#------------------------------------------------------------------------------
#$Date: 2016-03-24 14:09:40 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179654 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/51/07/4510701.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4510701
loop_
_publ_author_name
'Olejniczak, Anna'
'Anio\/la, Michalina'
'Szafra\'nski, Marek'
'Budzianowski, Armand'
'Katrusiak, Andrzej'
_publ_section_title
;
 New Polar Phases of 1,4-Diazabicyclo[2.2.2]octane Perchlorate, An
 NH+···N Hydrogen-Bonded Ferroelectric
;
_journal_issue                   7
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              2872
_journal_paper_doi               10.1021/cg400276c
_journal_volume                  13
_journal_year                    2013
_chemical_formula_moiety         'C6 H13 N2, Cl O4'
_chemical_formula_sum            'C6 H13 Cl N2 O4'
_chemical_formula_weight         212.63
_chemical_name_common
;
dabcoHClO4
;
_chemical_name_systematic
; 
1,4-diazabicyclo[2.2.2]octane perchlorate
;
_space_group_IT_number           31
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P -2ab -2'
_symmetry_space_group_name_H-M   'P m 21 n'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   8.7889(9)
_cell_length_b                   9.7596(12)
_cell_length_c                   5.3418(6)
_cell_measurement_reflns_used    2091
_cell_measurement_temperature    230(2)
_cell_measurement_theta_max      29.10
_cell_measurement_theta_min      3.81
_cell_volume                     458.20(9)
_computing_cell_refinement       'CrysAlis (Oxford Diffraction, 2002)'
_computing_data_collection       'CrysAlis (Oxford Diffraction, 2002)'
_computing_data_reduction        'CrysAlis (Oxford Diffraction, 2002)'
_computing_molecular_graphics
;X-Seed (Barbour, 2001) 
and POV-Ray (Persistence of Vision, 2004)
;
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      230(2)
_diffrn_measured_fraction_theta_full 0.952
_diffrn_measured_fraction_theta_max 0.952
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0288
_diffrn_reflns_av_sigmaI/netI    0.0196
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       -5
_diffrn_reflns_number            2091
_diffrn_reflns_theta_full        29.10
_diffrn_reflns_theta_max         29.10
_diffrn_reflns_theta_min         3.81
_exptl_absorpt_coefficient_mu    0.403
_exptl_absorpt_correction_T_max  0.95
_exptl_absorpt_correction_T_min  0.90
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details
; 
Correction for absorption was made using XEMP (SHELXTL, 
Sheldrick (1990)).
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.541
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             224
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.434
_refine_diff_density_min         -0.243
_refine_diff_density_rms         0.056
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.11(11)
_refine_ls_extinction_coef       0.037(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     71
_refine_ls_number_reflns         1008
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.071
_refine_ls_R_factor_all          0.0349
_refine_ls_R_factor_gt           0.0339
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0512P)^2^+0.1351P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0904
_refine_ls_wR_factor_ref         0.0913
_reflns_number_gt                975
_reflns_number_total             1008
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg400276c_si_002.cif
_cod_data_source_block           dabcoHClO4_II_230K
_cod_original_sg_symbol_H-M      Pm21n
_cod_database_code               4510701
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z'
'x+1/2, y+1/2, -z'
'-x, y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cl Cl 0.0000 -0.01744(11) -0.06951(12) 0.0326(2) Uani 1 2 d S
O1 O 0.0000 -0.0184(8) -0.3371(4) 0.0705(9) Uani 1 2 d S
O2 O 0.1329(2) -0.0875(3) 0.0176(4) 0.0542(6) Uani 1 1 d .
O3 O 0.0000 0.1198(4) 0.0209(7) 0.0659(9) Uani 1 2 d S
N2 N 0.0000 0.5490(4) 0.2797(5) 0.0343(7) Uani 1 2 d S
N1 N 0.0000 0.5480(4) 0.7524(5) 0.0377(7) Uani 1 2 d S
H1 H 0.0000 0.5487 0.9227 0.045 Uiso 1 2 calc SR
C2 C 0.0000 0.4098(5) 0.3711(8) 0.079(2) Uani 1 2 d S
H2A H 0.0892 0.3626 0.3081 0.095 Uiso 0.50 1 calc PR
H2B H -0.0892 0.3626 0.3081 0.095 Uiso 0.50 1 calc PR
C1 C 0.0000 0.4041(5) 0.6627(7) 0.0494(11) Uani 1 2 d S
H1A H -0.0896 0.3563 0.7228 0.059 Uiso 0.50 1 calc PR
H1B H 0.0896 0.3563 0.7228 0.059 Uiso 0.50 1 calc PR
C4 C 0.1340(3) 0.6202(4) 0.3767(5) 0.0577(9) Uani 1 1 d .
