.25 -9 3 9 20.36 1.18 -9 3 9 22.38 1.29 -9 3 9 23.23 1.36 -9 -3 9 20.32 1.21 -9 -3 9 20.86 1.22 9 -3 -9 18.74 1.28 -9 -3 9 21.08 1.30 -11 3 11 28.01 1.66 -11 3 11 26.85 1.69 11 3 -11 30.04 1.78 -11 3 11 29.64 1.96 -11 3 11 28.07 1.60 -11 -3 11 28.04 1.64 -11 -3 11 29.11 1.65 11 -3 -11 27.02 1.87 0 4 0 220.37 9.21 0 4 0 219.90 9.28 0 4 0 177.23 9.25 0 4 0 214.30 9.19 0 -4 0 208.66 9.18 0 -4 0 199.71 9.20 0 -4 0 193.83 9.24 -2 4 2 33.26 1.40 2 4 -2 25.78 1.40 -2 4 2 30.93 1.48 2 4 -2 29.12 1.50 -2 4 2 28.85 1.47 -2 4 2 31.97 1.49 2 4 -2 31.42 1.44 2 4 -2 28.41 1.50 2 4 -2 28.08 1.46 -2 4 2 31.69 1.53 -2 -4 2 31.94 1.47 -2 -4 2 31.51 1.51 -2 -4 2 31.47 1.44 2 -4 -2 33.35 1.49 -2 -4 2 30.61 1.45 4 4 -4 29.51 1.48 -4 4 4 27.63 1.41 4 4 -4 29.57 1.39 4 4 -4 28.76 1.39 -4 4 4 31.72 1.46 -4 4 4 27.22 1.49 -4 4 4 28.33 1.37 4 4 -4 28.94 1.34 -4 4 4 27.64 1.45 4 4 -4 26.46 1.46 -4 4 4 28.66 1.44 -4 -4 4 27.91 1.42 4 -4 -4 27.29 1.48 4 -4 -4 30.60 1.46 -4 -4 4 29.06 1.42 -6 4 6 32.00 1.65 -6 4 6 30.83 1.58 6 4 -6 31.89 1.52 -6 4 6 31.31 1.50 -6 4 6 30.19 1.51 6 4 -6 30.67 1.49 6 4 -6 27.70 1.59 -6 4 6 29.47 1.57 -6 -4 6 29.33 1.54 -6 -4 6 28.42 1.54 6 -4 -6 28.21 1.62 -6 -4 6 31.81 1.63 -8 4 8 5.43 0.47 -8 4 8 4.93 0.51 -8 4 8 4.55 0.45 -8 4 8 4.29 0.39 8 4 -8 4.87 0.49 8 4 -8 4.96 0.36 -8 -4 8 4.59 0.48 -8 -4 8 4.99 0.44 -8 -4 8 4.70 0.42 8 -4 -8 4.26 0.54 -10 4 10 19.71 1.36 -10 4 10 20.86 1.32 -10 4 10 21.41 1.23 10 4 -10 21.30 1.37 -10 4 10 22.64 1.33 -10 -4 10 20.43 1.26 -10 -4 10 19.41 1.25 10 -4 -10 22.88 1.41 -12 4 12 9.02 0.81 -12 4 12 9.71 0.85 -12 4 12 7.81 0.85 -12 -4 12 9.98 0.81 -12 -4 12 9.94 0.81 -1 5 1 8.23 0.46 1 5 -1 7.38 0.39 1 5 -1 7.18 0.47 1 5 -1 8.03 0.48 -1 5 1 7.79 0.49 -1 5 1 8.13 0.41 -1 5 1 7.53 0.48 1 5 -1 6.37 0.47 -1 5 1 8.21 0.46 1 5 -1 8.01 0.42 -1 -5 1 7.68 0.45 -1 -5 1 7.94 0.41 1 -5 -1 7.86 0.46 -1 -5 1 6.92 0.46 -1 -5 1 7.81 0.40 3 5 -3 21.97 1.03 3 5 -3 19.81 1.13 -3 5 3 21.75 1.12 -3 5 3 17.56 1.09 3 5 -3 20.55 1.06 -3 5 3 23.11 1.03 -3 5 3 22.24 1.18 3 5 -3 21.35 1.15 -3 5 3 22.40 1.12 -3 5 3 22.10 1.13 3 -5 -3 23.84 1.13 -3 -5 3 22.74 1.07 -3 -5 3 20.89 1.08 3 -5 -3 21.48 1.17 -3 -5 3 21.84 1.15 -3 -5 3 20.95 1.09 5 5 -5 13.54 0.83 5 5 -5 14.12 0.73 -5 5 5 13.49 0.80 -5 5 5 13.84 0.72 5 5 -5 13.60 0.73 -5 5 5 13.72 0.79 -5 5 5 13.45 0.76 5 5 -5 12.81 0.85 -5 5 5 12.90 0.84 5 5 -5 12.48 0.67 5 -5 -5 13.83 0.86 -5 -5 5 13.78 0.77 -5 -5 5 13.32 0.84 -5 -5 5 12.08 0.75 -7 5 7 31.29 1.63 7 5 -7 30.42 1.67 -7 5 7 27.76 1.67 -7 5 7 29.37 1.52 7 5 -7 30.66 1.51 -7 5 7 27.42 1.61 -7 -5 7 29.46 1.66 -7 -5 7 31.52 1.60 7 -5 -7 29.33 1.68 -7 -5 7 33.49 1.60 -9 5 9 2.95 0.43 9 5 -9 2.22 0.35 -9 5 9 2.56 0.34 -9 5 9 2.01 0.40 -9 5 9 2.35 0.39 9 5 -9 1.83 0.38 -9 -5 9 2.79 0.38 9 -5 -9 2.65 0.46 -9 -5 9 2.99 0.43 -11 5 11 3.24 0.50 -11 5 11 4.08 0.61 -11 -5 11 4.15 0.54 -11 -5 11 3.46 0.50 0 6 0 184.80 7.81 0 6 0 186.22 7.88 0 6 0 156.65 7.76 0 6 0 184.83 7.92 0 -6 0 176.16 7.85 0 -6 0 169.97 7.74 0 -6 0 151.36 7.77 -2 6 2 178.22 7.77 2 6 -2 162.82 7.80 -2 6 2 167.43 7.95 2 6 -2 182.49 7.95 -2 6 2 178.71 7.90 2 6 -2 168.07 7.92 -2 6 2 174.60 7.82 2 6 -2 170.90 7.84 -2 6 2 166.77 7.91 2 6 -2 174.32 7.91 -2 6 2 173.35 7.90 -2 -6 2 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3 -5 30.14 1.51 -3 3 5 28.97 1.52 3 3 -5 29.61 1.41 -3 3 5 30.17 1.43 -3 3 5 30.77 1.44 -3 3 5 28.43 1.42 -3 3 5 31.01 1.48 -3 -3 5 32.47 1.46 3 -3 -5 32.35 1.49 -3 -3 5 30.89 1.43 -3 -3 5 27.88 1.48 3 -3 -5 29.16 1.51 -5 3 7 169.55 7.76 -5 3 7 182.15 7.85 -5 3 7 162.06 7.93 5 3 -7 166.33 7.87 5 3 -7 156.60 7.75 5 3 -7 162.23 7.71 -5 3 7 169.06 7.85 5 3 -7 171.72 7.91 -5 3 7 173.20 7.81 5 3 -7 187.46 7.74 -5 3 7 184.61 7.86 -5 -3 7 185.63 7.83 -5 -3 7 166.39 7.89 5 -3 -7 159.98 7.91 -5 -3 7 172.34 7.85 -7 3 9 56.43 2.81 -7 3 9 56.10 2.81 -7 3 9 56.46 2.91 7 3 -9 61.53 2.91 -7 3 9 54.97 2.75 7 3 -9 53.42 2.66 -7 -3 9 53.90 2.78 -7 -3 9 57.52 2.86 -7 -3 9 58.20 2.77 7 -3 -9 61.80 2.92 9 3 -11 40.04 2.21 -9 3 11 40.22 2.24 9 3 -11 37.09 1.90 -9 3 11 39.35 2.06 -9 3 11 40.32 2.16 -9 3 11 39.02 2.12 -9 -3 11 40.67 2.11 9 -3 -11 40.39 2.23 -9 -3 11 40.07 2.08 -9 -3 11 42.66 2.22 -11 3 13 32.12 1.80 -11 3 13 32.70 1.86 -11 3 13 31.53 1.89 -11 -3 13 33.06 1.84 -11 -3 13 34.09 2.01 -11 -3 13 31.52 1.85 -12 4 10 10.99 0.80 -12 4 10 11.29 0.95 -12 4 10 10.93 0.88 -12 4 10 9.58 0.63 -12 -4 10 10.25 0.84 -12 -4 10 9.05 0.78 10 4 -8 16.94 1.15 -10 4 8 18.91 1.19 -10 4 8 17.55 1.16 -10 4 8 16.32 1.02 -10 4 8 16.37 1.10 -10 -4 8 16.21 1.07 10 -4 -8 16.44 1.16 -10 -4 8 16.84 1.08 8 4 -6 14.40 0.95 8 4 -6 13.56 0.82 -8 4 6 14.95 0.87 -8 4 6 13.39 0.95 -8 4 6 15.23 0.94 -8 4 6 15.89 0.98 8 -4 -6 15.56 0.99 -8 -4 6 15.08 0.91 -8 -4 6 15.21 0.92 -8 -4 6 15.27 0.99 -6 4 4 76.10 3.62 6 4 -4 77.40 3.49 6 4 -4 65.37 3.59 -6 4 4 76.08 3.51 -6 4 4 82.56 3.66 -6 4 4 75.64 3.53 6 4 -4 71.58 3.59 -6 4 4 71.70 3.58 6 4 -4 74.18 3.50 -6 -4 4 77.06 3.50 -6 -4 4 75.19 3.63 6 -4 -4 77.14 3.64 -6 -4 4 75.88 3.57 -6 -4 4 75.41 3.56 -4 4 2 33.65 1.63 -4 4 2 36.72 1.79 -4 4 2 34.77 1.76 4 4 -2 34.71 1.70 -4 4 2 34.63 1.73 4 4 -2 33.96 1.68 4 4 -2 35.91 1.76 4 4 -2 36.88 1.78 -4 4 2 36.29 1.67 -4 4 2 35.14 1.74 -4 -4 2 38.38 1.73 -4 -4 2 37.25 1.74 4 -4 -2 31.62 1.73 4 -4 -2 35.03 1.77 -4 -4 2 35.35 1.77 -4 -4 2 35.37 1.68 -4 -4 2 36.28 1.71 -2 4 0 61.11 2.83 2 4 0 62.59 2.86 -2 4 0 65.83 2.83 -2 4 0 61.86 2.93 -2 4 0 57.75 2.85 2 4 0 60.49 2.90 2 4 0 57.43 2.82 -2 4 0 60.34 2.92 -2 4 0 59.96 2.89 2 4 0 64.14 2.92 2 4 0 60.83 2.91 -2 -4 0 63.40 2.87 -2 -4 0 69.03 2.81 2 -4 0 59.97 2.89 -2 -4 0 59.96 2.85 -2 -4 0 65.43 2.92 -2 -4 0 65.98 2.93 -2 -4 0 65.74 2.90 0 4 -2 98.82 4.40 0 4 2 92.47 4.36 0 4 -2 94.49 4.40 0 4 -2 85.47 4.40 0 4 -2 101.39 4.35 0 4 2 98.60 4.40 0 4 2 100.99 4.31 0 4 -2 94.90 4.32 0 4 2 96.95 4.41 0 -4 2 95.20 4.32 0 -4 2 96.75 4.34 0 -4 -2 98.96 4.38 0 -4 -2 95.05 4.31 0 -4 2 90.01 4.35 2 4 -4 30.22 1.37 -2 4 4 28.19 1.40 -2 4 4 28.39 1.34 2 4 -4 29.73 1.33 -2 4 4 27.90 1.41 2 4 -4 27.92 1.44 2 4 -4 28.97 1.39 -2 4 4 27.60 1.37 2 4 -4 27.71 1.43 2 -4 -4 30.37 1.46 -2 -4 4 29.75 1.38 2 -4 -4 28.98 1.34 -2 -4 4 27.82 1.43 -2 -4 4 28.68 1.37 -4 4 6 58.83 2.65 4 4 -6 59.54 2.59 -4 4 6 56.76 2.63 -4 4 6 56.86 2.74 4 4 -6 53.47 2.54 -4 4 6 57.58 2.61 4 4 -6 52.60 2.71 -4 4 6 57.92 2.64 -4 4 6 55.10 2.68 4 4 -6 47.95 2.59 4 -4 -6 56.04 2.68 -4 -4 6 59.11 2.63 -4 -4 6 53.84 2.65 4 -4 -6 57.29 2.75 -4 -4 6 53.82 2.70 6 4 -8 36.71 1.83 -6 4 8 36.77 1.88 -6 4 8 37.30 1.94 -6 4 8 39.15 1.85 6 4 -8 38.61 2.01 -6 4 8 38.97 2.03 -6 4 8 36.58 1.92 -6 -4 8 36.96 1.89 6 -4 -8 37.81 2.02 -6 -4 8 39.03 2.00 -6 -4 8 42.68 1.96 8 4 -10 18.74 0.99 -8 4 10 18.23 1.13 -8 4 10 18.34 1.14 -8 4 10 18.19 1.07 8 4 -10 19.38 1.22 -8 4 10 20.11 1.25 -8 -4 10 21.51 1.23 -8 -4 10 19.50 1.11 -8 -4 10 17.30 1.11 8 -4 -10 19.14 1.23 -10 4 12 23.80 1.45 -10 4 12 22.92 1.53 -10 4 12 24.02 1.38 -10 4 12 25.13 1.47 10 4 -12 25.01 1.56 -10 -4 12 24.08 1.43 -10 -4 12 24.94 1.55 10 -4 -12 22.85 1.54 -10 -4 12 23.29 1.40 -11 5 9 2.88 0.50 11 5 -9 2.84 0.50 -11 5 9 2.95 0.31 -11 5 9 3.44 0.51 -11 5 9 3.39 0.55 -11 -5 9 3.04 0.46 11 -5 -9 3.23 0.55 -11 -5 9 2.93 0.44 -9 5 7 12.82 0.94 -9 5 7 12.59 0.79 9 5 -7 13.05 0.77 -9 5 7 11.66 0.86 -9 5 7 12.35 0.89 9 5 -7 12.44 0.90 -9 -5 7 12.58 0.84 9 -5 -7 13.20 0.94 -9 -5 7 12.74 0.85 -7 5 5 1.37 0.27 -7 5 5 1.56 0.28 -7 5 5 1.38 0.22 -7 5 5 1.58 0.30 7 5 -5 1.28 0.26 7 5 -5 1.53 0.21 -7 5 5 1.89 0.24 -7 -5 5 2.07 0.40 7 -5 -5 1.83 0.33 -7 -5 5 1.96 0.29 -7 -5 5 1.42 0.24 -5 5 3 27.67 1.35 -5 5 3 31.57 1.57 -5 5 3 28.47 1.47 5 5 -3 28.13 1.52 -5 5 3 28.34 1.51 5 5 -3 28.26 1.50 -5 5 3 28.37 1.40 5 5 -3 28.39 1.42 5 5 -3 28.32 1.36 -5 5 3 28.11 1.49 5 5 -3 28.70 1.43 5 -5 -3 27.39 1.52 -5 -5 3 29.49 1.47 -5 -5 3 30.11 1.46 -5 -5 3 29.81 1.54 3 5 -1 3.03 0.27 -3 5 1 2.77 0.28 -3 5 1 2.99 0.26 -3 5 1 3.28 0.19 3 5 -1 2.79 0.19 -3 5 1 3.19 0.27 3 5 -1 2.76 0.22 3 5 -1 3.07 0.28 3 5 -1 2.56 0.24 -3 5 1 3.47 0.19 -3 5 1 3.01 0.22 -3 5 1 2.91 0.28 3 -5 -1 2.12 0.27 -3 -5 1 2.85 0.23 -3 -5 1 2.70 0.27 -3 -5 1 3.12 0.26 -3 -5 1 2.77 0.21 1 5 1 21.90 0.92 1 5 1 20.53 1.04 1 5 1 18.44 1.00 -1 5 -1 21.23 1.04 -1 5 -1 16.44 0.95 -1 5 -1 20.33 0.91 -1 5 -1 20.00 0.93 -1 5 -1 20.05 0.99 1 5 1 19.67 1.03 1 5 1 20.97 0.95 -1 5 -1 18.84 1.03 -1 5 -1 17.40 1.02 -1 -5 -1 19.60 1.00 1 -5 1 20.67 0.96 -1 -5 -1 19.30 1.00 1 -5 1 20.69 0.91 -1 -5 -1 18.40 0.92 -1 -5 -1 21.38 0.94 1 -5 1 18.98 0.99 -1 5 3 0.76 0.11 1 5 -3 0.67 0.11 1 5 -3 0.62 0.14 1 5 -3 0.93 0.17 -1 5 3 0.61 0.06 1 5 -3 0.58 0.08 -1 5 3 0.62 0.13 -1 5 3 0.48 0.12 -1 5 3 0.93 0.17 1 5 -3 0.54 0.12 1 -5 -3 0.63 0.12 1 -5 -3 0.61 0.06 -1 -5 3 0.74 0.11 -1 -5 3 0.66 0.10 -1 -5 3 0.55 0.09 -3 5 5 8.06 0.51 3 5 -5 7.58 0.47 -3 5 5 9.37 0.51 3 5 -5 8.19 0.50 -3 5 5 7.95 0.52 3 5 -5 9.07 0.58 -3 5 5 8.48 0.45 3 5 -5 8.75 0.56 3 5 -5 7.28 0.43 -3 5 5 8.46 0.59 -3 5 5 