#------------------------------------------------------------------------------ #$Date: 2017-07-04 01:26:09 +0300 (Tue, 04 Jul 2017) $ #$Revision: 198341 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/41/4514156.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4514156 loop_ _publ_author_name 'Toma\ 2\s(I)' _cod_data_source_file co7b00027_si_006.cif _cod_data_source_block shelx _cod_database_code 4514156 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.807 _shelx_estimated_absorpt_t_max 0.921 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL cu603 in P-1 CELL 1.54184 8.7645 11.9515 15.6337 111.859 95.746 91.269 ZERR 2.00 0.0003 0.0005 0.0008 0.004 0.003 0.003 LATT 1 SFAC C H N O UNIT 72 72 4 4 MERG 2 FMAP 2 PLAN 20 SIZE 0.150 0.200 0.400 ACTA BOND BOND $H CONF htab REM Instructions for potential hydrogen bonds HTAB N1 O1 EQIV $1 x+1, y, z HTAB N1 O2_$1 EQIV $2 x-1, y, z HTAB N2 O1_$2 HTAB N2 O2 L.S. 5 TEMP 20.00 WGHT 0.075900 0.119300 FVAR 8.28643 O1 4 0.959112 0.010388 0.379879 11.00000 0.05594 0.06171 = 0.06404 0.00933 0.00642 0.00496 O2 4 -0.195241 0.252841 0.511709 11.00000 0.05468 0.07482 = 0.08356 0.00489 0.00671 0.00524 N1 3 0.669985 0.048787 0.336349 11.00000 0.04583 0.06133 = 0.06377 0.01399 0.01138 0.01082 H1N 2 0.753837 0.074833 0.379444 11.00000 0.07280 N2 3 0.100733 0.220735 0.549617 11.00000 0.04687 0.06170 = 0.06519 0.01319 0.01217 0.00894 H2N 2 0.010696 0.185444 0.517155 11.00000 0.07461 C1 1 1.163529 -0.028498 0.183363 11.00000 0.07746 0.09728 = 0.09193 0.04267 0.02203 0.01150 AFIX 43 H1 2 1.111176 0.035429 0.220025 11.00000 -1.20000 AFIX 0 C2 1 1.235033 -0.017384 0.111461 11.00000 0.10372 0.16417 = 0.11592 0.08001 0.02017 -0.00352 AFIX 43 H2 2 1.229391 0.052919 0.099208 11.00000 -1.20000 AFIX 0 C3 1 1.315127 -0.112367 0.057974 11.00000 0.09309 0.20740 = 0.08143 0.03764 0.02647 -0.01793 AFIX 43 H3 2 1.364237 -0.105465 0.009954 11.00000 -1.20000 AFIX 0 C4 1 1.322019 -0.214871 0.075418 11.00000 0.09238 0.15017 = 0.09106 -0.00504 0.03773 0.00398 AFIX 43 H4 2 1.376229 -0.278185 0.039666 11.00000 -1.20000 AFIX 0 C5 1 1.249016 -0.225357 0.145858 11.00000 0.07319 0.08735 = 0.09175 0.00410 0.02457 0.01235 AFIX 43 H5 2 1.253490 -0.296707 0.156680 11.00000 -1.20000 AFIX 0 C6 1 1.168953 -0.132781 0.201222 11.00000 0.04606 0.06919 = 0.06418 0.01240 0.00642 0.00552 C7 1 1.097327 -0.144400 0.281428 11.00000 0.05336 0.06298 = 0.07173 0.02184 0.00942 0.01263 AFIX 23 H7A 2 1.172785 -0.115142 0.335938 11.00000 -1.20000 H7B 2 1.072881 -0.229376 0.267466 11.00000 -1.20000 AFIX 0 C8 1 0.952364 -0.076878 0.304806 11.00000 0.05025 0.05239 = 0.06080 0.01868 0.01302 0.00587 C9 1 0.815069 -0.111281 0.240421 11.00000 0.05079 0.05428 = 0.05712 0.01465 0.01122 0.00611 C10 1 0.803964 -0.212949 0.148470 11.00000 0.05181 0.05991 = 0.05937 0.01152 0.01193 0.00305 C11 1 0.829753 -0.330509 0.139727 11.00000 0.08075 0.06204 = 0.06959 0.01382 0.01492 0.00507 AFIX 43 H11 2 0.857081 -0.346949 0.192683 11.00000 -1.20000 AFIX 0 C12 1 0.815532 -0.424016 0.053441 11.00000 0.10564 0.06376 = 0.08471 0.00459 0.02093 0.00470 AFIX 43 H12 2 0.836218 -0.501911 0.048833 11.00000 -1.20000 AFIX 0 C13 1 0.771247 -0.402058 -0.024775 11.00000 0.11376 0.08728 = 0.07016 -0.00666 0.01692 -0.00201 AFIX 43 H13 2 0.759899 -0.465123 -0.082515 11.00000 -1.20000 AFIX 0 C14 1 0.743531 -0.286721 -0.017970 11.00000 0.11907 0.10618 = 0.06010 0.01713 0.00488 0.00590 AFIX 43 H14 2 0.712916 -0.271689 -0.071176 11.00000 -1.20000 AFIX 0 C15 1 0.760985 -0.192670 0.067821 11.00000 0.08728 0.07554 = 0.06524 0.01787 0.00796 0.00885 AFIX 43 H15 2 0.743641 -0.114604 0.071511 11.00000 -1.20000 AFIX 0 C16 1 0.685812 -0.045980 0.260789 11.00000 0.04909 0.05885 = 0.05903 0.01653 0.00867 0.00345 AFIX 43 H16 2 0.600601 -0.071874 0.216164 11.00000 -1.20000 AFIX 0 C17 1 0.530693 0.113556 0.352480 11.00000 0.04989 0.06662 = 0.07089 0.02401 0.01368 0.01686 AFIX 23 H17A 2 0.459317 0.083987 0.296104 11.00000 -1.20000 H17B 2 0.555627 0.198743 0.367576 11.00000 -1.20000 AFIX 0 C18 1 0.454688 0.098455 0.430455 11.00000 0.04749 0.05981 = 0.07459 0.02427 0.01532 0.01263 AFIX 23 H18A 2 0.529327 0.121094 0.485183 11.00000 -1.20000 H18B 2 0.422111 0.013991 0.412846 11.00000 -1.20000 AFIX 0 C19 1 0.316465 0.174039 0.454402 11.00000 0.05017 0.06284 = 0.07211 0.02498 0.01568 0.01543 AFIX 23 H19A 2 0.348949 0.258654 0.472749 11.00000 -1.20000 H19B 2 0.241894 0.151932 0.399682 11.00000 -1.20000 AFIX 0 C20 1 0.241117 0.156886 0.531974 11.00000 0.04958 0.06513 = 0.06961 0.02297 0.01388 0.01477 AFIX 23 H20A 2 0.217104 0.071375 0.515975 11.00000 -1.20000 H20B 2 0.312863 0.185787 0.588195 11.00000 -1.20000 AFIX 0 C21 1 0.100448 0.335576 0.603295 11.00000 0.05071 0.06277 = 0.05370 0.01822 0.01132 0.00548 AFIX 43 H21 2 0.193600 0.372278 0.637269 11.00000 -1.20000 AFIX 0 C22 1 -0.023428 0.407991 0.614831 11.00000 0.05250 0.06132 = 0.05223 0.01813 0.01510 0.01031 C23 1 0.006571 0.536580 0.680435 11.00000 0.05212 0.06064 = 0.05830 0.02129 0.01483 0.01085 C24 1 0.042794 0.627228 0.649760 11.00000 0.12299 0.07563 = 0.07522 0.02961 0.02797 -0.00690 AFIX 43 H24 2 0.043574 0.608838 0.586539 11.00000 -1.20000 AFIX 0 C25 1 0.077964 0.744972 0.711421 11.00000 0.13810 0.07026 = 0.11624 0.03543 0.03071 -0.01041 AFIX 43 H25 2 0.100493 0.804810 0.689134 11.00000 -1.20000 AFIX 0 C26 1 0.079867 0.773934 0.804299 11.00000 0.08983 0.06045 = 0.10210 0.01010 0.00691 0.00690 AFIX 43 H26 2 0.107848 0.852449 0.845645 11.00000 -1.20000 AFIX 0 C27 1 0.040269 0.686575 0.836376 11.00000 0.10542 0.07644 = 0.06609 0.00809 0.01252 0.01742 AFIX 43 H27 2 0.038296 0.706047 0.899641 11.00000 -1.20000 AFIX 0 C28 1 0.003039 0.568857 0.774421 11.00000 0.09170 0.06523 = 0.05927 0.01997 0.01645 0.01202 AFIX 43 H28 2 -0.024961 0.510377 0.796906 11.00000 -1.20000 AFIX 0 C29 1 -0.168686 0.361131 0.562015 11.00000 0.05373 0.07028 = 0.05826 0.01877 0.01495 0.01094 C30 1 -0.295715 0.446584 0.565165 11.00000 0.05992 0.08550 = 0.07026 0.02901 0.00730 0.01769 AFIX 23 H30A 2 -0.250747 0.522082 0.566285 11.00000 -1.20000 H30B 2 -0.366542 0.411741 0.508806 11.00000 -1.20000 AFIX 0 C31 1 -0.384938 0.473160 0.647727 11.00000 0.04852 0.07883 = 0.06370 0.01698 0.00150 0.01818 C32 1 -0.437588 0.586734 0.689026 11.00000 0.10040 0.09851 = 0.09320 0.03001 0.01705 0.04736 AFIX 43 H32 2 -0.412681 0.647475 0.668147 11.00000 -1.20000 AFIX 0 C33 1 -0.527005 0.611011 0.761141 11.00000 0.11328 0.12631 = 0.10201 0.01655 0.02736 0.06289 AFIX 43 H33 2 -0.563600 0.687400 0.787320 11.00000 -1.20000 AFIX 0 C34 1 -0.561809 0.524736 0.794015 11.00000 0.07410 0.15875 = 0.07669 0.01762 0.01834 0.03290 AFIX 43 H34 2 -0.621858 0.541970 0.842609 11.00000 -1.20000 AFIX 0 C35 1 -0.508376 0.411878 0.755546 11.00000 0.06610 0.13237 = 0.09001 0.03781 0.01490 0.00277 AFIX 43 H35 2 -0.530774 0.352757 0.778576 11.00000 -1.20000 AFIX 0 C36 1 -0.420494 0.386125 0.681903 11.00000 0.06003 0.08607 = 0.08207 0.02242 0.01417 0.00845 AFIX 43 H36 2 -0.385372 0.309253 0.655466 11.00000 -1.20000 AFIX 0 HKLF 4 REM cu603 in P-1 REM R1 = 0.0460 for 4956 Fo > 4sig(Fo) and 0.0560 for all 6138 data REM 369 parameters refined using 0 restraints END WGHT 0.0726 0.1291 REM Instructions for potential hydrogen bonds HTAB N1 O1 HTAB N1 O2_$1 HTAB N2 O1_$2 HTAB N2 O2 REM Highest difference peak 0.137, deepest hole -0.157, 1-sigma level 0.032 Q1 1 -0.0870 0.3929 0.5923 11.00000 0.05 0.14 Q2 1 0.1509 0.6897 0.6955 11.00000 0.05 0.14 Q3 1 0.8812 -0.0871 0.2650 11.00000 0.05 0.11 Q4 1 -0.3139 0.2305 0.4924 11.00000 0.05 0.11 Q5 1 1.0779 0.0391 0.3937 11.00000 0.05 0.10 Q6 1 -0.3557 0.4603 0.6893 11.00000 0.05 0.09 Q7 1 -0.3565 0.5361 0.6820 11.00000 0.05 0.09 Q8 1 0.3378 0.2595 0.6142 11.00000 0.05 0.09 Q9 1 -0.4681 0.5749 0.8118 11.00000 0.05 0.09 Q10 1 1.3269 -0.0235 0.0896 11.00000 0.05 0.09 Q11 1 -0.2565 0.2804 0.7114 11.00000 0.05 0.09 Q12 1 0.3939 0.2876 0.4980 11.00000 0.05 0.09 Q13 1 0.8108 -0.1584 0.1995 11.00000 0.05 0.09 Q14 1 0.5967 0.2258 0.4032 11.00000 0.05 0.09 Q15 1 -0.1641 0.4216 0.7233 11.00000 0.05 0.09 Q16 1 0.1277 0.5781 0.6532 11.00000 0.05 0.09 Q17 1 0.4683 0.0309 0.4766 11.00000 0.05 0.09 Q18 1 0.5708 0.1617 0.4822 11.00000 0.05 0.09 Q19 1 1.3546 -0.0264 0.0168 11.00000 0.05 0.08 Q20 1 -0.2280 0.4026 0.5691 11.00000 0.05 0.08 ; _shelx_res_checksum 99078 _shelx_hkl_file ; 0 0 2 91371.3 495.964 2 0 0 3 5258.43 150.458 2 0 0 4 84.1432 30.8838 2 0 0 5 4230.85 180.276 2 0 0 6 7672.71 271.834 2 0 0 7 10991.0 361.931 2 0 0 8 11919.7 408.231 2 0 0 9 1154.11 142.776 2 0 0 10 10281.7 444.028 2 0 0 11 520.694 74.2125 34 0 0 11 366.189 95.9015 2 0 0 -11 422.629 58.9844 13 0 0 12 210.015 53.1945 34 0 0 -12 263.747 47.8970 13 0 0 -12 203.926 51.1214 32 0 0 -13 2458.77 159.732 32 0 0 13 2619.18 179.202 34 0 0 -13 2644.22 150.385 13 0 0 14 124.001 53.2633 34 0 0 -14 154.817 43.4359 13 0 0 -14 171.334 49.0483 32 0 0 -15-16.9526 32.7821 32 0 0 15 46.5527 40.9518 43 0 0 15 50.4656 42.2220 34 0 0 16 480.544 70.3007 34 0 0 -16 426.563 59.6029 32 0 0 16 345.876 61.8243 43 0 0 17 508.264 60.0884 34 0 0 17 469.082 54.9072 43 0 0 -17 431.755 52.6503 31 0 1 -18-4.11676 14.2231 31 0 -1 18 1.22132 16.2992 34 0 -1 17 72.7416 29.7421 43 0 -1 17 74.6352 34.6033 34 0 1 -17 11.9535 21.8961 32 0 1 -16 309.156 55.1286 32 0 -1 16 254.926 59.9861 34 0 -1 16 325.434 64.1341 43 0 1 -15 1993.74 137.618 32 0 -1 15 1939.71 151.009 34 0 1 -14 285.229 58.6833 32 0 -1 14 269.671 68.3735 34 0 -1 13 398.778 74.0635 34 0 1 -13 375.771 58.2107 13 0 -1 12 8881.38 453.862 2 0 1 -12 8371.68 248.976 13 0 -1 12 8926.97 311.895 34 0 -1 11 16033.6 583.416 2 0 -1 10 8528.97 401.501 2 0 -1 9 15229.8 495.226 2 0 -1 8-23.0177 34.5870 2 0 -1 7 3646.10 204.024 2 0 -1 6 11814.0 328.788 2 0 -1 5 155566. 1062.29 2 0 -1 4 942.379 74.4908 2 0 -1 3 286851. 1082.83 2 0 -1 2 34818.2 313.906 2 0 -1 1 78219.8 398.658 2 0 -1 0 572.538 27.8669 3 0 1 1 53272.8 369.446 2 0 1 1 53364.1 247.959 1 0 1 2 58345.3 469.643 2 0 1 2 56901.8 282.792 1 0 1 3 35896.4 438.684 2 0 1 4 21611.4 381.513 2 0 -1 -5 1618.51 62.6492 4 0 1 5 1625.88 120.401 2 0 1 6 41308.8 664.427 2 0 1 7 2677.22 186.992 2 0 1 8 2634.94 201.982 2 0 1 9 4038.40 266.880 2 0 -1 -10 5155.40 201.597 32 0 1 10 5201.72 320.153 2 0 1 10 5835.45 229.383 34 0 -1 -11 2662.04 149.377 13 0 1 11 2970.31 178.826 34 0 1 11 3049.47 254.945 2 0 -1 -11 2765.33 159.939 32 0 -1 -11 3023.99 154.828 7 0 1 12 11600.9 363.215 34 0 -1 -12 11546.5 337.905 32 0 -1 -12 11122.7 312.012 13 0 1 13 2488.59 173.151 34 0 -1 -13 2440.49 158.661 32 0 1 14 529.403 90.5846 43 0 -1 -14 459.042 71.9535 32 0 1 14 404.638 75.8278 34 0 -1 -15 19.3285 30.2022 32 0 1 15-4.65870 38.6003 43 0 1 15 10.5121 33.6194 34 0 1 16 556.969 73.7711 43 0 -1 -16 594.237 63.3873 31 0 1 16 633.038 71.9618 34 0 -1 -17 236.848 31.0402 23 0 1 17 259.873 36.8225 34 0 1 17 197.057 33.1752 43 0 -2 18 21.9641 23.6628 34 0 2 -17 64.4843 29.5502 32 0 -2 17 34.8646 36.0944 34 0 -2 17 57.8667 24.4598 43 0 -2 16 1608.13 133.915 34 0 2 -16 1565.52 115.875 32 0 2 -15 2358.38 150.334 32 0 -2 15 2358.03 156.847 5 0 -2 15 2584.39 178.562 34 0 -2 14 2680.30 182.166 34 0 -2 13 5000.27 350.745 2 0 -2 13 4793.26 248.197 38 0 -2 13 5325.48 246.636 34 0 -2 12 1490.60 135.189 38 0 -2 12 1325.25 175.359 2 0 -2 11 4247.11 305.925 2 0 -2 10 3642.81 262.377 2 0 -2 9 15589.6 502.447 2 0 -2 8 888.368 112.809 2 0 -2 7 99536.7 1060.11 2 0 -2 6 19522.7 427.869 2 0 -2 5 3262.40 159.188 2 0 -2 4 167561. 1021.15 2 0 -2 3 999999. 2259.77 2 0 -2 1 219512. 753.381 3 0 -2 0 7191.30 141.761 3 0 -2 -1 17288.8 257.087 3 0 2 1 18212.2 214.563 1 0 2 2 1736.72 100.031 2 0 2 2 1773.93 63.6192 1 0 2 3 4159.41 84.9310 1 0 2 3 4335.80 171.886 2 0 2 4 3988.16 181.278 2 0 2 5 105486. 1017.47 2 0 -2 -5 104618. 