H4A H 0.1335 0.7141 0.3171 0.069 Uiso 1 1 calc R
H4B H 0.2250 0.5761 0.3126 0.069 Uiso 1 1 calc R
C3 C 0.1392(3) 0.6203(3) 0.6585(5) 0.0432(6) Uani 1 1 d .
H3A H 0.2300 0.5735 0.7165 0.052 Uiso 1 1 calc R
H3B H 0.1414 0.7136 0.7208 0.052 Uiso 1 1 calc R
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Cl 0.0339(3) 0.0341(3) 0.0297(3) 0.0006(4) 0.000 0.000
O1 0.0612(14) 0.123(3) 0.0271(11) 0.009(3) 0.000 0.000
O2 0.0483(10) 0.0592(14) 0.0551(11) -0.0050(10) -0.0148(8) 0.0199(9)
O3 0.075(2) 0.0334(16) 0.090(3) -0.0109(16) 0.000 0.000
N2 0.0470(14) 0.0408(17) 0.0150(11) -0.0008(13) 0.000 0.000
N1 0.0638(17) 0.0367(16) 0.0125(11) -0.0005(12) 0.000 0.000
C2 0.177(6) 0.033(2) 0.0281(19) -0.009(2) 0.000 0.000
C1 0.090(3) 0.0298(19) 0.0282(17) 0.0049(18) 0.000 0.000
C4 0.0359(12) 0.099(3) 0.0386(13) 0.0021(16) 0.0113(10) -0.0166(13)
C3 0.0409(12) 0.0494(15) 0.0392(13) -0.0044(11) -0.0141(10) 0.0016(10)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O3 Cl O1 110.2(4) . .
O3 Cl O2 109.83(13) . .
O1 Cl O2 108.78(18) . .
O3 Cl O2 109.83(13) . 4
O1 Cl O2 108.78(18) . 4
O2 Cl O2 109.4(2) . 4
C2 N2 C4 109.1(2) . .
C2 N2 C4 109.1(2) . 4
C4 N2 C4 107.3(3) . 4
C1 N1 C3 109.73(19) . .
C1 N1 C3 109.73(19) . 4
C3 N1 C3 109.4(3) . 4
C1 N1 H1 109.3 . .
C3 N1 H1 109.3 . .
C3 N1 H1 109.3 4 .
N2 C2 C1 111.8(4) . .
N2 C2 H2A 109.2 . .
C1 C2 H2A 109.2 . .
N2 C2 H2B 109.2 . .
C1 C2 H2B 109.2 . .
H2A C2 H2B 107.9 . .
N1 C1 C2 106.8(4) . .
N1 C1 H1A 110.4 . .
C2 C1 H1A 110.4 . .
N1 C1 H1B 110.4 . .
C2 C1 H1B 110.4 . .
H1A C1 H1B 108.6 . .
N2 C4 C3 112.2(2) . .
N2 C4 H4A 109.2 . .
C3 C4 H4A 109.2 . .
N2 C4 H4B 109.2 . .
C3 C4 H4B 109.2 . .
H4A C4 H4B 107.9 . .
N1 C3 C4 108.0(2) . .
N1 C3 H3A 110.1 . .
C4 C3 H3A 110.1 . .
N1 C3 H3B 110.1 . .
C4 C3 H3B 110.1 . .
H3A C3 H3B 108.4 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cl O3 1.424(4) .
Cl O1 1.430(2) .
Cl O2 1.4311(19) .
Cl O2 1.4311(19) 4
N2 C2 1.443(5) .
N2 C4 1.463(3) .
N2 C4 1.463(3) 4
N1 C1 1.484(5) .
N1 C3 1.499(3) .
N1 C3 1.499(3) 4
N1 H1 0.9100 .
C2 C1 1.558(5) .
C2 H2A 0.9700 .
C2 H2B 0.9700 .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C4 C3 1.506(3) .
C4 H4A 0.9700 .
C4 H4B 0.9700 .
C3 H3A 0.9700 .
C3 H3B 0.9700 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
C4 N2 C2 C1 58.47(17) .
