#------------------------------------------------------------------------------ #$Date: 2017-07-12 00:28:33 +0300 (Wed, 12 Jul 2017) $ #$Revision: 198646 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/41/4514162.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4514162 loop_ _publ_author_name 'Reay, Alan J.' 'Hammarback, L. Anders' 'Bray, Joshua T. W.' 'Sheridan, Thomas' 'Turnbull, David' 'Whitwood, Adrian C.' 'Fairlamb, Ian J. S.' _publ_section_title ; Mild and Regioselective Pd(OAc)2-Catalyzed C--H Arylation of Tryptophans by [ArN2]X, Promoted by Tosic Acid ; _journal_name_full 'ACS Catalysis' _journal_page_first 5174 _journal_paper_doi 10.1021/acscatal.6b03121 _journal_year 2017 _chemical_absolute_configuration ad _chemical_formula_moiety 'C23 H26 N2 O3' _chemical_formula_sum 'C23 H26 N2 O3' _chemical_formula_weight 378.46 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2016-12-01 _audit_creation_method ; Olex2 1.2 (compiled 2016.11.30 svn.r3356 for OlexSys, GUI svn.r5269) ; _cell_angle_alpha 90 _cell_angle_beta 100.507(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.7152(3) _cell_length_b 13.5902(4) _cell_length_c 8.7625(3) _cell_measurement_reflns_used 3894 _cell_measurement_temperature 110.05(10) _cell_measurement_theta_max 70.7620 _cell_measurement_theta_min 10.2710 _cell_volume 1020.44(6) _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 110.05(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.1450 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.9990 _diffrn_measured_fraction_theta_max 0.9990 _diffrn_measurement_details ; #__ type_ start__ end____ width___ exp.time_ 1 omega -2.00 25.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 0.0000 57.0000 120.0000 27 #__ type_ start__ end____ width___ exp.time_ 2 omega -58.00 -31.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 0.0000 -57.0000 -90.0000 27 #__ type_ start__ end____ width___ exp.time_ 3 omega -29.00 43.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 0.0000 77.0000 -60.0000 72 #__ type_ start__ end____ width___ exp.time_ 4 omega -22.00 19.00 1.0000 1.0000 omega____ theta____ kappa____ phi______ frames - 0.0000 -57.0000 -90.0000 41 #__ type_ start__ end____ width___ exp.time_ 5 omega -15.00 78.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 -19.0000 -120.0000 93 #__ type_ start__ end____ width___ exp.time_ 6 omega 20.00 127.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 19.0000 -30.0000 107 #__ type_ start__ end____ width___ exp.time_ 7 omega -8.00 82.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 -77.0000 90.0000 90 #__ type_ start__ end____ width___ exp.time_ 8 omega -17.00 40.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 -37.0000 0.0000 57 #__ type_ start__ end____ width___ exp.time_ 9 omega 25.00 51.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 -125.0000 -90.0000 26 #__ type_ start__ end____ width___ exp.time_ 10 omega 69.00 96.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 -125.0000 -90.0000 27 #__ type_ start__ end____ width___ exp.time_ 11 omega 38.00 124.00 1.0000 4.0000 omega____ theta____ kappa____ phi______ frames - 54.0000 77.0000 30.0000 86 #__ type_ start__ end____ width___ exp.time_ 12 omega 66.00 111.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -111.0000 150.0000 45 #__ type_ start__ end____ width___ exp.time_ 13 omega 72.00 107.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -111.0000 60.0000 35 #__ type_ start__ end____ width___ exp.time_ 14 omega 44.00 94.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -25.0000 -120.0000 50 #__ type_ start__ end____ width___ exp.time_ 15 omega 87.00 119.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 50.0000 -120.0000 32 #__ type_ start__ end____ width___ exp.time_ 16 omega 50.00 78.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -50.0000 -120.0000 28 #__ type_ start__ end____ width___ exp.time_ 17 omega 120.00 175.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 111.0000 -150.0000 55 #__ type_ start__ end____ width___ exp.time_ 18 omega 35.00 89.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -25.0000 -60.0000 54 #__ type_ start__ end____ width___ exp.time_ 19 omega 45.00 77.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -37.0000 -180.0000 32 #__ type_ start__ end____ width___ exp.time_ 20 omega 89.00 174.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 50.0000 -150.0000 85 #__ type_ start__ end____ width___ exp.time_ 21 omega 42.00 103.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -50.0000 60.0000 61 #__ type_ start__ end____ width___ exp.time_ 22 omega 141.00 177.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 50.0000 60.0000 36 #__ type_ start__ end____ width___ exp.time_ 23 omega 144.00 174.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 63.0000 -90.0000 30 #__ type_ start__ end____ width___ exp.time_ 24 omega 90.00 134.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 50.0000 60.0000 44 #__ type_ start__ end____ width___ exp.time_ 25 omega 86.00 115.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -111.0000 -90.0000 29 #__ type_ start__ end____ width___ exp.time_ 26 omega 42.00 127.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 -63.0000 -60.0000 85 #__ type_ start__ end____ width___ exp.time_ 27 omega 99.00 177.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 37.0000 -90.0000 78 #__ type_ start__ end____ width___ exp.time_ 28 omega 114.00 141.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 63.0000 -90.0000 27 #__ type_ start__ end____ width___ exp.time_ 29 omega 36.00 170.00 1.0000 16.0000 omega____ theta____ kappa____ phi______ frames - 108.0000 12.0000 -180.0000 134 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_UB_11 0.0727338000 _diffrn_orient_matrix_UB_12 -0.0259487000 _diffrn_orient_matrix_UB_13 0.1689623000 _diffrn_orient_matrix_UB_21 0.0635651000 _diffrn_orient_matrix_UB_22 -0.0967750000 _diffrn_orient_matrix_UB_23 -0.0556658000 _diffrn_orient_matrix_UB_31 0.1515490000 _diffrn_orient_matrix_UB_32 0.0530049000 _diffrn_orient_matrix_UB_33 -0.0189676000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0256 _diffrn_reflns_av_unetI/netI 0.0341 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 6691 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 67.058 _diffrn_reflns_theta_max 67.058 _diffrn_reflns_theta_min 5.134 _diffrn_source 'sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.655 _exptl_absorpt_correction_T_max 0.980 _exptl_absorpt_correction_T_min 0.940 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.232 _exptl_crystal_description needle _exptl_crystal_F_000 404 _exptl_crystal_size_max 0.2485 _exptl_crystal_size_mid 0.1431 _exptl_crystal_size_min 0.0656 _refine_diff_density_max 0.209 _refine_diff_density_min -0.176 _refine_diff_density_rms 0.039 _refine_ls_abs_structure_details ; Flack x determined using 1605 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.09(12) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 266 _refine_ls_number_reflns 3634 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0359 _refine_ls_R_factor_gt 0.0342 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0608P)^2^+0.0666P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0893 _refine_ls_wR_factor_ref 0.0912 _reflns_Friedel_coverage 0.911 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 3483 _reflns_number_total 3634 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs6b03121_si_002.cif _cod_data_source_block ijsf1488 _cod_database_code 4514162 _chemical_oxdiff_formula 'C23 H26 N2 O3' _chemical_oxdiff_usercomment 'Alan AJR-5-402' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.90 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C10(H10) 2.b Secondary CH2 refined with riding coordinates: C9(H9A,H9B) 2.c Aromatic/amide H refined with riding coordinates: C2(H2A), C3(H3), C4(H4), C5(H5), C14(H14), C16(H16) 2.d Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C20(H20A,H20B,H20C), C21(H21A,H21B, H21C), C23(H23A,H23B,H23C) ; _shelx_res_file ; ijsf1488.res created by SHELXL-2014/7 TITL ijsf1488 in P21 #4 REM reset to P21 #4 CELL 1.54184 8.715158 13.590209 8.762498 90 100.5067 90 ZERR 2 0.000279 0.000402 0.0003 0 0.0032 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 46 52 4 6 EQIV $1 2-X,-0.5+Y,1-Z L.S. 8 PLAN 20 HTAB N1 O3_$1 HTAB N2 O2 BOND MORE -1 BOND $H CONF fmap 2 acta REM REM REM WGHT 0.060800 0.066600 FVAR 9.49454 O1 4 0.891515 0.493779 0.091115 11.00000 0.03348 0.02594 = 0.03109 0.00543 0.00806 0.00117 O2 4 0.741363 0.358490 0.080680 11.00000 0.03365 0.03327 = 0.03273 -0.00592 0.00765 -0.00620 O3 4 0.699913 0.489842 0.583592 11.00000 0.03126 0.02030 = 0.03027 -0.00466 0.00744 -0.00436 N1 3 1.134817 0.170333 