610.508 4 0 2 6 5183.07 250.324 2 0 -2 -6 5104.30 141.174 4 0 2 7 2542.41 193.537 2 0 2 8 14.0909 27.2768 2 0 2 9 7744.93 381.227 2 0 -2 -10 54.1856 42.2536 3 0 -2 -10 24.2593 29.2655 13 0 -2 -10 26.2726 30.8227 32 0 2 10 5.27525 30.7108 34 0 2 10 94.4198 45.5235 2 0 -2 -11 150.241 48.7877 32 0 -2 -11 126.849 40.5603 13 0 -2 -11 269.635 53.0909 7 0 2 11 160.085 55.9101 34 0 -2 -12 764.454 92.8210 32 0 2 12 827.476 102.267 34 0 -2 -12 821.454 85.8900 7 0 2 13 129.563 50.6729 34 0 2 13 96.0592 61.6257 43 0 -2 -13 142.687 53.3608 32 0 2 14 265.021 61.4599 34 0 2 14 227.690 67.4279 43 0 -2 -15 93.0208 37.8857 23 0 2 15 59.9351 44.4443 43 0 2 15 68.9999 38.6075 34 0 2 16 106.759 34.3487 43 0 -2 -16 90.9131 26.1334 23 0 2 16 75.8584 26.8951 34 0 -3 19 10.5639 14.8561 34 0 3 -19 45.0518 18.4631 31 0 3 -18 35.8211 19.0504 32 0 -3 18 92.2228 31.1077 34 0 -3 17 1069.25 104.034 34 0 3 -17 969.107 82.0054 32 0 -3 16 389.540 77.7231 34 0 3 -16 296.885 54.1702 32 0 3 -16 303.684 62.9479 10 0 -3 15 940.058 100.708 5 0 -3 15 1248.56 126.608 34 0 -3 14 2968.69 185.379 5 0 -3 14 3497.76 208.397 34 0 -3 14 3122.65 213.653 38 0 -3 13 219.645 80.6891 2 0 -3 13 195.586 62.8447 38 0 -3 12 196.745 46.4454 17 0 -3 12 226.859 76.2480 2 0 -3 12 224.817 56.1415 38 0 -3 11 5411.59 347.380 2 0 -3 10 22374.0 657.249 2 0 -3 9 534.285 105.700 2 0 -3 8 6905.23 318.854 2 0 -3 7 30346.8 613.701 2 0 -3 6 150.203 55.1334 2 0 -3 5 4951.03 129.761 5 0 -3 5 5315.69 217.521 2 0 -3 4 115852. 939.133 2 0 -3 4 117593. 575.508 5 0 -3 3 159785. 1040.94 2 0 -3 3 160015. 624.820 5 0 -3 2 34151.4 276.393 5 0 -3 1 2272.62 95.7660 3 0 -3 1 2300.12 71.3410 5 0 -3 0 4169.46 135.854 3 0 3 1 12407.3 225.137 1 0 -3 -1 12092.2 253.771 3 0 3 2 2361.93 132.935 2 0 3 2 2320.83 89.3290 1 0 -3 -2 2282.60 124.974 3 0 -3 -3 1607.77 118.857 3 0 3 3 1522.31 58.6084 1 0 3 3 1505.19 114.623 2 0 -3 -4 27093.7 551.144 3 0 3 4 28632.3 540.438 2 0 -3 -5 63954.4 567.595 4 0 3 5 64375.0 871.512 2 0 -3 -6 9986.46 233.287 4 0 3 6 10006.2 370.394 2 0 -3 -6 9752.75 396.841 3 0 3 7 312.130 72.9927 2 0 -3 -7 657.794 111.840 3 0 -3 -8 44076.4 970.294 3 0 3 8 46180.1 907.834 2 0 -3 -9 10169.2 300.622 32 0 3 9 10772.0 459.713 2 0 -3 -9 10652.9 292.949 7 0 -3 -9 10193.4 490.665 3 0 -3 -9 9881.20 288.719 13 0 3 9 10712.2 323.330 34 0 3 10 103.152 44.3300 34 0 -3 -10 115.224 41.9066 32 0 -3 -10-19.5411 26.8853 7 0 -3 -10 131.088 56.8433 3 0 -3 -11 240.861 60.6662 32 0 -3 -11 194.418 49.1628 7 0 3 11 213.195 67.3718 43 0 3 11 184.439 55.4274 34 0 -3 -12 2598.50 148.958 7 0 3 12 2614.04 194.132 43 0 3 12 2261.44 162.890 34 0 3 13-9.23579 31.3356 34 0 3 13-37.0582 63.0491 43 0 -3 -14 1083.33 99.1414 23 0 3 14 1094.73 98.1160 34 0 3 14 1003.67 110.826 43 0 3 15 2777.95 145.543 43 0 -3 -15 2842.82 131.665 23 0 3 15 2545.32 125.109 34 0 -4 19 433.092 45.4110 34 0 4 -18 38.2574 19.1348 32 0 4 -18 9.45260 13.9544 10 0 -4 17 602.390 84.4372 34 0 4 -17 582.058 67.1184 32 0 4 -17 522.139 75.1136 10 0 -4 16 36.0937 45.9275 34 0 -4 15 2034.91 175.753 38 0 -4 15 1845.74 141.037 5 0 -4 14-26.8346 33.8724 5 0 -4 14-25.8431 54.7304 38 0 -4 13 1324.26 122.202 17 0 -4 13 1472.32 151.912 38 0 -4 13 1449.46 130.463 5 0 -4 13 1511.16 202.677 2 0 -4 12 930.205 159.802 2 0 -4 12 882.226 94.7221 17 0 -4 12 1026.98 108.256 5 0 -4 12 1094.65 128.105 38 0 -4 11 2795.25 253.749 2 0 -4 11 2594.35 157.761 5 0 -4 10 20.5176 31.7047 5 0 -4 10 156.462 75.5397 2 0 -4 9 145.455 39.3870 5 0 -4 9 282.046 86.4241 2 0 -4 8 2596.21 202.469 2 0 -4 8 2746.73 129.116 5 0 -4 7 1662.25 152.524 2 0 -4 7 1721.31 95.9972 5 0 -4 6 30326.5 601.354 2 0 -4 6 28448.7 357.625 5 0 -4 5 6605.03 264.029 2 0 -4 5 6562.90 159.661 5 0 4 -5 6379.17 150.499 6 0 -4 4 3405.06 109.524 5 0 4 -4 3539.70 103.997 6 0 4 -3 14337.9 198.589 6 0 -4 3 14753.5 218.843 5 0 -4 2 2504.48 88.1504 5 0 -4 1 7519.35 152.565 5 0 -4 1 7513.87 202.496 3 0 4 0 5901.35 202.424 1 0 -4 0 5842.41 189.306 3 0 4 1 12473.4 336.797 2 0 -4 -1 11772.7 291.290 3 0 4 1 12206.9 261.335 1 0 4 2 14999.5 384.582 2 0 4 2 14587.7 261.236 1 0 -4 -2 14112.7 349.146 3 0 -4 -3 192044. 1412.83 3 0 4 3 196423. 1472.18 2 0 -4 -4 11117.2 372.402 3 0 4 4 11737.4 381.560 2 0 4 5 1171.69 131.746 2 0 -4 -5 1483.86 101.189 4 0 -4 -5 1109.66 129.221 3 0 4 6 6184.91 314.339 2 0 -4 -6 5987.69 322.768 3 0 -4 -6 6410.53 212.077 4 0 4 7 3384.18 246.487 2 0 -4 -7 3333.85 256.853 3 0 4 8 463.214 94.0496 2 0 -4 -8 269.659 78.3211 3 0 4 8 469.336 68.8851 34 0 4 8 524.090 83.6681 43 0 -4 -8 469.526 67.5072 32 0 -4 -8 476.925 63.5497 7 0 4 9 6205.25 259.131 34 0 -4 -9 6070.52 374.768 3 0 -4 -9 6520.98 246.711 7 0 -4 -9 6013.83 247.671 32 0 4 9 6455.39 288.997 43 0 4 10 6359.65 295.663 43 0 4 10 6325.31 268.160 34 0 -4 -10 6524.36 247.966 7 0 4 11 5881.31 258.036 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86.2673 32.4823 10 0 -11 14-9.37968 31.3118 17 0 -11 13 31.2744 46.4766 30 0 -11 13 8.32135 29.1703 33 0 -11 13-22.7221 32.3698 17 0 -11 12 29.8537 37.8273 17 0 -11 12 28.7298 49.0242 30 0 -11 12-3.95665 31.6244 33 0 -11 11 424.874 67.5052 33 0 -11 11 479.940 90.8568 30 0 -11 11 304.915 58.1411 17 0 -11 10 107.474 40.7408 33 0 -11 10 69.3455 34.7289 17 0 -11 10 52.7080 43.0286 9 0 -11 10 92.2931 52.2806 30 0 -11 9 1714.08 148.967 30 0 -11 9 1729.84 130.276 33 0 -11 9 1801.48 128.400 17 0 -11 9 1693.07 133.911 9 0 -11 8 109.501 35.4230 33 0 -11 8 67.6224 36.4581 9 0 -11 7 69.4287 32.6704 9 0 -11 7 68.3254 31.6417 33 0 -11 6 179.372 49.7695 9 0 -11 6 186.918 57.5344 12 0 -11 6 129.492 42.3480 4 0 -11 5 400.209 70.6762 4 0 -11 5 442.449 82.2402 16 0 -11 5 487.861 77.2490 12 0 -11 5 459.986 77.4050 14 0 -11 5 434.349 69.0276 9 0 -11 4 14.2546 45.0074 16 0 -11 4 12.3361 37.0706 14 0 -11 4 40.6982 33.5611 12 0 -11 4 2.79554 29.7549 4 0 -11 4 57.9568 36.1977 9 0 -11 3 4858.99 252.362 4 0 -11 3 5101.17 243.322 14 0 -11 3 5252.37 213.859 9 0 -11 3 5232.84 238.003 12 0 -11 3 5348.14 252.993 16 0 -11 2 147.281 58.3474 16 0 -11 2 122.101 38.5525 9 0 -11 2 18.6342 38.5951 12 0 -11 2 154.781 46.0748 4 0 -11 2 147.935 55.0666 14 0 -11 1 1456.45 127.463 12 0 -11 1 1484.59 134.584 14 0 -11 1 1519.77 139.636 16 0 -11 1 1664.70 150.667 4 0 -11 0 1178.21 113.289 12 0 -11 0 1184.36 126.292 4 0 -11 0 1269.32 126.603 16 0 -11 0 1122.08 120.688 14 0 -11 -1 1900.91 154.475 16 0 -11 -1 1959.99 150.862 14 0 -11 -1 1904.61 139.922 12 0 -11 -2 3411.79 179.057 12 0 -11 -2 3559.94 193.653 14 0 -11 -2 3469.05 197.353 16 0 -11 -3 70.2396 35.5456 12 0 -11 -3 91.8397 43.4933 14 0 -11 -3 79.6524 45.2977 16 0 -11 -4 15.4753 27.5576 14 0 -11 -4 32.8842 24.8158 12 0 -11 -4 66.2423 25.7646 19 0 -11 -4 15.6000 31.0226 16 0 -11 -5 32.2022 25.1218 16 0 -11 -5 38.8666 24.0342 14 0 -11 -5 52.8754 24.6450 12 0 -11 -6 138.083 24.4801 12 0 -11 -6 186.663 29.4784 14 0 -11 -6 158.021 32.6591 16 0 11 6 104.840 26.2890 37 0 -12 16-38.1322 22.1591 30 0 -12 16-6.59135 11.2357 11 0 -12 15 6.26973 29.9507 30 0 -12 15 67.9194 29.0052 11 0 -12 14-9.43284 30.9376 30 0 -12 14-11.3909 22.8936 33 0 -12 13 145.388 37.5308 33 0 -12 13 75.7331 28.5857 17 0 -12 13 133.745 46.8189 30 0 -12 12 964.701 107.078 30 0 -12 12 1000.26 87.9383 17 0 -12 12 1117.59 93.1957 33 0 -12 11 56.7333 36.1197 30 0 -12 11 23.4431 21.7925 17 0 -12 11-5.53904 29.2521 33 0 -12 10 546.165 79.0226 30 0 -12 10 602.827 75.3121 33 0 -12 9 179.518 44.3775 33 0 -12 9 198.901 52.4115 9 0 -12 8 145.790 43.4810 33 0 -12 8 133.485 46.1074 9 0 -12 7 33.2294 30.6084 33 0 -12 7 19.1609 35.3935 9 0 -12 6 1558.27 119.791 9 0 -12 6 1654.00 121.596 33 0 -12 5 71.9917 41.5564 12 0 -12 5 87.7628 37.6070 9 0 -12 4 44.4653 36.6362 12 0 -12 4 49.7917 33.7647 9 0 -12 4 44.7299 45.4162 14 0 -12 4 21.6008 40.5441 16 0 -12 3 28.5932 36.0746 12 0 -12 3 6.24023 21.7061 9 0 -12 3 13.7953 39.4059 14 0 -12 3 22.6158 42.0058 16 0 -12 2 58.9369 33.3784 12 0 -12 2 56.3501 43.2274 16 0 -12 2 28.0794 43.0378 14 0 -12 1 65.9209 46.0872 14 0 -12 1-17.0475 44.1682 16 0 -12 1-54.3043 34.3842 12 0 -12 0 13.1705 36.1314 16 0 -12 0-2.08312 36.7589 14 0 -12 0-5.58453 27.6061 12 0 -12 -1 787.993 88.8082 16 0 -12 -1 747.619 85.2557 14 0 -12 -1 719.074 75.1925 12 0 -12 -2 3238.38 154.984 14 0 -12 -2 2827.80 148.730 19 0 -12 -2 3046.54 137.234 12 0 -12 -2 3120.38 156.069 16 0 -12 -3 107.502 31.1955 14 0 -12 -3 154.897 30.2603 19 0 -12 -3 140.665 29.7136 12 0 -12 -3 98.2596 31.6865 16 0 -12 -4 15.7402 18.4105 16 0 -12 -4-5.95314 9.66123 12 0 -12 -4-5.01125 15.5485 14 0 -13 15 62.3004 20.4625 11 0 -13 14 89.1431 26.7384 30 0 -13 14 66.7727 27.0757 11 0 -13 13 84.9286 26.4720 30 0 -13 13 167.715 31.3473 33 0 -13 12-83.8968 26.9245 30 0 -13 12-7.82089 20.7913 33 0 -13 11 10.9867 22.3570 33 0 -13 10 255.963 44.9536 33 0 -13 9 46.9234 27.7621 33 0 -13 8-4.55614 25.0457 9 0 -13 8 26.3319 27.9385 19 0 -13 8-17.6477 23.9299 33 0 -13 7 1324.29 96.9468 33 0 -13 7 1277.01 96.6176 9 0 -13 7 1340.90 114.203 19 0 -13 6 40.9960 24.1727 33 0 -13 6 9.21415 21.6520 9 0 -13 5 288.293 48.3496 33 0 -13 5 237.197 41.3098 9 0 -13 4 543.184 56.7069 9 0 -13 3-40.0211 29.3535 12 0 -13 2 44.9987 30.4527 16 0 -13 2 68.6353 34.8620 14 0 -13 2 16.8101 22.7951 12 0 -13 1 52.9674 32.9189 14 0 -13 1 13.1344 26.6616 16 0 -13 1 56.1066 38.2087 19 0 -13 1 12.9709 21.6238 12 0 -13 0-8.21907 29.1955 19 0 -13 0-16.4355 16.7317 12 0 -13 0 28.2926 26.0204 16 0 -13 0 27.0606 22.3457 14 0 -13 -1 335.729 45.0122 16 0 -13 -1 332.965 44.6119 14 0 -13 -1 276.910 41.1695 19 0 -13 -1 288.283 33.3927 12 0 -13 -2 45.9840 17.7773 16 0 -14 13 23.0279 14.8900 11 0 -14 12 572.007 54.3007 11 0 -14 11-4.11561 15.0620 11 0 -14 11-3.77397 12.0112 33 0 -14 10 2.46520 12.4013 11 0 -14 10 23.1175 15.1964 33 0 -14 9 27.8073 16.5642 33 0 -14 9 7.75342 11.2975 11 0 -14 8 15.5544 15.4649 33 0 -14 8-1.12319 11.6052 19 0 -14 7 321.280 47.4474 41 0 -14 7 455.022 45.2330 33 0 -14 7 415.858 53.8664 19 0 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1 -13 1 1609.91 106.899 16 1 -13 1 1584.63 106.931 14 1 -13 2 122.767 28.1900 9 1 -13 2 127.973 39.9109 14 1 -13 3 117.260 32.2595 9 1 -13 4 317.714 49.1038 9 1 -13 5 208.403 46.5762 33 1 -13 5 207.108 43.6291 9 1 -13 6 47.5650 32.6259 9 1 -13 6-5.49473 30.6558 33 1 -13 7 1882.32 124.341 9 1 -13 7 1904.53 124.440 33 1 -13 8 1459.31 105.720 19 1 -13 8 1416.82 110.154 9 1 -13 8 1386.85 105.998 33 1 -13 9 348.508 56.0282 33 1 -13 9 463.328 66.0524 9 1 -13 10 466.244 61.9062 33 1 -13 11 787.547 76.0774 33 1 -13 11 682.580 62.2200 17 1 -13 12 16.6369 16.9620 17 1 -13 12-11.2517 22.4506 33 1 -13 12-26.1059 21.0440 30 1 -13 13-20.6713 17.9005 30 1 -13 13 9.59909 12.7945 17 1 -13 13 26.1460 21.5149 33 1 -13 14 76.7340 23.5549 30 1 -13 14 46.2311 19.6383 33 1 -12 -4 239.790 35.3134 16 1 -12 -4 277.618 38.7903 14 1 -12 -3 316.238 46.6890 16 1 -12 -3 367.636 50.8663 14 1 -12 -2 279.424 37.7216 12 1 -12 -2 206.329 45.2792 16 1 -12 -2 266.784 51.3490 14 1 -12 -1 119.328 41.9077 16 1 -12 -1 119.886 30.6141 12 1 -12 -1 82.8551 41.1158 14 1 -12 0 1326.41 114.688 14 1 -12 0 1229.91 107.602 16 1 -12 0 1397.87 98.7406 12 1 -12 0 1145.00 84.3034 9 1 -12 1 34.6411 24.2639 9 1 -12 1 56.9810 40.8195 14 1 -12 1 29.2219 32.7147 16 1 -12 1 91.3494 32.3467 12 1 -12 2 885.433 85.0726 9 1 -12 2 886.903 100.973 14 1 -12 2 836.761 83.5954 12 1 -12 2 898.658 100.764 16 1 -12 3 1155.82 108.724 14 1 -12 3 1153.34 99.6339 12 1 -12 3 1184.28 102.999 9 1 -12 3 1104.71 115.994 16 1 -12 4 89.7651 43.5160 16 1 -12 4 71.9513 40.5216 9 1 -12 4 37.5224 35.4271 14 1 -12 5 66.2082 33.9880 9 1 -12 6 62.5698 44.8956 9 1 -12 7 1918.75 138.283 33 1 -12 7 1799.09 134.669 9 1 -12 8 2601.46 161.766 9 1 -12 8 2633.55 161.402 33 1 -12 9 2985.22 168.286 33 1 -12 9 2798.31 168.023 9 1 -12 9 2532.08 144.163 17 1 -12 10 67.9289 32.1964 17 1 -12 10 59.5793 39.1845 33 1 -12 10 69.1517 39.8546 30 1 -12 10 16.8214 40.7846 9 1 -12 11 1078.48 96.6982 17 1 -12 11 1145.58 114.326 30 1 -12 11 1206.87 105.539 33 1 -12 12 467.807 67.1020 33 1 -12 12 402.307 71.7514 30 1 -12 12 434.377 62.8969 17 1 -12 13 17.1467 28.4374 33 1 -12 13 39.8576 37.7576 30 1 -12 13 45.7579 26.8303 17 1 -12 14 151.460 32.9784 17 1 -12 14 184.644 41.6281 33 1 -12 14 148.256 43.8250 30 1 -12 15 47.4977 30.7947 30 1 -12 16-22.5068 18.9870 30 1 -11 -6 170.594 31.7143 16 -1 11 6 103.738 26.8443 37 1 -11 -6 145.900 30.1918 14 1 -11 -5 12.4918 13.2029 12 -1 11 5 11.5395 21.8609 37 1 -11 -5-3.07543 22.3103 16 1 -11 -5 1.83372 23.0397 14 -1 11 4 330.040 53.6677 37 1 -11 -4 402.214 49.0129 12 1 -11 -4 347.704 59.1122 16 1 -11 -4 371.036 60.9587 14 1 -11 -3 1069.16 87.6639 12 1 -11 -3 1114.42 108.338 14 -1 11 3 1036.92 98.3386 37 1 -11 -3 1027.43 101.412 16 1 -11 -2 132.455 56.5989 14 1 -11 -2 178.238 43.1490 12 1 -11 -2 100.513 45.2124 16 1 -11 -1 25.4455 27.2841 12 1 -11 -1 17.0606 36.4763 16 1 -11 -1 10.1554 21.3327 9 1 -11 -1 33.6777 43.7398 14 1 -11 0 379.538 77.4628 4 1 -11 0 381.265 74.6140 16 1 -11 0 361.413 57.7452 9 1 -11 0 332.810 71.6779 14 1 -11 0 284.644 54.9753 12 1 -11 1 51.1403 38.4895 16 1 -11 1 53.9459 35.9833 4 1 -11 1 15.9186 26.9152 12 1 -11 1 52.4614 43.0218 14 1 -11 1 10.3642 32.8227 9 1 -11 2 765.008 100.300 16 1 -11 2 788.675 88.2009 9 1 -11 2 702.901 83.3116 12 1 -11 2 760.900 96.1448 14 1 -11 2 744.314 103.574 4 1 -11 3 1600.39 125.836 12 1 -11 3 1844.03 135.686 9 1 -11 3 1810.86 143.250 14 1 -11 3 1805.32 148.966 16 1 -11 4 9745.19 310.233 9 1 -11 4 9467.89 304.599 12 1 -11 4 9303.46 329.270 16 1 -11 4 9811.57 321.113 14 1 -11 5 10498.5 349.367 16 1 -11 5 10162.0 322.138 9 1 -11 5 9758.54 317.260 14 1 -11 5 10087.9 314.722 12 1 -11 6 534.527 78.5186 9 1 -11 7-25.8553 31.2607 17 1 -11 7 33.3576 39.2642 9 1 -11 8 1917.74 143.552 33 1 -11 8 1710.49 137.151 9 1 -11 8 1932.98 136.987 17 1 -11 9 508.424 82.6589 30 1 -11 9 361.240 72.2060 9 1 -11 9 467.565 76.0181 33 1 -11 9 425.258 75.2359 17 1 -11 10 1087.68 111.023 33 1 -11 10 1082.00 109.172 17 1 -11 10 1049.85 110.791 9 1 -11 10 1078.86 126.589 30 1 -11 11 435.564 85.3782 30 1 -11 11 479.331 77.7473 33 1 -11 11 379.906 71.1188 17 1 -11 12-15.4225 38.3353 33 1 -11 12-30.2989 42.2732 17 1 -11 12 27.5821 44.1817 30 1 -11 13 168.865 51.3017 17 1 -11 13 131.037 46.0685 38 1 -11 13 242.823 68.6812 30 1 -11 13 200.523 50.5471 33 1 -11 14 16.3873 38.1510 30 -1 11 -14-2.74318 12.4269 10 1 -11 14 11.3207 33.6790 33 1 -11 14-12.5328 36.6063 38 1 -11 14-27.7962 35.2137 17 -1 11 -15 332.992 49.5285 10 1 -11 15 366.064 70.1807 30 1 -11 15 429.314 59.8609 33 1 -11 15 370.755 58.6873 17 -1 11 -16 156.585 29.5597 10 1 -11 16 68.7525 38.1788 30 1 -11 16 108.135 24.6694 11 1 -11 17 21.4933 17.5145 30 1 -10 -8 711.157 53.9197 14 -1 10 8 713.350 67.3933 37 1 -10 -8 715.238 55.4875 16 -1 10 7 74.5946 34.3848 37 1 -10 -7 64.0742 25.4157 14 1 -10 -7 83.3271 23.2477 12 1 -10 -6 26.4052 26.8174 14 1 -10 -6-3.02441 14.2797 12 1 -10 -5 209.795 54.8926 14 1 -10 -5 222.892 45.0137 12 1 -10 -4 362.706 73.2349 14 1 -10 -4 311.142 53.5561 12 1 -10 -3 702.016 83.6794 12 1 -10 -3 700.670 98.7087 14 1 -10 -3 627.298 87.1679 4 1 -10 -2 937.146 112.942 14 1 -10 -2 1031.68 104.401 12 1 -10 -2 874.216 110.227 4 1 -10 -1 331.633 71.0845 14 1 -10 -1 486.302 74.2283 12 1 -10 -1 412.635 83.0837 4 1 -10 0 630.692 84.4122 12 1 -10 0 669.083 80.1956 9 1 -10 0 622.012 90.2846 14 1 -10 0 610.172 93.0610 16 1 -10 1 16.7066 24.4388 12 1 -10 1 22.6505 37.6276 14 1 -10 1-19.6492 27.0128 9 1 -10 1 20.7846 37.1198 16 1 -10 2 5716.74 231.907 9 1 -10 2 5847.57 256.235 16 1 -10 2 5663.68 233.652 12 1 -10 2 5346.57 241.275 14 1 -10 3 27.9117 36.3182 14 1 -10 3 64.5981 38.8583 9 1 -10 3-20.5920 50.6452 16 1 -10 3-6.03099 34.1682 12 1 -10 4 12489.3 351.001 14 1 -10 4 12885.6 351.159 9 1 -10 4 12054.9 337.937 12 1 -10 4 12528.4 367.373 16 1 -10 5 6866.81 272.035 16 1 -10 5 6533.92 251.260 14 1 -10 5 6513.71 249.321 12 1 -10 5 6969.20 261.683 9 -1 10 -5 6631.89 417.711 1 1 -10 6 57.8007 32.1527 9 -1 10 -6 121.102 67.1236 1 1 -10 6 131.588 40.0911 17 1 -10 6 20.2479 24.9497 14 1 -10 7 1022.89 105.539 9 1 -10 7 1018.89 100.239 17 1 -10 8 3833.38 199.390 33 1 -10 8 3901.96 201.066 17 1 -10 8 3883.72 198.825 9 1 -10 9 2422.21 163.772 17 1 -10 9 2386.39 160.037 33 1 -10 9 2322.40 156.497 9 1 -10 10 2168.53 156.748 17 1 -10 10 2329.28 158.995 9 1 -10 10 2328.01 158.974 33 1 -10 11 615.206 90.4370 17 1 -10 11 663.900 87.9311 33 1 -10 11 645.766 86.9191 9 1 -10 11 634.335 96.2083 38 1 -10 12 12.7067 42.9833 17 1 -10 12 18.7794 46.7985 38 1 -10 12-30.9075 44.4739 33 1 -10 13 116.507 44.5861 33 -1 10 -13 84.0513 41.6895 10 1 -10 13 150.609 59.1348 38 1 -10 13 101.299 48.7140 17 1 -10 14 783.639 118.917 30 1 -10 14 617.876 92.5402 38 -1 10 -14 727.812 93.8094 10 1 -10 14 730.512 89.4406 33 1 -10 14 736.044 92.1865 17 1 -10 15-9.05141 36.6656 17 -1 10 -15 1.95666 24.0476 10 1 -10 15 81.6593 55.7825 30 1 -10 15 26.5976 34.6979 33 1 -10 16 278.604 61.3059 30 -1 10 -16 202.291 44.7403 10 1 -10 17 19.2095 23.7952 30 -1 10 -17-47.2079 25.1797 10 1 -10 18-7.00872 12.2335 34 -1 9 10 84.6933 24.4910 37 1 -9 -9 10.0984 11.8552 12 1 -9 -9 6.10004 16.0037 14 1 -9 -8-47.4617 22.0266 12 1 -9 -8 12.1574 20.9311 14 1 -9 -7 15.0645 20.4552 12 1 -9 -7 44.9111 32.6999 14 1 -9 -6 435.464 63.5758 12 1 -9 -6 587.511 88.0032 14 1 -9 -5 1434.74 124.975 4 1 -9 -5 1674.11 127.516 12 1 -9 -5 1773.15 144.853 14 1 -9 -4 807.081 100.765 4 1 -9 -4 963.027 114.569 14 1 -9 -4 848.585 95.2242 12 1 -9 -3 4449.75 229.705 14 1 -9 -3 4032.82 201.641 12 1 -9 -3 4206.02 236.955 4 1 -9 -2 8.99375 33.5898 12 1 -9 -2 91.1765 50.3387 14 1 -9 -1 2219.46 147.176 12 1 -9 -1 2445.50 166.456 14 -1 9 1 2111.70 224.737 2 1 -9 0 2182.79 154.174 14 -1 9 0 2015.09 221.860 2 1 -9 0 1948.44 135.138 12 1 -9 1 2306.29 152.770 14 1 -9 1 2298.22 143.110 12 -1 9 -1 2512.84 248.143 2 1 -9 2 15015.3 358.967 12 1 -9 2 16275.4 398.997 16 1 -9 2 16284.3 391.166 14 -1 9 -2 15480.7 616.803 2 1 -9 3 509.897 68.8689 9 1 -9 3 489.321 69.9957 14 1 -9 3 406.877 59.3653 12 1 -9 3 410.813 65.5331 16 -1 9 -3 460.802 102.855 1 1 -9 4 2833.82 156.173 9 1 -9 4 2493.32 146.020 12 1 -9 4 2851.90 163.836 16 -1 9 -4 2727.44 260.117 1 1 -9 4 2724.53 152.115 14 1 -9 5-13.3441 21.6079 14 1 -9 5-19.4577 27.8855 16 -1 9 -5 5.83913 37.7156 1 1 -9 5 27.3593 25.1709 17 1 -9 5 10.1404 21.3372 12 1 -9 5-0.81481 22.3156 9 -1 9 -6 807.348 150.451 1 1 -9 6 841.720 88.3169 9 1 -9 6 955.082 91.1299 17 1 -9 6 771.232 81.1879 14 1 -9 7 76.5646 36.8473 9 1 -9 7 101.140 33.0088 5 -1 9 -7 69.2349 53.6986 1 1 -9 8 7601.52 273.743 17 1 -9 8 7462.71 244.544 5 1 -9 8 7731.96 272.182 9 -1 9 -8 7901.60 496.541 1 1 -9 8 7180.89 263.183 33 1 -9 9 270.242 57.9858 33 1 -9 9 298.653 62.0417 9 1 -9 9 273.582 51.5166 5 1 -9 9 277.285 64.9744 17 -1 9 -9 328.770 115.713 1 1 -9 10 3.58133 32.7842 9 1 -9 10 19.6946 18.6509 5 1 -9 10 68.1659 49.1903 38 1 -9 10 13.5217 29.9806 33 1 -9 11 25.4609 38.2247 33 1 -9 11 148.152 59.5290 17 1 -9 11 17.1864 42.6420 38 1 -9 12 1364.62 148.391 38 1 -9 12 1352.17 123.684 33 1 -9 12 1454.04 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377.411 14 1 -8 -1 277.599 53.5029 14 1 -8 -1 209.013 45.5673 12 -1 8 1 198.569 82.8702 2 -1 8 0 375.035 97.7185 2 -1 8 -1 7859.24 415.561 2 -1 8 -2 703.712 122.119 1 -1 8 -3 3786.20 285.267 1 -1 8 -4 407.189 102.176 1 -1 8 -5 6763.30 407.015 1 -1 8 -6 2152.55 241.659 1 1 -8 6 2269.72 127.095 5 -1 8 -7 7014.24 439.676 1 1 -8 7 6897.22 224.087 5 1 -8 8 340.401 56.0922 33 -1 8 -8 246.359 101.115 1 1 -8 8 219.395 42.1663 5 1 -8 8 211.989 44.7723 9 1 -8 8 348.184 58.6815 17 1 -8 9 1642.85 129.614 17 1 -8 9 1522.76 110.403 5 -1 8 -9 1857.41 247.320 1 1 -8 9 1680.50 124.566 33 1 -8 9 1473.55 115.342 9 1 -8 10 83.8062 36.2492 9 1 -8 10 74.2143 39.1030 17 1 -8 10 5.84043 31.2139 5 -1 8 -10 42.6334 35.4070 6 1 -8 10 69.6698 36.2961 33 -1 8 -10 2.88798 58.1500 1 1 -8 11 3523.56 202.982 17 1 -8 11 3492.78 191.529 33 -1 8 -11 3345.07 191.327 6 -1 8 -11 2794.84 298.257 1 1 -8 11 3405.80 168.450 5 1 -8 12 163.070 67.8288 38 1 -8 12 70.4224 41.6232 33 -1 8 -12 60.7257 36.3354 6 1 -8 12 90.8473 52.1517 17 1 -8 13 2582.62 169.825 33 1 -8 13 2483.56 174.138 17 1 -8 13 2205.93 193.554 38 -1 8 -13 2225.31 159.950 6 -1 8 -14 2620.64 166.973 6 1 -8 14 3254.94 191.634 33 1 -8 14 3217.79 198.951 17 1 -8 14 2870.11 219.064 38 1 -8 15 110.082 50.4367 17 1 -8 15 107.160 75.4430 38 1 -8 16 154.009 59.7859 30 -1 8 -16 126.982 59.0089 10 1 -8 16 109.426 53.1787 38 -1 8 -17 1.13411 33.0063 10 1 -8 17 54.7147 30.3606 30 -1 8 -18 36.4098 26.6267 10 1 -8 18-14.7094 22.4957 34 1 -8 18 44.7290 19.1894 30 -1 7 12 17.0754 20.9028 37 1 -7 -12 30.6965 11.1660 14 1 -7 -11 476.473 54.5086 14 1 -7 -10 771.657 81.3585 14 1 -7 -10 849.096 90.1546 23 1 -7 -9 4787.12 224.701 23 1 -7 -9 4691.95 214.044 14 -1 7 9 4528.08 219.135 34 1 -7 -8 3609.01 198.401 14 -1 7 8 3664.02 206.317 34 1 -7 -8 3540.34 202.498 23 -1 7 8 3453.11 218.029 43 1 -7 -7 153.373 50.0791 14 -1 7 7 34.3962 46.0580 43 1 -7 -7 107.922 46.8965 23 -1 7 7 185.171 57.1764 34 1 -7 -6 943.875 99.7197 4 -1 7 6 961.710 107.784 34 -1 7 6 1034.26 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9 4749.79 187.353 5 -1 7 -10 353.098 113.570 1 -1 7 -10 144.605 44.9590 6 1 -7 10 180.106 45.0971 9 1 -7 10 184.247 44.1643 33 1 -7 10 201.746 52.4528 17 1 -7 10 223.934 47.5976 5 -1 7 -11 2467.09 167.303 6 -1 7 -11 2389.74 273.641 1 1 -7 11 2582.49 146.661 5 1 -7 11 2656.72 170.459 17 1 -7 11 2560.95 160.256 33 1 -7 12 2830.43 155.223 5 1 -7 12 3068.63 225.755 38 1 -7 12 2954.04 187.618 17 -1 7 -12 2726.35 286.876 1 -1 7 -12 2879.53 184.706 6 1 -7 12 3034.16 181.139 33 -1 7 -13 537.063 83.6404 6 1 -7 13 606.276 94.4784 17 1 -7 13 546.316 111.157 38 1 -7 13 627.725 90.2076 33 1 -7 14 1623.44 140.381 17 1 -7 14 2098.52 154.866 33 -1 7 -14 1496.74 136.900 6 1 -7 14 1918.65 183.609 38 1 -7 15 548.020 88.4167 17 1 -7 15 580.415 111.062 38 1 -7 16 1698.11 140.467 30 -1 7 -16 2120.21 183.397 10 1 -7 16 2024.79 170.881 38 -1 7 -17 32.3228 39.2189 10 1 -7 17-5.50356 22.3438 30 1 -7 18 30.2203 27.0523 34 -1 7 -18 21.4622 25.7493 10 1 -7 19 206.397 30.0643 34 -1 6 13 212.791 37.8840 37 1 -6 -12 48.4679 25.8301 14 -1 6 12 39.9006 29.8181 34 1 -6 -12 27.1490 21.0738 23 -1 6 11 470.114 72.0033 34 1 -6 -11 476.900 68.6436 23 -1 6 11 380.846 81.9464 43 1 -6 -11 450.668 63.7975 14 -1 6 10 4.81527 56.1120 43 -1 6 10 15.8746 39.1361 34 1 -6 -10-24.0190 41.0156 23 1 -6 -10-10.3073 35.0294 14 -1 6 9 2855.34 183.195 34 1 -6 -9 3075.42 182.274 14 -1 6 9 2765.41 197.902 43 1 -6 -9 2926.47 183.605 23 1 -6 -8 227.649 60.8669 23 -1 6 8 173.681 64.4444 43 1 -6 -8 256.060 58.3910 14 -1 6 8 203.322 59.0894 34 1 -6 -7 3893.56 211.661 23 -1 6 7 4301.23 222.831 34 -1 6 7 3930.84 228.886 43 -1 6 7 4179.60 303.437 2 1 -6 -6 3673.10 193.008 7 -1 6 6 3609.73 279.681 2 -1 6 6 3457.18 193.358 34 1 -6 -6 3509.54 194.125 23 1 -6 -6 3881.31 193.878 4 -1 6 6 3854.27 218.645 43 -1 6 5 1536.46 180.736 2 1 -6 -5 1795.14 130.938 7 -1 6 5 1600.71 125.461 34 1 -6 -5 1604.18 125.737 23 -1 6 5 1678.20 136.678 43 -1 6 4 2497.38 222.778 2 -1 6 3 2182.40 201.402 2 -1 6 2 1398.36 156.961 2 -1 6 1 92.9722 47.6473 1 -1 6 1 91.8512 52.9403 2 -1 6 0 7409.70 308.931 1 -1 6 -1 3803.39 229.332 1 -1 6 -2-30.8777 39.4613 1 1 -6 3 1346.90 80.5038 5 -1 6 -3 1555.22 162.365 1 -1 6 -4 3754.67 258.214 1 1 -6 4 3622.81 131.921 5 1 -6 5 145.901 30.3336 5 -1 6 -5 77.0542 65.4146 1 -1 6 -6 1505.10 99.5274 6 1 -6 6 1647.71 95.1772 5 1 -6 7 355.946 46.1735 5 -1 6 -7 467.838 62.6692 6 -1 6 -8 491.976 65.9205 6 1 -6 8 567.249 60.9685 5 1 -6 9 1835.36 113.034 5 -1 6 -9 1848.01 127.026 6 1 -6 10 6891.39 227.919 5 -1 6 -10 6406.15 408.894 1 -1 6 -10 6838.97 255.793 6 1 -6 11 4292.23 188.748 5 1 -6 11 4170.10 195.701 33 -1 6 -11 4217.36 214.149 6 -1 6 -11 3981.94 328.876 1 1 -6 11 4315.87 209.183 17 -1 6 -12 128.766 50.0109 6 1 -6 12 217.279 79.9814 38 1 -6 12 141.827 46.0162 33 1 -6 12 99.2701 39.6229 17 1 -6 12 125.016 33.4396 5 -1 6 -13 126.007 53.7291 6 1 -6 13 57.5353 47.5319 17 1 -6 13 155.431 77.7839 38 1 -6 13 109.848 50.3743 33 1 -6 14 143.532 48.7951 17 1 -6 14 112.661 69.9177 38 -1 6 -14 198.280 61.4863 6 1 -6 15 3439.70 233.051 38 -1 6 -15 3431.25 198.908 6 1 -6 16 98.7482 39.5819 30 1 -6 16 42.0620 53.0645 38 -1 6 -16 85.1306 59.6589 10 1 -6 17-11.3867 35.1409 34 -1 6 -17-72.8978 42.3364 10 1 -6 18 67.3375 33.1365 34 -1 6 -18 61.4674 31.3491 10 -1 6 -18 24.7513 21.1014 32 1 -6 19 61.3600 18.3792 34 -1 5 13 25.2532 27.9884 34 -1 5 13-30.5342 43.5967 43 1 -5 -13 20.2656 20.3535 23 1 -5 -13 12.6398 16.5486 14 -1 5 13 43.6770 33.1604 37 1 -5 -12 2516.97 140.768 14 -1 5 12 2536.58 157.495 34 1 -5 -12 2701.24 154.303 23 -1 5 12 2642.79 179.740 43 1 -5 -11 2562.00 165.615 23 1 -5 -11 2581.12 157.607 14 -1 5 11 2511.68 187.209 43 -1 5 11 2304.44 161.975 34 -1 5 10-16.7389 40.7078 34 1 -5 -10 72.2001 45.2033 23 -1 5 10-0.24043 51.7537 43 1 -5 -10-2.44107 34.6927 7 -1 5 9 31.6246 39.0366 34 -1 5 9 7.56673 47.0835 43 1 -5 -9 41.9408 33.6793 7 1 -5 -9 69.2661 42.2070 23 1 -5 -8 54.0839 36.5037 7 -1 5 8 73.9231 52.8364 43 -1 5 8 75.1537 38.6327 34 1 -5 -8 56.7611 44.3042 23 1 -5 -7 199.341 50.3553 23 -1 5 7 345.012 88.3575 2 1 -5 -7 257.508 50.5356 7 -1 5 7 340.936 73.5269 43 -1 5 7 378.896 66.0008 34 1 -5 -6 22730.3 432.702 4 -1 5 6 21240.5 647.445 2 -1 5 5 9624.78 422.608 2 -1 5 4 1207.00 140.817 2 -1 5 3 12526.9 435.343 2 -1 5 2 16316.9 392.221 1 -1 5 2 16316.7 476.141 2 -1 5 1 7260.67 309.100 2 -1 5 1 7128.82 268.516 1 -1 5 0 6118.21 258.713 1 -1 5 -1 19058.7 466.232 1 1 -5 2 273.951 33.2782 5 -1 5 -2 224.229 64.1929 1 1 -5 3 14442.8 228.716 5 -1 5 -3 14568.2 442.476 1 1 -5 4 2776.47 103.237 5 -1 5 -4 2646.35 113.366 6 1 -5 5 136081. 