#------------------------------------------------------------------------------ #$Date: 2021-05-26 00:34:25 +0300 (Wed, 26 May 2021) $ #$Revision: 265486 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/87/4518740.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4518740 loop_ _publ_author_name 'Das, Riyanka' 'Bej, Sourav' 'Hirani, Harish' 'Banerjee, Priyabrata' _publ_section_title ; Trace-Level Humidity Sensing from Commercial Organic Solvents and Food Products by an AIE/ESIPT-Triggered Piezochromic Luminogen and ppb-Level “OFF--ON--OFF” Sensing of Cu2+: A Combined Experimental and Theoretical Outcome ; _journal_name_full 'ACS Omega' _journal_paper_doi 10.1021/acsomega.1c00565 _journal_year 2021 _chemical_formula_moiety '2(C17 H13 N O2)' _chemical_formula_sum 'C34 H26 N2 O4' _chemical_formula_weight 526.57 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-03-30 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.617(2) _cell_length_b 21.565(7) _cell_length_c 13.651(4) _cell_measurement_reflns_used 1606 _cell_measurement_temperature 110(2) _cell_measurement_theta_max 24.81 _cell_measurement_theta_min 2.41 _cell_volume 2536.7(13) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 109.67 _diffrn_measured_fraction_theta_full 0.983 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1784 _diffrn_reflns_av_unetI/netI 0.0935 _diffrn_reflns_Laue_measured_fraction_full 0.983 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 22004 _diffrn_reflns_point_group_measured_fraction_full 0.983 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.117 _diffrn_reflns_theta_min 2.407 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.091 _exptl_absorpt_correction_T_max 0.7414 _exptl_absorpt_correction_T_min 0.6098 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1373 before and 0.1040 after correction. The Ratio of minimum to maximum transmission is 0.8225. The \l/2 correction factor is Not present. ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.379 _exptl_crystal_description neddle _exptl_crystal_F_000 1104 _refine_diff_density_max 0.501 _refine_diff_density_min -0.376 _refine_diff_density_rms 0.077 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 182 _refine_ls_number_reflns 2260 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.055 _refine_ls_R_factor_all 0.1484 _refine_ls_R_factor_gt 0.0767 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0936P)^2^+1.7838P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1733 _refine_ls_wR_factor_ref 0.2189 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1255 _reflns_number_total 2260 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao1c00565_si_002.cif _cod_data_source_block NAP-1 _cod_database_code 4518740 _shelxl_version_number 2014-3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: C008(H008), C009(H009), C00A(H00A), C00B(H00B), C00E(H00E), C00F(H00F), C00G(H00G), C00H(H00H), C00I(H00I), C00J(H00J), C00K(H00K) 2.b Tetrahedral OH refined with riding coordinates: O001(H001) 2.c Idealised tetrahedral OH refined as rotating group: O002(H002) ; _shelx_res_file ; TITL mo_pbcmerirsm1261119_0ma_a.res in Pbca REM Old TITL mo_PBCMERIRSM1261119_0ma in Pbca #61 REM SHELXT solution in Pbca REM R1 0.196, Rweak 0.009, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C17 N O2 CELL 0.71073 8.6168 21.5653 13.6511 