0.362639 11.00000 0.02300 0.01517 = 0.03381 0.00023 0.00502 0.00211 N2 3 0.694881 0.391384 0.376272 11.00000 0.02067 0.01510 = 0.03011 -0.00229 0.00391 -0.00072 C1 1 1.217899 0.222266 0.271353 11.00000 0.01771 0.01911 = 0.02794 -0.00221 0.00152 -0.00042 C2 1 1.335539 0.191647 0.192725 11.00000 0.02093 0.02117 = 0.03208 -0.00368 0.00315 0.00187 AFIX 43 H2A 2 1.367730 0.126332 0.195150 11.00000 -1.20000 AFIX 0 C3 1 1.402091 0.261778 0.111469 11.00000 0.02247 0.02941 = 0.02971 -0.00716 0.00577 -0.00164 AFIX 43 H3 2 1.480773 0.243437 0.058399 11.00000 -1.20000 AFIX 0 C4 1 1.353133 0.360587 0.107381 11.00000 0.02355 0.02463 = 0.03033 -0.00133 0.00479 -0.00496 AFIX 43 H4 2 1.399358 0.406145 0.050739 11.00000 -1.20000 AFIX 0 C5 1 1.237993 0.391204 0.185682 11.00000 0.02329 0.01909 = 0.03181 -0.00086 0.00314 -0.00177 AFIX 43 H5 2 1.206494 0.456679 0.181854 11.00000 -1.20000 AFIX 0 C6 1 1.168938 0.321942 0.271388 11.00000 0.01648 0.01780 = 0.02956 -0.00273 0.00016 -0.00141 C7 1 1.055596 0.327215 0.370659 11.00000 0.01665 0.01853 = 0.02708 -0.00203 0.00059 -0.00049 C8 1 1.037572 0.233204 0.423775 11.00000 0.01801 0.01751 = 0.02684 -0.00247 0.00088 0.00096 C9 1 0.982379 0.421132 0.414187 11.00000 0.02138 0.01568 = 0.02912 -0.00264 0.00382 -0.00108 AFIX 23 H9A 2 1.051590 0.475210 0.401468 11.00000 -1.20000 H9B 2 0.976115 0.417701 0.523453 11.00000 -1.20000 AFIX 0 C10 1 0.817356 0.445911 0.321730 11.00000 0.02289 0.01511 = 0.03103 -0.00017 0.00621 0.00090 AFIX 13 H10 2 0.798438 0.516212 0.334958 11.00000 -1.20000 AFIX 0 C11 1 0.809258 0.426561 0.151516 11.00000 0.01827 0.02262 = 0.03157 0.00179 0.00378 0.00475 C12 1 0.927449 0.196968 0.521566 11.00000 0.02098 0.01335 = 0.03104 0.00154 0.00433 0.00439 C13 1 0.790976 0.147758 0.450680 11.00000 0.02325 0.01363 = 0.03251 0.00172 0.00565 0.00366 C14 1 0.679568 0.123315 0.538856 11.00000 0.02456 0.01289 = 0.03883 0.00149 0.00670 0.00025 AFIX 43 H14 2 0.588662 0.091587 0.491711 11.00000 -1.20000 AFIX 0 C15 1 0.701030 0.145290 0.696380 11.00000 0.03151 0.01548 = 0.03820 0.00401 0.01255 0.00643 C16 1 0.839689 0.189120 0.766555 11.00000 0.03907 0.02152 = 0.02584 0.00232 0.00735 0.00719 AFIX 43 H16 2 0.856630 0.201662 0.872640 11.00000 -1.20000 AFIX 0 C17 1 0.954513 0.214865 0.681513 11.00000 0.02772 0.01799 = 0.03059 0.00005 0.00206 0.00562 C18 1 0.764689 0.121219 0.280463 11.00000 0.02379 0.02512 = 0.03355 -0.00314 0.00409 -0.00198 AFIX 137 H18A 2 0.785259 0.177570 0.221267 11.00000 -1.50000 H18B 2 0.658480 0.100628 0.247225 11.00000 -1.50000 H18C 2 0.833625 0.068594 0.264738 11.00000 -1.50000 AFIX 0 C19 1 0.573216 0.123088 0.786925 11.00000 0.04056 0.02861 = 0.04821 0.00349 0.02269 0.00523 AFIX 137 H19A 2 0.498022 0.175449 0.772437 11.00000 -1.50000 H19B 2 0.617489 0.117276 0.895191 11.00000 -1.50000 H19C 2 0.522940 0.062435 0.750669 11.00000 -1.50000 AFIX 0 C20 1 1.105650 0.259241 0.762643 11.00000 0.03516 0.03294 = 0.03363 -0.00411 0.00042 0.00075 AFIX 137 H20A 2 1.191518 0.222874 0.736141 11.00000 -1.50000 H20B 2 1.110254 0.256683 0.872871 11.00000 -1.50000 H20C 2 1.111637 0.326486 0.730695 11.00000 -1.50000 AFIX 0 C21 1 0.906458 0.478508 -0.068575 11.00000 0.04055 0.04064 = 0.03266 0.00949 0.01225 0.00807 AFIX 137 H21A 2 0.804621 0.472070 -0.131601 11.00000 -1.50000 H21B 2 0.965389 0.419634 -0.076437 11.00000 -1.50000 H21C 2 0.959301 0.533667 -0.103869 11.00000 -1.50000 AFIX 0 C22 1 0.642577 0.418835 0.504007 11.00000 0.02123 0.01453 = 0.02754 0.00134 0.00219 0.00273 C23 1 0.509854 0.361845 0.547953 11.00000 0.02584 0.02038 = 0.03384 0.00164 0.00671 -0.00014 AFIX 137 H23A 2 0.535322 0.343747 0.655503 11.00000 -1.50000 H23B 2 0.491837 0.303531 0.485416 11.00000 -1.50000 H23C 2 0.417434 0.401770 0.531074 11.00000 -1.50000 AFIX 0 H2 2 0.651252 0.346904 0.319732 11.00000 0.04001 H1 2 1.155451 0.115448 0.394004 11.00000 0.03413 HKLF 4 REM ijsf1488 in P21 #4 REM R1 = 0.0342 for 3483 Fo > 4sig(Fo) and 0.0359 for all 3634 data REM 266 parameters refined using 1 restraints END WGHT 0.0608 0.0666 REM Highest difference peak 0.209, deepest hole -0.176, 1-sigma level 0.039 Q1 1 0.6058 0.4176 0.3829 11.00000 0.05 0.21 Q2 1 0.9694 0.1962 0.6127 11.00000 0.05 0.19 Q3 1 0.9209 0.2186 0.5908 11.00000 0.05 0.19 Q4 1 0.8913 0.4333 0.3706 11.00000 0.05 0.18 Q5 1 1.0639 0.3241 0.2653 11.00000 0.05 0.17 Q6 1 0.7105 0.1204 0.6247 11.00000 0.05 0.17 Q7 1 0.7327 0.3866 0.4753 11.00000 0.05 0.17 Q8 1 0.7246 0.4867 0.7014 11.00000 0.05 0.16 Q9 1 0.7971 0.1317 0.3722 11.00000 0.05 0.16 Q10 1 0.8291 0.4356 0.2459 11.00000 0.05 0.16 Q11 1 0.7935 0.1464 0.7363 11.00000 0.05 0.15 Q12 1 0.6417 0.1285 0.7496 11.00000 0.05 0.15 Q13 1 0.8617 0.1632 0.4882 11.00000 0.05 0.15 Q14 1 1.3260 0.2079 0.3026 11.00000 0.05 0.15 Q15 1 0.8354 0.4910 -0.0124 11.00000 0.05 0.14 Q16 1 0.6415 0.3560 0.0132 11.00000 0.05 0.13 Q17 1 0.7547 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14 -2 688.508 120.510 19 -2 14 2 809.144 138.926 22 -2 14 1 13526.1 505.093 19 2 14 -1 13390.4 503.619 19 2 14 0 96.3037 88.3633 19 -2 14 0 128.268 90.5907 19 -2 14 -1 6722.62 340.932 19 -2 14 -2 2723.31 214.884 19 2 14 2 2367.91 183.895 22 -2 14 -3 6631.21 324.907 19 2 14 3 7529.93 337.084 16 -2 14 -4 2280.14 170.665 19 2 14 4 2507.46 175.430 16 2 15 -3 437.585 83.2412 19 -2 15 3 442.614 94.5474 22 2 15 -2 3869.45 216.232 19 -2 15 2 3644.78 217.258 22 -2 15 1 5216.81 262.198 19 2 15 -1 5320.01 261.457 19 -2 15 1 4682.15 250.345 22 -2 15 0 928.123 121.840 19 -2 15 0 700.959 99.7091 22 -2 15 -1 966.441 118.719 19 -2 15 -2 1797.76 147.237 19 -2 15 -3 1474.52 123.546 19 2 15 3 1926.87 141.453 16 3 -15 -3 8240.05 290.847 27 3 -15 -2 1420.05 122.956 27 3 -15 -1 3453.24 185.712 27 3 -15 0 1149.66 110.434 27 3 -15 1 2078.96 139.094 27 3 -15 2 46.7438 50.5034 27 3 -14 -4 451.843 80.8903 28 3 -14 -4 556.365 89.1375 27 3 -14 -3 4150.00 226.021 27 3 -14 -2 8220.13 335.284 27 3 -14 -1 4356.33 242.422 27 3 -14 0 8226.76 342.587 27 3 -14 1 13401.6 465.526 15 3 -14 1 12499.9 430.999 20 3 -14 2 8805.74 347.506 15 3 -14 2 8147.21 324.454 20 3 -14 3 3755.30 199.060 15 3 -14 3 3554.00 191.375 20 3 -13 -5 6377.33 263.717 28 3 -13 -5 6231.98 274.463 27 3 -13 -4 2370.43 184.800 27 3 -13 -3 14138.7 497.438 27 3 -13 -2 7419.68 347.961 27 3 -13 -1 10550.6 430.589 27 3 -13 0 1217.26 157.001 15 3 -13 0 1198.97 137.471 20 3 -13 1 23257.5 704.746 15 3 -13 1 20796.9 661.032 20 3 -13 2 11180.9 438.197 15 3 -13 2 10437.9 419.912 20 3 -13 3 4894.72 262.596 15 3 -13 3 4637.99 252.090 20 3 -13 4 39.2442 67.6832 20 3 -13 4 73.1451 60.4398 15 3 -12 -6 3984.38 204.776 28 3 -12 -6 3678.48 209.848 27 3 -12 -5 3076.75 214.499 27 3 -12 -5 3024.19 200.436 28 3 -12 -4 4972.81 281.613 27 3 -12 -3 7242.82 344.909 27 3 -12 -2 10548.1 431.243 27 3 -12 -1 32300.6 939.428 15 3 -12 0 3041.94 222.902 20 3 -12 0 3037.99 236.635 15 3 -12 1 729.675 126.352 20 3 -12 1 697.354 134.111 15 3 -12 2 4640.43 288.965 15 3 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279.111 28 3 -10 -6 5035.13 285.250 27 3 -10 -5 2864.54 222.519 27 3 -10 -4 1510.86 343.768 6 3 -10 -4 1615.65 179.834 27 3 -10 -3 23760.9 1261.30 6 3 -10 -3 22331.1 709.646 27 3 -10 -2 6163.29 315.326 27 3 -10 -2 6955.00 660.893 6 3 -10 -2 6023.60 317.446 20 3 -10 -1 33010.0 936.116 15 3 -10 -1 32101.1 918.292 20 3 -10 0 12003.8 482.618 15 3 -10 0 12232.7 920.605 6 3 -10 0 11698.3 466.229 20 3 -10 1 42099.8 1139.71 20 3 -10 1 43024.0 1151.25 15 3 -10 1 41996.9 1887.07 6 3 -10 2 27408.6 837.682 20 3 -10 2 23993.6 865.904 18 3 -10 2 27631.5 1496.11 6 3 -10 2 26183.2 817.730 15 3 -10 3 11490.0 501.501 15 3 -10 3 13615.4 533.097 20 3 -10 4 4641.69 301.397 20 3 -10 4 3880.21 267.817 15 3 -10 5 4030.61 264.982 20 3 -10 5 3051.41 216.804 15 3 -10 6 643.048 115.252 20 3 -9 -8 1044.09 125.372 27 3 -9 -7 1892.43 181.130 27 3 -9 -7 2145.78 182.990 28 3 -9 -6 2086.95 189.214 28 3 -9 -6 1825.63 183.690 27 3 -9 -5 1724.86 182.660 27 3 -9 -5 1732.12 348.045 6 3 -9 -4 1126.08 141.176 27 3 -9 -4 1342.23 303.234 6 3 -9 -3 26621.0 1311.65 6 3 -9 -3 25129.5 753.264 27 3 -9 -3 24647.6 1317.04 7 3 -9 -2 2374.76 379.484 6 3 -9 -1 25320.1 1268.51 6 3 -9 0 34203.4 1562.85 6 3 -9 1 11544.2 805.842 8 3 -9 1 11348.3 878.739 6 3 -9 2 11564.1 530.281 18 3 -9 2 11654.6 488.541 20 3 -9 2 10558.3 461.952 15 3 -9 3 4471.44 293.950 20 3 -9 3 3956.57 299.743 18 3 -9 3 4576.52 301.857 29 3 -9 4 13805.4 554.221 20 3 -9 4 13247.3 548.869 29 3 -9 5 7220.45 377.998 20 3 -9 5 7023.37 382.513 29 3 -9 6 8204.78 376.313 20 3 -9 6 8502.65 394.450 29 3 -9 7 1053.76 117.294 20 3 -9 7 995.136 127.794 29 3 -8 -9 301.040 78.4219 27 3 -8 -9 293.517 71.4367 23 3 -8 -8 3132.82 198.761 28 3 -8 -8 2978.01 208.433 27 3 -8 -7 1680.19 173.149 28 3 -8 -7 1694.51 182.381 27 3 -8 -6 1329.38 155.300 28 3 -8 -6 1250.21 155.903 27 3 -8 -5 4168.68 498.364 6 