743.691 5 -1 5 -5 135105. 829.881 6 -1 5 -6 56.5040 25.1326 6 1 -5 6 35.2179 16.5146 5 -1 5 -7 12308.1 278.078 6 1 -5 7 11739.0 243.947 5 1 -5 8 363.119 48.3264 5 -1 5 -8 373.197 54.6115 6 1 -5 8 237.104 75.2500 2 1 -5 9 12.0754 19.7357 5 1 -5 9 22.5187 51.7285 2 -1 5 -9 18.3576 30.6786 6 1 -5 10 5889.71 360.134 2 1 -5 10 6605.30 222.819 5 -1 5 -11 4538.71 323.595 1 1 -5 11 4568.17 330.974 2 1 -5 11 5306.33 210.979 5 1 -5 11 5177.77 218.568 17 1 -5 11 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806.265 1 1 -4 3 607.602 40.8506 5 -1 4 -3 730.334 53.0341 6 1 -4 4 5414.77 126.491 5 -1 4 -4 5335.86 146.755 6 -1 4 -5 7209.76 179.465 6 1 -4 5 7098.12 154.563 5 -1 4 -6 2021.51 102.991 6 1 -4 6 2003.71 160.604 2 1 -4 6 1994.47 89.6053 5 1 -4 7 26169.8 348.415 5 1 -4 7 25628.6 594.823 2 1 -4 8 44640.6 829.814 2 1 -4 8 43678.7 490.229 5 1 -4 9 786.569 121.702 2 1 -4 9 935.328 80.1586 5 1 -4 10 1286.51 164.284 2 1 -4 10 1248.51 98.8232 5 1 -4 11 112.543 56.3290 2 1 -4 11 116.510 37.5560 5 -1 4 -12 3878.53 170.762 36 1 -4 12 4328.49 201.380 5 1 -4 12 4441.90 249.087 38 1 -4 12 3887.26 194.233 17 1 -4 12 3620.13 294.199 2 1 -4 13 3780.84 238.867 38 -1 4 -13 3797.26 170.907 13 1 -4 13 3452.97 289.176 2 1 -4 13 4163.51 202.023 5 1 -4 13 4006.78 202.554 17 1 -4 14 3.44381 27.5328 5 1 -4 14 51.5700 60.3307 38 -1 4 -14 54.8279 32.6227 13 1 -4 15 3256.08 197.477 34 1 -4 15 2809.91 199.881 38 -1 4 -15 2900.79 211.205 10 -1 4 -15 3212.02 197.521 6 1 -4 16 6485.56 263.354 34 -1 4 -16 5995.18 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92.6184 2 -1 3 5 11767.9 396.254 2 -1 3 4 4585.55 230.505 2 -1 3 4 4702.00 171.248 1 -1 3 3 3282.59 145.521 1 -1 3 3 2976.64 172.621 2 -1 3 2 66782.5 755.042 2 -1 3 2 65843.2 659.798 1 1 -3 -2 64295.6 561.829 3 -1 3 1 6937.70 213.693 1 1 -3 -1 6783.34 141.724 3 -1 3 0 37799.0 508.204 1 1 -3 0 37013.6 232.869 3 -1 3 -1 17440.9 357.538 1 -1 3 -2 84.3906 18.5498 6 -1 3 -2 106.044 48.3415 1 -1 3 -3 14630.3 208.356 6 -1 3 -4 25040.1 289.172 6 1 -3 4 24885.2 242.986 5 1 -3 4 24823.2 448.755 2 1 -3 5 2241.05 144.520 2 1 -3 5 2612.42 87.1403 5 1 -3 6 301.900 63.0071 2 1 -3 6 264.521 31.8107 5 1 -3 7 34821.4 660.435 2 1 -3 8 13672.4 446.148 2 1 -3 9 2303.86 195.728 2 1 -3 10 1709.08 180.740 2 1 -3 11 3033.19 255.179 2 1 -3 12 261.728 64.4750 38 1 -3 12 379.402 92.2908 2 -1 3 -12 268.026 47.2203 13 1 -3 12 253.445 51.7898 17 1 -3 13-18.7521 42.9580 38 -1 3 -13-12.9909 30.4367 13 1 -3 13-21.1531 30.9506 5 1 -3 14 1028.56 115.337 34 1 -3 14 797.827 109.515 38 1 -3 14 863.318 93.8910 5 -1 3 -14 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17 2 -9 8 284.880 61.2685 9 2 -9 8 229.024 55.2092 33 2 -9 9 6635.17 257.507 9 2 -9 9 6972.41 269.894 33 2 -9 9 7075.11 281.673 17 -2 9 -10 432.315 75.3235 10 2 -9 10 505.362 78.2579 33 2 -9 10 393.455 67.8605 9 2 -9 10 526.440 85.0954 17 2 -9 11 2316.36 159.503 33 2 -9 11 2240.88 165.781 17 2 -9 11 1996.60 142.604 9 -2 9 -11 2212.39 172.764 10 2 -9 12 149.520 55.4729 17 2 -9 12 77.9329 42.3200 33 -2 9 -12 174.104 49.0224 10 2 -9 12 141.121 70.1778 38 -2 9 -13 538.366 91.1924 10 2 -9 13 590.058 92.7257 17 2 -9 13 647.207 88.7107 33 2 -9 13 677.717 113.338 38 2 -9 14 228.836 59.1947 33 2 -9 14 281.725 80.7918 38 -2 9 -14 205.638 60.5982 10 2 -9 14 178.428 59.4293 17 2 -9 15 183.182 64.7852 38 2 -9 15 251.925 58.6587 17 -2 9 -15 222.157 62.7902 10 2 -9 16 11.3607 33.4027 30 2 -9 16-15.2987 32.9970 17 2 -9 16-33.3136 49.6117 38 -2 9 -16-49.9494 35.8323 10 -2 9 -17 100.963 33.2159 10 2 -9 17 79.0121 33.7011 30 -2 9 -18-7.78530 13.3047 10 2 -8 -11 5.33623 10.3719 14 -2 8 11-29.3756 21.8895 37 -2 8 10 19.8824 30.1868 37 2 -8 -10 17.5246 21.7175 14 -2 8 9 218.900 65.3449 37 2 -8 -9 198.537 46.7789 14 2 -8 -8 90.1506 43.7759 14 2 -8 -7 297.407 69.8883 14 2 -8 -6 462.987 79.8600 14 2 -8 -5-13.4064 44.2241 14 2 -8 -5-58.3783 30.6556 4 2 -8 -4 4712.02 231.681 14 2 -8 -3 18850.5 452.397 14 -2 8 3 19189.8 684.542 2 -2 8 2 7364.29 425.022 2 2 -8 -2 7478.43 275.470 14 -2 8 1 3851.25 307.902 2 2 -8 -1 3924.31 192.988 14 -2 8 0 5058.40 351.077 2 2 -8 0 5556.32 219.615 14 -2 8 -1 2137.09 228.228 2 -2 8 -1 2011.71 207.929 1 -2 8 -2 236.117 85.6097 1 -2 8 -3 45.9751 54.8213 1 -2 8 -4 276.803 89.4362 1 -2 8 -5 18.9049 51.6045 1 -2 8 -6 123.850 78.1243 1 -2 8 -7 7569.00 469.693 1 2 -8 7 7717.80 266.279 17 2 -8 7 7493.02 247.423 9 -2 8 -8 4628.75 183.407 28 2 -8 8 5298.34 218.893 33 -2 8 -8 5313.52 400.768 1 2 -8 8 5329.52 230.018 17 2 -8 8 5282.96 212.788 9 2 -8 9 1141.79 107.434 33 2 -8 9 1077.17 101.096 9 -2 8 -9 849.694 86.0256 28 -2 8 -9 1092.25 187.329 1 2 -8 9 1020.63 105.031 17 2 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14 2 -7 -8-2.47433 35.1077 23 2 -7 -7 32.7730 36.5829 23 2 -7 -7 107.333 52.4032 14 -2 7 7 64.3308 46.2661 34 2 -7 -6 113.610 52.8435 14 2 -7 -6 85.3056 39.1421 23 -2 7 6 117.545 47.9581 34 -2 7 5 122.245 62.9587 2 2 -7 -5 36.8855 38.3463 14 -2 7 5 45.0364 39.0761 34 2 -7 -5 16.0839 31.0090 23 -2 7 4 22852.2 738.794 2 -2 7 4 22640.5 504.672 34 2 -7 -4 21434.0 470.051 23 2 -7 -4 22685.2 480.558 14 -2 7 3 537.866 118.240 2 -2 7 3 551.233 77.7490 34 2 -7 -3 669.548 82.5808 14 -2 7 2 4357.61 312.735 2 -2 7 1 13.5292 39.4880 2 -2 7 0 6878.11 375.731 2 -2 7 0 6893.58 358.803 1 -2 7 -1 8911.76 417.812 1 -2 7 -2 845.607 138.138 1 -2 7 -3 2253.45 220.003 1 -2 7 -4 13251.9 544.299 1 -2 7 -5 132.146 63.5553 1 -2 7 -6 161.174 83.9932 1 -2 7 -7 3381.22 297.497 1 -2 7 -8 13289.9 602.462 1 -2 7 -8 13391.2 357.904 6 -2 7 -9 2605.97 146.492 28 2 -7 9 2864.79 158.072 33 -2 7 -9 3031.70 292.046 1 2 -7 9 3006.07 169.939 17 2 -7 9 3045.86 154.445 9 -2 7 -9 2871.84 175.914 6 2 -7 10 42.1071 39.2489 17 2 -7 10 12.4777 27.2308 33 -2 7 -10 106.804 60.0113 1 -2 7 -10 82.2433 45.8161 6 -2 7 -10-21.9427 37.2807 28 2 -7 10 9.40398 19.6513 9 -2 7 -11 1996.33 236.812 1 2 -7 11 1900.10 140.571 33 2 -7 11 1813.15 143.642 17 -2 7 -11 1863.29 150.809 6 2 -7 12 410.019 70.1389 33 -2 7 -12 386.604 74.5756 6 2 -7 12 310.095 64.9616 17 -2 7 -12 385.370 57.9801 36 2 -7 13 1299.31 127.842 17 2 -7 13 1471.13 128.939 33 2 -7 13 1443.85 159.650 38 -2 7 -13 1300.30 129.386 6 -2 7 -13 1525.91 107.486 36 2 -7 14 4308.23 219.265 17 -2 7 -14 4268.97 173.591 36 2 -7 14 4473.86 218.079 33 -2 7 -14 4247.85 226.192 6 -2 7 -14 4871.82 286.380 10 2 -7 14 4531.22 270.993 38 2 -7 15 924.835 131.206 38 2 -7 15 838.523 97.6824 17 -2 7 -15 864.647 78.3916 13 -2 7 -15 930.736 133.318 10 2 -7 16 6.15318 36.5018 30 2 -7 16 5.03962 49.4121 38 -2 7 -16 18.8084 42.5103 10 -2 7 -17 60.3992 37.0837 10 2 -7 17 48.5208 26.9878 30 2 -7 17-22.4192 30.2944 34 2 -7 17 4.12311 44.3983 38 -2 7 -18 80.6810 30.0564 10 2 -7 18 58.5433 23.3010 34 2 -6 -13 71.7566 19.6371 14 -2 6 13 96.1882 27.8078 37 -2 6 12 508.380 72.2394 37 2 -6 -12 510.871 60.8281 14 -2 6 12 559.996 69.3153 34 2 -6 -11 226.988 52.0745 14 -2 6 11 171.736 53.7571 34 2 -6 -11 223.624 44.6667 23 2 -6 -10 3439.10 191.391 14 2 -6 -10 3205.07 174.580 23 -2 6 10 3308.60 195.835 34 -2 6 9 14177.9 414.281 34 -2 6 9 14487.3 449.807 43 2 -6 -9 14084.2 385.198 23 2 -6 -8 474.860 79.7768 7 2 -6 -8 512.581 76.6622 23 -2 6 8 489.193 95.1536 43 -2 6 8 513.951 86.1311 34 2 -6 -7 9172.43 318.107 7 -2 6 7 9222.19 330.850 34 2 -6 -7 8316.28 299.553 23 -2 6 7 9435.34 354.945 43 -2 6 6 1328.46 179.494 2 -2 6 6 1564.95 136.414 34 -2 6 6 1744.72 150.645 43 2 -6 -6 1510.33 124.635 23 2 -6 -6 1626.95 133.961 7 2 -6 -5 2391.73 151.738 7 -2 6 5 2087.53 221.010 2 -2 6 5 2237.44 162.395 43 2 -6 -5 1850.95 131.334 23 -2 6 5 2113.67 149.149 34 -2 6 4-208.774 70.5486 2 -2 6 3 8020.28 399.627 2 -2 6 2 452.506 82.4626 1 -2 6 2 379.059 92.1314 2 -2 6 1 22118.0 627.512 2 -2 6 1 21448.3 584.362 1 -2 6 0 6466.03 334.555 2 -2 6 0 6327.36 320.207 1 -2 6 -1 67.6927 45.4475 1 -2 6 -2 34890.4 778.186 1 -2 6 -3 23785.7 655.663 1 -2 6 -4 2410.55 219.346 1 2 -6 4 2168.54 94.2289 5 -2 6 -5 29092.0 769.100 1 2 -6 5 27265.7 336.566 5 -2 6 -6 38587.6 906.319 1 -2 6 -6 37877.9 532.681 6 -2 6 -7 22729.0 439.107 6 -2 6 -7 23585.5 728.491 1 -2 6 -8 5979.22 235.247 6 -2 6 -8 5318.51 356.933 1 -2 6 -9 3129.43 179.488 6 -2 6 -9 2940.52 276.756 1 -2 6 -10 2826.45 159.100 28 -2 6 -10 2617.57 266.092 1 -2 6 -10 2986.27 184.309 6 2 -6 10 3095.01 171.293 17 2 -6 10 2926.40 159.404 33 -2 6 -11 444.354 70.9608 28 2 -6 11 561.630 75.4739 33 2 -6 11 578.269 81.9225 17 -2 6 -11 517.104 118.431 1 -2 6 -11 535.302 86.5339 6 -2 6 -11 550.213 65.6216 36 2 -6 12 627.103 83.5040 33 2 -6 12 508.985 79.4245 17 -2 6 -12 524.025 88.1125 6 -2 6 -12 541.920 67.5711 36 2 -6 13 342.242 68.7558 33 2 -6 13 417.381 72.9519 17 -2 6 -13 427.037 62.0118 36 -2 6 -13 381.538 78.6704 6 -2 6 -14 161.909 72.6905 10 -2 6 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30.4120 23 -2 5 9 12723.1 392.397 34 2 -5 -9 12797.0 374.338 7 2 -5 -9 11785.9 351.107 23 -2 5 9 12716.6 416.933 43 -2 5 8 798.322 142.146 2 -2 5 8 774.419 98.9985 34 -2 5 8 913.879 118.603 43 2 -5 -8 768.256 89.8625 23 2 -5 -8 784.458 96.2406 7 2 -5 -7 8825.29 296.749 7 2 -5 -7 8215.06 277.489 23 -2 5 7 8579.17 444.107 2 -2 5 7 8760.19 308.245 34 -2 5 7 8978.74 333.548 43 -2 5 6 214.548 49.1673 34 -2 5 6 141.144 45.9497 43 2 -5 -6 226.251 48.7074 7 -2 5 6 146.489 63.4317 2 -2 5 5 1510.58 177.171 2 -2 5 4 1551.12 169.828 2 -2 5 3 15175.3 501.576 2 -2 5 3 14951.6 431.764 1 -2 5 2 5953.18 281.642 1 -2 5 2 6556.42 320.219 2 -2 5 1 52481.9 849.947 1 -2 5 1 55670.8 911.857 2 -2 5 0 680.388 101.766 1 -2 5 -1 3093.37 210.530 1 -2 5 -2 3814.32 238.805 1 -2 5 -3 18491.9 535.413 1 -2 5 -4 555.091 103.313 1 2 -5 4 606.245 44.8152 5 -2 5 -5 22582.9 379.555 6 2 -5 5 22268.5 273.058 5 -2 5 -6 12951.9 301.485 6 2 -5 6 12895.3 219.516 5 2 -5 7 219.753 30.6713 5 -2 5 -7 230.604 50.0268 6 -2 5 -7 275.987 83.9815 1 -2 5 -8 38.2435 32.5549 6 -2 5 -8 171.176 80.8935 1 -2 5 -9 840.056 93.2604 6 -2 5 -9 596.131 131.034 1 -2 5 -10 2927.62 179.108 6 -2 5 -10 2395.13 233.487 1 2 -5 11 5021.15 212.126 33 -2 5 -11 4528.76 208.862 28 -2 5 -11 4608.93 188.370 36 -2 5 -11 4865.27 238.165 6 2 -5 11 4863.66 214.348 17 -2 5 -12 2169.87 137.869 36 2 -5 12 2140.36 147.632 33 2 -5 12 2075.48 146.403 17 -2 5 -13 95.3099 52.7764 6 2 -5 13 102.374 66.8246 38 2 -5 