90 90 90 ZERR 4 0.0024 0.0068 0.0041 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 136 104 8 16 L.S. 4 0 0 PLAN 10 TEMP -163.48 BOND $H list 4 fmap 2 53 acta REM REM REM WGHT 0.093600 1.783800 FVAR 0.35004 O001 4 0.334752 0.670298 0.457683 11.00000 0.03219 0.03803 = 0.03270 -0.00357 0.00205 -0.00239 AFIX 83 H001 2 0.417879 0.681348 0.430695 11.00000 -1.50000 AFIX 0 O002 4 0.648850 0.776179 0.416347 11.00000 0.04753 0.04155 = 0.03475 -0.00317 -0.00627 -0.01057 AFIX 147 H002 2 0.710291 0.798425 0.448709 11.00000 -1.50000 AFIX 0 N003 3 0.466367 0.713052 0.300732 11.00000 0.02257 0.02311 = 0.03899 -0.00185 -0.00098 0.00364 C004 1 0.287822 0.628065 0.299238 11.00000 0.02160 0.02238 = 0.03435 -0.00312 -0.00224 0.00789 C005 1 0.560473 0.759058 0.256393 11.00000 0.02027 0.02589 = 0.03269 -0.00058 0.00002 0.00199 C006 1 0.208268 0.580759 0.241314 11.00000 0.02545 0.02883 = 0.03584 -0.00098 -0.00518 0.00837 C007 1 0.653303 0.793281 0.320506 11.00000 0.02832 0.02440 = 0.03656 0.00150 -0.00028 0.00607 C008 1 0.387126 0.669968 0.253646 11.00000 0.02591 0.02728 = 0.02894 -0.00174 -0.00350 0.00617 AFIX 43 H008 2 0.398575 0.667422 0.184548 11.00000 -1.20000 AFIX 0 C009 1 0.562796 0.771760 0.157093 11.00000 0.02934 0.03051 = 0.03758 -0.00161 -0.00266 0.00116 AFIX 43 H009 2 0.501479 0.747750 0.113430 11.00000 -1.20000 AFIX 0 C00A 1 0.742810 0.842205 0.284362 11.00000 0.03098 0.02253 = 0.04298 -0.00377 -0.00049 0.00421 AFIX 43 H00A 2 0.803478 0.866676 0.327745 11.00000 -1.20000 AFIX 0 C00B 1 0.742545 0.854761 0.185268 11.00000 0.03184 0.02434 = 0.05021 0.00463 0.00386 -0.00075 AFIX 43 H00B 2 0.803463 0.887995 0.160609 11.00000 -1.20000 AFIX 0 C00C 1 0.112269 0.537483 0.289830 11.00000 0.03158 0.02413 = 0.04574 0.00424 -0.01011 0.00454 C00D 1 0.265845 0.630166 0.403568 11.00000 0.02886 0.02468 = 0.03735 -0.00124 -0.00225 0.00062 C00E 1 0.654238 0.819362 0.121209 11.00000 0.03707 0.03473 = 0.03861 0.00383 -0.00189 0.00259 AFIX 43 H00E 2 0.656571 0.827792 0.052919 11.00000 -1.20000 AFIX 0 C00F 1 0.161619 0.586043 0.446635 11.00000 0.03865 0.03933 = 0.03453 0.00567 0.00184 0.00087 AFIX 43 H00F 2 0.141334 0.587776 0.514984 11.00000 -1.20000 AFIX 0 C00G 1 0.092060 0.542214 0.391812 11.00000 0.03478 0.03521 = 0.04718 0.00807 -0.00300 -0.00372 AFIX 43 H00G 2 0.026235 0.513116 0.423489 11.00000 -1.20000 AFIX 0 C00H 1 0.221226 0.575583 0.139322 11.00000 0.03427 0.03767 = 0.03920 -0.00617 -0.00217 0.00177 AFIX 43 H00H 2 0.281306 0.605083 0.104207 11.00000 -1.20000 AFIX 0 C00I 1 0.037973 0.490177 0.236528 11.00000 0.04256 0.02558 = 0.05794 0.00261 -0.01687 -0.00194 AFIX 43 H00I 2 -0.027068 0.461431 0.269624 11.00000 -1.20000 AFIX 0 C00J 1 0.058499 0.485231 0.137818 11.00000 0.04826 0.03172 = 0.06267 -0.01122 -0.02470 0.00341 AFIX 43 H00J 2 0.011304 0.452241 0.102612 11.00000 -1.20000 AFIX 0 C00K 1 0.148508 0.528563 0.089222 11.00000 0.04865 0.03973 = 0.04915 -0.01347 -0.01302 0.00536 AFIX 43 H00K 2 0.160213 0.525764 0.020165 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_pbcmerirsm1261119_0ma_a.res in Pbca REM R1 = 0.0767 for 1255 Fo > 4sig(Fo) and 0.1484 for all 2260 data REM 182 parameters refined using 0 restraints END WGHT 0.0936 1.7838 REM Highest difference peak 0.501, deepest hole -0.376, 1-sigma level 0.077 Q1 1 0.4548 0.7173 0.3805 11.00000 0.05 0.50 Q2 1 0.3295 0.5364 0.1763 11.00000 