3 -8 -5 3720.92 252.774 27 3 -8 -4 1755.16 322.965 6 3 -8 -4 1501.06 155.007 27 3 -8 -3 5712.20 565.374 6 3 -8 -3 5792.58 598.284 7 3 -8 -2 1868.01 316.864 6 3 -8 -1 9338.37 711.238 6 3 -8 0 20420.0 1061.85 8 3 -8 0 20160.4 1099.72 6 3 -8 1 1535.95 287.800 8 3 -8 2 9129.35 741.412 8 3 -8 3 3320.45 252.107 20 3 -8 3 3196.18 261.260 18 3 -8 3 3107.45 251.468 29 3 -8 3 2860.05 441.544 8 3 -8 4 15621.5 596.791 20 3 -8 4 14130.4 596.620 18 3 -8 4 14311.9 1033.72 8 3 -8 4 16096.6 611.953 29 3 -8 5 3830.62 277.876 20 3 -8 5 3915.66 289.711 18 3 -8 5 4004.71 293.478 29 3 -8 6 151.886 95.2596 20 3 -8 6 86.9752 107.734 29 3 -8 7 4569.10 248.245 20 3 -8 7 4609.63 270.848 29 3 -7 -9 2012.79 157.490 27 3 -7 -9 1942.34 149.489 23 3 -7 -8 3445.30 235.014 27 3 -7 -7 14660.7 542.794 27 3 -7 -7 14887.3 522.241 28 3 -7 -6 3154.69 429.198 6 3 -7 -6 3845.03 258.109 27 3 -7 -6 3696.12 242.030 28 3 -7 -5 23539.9 1184.67 6 3 -7 -5 23410.5 715.864 27 3 -7 -4 437.753 193.522 7 3 -7 -4 740.918 213.688 6 3 -7 -3 12264.0 771.281 6 3 -7 -3 12213.7 834.504 7 3 -7 -2 47841.2 1658.84 6 3 -7 -1 9693.07 683.991 6 3 -7 0 23438.0 1147.68 6 3 -7 0 24931.9 1132.42 8 3 -7 1 29072.0 1295.37 8 3 -7 2 13824.3 907.410 8 3 -7 3 3617.26 495.875 8 3 -7 4 11365.2 483.027 20 3 -7 4 11122.8 501.744 18 3 -7 4 10458.4 881.186 8 3 -7 4 11053.1 491.049 29 3 -7 5 16785.1 637.208 20 3 -7 5 15548.2 633.053 18 3 -7 5 16907.6 640.244 29 3 -7 5 15696.5 1127.45 8 3 -7 6 11704.7 490.568 20 3 -7 6 11119.2 496.994 18 3 -7 6 11622.2 511.781 29 3 -7 7 2188.37 179.497 20 3 -7 7 2401.61 213.317 29 3 -7 8 2944.47 191.285 29 3 -6 -9 1774.36 161.938 27 3 -6 -9 2121.14 160.799 23 3 -6 -8 7872.99 372.181 27 3 -6 -7 4348.44 259.987 28 3 -6 -7 4344.41 278.365 27 3 -6 -6 13404.7 875.118 6 3 -6 -6 14691.7 513.209 28 3 -6 -6 14572.3 532.396 27 3 -6 -5 2771.46 389.727 6 3 -6 -4 7365.20 579.191 6 3 -6 -4 7261.39 627.559 7 3 -6 -3 38564.0 1398.20 6 3 -6 -3 38743.5 1523.74 7 3 -6 -2 40546.7 1426.66 6 3 -6 -1 36538.8 1364.58 8 3 -6 -1 35025.3 1330.59 6 3 -6 0 23239.3 1068.31 8 3 -6 1 21005.1 1040.91 8 3 -6 2 3655.30 455.012 8 3 -6 3 8207.58 719.213 8 3 -6 4 10264.5 859.445 8 3 -6 5 563.398 127.295 20 3 -6 5 796.507 153.149 29 3 -6 5 655.035 141.149 18 3 -6 5 588.924 276.172 8 3 -6 6 1596.69 182.679 20 3 -6 6 1747.77 205.828 18 3 -6 6 1628.87 204.032 29 3 -6 7 340.743 95.9290 20 3 -6 7 385.930 118.378 18 3 -6 7 373.296 125.425 29 3 -6 8 497.986 110.885 29 3 -5 -9 7835.06 351.238 27 3 -5 -9 7813.41 331.152 23 3 -5 -8 576.614 126.828 27 3 -5 -7 2765.75 211.944 28 3 -5 -7 2948.54 228.868 27 3 -5 -6 4321.86 472.267 6 3 -5 -6 4833.93 260.280 28 3 -5 -6 4784.99 270.915 27 3 -5 -6 4431.81 280.600 21 3 -5 -5 14576.0 830.862 6 3 -5 -4 2788.22 331.824 6 3 -5 -4 2614.44 368.616 7 3 -5 -3 25264.3 1003.93 6 3 -5 -3 25349.4 1139.59 7 3 -5 -2 22896.3 917.993 6 3 -5 -1 11804.4 685.344 8 3 -5 -1 10659.7 617.319 6 3 -5 0 41874.0 1471.77 8 3 -5 1 133969. 3484.09 8 3 -5 2 21427.8 1085.61 8 3 -5 3 30238.0 1418.89 8 3 -5 4 38995.2 1766.17 8 3 -5 5 33378.8 974.399 20 3 -5 5 33278.3 1026.39 18 3 -5 5 30768.9 1662.11 8 3 -5 5 34962.2 1014.27 29 3 -5 6 2039.94 198.664 20 3 -5 6 2149.32 220.742 18 3 -5 6 2133.20 221.671 29 3 -5 7 10190.3 472.196 18 3 -5 7 10662.8 480.016 29 3 -5 8 1465.44 152.326 18 3 -5 8 1537.90 169.372 29 3 -4 -10 4449.40 203.385 23 3 -4 -9 134.059 96.9984 27 3 -4 -9 71.6563 88.6115 23 3 -4 -8 5655.49 313.433 27 3 -4 -8 4752.03 298.949 23 3 -4 -7 42663.3 1108.60 28 3 -4 -7 45637.9 1159.43 27 3 -4 -7 42115.0 1172.56 21 3 -4 -7 40452.3 1658.47 6 3 -4 -6 1683.43 303.477 6 3 -4 -5 1340.70 243.159 6 3 -4 -5 1201.60 266.637 7 3 -4 -4 7321.39 499.896 6 3 -4 -4 6795.96 556.863 7 3 -4 -3 8831.26 510.433 6 3 -4 -3 9112.81 610.091 7 3 -4 -2 1136.92 232.084 7 3 -4 -2 1129.32 184.186 6 3 -4 -1 142674. 3393.62 8 3 -4 -1 134373. 3212.96 6 3 -4 0 8926.89 579.717 8 3 -4 1 27773.4 1143.67 8 3 -4 2 18862.9 976.831 8 3 -4 3 1151.86 298.158 8 3 -4 4 12629.9 931.637 8 -3 -4 -4 11553.1 702.843 6 3 -4 5 27735.2 1541.81 8 3 -4 5 26957.0 876.193 18 -3 -4 -5 25547.8 1209.27 6 3 -4 5 28456.6 866.275 29 3 -4 6 69.2895 92.3752 18 3 -4 6 181.895 118.558 29 3 -4 7 809.740 151.792 18 3 -4 7 1234.68 182.218 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14633.3 976.118 5 -3 6 6 14780.1 589.243 29 3 6 -6 13974.8 560.780 21 -3 6 5 3057.81 438.173 5 -3 6 4 8209.35 674.598 5 -3 6 3 39560.8 1537.61 5 -3 6 2 40162.6 1376.71 11 -3 6 1 35870.7 1287.95 11 -3 6 0 22507.5 984.344 11 3 6 1 19319.2 930.227 10 -3 6 -1 19540.1 940.034 11 -3 6 -2 3586.90 400.658 11 3 6 3 7345.10 625.324 5 -3 6 -3 8100.01 626.850 11 -3 6 -4 10085.3 728.925 11 3 6 4 10029.5 805.856 5 3 6 5 444.572 129.692 16 3 6 5 634.129 144.996 14 3 6 6 1500.09 209.182 14 3 6 6 1555.89 193.751 16 3 6 7 274.791 141.616 14 3 6 8 539.404 105.829 26 3 6 8 469.543 138.087 14 -3 7 9 2191.24 181.300 29 -3 7 8 3234.03 259.185 29 -3 7 7 15392.6 616.401 29 -3 7 6 3455.23 273.602 29 3 7 -6 3386.29 256.138 21 -3 7 6 3207.93 477.309 5 -3 7 5 24096.4 1314.57 5 -3 7 5 23695.2 784.323 29 -3 7 4 538.790 226.616 5 -3 7 3 12063.1 840.791 5 -3 7 2 44800.5 1576.21 11 -3 7 1 9816.06 658.436 11 -3 7 0 24703.5 1115.97 11 3 7 1 27098.3 1191.53 10 -3 7 -1 28089.4 1219.20 11 -3 7 -2 13716.5 838.403 11 3 7 3 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335.289 20 4 -14 1 13257.6 429.072 27 4 -14 1 15336.5 468.787 20 4 -14 2 169.524 69.1440 20 4 -14 2 67.1546 51.1823 27 4 -13 -5 383.826 70.8633 28 4 -13 -5 305.913 76.4079 27 4 -13 -4 4345.64 207.346 28 4 -13 -4 4707.71 236.569 27 4 -13 -3 8519.15 343.617 27 4 -13 -2 16109.5 524.340 27 4 -13 -1 7868.42 334.174 27 4 -13 -1 7231.36 341.766 20 4 -13 0 1490.79 147.428 27 4 -13 0 1886.17 168.834 20 4 -13 1 8965.37 375.572 15 4 -13 1 8569.16 365.673 20 4 -13 2 42192.7 1059.77 15 4 -13 2 42632.2 1071.96 20 4 -13 3 160.573 82.8117 20 4 -13 3 179.798 70.0334 15 4 -12 -6 3648.04 183.241 28 4 -12 -6 3612.34 196.331 27 4 -12 -5 10241.4 385.944 27 4 -12 -5 10131.8 356.510 28 4 -12 -4 6381.91 307.464 27 4 -12 -3 298.241 99.0385 27 4 -12 -2 12209.4 460.524 27 4 -12 -2 11102.5 463.580 20 4 -12 -1 2051.09 181.122 27 4 -12 -1 2057.54 194.073 20 4 -12 0 15083.0 547.175 15 4 -12 0 13836.6 526.960 20 4 -12 1 950.486 145.915 20 4 -12 1 885.527 134.303 15 4 -12 2 643.572 127.188 20 4 -12 2 654.430 119.571 15 4 -12 3 7393.19 320.006 15 4 -12 3 7247.36 341.964 20 4 -12 4 917.149 118.704 20 4 -12 4 733.062 94.1237 15 4 -11 -7 1909.99 129.766 28 4 -11 -7 1909.44 143.502 27 4 -11 -6 1562.05 142.179 28 4 -11 -6 1575.72 150.740 27 4 -11 -5 3689.95 219.856 28 4 -11 -5 3726.37 241.113 27 4 -11 -4 1069.52 145.354 27 4 -11 -3 6837.37 335.805 27 4 -11 -3 6082.69 334.177 20 4 -11 -2 24854.1 745.513 27 4 -11 -2 23992.6 768.894 20 4 -11 -1 1872.43 176.837 27 4 -11 -1 1863.80 191.424 20 4 -11 0 31664.3 908.037 15 4 -11 0 29514.0 896.913 20 4 -11 1 20071.8 673.958 15 4 -11 1 19965.5 675.910 20 4 -11 2 2561.44 212.115 15 4 -11 2 2820.15 227.786 20 4 -11 3 2258.61 206.790 20 4 -11 3 1789.98 171.811 15 4 -11 4 18471.4 607.855 20 4 -11 5 1358.49 141.565 20 4 -10 -7 3543.05 197.144 28 4 -10 -7 3607.61 212.739 27 4 -10 -6 8122.01 336.981 28 4 -10 -6 8174.47 360.908 27 4 -10 -5 9291.09 379.431 28 4 -10 -5 9309.13 402.764 27 4 -10 -4 9893.19 411.042 27 4 -10 -4 8764.03 412.991 20 4 -10 -3 21618.5 1166.90 6 4 -10 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23252.4 701.580 28 4 -8 -5 24251.6 738.717 27 4 -8 -4 2977.26 218.004 27 4 -8 -4 2589.27 230.938 20 4 -8 -3 19798.4 1055.30 6 4 -8 -3 19336.5 612.300 27 4 -8 -3 18361.5 1155.96 7 4 -8 -3 18892.7 653.502 20 4 -8 -2 18949.0 1013.15 6 4 -8 -2 18523.4 1150.40 7 4 -8 -1 30439.1 1355.20 6 4 -8 0 10892.2 812.051 8 4 -8 0 10823.4 806.898 6 4 -8 1 13863.0 947.689 8 4 -8 1 12494.8 914.249 6 4 -8 2 11295.4 468.436 20 4 -8 2 10188.7 516.365 18 4 -8 2 10925.0 868.878 8 4 -8 3 3903.17 273.466 20 4 -8 3 3806.27 300.811 18 4 -8 3 3861.83 282.591 29 4 -8 3 3209.42 489.915 8 4 -8 4 6138.41 350.091 20 4 -8 4 5867.31 379.827 18 4 -8 4 6085.71 366.470 29 4 -8 5 6703.07 346.556 20 4 -8 5 7227.30 387.003 29 4 -8 5 6219.16 373.557 18 4 -8 6 10809.4 411.694 20 4 -8 6 10063.3 446.417 18 4 -8 6 10564.1 451.778 29 4 -8 7 922.744 118.826 29 4 -7 -9 18.1579 62.1733 27 4 -7 -9 139.562 71.5740 23 4 -7 -8 3443.13 228.602 27 4 -7 -7 1355.54 166.041 27 4 -7 -7 1502.35 164.992 28 4 -7 -6 9232.39 390.008 28 4 -7 -6 9251.69 407.102 27 4 -7 -6 9032.55 428.948 21 4 -7 -5 2265.60 180.334 28 4 -7 -5 2181.81 194.583 27 4 -7 -4 16440.9 546.377 27 4 -7 -4 16784.4 1061.43 7 4 -7 -3 1587.71 337.431 7 4 -7 -3 1870.22 305.198 6 4 -7 -2 7112.14 559.878 6 4 -7 -2 6977.81 673.834 7 4 -7 -1 12693.1 781.784 6 4 -7 0 13666.6 891.224 8 4 -7 0 13391.6 842.618 6 4 -7 1 28404.3 1386.83 8 4 -7 2 5381.19 613.213 8 4 -7 3 5789.11 325.736 20 4 -7 3 5779.42 