13 101.748 42.6424 17 -2 5 -13 43.5098 28.0174 36 -2 5 -14 45.9078 41.8454 6 -2 5 -14 74.9712 44.5102 10 2 -5 14 52.3770 56.5724 38 -2 5 -14 19.3717 27.6764 13 2 -5 14-10.7459 29.7705 17 -2 5 -15 708.157 77.5957 13 2 -5 15 733.374 107.754 38 -2 5 -15 657.544 106.858 10 -2 5 -16 836.822 73.1041 13 2 -5 16 828.680 99.3894 38 2 -5 16 775.727 89.2240 34 -2 5 -16 943.434 116.576 10 -2 5 -17 192.243 47.5009 10 2 -5 17 198.432 46.7181 34 2 -5 18 38.8521 21.3069 34 -2 5 -18 72.8353 28.3169 31 -2 5 -18 75.0004 27.4231 32 -2 4 15 403.847 46.6020 34 -2 4 14 2748.84 143.985 34 2 -4 -14 2617.58 125.221 14 -2 4 13 1204.86 117.095 43 -2 4 13 1199.79 114.109 37 -2 4 13 1288.46 116.842 34 2 -4 -13 1214.58 101.857 7 2 -4 -13 1172.01 90.2423 23 2 -4 -12 19647.1 411.581 23 -2 4 12 20161.9 476.488 34 -2 4 12 19321.5 486.893 43 2 -4 -12 19280.4 438.058 7 2 -4 -11 236.963 60.9486 7 -2 4 11 391.696 76.7270 34 2 -4 -11 325.735 62.0950 23 -2 4 11 313.418 79.9011 43 2 -4 -10 14718.7 382.881 23 -2 4 10 15530.8 435.137 34 -2 4 10 14692.0 446.460 43 2 -4 -10 14809.7 403.461 7 -2 4 9 1027.63 158.652 2 -2 4 9 1105.62 117.062 34 2 -4 -9 970.073 97.5817 23 2 -4 -9 1065.09 107.525 7 -2 4 9 1196.41 129.658 43 -2 4 8 5248.73 347.737 2 -2 4 8 5525.40 242.437 34 -2 4 8 5272.99 253.864 43 2 -4 -8 5532.46 230.453 7 2 -4 -8 4935.17 208.079 23 -2 4 7 5538.30 341.880 2 -2 4 6 160.914 69.2222 2 -2 4 5 2955.05 227.597 2 -2 4 4 28144.9 651.574 2 -2 4 4 28249.8 558.209 1 -2 4 3 1312.80 139.228 2 -2 4 3 1279.77 122.130 1 -2 4 2 78.2410 40.1767 1 -2 4 2 86.2539 40.1438 2 -2 4 1 721.561 99.6434 2 -2 4 1 680.761 91.9995 1 -2 4 0 38927.7 671.862 1 -2 4 -1 6572.63 280.391 1 -2 4 -2 28149.1 587.562 1 -2 4 -3 23370.3 547.304 1 2 -4 3 21209.6 212.299 5 -2 4 -4 24920.7 584.352 1 -2 4 -4 24822.8 351.215 6 2 -4 5 8545.64 152.419 5 -2 4 -5 9256.52 369.118 1 -2 4 -5 9228.56 224.872 6 -2 4 -6 261.306 81.5373 1 2 -4 6 396.114 36.4124 5 -2 4 -6 254.735 44.8695 6 2 -4 7 25147.7 313.337 5 -2 4 -7 25775.5 421.609 6 2 -4 8 208.452 33.1953 5 -2 4 -8 225.817 55.3154 6 2 -4 8 304.343 73.6782 2 -2 4 -8 260.941 83.1754 1 2 -4 9 7214.52 359.354 2 -2 4 -9 7282.38 370.456 1 -2 4 -10 702.555 116.773 1 2 -4 10 618.388 116.017 2 2 -4 11 598.634 73.3999 17 2 -4 11 534.800 69.7544 33 2 -4 11 656.675 115.486 2 -2 4 -11 515.457 65.8738 36 -2 4 -12 1986.50 134.629 36 2 -4 12 2022.18 138.093 17 -2 4 -13-42.6975 45.7382 13 -2 4 -13-26.4865 29.5283 36 -2 4 -13 75.3445 46.3849 10 2 -4 13 14.6082 50.8661 38 2 -4 13 132.398 36.4976 17 2 -4 14 384.350 83.8480 38 -2 4 -14 411.017 64.2139 13 -2 4 -14 592.785 91.7429 6 -2 4 -14 500.917 97.9779 10 2 -4 15 729.019 104.549 38 -2 4 -15 726.955 78.5930 13 2 -4 15 742.570 92.3465 34 -2 4 -15 856.729 115.876 10 2 -4 16-47.2517 36.1641 38 2 -4 16 11.6485 29.8741 34 -2 4 -16-5.54725 21.0980 13 -2 4 -16 39.9596 31.2168 10 2 -4 17 218.676 44.1789 34 -2 4 -17 231.415 48.3742 32 -2 4 -17 156.749 39.3169 10 -2 4 -18-4.70385 19.7365 32 -2 4 -18 8.98825 21.7324 31 2 -4 18-26.9987 16.6044 34 -2 3 16 68.2194 24.0872 34 -2 3 15 32.4554 30.3472 34 2 -3 -15 46.8417 22.4627 14 -2 3 14 22.9218 39.7889 34 2 -3 -14 4.37681 23.9318 7 -2 3 14-23.7387 36.6971 43 2 -3 -13 2948.81 155.575 23 2 -3 -13 2899.50 166.980 7 -2 3 13 2618.80 170.107 37 -2 3 13 2880.07 185.775 43 -2 3 13 3181.37 192.546 34 2 -3 -12 33.3623 31.3412 23 -2 3 12 30.5944 54.4068 43 -2 3 12 21.6215 41.7482 34 2 -3 -12 21.2230 38.9266 7 -2 3 11 4241.70 230.098 34 2 -3 -11 4150.99 212.215 7 -2 3 11 4288.41 241.701 43 -2 3 10 4677.62 234.316 34 -2 3 10 4508.35 239.613 43 -2 3 10 4780.00 342.400 2 2 -3 -10 4627.33 218.315 7 -2 3 9 2370.39 157.746 34 2 -3 -9 2290.22 148.334 7 -2 3 9 2404.30 170.501 43 -2 3 9 2219.17 231.922 2 -2 3 8 646.036 122.490 2 -2 3 7 3305.39 250.306 2 -2 3 6 8714.29 378.317 2 -2 3 5 2128.20 149.749 1 -2 3 5 2117.74 178.536 2 -2 3 4 1358.97 121.066 1 -2 3 4 978.466 114.837 2 -2 3 3 13044.6 367.064 1 -2 3 3 14050.7 397.344 2 -2 3 2 55240.5 745.062 2 -2 3 2 53675.8 733.586 1 -2 3 1 29949.6 544.980 1 -2 3 1 30055.1 518.700 2 -2 3 0 87781.2 914.607 1 -2 3 -1 835.711 93.7057 1 -2 3 -2 4745.80 89.7842 3 -2 3 -2 5064.32 226.503 1 -2 3 -3 3612.85 120.053 3 -2 3 -3 3328.10 116.489 6 -2 3 -3 3563.19 196.133 1 -2 3 -4 78.5941 24.4652 6 -2 3 -4 72.1701 44.8668 1 2 -3 5 4.70649 8.30073 5 -2 3 -5-8.83708 21.4665 6 2 -3 6 19089.7 461.237 2 -2 3 -6 18910.8 500.483 1 2 -3 6 19824.4 246.703 5 2 -3 7 64548.9 495.553 5 -2 3 -7 62782.5 933.850 1 2 -3 8 4.68683 34.9038 2 -2 3 -8 35.1985 35.4123 1 2 -3 9 19146.7 556.711 2 -2 3 -9 21132.3 556.157 1 2 -3 10 294.730 76.0287 2 2 -3 11-25.8590 28.4154 2 -2 3 -11 102.234 40.1302 36 2 -3 12 463.678 87.9218 38 -2 3 -12 410.464 106.799 3 -2 3 -12 293.980 57.6455 36 -2 3 -12 307.934 58.1754 13 -2 3 -12 459.507 88.8672 10 2 -3 13 1136.44 127.410 38 -2 3 -13 1300.50 114.556 13 -2 3 -13 1275.32 142.140 10 2 -3 14 378.060 78.3099 38 -2 3 -14 291.934 71.5201 10 -2 3 -14 419.192 78.9647 6 2 -3 14 263.069 60.0633 34 -2 3 -14 311.131 61.3801 13 -2 3 -15 58.3390 34.2862 13 2 -3 15 29.8258 33.8350 34 2 -3 15-8.17514 33.9498 38 -2 3 -15 19.6203 35.6079 10 -2 3 -16 16.3736 37.3303 32 -2 3 -16 29.0241 24.3686 13 -2 3 -16 16.7539 21.9506 10 -2 3 -17 420.390 43.5991 13 -2 3 -17 525.480 63.8693 32 2 -3 17 540.346 61.2932 34 -2 3 -18 10.8572 17.1429 32 -2 3 -18 16.5375 20.2803 31 -2 2 16 811.784 74.0587 34 2 -2 -16 774.234 57.2154 14 2 -2 -15 430.004 57.0426 7 -2 2 15 393.182 67.5050 34 -2 2 15 398.601 60.6021 43 2 -2 -14 818.195 88.0224 7 -2 2 14 863.511 106.107 34 -2 2 14 757.437 94.4863 43 2 -2 -13 4350.77 209.746 7 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68.2453 34 -3 5 11 613.129 103.121 37 3 -5 -11 610.305 87.2279 7 -3 5 11 704.440 95.0172 34 -3 5 10 1000.13 134.834 37 -3 5 10 810.576 102.672 34 3 -5 -10 952.046 110.281 7 3 -5 -9 843.065 103.202 7 -3 5 9 798.628 104.541 34 -3 5 9 794.578 113.355 43 3 -5 -8 6585.06 270.701 7 -3 5 8 6512.73 295.827 43 -3 5 8 6327.95 273.588 34 -3 5 7 214.496 53.9342 34 3 -5 -7 201.095 52.8403 7 -3 5 7 233.052 67.4646 43 -3 5 7 254.627 89.2972 2 -3 5 6 4665.99 218.052 34 3 -5 -6 4733.01 210.291 7 -3 5 6 4728.22 330.112 2 -3 5 6 4909.57 239.905 43 -3 5 5 886.674 148.420 2 -3 5 4-19.0322 49.3367 2 -3 5 4 78.8669 39.1773 1 -3 5 3 4646.72 280.297 1 -3 5 3 5115.80 306.403 2 -3 5 2 10030.9 415.165 2 -3 5 2 9270.67 401.768 1 -3 5 1 33280.6 766.861 1 -3 5 1 34907.9 747.559 2 -3 5 0 21466.3 573.811 2 -3 5 0 20515.0 606.556 1 -3 5 -1 91275.4 1274.93 1 -3 5 -2 5986.04 333.797 1 -3 5 -3 1880.13 192.838 1 -3 5 -4 681.719 125.077 1 -3 5 -5 7243.81 381.750 1 -3 5 -6 529.884 75.2805 6 -3 5 -6 507.901 111.299 1 -3 5 -7 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4 3513.95 190.433 9 -4 9 -4 3599.15 183.217 35 -4 9 -5 336.567 63.3427 35 4 -9 5 340.741 66.4239 9 -4 9 -6 3001.07 171.282 35 4 -9 6 2845.87 167.621 9 4 -9 7 567.140 93.1766 17 4 -9 7 510.701 76.7587 33 -4 9 -7 437.106 62.2932 28 4 -9 7 578.155 78.1369 9 4 -9 8 193.436 51.8646 33 -4 9 -8 174.716 41.8028 28 4 -9 8 189.177 64.7539 17 4 -9 8 230.515 51.7323 9 -4 9 -9 819.876 90.0912 28 4 -9 9 742.905 88.2451 33 4 -9 9 835.907 90.9136 9 4 -9 9 825.333 105.208 17 4 -9 10 3725.87 210.495 17 4 -9 10 3432.46 183.894 33 -4 9 -10 3482.66 183.804 28 4 -9 10 3273.13 165.083 9 -4 9 -10 3422.68 204.236 10 4 -9 11 236.982 62.8632 17 4 -9 11 202.499 51.7499 33 -4 9 -11 263.322 61.3033 10 4 -9 12 814.565 96.3984 17 -4 9 -12 984.276 88.8650 36 4 -9 12 894.093 91.8678 33 -4 9 -12 1044.30 115.458 10 4 -9 13 1228.11 99.3501 33 -4 9 -13 1410.56 98.6463 36 4 -9 13 1297.17 112.615 17 -4 9 -13 1339.53 124.079 10 -4 9 -14 698.212 61.0865 36 4 -9 14 747.279 98.4311 38 4 -9 14 601.372 71.0615 17 -4 9 -15 994.090 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3027.24 166.491 35 -4 8 -4 3010.26 165.109 35 -4 8 -4 3211.82 178.934 18 -4 8 -4 2988.88 312.152 1 4 -8 4 2997.53 166.411 9 -4 8 -5 2705.53 160.285 35 -4 8 -5 2831.49 145.818 28 -4 8 -5 3022.25 317.842 1 4 -8 5 2652.99 156.777 9 -4 8 -6 103.732 76.7338 1 -4 8 -6 143.267 44.1276 28 4 -8 6 81.8439 34.1250 9 -4 8 -6 76.5100 36.6498 35 -4 8 -7 1021.85 97.5602 28 4 -8 7 875.348 92.1150 33 4 -8 7 1055.80 110.994 17 -4 8 -7 1050.21 184.939 1 4 -8 7 936.349 92.2414 9 4 -8 8 6818.55 282.288 17 4 -8 8 6246.18 246.159 33 -4 8 -8 6360.82 244.703 28 -4 8 -8 6729.83 284.419 10 4 -8 8 6441.24 235.752 9 4 -8 9 685.267 99.5846 17 4 -8 9 481.474 66.2575 9 4 -8 9 482.297 72.9173 33 -4 8 -9 486.387 76.4388 28 -4 8 -9 595.821 91.8109 10 4 -8 10 1543.23 110.444 9 4 -8 10 1538.01 134.996 17 4 -8 10 1513.15 123.057 33 -4 8 -10 1649.93 133.048 28 -4 8 -10 1528.86 149.539 10 4 -8 11 755.649 98.4852 17 4 -8 11 708.300 87.4151 33 -4 8 -11 786.359 96.5365 28 -4 8 -11 711.877 103.627 10 4 -8 12 1942.75 144.977 17 4 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-2 3207.77 165.506 14 -4 7 1 1832.53 152.804 37 -4 7 1 1813.07 216.693 1 -4 7 1 2124.79 230.793 2 -4 7 0 7545.01 292.450 37 -4 7 0 7461.36 235.556 18 -4 7 0 7665.31 426.613 2 -4 7 0 7125.26 439.167 1 -4 7 -1 1655.70 196.714 2 -4 7 -1 1586.11 112.964 18 -4 7 -1 1688.69 216.143 1 -4 7 -2 8766.07 266.327 18 -4 7 -2 9285.05 460.713 2 -4 7 -2 9388.97 520.074 1 -4 7 -3 845.878 160.197 1 -4 7 -3 914.911 90.4447 18 -4 7 -3 642.597 74.2705 35 -4 7 -4 1149.19 184.229 1 -4 7 -4 1182.28 100.527 35 -4 7 -4 1090.25 99.2277 18 -4 7 -5 1094.30 98.6196 35 -4 7 -5 1051.17 91.6875 28 -4 7 -5 1211.19 197.426 1 -4 7 -5 1125.27 102.854 18 4 -7 5 891.174 83.8164 9 -4 7 -6 856.904 85.3213 28 -4 7 -6 726.719 88.5698 18 -4 7 -6 811.162 88.5516 35 4 -7 6 722.144 74.7365 9 -4 7 -6 960.878 176.818 1 4 -7 7 2166.14 134.178 33 4 -7 7 2032.65 148.791 17 -4 7 -7 2012.28 135.554 28 -4 7 -7 1975.24 247.609 1 -4 7 -7 2109.99 157.850 10 4 -7 7 2023.16 124.639 9 4 -7 8 4136.67 210.870 17 4 -7 8 4109.10 189.277 33 -4 7 -8 4433.96 204.634 28 -4 7 -8 4467.04 372.951 1 -4 7 -8 4285.15 235.809 10 4 -7 9 1294.60 123.027 17 4 -7 9 1039.61 100.049 33 -4 7 -9 1249.94 115.923 28 -4 7 -9 1313.74 138.009 10 -4 7 -9 884.043 163.676 1 4 -7 10 1227.62 119.207 17 4 -7 10 1192.28 106.107 33 -4 7 -10 1176.37 116.514 28 -4 7 -10 1370.50 144.667 10 4 -7 11 4830.54 228.462 17 4 -7 11 4347.64 201.208 33 -4 7 -11 4747.53 226.329 28 -4 7 -11 4553.26 269.059 10 -4 7 -12 5184.34 219.233 36 4 -7 12 4603.88 204.363 33 -4 7 -12 4816.29 231.237 28 4 -7 12 4861.54 224.090 17 -4 7 -12 5062.39 286.047 10 -4 7 -13 1417.90 114.763 36 4 -7 13 1457.02 118.946 17 -4 7 -13 1300.01 146.387 10 4 -7 14 944.550 121.587 38 -4 7 -14 970.448 89.4935 36 4 -7 14 955.035 88.9437 17 -4 7 -14 1046.62 128.487 10 4 -7 15 56.5016 51.8605 38 -4 7 -15 5.88165 24.8564 13 -4 7 -15 31.9810 36.0201 10 4 -7 16 88.2259 38.0855 38 -4 7 -16 109.507 26.0646 13 -4 7 -17 0.06975 13.8620 32 4 -6 -13 3.10259 9.97688 14 4 -6 -12 13.2305 20.3288 14 -4 6 12 6.38924 22.5836 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293.550 67.2298 22 -7 -6 6 409.713 84.3361 21 -7 -6 6 379.966 78.9996 41 -7 -6 5 662.032 109.488 19 -7 -6 5 776.394 105.605 29 -7 -6 5 509.108 92.8021 27 -7 -6 5 631.944 96.1571 25 -7 -6 5 700.583 97.5339 22 -7 -6 5 595.508 88.9504 21 -7 -6 5 744.969 95.1753 44 -7 -6 4 56.7198 50.9215 19 -7 -6 4 19.2038 49.5843 15 -7 -6 4 139.263 61.9617 29 -7 -6 4 62.0431 45.8577 27 -7 -6 4 1.61371 50.2806 25 -7 -6 4-12.3481 49.0257 21 -7 -6 4 35.3504 39.2187 44 -7 -6 3 150.713 65.2060 19 -7 -6 3 95.1448 43.3560 15 -7 -6 3 228.480 68.5218 29 -7 -6 3 287.137 74.5046 25 -7 -6 3 161.791 59.3085 21 -7 -6 3 179.093 53.7180 44 -7 -6 3 122.211 55.2803 42 -7 -6 2 1434.54 136.324 15 -7 -6 2 1862.89 153.048 29 -7 -6 2 1629.19 145.540 25 -7 -6 2 1464.06 136.220 21 -7 -6 2 1511.55 129.087 44 -7 -6 2 1871.74 169.594 19 -7 -6 2 1569.31 159.696 42 -7 -6 1 1956.78 147.584 15 -7 -6 1 2303.80 168.519 29 -7 -6 1 2122.56 162.388 25 -7 -6 1 1984.74 146.412 44 -7 -6 1 1977.34 167.228 19 -7 -6 1 2111.49 183.217 42 -7 -6 0 592.383 