8.94 0.50 -3 -5 5 8.16 0.49 -3 -5 5 8.75 0.56 3 -5 -5 8.32 0.53 3 -5 -5 7.91 0.57 -3 -5 5 8.46 0.50 -5 5 7 10.35 0.66 -5 5 7 9.93 0.63 5 5 -7 10.91 0.71 5 5 -7 9.09 0.57 -5 5 7 10.89 0.59 -5 5 7 10.48 0.61 5 5 -7 9.80 0.57 -5 -5 7 9.66 0.61 5 -5 -7 10.77 0.67 5 -5 -7 10.26 0.72 -5 -5 7 9.65 0.63 -5 -5 7 11.36 0.71 -7 5 9 7.69 0.62 -7 5 9 6.19 0.46 7 5 -9 7.06 0.59 -7 5 9 6.76 0.54 7 5 -9 6.45 0.43 -7 5 9 6.82 0.52 -7 -5 9 5.59 0.54 7 -5 -9 5.03 0.55 -7 -5 9 6.21 0.50 -7 -5 9 6.08 0.48 9 5 -11 0.31 0.21 -9 5 11 0.22 0.14 -9 5 11 0.59 0.21 -9 5 11 0.61 0.24 -9 5 11 0.52 0.21 -9 -5 11 0.75 0.40 9 -5 -11 0.21 0.18 -9 -5 11 0.34 0.17 -9 -5 11 0.27 0.16 -11 5 13 1.50 0.35 -11 5 13 0.67 0.26 -11 -5 13 0.74 0.26 -12 6 10 33.51 1.70 -12 6 10 33.57 2.00 -12 -6 10 34.24 1.96 10 6 -8 79.71 3.99 -10 6 8 80.11 3.94 -10 6 8 78.18 3.95 -10 6 8 82.82 3.66 -10 6 8 77.62 4.01 10 -6 -8 72.89 3.98 -10 -6 8 78.03 3.88 -10 -6 8 77.77 3.88 -8 6 6 37.12 2.09 -8 6 6 41.10 1.89 8 6 -6 39.74 2.14 8 6 -6 40.17 1.99 -8 6 6 42.50 2.20 -8 6 6 37.56 2.12 -8 -6 6 40.07 2.06 -8 -6 6 39.50 2.07 8 -6 -6 40.41 2.18 6 6 -4 80.58 3.93 6 6 -4 79.23 3.74 -6 6 4 81.00 3.87 -6 6 4 92.75 4.02 -6 6 4 82.61 3.94 -6 6 4 81.44 3.73 6 6 -4 83.63 3.96 6 6 -4 80.72 3.82 6 6 -4 78.95 3.82 -6 6 4 82.16 3.78 -6 6 4 79.14 3.90 6 -6 -4 78.37 3.95 -6 -6 4 80.39 3.86 -6 -6 4 81.53 3.88 -4 6 2 112.20 5.08 4 6 -2 109.49 4.89 -4 6 2 107.67 4.89 -4 6 2 101.84 5.02 -4 6 2 106.10 5.01 4 6 -2 106.72 5.03 4 6 -2 106.84 4.99 4 6 -2 96.76 5.03 -4 6 2 109.61 5.02 4 6 -2 106.60 4.94 -4 6 2 107.74 4.87 -4 -6 2 118.57 5.07 -4 -6 2 110.38 4.93 4 -6 -2 105.53 5.01 4 -6 -2 103.64 5.05 -4 -6 2 106.77 4.96 -4 -6 2 112.59 5.00 2 6 0 29.53 1.54 2 6 0 31.16 1.46 -2 6 0 31.11 1.51 -2 6 0 27.33 1.41 -2 6 0 28.88 1.46 2 6 0 28.28 1.52 -2 6 0 31.86 1.57 2 6 0 34.76 1.42 -2 6 0 28.89 1.54 2 6 0 33.95 1.59 -2 -6 0 30.74 1.43 -2 -6 0 31.73 1.51 2 -6 0 27.88 1.49 -2 -6 0 30.08 1.45 0 6 -2 382.72 16.20 0 6 2 363.75 16.20 0 6 -2 368.41 16.11 0 6 -2 318.74 16.17 0 6 -2 374.17 16.22 0 6 2 360.00 16.15 0 6 2 375.08 16.03 0 6 -2 357.26 16.07 0 6 2 333.24 16.08 0 6 2 412.39 16.23 0 -6 2 350.97 16.10 0 -6 2 372.05 16.14 0 -6 -2 366.34 16.16 0 -6 2 335.98 16.06 0 -6 -2 306.05 16.04 -2 6 4 221.54 9.33 2 6 -4 200.12 9.14 2 6 -4 200.73 9.24 -2 6 4 197.27 9.25 -2 6 4 204.91 9.21 2 6 -4 208.34 9.19 -2 6 4 204.42 9.12 -2 6 4 201.73 9.25 2 6 -4 179.02 9.26 -2 -6 4 203.63 9.20 -2 -6 4 201.09 9.18 2 -6 -4 215.63 9.32 2 -6 -4 200.55 9.24 -2 -6 4 203.15 9.28 4 6 -6 187.73 8.59 -4 6 6 198.83 8.76 -4 6 6 197.90 8.53 4 6 -6 185.67 8.69 4 6 -6 182.16 8.50 -4 6 6 185.94 8.65 -4 6 6 203.84 8.63 4 6 -6 180.30 8.56 -4 6 6 191.81 8.63 4 6 -6 187.42 8.71 4 -6 -6 195.51 8.74 -4 -6 6 194.65 8.60 -4 -6 6 181.18 8.60 4 -6 -6 167.07 8.63 -4 -6 6 188.93 8.70 -6 6 8 147.35 7.27 6 6 -8 154.87 7.35 6 6 -8 156.27 7.17 -6 6 8 151.75 7.24 -6 6 8 162.41 7.17 -6 6 8 160.60 7.21 -6 6 8 165.79 7.41 -6 -6 8 154.77 7.25 -6 -6 8 154.08 7.21 6 -6 -8 159.78 7.39 -6 -6 8 155.23 7.34 8 6 -10 13.78 0.81 -8 6 10 13.41 0.94 8 6 -10 14.90 1.02 -8 6 10 14.57 0.95 -8 6 10 14.40 1.03 -8 -6 10 13.65 0.91 8 -6 -10 15.61 1.05 -8 -6 10 13.54 0.88 -10 6 12 18.20 1.23 -10 6 12 18.83 1.23 -10 -6 12 18.59 1.20 -10 -6 12 18.40 1.17 -11 7 9 51.67 2.85 -11 7 9 51.70 2.55 -11 7 9 56.83 2.93 -11 -7 9 52.29 2.79 -11 -7 9 54.19 2.80 -9 7 7 26.92 1.65 9 7 -7 24.24 1.56 -9 7 7 27.58 1.61 -9 7 7 26.79 1.32 -9 7 7 27.92 1.58 -9 -7 7 26.05 1.51 -9 -7 7 26.94 1.52 9 -7 -7 26.52 1.63 -7 7 5 35.82 1.82 -7 7 5 31.27 1.76 7 7 -5 33.01 1.58 7 7 -5 32.13 1.66 7 7 -5 31.20 1.79 -7 7 5 32.64 1.73 -7 7 5 34.79 1.58 -7 7 5 32.64 1.84 7 -7 -5 31.06 1.83 -7 -7 5 33.41 1.74 -7 -7 5 33.65 1.73 5 7 -3 53.93 2.65 -5 7 3 50.97 2.59 5 7 -3 50.59 2.51 -5 7 3 51.63 2.60 -5 7 3 57.69 2.70 5 7 -3 53.01 2.45 5 7 -3 53.93 2.64 -5 7 3 56.06 2.44 -5 7 3 53.74 2.63 5 -7 -3 52.30 2.66 -5 -7 3 52.51 2.54 5 -7 -3 52.51 2.60 -5 -7 3 45.86 2.55 -3 7 1 41.36 1.70 3 7 -1 31.86 1.77 -3 7 1 33.96 1.74 -3 7 1 33.99 1.80 3 7 -1 33.66 1.68 -3 7 1 33.54 1.77 -3 7 1 34.22 1.77 -3 7 1 37.67 1.63 3 7 -1 34.60 1.63 3 7 -1 30.32 1.76 3 7 -1 34.11 1.76 -3 -7 1 35.64 1.68 -3 -7 1 34.90 1.70 -3 -7 1 35.32 1.58 3 -7 -1 35.63 1.75 -3 -7 1 36.58 1.75 -1 7 -1 21.36 1.04 1 7 1 22.99 0.98 -1 7 -1 21.31 1.14 1 7 1 21.05 1.12 1 7 1 21.67 1.14 -1 7 -1 18.65 0.98 -1 7 -1 20.09 1.07 1 7 1 19.07 1.09 1 7 1 20.19 1.02 -1 7 -1 19.93 1.11 -1 7 -1 21.86 1.14 -1 -7 -1 