361.834 18 4 -7 3 5546.58 649.661 8 4 -7 3 5867.00 347.190 29 4 -7 4 5239.33 325.451 20 4 -7 4 5596.03 366.808 18 4 -7 4 5447.30 681.374 8 4 -7 4 5795.03 361.886 29 4 -7 5 904.888 147.372 20 4 -7 5 861.517 159.307 18 4 -7 5 783.662 159.500 29 4 -7 6 2131.83 182.144 20 4 -7 6 2226.80 218.638 18 4 -7 6 2783.62 238.802 29 4 -7 7 2861.00 207.340 18 4 -7 7 2967.13 215.135 29 4 -6 -9 622.984 106.884 27 4 -6 -9 636.467 106.918 23 4 -6 -8 4598.99 277.703 27 4 -6 -7 2326.19 198.468 28 4 -6 -7 2216.06 200.213 27 4 -6 -7 2291.81 207.394 21 4 -6 -6 6210.10 309.051 28 4 -6 -6 6278.23 324.024 27 4 -6 -6 5907.41 343.299 21 4 -6 -5 1609.46 151.356 28 4 -6 -5 1600.18 158.048 27 4 -6 -5 1391.29 341.038 7 4 -6 -4 1983.31 394.926 7 4 -6 -3 4820.73 548.808 7 4 -6 -2 24881.9 1063.10 6 4 -6 -2 26246.4 1276.53 7 4 -6 -1 324.234 182.071 8 4 -6 -1 340.750 145.050 6 4 -6 0 20823.2 1092.33 8 4 -6 0 19400.2 968.130 6 4 -6 1 17114.3 1022.33 8 4 -6 2 27675.5 1401.40 8 4 -6 3 21390.4 1285.63 8 4 -6 4 11726.5 484.988 20 4 -6 4 11836.8 540.921 18 4 -6 4 10701.6 948.102 8 4 -6 4 11682.7 517.412 29 4 -6 5 2623.73 216.971 20 4 -6 5 2945.28 266.878 18 4 -6 5 2638.77 239.836 29 4 -6 6 992.786 163.008 18 4 -6 6 1155.47 171.435 29 4 -6 7 539.358 122.301 18 4 -6 7 430.990 120.838 29 4 -5 -9 6774.51 314.511 27 4 -5 -9 6571.99 294.140 23 4 -5 -8 6242.81 317.917 23 4 -5 -8 5952.49 315.797 27 4 -5 -7 19027.8 608.718 28 4 -5 -7 18878.6 631.838 27 4 -5 -7 17163.9 646.471 21 4 -5 -6 8044.79 365.107 27 4 -5 -6 8461.68 359.454 28 4 -5 -5 1942.96 370.423 7 4 -5 -4 3597.22 470.745 7 4 -5 -3 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333.821 8 4 -4 4 3785.89 550.495 8 4 -4 5 3002.21 272.061 18 4 -4 5 3183.79 257.104 29 4 -4 5 2573.15 484.549 8 4 -4 6 3834.29 308.262 18 4 -4 6 3931.00 292.876 29 4 -4 7 439.023 141.784 18 4 -4 7 466.240 127.718 29 4 -4 8 647.575 111.623 18 4 -4 8 501.438 106.778 29 4 -3 -10 1686.17 133.337 23 4 -3 -9 6293.13 301.929 23 4 -3 -9 5169.89 287.167 21 4 -3 -8 651.542 132.489 27 4 -3 -8 730.511 136.636 23 4 -3 -8 469.855 124.652 21 4 -3 -7 688.740 129.729 27 4 -3 -7 569.063 141.739 21 4 -3 -6 16633.9 540.059 28 4 -3 -6 16813.9 559.261 27 4 -3 -6 15248.5 1025.97 7 4 -3 -6 16641.1 611.368 21 4 -3 -5 6336.19 618.441 7 4 -3 -4 24059.8 1164.42 7 4 -3 -3 5146.02 486.715 7 4 -3 -2 58448.8 1865.68 7 4 -3 -1 29895.3 1184.15 8 4 -3 -1 29467.7 1168.40 7 4 -3 0 8150.48 597.577 8 4 -3 1 23743.8 1111.25 8 4 -3 2 40876.8 1624.26 8 4 -3 3 20597.6 1175.31 8 4 -3 4 579.265 259.838 8 4 -3 5 46630.3 1331.82 18 4 -3 5 46875.3 1272.18 29 4 -3 5 47193.8 2147.84 8 4 -3 6 10586.2 529.557 18 4 -3 6 10757.2 491.693 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54538.2 1670.28 7 4 2 -1 10191.5 651.370 10 4 2 -1 10239.8 561.943 7 -4 2 1 10485.6 516.102 11 4 2 0 17929.4 883.830 10 -4 2 0 17223.4 737.690 11 -4 2 -1 15483.2 728.178 11 4 2 2 25647.7 1072.48 5 -4 2 -2 28735.5 1099.46 11 -4 2 -3 9.79852 118.430 11 4 2 3-38.7788 129.462 5 4 2 4 15373.7 988.678 5 -4 2 -4 16636.9 897.664 11 4 2 5 46897.9 1322.68 14 4 2 5 43595.7 1298.28 26 4 2 5 44980.6 1972.67 5 4 2 6 5050.39 376.198 14 4 2 6 4514.93 326.352 26 4 2 7 2869.78 302.343 14 4 2 8 866.138 167.482 14 -4 3 10 1677.69 125.275 29 -4 3 9 5868.12 306.026 29 4 3 -9 5828.45 326.294 21 -4 3 8 626.665 135.649 29 4 3 -8 644.947 144.069 21 -4 3 7 774.127 142.430 29 4 3 -7 667.052 134.679 23 4 3 -7 720.613 284.715 7 4 3 -7 866.797 149.985 21 -4 3 6 16058.1 588.142 29 4 3 -6 16129.8 1082.47 7 4 3 -6 16489.2 566.476 23 4 3 -6 16437.4 604.143 21 4 3 -5 6964.81 642.510 7 4 3 -4 25366.3 1188.84 7 4 3 -3 5775.47 501.602 7 4 3 -2 55531.1 1779.64 10 4 3 -2 53856.5 1685.31 7 -4 3 2 53464.1 1512.86 11 4 3 -1 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5748.57 549.279 11 -6 3 -2 865.369 260.186 11 6 3 2 690.566 155.507 26 6 3 2 1043.03 214.109 25 6 3 3 5893.68 408.208 26 6 3 3 6688.55 377.909 25 -6 3 -3 6302.55 628.136 11 6 3 4 545.914 164.890 26 6 3 5 2521.23 264.505 26 6 3 6 441.125 107.357 18 6 3 6 518.701 142.292 26 6 3 7 20321.4 590.833 18 6 3 7 22294.1 605.325 26 6 4 -9 799.817 99.9811 21 6 4 -8 3849.43 241.398 21 6 4 -7 342.943 110.498 12 6 4 -7 571.632 117.538 21 6 4 -6 5403.26 323.012 12 6 4 -5 28116.4 1508.42 7 6 4 -5 29695.0 907.750 12 6 4 -4 6346.69 663.628 10 6 4 -4 6428.16 359.409 17 6 4 -4 5872.61 623.872 7 6 4 -4 6620.23 394.139 13 6 4 -4 6081.67 340.315 12 6 4 -3 4328.40 587.353 10 6 4 -3 4686.26 294.791 17 6 4 -3 3950.40 495.079 7 6 4 -3 4110.54 314.228 13 6 4 -3 4401.33 273.351 12 6 4 -2 11703.6 903.532 10 6 4 -1 23853.2 1321.50 10 -6 4 1 21377.9 1057.71 11 -6 4 0 16156.9 934.860 11 6 4 1 4750.75 331.838 25 -6 4 -1 5094.70 532.721 11 6 4 2 4082.15 327.660 26 6 4 2 4260.27 332.693 25 -6 4 -2 4097.20 506.922 11 6 4 3 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335.804 26 7 -9 1 6974.06 335.329 20 7 -9 2 5588.43 290.034 26 7 -9 2 7223.68 314.481 20 7 -9 3 50.8540 60.6014 20 7 -8 -6 839.377 130.681 21 7 -8 -5 3024.98 217.556 17 7 -8 -4-58.0226 109.851 17 7 -8 -3 2580.88 233.374 17 7 -8 -3 2463.29 232.707 20 7 -8 -2 120.094 103.874 20 7 -8 -2 274.468 130.192 17 7 -8 -1 10200.8 458.925 17 7 -8 -1 10700.0 509.718 26 7 -8 -1 10612.8 468.934 20 7 -8 0 5862.30 324.379 17 7 -8 0 6405.06 374.710 26 7 -8 0 6574.40 349.397 20 7 -8 1 5696.30 339.361 26 7 -8 1 5590.79 311.991 20 7 -8 2 5885.05 381.442 18 7 -8 2 5689.89 315.820 26 7 -8 2 6399.73 308.115 20 7 -8 3 27767.8 871.938 18 7 -8 4 4336.53 267.226 18 7 -7 -7 16493.8 522.686 21 7 -7 -6 316.076 108.313 21 7 -7 -5 4100.75 269.202 17 7 -7 -4 4952.81 310.214 17 7 -7 -3 881.343 160.542 20 7 -7 -3 852.236 165.354 17 7 -7 -2 3572.23 270.943 17 7 -7 -2 3527.91 292.666 26 7 -7 -2 3441.58 268.574 20 7 -7 -1 2748.38 238.639 17 7 -7 -1 2866.33 272.796 26 7 -7 -1 2640.82 226.743 20 7 -7 0 25168.8 789.492 17 7 -7 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-5 -6 207.653 99.0265 17 7 -5 -6 394.725 124.398 21 7 -5 -5 2398.10 219.677 17 7 -5 -4 3967.67 286.830 17 7 -5 -3 22002.0 728.407 17 7 -5 -3 20476.8 748.025 26 7 -5 -3 20689.2 721.455 20 7 -5 -2 41114.5 1142.25 17 7 -5 -2 41820.2 1208.45 26 7 -5 -2 39887.3 1851.99 7 7 -5 -2 40197.7 1135.89 20 7 -5 -1 9674.80 434.397 17 7 -5 -1 9501.08 481.895 26 7 -5 -1 8737.01 803.868 7 7 -5 -1 9270.30 424.325 20 7 -5 0 16705.2 694.820 18 7 -5 0 17930.6 1178.92 8 7 -5 0 17642.3 613.133 17 7 -5 0 18183.0 692.828 26 7 -5 1 894.683 172.677 18 7 -5 1 1220.21 181.848 26 7 -5 2 15223.3 655.828 18 7 -5 2 15222.4 610.610 26 7 -5 3 852.149 166.896 18 7 -5 3 933.866 158.706 26 7 -5 4 122.318 116.034 18 7 -5 4 181.279 88.0110 26 7 -5 5 2288.82 202.103 18 7 -4 -8 441.914 102.612 21 7 -4 -7 774.663 148.472 21 7 -4 -6 5028.06 300.458 17 7 -4 -6 6196.14 356.975 21 7 -4 -5 8945.79 429.135 17 7 -4 -4 26839.1 847.782 17 7 -4 -3 8926.52 422.914 17 7 -4 -3 7998.73 432.441 26 7 -4 -3 7520.64 759.820 7 7 -4 -3 7722.39 396.047 20 7 -4 -2 1790.25 200.304 17 7 -4 -2 1894.70 213.437 26 7 -4 -2 1878.23 391.927 7 7 -4 -2 1702.30 183.064 20 7 -4 -1 5977.84 337.240 17 7 -4 -1 5608.75 367.686 26 7 -4 -1 5632.39 638.445 7 7 -4 0 924.870 290.447 8 7 -4 0 662.388 153.278 26 7 -4 1 4386.16 320.620 18 7 -4 1 3739.89 536.726 8 7 -4 1 4239.89 316.926 26 7 -4 2 9913.14 505.141 18 7 -4 2 10664.8 498.950 26 7 -4 3 19911.5 752.217 18 7 -4 3 20809.4 725.611 26 7 -4 4 8177.22 430.700 18 7 -4 4 8008.61 380.665 26 7 -4 5 2966.68 232.377 18 7 -3 -8 821.494 100.556 23 7 -3 -8 977.157 131.806 21 7 -3 -7 159.718 102.390 21 7 -3 -6 8578.73 396.311 17 7 -3 -6 9505.20 442.180 21 7 -3 -5 27272.7 858.847 17 7 -3 -4 7219.05 378.388 17 7 -3 -4 7052.78 738.261 7 7 -3 -3 14104.2 551.408 17 7 -3 -3 12686.0 975.652 7 7 -3 -2 601.255 133.138 17 7 -3 -2 503.432 136.509 26 7 -3 -2 552.600 203.711 7 7 -3 -1 37106.4 1051.09 17 7 -3 -1 39270.4 1120.72 26 7 -3 -1 34966.1 1624.02 7 7 -3 0 8186.47 758.015 8 7 -3 0 8593.60 449.886 26 7 -3 1 5680.24 641.785 8 7 -3 1 6156.94 386.531 26 7 -3 2 6936.13 405.139 18 7 -3 2 7666.90 421.161 26 7 -3 3 1786.23 217.293 18 7 -3 3 1841.58 211.607 26 7 -3 4 2972.51 260.176 18 7 -3 4 2990.42 238.447 26 7 -3 5 5143.55 309.897 18 7 -3 5 4524.73 256.918 26 7 -3 6 943.572 122.928 18 7 -2 -8 3880.54 245.469 21 7 -2 -7-34.4595 98.0793 21 7 -2 -6 6053.62 337.672 17 7 -2 -6 6378.57 366.178 21 7 -2 -5 1664.81 192.052 17 7 -2 -5 2345.66 221.869 21 7 -2 -4 6396.05 365.111 17 7 -2 -4 7232.27 745.991 7 7 -2 -3 7850.39 391.438 17 7 -2 -3 7560.63 743.046 7 7 -2 -2 10988.3 466.781 17 7 -2 -2 10469.9 487.092 26 7 -2 -2 9875.36 816.187 7 7 -2 -1 43403.9 1171.26 17 7 -2 -1 45029.1 1234.32 26 7 -2 0 4869.72 557.855 8 7 -2 0 4769.34 329.290 26 7 -2 1 4122.12 531.224 8 7 -2 1 3940.35 309.437 26 -7 -2 -2 1330.45 294.816 11 7 -2 2 1606.46 341.434 8 7 -2 2 1453.29 203.020 26 7 -2 3 2815.44 257.855 18 7 -2 3 3093.76 270.009 26 7 -2 4 331.155 120.414 18 7 -2 4 485.141 131.061 26 7 -2 5 1737.95 187.659 18 7 -2 5 1584.74 164.137 26 7 -2 6 2386.13 183.623 18 7 -1 -8 556.606 113.265 21 7 -1 -7 6766.50 352.894 21 7 -1 -6 5239.57 311.459 17 7 -1 -6 5575.14 327.277 21 7 -1 -5 30377.9 913.639 17 7 -1 -5 29881.8 917.158 21 7 -1 -4 300.448 119.623 17 7 -1 -4 158.601 207.925 7 7 -1 -3 7451.19 384.029 17 7 -1 -3 6851.99 693.451 7 7 -1 -3 6665.87 399.657 13 7 -1 -2 11302.9 469.039 17 7 -1 -2 10065.9 808.948 7 7 -1 -1 14765.9 548.693 17 7 -1 -1 14916.9 584.199 26 -7 -1 0 4665.65 495.438 11 7 -1 0 4785.99 322.303 26 -7 -1 -1 9030.77 728.883 11 7 -1 1 9679.05 478.988 26 -7 -1 -2 1565.49 321.206 11 7 -1 2 1406.15 199.235 26 7 -1 3 6854.80 407.796 26 7 -1 4 922.245 154.121 18 7 -1 4 786.572 154.676 26 7 -1 5-75.2753 102.469 18 7 -1 5 20.1540 88.0039 26 7 -1 6 3545.63 219.076 18 7 0 -8 323.705 96.7085 21 7 0 -7 1608.94 182.762 21 7 0 -6 13926.3 534.786 17 7 0 -6 13573.9 538.874 21 7 0 -5 62028.7 1593.01 17 7 0 -5 63871.6 1622.23 13 7 0 -5 63193.8 1576.61 21 7 0 -4 5495.66 339.641 17 7 0 -4 5494.21 629.762 7 7 0 -4 5352.69 350.609 13 7 0 -3 12007.5 499.269 17 7 0 -3 10721.7 853.498 7 7 0 -3 11065.3 528.382 13 7 0 -2 6793.51 355.235 17 7 0 -2 6183.46 623.485 7 7 0 -1 11845.8 485.213 17 7 0 -1 12456.9 529.845 26 7 0 -1 12759.0 540.336 25 7 0 0 6966.77 402.662 26 -7 0 0 6884.71 609.014 11 7 0 1 5007.12 342.985 26 -7 0 -1 4861.57 530.218 11 -7 0 -2 92.4426 176.567 11 7 0 2 93.9604 125.362 26 7 0 3 11850.8 557.494 26 7 0 4 6885.05 392.728 26 7 0 5 981.567 143.095 18 7 0 5 1075.99 156.750 26 7 0 6 690.090 108.433 18 7 0 6 325.013 81.5285 26 7 1 -8 537.049 106.490 12 7 1 -8 575.973 111.912 21 7 1 -7 6533.31 342.978 21 7 1 -6 4630.97 304.455 17 7 1 -6 5132.31 300.488 21 7 1 -5 30982.1 915.146 17 7 1 -5 27904.3 926.240 13 7 1 -4 302.830 119.653 17 7 1 -4 230.398 136.876 13 7 1 -4 630.088 248.365 7 7 1 -3 7302.64 382.277 17 7 1 -3 6869.21 666.342 7 7 1 -3 6536.49 400.910 13 7 1 -2 10563.8 464.314 17 7 1 -2 10811.2 486.091 25 7 1 -1 13965.6 535.611 17 7 1 -1 14704.4 601.108 25 7 1 0 4332.48 301.459 26 7 1 0 5211.95 359.685 25 -7 1 0 3859.63 454.001 11 7 1 1 9196.22 473.583 26 -7 1 -1 8513.62 713.889 11 -7 1 -2 1532.38 318.744 11 7 1 2 1714.68 226.284 26 7 1 3 6615.61 415.208 26 7 1 4 632.409 165.264 26 7 1 5 29.4778 96.6869 26 7 1 6 3214.31 194.811 18 7 1 6 3524.81 208.827 26 7 2 -8 3576.95 210.543 12 7 2 -8 3669.21 220.556 21 7 2 -7 57.6148 112.985 12 7 2 -7 89.3473 83.8219 21 7 2 -6 6207.43 348.397 17 7 2 -6 6226.99 329.042 21 7 2 -5 2059.98 218.830 17 7 2 -5 2508.89 256.693 13 7 2 -4 6875.86 378.561 17 7 2 -4 6108.01 658.137 7 7 2 -4 6991.91 415.147 13 7 2 -3 7420.15 386.540 17 7 2 -3 6835.27 657.671 7 7 2 -3 7301.50 425.933 13 7 2 -2 9956.08 453.076 17 7 2 -2 10791.2 490.136 25 7 2 -2 10198.9 426.789 12 7 2 -1 41260.0 1142.00 17 7 2 -1 43957.7 1216.56 25 7 2 0 4780.59 315.129 26 7 2 0 5464.82 366.441 25 -7 2 0 4770.13 515.793 11 7 2 1 4229.72 312.780 26 7 2 1 4419.23 349.812 25 -7 2 -1 3801.30 484.561 11 -7 2 -2 1332.71 306.625 11 7 2 2 1542.03 220.327 26 7 2 3 2875.09 280.283 26 7 2 4 460.099 155.225 26 7 2 5 1653.94 193.660 26 7 2 6 2557.43 179.033 26 7 3 -8 842.277 112.479 12 7 3 -8 607.514 97.6138 21 7 3 -7 129.971 107.013 12 7 3 -7 89.5218 73.2103 21 7 3 -6 9149.34 420.087 12 7 3 -5 28581.1 899.832 17 7 3 -5 29152.6 946.734 13 7 3 -5 30230.5 899.036 12 7 3 -4 6509.43 373.359 17 7 3 -4 6394.45 399.347 13 7 3 -4 6321.85 363.510 12 7 3 -3 13761.0 550.434 17 7 3 -3 13523.3 604.190 13 7 3 -3 13291.0 528.314 12 7 3 -2 513.331 137.217 17 7 3 -2 508.767 146.125 13 7 3 -2 436.732 148.952 25 7 3 -2 531.727 121.610 12 7 3 -1 36464.9 1035.12 17 7 3 -1 38542.9 1123.87 25 7 3 0 8485.34 457.555 25 -7 3 0 7390.67 648.749 11 7 3 1 5413.12 365.476 26 7 3 1 6782.89 411.772 25 -7 3 -1 5534.29 597.914 11 7 3 2 7237.46 428.104 26 7 3 2 7519.44 441.981 25 7 3 3 1862.90 239.479 26 7 3 4 3503.11 295.722 26 7 3 5 5298.43 318.074 26 7 3 6 930.084 119.217 26 7 4 -8 421.283 88.0126 12 7 4 -8 341.409 75.1761 21 7 4 -7 920.135 137.854 12 7 4 -6 6193.34 337.965 12 7 4 -5 10084.4 511.408 13 7 4 -5 10427.5 460.889 12 7 4 -4 27202.8 861.346 17 7 4 -4 26734.4 902.767 13 7 4 -4 26954.4 841.991 12 7 4 -3 8221.26 417.640 17 7 4 -3 8493.28 454.163 13 7 4 -3 8046.20 420.364 25 7 4 -3 7834.02 396.083 12 7 4 -2 2106.92 216.555 17 7 4 -2 1689.59 224.339 13 7 4 -2 1552.64 211.677 25 7 4 -2 1889.87 200.208 12 7 4 -1 5807.11 332.119 17 7 4 -1 5681.35 386.327 13 7 4 -1 5199.96 368.441 25 -7 4 0 348.581 160.419 11 7 4 0 693.324 181.253 25 7 4 1 4127.75 312.066 26 7 4 1 5006.02 357.614 25 -7 4 -1 3997.13 500.143 11 7 4 2 9759.68 507.578 26 7 4 2 9785.15 508.546 25 7 4 3 19932.8 757.084 26 7 4 4 8612.81 443.860 26 7 4 5 2753.14 228.136 26 7 5 -8-68.6374 62.3136 12 7 5 -7 116.132 88.5716 12 7 5 -6 454.431 121.648 12 7 5 -5 2615.28 232.893 12 7 5 -4 4374.44 342.801 13 7 5 -4 4335.62 302.281 12 7 5 -3 20725.6 761.470 13 7 5 -3 20580.8 741.090 25 7 5 -3 19979.0 700.825 12 7 5 -2 43102.5 1245.45 13 7 5 -2 42118.6 1235.10 25 7 5 -2 41453.9 1133.54 12 7 5 -1 8984.56 475.621 13 7 5 -1 9139.63 482.245 25 7 5 -1 8878.23 394.284 12 7 5 0 16287.7 657.447 13 7 5 0 16454.9 676.966 25 -7 5 0 16319.7 1019.57 11 7 5 1 940.393 160.200 26 7 5 1 986.547 230.828 25 7 5 2 14539.6 613.856 26 7 5 2 14277.3 617.055 25 7 5 3 945.609 180.853 26 7 5 4 212.550 131.638 26 7 5 5 2477.65 211.688 26 7 6 -7 701.487 107.084 12 7 6 -6 118.518 95.9202 12 7 6 -5 2545.59 227.672 12 7 6 -4 2750.44 277.884 13 7 6 -4 2364.41 222.080 12 7 6 -3 13861.4 596.493 13 7 6 -3 12295.7 553.530 25 7 6 -3 13253.6 526.150 12 7 6 -2 5521.46 353.536 13 7 6 -2 5021.94 305.642 12 7 6 -1 12609.0 550.787 13 7 6 -1 12290.6 568.020 25 7 6 -1 12365.3 481.609 12 -7 6 1 12210.7 509.515 24 7 6 0 5258.73 336.065 13 7 6 0 4837.62 362.063 25 7 6 1 14399.5 619.639 25 7 6 2 7260.37 411.468 26 7 6 2 9143.41 454.919 25 7 6 3 838.183 169.337 26 7 6 4 2853.76 244.852 26 7 6 5 1413.35 152.054 26 7 7 -7 15707.3 459.827 12 -7 7 6 238.381 83.5605 29 7 7 -6 188.774 98.3867 12 -7 7 5 4573.85 270.115 29 7 7 -5 4374.87 273.156 12 -7 7 4 4837.33 295.311 29 7 7 -4 5046.55 309.347 12 -7 7 3 877.778 135.717 29 7 7 -3 788.462 173.662 13 7 7 -3 566.549 139.699 12 7 7 -2 3695.28 284.422 13 7 7 -2 2567.05 255.667 25 7 7 -2 2727.24 237.125 12 -7 7 2 3263.90 243.706 24 7 7 -1 2308.83 230.876 13 7 7 -1 2093.61 237.650 25 7 7 -1 2546.10 213.626 12 -7 7 1 2914.85 239.872 24 7 7 0 24708.5 871.208 25 -7 7 0 24742.6 809.245 24 7 7 1 2577.52 270.454 25 7 7 2 1406.38 181.934 26 7 7 2 1936.29 239.376 25 7 7 3 6958.98 372.053 26 7 7 4 2766.96 220.788 26 -7 8 6 648.413 103.800 29 7 8 -6 575.363 101.029 12 -7 8 5 3546.75 228.484 29 7 8 -5 2995.62 211.718 12 -7 8 4 33.0836 74.4931 29 7 8 -4-57.2633 115.635 12 -7 8 3 2615.85 216.920 29 7 8 -3 2385.62 221.028 12 7 8 -2 407.986 138.056 13 -7 8 2 214.682 100.904 24 7 8 -2 210.732 106.107 12 7 8 -1 10039.9 501.608 25 7 8 -1 9837.50 421.308 12 -7 8 1 10850.2 468.520 24 7 8 0 5966.64 382.444 25 -7 8 0 5854.64 350.473 24 7 8 1 5629.08 366.894 25 -7 8 -1 5748.06 336.982 24 7 8 2 6403.29 352.557 25 -7 8 -2 6698.27 358.551 24 7 8 3 25650.7 797.326 26 -7 8 -3 29316.6 813.357 24 7 8 4 4458.80 247.932 26 -7 8 -4 4730.17 242.629 24 -7 9 6 6660.29 278.190 29 7 9 -6 6799.59 261.154 12 -7 9 5 2315.05 180.558 29 7 9 -5 2030.99 166.512 12 -7 9 4 2956.69 216.024 29 7 9 -4 2300.54 205.358 25 7 9 -4 2658.67 201.531 12 -7 9 3 1306.92 158.309 29 7 9 -3 1379.63 174.774 12 7 9 -2 2878.03 255.058 25 7 9 -2 3603.17 254.529 12 -7 9 2 3143.35 236.470 24 7 9 -1 4149.72 309.101 25 -7 9 1 4196.70 279.774 24 7 9 0 2119.02 230.258 25 -7 9 0 2475.99 223.141 24 7 9 1 6863.87 369.403 25 -7 9 -1 6642.55 348.201 24 7 9 2 6645.73 336.814 25 -7 9 -2 7010.72 339.439 24 7 9 3 194.789 83.4142 26 -7 9 -3 103.580 87.9435 24 -7 10 5 1783.92 146.196 29 -7 10 4 3544.52 218.994 29 7 10 -4 2783.75 206.220 25 -7 10 3 1357.99 148.471 29 -7 10 3 1075.97 132.508 24 7 10 -2 4299.30 287.545 25 -7 10 2 4700.21 272.971 24 7 10 -1 6212.74 360.851 25 -7 10 1 6740.66 334.682 24 7 10 0 3224.49 257.433 25 -7 10 0 3855.88 252.885 24 7 10 1 1980.18 206.005 25 -7 10 -1 1797.19 175.744 24 -7 10 -2 4997.33 262.299 24 -7 11 4 1251.61 122.172 29 7 11 -4 567.785 102.087 25 -7 11 3 4781.26 243.718 29 7 11 -3 4111.95 248.069 25 -7 11 2 7375.75 320.352 29 7 11 -2 6401.73 328.491 25 -7 11 2 6639.18 302.581 24 7 11 -1 6178.25 329.635 25 -7 11 1 6466.33 306.268 24 7 11 0 579.013 132.164 25 -7 11 0 696.988 118.870 24 7 11 1 1905.91 174.123 25 -7 11 -1 1812.78 157.002 24 -7 12 1 991.154 107.471 29 -7 12 1 879.696 110.772 24 8 -10 -3 277.925 88.1304 17 8 -10 -2 1471.96 136.903 17 8 -10 -1 259.656 84.4551 20 8 -10 -1 309.574 86.5178 17 8 -10 0 8504.43 322.235 20 8 -9 -4 4970.88 250.522 17 8 -9 -3 45.0090 