93.7110 19 -7 -6 0 606.873 79.2258 15 -7 -6 0 766.162 104.480 29 -7 -6 0 647.129 97.1872 25 -7 -6 0 685.562 91.9654 44 -7 -6 0 687.926 106.469 42 -7 -6 -1 41.5568 39.1459 19 -7 -6 -1 39.0137 50.0698 29 -7 -6 -1 33.4444 45.9418 25 -7 -6 -1 51.6292 41.8834 44 -7 -6 -1 25.8845 46.9576 42 -7 -6 -2 250.326 63.9279 29 -7 -6 -2 190.759 58.0982 25 -7 -6 -2 271.140 75.4608 20 -7 -6 -2 235.090 55.6178 44 -7 -6 -2 298.152 58.4577 19 -7 -6 -3 86.1680 41.7135 29 -7 -6 -3 16.6010 39.9415 25 -7 -6 -3 14.3058 27.5523 44 -7 -6 -3 32.6482 42.5043 20 -7 -6 -4 286.659 53.3430 29 -7 -6 -4 222.958 51.1689 25 -7 -6 -4 180.590 43.0941 44 -7 -6 -4 292.913 64.0121 20 -7 -6 -5 611.296 60.2936 29 -7 -6 -5 587.844 70.1993 25 -7 -6 -5 547.114 59.2032 44 -7 -6 -5 596.479 76.4915 20 -7 -6 -6 36.8389 25.8523 25 -7 -6 -6 86.3915 34.7167 20 -7 -6 -6 49.5431 21.0183 44 -7 -7 15 18.5317 12.9134 27 -7 -7 15-7.15822 12.7083 22 -7 -7 14 210.705 41.7600 27 -7 -7 14 142.803 35.6104 22 -7 -7 13 841.675 89.1493 27 -7 -7 13 699.077 79.0090 22 -7 -7 12 85.0935 28.3358 15 -7 -7 12 87.4687 48.9209 27 -7 -7 12 46.7137 26.3318 22 -7 -7 11 71.8761 35.9989 15 -7 -7 11 60.5818 45.6692 27 -7 -7 11 112.045 51.1337 11 -7 -7 11-39.3065 29.1126 22 -7 -7 10 642.573 85.5348 15 -7 -7 10 638.559 97.2313 27 -7 -7 10 785.293 104.894 11 -7 -7 10 621.918 85.0208 22 -7 -7 9-12.4879 53.0655 27 -7 -7 9 57.7995 56.9994 11 -7 -7 9-35.2708 30.4914 22 -7 -7 8 2783.19 199.362 27 -7 -7 8 2634.15 185.087 11 -7 -7 8 2555.48 167.758 22 -7 -7 8 2940.61 193.403 19 -7 -7 8 2978.98 198.498 41 -7 -7 7 1915.10 164.474 27 -7 -7 7 1895.60 155.646 11 -7 -7 7 1933.95 145.097 22 -7 -7 7 2086.94 159.706 21 -7 -7 7 2223.01 176.325 19 -7 -7 7 1980.12 173.164 41 -7 -7 6 23.2199 56.4716 19 -7 -7 6 63.8177 44.6182 27 -7 -7 6 95.4499 63.1330 25 -7 -7 6 33.1589 37.5779 11 -7 -7 6 12.8137 22.4437 22 -7 -7 6-0.74805 54.8381 21 -7 -7 6 22.8704 53.4141 41 -7 -7 5 863.129 107.513 27 -7 -7 5 1026.99 115.994 25 -7 -7 5 966.349 114.081 21 -7 -7 5 887.195 101.530 44 -7 -7 5 1014.14 130.130 19 -7 -7 4 269.019 80.1099 19 -7 -7 4 114.361 49.9719 15 -7 -7 4 163.551 54.0493 27 -7 -7 4 142.102 62.8532 25 -7 -7 4 182.486 67.5374 21 -7 -7 4 181.472 56.2190 44 -7 -7 4 89.0693 53.8121 42 -7 -7 3 687.356 109.496 19 -7 -7 3 505.943 79.1294 15 -7 -7 3 783.060 107.388 29 -7 -7 3 601.036 92.6745 25 -7 -7 3 645.145 94.9409 21 -7 -7 3 618.472 88.1331 44 -7 -7 3 480.946 93.6343 42 -7 -7 2 351.484 78.4615 19 -7 -7 2 372.551 68.1866 15 -7 -7 2 610.323 95.6961 29 -7 -7 2 626.741 93.4357 25 -7 -7 2 342.151 75.8665 21 -7 -7 2 400.489 69.5255 44 -7 -7 2 339.971 76.5926 42 -7 -7 1 554.686 91.1222 19 -7 -7 1 617.894 76.3036 15 -7 -7 1 683.741 94.7756 29 -7 -7 1 636.693 90.1820 25 -7 -7 1 583.448 84.1156 44 -7 -7 1 526.267 84.1150 21 -7 -7 1 552.092 92.0518 42 -7 -7 0 153.521 50.4122 19 -7 -7 0 246.554 63.7849 29 -7 -7 0 327.176 70.7736 25 -7 -7 0 149.530 49.4281 44 -7 -7 0 251.687 67.4682 42 -7 -7 -1 42.4132 29.0068 19 -7 -7 -1 121.450 50.0656 29 -7 -7 -1 178.608 54.8891 25 -7 -7 -1 167.946 47.5324 44 -7 -7 -2 549.178 71.8192 29 -7 -7 -2 563.315 76.0911 25 -7 -7 -2 487.132 67.6950 44 -7 -7 -3 352.062 53.5835 29 -7 -7 -3 346.002 57.8778 25 -7 -7 -3 303.857 52.2533 44 -7 -7 -4 632.599 54.0489 29 -7 -7 -4 579.610 60.3006 44 -7 -7 -5 1581.87 81.1686 25 -7 -7 -5 1372.05 73.9694 44 -7 -7 -6-65.9261 20.8519 21 -7 -8 14 172.948 36.7974 27 -7 -8 14 169.502 28.2036 22 -7 -8 13-24.9439 14.5439 15 -7 -8 13 42.1117 28.9519 27 -7 -8 13 31.9999 18.0855 22 -7 -8 12 94.0479 31.2512 15 -7 -8 12 110.712 42.8652 27 -7 -8 12 149.863 34.5540 22 -7 -8 11 378.212 59.7159 15 -7 -8 11 462.626 76.1694 27 -7 -8 11 557.933 79.7628 11 -7 -8 11 402.565 53.3258 22 -7 -8 10 59.2253 37.5538 15 -7 -8 10 49.1215 40.9082 27 -7 -8 10 104.243 45.5238 11 -7 -8 10 172.679 40.3302 22 -7 -8 9 127.945 56.3868 27 -7 -8 9 173.313 54.9887 11 -7 -8 8-38.8325 38.6600 27 -7 -8 8-1.14812 32.0635 11 -7 -8 8-21.0444 37.8683 41 -7 -8 8 11.0066 41.3844 19 -7 -8 7 107.396 52.5317 19 -7 -8 7 80.8692 42.9357 27 -7 -8 7 103.599 41.7904 11 -7 -8 7 72.6833 52.2999 41 -7 -8 6 333.113 76.5672 19 -7 -8 6 382.955 72.2778 27 -7 -8 6 386.721 83.0983 21 -7 -8 5 1673.62 139.643 15 -7 -8 5 1830.82 137.653 27 -7 -8 5 2008.08 143.947 25 -7 -8 5 1947.45 150.086 21 -7 -8 5 1752.59 162.479 19 -7 -8 5 1705.03 157.595 42 -7 -8 4 1573.88 131.167 15 -7 -8 4 1717.49 134.636 25 -7 -8 4 1654.42 140.848 21 -7 -8 4 1803.49 135.261 44 -7 -8 4 1690.56 153.153 19 -7 -8 4 1554.89 146.511 42 -7 -8 3 410.011 82.2756 19 -7 -8 3 332.088 58.6283 15 -7 -8 3 444.190 75.5307 25 -7 -8 3 397.784 76.7452 21 -7 -8 3 442.656 76.3987 44 -7 -8 3 471.797 83.8311 42 -7 -8 2 433.228 77.2126 19 -7 -8 2 401.780 59.4686 15 -7 -8 2 376.027 69.5531 25 -7 -8 2 309.970 69.1229 21 -7 -8 2 362.870 69.4327 44 -7 -8 2 294.850 65.3035 42 -7 -8 1 58.5837 36.2291 19 -7 -8 1-2.98113 40.7797 25 -7 -8 1-63.6062 60.4238 21 -7 -8 1 11.2987 38.1287 44 -7 -8 1 38.8248 38.6764 42 -7 -8 0 1.14281 28.2559 19 -7 -8 0 36.5435 31.2564 25 -7 -8 0-3.45569 50.4065 21 -7 -8 0 76.9083 39.6681 44 -7 -8 -1 525.795 64.1967 25 -7 -8 -1 593.055 75.5346 21 -7 -8 -1 569.477 69.9220 44 -7 -8 -1 609.975 66.6341 19 -7 -8 -2 1181.19 81.9827 25 -7 -8 -2 1104.34 90.8817 21 -7 -8 -2 1136.98 87.0839 44 -7 -8 -3 113.192 25.0688 25 -7 -8 -3 146.918 36.4892 21 -7 -8 -3 172.637 35.9642 44 -7 -8 -4 83.5276 24.9460 21 -7 -9 14 22.1340 15.4425 27 -7 -9 13 81.7801 29.0930 27 -7 -9 12 115.439 30.0521 15 -7 -9 12 176.308 42.2346 27 -7 -9 11 14.6259 24.6529 15 -7 -9 11 14.4346 26.7526 27 -7 -9 10-26.1201 38.5758 15 -7 -9 10-1.27777 28.7296 27 -7 -9 10 32.6308 28.3204 11 -7 -9 9-1.72553 42.1333 15 -7 -9 9-4.46865 24.6370 27 -7 -9 8 742.380 90.0319 15 -7 -9 8 760.807 85.1243 27 -7 -9 8 880.313 95.0867 19 -7 -9 7-39.5443 38.7178 19 -7 -9 7-94.8454 54.3639 15 -7 -9 7-1.59948 21.1973 27 -7 -9 7-8.61033 40.6934 42 -7 -9 6 261.688 67.9828 19 -7 -9 6 201.988 50.2780 15 -7 -9 6 295.643 69.4568 21 -7 -9 6 168.128 55.4307 42 -7 -9 5 89.2241 51.1312 19 -7 -9 5 29.6467 30.1502 15 -7 -9 5 125.118 54.4681 21 -7 -9 5 41.6101 38.7417 42 -7 -9 4 454.213 78.6345 19 -7 -9 4 283.212 50.1760 15 -7 -9 4 401.713 65.6504 21 -7 -9 4 539.945 75.6940 44 -7 -9 4 291.263 58.3068 42 -7 -9 3 37.0292 37.7327 19 -7 -9 3-8.55970 18.8291 15 -7 -9 3 79.1785 38.4434 25 -7 -9 3 55.6188 41.6253 21 -7 -9 3 53.4425 41.1688 44 -7 -9 3 24.3716 29.4910 42 -7 -9 2 50.4778 34.0380 19 -7 -9 2 78.8087 35.7871 25 -7 -9 2 84.4937 41.2942 21 -7 -9 2 70.2331 39.8648 44 -7 -9 2 78.1271 36.6507 42 -7 -9 1 845.222 70.6248 25 -7 -9 1 813.985 81.2410 21 -7 -9 1 853.984 81.2487 44 -7 -9 1 724.196 77.5172 19 -7 -9 0 247.049 36.0963 25 -7 -9 0 270.425 50.6462 21 -7 -9 0 270.391 46.9115 44 -7 -9 0 269.282 43.9014 19 -7 -9 -1 54.3848 27.3175 21 -7 -9 -1 47.3328 25.5705 44 -7 -9 -2 648.970 52.6217 21 -7 -9 -2 620.874 49.6648 44 -7 -10 12 67.8293 18.8873 15 -7 -10 12 139.157 27.8329 27 -7 -10 11-29.3068 23.1468 15 -7 -10 11 1.74062 14.5396 27 -7 -10 10 983.886 80.5370 15 -7 -10 10 848.693 71.2649 27 -7 -10 9 44.8470 29.1957 15 -7 -10 9 120.132 28.7126 27 -7 -10 9 27.5548 24.6038 42 -7 -10 8 38.7933 27.4997 15 -7 -10 8 90.3284 36.5739 19 -7 -10 8 58.9856 30.7713 42 -7 -10 7 333.034 57.9495 19 -7 -10 7 264.632 46.5395 15 -7 -10 7 372.703 58.7305 42 -7 -10 6 20.8072 31.8010 19 -7 -10 6-30.4651 29.7960 15 -7 -10 6 15.6529 21.9497 42 -7 -10 5 108.946 41.2110 19 -7 -10 5 33.5609 20.8880 15 -7 -10 5 84.1414 31.8548 42 -7 -10 4 93.9621 38.9178 19 -7 -10 4 32.5002 17.0361 15 -7 -10 4 144.259 39.6543 21 -7 -10 4 80.4766 29.4520 42 -7 -10 3 43.1640 27.1911 19 -7 -10 3 81.2416 32.8400 21 -7 -10 2 47.5915 27.7043 21 -7 -10 2 97.4601 32.6867 19 -7 -10 1 1211.81 71.1550 21 -7 -10 1 1250.35 75.3978 44 -7 -11 9 74.8277 21.7001 15 -7 -11 8-8.59327 15.1455 15 -7 -11 7 33.0737 16.2215 15 -7 -11 6 251.969 39.7714 19 -7 -11 5 23.3469 18.9288 19 -7 -11 4 0.16756 16.0176 19 8 -10 0 105.662 22.3498 17 8 -10 1 29.5009 17.8016 17 8 -10 2 95.7626 26.4307 17 8 -10 3 745.604 59.5798 17 8 -10 4 1083.48 70.4003 17 8 -10 5 20.0905 15.6250 17 8 -10 6 78.8051 19.1691 17 -8 10 -7 20.2938 13.8240 36 -8 9 3 425.638 39.3569 35 -8 9 2 8.53617 17.2890 35 -8 9 1 139.115 33.0760 35 -8 9 0 4.15886 25.1843 35 -8 9 -1 24.9309 28.6782 35 -8 9 -2 50.6442 32.4790 35 8 -9 3 126.613 33.8583 17 8 -9 4 56.2960 28.6543 17 -8 9 -4 15.6060 17.3508 28 8 -9 5 127.823 33.7741 17 -8 9 -5 135.149 29.5401 28 8 -9 6 52.1719 23.5941 17 -8 9 -6 9.88782 21.2477 28 8 -9 7 11.0958 15.8250 17 -8 9 -7 20.1877 18.3512 28 -8 9 -8-0.73403 17.7373 36 -8 9 -8-20.9260 19.5699 28 -8 9 -9 115.530 23.5977 36 -8 8 5 332.749 42.1099 37 -8 8 5 327.547 37.9280 35 8 -8 -4 4.09061 8.26435 9 -8 8 4-29.7511 24.6288 37 -8 8 4 1.48680 19.9925 35 8 -8 -3-41.4547 15.1205 9 -8 8 3 15.1232 24.4795 37 -8 8 3 29.7699 27.2067 35 -8 8 2 43.9208 23.8693 18 8 -8 -2 41.4016 16.1887 9 -8 8 2 27.9504 21.4430 37 -8 8 2 52.5551 33.0480 35 -8 8 1-28.2977 27.7199 18 -8 8 1-37.1647 27.3280 37 -8 8 1 6.75820 29.7843 35 -8 8 0 149.670 41.7398 18 -8 8 0 155.996 37.7827 37 -8 8 0 191.256 49.9527 35 -8 8 0 144.286 30.0026 28 -8 8 -1 1775.94 119.075 18 -8 8 -1 1815.73 124.056 35 -8 8 -1 1709.91 99.0152 28 -8 8 -2 274.577 57.1866 18 -8 8 -2 298.351 58.9341 35 -8 8 -2 268.223 48.2873 28 -8 8 -3 516.204 72.3256 35 -8 8 -3 529.995 64.3539 28 8 -8 4 126.066 42.1196 17 -8 8 -4 123.050 39.5259 28 8 -8 5 135.311 39.2753 17 -8 8 -5 181.848 44.7622 28 8 -8 6 309.301 48.8765 17 -8 8 -6 424.614 60.2131 28 8 -8 7 289.066 39.2559 17 -8 8 -7 335.537 54.3009 28 -8 8 -8 28.1196 25.5950 36 -8 8 -8 58.8715 30.5885 28 -8 8 -9 214.542 35.3756 36 -8 8 -9 208.185 37.9276 28 -8 8 -10 1103.95 62.8521 36 -8 7 7 993.930 73.7948 37 -8 7 7 991.605 61.1876 35 -8 7 6 447.242 59.1697 37 -8 7 6 482.998 53.8751 35 -8 7 5 174.608 32.1513 40 -8 7 5 155.562 43.7972 37 -8 7 5 72.6625 33.6268 35 -8 7 4 41.3605 25.7439 40 -8 7 4 26.7361 23.5592 18 -8 7 4 53.4493 33.5237 37 -8 7 4 0.72336 31.5381 35 -8 7 3 24.3629 26.0983 40 -8 7 3-0.33647 25.5119 18 -8 7 3-2.67806 29.5803 37 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89.1563 28 -8 7 -9 12.5377 23.5198 36 -8 7 -9 2.65459 14.7454 8 -8 7 -9-6.21715 30.6006 28 -8 7 -9-13.2843 15.5765 13 -8 7 -10 37.7077 23.6116 36 -8 7 -10 70.0378 22.6341 8 -8 7 -10-19.7183 28.6291 28 -8 7 -10 13.5682 14.3839 13 -8 7 -11 222.423 28.7379 36 -8 6 8 922.848 58.8436 40 -8 6 8 982.060 80.2455 37 -8 6 7 19.0646 16.9219 40 -8 6 7 14.5407 27.3414 37 -8 6 6 283.565 50.0405 40 -8 6 6 259.875 58.1560 37 -8 6 5 216.680 50.1129 40 -8 6 5 226.219 40.1111 18 -8 6 5 178.096 58.9126 37 -8 6 5 100.435 29.3323 28 -8 6 4 399.239 66.9087 40 -8 6 4 390.403 60.4885 18 -8 6 4 227.843 57.6797 37 -8 6 4 299.856 49.3391 28 -8 6 3 481.891 73.9729 40 -8 6 3 511.398 74.8353 18 -8 6 3 410.743 76.3583 37 -8 6 3 492.355 67.1614 28 -8 6 2 92.8522 49.1095 40 -8 6 2 108.554 53.9768 18 -8 6 2 43.2295 42.2824 37 -8 6 2 5.84297 42.2894 35 -8 6 2 98.3325 44.4359 28 -8 6 1 415.850 74.8506 40 -8 6 1 483.118 83.9460 18 -8 6 1 276.194 65.5801 37 -8 6 1 408.647 70.7012 35 -8 6 1 422.378 71.8239 28 -8 6 0 341.782 70.9797 40 -8 6 0 268.567 76.0843 18 -8 6 0 162.336 52.4398 37 -8 6 0 292.020 65.7109 35 -8 6 0 251.611 60.3895 28 -8 6 -1 18.6693 54.7665 18 -8 6 -1-5.98602 32.4871 37 -8 6 -1-20.2722 42.1119 35 -8 6 -1 91.4647 51.7349 28 -8 6 -2 172.984 63.6147 18 -8 6 -2 105.423 46.1890 37 -8 6 -2 73.1072 43.6657 35 -8 6 -2 157.604 62.1253 28 -8 6 -3 17.7000 55.4194 18 -8 6 -3 70.7388 34.0621 37 -8 6 -3 51.9574 46.0129 35 -8 6 -3 69.5112 56.9086 28 -8 6 -4 538.264 86.9707 18 -8 6 -4 470.897 64.8697 8 -8 6 -4 585.152 92.5132 28 -8 6 -5 3123.64 172.141 18 -8 6 -5 2772.46 158.747 8 8 -6 5 2489.77 135.396 17 -8 6 -5 3307.95 183.059 28 -8 6 -6 36.8326 27.7459 8 -8 6 -6 108.393 59.5034 28 -8 6 -7 794.590 86.2710 8 -8 6 -7 915.388 86.7422 36 -8 6 -7 891.026 96.6985 28 -8 6 -8-9.18461 27.5874 36 -8 6 -8 8.49774 