20.62 0.98 -1 -7 -1 23.18 0.98 1 -7 1 19.72 1.07 1 -7 1 19.01 1.00 -1 -7 -1 19.56 1.08 -1 7 3 76.18 3.47 1 7 -3 79.45 3.47 1 7 -3 76.07 3.59 1 7 -3 65.10 3.58 -1 7 3 72.29 3.62 -1 7 3 74.79 3.57 -1 7 3 74.94 3.60 1 7 -3 74.05 3.51 1 7 -3 80.83 3.64 -1 7 3 71.35 3.54 -1 -7 3 77.43 3.53 -1 -7 3 80.57 3.51 1 -7 -3 78.86 3.57 -1 -7 3 79.31 3.47 3 7 -5 10.79 0.60 3 7 -5 9.97 0.63 -3 7 5 10.90 0.63 3 7 -5 9.46 0.68 3 7 -5 10.20 0.54 -3 7 5 10.00 0.65 3 7 -5 10.39 0.69 -3 7 5 10.58 0.66 -3 7 5 9.94 0.71 3 -7 -5 8.94 0.68 -3 -7 5 9.84 0.60 -3 -7 5 11.12 0.70 -3 -7 5 11.78 0.62 3 -7 -5 10.77 0.66 -5 7 7 79.65 3.87 5 7 -7 78.95 3.76 5 7 -7 82.18 3.68 -5 7 7 81.76 3.97 5 7 -7 82.45 3.79 -5 7 7 84.78 3.83 5 7 -7 79.82 3.92 -5 7 7 80.89 3.83 5 -7 -7 68.97 3.83 -5 -7 7 79.88 3.91 -5 -7 7 82.86 3.80 5 -7 -7 82.34 3.96 -5 -7 7 80.21 3.81 7 7 -9 12.80 0.77 7 7 -9 12.86 0.94 -7 7 9 12.92 0.87 -7 7 9 17.36 1.06 -7 7 9 12.92 0.89 7 -7 -9 12.77 0.95 -7 -7 9 13.28 0.83 -7 -7 9 13.53 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93.98 4.39 2 4 -6 88.29 4.52 2 4 -6 101.55 4.47 2 4 -6 100.44 4.47 -2 4 6 84.20 4.40 -2 -4 6 86.37 4.41 2 -4 -6 101.78 4.44 2 -4 -6 93.21 4.54 -2 -4 6 102.78 4.47 2 -4 -6 99.63 4.48 -4 4 8 66.28 3.21 -4 4 8 64.32 3.07 -4 4 8 65.55 3.07 -4 4 8 68.14 3.07 4 4 -8 64.26 3.04 -4 4 8 65.97 3.07 -4 4 8 67.79 3.14 4 4 -8 65.56 3.16 4 4 -8 67.00 3.20 4 -4 -8 64.13 3.20 -4 -4 8 64.28 3.11 4 -4 -8 71.58 3.15 -4 -4 8 63.37 3.06 -4 -4 8 62.17 3.15 6 4 -10 73.25 3.19 6 4 -10 70.02 3.41 -6 4 10 63.47 3.27 -6 4 10 69.66 3.27 -6 4 10 68.83 3.32 -6 4 10 67.07 3.43 6 -4 -10 60.90 3.39 -6 -4 10 68.69 3.26 -6 -4 10 74.11 3.34 -6 -4 10 70.48 3.37 -8 4 12 29.79 1.75 8 4 -12 29.70 1.44 -8 4 12 31.03 1.59 -8 4 12 24.27 1.58 -8 4 12 30.54 1.65 8 4 -12 29.01 1.72 -8 -4 12 30.40 1.70 -8 -4 12 31.69 1.59 -8 -4 12 29.52 1.63 8 -4 -12 29.22 1.74 -10 4 14 15.17 1.05 -10 4 14 15.59 0.99 -10 4 14 14.58 1.03 -10 -4 14 13.91 1.01 -10 -4 14 16.25 1.13 -11 5 7 5.31 0.67 11 5 -7 5.44 0.67 -11 5 7 5.80 0.42 -11 5 7 6.55 0.64 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6 4 20.39 1.13 8 6 -4 20.00 1.07 -8 6 4 18.77 1.16 -8 6 4 17.70 1.19 -8 -6 4 19.65 0.97 8 -6 -4 19.01 1.20 -8 -6 4 20.39 1.14 -8 -6 4 18.95 1.14 -6 6 2 91.96 4.29 6 6 -2 91.46 4.15 6 6 -2 86.05 4.07 -6 6 2 94.24 4.30 6 6 -2 85.70 4.27 -6 6 2 91.84 4.24 6 6 -2 88.40 4.18 6 6 -2 89.62 4.24 -6 6 2 96.02 4.12 -6 6 2 86.17 4.21 -6 6 2 88.87 4.07 6 -6 -2 83.44 4.26 -6 -6 2 84.40 4.04 -6 -6 2 86.52 4.21 -6 -6 2 85.76 4.18 -6 -6 2 92.01 4.19 4 6 0 99.90 4.87 4 6 0 106.40 4.86 4 6 0 112.17 4.72 -4 6 0 99.83 4.88 4 6 0 102.72 4.77 -4 6 0 103.69 4.72 -4 6 0 107.62 4.78 4 6 0 103.10 4.84 -4 6 0 98.44 4.87 -4 6 0 97.74 4.72 -4 6 0 105.36 4.87 -4 6 0 102.12 4.84 -4 -6 0 107.83 4.76 -4 -6 0 97.99 4.79 4 -6 0 107.87 4.85 -4 -6 0 97.43 4.83 -4 -6 0 116.60 4.87 -2 6 -2 100.99 4.46 -2 6 -2 103.54 4.62 2 6 2 96.24 4.49 2 6 2 99.40 4.60 2 6 2 101.00 4.57 -2 6 -2 89.38 4.46 -2 6 -2 99.65 4.61 2 6 2 103.08 4.60 2 6 2 97.87 4.57 2 6 2 90.18 4.44 -2 6 -2 103.22 4.52 -2 6 -2 96.25 4.60 -2 6 -2 100.36 4.54 -2 -6 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94.85 4.01 2 4 -7 84.47 4.12 -2 4 7 89.16 4.11 2 -4 -7 90.41 4.17 2 -4 -7 77.25 4.08 -2 -4 7 86.99 4.09 2 -4 -7 91.22 4.06 -2 -4 7 91.04 4.02 4 4 -9 49.93 2.46 -4 4 9 48.85 2.48 4 4 -9 53.83 2.64 -4 4 9 58.42 2.51 -4 4 9 50.08 2.56 -4 4 9 54.20 2.52 -4 4 9 51.47 2.50 -4 4 9 47.85 2.63 4 -4 -9 54.93 2.66 -4 -4 9 52.41 2.56 -4 -4 9 53.85 2.60 4 -4 -9 57.26 2.58 -4 -4 9 55.79 2.50 6 4 -11 16.00 0.78 -6 4 11 14.87 0.91 6 4 -11 14.35 0.97 -6 4 11 17.26 1.05 -6 4 11 15.31 0.87 -6 4 11 13.95 0.86 6 -4 -11 14.82 1.00 -6 -4 11 14.64 0.85 -6 -4 11 15.14 0.95 -6 -4 11 14.90 0.91 -8 4 13 1.99 0.31 8 4 -13 1.75 0.18 -8 4 13 3.14 0.50 -8 4 13 2.10 0.34 8 4 -13 2.18 0.41 -8 4 13 1.69 0.33 8 -4 -13 1.68 0.37 -8 -4 13 1.96 0.38 -8 -4 13 1.83 0.31 -10 4 15 24.99 1.41 -10 4 15 23.24 1.44 -10 4 15 23.14 1.45 -10 -4 15 23.15 1.45 -10 -4 15 24.11 1.53 -11 5 6 42.42 2.24 -11 5 6 38.41 1.89 -11 5 6 35.87 2.11 -11 5 6 40.75 2.21 11 -5 -6 37.86 2.18 -11 -5 6 37.70 2.11 -11 -5 6 37.02 1.87 -11 -5 6 38.80 2.10 9 5 -4 16.60 1.01 -9 5 4 14.84 0.99 9 5 -4 15.20 0.89 -9 5 4 14.49 0.89 -9 5 4 14.97 1.02 -9 5 4 15.79 1.06 -9 5 4 14.34 0.80 9 -5 -4 15.31 1.02 -9 -5 4 17.58 1.01 -9 -5 4 14.87 0.79 -9 -5 4 14.05 0.94 7 5 -2 51.34 2.43 7 5 -2 49.53 2.47 -7 5 2 51.05 2.39 7 5 -2 49.28 2.32 -7 5 2 50.23 2.32 -7 5 2 46.30 2.53 7 5 -2 50.38 2.40 7 5 -2 49.52 2.54 -7 5 2 48.89 2.45 -7 5 2 50.79 2.49 -7 -5 2 49.82 2.47 -7 -5 2 50.99 2.46 -7 -5 2 48.18 2.29 -7 -5 2 49.23 2.42 7 -5 -2 47.66 2.50 -5 5 0 127.96 5.78 5 5 0 126.10 5.80 -5 5 0 123.28 5.76 5 5 0 124.57 5.74 5 5 0 123.76 5.74 -5 5 0 126.49 5.63 -5 5 0 127.77 5.75 -5 5 0 123.39 5.66 -5 5 0 122.51 5.69 5 5 0 120.93 5.68 5 5 0 123.39 5.62 -5 -5 0 117.33 5.73 5 -5 0 130.75 5.78 -5 -5 0 116.44 5.74 -5 -5 0 126.87 5.72 -5 -5 0 122.75 5.58 -3 5 -2 44.45 2.19 -3 5 -2 45.43 2.18 3 5 2 46.29 2.18 -3 5 -2 46.67 2.14 3 5 2 45.07 2.05 -3 5 -2 45.80 2.07 3 5 2 51.57 2.26 3 5 2 44.41 2.09 3 5 2 45.72 2.15 -3 5 -2 38.28 2.07 -3 5 -2 45.81 2.11 -3 5 -2 39.34 2.18 3 5 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47.25 2.37 3 -5 -8 49.93 2.33 3 -5 -8 49.54 2.48 -3 -5 8 47.12 2.43 3 -5 -8 51.96 2.41 -5 5 10 122.30 5.53 -5 5 10 117.03 5.41 5 5 -10 122.70 5.28 5 5 -10 122.00 5.50 -5 5 10 115.22 5.32 -5 5 10 103.28 5.30 -5 5 10 118.61 5.32 -5 -5 10 116.30 5.38 5 -5 -10 113.94 5.40 5 -5 -10 101.73 5.46 -5 -5 10 114.36 5.45 7 5 -12 25.97 1.59 -7 5 12 25.01 1.49 -7 5 12 28.00 1.45 -7 5 12 27.78 1.64 7 5 -12 27.70 1.35 -7 5 12 27.83 1.47 7 -5 -12 26.83 1.62 -7 -5 12 27.18 1.57 -7 -5 12 28.32 1.52 -9 5 14 34.13 1.74 9 5 -14 28.96 1.98 -9 5 14 31.30 1.66 -9 5 14 31.54 1.75 -9 -5 14 29.17 1.79 -9 -5 14 26.15 1.68 -12 6 7 1.08 0.32 -12 6 7 2.27 0.28 -12 -6 7 1.60 0.22 -12 -6 7 0.99 0.30 -12 -6 7 1.72 0.37 -10 6 5 0.24 0.18 -10 6 5 0.00 0.09 10 6 -5 -0.07 0.15 -10 6 5 0.14 0.14 -10 6 5 -0.04 0.15 10 -6 -5 0.02 0.15 -10 -6 5 0.06 0.08 -10 -6 5 0.16 0.16 -10 -6 5 0.09 0.16 8 6 -3 1.68 0.25 -8 6 3 1.17 0.27 -8 6 3 1.72 0.33 -8 6 3 1.75 0.35 -8 6 3 2.06 0.31 8 6 -3 2.03 0.33 -8 6 3 2.14 0.37 -8 6 3 1.91 0.22 -8 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-6 -13 5.01 0.59 -6 -6 -13 5.16 0.65 4 6 15 0.92 0.24 -4 6 -15 0.92 0.35 -4 6 -15 0.41 0.19 -4 -6 -15 0.61 0.22 -2 6 -17 2.61 0.39 2 6 17 2.25 0.42 -2 6 -17 1.95 0.39 2 6 17 2.22 0.30 2 -6 17 1.77 0.33 -2 -6 -17 1.57 0.31 -2 -6 -17 1.87 0.39 0 6 19 0.17 0.19 0 6 19 0.58 0.23 0 6 -19 0.53 0.23 0 -6 -19 0.35 0.18 0 -6 -19 0.26 0.22 0 -6 19 0.41 0.21 -2 6 21 2.09 0.37 2 6 -21 1.55 0.37 -2 -6 21 2.29 0.41 2 -6 -21 1.48 0.32 7 7 12 6.43 0.67 -7 -7 -12 7.02 0.65 -7 -7 -12 7.56 0.66 5 7 14 10.23 0.78 -5 7 -14 10.86 0.79 -5 -7 -14 11.10 0.81 3 7 16 7.28 0.55 -3 7 -16 4.67 0.57 3 -7 16 7.02 0.60 -3 -7 -16 7.90 0.62 1 7 18 2.96 0.29 -1 7 -18 2.84 0.47 -1 7 -18 2.27 0.40 1 7 18 2.74 0.41 1 -7 18 3.09 0.45 -1 -7 -18 4.14 0.49 1 7 -20 8.49 0.73 -1 -7 20 8.93 0.75 -8 -8 -11 14.18 1.03 -6 -8 -13 24.24 1.44 -6 -8 -13 22.30 1.39 4 8 15 35.18 1.88 -4 -8 -15 34.69 1.91 -2 8 -17 19.63 1.16 2 8 17 16.29 0.99 2 -8 17 17.84 1.46 0 8 -19 13.12 0.93 0 8 19 12.10 0.67 0 -8 19 13.10 0.92 -5 -9 -14 7.33 0.68 1 9 18 2.14 0.38 -4 -10 -15 12.57 0.94 -10 0 -10 30.51 1.80 8 0 12 27.42 1.73 -8 0 -12 27.69 1.63 -6 0 -14 30.05 1.81 -6 0 -14 30.03 1.72 6 0 14 30.94 1.80 -4 0 -16 46.01 2.51 -4 0 -16 51.90 2.63 4 0 16 48.08 2.55 -2 0 -18 21.43 1.32 2 0 18 21.14 1.25 -2 0 -18 18.88 1.22 0 0 20 56.81 2.85 0 0 -20 53.35 2.82 -2 0 22 49.28 2.61 2 0 -22 48.91 2.60 -9 1 -11 10.78 0.86 9 1 11 11.57 0.99 -9 -1 -11 12.24 0.90 -7 1 -13 5.91 0.65 7 1 13 5.67 0.72 -7 -1 -13 5.85 0.64 7 -1 13 4.44 0.64 -5 1 -15 8.15 0.77 -5 1 -15 9.32 0.73 5 1 15 9.40 0.77 -5 -1 -15 9.93 0.81 -5 -1 -15 9.61 0.74 5 -1 15 10.21 0.81 3 1 17 3.42 0.47 -3 1 -17 3.38 0.47 -3 1 -17 4.16 0.56 -3 -1 -17 2.95 0.48 -3 -1 -17 3.35 0.46 -1 1 -19 3.59 0.50 1 1 19 4.47 0.52 -1 1 -19 3.23 0.45 1 -1 19 3.71 0.48 -1 -1 -19 4.32 0.51 -1 -1 -19 3.63 0.51 -1 1 21 3.73 0.49 1 1 -21 3.62 0.49 -1 -1 21 2.91 0.46 1 -1 -21 2.93 0.45 -3 1 23 0.42 0.23 3 1 -23 0.74 0.29 3 -1 -23 0.71 0.26 -3 -1 23 0.83 0.33 -10 2 -10 2.68 0.46 8 2 12 9.98 0.89 -8 2 -12 10.49 0.82 -8 -2 -12 9.99 0.81 8 -2 12 11.92 0.98 6 2 14 3.78 0.54 -6 2 -14 3.27 0.46 6 -2 14 3.10 0.55 -6 -2 -14 3.58 0.48 -4 2 -16 11.27 0.82 4 2 16 11.77 0.84 -4 2 -16 10.47 0.87 -4 -2 -16 11.88 0.83 -4 -2 -16 11.39 0.89 2 2 18 0.06 0.11 -2 2 -18 0.33 0.18 -2 2 -18 0.05 0.16 2 -2 18 0.28 0.15 -2 -2 -18 0.56 0.21 -2 -2 -18 0.22 0.18 0 2 -20 4.58 0.55 0 2 20 5.34 0.61 0 -2 -20 6.31 0.65 0 -2 20 4.72 0.57 2 2 -22 0.18 0.20 -2 2 22 0.16 0.19 2 -2 -22 0.01 0.16 -2 -2 22 0.32 0.18 9 3 11 13.32 1.05 -9 3 -11 12.30 0.92 -9 -3 -11 11.44 0.91 7 3 13 7.74 0.72 -7 3 -13 8.68 0.70 -7 -3 -13 8.08 0.69 7 -3 13 8.72 