C4 N2 C2 C1 -58.47(17) 4
C3 N1 C1 C2 -60.14(16) .
C3 N1 C1 C2 60.14(16) 4
N2 C2 C1 N1 0.000(1) .
C2 N2 C4 C3 -58.1(3) .
C4 N2 C4 C3 59.9(4) 4
C1 N1 C3 C4 61.5(3) .
C3 N1 C3 C4 -59.0(4) 4
N2 C4 C3 N1 -1.2(4) .
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
4 -6 0 140.82 151.06 2.19 o
6 -6 0 61.28 67.87 1.96 o
3 -5 0 755.67 808.74 3.97 o
7 -5 0 140.19 149.03 2.78 o
9 -5 0 38.74 34.83 1.81 o
2 -4 0 243.59 219.03 1.76 o
4 -4 0 945.42 1008.69 4.70 o
6 -4 0 61.56 59.02 1.79 o
8 -4 0 15.05 14.08 1.23 o
10 -4 0 51.36 54.36 2.23 o
1 -3 0 1829.09 1787.52 3.95 o
3 -3 0 419.58 489.45 2.85 o
5 -3 0 42.79 50.75 1.39 o
7 -3 0 379.87 408.97 4.19 o
9 -3 0 50.02 53.14 2.16 o
11 -3 0 6.21 6.33 1.30 o
2 -2 0 2972.65 2998.66 5.69 o
4 -2 0 1159.52 1133.90 4.94 o
8 -2 0 228.73 246.58 3.99 o
10 -2 0 49.31 48.48 2.03 o
3 -1 0 1410.24 1439.85 4.69 o
5 -1 0 192.58 186.61 2.50 o
7 -1 0 173.14 153.66 2.84 o
9 -1 0 46.45 51.55 2.12 o
11 -1 0 34.93 37.39 2.15 o
2 0 0 7077.82 7822.40 19.13 o
4 0 0 299.37 311.00 2.63 o
6 0 0 1415.93 1495.09 7.10 o
8 0 0 792.61 806.47 6.59 o
10 0 0 27.10 24.80 1.84 o
3 1 0 1448.23 1435.91 4.35 o
5 1 0 201.35 196.21 2.63 o
7 1 0 165.56 148.68 2.87 o
9 1 0 45.55 49.04 2.13 o
11 1 0 36.29 38.03 2.23 o
0 2 0 7146.25 6460.35 16.25 o
2 2 0 2975.66 3049.65 4.18 o
4 2 0 1164.91 1123.81 23.56 o
6 2 0 617.73 678.50 6.85 o
8 2 0 232.94 253.00 4.06 o
10 2 0 48.79 42.84 2.15 o
1 3 0 1811.11 1621.37 4.58 o
3 3 0 440.62 514.96 12.56 o
5 3 0 46.00 52.25 1.82 o
7 3 0 372.95 401.20 4.53 o
9 3 0 48.77 51.41 2.40 o
11 3 0 7.17 6.81 1.42 o
0 4 0 659.64 689.64 3.52 o
2 4 0 245.92 224.30 1.35 o
4 4 0 962.64 1034.93 21.04 o
6 4 0 60.91 57.45 1.44 o
8 4 0 13.04 11.34 1.18 o
10 4 0 52.38 57.17 2.53 o
1 5 0 1078.89 1058.83 4.90 o
3 5 0 746.03 724.91 4.22 o
5 5 0 457.19 432.04 8.54 o
7 5 0 139.30 142.75 3.01 o
9 5 0 38.03 34.23 1.97 o
0 6 0 219.95 233.27 2.73 o
2 6 0 59.91 37.33 1.30 o
4 6 0 147.66 158.95 7.60 o
6 6 0 58.36 66.60 2.26 o
8 6 0 27.12 30.82 1.91 o
10 6 0 21.33 22.68 2.03 o
1 7 0 475.70 465.62 12.44 o
3 7 0 1306.51 1367.47 6.94 o
5 7 0 539.00 569.50 16.34 o
7 7 0 33.02 33.58 1.99 o
9 7 0 39.37 42.24 2.17 o
0 8 0 111.60 123.17 2.60 o
2 8 0 47.44 43.64 1.30 o
4 8 0 25.46 34.08 1.51 o
6 8 0 26.41 27.44 1.58 o
8 8 0 23.64 25.03 2.10 o
1 9 0 164.29 175.66 2.35 o
3 9 0 256.75 249.98 4.08 o
5 9 0 104.18 101.67 2.43 o
0 10 0 50.92 35.42 1.88 o
2 10 0 25.54 26.89 1.19 o
4 10 0 50.25 51.53 1.47 o
1 11 0 30.94 26.63 1.37 o
3 11 0 3.56 5.86 0.85 o
5 11 0 3.31 6.31 1.33 o
0 12 0 44.28 69.17 2.58 o
2 12 0 44.37 53.61 1.79 o
4 12 0 28.78 24.77 2.12 o
1 13 0 3.58 1.83 0.65 o