91.8729 17 8 -9 -2 1695.78 162.690 17 8 -9 -2 1622.88 166.015 20 8 -9 -1 2503.43 184.714 17 8 -9 -1 2476.30 193.081 20 8 -9 0 859.189 119.343 20 8 -9 1 6920.93 281.557 20 8 -8 -5 5377.04 252.792 17 8 -8 -5 5423.15 276.746 21 8 -8 -4 3001.94 210.790 17 8 -8 -3 163.597 105.825 17 8 -8 -2 4252.30 265.369 17 8 -8 -2 3744.20 252.523 20 8 -8 -1 7933.54 358.640 17 8 -8 -1 8464.96 376.159 20 8 -8 0 4295.44 285.988 26 8 -8 0 4603.50 259.211 20 8 -8 1 6258.77 323.337 26 8 -8 1 6967.40 298.486 20 8 -8 2 4516.92 238.278 26 8 -7 -6 420.718 80.0583 17 8 -7 -6 559.547 100.239 21 8 -7 -5 2940.27 203.551 17 8 -7 -5 2960.42 217.885 21 8 -7 -4 2500.83 214.258 17 8 -7 -3 541.281 137.289 17 8 -7 -2 2340.00 212.273 17 8 -7 -2 2043.16 222.202 26 8 -7 -2 2112.09 199.789 20 8 -7 -1 2431.69 206.028 17 8 -7 -1 2273.88 241.035 26 8 -7 -1 2080.44 193.421 20 8 -7 0 3243.10 261.932 26 8 -7 0 3359.77 229.137 20 8 -7 1 1248.88 166.741 26 8 -7 2 6309.09 314.274 26 8 -7 3 5843.26 257.599 26 8 -6 -6 917.688 121.512 17 8 -6 -6 962.439 128.063 21 8 -6 -5 730.028 137.537 17 8 -6 -5 872.260 140.637 21 8 -6 -4 4589.24 293.431 17 8 -6 -3 715.981 155.320 17 8 -6 -2 6344.74 343.383 17 8 -6 -2 5691.55 364.893 26 8 -6 -2 5794.97 328.469 20 8 -6 -1 14786.1 549.024 17 8 -6 -1 14991.0 612.517 26 8 -6 -1 15113.2 548.801 20 8 -6 0 3405.76 274.959 26 8 -6 1 7048.80 377.945 26 8 -6 2 5811.79 343.611 18 8 -6 2 6329.87 332.147 26 8 -6 3 1373.13 163.897 18 8 -6 3 1427.51 144.011 26 8 -5 -7 421.340 91.9461 21 8 -5 -6 1443.45 150.890 17 8 -5 -6 1538.56 162.174 21 8 -5 -5 3859.49 261.525 17 8 -5 -5 3599.19 261.457 21 8 -5 -4 418.918 129.492 17 8 -5 -3 5846.03 340.617 17 8 -5 -3 4904.62 337.868 26 8 -5 -2 15278.2 573.179 17 8 -5 -2 14930.1 605.096 26 8 -5 -2 13935.2 540.956 20 8 -5 -1 27308.3 833.550 17 8 -5 -1 27887.4 902.247 26 8 -5 0 14093.0 586.827 26 8 -5 1 4488.75 310.276 18 8 -5 1 5432.73 345.929 26 8 -5 2 3310.20 266.543 18 8 -5 2 3995.58 274.998 26 8 -5 3 2612.61 221.517 18 8 -5 3 2879.40 212.524 26 8 -5 4 6718.84 319.630 18 8 -5 4 6863.84 278.229 26 8 -4 -7 6894.64 307.183 21 8 -4 -6 1112.28 140.002 17 8 -4 -6 1445.66 159.854 21 8 -4 -5 1441.62 181.100 17 8 -4 -5 1609.29 176.635 21 8 -4 -4 1403.36 194.225 17 8 -4 -3 17642.4 628.523 17 8 -4 -3 15193.9 609.587 26 8 -4 -2 34.1326 115.397 17 8 -4 -2 147.533 113.400 26 8 -4 -1 3530.08 258.729 17 8 -4 -1 3996.13 307.983 26 8 -4 0 3092.97 273.670 26 8 -4 1 451.472 143.784 26 8 -4 2 2637.95 240.144 18 8 -4 2 2626.34 241.038 26 8 -4 3 6940.29 367.089 18 8 -4 3 7436.92 363.980 26 8 -4 4 1180.43 145.547 18 8 -4 4 1264.51 132.835 26 8 -3 -7 464.535 107.837 21 8 -3 -6 330.666 111.195 17 8 -3 -6 462.130 114.684 21 8 -3 -5 19566.9 658.995 17 8 -3 -5 18698.1 650.972 21 8 -3 -4 21295.6 722.126 17 8 -3 -3 3215.01 261.253 17 8 -3 -2 61303.6 1546.32 17 8 -3 -2 59808.4 1575.60 26 8 -3 -1 4033.39 275.532 17 8 -3 -1 3682.68 289.588 26 8 -3 0 32.6709 112.802 26 8 -3 1 10657.1 501.326 26 8 -3 2 764.325 160.129 26 8 -3 3 317.512 111.623 18 8 -3 3 332.092 123.250 26 8 -3 4 5431.95 294.293 18 8 -3 4 5496.93 282.335 26 8 -2 -7 290.526 99.1705 21 8 -2 -6 193.606 113.525 17 8 -2 -6 301.840 101.868 21 8 -2 -5 3881.31 274.315 17 8 -2 -5 3862.79 260.152 21 8 -2 -4 9013.64 437.750 17 8 -2 -4 8865.59 411.427 21 8 -2 -3 34230.5 988.530 17 8 -2 -3 30875.5 990.847 13 8 -2 -2 13806.4 551.341 17 8 -2 -2 13650.7 561.294 26 8 -2 -1 8579.80 410.419 17 8 -2 -1 8980.71 455.347 26 8 -2 0 3668.32 302.642 26 8 -2 1 4469.14 325.273 26 8 -2 2 3152.90 277.679 26 8 -2 3 3726.38 278.091 26 8 -2 4 4775.83 270.961 18 8 -2 4 5485.85 294.470 26 8 -1 -8 3562.00 191.749 12 8 -1 -8 3474.45 190.589 21 8 -1 -7 145.522 86.9647 21 8 -1 -6 245.472 115.700 17 8 -1 -6 326.519 99.0401 21 8 -1 -5 10606.7 472.787 17 8 -1 -5 10660.9 444.055 21 8 -1 -4 7828.11 398.994 17 8 -1 -4 6877.96 386.162 13 8 -1 -3 4563.61 302.627 17 8 -1 -3 3495.91 300.774 13 8 -1 -2 17313.4 638.192 17 8 -1 -1 21265.5 715.014 17 8 -1 -1 21814.6 756.985 26 8 -1 0 57.2085 104.339 26 8 -1 1 3486.37 286.438 26 8 -1 2 22131.3 783.020 26 8 -1 3 1364.57 194.923 26 8 -1 4 453.436 115.594 26 8 -1 5 274.754 72.5977 26 8 0 -8 354.934 84.7117 12 8 0 -8 323.720 76.7540 21 8 0 -7 8507.24 351.375 21 8 0 -6 7609.38 367.920 17 8 0 -6 7370.92 344.874 21 8 0 -5 1151.87 182.511 17 8 0 -5 1389.88 185.616 13 8 0 -4 59.2219 134.058 17 8 0 -4 281.474 131.532 13 8 0 -3 2601.44 239.197 17 8 0 -3 2201.34 251.745 13 8 0 -2 186.774 124.426 17 8 0 -1 31877.5 935.079 17 8 0 -1 32201.6 973.406 26 8 0 0 5551.27 357.646 26 8 0 1 1766.13 217.976 26 8 0 2 8619.04 451.505 26 8 0 3 561.934 144.694 26 8 0 4 90.6791 99.8574 26 8 0 5 1148.90 124.662 26 8 1 -8 3670.93 188.984 12 8 1 -8 3301.29 177.595 21 8 1 -7 113.271 94.9027 12 8 1 -7 70.6416 70.7720 21 8 1 -6 225.077 110.185 17 8 1 -5 10851.4 479.573 17 8 1 -5 10756.8 488.353 13 8 1 -4 7596.62 403.874 17 8 1 -4 7812.69 429.841 13 8 1 -4 7542.03 381.367 12 8 1 -3 4520.50 306.398 17 8 1 -3 4088.74 333.373 13 8 1 -3 3885.10 264.126 12 8 1 -2 18000.3 638.372 17 8 1 -2 16153.4 692.103 13 8 1 -1 19916.3 683.525 17 8 1 0 116.518 105.572 26 8 1 1 3216.98 279.287 26 8 1 2 22224.2 783.539 26 8 1 3 1572.78 203.744 26 8 1 4 372.485 127.148 26 8 1 5 324.495 85.5330 26 8 2 -7 272.798 103.573 12 8 2 -6 133.161 119.709 12 8 2 -5 3906.19 287.508 17 8 2 -5 4309.64 311.532 13 8 2 -5 4042.86 281.876 12 8 2 -4 9352.82 445.540 17 8 2 -4 8767.77 459.890 13 8 2 -4 8625.61 412.318 12 8 2 -3 34155.6 995.849 17 8 2 -3 33707.3 1062.59 13 8 2 -3 31364.5 932.407 12 8 2 -2 13257.1 538.690 17 8 2 -2 13130.9 568.208 25 8 2 -2 13199.9 619.380 13 8 2 -1 8691.41 405.378 17 8 2 -1 9008.92 485.896 25 8 2 0 3227.61 267.630 26 8 2 1 3673.87 294.245 26 8 2 2 3269.13 279.278 26 8 2 3 3228.36 275.378 26 8 2 4 5883.71 322.467 26 8 3 -7 483.082 106.727 12 8 3 -6 433.841 125.947 12 8 3 -5 19709.2 704.392 13 8 3 -5 19875.2 663.077 12 8 3 -4 21077.1 721.537 17 8 3 -4 21357.6 761.185 13 8 3 -3 3770.37 285.025 17 8 3 -3 3581.62 309.633 13 8 3 -3 3150.43 254.300 12 8 3 -2 60139.7 1525.83 17 8 3 -2 61294.1 1647.53 13 8 3 -2 59088.4 1566.30 25 8 3 -1 4027.97 273.034 17 8 3 -1 4755.37 354.311 25 8 3 -1 3712.82 320.232 13 8 3 0 743.178 221.879 25 8 3 1 10414.5 488.645 26 8 3 2 518.904 154.534 26 8 3 3 294.125 129.133 26 8 3 4 6374.43 327.111 26 8 4 -7 6714.96 285.872 12 8 4 -6 1473.06 168.479 12 8 4 -5 2047.50 243.513 13 8 4 -5 1742.16 189.814 12 8 4 -4 1566.19 216.704 13 8 4 -4 1124.76 172.967 12 8 4 -3 17389.8 675.624 13 8 4 -3 16166.8 622.173 25 8 4 -3 15807.6 578.352 12 8 4 -2 212.134 139.189 13 8 4 -2 417.997 181.054 25 8 4 -2 210.420 101.630 12 8 4 -1 3880.23 320.287 13 8 4 -1 4936.19 358.946 25 8 4 0 3653.44 328.463 25 8 4 0 2415.76 248.924 13 8 4 1 493.373 131.943 26 8 4 1 2176.85 289.902 25 8 4 2 2848.96 243.999 26 8 4 3 7285.15 378.046 26 8 4 4 1351.78 163.237 26 8 5 -7 269.520 74.5235 12 8 5 -6 1579.16 157.772 12 8 5 -5 4257.28 270.009 12 8 5 -4 565.696 173.607 13 8 5 -4 468.148 139.876 12 8 5 -3 5865.88 370.375 13 8 5 -3 5736.92 354.111 25 8 5 -3 5377.09 309.602 12 8 5 -2 14657.8 609.677 13 8 5 -2 14711.7 609.158 25 8 5 -2 13950.0 526.259 12 8 5 -1 27611.1 916.954 13 8 5 -1 29154.3 934.477 25 8 5 0 12659.8 556.386 13 8 5 0 14608.3 607.961 25 8 5 1 4373.14 298.957 13 8 5 1 6284.71 380.756 25 8 5 2 3302.72 258.756 26 8 5 3 2827.48 225.923 26 8 5 4 7606.92 336.341 26 8 6 -6 1046.77 127.420 12 8 6 -5 936.115 142.833 12 8 6 -4 5436.35 347.960 13 8 6 -4 4477.31 277.897 12 8 6 -3 614.297 156.298 13 8 6 -3 450.071 155.920 25 8 6 -3 383.141 117.517 12 8 6 -2 5793.99 352.601 13 8 6 -2 5757.07 374.525 25 8 6 -2 5377.34 306.512 12 8 6 -1 14203.7 574.983 13 8 6 -1 15962.8 634.708 25 -8 6 1 14637.5 536.281 24 8 6 0 3040.68 245.217 13 -8 6 0 3157.58 240.202 24 8 6 1 7684.47 420.104 25 8 6 2 5360.37 297.250 26 8 6 3 1464.29 157.254 26 8 7 -6 530.723 92.6440 12 8 7 -5 3108.92 203.813 12 8 7 -4 2310.04 199.247 12 8 7 -3 844.008 166.313 13 8 7 -3 597.559 158.739 25 8 7 -3 427.212 112.482 12 8 7 -2 1888.36 202.094 13 8 7 -2 2291.75 240.676 25 8 7 -2 1855.07 184.580 12 8 7 -1 2060.88 199.715 13 8 7 -1 2565.93 275.687 25 8 7 -1 2527.83 201.023 12 -8 7 1 1916.30 182.956 24 8 7 0 4231.26 319.700 25 -8 7 0 2994.96 228.022 24 8 7 1 1847.06 228.506 25 -8 7 -1 1196.04 158.188 24 -8 7 -2 6729.13 325.627 24 8 7 3 6181.90 280.508 26 -8 7 -3 7114.70 305.240 24 8 8 -5 5849.54 261.451 12 8 8 -4 3014.42 203.194 12 8 8 -3 110.143 123.795 25 8 8 -3 142.588 99.4581 12 8 8 -2 4130.48 255.750 13 8 8 -2 3874.20 281.726 25 8 8 -2 4045.36 240.628 12 8 8 -1 9002.77 435.254 25 -8 8 1 7819.16 353.880 24 8 8 0 5278.94 329.324 25 -8 8 0 4341.53 263.601 24 8 8 1 7258.92 362.621 25 -8 8 -1 6512.38 316.149 24 -8 8 -2 5140.60 263.117 24 8 9 -4 6288.84 273.134 12 -8 9 3 179.321 70.2674 29 8 9 -3 145.848 111.375 25 -8 9 2 1539.30 137.207 29 8 9 -2 1649.75 190.664 25 -8 9 2 1386.49 132.354 24 8 9 -1 2784.88 240.913 25 -8 9 1 2308.65 177.350 24 8 9 0 1249.38 187.766 25 -8 9 0 825.186 121.108 24 8 9 1 6922.44 315.556 25 -8 9 -1 6477.10 292.502 24 -8 10 3 294.235 67.7014 29 8 10 -3 410.993 108.071 25 -8 10 2 1506.34 125.952 29 8 10 -2 1628.03 170.914 25 -8 10 2 1304.76 115.060 24 -8 10 1 303.203 71.6653 29 -8 10 1 340.620 84.2610 24 8 10 0 8978.70 350.854 25 -8 10 0 8156.28 317.205 24 9 -8 -2 4342.65 217.489 17 9 -8 -1 4775.57 211.214 17 9 -7 -4 4015.69 215.189 17 9 -7 -4 3689.91 205.668 21 9 -7 -3 259.463 96.7883 17 9 -7 -2 1514.61 147.943 17 9 -7 -1 5055.79 242.524 17 9 -7 0 404.727 102.804 26 9 -7 1 1155.56 125.971 26 9 -6 -5 1207.98 125.845 17 9 -6 -5 1500.89 131.646 21 9 -6 -4 6671.48 303.819 17 9 -6 -4 6131.85 289.161 21 9 -6 -3 1317.66 155.669 17 9 -6 -2 8523.64 361.003 17 9 -6 -1 12352.0 439.699 17 9 -6 -1 13597.4 508.056 26 9 -6 0 2217.68 198.111 26 9 -6 1 5631.05 291.194 26 9 -5 -5 316.601 96.9228 17 9 -5 -5 468.959 90.0820 21 9 -5 -4 707.872 135.799 17 9 -5 -4 619.503 106.113 21 9 -5 -3 2932.63 225.268 17 9 -5 -2 658.350 132.581 17 9 -5 -2 657.280 132.467 26 9 -5 -1 8237.27 349.222 17 9 -5 -1 8255.01 394.532 26 9 -5 0 1806.81 192.760 26 9 -5 1 11702.4 453.837 26 9 -5 2 3250.96 209.691 26 9 -4 -6 2027.67 151.541 17 9 -4 -6 2194.04 150.602 21 9 -4 -5 1018.00 139.307 17 9 -4 -5 843.931 112.438 21 9 -4 -4 2369.76 204.172 17 9 -4 -4 2139.43 171.575 21 9 -4 -3 1914.99 199.875 17 9 -4 -2 637.627 135.670 17 9 -4 -2 504.352 125.732 26 9 -4 -1 3773.82 241.394 17 9 -4 -1 3953.12 277.211 26 9 -4 0 3365.94 250.614 26 9 -4 1 5869.67 318.992 26 9 -4 2 42.6908 83.5218 26 9 -3 -6 1727.46 148.479 17 9 -3 -6 1416.17 128.423 21 9 -3 -5 577.085 124.306 17 9 -3 -5 764.560 108.627 21 9 -3 -4 1744.32 194.000 17 9 -3 -3 1113.58 165.557 17 9 -3 -2 11224.2 455.711 17 9 -3 -2 11058.5 461.841 26 9 -3 -2 9753.86 448.799 13 9 -3 -1 26442.5 779.458 17 9 -3 -1 27867.6 847.021 26 9 -3 0 15389.9 580.227 26 9 -3 1 5305.55 317.052 26 9 -3 2 5208.06 294.138 26 9 -3 3 2308.75 173.647 26 9 -2 -6 5452.96 260.970 17 9 -2 -6 5138.23 250.160 12 9 -2 -6 5175.42 239.970 21 9 -2 -5 7164.45 343.991 17 9 -2 -5 6785.12 305.124 12 9 -2 -4 1072.21 168.593 17 9 -2 -3 3962.44 267.707 17 9 -2 -3 2842.70 229.939 13 9 -2 -2 11491.5 468.815 17 9 -2 -2 10998.5 461.498 26 9 -2 -2 10207.2 488.594 13 9 -2 -1 9025.93 396.219 17 9 -2 -1 9302.74 436.624 26 9 -2 0 8575.18 423.356 26 9 -2 1 325.784 118.476 26 9 -2 2 38.5828 96.4202 26 9 -2 3 1809.19 159.689 26 9 -1 -6 3466.26 215.157 17 9 -1 -6 3513.42 209.120 12 9 -1 -5 977.556 155.991 17 9 -1 -5 649.899 115.284 12 9 -1 -4 410.921 139.293 17 9 -1 -4 705.202 131.933 13 9 -1 -3 831.827 153.205 17 9 -1 -3 918.342 154.297 13 9 -1 -2 6426.25 337.431 17 9 -1 -2 5775.09 363.102 13 9 -1 -1 12718.2 512.152 26 9 -1 0 4068.30 279.281 26 9 -1 1 993.417 159.625 26 9 -1 2 798.894 143.227 26 9 -1 3 6597.48 307.560 26 9 0 -6 41.5217 82.6499 12 9 0 -5 5605.09 300.059 17 9 0 -5 4919.21 274.500 13 9 0 -5 5189.76 276.199 12 9 0 -4 198.388 119.100 17 9 0 -4 88.3491 117.379 13 9 0 -4 26.8554 82.7142 12 9 0 -3 2561.11 229.603 17 9 0 -3 2134.74 225.834 13 9 0 -2 1344.01 167.115 17 9 0 -2 1402.38 199.166 13 9 0 -1 5778.82 329.038 26 9 0 0 33.1609 94.9637 26 9 0 1-29.2744 101.476 26 9 0 2-62.4957 102.680 26 9 0 3 4408.83 253.642 26 9 1 -6 3565.88 217.150 12 9 1 -5 1019.65 155.548 17 9 1 -5 1039.02 153.903 13 9 1 -5 813.535 124.973 12 9 1 -4 498.053 146.028 17 9 1 -4 430.650 129.749 13 9 1 -4 369.647 104.561 12 9 1 -3 756.500 155.175 17 9 1 -3 776.715 167.700 13 9 1 -2 6365.35 336.245 17 9 1 -2 6333.39 390.244 13 9 1 -1 13313.1 583.885 13 9 1 0 3175.98 247.915 26 9 1 1 947.240 148.389 26 9 1 2 984.615 145.798 26 9 1 3 6632.30 310.151 26 9 2 -6 5613.51 265.260 12 9 2 -5 7037.89 324.329 12 9 2 -4 1335.96 178.487 17 9 2 -4 1379.49 189.951 13 9 2 -4 1187.46 147.308 12 9 2 -3 3351.25 251.251 17 9 2 -3 3005.27 267.818 13 9 2 -2 11146.2 458.385 17 9 2 -2 11888.2 531.303 13 9 2 -1 10365.0 505.320 13 9 2 0 8167.89 379.221 26 9 2 1 268.650 107.114 26 9 2 2 86.6065 94.1742 26 9 2 3 1735.63 156.867 26 9 3 -6 1783.63 153.451 12 9 3 -5 806.012 135.152 12 9 3 -4 1558.87 197.367 13 9 3 -4 1662.02 170.032 12 9 3 -3 1143.64 195.013 13 9 3 -3 983.178 133.230 12 9 3 -2 12255.9 539.810 13 9 3 -1 28639.6 917.834 13 9 3 0 14100.6 577.097 13 9 3 1 4763.32 276.836 26 9 3 1 4648.26 299.497 13 9 3 2 5426.56 285.253 26 9 3 2 4859.71 281.307 13 9 3 3 2187.82 167.573 26 9 4 -6 2429.37 162.178 12 9 4 -5 950.175 123.518 12 9 4 -4 2566.27 232.419 13 9 4 -4 2236.99 178.555 12 9 4 -3 2034.14 220.214 13 9 4 -3 1561.12 148.375 12 9 4 -2 655.936 158.631 13 9 4 -1 3916.36 284.130 13 9 4 0 2715.14 232.255 13 9 4 1 4974.03 262.969 26 9 4 1 4934.58 291.712 13 9 4 2-35.6940 73.2510 26 9 4 2-21.4728 78.6009 13 9 5 -5 171.460 80.7482 12 9 5 -4 1384.46 185.208 13 9 5 -4 545.945 106.686 12 9 5 -3 3359.49 258.995 13 9 5 -3 3597.65 245.542 25 9 5 -3 2972.67 195.918 12 9 5 -2 1353.81 205.909 25 9 5 -2 877.686 154.214 13 9 5 -1 8482.73 397.984 13 9 5 -1 9089.51 437.070 25 9 5 0 1656.65 172.270 13 -9 5 0 1633.61 148.570 24 9 5 1 9869.89 391.422 13 -9 5 -1 10604.4 392.886 24 9 5 2 3052.86 184.659 26 -9 5 -2 3703.01 210.557 24 9 6 -5 1164.62 117.790 12 9 6 -4 6332.77 272.286 12 9 6 -3 1786.65 184.710 13 9 6 -3 1828.42 179.833 25 9 6 -2 8818.59 388.749 13 9 6 -2 9271.86 403.768 25 9 6 -1 13127.2 483.466 13 9 6 -1 14173.4 528.682 25 9 6 0 2212.18 175.103 13 -9 6 0 2123.24 158.623 24 -9 6 -1 5397.64 255.385 24 9 7 -4 3825.50 195.172 12 9 7 -3 844.881 143.941 25 9 7 -3 560.490 108.860 12 9 7 -2 2007.63 173.852 13 9 7 -2 2384.06 216.969 25 9 7 -1 5763.01 268.194 13 9 7 -1 6656.93 323.997 25 -9 7 0 451.665 87.1114 24 -9 7 -1 1130.42 113.396 24 9 8 -2 5182.27 257.598 25 9 8 -1 6391.55 299.851 25 10 -4 -3 769.352 109.144 17 10 -4 -2 5187.64 232.555 17 10 -4 -1 13561.7 450.508 26 10 -3 -3 130.454 82.1207 17 10 -3 -2 6179.82 265.219 17 10 -3 -2 5753.57 259.892 26 10 -3 -1 3897.85 220.635 26 10 -3 -1 3544.16 209.146 13 10 -3 0 3715.18 213.366 26 10 -3 0 3039.35 199.132 13 10 -2 -4 4082.51 223.345 17 10 -2 -3 19.3815 81.7353 17 10 -2 -2 558.125 100.250 17 10 -2 -2 459.802 97.5957 13 10 -2 -1 2161.11 167.323 26 10 -2 -1 2069.51 175.698 13 10 -2 0 5509.10 266.773 26 10 -2 0 5221.45 276.587 13 10 -1 -4 51.8848 82.1244 17 10 -1 -3 379.762 105.804 17 10 -1 -3 412.572 98.9273 13 10 -1 -2 124.830 84.7319 17 10 -1 -2 37.1089 82.7479 13 10 -1 -1 984.115 117.479 26 10 -1 -1 920.109 136.907 13 10 -1 0 2315.97 170.443 26 10 -1 0 2356.17 194.490 13 10 0 -4 1485.27 137.673 13 10 0 -3 432.506 106.963 17 10 0 -3 530.116 108.957 13 10 0 -2 3255.93 229.240 13 10 0 -1 202.924 104.911 13 10 0 0 325.732 82.1109 26 10 0 0 24.0981 97.1786 13 10 0 1 763.816 103.395 26 10 0 1 644.202 111.864 13 10 1 -4 128.439 86.3465 13 10 1 -3 542.986 118.941 13 10 1 -2 143.031 102.292 13 10 1 -1 847.018 136.937 13 10 1 0 2456.62 198.845 13 10 2 -4 4176.68 229.232 13 10 2 -3 170.695 97.8687 13 10 2 -2 564.715 123.819 13 10 2 -1 2321.01 200.891 13 10 2 0 5685.42 290.959 13 10 3 -3 301.177 101.396 13 10 3 -2 7370.74 332.940 13 10 3 -1 4421.86 251.042 13 10 3 0 3697.69 220.742 13 10 4 -3 818.292 127.057 13 10 4 -2 5865.37 279.059 13 10 4 -1 14981.6 487.724 13 0 0 0 0.00 0.00 0 TITL ijsf1488 in P2(1) REM P2(1) (#4 in standard setting) CELL 1.54184 8.715158 13.590209 8.762498 90.0000 100.5067 90.0000 ZERR 2.00 0.000279 0.000402 0.000300 0.0000 0.0032 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 46.00 52.00 4.