0.81 5 3 15 31.98 1.74 -5 3 -15 28.78 1.87 -5 3 -15 31.74 1.72 -5 -3 -15 28.99 1.92 -5 -3 -15 29.34 1.70 -3 3 -17 21.70 1.38 3 3 17 21.67 1.27 -3 3 -17 22.17 1.32 -3 -3 -17 21.73 1.38 -3 -3 -17 21.95 1.32 1 3 19 31.21 1.82 -1 3 -19 37.62 1.94 -1 3 -19 29.92 1.81 -1 -3 -19 33.84 1.89 1 -3 19 34.73 1.86 -1 -3 -19 31.57 1.82 -1 3 21 16.25 1.09 1 3 -21 16.29 1.11 -1 -3 21 16.50 1.11 1 -3 -21 17.40 1.11 -3 3 23 14.21 1.01 3 -3 -23 13.15 0.99 -8 4 -12 9.28 0.73 8 4 12 7.92 0.77 -8 -4 -12 7.97 0.72 6 4 14 11.37 0.85 -6 4 -14 10.44 0.80 -6 -4 -14 10.59 0.81 -4 4 -16 10.99 0.90 -4 4 -16 11.08 0.80 4 4 16 9.38 0.75 -4 -4 -16 11.69 0.81 -4 -4 -16 11.02 0.99 -2 4 -18 6.41 0.66 -2 4 -18 5.34 0.66 2 4 18 5.24 0.46 2 -4 18 5.34 0.60 -2 -4 -18 6.52 0.63 -2 -4 -18 4.86 0.56 0 4 -20 13.99 0.99 0 4 20 15.13 1.05 0 4 20 14.74 1.00 0 -4 -20 13.95 0.97 0 -4 20 15.47 1.02 -2 4 22 4.89 0.59 2 4 -22 4.49 0.59 -2 -4 22 4.21 0.56 2 -4 -22 3.75 0.52 -9 5 -11 0.96 0.30 -9 -5 -11 0.66 0.29 -9 -5 -11 1.85 0.54 7 5 13 0.21 0.18 -7 5 -13 0.20 0.19 -7 -5 -13 0.19 0.19 -5 5 -15 1.21 0.30 5 5 15 1.51 0.32 -5 -5 -15 1.96 0.36 -3 5 -17 3.62 0.62 3 5 17 4.73 0.44 -3 5 -17 4.14 0.52 3 -5 17 4.57 0.55 -3 -5 -17 4.31 0.52 1 5 19 0.49 0.22 1 5 19 0.19 0.18 1 5 19 0.42 0.15 -1 5 -19 0.18 0.20 -1 5 -19 0.19 0.15 -1 -5 -19 0.05 0.20 -1 -5 -19 0.55 0.22 1 -5 19 0.47 0.20 1 5 -21 1.71 0.37 -1 5 21 2.18 0.39 -1 -5 21 2.50 0.41 1 -5 -21 2.42 0.40 -8 6 -12 23.61 1.43 -8 -6 -12 23.70 1.64 -8 -6 -12 21.02 1.39 6 6 14 24.99 1.49 -6 6 -14 24.67 1.45 -6 -6 -14 23.53 1.46 4 6 16 35.31 2.02 -4 6 -16 41.14 2.10 -4 -6 -16 39.70 2.08 4 -6 16 38.13 2.07 2 6 18 13.90 0.89 -2 6 -18 15.43 1.03 2 -6 18 17.49 1.07 -2 -6 -18 15.63 1.02 0 6 -20 24.70 1.48 0 6 20 24.56 1.46 0 -6 20 24.67 1.48 0 -6 -20 23.58 1.44 -7 -7 -13 9.17 0.78 -5 7 -15 20.03 1.23 -5 -7 -15 19.10 1.23 -3 7 -17 13.20 0.95 3 7 17 14.77 0.90 -3 -7 -17 13.33 0.94 3 -7 17 13.37 0.95 1 7 19 6.74 0.47 1 7 19 6.37 0.59 -1 7 -19 6.58 0.69 1 -7 19 6.48 0.68 -1 -7 -19 6.29 0.59 -6 -8 -14 2.01 0.38 -4 -8 -16 1.28 0.31 -2 8 -18 0.12 0.18 -8 0 -13 0.28 0.18 8 0 13 -0.09 0.19 -6 0 -15 -0.20 0.12 6 0 15 0.05 0.15 -4 0 -17 -0.02 0.14 4 0 17 -0.24 0.11 -2 0 -19 0.23 0.19 -2 0 -19 -0.20 0.15 2 0 19 0.08 0.16 0 0 -21 0.40 0.21 0 0 21 0.18 0.18 -2 0 23 0.12 0.19 2 0 -23 0.40 0.24 -9 1 -12 9.94 0.84 9 1 12 11.77 1.00 -9 -1 -12 9.83 0.84 -7 1 -14 11.96 0.89 7 1 14 11.91 0.96 -7 -1 -14 11.24 0.88 7 -1 14 12.05 0.98 5 1 16 24.96 1.48 -5 1 -16 23.88 1.42 -5 -1 -16 23.63 1.43 5 -1 16 22.74 1.48 3 1 18 23.01 1.39 -3 1 -18 24.06 1.41 -3 1 -18 23.79 1.48 -3 -1 -18 23.22 1.48 -3 -1 -18 22.77 1.40 -1 1 -20 15.48 1.06 -1 1 -20 14.56 1.08 1 1 20 14.96 1.05 1 -1 20 16.03 1.07 -1 -1 -20 15.88 1.07 -1 -1 -20 18.71 1.15 -1 1 22 11.86 0.93 1 1 -22 12.37 0.94 -1 -1 22 14.19 0.97 1 -1 -22 13.27 0.95 -8 2 -13 21.27 1.38 8 2 13 21.67 1.49 -8 -2 -13 22.79 1.41 8 -2 13 24.77 1.57 -6 2 -15 13.49 0.96 6 2 15 13.64 1.00 6 -2 15 13.49 1.05 -6 -2 -15 13.78 0.97 4 2 17 42.16 2.20 -4 2 -17 39.80 2.18 -4 -2 -17 39.82 2.19 -2 2 -19 31.58 1.86 2 2 19 31.58 1.86 -2 2 -19 34.75 1.96 -2 -2 -19 33.76 1.87 2 -2 19 35.23 1.89 -2 -2 -19 34.95 1.94 0 2 -21 17.94 1.21 0 2 21 19.27 1.22 0 -2 21 19.06 1.22 0 -2 -21 19.57 1.23 -2 2 23 7.88 0.82 2 -2 -23 8.86 0.75 -9 3 -12 3.27 0.51 7 3 14 0.20 0.20 -7 3 -14 0.33 0.21 7 -3 14 0.76 0.29 -7 -3 -14 0.35 0.22 -5 3 -16 1.18 0.29 5 3 16 0.83 0.26 -5 -3 -16 1.38 0.34 -3 3 -18 9.99 0.77 3 3 18 9.79 0.73 3 -3 18 10.60 0.80 -3 -3 -18 10.05 0.78 -1 3 -20 0.56 0.22 1 3 20 0.80 0.24 -1 3 -20 0.26 0.21 -1 -3 -20 0.47 0.25 1 -3 20 0.57 0.23 -1 -3 -20 0.09 0.15 1 3 -22 0.46 0.23 -1 3 22 0.33 0.20 -1 -3 22 -0.12 0.16 1 -3 -22 0.83 0.28 -8 4 -13 5.84 0.67 -8 -4 -13 7.49 0.77 -6 4 -15 5.13 0.61 6 4 15 5.54 0.67 -6 -4 -15 5.33 0.62 4 4 17 7.02 0.61 -4 4 -17 6.69 0.60 -4 -4 -17 6.45 0.60 2 4 19 0.87 0.28 -2 4 -19 0.86 0.29 2 4 19 0.88 0.22 2 -4 19 1.12 0.31 -2 -4 -19 1.02 0.28 0 4 -21 18.44 1.20 0 4 21 18.20 1.17 0 -4 21 16.77 1.16 0 -4 -21 18.11 1.17 -7 5 -14 15.04 1.06 -7 -5 -14 16.51 1.11 5 5 16 31.89 1.81 -5 5 -16 30.93 1.80 -5 -5 -16 33.50 1.84 3 5 18 7.47 0.60 -3 5 -18 8.07 0.68 3 -5 18 7.35 0.64 -3 -5 -18 7.69 0.66 1 5 20 10.92 0.81 -1 5 -20 9.45 0.80 -1 -5 -20 10.61 0.81 1 -5 20 11.11 0.84 1 5 -22 24.39 1.63 -1 5 22 25.13 1.51 -1 -5 22 23.92 1.61 1 -5 -22 25.64 1.52 -6 6 -15 2.87 0.45 -6 -6 -15 3.57 0.50 -4 6 -17 0.39 0.22 4 -6 17 0.70 0.24 -4 -6 -17 1.11 0.30 2 6 19 