41.3594 28 -8 6 -9 1229.72 89.1103 36 -8 6 -9 1384.28 100.510 28 -8 6 -9 1049.08 73.8156 13 -8 6 -10 64.7887 25.5299 36 -8 6 -10 55.7030 25.4033 8 -8 6 -10 69.4790 32.0029 28 -8 6 -10 50.6110 18.1796 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42 -9 -5 1 1229.26 93.1637 15 -9 -5 1 1357.77 106.288 29 -9 -5 1 1056.04 95.8422 26 -9 -5 1 1234.76 100.347 25 -9 -5 1 1186.10 88.1222 21 -9 -5 0 174.656 32.8347 15 -9 -5 0 138.609 44.0567 29 -9 -5 0 119.841 36.1871 26 -9 -5 0 118.595 42.9344 25 -9 -5 0 128.849 33.0209 21 -9 -5 -1-2.41675 28.7826 29 -9 -5 -1 77.3029 24.5323 26 -9 -5 -1-15.2574 31.1861 25 -9 -5 -1 1.72038 18.0222 21 -9 -5 -2 42.5716 30.1050 29 -9 -5 -2 26.6180 23.3770 25 -9 -5 -2-4.77748 15.9322 21 -9 -5 -3 10.4633 19.0343 29 -9 -5 -3-44.1838 23.4918 25 -9 -6 11-8.05213 18.0983 24 -9 -6 10 93.9785 26.7606 15 -9 -6 10 25.4845 21.6553 24 -9 -6 9 899.291 73.4334 15 -9 -6 9 826.713 64.5749 26 -9 -6 9 747.749 71.6634 24 -9 -6 9 695.453 63.7268 42 -9 -6 8 244.777 48.6675 15 -9 -6 8 223.278 42.2711 26 -9 -6 8 172.840 39.2063 24 -9 -6 8 205.234 41.8724 42 -9 -6 7 1103.42 95.5235 15 -9 -6 7 1145.59 96.5414 26 -9 -6 7 911.612 81.5171 24 -9 -6 7 1027.28 92.3549 42 -9 -6 6 527.720 71.8217 15 -9 -6 6 352.675 63.1825 26 -9 -6 6 315.825 47.6719 24 -9 -6 6 410.310 64.9776 42 -9 -6 5 771.413 82.4638 15 -9 -6 5 669.029 82.0824 26 -9 -6 5 576.811 59.6975 24 -9 -6 5 714.996 86.2321 42 -9 -6 4 1086.41 93.2516 15 -9 -6 4 968.348 96.0073 26 -9 -6 4 939.181 67.2289 24 -9 -6 4 1135.08 105.665 42 -9 -6 3 379.730 55.3663 15 -9 -6 3 452.881 68.9598 26 -9 -6 3 519.184 60.8514 21 -9 -6 3 566.262 78.6736 42 -9 -6 2 65.7964 26.5837 15 -9 -6 2 69.8226 32.8055 26 -9 -6 2 193.448 46.7330 25 -9 -6 2 151.907 37.8167 21 -9 -6 1 747.306 56.9790 15 -9 -6 1 638.646 63.4091 26 -9 -6 1 698.950 63.6720 21 -9 -6 0 36.4486 17.8375 26 -9 -6 0 64.1936 29.1652 25 -9 -6 0 34.4417 20.1823 21 -9 -6 -1 354.341 45.2911 25 -9 -6 -1 272.689 35.1308 21 -9 -6 -2 4.93332 14.1023 25 -9 -7 10 281.587 36.1692 24 -9 -7 9 212.784 31.6590 26 -9 -7 9 148.607 28.9457 24 -9 -7 9 192.188 33.8091 42 -9 -7 8 691.086 64.2542 15 -9 -7 8 552.571 55.3877 26 -9 -7 8 663.405 64.2900 42 -9 -7 7 1859.35 105.968 15 -9 -7 7 1754.83 104.005 26 -9 -7 7 1493.15 82.9913 24 -9 -7 7 1743.14 108.318 42 -9 -7 6 277.111 45.9485 15 -9 -7 6 166.538 42.5815 26 -9 -7 6 159.338 27.9502 24 -9 -7 6 229.893 43.5378 42 -9 -7 5 2245.82 115.290 15 -9 -7 5 2539.05 129.846 26 -9 -7 5 2506.18 136.087 42 -9 -7 4 1627.68 93.9767 15 -9 -7 4 1716.34 104.934 26 -9 -7 3-11.1685 18.6127 15 -9 -7 3-0.30912 25.3241 26 -9 -7 2 66.0625 29.7881 25 -9 -7 2 64.0004 24.9276 21 -9 -7 1 458.517 48.1442 25 -9 -7 1 390.841 41.5281 21 -9 -7 0 26.5893 15.7229 25 -9 -8 8 45.0749 18.7035 15 -9 -8 7 99.2063 24.9617 15 -9 -8 7 135.957 28.0794 26 -9 -8 7 115.879 27.4848 42 -9 -8 6 13.4728 15.6410 15 -9 -8 6 11.2496 17.4638 26 -9 -8 5 95.4484 25.2869 26 -9 -8 4 180.819 29.6169 26 -10 6 1 131.164 25.5187 18 -10 6 0 54.1830 20.3235 28 -10 6 -1 872.375 57.3729 28 -10 6 -2 523.558 45.6958 28 -10 6 -3 42.2829 19.9869 28 -10 5 4 273.631 35.9310 37 -10 5 3 73.4878 24.4578 18 -10 5 3 99.8293 29.3621 37 -10 5 3 106.129 23.3520 28 -10 5 2 167.340 34.5401 18 -10 5 2 195.337 33.0599 28 -10 5 1 290.907 43.9141 18 -10 5 1 265.172 39.0358 28 -10 5 0 29.5332 26.4533 18 -10 5 0 48.8544 27.7604 28 -10 5 -1 14.2326 23.1500 18 -10 5 -1 4.52273 25.9338 28 -10 5 -2 22.7514 27.6341 28 -10 5 -3 1290.23 79.3043 28 -10 5 -4 1343.18 74.5409 28 -10 5 -5 442.407 40.1622 28 -10 4 5 109.809 26.4835 18 -10 4 5 131.043 30.1502 37 -10 4 5 121.984 25.4214 28 -10 4 4 326.121 43.5505 18 -10 4 4 330.816 50.5218 37 -10 4 4 333.227 43.5382 28 -10 4 3 60.3788 30.2109 18 -10 4 3 36.2941 31.7636 37 -10 4 3 40.0305 27.6567 28 -10 4 2 1115.71 81.4276 18 -10 4 2 1191.59 95.9596 37 -10 4 2 1247.54 87.2458 28 -10 4 1 1817.32 103.526 18 -10 4 1 2059.62 113.157 28 -10 4 0 54.9210 30.4033 18 -10 4 0 129.718 41.8173 28 -10 4 -1 156.982 35.4285 18 -10 4 -1 194.729 44.7543 28 -10 4 -2 2.94236 11.5360 8 -10 4 -2 29.3983 30.9826 28 -10 4 -3 332.856 39.7504 8 -10 4 -3 504.230 57.0663 28 -10 4 -4 795.748 58.4012 8 -10 4 -4 1081.36 71.2527 28 -10 4 -5 376.407 37.5720 8 -10 4 -5 494.527 43.9548 28 -10 3 7 738.667 54.1491 40 -10 3 6 112.571 29.5412 40 -10 3 6 129.372 28.4050 18 -10 3 6 118.705 31.4421 37 -10 3 6 85.5249 23.6007 28 -10 3 5 80.5660 31.8820 40 -10 3 5 59.2376 29.1414 18 -10 3 5 80.3688 31.8407 37 -10 3 5 17.4671 23.3264 28 -10 3 4 147.175 37.7540 18 -10 3 4 162.764 43.0052 37 -10 3 4 129.053 38.1310 28 -10 3 3 676.015 69.1562 18 -10 3 3 751.260 83.1069 37 -10 3 3 703.568 71.9296 28 -10 3 2 171.533 45.2645 18 -10 3 2 188.154 45.4815 28 -10 3 1 597.767 64.9165 18 -10 3 1 686.965 73.9026 28 -10 3 0 891.924 74.1292 18 -10 3 0 871.907 70.0789 8 -10 3 0 932.226 83.1800 28 -10 3 -1 20.3522 22.8636 18 -10 3 -1 25.7853 20.0279 8 -10 3 -1 52.9362 34.5168 28 -10 3 -2 37.7707 22.4875 18 -10 3 -2-33.7655 21.1395 8 -10 3 -2 37.6309 29.2340 28 -10 3 -3-8.15570 18.8714 8 -10 3 -3 58.7753 29.0965 28 -10 3 -4 12.4556 16.0731 8 -10 3 -4 18.7971 20.1870 28 -10 3 -5 18.2430 17.8005 8 -10 3 -5 51.7402 18.9085 28 -10 3 -6 360.525 38.2680 8 -10 2 7 818.401 63.8623 40 -10 2 7 836.514 61.3553 18 -10 2 7 767.707 63.8725 37 -10 2 7 805.497 62.2393 28 -10 2 6 1.32492 21.1187 40 -10 2 6 40.1132 26.8469 37 -10 2 6-5.18142 27.2801 28 -10 2 5 235.110 46.1301 40 -10 2 5 171.266 46.7628 37 -10 2 5 137.127 35.5161 28 -10 2 4 40.5111 35.2571 37 -10 2 4-36.8261 35.2668 18 -10 2 4-23.0519 33.6141 28 -10 2 3 44.7842 31.4636 18 -10 2 3 77.4420 39.6381 28 -10 2 2 117.309 36.9737 18 -10 2 2 181.134 51.2857 28 -10 2 1 118.363 36.7517 18 -10 2 1 106.854 42.0688 28 -10 2 0 16.7113 24.5933 18 -10 2 0 18.9000 23.4670 8 -10 2 0 15.9534 34.0594 28 -10 2 -1 1486.05 83.4360 18 -10 2 -1 1436.73 102.818 8 -10 2 -1 1530.44 99.9163 28 -10 2 -2 1061.37 87.4446 8 -10 2 -2 1048.50 78.7617 28 -10 2 -3 170.555 39.6020 8 -10 2 -3 192.795 34.7100 28 -10 2 -4 23.0377 22.5342 8 -10 2 -4 1.84918 14.8351 28 -10 2 -5 198.942 33.8330 8 -10 2 -6 92.6986 22.4255 8 -10 1 8 40.4673 18.3566 40 -10 1 8-45.0100 24.2994 28 -10 1 7 24.0454 21.7770 40 -10 1 7-52.7855 30.6446 28 -10 1 6 127.123 35.2122 40 -10 1 6 46.2914 27.4800 28 -10 1 5 67.0147 30.2916 28 -10 1 4 704.750 73.5866 28 -10 1 3 195.570 45.6458 28 -10 1 2 13.3509 28.3519 18 -10 1 2 78.5629 35.9276 28 -10 1 1 185.711 44.8134 8 -10 1 1 146.844 35.4200 18 -10 1 1 162.799 40.6717 28 -10 1 0 553.880 53.6597 18 -10 1 0 594.635 71.3922 8 -10 1 0 568.361 63.5077 28 -10 1 -1 4.16112 30.3297 8 -10 1 -1-3.39766 23.6492 28 -10 1 -2 295.849 52.7176 8 -10 1 -2 290.853 40.2894 28 -10 1 -3 1938.02 115.512 8 -10 1 -4 1973.04 108.435 8 -10 1 -4 1221.82 66.8924 29 -10 1 -5 147.013 29.2153 8 -10 0 9 46.3973 17.3153 28 -10 0 8 380.884 39.1503 40 -10 0 8 441.978 49.8661 28 -10 0 7 153.649 30.5569 40 -10 0 7 110.833 32.2094 28 -10 0 6 135.163 34.8994 28 -10 0 5-2.79090 28.5211 28 -10 0 4 1559.86 104.196 28 -10 0 3-48.1914 33.1491 28 -10 0 2 187.347 35.3455 18 -10 0 2 213.834 44.4142 28 -10 0 1 644.623 56.6550 18 -10 0 1 770.871 82.7995 8 -10 0 1 593.961 60.0047 28 -10 0 0 336.347 57.7531 8 -10 0 0 373.535 46.3014 28 -10 0 -1 59.6862 37.2423 8 -10 0 -2 210.064 45.6429 8 -10 0 -2 162.422 30.2545 29 -10 0 -3 34.4205 25.7561 8 -10 0 -3 78.1524 24.4984 29 -10 0 -4 51.4616 22.0840 8 -10 0 -4 59.7085 21.1524 29 -10 0 -5-2.08077 11.7963 8 -10 -1 9 596.406 49.7841 28 -10 -1 8 89.0423 32.6839 24 -10 -1 7 244.743 40.5008 28 -10 -1 7 419.993 56.8996 24 -10 -1 6 248.983 42.3346 28 -10 -1 6 370.107 57.9998 24 -10 -1 5 178.793 37.2216 28 -10 -1 5 365.235 62.0497 24 -10 -1 4 106.625 30.0214 28 -10 -1 4 237.448 54.9069 24 -10 -1 3 38.5797 23.1328 28 -10 -1 3 72.8779 45.8447 24 -10 -1 2 152.564 32.4373 28 -10 -1 0 1953.45 124.850 8 -10 -1 0 1675.45 88.5632 29 -10 -1 -1 4948.80 187.117 8 -10 -1 -1 4541.71 147.466 29 -10 -1 -2 835.253 75.8373 8 -10 -1 -2 895.082 66.8831 29 -10 -1 -3 17.1277 17.9823 8 -10 -1 -3-0.25028 17.7011 29 -10 -1 -4 32.6117 17.1557 8 -10 -1 -4 17.6552 14.2052 29 -10 -2 9 70.8721 19.4344 28 -10 -2 9 170.432 30.5598 24 -10 -2 8-25.0878 18.4179 28 -10 -2 8 33.5315 28.6711 24 -10 -2 7 4.09242 16.7048 28 -10 -2 7 63.4081 34.5504 24 -10 -2 6 207.103 34.2914 28 -10 -2 6 283.861 54.5426 24 -10 -2 5 63.0923 41.6197 15 -10 -2 5-24.5133 16.7727 28 -10 -2 5 5.93077 32.4991 24 -10 -2 4 76.8231 46.8831 15 -10 -2 4 27.8301 33.3504 24 -10 -2 3 802.011 86.7148 15 -10 -2 3 638.889 72.1085 24 -10 -2 2 98.5241 47.0262 15 -10 -2 1-17.4255 18.9251 29 -10 -2 0 1385.28 83.2527 29 -10 -2 0 1126.89 67.8267 25 -10 -2 -1 1802.50 94.5901 29 -10 -2 -1 1496.87 75.5999 25 -10 -2 -2 105.432 27.1090 29 -10 -2 -2 72.0109 18.7117 25 -10 -2 -3 5.15488 14.7025 29 -10 -3 9 691.602 54.5762 24 -10 -3 8 33.4347 25.1335 24 -10 -3 7 102.364 32.4488 15 -10 -3 7 91.3416 34.3884 24 -10 -3 6 849.566 76.8796 15 -10 -3 6 709.401 69.0540 24 -10 -3 5 259.822 53.0668 15 -10 -3 5 246.262 52.5928 26 -10 -3 5 169.693 41.6973 24 -10 -3 4 48.2150 38.5217 15 -10 -3 4 46.2153 40.8352 26 -10 -3 4 46.6599 29.4903 24 -10 -3 3 41.2641 37.3383 15 -10 -3 3 62.7474 41.0381 26 -10 -3 3 70.6079 30.2546 24 -10 -3 2 561.316 66.4945 15 -10 -3 2 477.794 66.4774 26 -10 -3 1 240.806 37.9658 29 -10 -3 1 306.128 40.2531 25 -10 -3 0 96.5419 27.6976 29 -10 -3 0 96.6332 28.0136 25 -10 -3 -1 91.2265 26.2057 29 -10 -3 -1 83.2380 21.1702 25 -10 -3 -2 79.3632 22.7028 29 -10 -4 9 108.716 23.8849 24 -10 -4 8 147.728 29.5871 15 -10 -4 8 138.194 29.7080 24 -10 -4 7 262.857 41.6640 15 -10 -4 7 169.449 34.9984 24 -10 -4 6 28.2143 28.0547 15 -10 -4 6 57.8085 29.8763 26 -10 -4 6 10.5043 22.0630 24 -10 -4 5 78.0812 35.0792 15 -10 -4 5 108.832 38.4301 26 -10 -4 5 37.5567 21.1656 24 -10 -4 4 181.326 42.6927 15 -10 -4 4 132.181 41.4655 26 -10 -4 4 132.333 31.1707 24 -10 -4 3 504.778 59.4833 15 -10 -4 3 509.804 62.3617 26 -10 -4 2 2278.81 108.006 15 -10 -4 2 2292.83 115.723 26 -10 -4 0 262.425 33.0925 25 -10 -5 7 81.8989 26.2845 15 -10 -5 7 66.3931 19.8570 24 -10 -5 6 98.6205 29.8131 15 -10 -5 6 121.580 30.2597 26 -10 -5 6 87.0320 20.8414 24 -10 -5 5 231.367 38.4720 15 -10 -5 5 296.432 44.8874 26 -10 -5 4 361.005 44.3973 15 -10 -5 4 342.383 46.0393 26 -10 -5 3 450.211 44.8454 15 -10 -5 3 474.615 51.0139 26 0 0 0 0.00 0.00 0 TITL cu603 in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 8.764455 11.951469 15.633736 111.8595 95.7465 91.2687 ZERR 2.00 0.000288 0.000539 0.000774 0.0044 0.0033 0.0031 LATT 1 SFAC C H N O UNIT 72.00 68.00 4.