4 -7 1 38.86 40.10 1.51 o
6 -7 1 10.41 10.40 1.11 o
7 -7 1 34.88 36.75 1.64 o
8 -7 1 7.39 8.42 1.20 o
3 -6 1 27.29 31.08 1.33 o
5 -6 1 19.61 19.50 1.36 o
6 -6 1 69.08 67.35 2.03 o
7 -6 1 17.79 20.04 1.48 o
8 -6 1 8.18 6.47 1.02 o
9 -6 1 4.67 3.79 1.00 o
10 -6 1 21.65 19.54 1.63 o
3 -5 1 193.81 192.86 1.34 o
4 -5 1 61.06 64.42 0.97 o
5 -5 1 90.45 92.04 1.32 o
6 -5 1 33.32 35.49 1.02 o
8 -5 1 20.62 20.43 1.49 o
9 -5 1 12.94 13.74 1.44 o
10 -5 1 6.91 6.32 1.18 o
2 -4 1 48.29 46.50 0.72 o
3 -4 1 159.96 165.43 1.96 o
4 -4 1 66.64 69.48 0.98 o
5 -4 1 66.82 66.85 1.12 o
6 -4 1 96.19 98.51 1.52 o
7 -4 1 21.83 22.53 1.30 o
8 -4 1 50.25 54.48 2.09 o
9 -4 1 13.30 13.56 0.91 o
10 -4 1 3.40 3.70 0.87 o
11 -4 1 4.67 4.53 1.13 o
2 -3 1 247.19 260.15 5.68 o
3 -3 1 204.54 195.45 1.91 o
4 -3 1 115.55 112.54 1.23 o
5 -3 1 116.58 120.92 1.44 o
6 -3 1 72.06 71.72 1.67 o
7 -3 1 17.87 18.99 0.95 o
8 -3 1 21.26 23.06 1.16 o
9 -3 1 18.16 18.42 1.11 o
10 -3 1 5.60 5.59 0.66 o
11 -3 1 20.41 20.63 1.90 o
1 -2 1 406.50 383.69 2.28 o
2 -2 1 522.37 525.28 1.71 o
3 -2 1 350.59 351.30 1.73 o
4 -2 1 823.66 908.05 5.01 o
5 -2 1 122.14 125.39 1.46 o
6 -2 1 106.19 101.85 2.13 o
7 -2 1 33.81 32.88 2.53 o
8 -2 1 107.83 116.03 2.12 o
9 -2 1 16.78 15.58 0.86 o
10 -2 1 19.99 19.77 1.38 o
11 -2 1 5.81 4.64 0.65 o
1 -1 1 4139.93 4150.00 86.33 o
2 -1 1 336.01 347.37 10.49 o
3 -1 1 10.93 7.53 0.38 o
4 -1 1 200.14 218.66 1.64 o
5 -1 1 98.66 99.11 2.76 o
6 -1 1 58.37 64.00 2.36 o
7 -1 1 375.20 400.49 3.13 o
8 -1 1 18.96 19.16 1.04 o
9 -1 1 58.06 57.20 2.00 o
10 -1 1 11.30 10.64 0.82 o
11 -1 1 2.47 1.59 0.41 o
0 0 1 314.79 327.86 1.60 o
1 0 1 578.41 549.78 2.36 o
2 0 1 453.42 401.90 4.84 o
3 0 1 303.63 291.04 1.64 o
4 0 1 154.15 134.27 2.53 o
5 0 1 175.75 153.30 3.26 o
6 0 1 103.97 105.30 1.74 o
7 0 1 50.98 54.57 1.21 o
8 0 1 62.39 63.24 2.19 o
9 0 1 8.27 9.19 0.76 o
10 0 1 35.89 40.92 1.40 o
11 0 1 4.91 3.49 1.01 o
0 1 1 264.01 268.72 7.63 o
1 1 1 4149.63 4194.15 88.88 o
2 1 1 336.67 340.90 8.91 o
3 1 1 9.92 6.79 0.36 o
4 1 1 200.13 215.17 3.88 o
5 1 1 100.99 99.27 1.10 o
6 1 1 57.97 59.84 1.00 o
7 1 1 377.78 406.71 4.24 o
8 1 1 19.13 17.90 1.01 o
9 1 1 58.15 58.19 1.28 o
10 1 1 11.48 10.86 1.06 o
11 1 1 2.16 1.36 0.56 o
0 2 1 1247.42 1111.59 49.75 o
1 2 1 406.75 359.26 13.64 o
2 2 1 543.86 537.28 11.95 o
3 2 1 348.33 340.82 6.70 o
4 2 1 849.14 934.08 20.98 o
5 2 1 121.34 123.97 3.05 o
6 2 1 105.67 101.24 1.40 o
7 2 1 33.79 32.60 0.90 o
8 2 1 104.98 110.71 2.34 o
9 2 1 16.57 16.18 1.07 o
10 2 1 21.34 18.78 1.24 o
11 2 1 5.72 4.80 0.99 o
0 3 1 459.65 426.45 19.75 o
1 3 1 119.80 106.50 3.06 o
2 3 1 247.39 249.56 5.08 o