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 15206 _shelx_shelxl_version_number 2014/7 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O1 O 0.8915(2) 0.49378(13) 0.0911(2) 0.0299(4) Uani 1 1 d . O2 O 0.7414(2) 0.35849(15) 0.0807(2) 0.0330(4) Uani 1 1 d . O3 O 0.6999(2) 0.48984(12) 0.58359(19) 0.0271(4) Uani 1 1 d . N1 N 1.1348(2) 0.17033(15) 0.3626(2) 0.0240(4) Uani 1 1 d . N2 N 0.6949(2) 0.39138(14) 0.3763(2) 0.0220(4) Uani 1 1 d . C1 C 1.2179(3) 0.22227(16) 0.2714(3) 0.0219(5) Uani 1 1 d . C2 C 1.3355(3) 0.19165(18) 0.1927(3) 0.0249(5) Uani 1 1 d . H2A H 1.3677 0.1263 0.1951 0.030 Uiso 1 1 calc R C3 C 1.4021(3) 0.26178(19) 0.1115(3) 0.0271(5) Uani 1 1 d . H3 H 1.4808 0.2434 0.0584 0.032 Uiso 1 1 calc R C4 C 1.3531(3) 0.36059(19) 0.1074(3) 0.0262(5) Uani 1 1 d . H4 H 1.3994 0.4061 0.0507 0.031 Uiso 1 1 calc R C5 C 1.2380(3) 0.39120(17) 0.1857(3) 0.0250(5) Uani 1 1 d . H5 H 1.2065 0.4567 0.1819 0.030 Uiso 1 1 calc R C6 C 1.1689(3) 0.32194(17) 0.2714(3) 0.0218(5) Uani 1 1 d . C7 C 1.0556(3) 0.32722(17) 0.3707(3) 0.0212(5) Uani 1 1 d . C8 C 1.0376(3) 0.23320(16) 0.4238(3) 0.0212(5) Uani 1 1 d . C9 C 0.9824(3) 0.42113(17) 0.4142(3) 0.0222(4) Uani 1 1 d . H9A H 1.0516 0.4752 0.4015 0.027 Uiso 1 1 calc R H9B H 0.9761 0.4177 0.5235 0.027 Uiso 1 1 calc R C10 C 0.8174(3) 0.44591(16) 0.3217(3) 0.0228(5) Uani 1 1 d . H10 H 0.7984 0.5162 0.3350 0.027 Uiso 1 1 calc R C11 C 0.8093(3) 0.42656(18) 0.1515(3) 0.0242(5) Uani 1 1 d . C12 C 0.9274(3) 0.19697(16) 0.5216(3) 0.0218(5) Uani 1 1 d . C13 C 0.7910(3) 0.14776(16) 0.4507(3) 0.0231(5) Uani 1 1 d . C14 C 0.6796(3) 0.12331(16) 0.5389(3) 0.0253(5) Uani 1 1 d . H14 H 0.5887 0.0916 0.4917 0.030 Uiso 1 1 calc R C15 C 0.7010(3) 0.14529(17) 0.6964(3) 0.0276(5) Uani 1 1 d . C16 C 0.8397(3) 0.18912(18) 0.7666(3) 0.0286(5) Uani 1 1 d . H16 H 0.8566 0.2017 0.8726 0.034 Uiso 1 1 calc R C17 C 0.9545(3) 0.21486(17) 0.6815(3) 0.0258(5) Uani 1 1 d . C18 C 0.7647(3) 0.12122(19) 0.2805(3) 0.0276(5) Uani 1 1 d . H18A H 0.7853 0.1776 0.2213 0.041 Uiso 1 1 calc GR H18B H 0.6585 0.1006 0.2472 0.041 Uiso 1 1 calc GR H18C H 0.8336 0.0686 0.2647 0.041 Uiso 1 1 calc GR C19 C 0.5732(3) 0.1231(2) 0.7869(3) 0.0373(6) Uani 1 1 d . H19A H 0.4980 0.1754 0.7724 0.056 Uiso 1 1 calc GR H19B H 0.6175 0.1173 0.8952 0.056 Uiso 1 1 calc GR H19C H 0.5229 0.0624 0.7507 0.056 Uiso 1 1 calc GR C20 C 1.1056(3) 0.2592(2) 0.7626(3) 0.0346(6) Uani 1 1 d . H20A H 1.1915 0.2229 0.7361 0.052 Uiso 1 1 calc GR H20B H 1.1103 0.2567 0.8729 0.052 Uiso 1 1 calc GR H20C H 1.1116 0.3265 0.7307 0.052 Uiso 1 1 calc GR C21 C 0.9065(3) 0.4785(2) -0.0686(3) 0.0372(6) Uani 1 1 d . H21A H 0.8046 0.4721 -0.1316 0.056 Uiso 1 1 calc GR H21B H 0.9654 0.4196 -0.0764 0.056 Uiso 1 1 calc GR H21C H 0.9593 0.5337 -0.1039 0.056 Uiso 1 1 calc GR C22 C 0.6426(3) 0.41883(16) 0.5040(3) 0.0214(4) Uani 1 1 d . C23 C 0.5099(3) 0.36184(18) 0.5480(3) 0.0265(5) Uani 1 1 d . H23A H 0.5353 0.3437 0.6555 0.040 Uiso 1 1 calc GR H23B H 0.4918 0.3035 0.4854 0.040 Uiso 1 1 calc GR H23C H 0.4174 0.4018 0.5311 0.040 Uiso 1 1 calc GR H2 H 0.651(4) 0.347(3) 0.320(4) 0.040(9) Uiso 1 1 d . H1 H 1.155(4) 0.115(3) 0.394(4) 0.034(8) Uiso 1 1 d . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0335(9) 0.0259(9) 0.0311(9) 0.0054(7) 0.0081(7) 0.0012(7) O2 0.0336(9) 0.0333(10) 0.0327(9) -0.0059(8) 0.0077(7) -0.0062(8) O3 0.0313(9) 0.0203(8) 0.0303(8) -0.0047(7) 0.0074(7) -0.0044(7) N1 0.0230(10) 0.0152(10) 0.0338(11) 0.0002(8) 0.0050(8) 0.0021(7) N2 0.0207(9) 0.0151(9) 0.0301(10) -0.0023(8) 0.0039(8) -0.0007(7) C1 0.0177(10) 0.0191(11) 0.0279(11) -0.0022(9) 0.0015(9) -0.0004(8) C2 0.0209(11) 0.0212(11) 0.0321(12) -0.0037(9) 0.0031(9) 0.0019(9) C3 0.0225(11) 0.0294(13) 0.0297(12) -0.0072(10) 0.0058(9) -0.0016(9) C4 0.0236(11) 0.0246(12) 0.0303(11) -0.0013(9) 0.0048(9) -0.0050(9) C5 0.0233(11) 0.0191(11) 0.0318(11) -0.0009(9) 0.0031(9) -0.0018(8) C6 0.0165(10) 0.0178(10) 0.0296(11) -0.0027(9) 0.0002(8) -0.0014(8) C7 0.0167(10) 0.0185(10) 0.0271(10) -0.0020(9) 0.0006(8) -0.0005(8) C8 0.0180(10) 0.0175(10) 0.0268(11) -0.0025(8) 0.0009(9) 0.0010(8) C9 0.0214(11) 0.0157(10) 0.0291(11) -0.0026(8) 0.0038(9) -0.0011(8) C10 0.0229(11) 0.0151(10) 0.0310(12) -0.0002(9) 0.0062(9) 0.0009(8) C11 0.0183(11) 0.0226(11) 0.0316(11) 0.0018(9) 0.0038(9) 0.0047(9) C12 0.0210(11) 0.0133(10) 0.0310(12) 0.0015(8) 0.0043(9) 0.0044(8) C13 0.0233(11) 0.0136(10) 0.0325(12) 0.0017(9) 0.0057(9) 0.0037(9) C14 0.0246(11) 0.0129(10) 0.0388(13) 0.0015(9) 0.0067(9) 0.0003(8) C15 0.0315(12) 0.0155(10) 0.0382(13) 0.0040(9) 0.0126(10) 0.0064(9) C16 0.0391(14) 0.0215(11) 0.0258(11) 0.0023(9) 0.0073(10) 0.0072(10) C17 0.0277(12) 0.0180(11) 0.0306(12) 0.0000(9) 0.0021(9) 0.0056(9) C18 0.0238(12) 0.0251(11) 0.0335(12) -0.0031(10) 0.0041(9) -0.0020(9) C19 0.0406(14) 0.0286(13) 0.0482(15) 0.0035(11) 0.0227(12) 0.0052(11) C20 0.0352(14) 0.0329(14) 0.0336(13) -0.0041(11) 0.0004(11) 0.0007(11) C21 0.0405(15) 0.0406(15) 0.0327(13) 0.0095(12) 0.0122(11) 0.0081(12) C22 0.0212(11) 0.0145(10) 0.0275(11) 0.0013(9) 0.0022(8) 0.0027(9) C23 0.0258(12) 0.0204(11) 0.0338(12) 0.0016(10) 0.0067(9) -0.0001(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 0 0 -1 0.0328 -0.0010 -0.0018 -0.9995 -0.1689 0.0558 0.0187 0 0 1 0.0328 0.0010 0.0018 0.9995 0.1689 -0.0558 -0.0187 1 0 0 0.0709 1.0009 0.0013 -0.0015 0.0725 0.0636 0.1518 -1 0 0 0.0709 -1.0009 -0.0013 0.0015 -0.0725 -0.0636 -0.1518 0 -1 0 0.1242 -0.0005 -1.0000 0.0007 0.0260 0.0967 -0.0531 0 1 0 0.1242 0.0005 1.0000 -0.0007 -0.0260 -0.0967 0.0531 -5 0 -3 0.0466 -5.0073 -0.0121 -2.9908 -0.8692 -0.1506 -0.7028 -6 0 2 0.0653 -6.0033 -0.0042 2.0082 -0.0972 -0.4930 -0.9481 5 -3 -2 0.0881 5.0010 -2.9970 -2.0046 0.1028 0.7195 0.6371 -5 3 2 0.0881 -5.0010 2.9970 2.0046 -0.1028 -0.7195 -0.6371 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C11 O1 C21 116.0(2) C1 N1 C8 109.61(19) C1 N1 H1 125(2) C8 N1 H1 124(2) C10 N2 H2 117(2) C22 N2 C10 121.16(19) C22 N2 H2 121(2) N1 C1 C2 130.4(2) N1 C1 C6 107.5(2) C2 C1 C6 122.1(2) C1 C2 H2A 121.2 C3 C2 C1 117.6(2) C3 C2 H2A 121.2 C2 C3 H3 119.4 C2 C3 C4 121.2(2) C4 C3 H3 119.4 C3 C4 H4 119.3 C5 C4 C3 121.3(2) C5 C4 H4 119.3 C4 C5 H5 120.5 C4 C5 C6 119.0(2) C6 C5 H5 120.5 C1 C6 C7 106.8(2) C5 C6 C1 118.7(2) C5 C6 C7 134.5(2) C6 C7 C9 124.5(2) C8 C7 C6 107.0(2) C8 C7 C9 128.3(2) N1 C8 C12 121.8(2) C7 C8 N1 109.1(2) C7 C8 C12 129.0(2) C7 C9 H9A 108.2 C7 C9 H9B 108.2 C7 C9 C10 116.50(18) H9A C9 H9B 107.3 C10 C9 H9A 108.2 C10 C9 H9B 108.2 N2 C10 C9 112.61(18) N2 C10 H10 108.0 N2 C10 C11 109.47(19) C9 C10 H10 108.0 C11 C10 C9 110.55(18) C11 C10 H10 108.0 O1 C11 C10 110.1(2) O2 C11 O1 124.8(2) O2 C11 C10 125.0(2) C13 C12 C8 119.2(2) C17 C12 C8 120.8(2) C17 C12 C13 120.0(2) C12 C13 C18 120.9(2) C14 C13 C12 119.3(2) C14 C13 C18 119.8(2) C13 C14 H14 119.3 C13 C14 C15 121.3(2) C15 C14 H14 119.3 C14 C15 C19 120.0(2) C16 C15 C14 118.7(2) C16 C15 C19 121.3(2) C15 C16 H16 119.3 C15 C16 C17 121.5(2) C17 C16 H16 119.3 C12 C17 C20 121.1(2) C16 C17 C12 119.0(2) C16 C17 C20 119.9(2) C13 C18 H18A 109.5 C13 C18 H18B 109.5 C13 C18 H18C 109.5 H18A C18 H18B 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 C15 C19 H19A 109.5 C15 C19 H19B 109.5 C15 C19 H19C 109.5 H19A C19 H19B 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 C17 C20 H20A 109.5 C17 C20 H20B 109.5 C17 C20 H20C 109.5 H20A C20 H20B 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 O1 C21 H21A 109.5 O1 C21 H21B 109.5 O1 C21 H21C 109.5 H21A C21 H21B 109.5 H21A C21 H21C 109.5 H21B C21 H21C 109.5 O3 C22 N2 121.6(2) O3 C22 C23 120.5(2) N2 C22 C23 117.9(2) C22 C23 H23A 109.5 C22 C23 H23B 109.5 C22 C23 H23C 109.5 H23A C23 H23B 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C11 1.329(3) O1 C21 1.444(3) O2 C11 1.207(3) O3 C22 1.241(3) N1 C1 1.369(3) N1 C8 1.379(3) N1 H1 0.80(4) N2 C10 1.450(3) N2 C22 1.336(3) N2 H2 0.83(4) C1 C2 1.399(3) C1 C6 1.420(3) C2 H2A 0.9300 C2 C3 1.379(4) C3 H3 0.9300 C3 C4 1.407(4) C4 H4 0.9300 C4 C5 1.379(3) C5 H5 0.9300 C5 C6 1.406(3) C6 C7 1.432(3) C7 C8 1.379(3) C7 C9 1.507(3) C8 C12 1.483(3) C9 H9A 0.9700 C9 H9B 0.9700 C9 C10 1.553(3) C10 H10 0.9800 C10 C11 1.503(3) C12 C13 1.407(3) C12 C17 1.399(3) C13 C14 1.387(3) C13 C18 1.511(3) C14 H14 0.9300 C14 C15 1.391(4) C15 C16 1.386(4) C15 C19 1.511(3) C16 H16 0.9300 C16 C17 1.397(4) C17 C20 1.504(4) C18 H18A 0.9600 C18 H18B 0.9600 C18 H18C 0.9600 C19 H19A 0.9600 C19 H19B 0.9600 C19 H19C 0.9600 C20 H20A 0.9600 C20 H20B 0.9600 C20 H20C 0.9600 C21 H21A 0.9600 C21 H21B 0.9600 C21 H21C 0.9600 C22 C23 1.500(3) C23 H23A 0.9600 C23 H23B 0.9600 C23 H23C 0.9600 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N2 H2 O2 0.83(4) 2.37(3) 2.730(3) 107(3) . N1 H1 O3 0.80(4) 2.11(4) 2.840(3) 151(3) 2_746 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion N1 C1 C2 C3 -178.4(2) N1 C1 C6 C5 179.7(2) N1 C1 C6 C7 1.5(2) N1 C8 C12 C13 -74.9(3) N1 C8 C12 C17 107.8(3) N2 C10 C11 O1 163.90(17) N2 C10 C11 O2 -17.9(3) C1 N1 C8 C7 0.7(3) C1 N1 C8 C12 177.0(2) C1 C2 C3 C4 -0.2(4) C1 C6 C7 C8 -1.1(3) C1 C6 C7 C9 174.9(2) C2 C1 C6 C5 1.9(3) C2 C1 C6 C7 -176.3(2) C2 C3 C4 C5 0.7(4) C3 C4 C5 C6 0.2(4) C4 C5 C6 C1 -1.4(3) C4 C5 C6 C7 176.2(2) C5 C6 C7 C8 -178.9(3) C5 C6 C7 C9 -2.9(4) C6 C1 C2 C3 -1.1(3) C6 C7 C8 N1 0.3(3) C6 C7 C8 C12 -175.7(2) C6 C7 C9 C10 99.1(3) C7 C8 C12 C13 100.6(3) C7 C8 C12 C17 -76.7(3) C7 C9 C10 N2 79.6(2) C7 C9 C10 C11 -43.2(3) C8 N1 C1 C2 176.2(2) C8 N1 C1 C6 -1.4(3) C8 C7 C9 C10 -85.8(3) C8 C12 C13 C14 -172.99(19) C8 C12 C13 C18 7.1(3) C8 C12 C17 C16 173.0(2) C8 C12 C17 C20 -8.2(3) C9 C7 C8 N1 -175.5(2) C9 C7 C8 C12 8.6(4) C9 C10 C11 O1 -71.5(2) C9 C10 C11 O2 106.7(3) C10 N2 C22 O3 -2.4(3) C10 N2 C22 C23 176.8(2) C12 C13 C14 C15 -0.9(3) C13 C12 C17 C16 -4.2(3) C13 C12 C17 C20 174.6(2) C13 C14 C15 C16 -2.5(3) C13 C14 C15 C19 176.4(2) C14 C15 C16 C17 2.5(4) C15 C16 C17 C12 0.8(3) C15 C16 C17 C20 -178.0(2) C17 C12 C13 C14 4.3(3) C17 C12 C13 C18 -175.6(2) C18 C13 C14 C15 179.0(2) C19 C15 C16 C17 -176.3(2) C21 O1 C11 O2 -4.1(3) C21 O1 C11 C10 174.2(2) C22 N2 C10 C9 79.0(2) C22 N2 C10 C11 -157.6(2)