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 20939 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp O1 O 0.95911(10) 0.01039(8) 0.37988(7) 0.0648(2) Uani 1 1 d . . O2 O -0.19524(11) 0.25284(10) 0.51171(8) 0.0783(3) Uani 1 1 d . . N1 N 0.66998(12) 0.04879(10) 0.33635(8) 0.0593(3) Uani 1 1 d . . H1N H 0.754(2) 0.0748(15) 0.3794(12) 0.073(5) Uiso 1 1 d . . N2 N 0.10073(12) 0.22073(10) 0.54962(8) 0.0605(3) Uani 1 1 d . . H2N H 0.011(2) 0.1854(15) 0.5172(12) 0.075(5) Uiso 1 1 d . . C1 C 1.1635(2) -0.02850(18) 0.18336(13) 0.0859(5) Uani 1 1 d . . H1 H 1.1112 0.0354 0.2200 0.103 Uiso 1 1 calc R U C2 C 1.2350(3) -0.0174(3) 0.11146(18) 0.1197(8) Uani 1 1 d . . H2 H 1.2294 0.0529 0.0992 0.144 Uiso 1 1 calc R U C3 C 1.3151(3) -0.1124(4) 0.05797(17) 0.1314(11) Uani 1 1 d . . H3 H 1.3642 -0.1055 0.0100 0.158 Uiso 1 1 calc R U C4 C 1.3220(3) -0.2149(3) 0.07542(17) 0.1240(9) Uani 1 1 d . . H4 H 1.3762 -0.2782 0.0397 0.149 Uiso 1 1 calc R U C5 C 1.2490(2) -0.22536(18) 0.14586(14) 0.0915(5) Uani 1 1 d . . H5 H 1.2535 -0.2967 0.1567 0.110 Uiso 1 1 calc R U C6 C 1.16895(14) -0.13278(13) 0.20122(10) 0.0635(3) Uani 1 1 d . . C7 C 1.09733(15) -0.14440(13) 0.28143(10) 0.0634(3) Uani 1 1 d . . H7A H 1.1728 -0.1151 0.3359 0.076 Uiso 1 1 calc R U H7B H 1.0729 -0.2294 0.2675 0.076 Uiso 1 1 calc R U C8 C 0.95236(14) -0.07688(11) 0.30481(9) 0.0547(3) Uani 1 1 d . . C9 C 0.81507(14) -0.11128(11) 0.24042(9) 0.0555(3) Uani 1 1 d . . C10 C 0.80396(14) -0.21295(12) 0.14847(9) 0.0598(3) Uani 1 1 d . . C11 C 0.82975(19) -0.33051(13) 0.13973(11) 0.0735(4) Uani 1 1 d . . H11 H 0.8571 -0.3469 0.1927 0.088 Uiso 1 1 calc R U C12 C 0.8155(2) -0.42402(16) 0.05344(14) 0.0908(5) Uani 1 1 d . . H12 H 0.8362 -0.5019 0.0488 0.109 Uiso 1 1 calc R U C13 C 0.7712(3) -0.40206(19) -0.02477(13) 0.1006(6) Uani 1 1 d . . H13 H 0.7599 -0.4651 -0.0825 0.121 Uiso 1 1 calc R U C14 C 0.7435(3) -0.2867(2) -0.01797(13) 0.0997(6) Uani 1 1 d . . H14 H 0.7129 -0.2717 -0.0712 0.120 Uiso 1 1 calc R U C15 C 0.7610(2) -0.19267(16) 0.06782(11) 0.0785(4) Uani 1 1 d . . H15 H 0.7436 -0.1146 0.0715 0.094 Uiso 1 1 calc R U C16 C 0.68581(14) -0.04598(11) 0.26079(9) 0.0571(3) Uani 1 1 d . . H16 H 0.6006 -0.0719 0.2162 0.069 Uiso 1 1 calc R U C17 C 0.53069(15) 0.11356(13) 0.35248(10) 0.0623(3) Uani 1 1 d . . H17A H 0.4593 0.0840 0.2961 0.075 Uiso 1 1 calc R U H17B H 0.5556 0.1987 0.3676 0.075 Uiso 1 1 calc R U C18 C 0.45469(14) 0.09846(12) 0.43045(10) 0.0602(3) Uani 1 1 d . . H18A H 0.5293 0.1211 0.4852 0.072 Uiso 1 1 calc R U H18B H 0.4221 0.0140 0.4128 0.072 Uiso 1 1 calc R U C19 C 0.31647(14) 0.17404(12) 0.45440(10) 0.0610(3) Uani 1 1 d . . H19A H 0.3489 0.2587 0.4727 0.073 Uiso 1 1 calc R U H19B H 0.2419 0.1519 0.3997 0.073 Uiso 1 1 calc R U C20 C 0.24112(14) 0.15689(13) 0.53197(10) 0.0615(3) Uani 1 1 d . . H20A H 0.2171 0.0714 0.5160 0.074 Uiso 1 1 calc R U H20B H 0.3129 0.1858 0.5882 0.074 Uiso 1 1 calc R U C21 C 0.10045(14) 0.33558(12) 0.60329(9) 0.0564(3) Uani 1 1 d . . H21 H 0.1936 0.3723 0.6373 0.068 Uiso 1 1 calc R U C22 C -0.02343(14) 0.40799(12) 0.61483(9) 0.0555(3) Uani 1 1 d . . C23 C 0.00657(14) 0.53658(12) 0.68044(9) 0.0566(3) Uani 1 1 d . . C24 C 0.0428(3) 0.62723(16) 0.64976(13) 0.0899(5) Uani 1 1 d . . H24 H 0.0436 0.6088 0.5865 0.108 Uiso 1 1 calc R U C25 C 0.0780(3) 0.74497(18) 0.71142(17) 0.1072(7) Uani 1 1 d . . H25 H 0.1005 0.8048 0.6891 0.129 Uiso 1 1 calc R U C26 C 0.0799(2) 0.77393(15) 0.80430(15) 0.0904(5) Uani 1 1 d . . H26 H 0.1078 0.8524 0.8456 0.108 Uiso 1 1 calc R U C27 C 0.0403(2) 0.68658(16) 0.83638(12) 0.0877(5) Uani 1 1 d . . H27 H 0.0383 0.7060 0.8996 0.105 Uiso 1 1 calc R U C28 C 0.0030(2) 0.56886(14) 0.77442(10) 0.0724(4) Uani 1 1 d . . H28 H -0.0250 0.5104 0.7969 0.087 Uiso 1 1 calc R U C29 C -0.16869(15) 0.36113(13) 0.56202(9) 0.0616(3) Uani 1 1 d . . C30 C -0.29572(17) 0.44658(15) 0.56516(11) 0.0718(4) Uani 1 1 d . . H30A H -0.2507 0.5221 0.5663 0.086 Uiso 1 1 calc R U H30B H -0.3665 0.4117 0.5088 0.086 Uiso 1 1 calc R U C31 C -0.38494(15) 0.47316(14) 0.64773(10) 0.0667(4) Uani 1 1 d . . C32 C -0.4376(2) 0.58673(19) 0.68903(14) 0.0981(6) Uani 1 1 d . . H32 H -0.4127 0.6475 0.6681 0.118 Uiso 1 1 calc R U C33 C -0.5270(3) 0.6110(3) 0.76114(17) 0.1196(8) Uani 1 1 d . . H33 H -0.5636 0.6874 0.7873 0.144 Uiso 1 1 calc R U C34 C -0.5618(2) 0.5247(3) 0.79402(14) 0.1098(8) Uani 1 1 d . . H34 H -0.6219 0.5420 0.8426 0.132 Uiso 1 1 calc R U C35 C -0.5084(2) 0.4119(2) 0.75555(14) 0.0970(6) Uani 1 1 d . . H35 H -0.5308 0.3528 0.7786 0.116 Uiso 1 1 calc R U C36 C -0.42049(17) 0.38613(16) 0.68190(12) 0.0783(4) Uani 1 1 d . . H36 H -0.3854 0.3093 0.6555 0.094 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0559(5) 0.0617(5) 0.0640(5) 0.0093(4) 0.0064(4) 0.0050(4) O2 0.0547(5) 0.0748(6) 0.0836(7) 0.0049(5) 0.0067(5) 0.0052(4) N1 0.0458(5) 0.0613(6) 0.0638(6) 0.0140(5) 0.0114(5) 0.0108(4) N2 0.0469(5) 0.0617(6) 0.0652(6) 0.0132(5) 0.0122(5) 0.0089(4) C1 0.0775(10) 0.0973(12) 0.0919(12) 0.0427(10) 0.0220(9) 0.0115(8) C2 0.1037(15) 0.164(2) 0.1159(18) 0.0800(18) 0.0202(13) -0.0035(15) C3 0.0931(15) 0.207(3) 0.0814(14) 0.0376(18) 0.0265(11) -0.0179(18) C4 0.0924(14) 0.150(2) 0.0911(15) -0.0050(15) 0.0377(12) 0.0040(14) C5 0.0732(10) 0.0874(11) 0.0917(12) 0.0041(9) 0.0246(9) 0.0123(8) C6 0.0461(6) 0.0692(8) 0.0642(8) 0.0124(6) 0.0064(5) 0.0055(5) C7 0.0534(7) 0.0630(7) 0.0717(8) 0.0218(6) 0.0094(6) 0.0126(5) C8 0.0503(6) 0.0524(6) 0.0608(7) 0.0187(5) 0.0130(5) 0.0059(5) C9 0.0508(6) 0.0543(6) 0.0571(7) 0.0146(5) 0.0112(5) 0.0061(5) C10 0.0518(6) 0.0599(7) 0.0594(7) 0.0115(6) 0.0119(5) 0.0031(5) C11 0.0807(9) 0.0620(8) 0.0696(9) 0.0138(7) 0.0149(7) 0.0051(7) C12 0.1056(13) 0.0638(9) 0.0847(12) 0.0046(8) 0.0209(10) 0.0047(8) C13 0.1138(15) 0.0873(12) 0.0702(11) -0.0067(9) 0.0169(10) -0.0020(11) C14 0.1191(16) 0.1062(14) 0.0601(9) 0.0171(9) 0.0049(9) 0.0059(12) C15 0.0873(10) 0.0755(9) 0.0652(9) 0.0179(7) 0.0080(7) 0.0088(8) C16 0.0491(6) 0.0588(7) 0.0590(7) 0.0165(5) 0.0087(5) 0.0035(5) C17 0.0499(6) 0.0666(7) 0.0709(8) 0.0240(6) 0.0137(6) 0.0169(5) C18 0.0475(6) 0.0598(7) 0.0746(8) 0.0243(6) 0.0153(6) 0.0126(5) C19 0.0502(6) 0.0628(7) 0.0721(8) 0.0250(6) 0.0157(6) 0.0154(5) C20 0.0496(6) 0.0651(7) 0.0696(8) 0.0230(6) 0.0139(5) 0.0148(5) C21 0.0507(6) 0.0628(7) 0.0537(6) 0.0182(5) 0.0113(5) 0.0055(5) C22 0.0525(6) 0.0613(7) 0.0522(6) 0.0181(5) 0.0151(5) 0.0103(5) C23 0.0521(6) 0.0606(7) 0.0583(7) 0.0213(5) 0.0148(5) 0.0109(5) C24 0.1230(15) 0.0756(10) 0.0752(10) 0.0296(8) 0.0280(10) -0.0069(10) C25 0.1381(18) 0.0703(10) 0.1162(17) 0.0354(11) 0.0307(14) -0.0104(11) C26 0.0898(11) 0.0605(9) 0.1021(13) 0.0101(9) 0.0069(10) 0.0069(8) C27 0.1054(13) 0.0764(10) 0.0661(9) 0.0081(8) 0.0125(9) 0.0174(9) C28 0.0917(10) 0.0652(8) 0.0593(8) 0.0200(6) 0.0164(7) 0.0120(7) C29 0.0537(7) 0.0703(8) 0.0583(7) 0.0188(6) 0.0149(5) 0.0109(6) C30 0.0599(7) 0.0855(10) 0.0703(9) 0.0290(7) 0.0073(6) 0.0177(7) C31 0.0485(6) 0.0788(9) 0.0637(8) 0.0170(7) 0.0015(5) 0.0182(6) C32 0.1004(13) 0.0985(13) 0.0932(12) 0.0300(10) 0.0170(10) 0.0474(11) C33 0.1133(17) 0.1263(19) 0.1020(16) 0.0165(14) 0.0274(13) 0.0629(15) C34 0.0741(11) 0.159(2) 0.0767(12) 0.0176(13) 0.0183(9) 0.0329(13) C35 0.0661(9) 0.1324(17) 0.0900(12) 0.0378(12) 0.0149(8) 0.0028(10) C36 0.0600(8) 0.0861(10) 0.0821(10) 0.0224(8) 0.0142(7) 0.0084(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C16 N1 C17 124.22(12) C16 N1 H1N 116.3(11) C17 N1 H1N 119.5(11) C21 N2 C20 122.96(12) C21 N2 H2N 116.2(11) C20 N2 H2N 120.2(11) C6 C1 C2 120.9(2) C6 C1 H1 119.5 C2 C1 H1 119.5 C1 C2 C3 119.3(3) C1 C2 H2 120.4 C3 C2 H2 120.4 C4 C3 C2 120.3(2) C4 C3 H3 119.9 C2 C3 H3 119.9 C3 C4 C5 119.9(2) C3 C4 H4 120.0 C5 C4 H4 120.0 C4 C5 C6 121.8(2) C4 C5 H5 119.1 C6 C5 H5 119.1 C1 C6 C5 117.89(17) C1 C6 C7 121.54(13) C5 C6 C7 120.50(15) C6 C7 C8 115.18(11) C6 C7 H7A 108.5 C8 C7 H7A 108.5 C6 C7 H7B 108.5 C8 C7 H7B 108.5 H7A C7 H7B 107.5 O1 C8 C9 121.68(11) O1 C8 C7 117.63(11) C9 C8 C7 120.65(11) C16 C9 C8 120.13(11) C16 C9 C10 116.56(11) C8 C9 C10 123.27(11) C11 C10 C15 117.56(13) C11 C10 C9 122.27(13) C15 C10 C9 120.13(13) C10 C11 C12 121.17(17) C10 C11 H11 119.4 C12 C11 H11 119.4 C13 C12 C11 120.17(18) C13 C12 H12 119.9 C11 C12 H12 119.9 C12 C13 C14 119.81(17) C12 C13 H13 120.1 C14 C13 H13 120.1 C13 C14 C15 120.19(19) C13 C14 H14 119.9 C15 C14 H14 119.9 C14 C15 C10 121.07(17) C14 C15 H15 119.5 C10 C15 H15 119.5 N1 C16 C9 127.34(12) N1 C16 H16 116.3 C9 C16 H16 116.3 N1 C17 C18 111.90(11) N1 C17 H17A 109.2 C18 C17 H17A 109.2 N1 C17 H17B 109.2 C18 C17 H17B 109.2 H17A C17 H17B 107.9 C17 C18 C19 112.98(11) C17 C18 H18A 109.0 C19 C18 H18A 109.0 C17 C18 H18B 109.0 C19 C18 H18B 109.0 H18A C18 H18B 107.8 C20 C19 C18 112.20(11) C20 C19 H19A 109.2 C18 C19 H19A 109.2 C20 C19 H19B 109.2 C18 C19 H19B 109.2 H19A C19 H19B 107.9 N2 C20 C19 112.40(11) N2 C20 H20A 109.1 C19 C20 H20A 109.1 N2 C20 H20B 109.1 C19 C20 H20B 109.1 H20A C20 H20B 107.9 N2 C21 C22 127.20(12) N2 C21 H21 116.4 C22 C21 H21 116.4 C21 C22 C29 120.27(12) C21 C22 C23 116.77(11) C29 C22 C23 122.88(11) C28 C23 C24 117.25(14) C28 C23 C22 121.20(12) C24 C23 C22 121.53(13) C23 C24 C25 121.18(17) C23 C24 H24 119.4 C25 C24 H24 119.4 C26 C25 C24 120.59(18) C26 C25 H25 119.7 C24 C25 H25 119.7 C25 C26 C27 119.42(17) C25 C26 H26 120.3 C27 C26 H26 120.3 C26 C27 C28 119.93(17) C26 C27 H27 120.0 C28 C27 H27 120.0 C23 C28 C27 121.56(15) C23 C28 H28 119.2 C27 C28 H28 119.2 O2 C29 C22 122.50(12) O2 C29 C30 118.23(13) C22 C29 C30 119.26(13) C31 C30 C29 114.02(12) C31 C30 H30A 108.7 C29 C30 H30A 108.7 C31 C30 H30B 108.7 C29 C30 H30B 108.7 H30A C30 H30B 107.6 C36 C31 C32 118.22(16) C36 C31 C30 122.07(14) C32 C31 C30 119.67(16) C31 C32 C33 120.6(2) C31 C32 H32 119.7 C33 C32 H32 119.7 C34 C33 C32 120.7(2) C34 C33 H33 119.7 C32 C33 H33 119.7 C33 C34 C35 119.9(2) C33 C34 H34 120.1 C35 C34 H34 120.1 C34 C35 C36 119.8(2) C34 C35 H35 120.1 C36 C35 H35 120.1 C31 C36 C35 120.78(18) C31 C36 H36 119.6 C35 C36 H36 119.6 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C8 1.2412(15) O2 C29 1.2409(17) N1 C16 1.3195(16) N1 C17 1.4530(15) N1 H1N 0.909(17) N2 C21 1.3156(17) N2 C20 1.4578(15) N2 H2N 0.897(18) C1 C6 1.376(2) C1 C2 1.387(3) C1 H1 0.9300 C2 C3 1.388(4) C2 H2 0.9300 C3 C4 1.352(4) C3 H3 0.9300 C4 C5 1.370(3) C4 H4 0.9300 C5 C6 1.382(2) C5 H5 0.9300 C6 C7 1.506(2) C7 C8 1.5224(17) C7 H7A 0.9700 C7 H7B 0.9700 C8 C9 1.4344(18) C9 C16 1.3857(17) C9 C10 1.4894(17) C10 C11 1.386(2) C10 C15 1.388(2) C11 C12 1.386(2) C11 H11 0.9300 C12 C13 1.365(3) C12 H12 0.9300 C13 C14 1.372(3) C13 H13 0.9300 C14 C15 1.384(2) C14 H14 0.9300 C15 H15 0.9300 C16 H16 0.9300 C17 C18 1.5111(19) C17 H17A 0.9700 C17 H17B 0.9700 C18 C19 1.5203(16) C18 H18A 0.9700 C18 H18B 0.9700 C19 C20 1.5127(19) C19 H19A 0.9700 C19 H19B 0.9700 C20 H20A 0.9700 C20 H20B 0.9700 C21 C22 1.3874(17) C21 H21 0.9300 C22 C29 1.4247(19) C22 C23 1.4958(18) C23 C28 1.3771(19) C23 C24 1.381(2) C24 C25 1.384(3) C24 H24 0.9300 C25 C26 1.360(3) C25 H25 0.9300 C26 C27 1.368(3) C26 H26 0.9300 C27 C28 1.388(2) C27 H27 0.9300 C28 H28 0.9300 C29 C30 1.5195(19) C30 C31 1.512(2) C30 H30A 0.9700 C30 H30B 0.9700 C31 C36 1.377(2) C31 C32 1.381(2) C32 C33 1.383(3) C32 H32 0.9300 C33 C34 1.354(4) C33 H33 0.9300 C34 C35 1.371(3) C34 H34 0.9300 C35 C36 1.392(3) C35 H35 0.9300 C36 H36 0.9300 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N1 H1N O1 0.909(17) 1.973(17) 2.6522(14) 130.2(14) . N1 H1N O2 0.909(17) 2.345(17) 3.0173(16) 130.7(14) 1_655 N2 H2N O1 0.897(18) 2.368(17) 3.0228(15) 129.9(14) 1_455 N2 H2N O2 0.897(18) 2.000(18) 2.6708(15) 130.5(14) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C6 C1 C2 C3 -1.1(3) C1 C2 C3 C4 0.6(4) C2 C3 C4 C5 0.3(4) C3 C4 C5 C6 -0.8(4) C2 C1 C6 C5 0.6(3) C2 C1 C6 C7 177.50(18) C4 C5 C6 C1 0.3(3) C4 C5 C6 C7 -176.60(18) C1 C6 C7 C8 33.52(19) C5 C6 C7 C8 -149.66(14) C6 C7 C8 O1 -112.58(14) C6 C7 C8 C9 65.41(16) O1 C8 C9 C16 0.6(2) C7 C8 C9 C16 -177.28(12) O1 C8 C9 C10 178.03(12) C7 C8 C9 C10 0.13(19) C16 C9 C10 C11 -123.10(15) C8 C9 C10 C11 59.40(19) C16 C9 C10 C15 54.44(18) C8 C9 C10 C15 -123.06(15) C15 C10 C11 C12 1.0(2) C9 C10 C11 C12 178.62(15) C10 C11 C12 C13 -1.9(3) C11 C12 C13 C14 1.2(3) C12 C13 C14 C15 0.3(3) C13 C14 C15 C10 -1.1(3) C11 C10 C15 C14 0.5(2) C9 C10 C15 C14 -177.19(16) C17 N1 C16 C9 179.39(13) C8 C9 C16 N1 -0.7(2) C10 C9 C16 N1 -178.31(13) C16 N1 C17 C18 112.57(15) N1 C17 C18 C19 175.00(11) C17 C18 C19 C20 179.49(12) C21 N2 C20 C19 -84.26(16) C18 C19 C20 N2 -174.90(11) C20 N2 C21 C22 170.92(12) N2 C21 C22 C29 -3.2(2) N2 C21 C22 C23 179.98(12) C21 C22 C23 C28 -84.40(16) C29 C22 C23 C28 98.90(17) C21 C22 C23 C24 93.90(18) C29 C22 C23 C24 -82.81(19) C28 C23 C24 C25 1.6(3) C22 C23 C24 C25 -176.71(18) C23 C24 C25 C26 1.0(4) C24 C25 C26 C27 -2.8(4) C25 C26 C27 C28 1.9(3) C24 C23 C28 C27 -2.5(2) C22 C23 C28 C27 175.84(15) C26 C27 C28 C23 0.8(3) C21 C22 C29 O2 7.6(2) C23 C22 C29 O2 -175.83(13) C21 C22 C29 C30 -171.03(12) C23 C22 C29 C30 5.56(19) O2 C29 C30 C31 98.39(17) C22 C29 C30 C31 -82.95(17) C29 C30 C31 C36 -37.6(2) C29 C30 C31 C32 144.56(16) C36 C31 C32 C33 -1.7(3) C30 C31 C32 C33 176.22(18) C31 C32 C33 C34 1.5(4) C32 C33 C34 C35 -0.1(4) C33 C34 C35 C36 -1.0(3) C32 C31 C36 C35 0.6(2) C30 C31 C36 C35 -177.26(15) C34 C35 C36 C31 0.7(3)