3 3 1 209.44 195.38 4.31 o
4 3 1 115.43 111.71 1.86 o
5 3 1 120.10 123.34 2.99 o
6 3 1 72.30 71.87 2.00 o
7 3 1 16.83 17.57 0.59 o
8 3 1 21.52 22.98 1.16 o
9 3 1 17.72 17.87 1.15 o
10 3 1 5.72 5.91 1.22 o
11 3 1 20.53 20.62 1.67 o
0 4 1 389.26 344.30 2.77 o
1 4 1 171.79 163.48 4.77 o
2 4 1 52.32 47.86 0.66 o
3 4 1 159.82 162.05 3.12 o
4 4 1 72.91 72.29 0.86 o
5 4 1 66.01 64.38 1.25 o
6 4 1 95.41 98.00 1.07 o
7 4 1 21.50 21.23 0.94 o
8 4 1 49.32 50.77 1.78 o
9 4 1 13.38 13.97 1.51 o
10 4 1 3.64 3.57 0.78 o
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4 3 4 104.75 104.66 1.97 o
5 3 4 23.06 22.80 0.89 o
6 3 4 98.63 100.24 1.96 o
7 3 4 35.35 33.00 1.78 o
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1 -2 5 25.40 29.22 1.13 o
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1 -1 5 6.89 5.30 0.67 o
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5 -1 5 16.04 13.02 1.25 o
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7 -1 5 3.26 3.29 0.73 o
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0 0 5 11.46 11.25 1.25 o
1 0 5 11.71 16.91 0.95 o
2 0 5 69.79 73.76 1.52 o
3 0 5 44.38 51.69 1.40 o
4 0 5 97.04 98.77 5.76 o
5 0 5 19.34 18.62 1.12 o
6 0 5 7.52 5.56 0.83 o
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1 1 5 6.80 5.36 0.71 o
2 1 5 9.21 10.97 0.66 o
3 1 5 34.95 32.66 1.37 o
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5 1 5 15.67 13.00 0.96 o
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7 1 5 3.49 2.74 1.34 o
8 1 5 3.28 2.78 0.78 o
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1 2 5 26.18 29.26 1.44 o
2 2 5 59.66 61.26 1.60 o
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7 2 5 9.54 10.40 1.14 o
8 2 5 10.40 9.40 0.76 o
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1 3 5 22.10 22.70 0.88 o
2 3 5 26.25 27.86 0.98 o
3 3 5 68.21 70.54 1.71 o
4 3 5 33.32 29.16 1.32 o
5 3 5 17.81 13.49 1.13 o
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1 6 5 21.92 23.04 1.02 o
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1 7 5 27.13 22.50 1.00 o
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1 8 5 7.10 8.64 1.03 o
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0 0 6 2.30 1.33 0.98 o
1 0 6 4.61 4.03 0.83 o
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1 1 6 3.88 4.11 0.77 o
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1 3 6 13.24 9.73 1.16 o
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3 5 6 21.09 18.27 2.88 o
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1 0 7 4.43 4.18 0.83 o
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1 2 7 0.65 0.72 0.83 o