0.13 0.16 -2 6 -19 -0.19 0.14 2 6 19 0.19 0.16 -2 -6 -19 -0.08 0.17 2 -6 19 -0.01 0.15 0 6 -21 1.20 0.31 0 6 21 1.67 0.35 0 -6 -21 1.55 0.35 0 -6 21 1.88 0.37 -5 7 -16 11.62 0.92 -5 -7 -16 12.60 0.90 -3 7 -18 11.41 0.86 -3 -7 -18 11.37 0.85 3 -7 18 11.03 0.85 -1 7 -20 2.11 0.41 1 7 20 2.49 0.42 1 -7 20 3.36 0.48 -1 -7 -20 3.15 0.47 -8 0 -14 12.59 0.99 8 0 14 14.92 1.14 6 0 16 14.64 1.07 -6 0 -16 13.99 1.01 -4 0 -18 26.58 1.57 2 0 20 19.17 1.23 -2 0 -20 19.12 1.23 0 0 22 23.80 1.43 0 0 -22 21.85 1.41 7 1 15 6.56 0.70 -7 1 -15 7.16 0.75 -7 -1 -15 6.21 0.71 7 -1 15 6.93 0.73 -5 1 -17 3.52 0.50 5 1 17 3.23 0.50 -5 -1 -17 3.14 0.48 5 -1 17 4.18 0.61 -3 1 -19 5.39 0.62 -3 -1 -19 6.45 0.67 3 -1 19 4.75 0.58 1 1 21 1.95 0.41 -1 1 -21 2.01 0.39 1 -1 21 2.39 0.40 -1 -1 -21 2.90 0.48 -8 2 -14 5.86 0.68 8 -2 14 6.44 0.82 -8 -2 -14 5.09 0.87 -6 2 -16 10.31 0.82 6 2 16 9.56 0.84 -6 -2 -16 10.26 0.83 6 -2 16 10.51 0.91 4 2 18 8.80 0.72 -4 2 -18 7.98 0.70 -4 -2 -18 8.64 0.74 2 2 20 9.51 0.76 -2 2 -20 8.81 0.74 -2 -2 -20 8.13 0.73 2 -2 20 8.34 0.73 0 2 -22 0.47 0.23 0 2 22 0.82 0.26 0 -2 -22 1.10 0.28 0 -2 22 0.55 0.22 -7 3 -15 8.19 0.74 -7 -3 -15 9.71 0.80 -5 3 -17 15.58 1.10 5 3 17 17.17 1.24 -5 -3 -17 18.00 1.15 3 3 19 25.48 1.48 -3 3 -19 23.91 1.46 -3 -3 -19 23.66 1.45 3 -3 19 22.68 1.44 -1 3 -21 15.19 1.03 1 3 21 15.21 1.03 -1 -3 -21 14.16 1.00 1 -3 21 12.79 0.98 -6 4 -16 8.46 0.71 -6 -4 -16 6.27 0.71 -4 4 -18 16.27 1.11 -4 -4 -18 16.76 1.12 2 4 20 13.04 0.92 -2 4 -20 11.85 0.90 -2 -4 -20 11.36 0.89 2 -4 20 12.22 0.92 0 4 -22 5.13 0.91 0 4 22 7.09 0.74 0 -4 -22 6.61 0.72 -5 5 -17 2.04 0.41 -5 -5 -17 2.60 0.42 -3 5 -19 0.93 0.28 3 -5 19 0.66 0.26 -3 -5 -19 0.75 0.27 -1 5 -21 1.45 0.36 1 5 21 0.78 0.29 1 -5 21 1.07 0.30 -1 -5 -21 1.36 0.34 -4 6 -18 25.12 1.52 4 -6 18 23.75 1.50 -4 -6 -18 26.56 1.54 -2 6 -20 10.23 0.83 2 6 20 11.06 0.84 2 -6 20 9.09 0.80 -2 -6 -20 10.48 0.83 -6 0 -17 -0.12 0.17 -4 0 -19 0.02 0.16 2 0 21 0.00 0.18 -2 0 -21 0.05 0.18 -7 1 -16 4.85 0.91 -5 1 -18 19.79 1.28 -5 -1 -18 19.33 1.27 3 1 20 17.15 1.15 -3 1 -20 16.65 1.15 3 -1 20 17.45 1.16 -3 -1 -20 16.40 1.14 -6 2 -17 20.70 1.32 -6 -2 -17 19.87 1.40 -4 2 -19 24.76 1.52 -4 -2 -19 25.23 1.53 2 2 21 13.58 1.00 -2 2 -21 14.12 1.04 2 -2 21 13.35 1.02 -2 -2 -21 14.07 1.01 -5 3 -18 0.67 0.26 -5 -3 -18 0.34 0.24 -3 3 -20 -0.06 0.14 -3 -3 -20 0.07 0.18 3 -3 20 0.04 0.16 -4 4 -19 1.44 0.35 -4 -4 -19 1.69 0.38 4 -4 19 1.56 0.36 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 60026 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy Sb1 Sb 0.0000 0.40951(2) 0.2500 0.01239(6) Uani 1 2 d S T P C1 C 0.02915(16) 0.32339(13) 0.35351(9) 0.0148(3) Uani 1 1 d . . . F1 F -0.19646(10) 0.41014(7) 0.24074(6) 0.0184(2) Uani 1 1 d . . . C2 C -0.03223(16) 0.35687(13) 0.41053(10) 0.0159(3) Uani 1 1 d . . . C3 C -0.01917(17) 0.29461(13) 0.47546(10) 0.0185(3) Uani 1 1 d . . . H3 H -0.0597 0.3171 0.5146 0.022 Uiso 1 1 calc R U . C4 C 0.05148(18) 0.20053(14) 0.48473(10) 0.0200(3) Uani 1 1 d . . . C7 C -0.11353(17) 0.45651(13) 0.40557(10) 0.0184(3) Uani 1 1 d . . . H7A H -0.0669 0.5132 0.3863 0.028 Uiso 1 1 calc R U . H7B H -0.1239 0.4748 0.4565 0.028 Uiso 1 1 calc R U . H7C H -0.2025 0.4460 0.3707 0.028 Uiso 1 1 calc R U . C6 C 0.10401(16) 0.22967(13) 0.36237(10) 0.0170(3) Uani 1 1 d . . . C5 C 0.11257(18) 0.17038(13) 0.42802(10) 0.0199(3) Uani 1 1 d . . . H5 H 0.1622 0.1069 0.4341 0.024 Uiso 1 1 calc R U . C8 C 0.0613(2) 0.13396(17) 0.55456(11) 0.0302(4) Uani 1 1 d . . . H8A H 0.0845 0.0622 0.5438 0.045 Uiso 1 1 calc R U . H8B H -0.0253 0.1342 0.5682 0.045 Uiso 1 1 calc R U . H8C H 0.1311 0.1621 0.5972 0.045 Uiso 1 1 calc R U . C10 C 0.0000 0.57569(17) 0.2500 0.0145(4) Uani 1 2 d S T P C9 C 0.17548(19) 0.18852(14) 0.30465(11) 0.0219(4) Uani 1 1 d . . . H9A H 0.1179 0.1980 0.2529 0.033 Uiso 1 1 calc R U . H9B H 0.1950 0.1140 0.3140 0.033 Uiso 1 1 calc R U . H9C H 0.2598 0.2269 0.3096 0.033 Uiso 1 1 calc R U . C11 C 0.09568(16) 0.63051(13) 0.30599(10) 0.0152(3) Uani 1 1 d . . . C12 C 0.09300(16) 0.73975(13) 0.30472(10) 0.0167(3) Uani 1 1 d . . . H12 H 0.1571 0.7769 0.3427 0.020 Uiso 1 1 calc R U . C13 C 0.0000 0.79635(18) 0.2500 0.0169(5) Uani 1 2 d S T P C14 C 0.20391(18) 0.57852(13) 0.36717(10) 0.0192(3) Uani 1 1 d . . . H14A H 0.2765 0.5547 0.3449 0.029 Uiso 1 1 calc R U . H14B H 0.1656 0.5185 0.3880 0.029 Uiso 1 1 calc R U . H14C H 0.2398 0.6287 0.4082 0.029 Uiso 1 1 calc R U . C15 C 0.0000 0.91391(18) 0.2500 0.0212(5) Uani 1 2 d S T P H15A H 0.0263 0.9395 0.2047 0.032 Uiso 0.5 1 calc R U P H15B H 0.0640 0.9395 0.2962 0.032 Uiso 0.5 1 calc R U P H15C H -0.0904 0.9395 0.2491 0.032 Uiso 0.5 1 calc R U P loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.01239(8) 0.01030(8) 0.01557(9) 0.000 0.00558(6) 0.000 C1 0.0141(7) 0.0140(7) 0.0166(8) 0.0003(6) 0.0046(6) -0.0005(6) F1 0.0132(5) 0.0193(5) 0.0238(5) 0.0002(4) 0.0068(4) -0.0006(4) C2 0.0145(7) 0.0144(8) 0.0191(8) -0.0022(6) 0.0047(6) -0.0001(6) C3 0.0204(8) 0.0196(8) 0.0169(8) -0.0017(7) 0.0073(7) 0.0010(6) C4 0.0214(8) 0.0199(8) 0.0183(8) 0.0024(7) 0.0042(7) 0.0015(7) C7 0.0204(8) 0.0165(8) 0.0204(8) -0.0023(7) 0.0089(7) 0.0035(6) C6 0.0158(7) 0.0153(7) 0.0206(8) -0.0009(7) 0.0062(6) 0.0005(6) C5 0.0206(8) 0.0164(8) 0.0231(9) 0.0022(7) 0.0060(7) 0.0043(6) C8 0.0411(12) 0.0300(10) 0.0214(9) 0.0078(8) 0.0116(9) 0.0116(9) C10 0.0157(11) 0.0122(10) 0.0172(11) 0.000 0.0073(9) 0.000 C9 0.0260(9) 0.0167(8) 0.0270(9) 0.0024(7) 0.0141(8) 0.0081(7) C11 0.0140(7) 0.0159(8) 0.0177(8) 0.0002(6) 0.0075(6) -0.0002(6) C12 0.0159(7) 0.0152(8) 0.0213(8) -0.0036(6) 0.0090(7) -0.0029(6) C13 0.0168(11) 0.0130(11) 0.0253(12) 0.000 0.0133(10) 0.000 C14 0.0173(8) 0.0186(8) 0.0200(9) -0.0007(7) 0.0015(7) -0.0003(6) C15 0.0199(12) 0.0131(11) 0.0329(15) 0.000 0.0110(11) 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 F1 Sb1 F1 179.53(5) . 2 F1 Sb1 C1 89.60(5) . . F1 Sb1 C1 90.65(5) 2 . F1 Sb1 C1 90.65(5) . 2 F1 Sb1 C1 89.59(5) 2 2 C1 Sb1 C1 117.55(9) . 2 F1 Sb1 C10 89.77(3) . . F1 Sb1 C10 89.77(3) 2 . C1 Sb1 C10 121.22(4) . . C1 Sb1 C10 121.22(4) 2 . C2 C1 C6 120.55(15) . . C2 C1 Sb1 119.81(12) . . C6 C1 Sb1 119.54(12) . . C3 C2 C1 118.43(15) . . C3 C2 C7 117.76(15) . . C1 C2 C7 123.80(15) . . C4 C3 C2 122.10(16) . . C4 C3 H3 118.9 . . C2 C3 H3 118.9 . . C5 C4 C3 118.09(16) . . C5 C4 C8 121.02(16) . . C3 C4 C8 120.90(16) . . C2 C7 H7A 109.5 . . C2 C7 H7B 109.5 . . H7A C7 H7B 109.5 . . C2 C7 H7C 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . C5 C6 C1 118.44(15) . . C5 C6 C9 117.36(15) . . C1 C6 C9 124.21(15) . . C4 C5 C6 122.36(16) . . C4 C5 H5 118.8 . . C6 C5 H5 118.8 . . C4 C8 H8A 109.5 . . C4 C8 H8B 109.5 . . H8A C8 H8B 109.5 . . C4 C8 H8C 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . C11 C10 C11 120.3(2) 2 . C11 C10 Sb1 119.87(10) 2 . C11 C10 Sb1 119.87(10) . . C6 C9 H9A 109.5 . . C6 C9 H9B 109.5 . . H9A C9 H9B 109.5 . . C6 C9 H9C 109.5 . . H9A C9 H9C 109.5 . . H9B C9 H9C 109.5 . . C12 C11 C10 118.61(16) . . C12 C11 C14 117.38(15) . . C10 C11 C14 124.00(15) . . C13 C12 C11 122.58(16) . . C13 C12 H12 118.7 . . C11 C12 H12 118.7 . . C12 C13 C12 117.4(2) 2 . C12 C13 C15 121.31(11) 2 . C12 C13 C15 121.31(11) . . C11 C14 H14A 109.5 . . C11 C14 H14B 109.5 . . H14A C14 H14B 109.5 . . C11 C14 H14C 109.5 . . H14A C14 H14C 109.5 . . H14B C14 H14C 109.5 . . C13 C15 H15A 109.5 . . C13 C15 H15B 109.5 . . H15A C15 H15B 109.5 . . C13 C15 H15C 109.5 . . H15A C15 H15C 109.5 . . H15B C15 H15C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Sb1 F1 1.9821(10) . Sb1 F1 1.9821(10) 2 Sb1 C1 2.1252(16) . Sb1 C1 2.1252(16) 2 Sb1 C10 2.126(2) . C1 C2 1.402(2) . C1 C6 1.411(2) . C2 C3 1.396(2) . C2 C7 1.514(2) . C3 C4 1.394(2) . C3 H3 0.9500 . C4 C5 1.383(3) . C4 C8 1.504(3) . C7 H7A 0.9800 . C7 H7B 0.9800 . C7 H7C 0.9800 . C6 C5 1.391(2) . C6 C9 1.511(2) . C5 H5 0.9500 . C8 H8A 0.9800 . C8 H8B 0.9800 . C8 H8C 0.9800 . C10 C11 1.408(2) 2 C10 C11 1.408(2) . C9 H9A 0.9800 . C9 H9B 0.9800 . C9 H9C 0.9800 . C11 C12 1.398(2) . C11 C14 1.511(2) . C12 C13 1.393(2) . C12 H12 0.9500 . C13 C12 1.393(2) 2 C13 C15 1.504(3) . C14 H14A 0.9800 . C14 H14B 0.9800 . C14 H14C 0.9800 . C15 H15A 0.9800 . C15 H15B 0.9800 . C15 H15C 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 C6 C1 C2 C3 -1.0(2) . . Sb1 C1 C2 C3 175.44(12) . . C6 C1 C2 C7 179.71(16) . . Sb1 C1 C2 C7 -3.9(2) . . C1 C2 C3 C4 -0.6(3) . . C7 C2 C3 C4 178.78(16) . . C2 C3 C4 C5 1.5(3) . . C2 C3 C4 C8 -178.66(17) . . C2 C1 C6 C5 1.5(2) . . Sb1 C1 C6 C5 -174.90(12) . . C2 C1 C6 C9 -178.90(16) . . Sb1 C1 C6 C9 4.7(2) . . C3 C4 C5 C6 -1.0(3) . . C8 C4 C5 C6 179.25(18) . . C1 C6 C5 C4 -0.5(3) . . C9 C6 C5 C4 179.85(17) . . C11 C10 C11 C12 0.19(10) 2 . Sb1 C10 C11 C12 -179.81(10) . . C11 C10 C11 C14 -178.61(18) 2 . Sb1 C10 C11 C14 1.39(18) . . C10 C11 C12 C13 -0.4(2) . . C14 C11 C12 C13 178.48(13) . . C11 C12 C13 C12 0.21(11) . 2 C11 C12 C13 C15 -179.79(11) . .