0.05 0.24 Q3 1 0.0950 0.4440 0.4578 11.00000 0.05 0.23 Q4 1 -0.0072 0.4644 0.0389 11.00000 0.05 0.22 Q5 1 0.5397 0.6783 0.4737 11.00000 0.05 0.22 Q6 1 0.8183 0.8166 0.2259 11.00000 0.05 0.22 Q7 1 -0.0516 0.5353 0.1120 11.00000 0.05 0.22 Q8 1 0.4942 0.7672 0.4214 11.00000 0.05 0.21 Q9 1 0.4898 0.7581 0.0807 11.00000 0.05 0.21 Q10 1 0.9490 0.8632 0.0780 11.00000 0.05 0.21 ; _shelx_res_checksum 25644 _shelx_hkl_file ; 1 0 0 0.60 1.50 1 0 0 1.90 1.80 1 0 0 0.70 2.40 -1 0 0 -2.00 1.10 -1 0 0 -0.40 1.50 -1 0 0 0.30 1.30 -2 0 0 1577.74 142.29 -2 0 0 1519.55 142.09 -2 0 0 1559.44 144.49 2 0 0 1569.44 144.49 3 0 0 -1.80 3.00 3 0 0 -3.70 4.60 -3 0 0 0.60 2.90 -3 0 0 -2.00 2.70 -3 0 0 -0.60 3.90 -4 0 0 54.69 10.40 -4 0 0 39.00 12.00 -4 0 0 53.99 10.30 4 0 0 44.80 13.40 4 0 0 45.90 10.50 -5 0 0 -3.80 3.70 5 0 0 13.20 8.40 5 0 0 -2.50 2.90 -5 0 0 2.30 7.50 -5 0 0 9.10 5.80 -6 0 0 10.60 5.90 -6 0 0 8.20 6.50 6 0 0 0.70 5.90 6 0 0 5.50 11.30 -6 0 0 6.10 6.90 -7 0 0 7.00 7.00 -7 0 0 8.90 6.80 7 0 0 -10.70 6.60 7 0 0 5.80 11.40 -8 0 0 -2.90 6.10 -8 0 0 10.40 8.10 8 0 0 -2.00 9.10 9 0 0 12.20 13.70 10 0 0 129.59 37.30 -10 0 0 143.69 21.90 -10 0 0 163.08 28.90 1 0 1 -0.50 1.70 1 0 -1 1.70 3.10 -1 0 1 -0.60 1.40 -1 0 1 -0.30 1.70 1 0 -1 -1.50 1.40 -1 0 1 -1.50 2.10 1 0 1 -0.50 2.00 -1 0 -1 4.00 2.10 -1 0 -1 -1.20 1.90 -2 0 -1 0.60 3.60 -2 0 -1 -3.90 2.30 2 0 1 -1.80 4.10 -2 0 1 -4.20 2.80 -2 0 -1 -6.70 2.70 2 0 -1 -5.50 3.00 2 0 -1 3.50 5.90 -2 0 1 -3.60 4.50 2 0 1 -3.50 3.60 -3 0 1 3.70 3.50 -3 0 -1 6.10 4.40 3 0 1 -2.50 4.20 3 0 -1 -1.40 3.10 -3 0 -1 -1.60 3.40 -3 0 -1 -0.40 3.00 3 0 1 -3.10 4.50 3 0 -1 -6.60 3.80 -3 0 1 2.40 3.60 4 0 1 -0.60 4.90 -4 0 1 0.10 5.40 4 0 -1 -8.10 3.60 4 0 1 0.60 5.70 -4 0 1 0.70 4.20 -4 0 1 -5.90 2.90 4 0 -1 -1.90 5.80 -4 0 -1 -4.60 3.60 -4 0 -1 1.00 4.60 -4 0 -1 4.40 5.40 -5 0 1 -1.60 6.00 -5 0 1 1.70 4.20 -5 0 1 -6.30 3.10 5 0 -1 -0.80 5.00 -5 0 -1 -1.20 3.80 5 0 -1 -5.00 6.10 -5 0 -1 -3.10 4.80 5 0 1 -1.10 5.20 -5 0 -1 8.70 5.60 -6 0 -1 -3.20 4.80 -6 0 -1 -8.50 4.50 -6 0 1 -1.80 5.30 6 0 1 1.50 7.40 -6 0 1 14.00 9.10 -6 0 -1 -8.00 4.50 6 0 -1 -0.90 5.40 -7 0 1 -1.90 7.10 -7 0 1 -1.80 5.00 -7 0 -1 2.10 6.10 7 0 -1 -4.20 6.10 -7 0 -1 -3.00 7.30 7 0 1 -13.40 6.20 7 0 -1 -0.40 10.60 8 0 1 -0.20 7.90 -8 0 -1 6.20 7.00 8 0 -1 3.50 7.20 -8 0 1 1.90 6.70 8 0 -1 1.80 12.70 -8 0 1 -0.50 5.50 -8 0 -1 7.10 7.90 9 0 1 44.00 19.50 -9 0 -1 -13.00 6.60 -9 0 1 -3.60 6.50 9 0 -1 7.00 13.00 -9 0 -1 5.30 8.30 -9 0 -1 -10.90 11.80 10 0 1 4.70 15.70 -10 0 -1 8.90 9.70 10 0 -1 -16.20 11.80 -10 0 -1 -1.10 10.70 -10 0 1 24.40 8.50 0 0 -2 6129.89 483.15 0 0 2 4938.91 482.65 0 0 -2 5830.52 482.15 0 0 2 4502.15 481.95 1 0 2 194.88 20.80 -1 0 2 199.68 19.40 1 0 -2 177.88 21.10 1 0 2 190.08 18.70 -1 0 2 208.78 21.60 2 0 2 234.88 26.30 2 0 -2 251.87 27.90 -2 0 -2 237.48 22.20 2 0 2 218.08 26.00 -2 0 -2 270.47 25.40 2 0 -2 232.28 24.60 -3 0 -2 33.80 8.30 -3 0 2 39.70 11.40 3 0 2 27.10 8.90 -3 0 -2 32.10 7.90 -3 0 2 36.40 8.10 3 0 -2 22.50 6.90 3 0 2 24.90 8.40 -3 0 -2 32.40 8.00 3 0 -2 34.30 11.20 -4 0 -2 739.83 73.59 -4 0 -2 675.53 74.59 4 0 -2 820.32 79.29 -4 0 2 810.82 78.69 -4 0 2 727.23 72.39 4 0 -2 718.93 72.69 4 0 2 764.32 74.99 -4 0 -2 742.33 73.19 4 0 2 831.42 76.29 -5 0 2 100.99 14.00 5 0 2 113.49 21.20 -5 0 -2 113.49 21.10 5 0 -2 109.29 16.00 -5 0 -2 109.69 18.20 -5 0 -2 120.89 17.20 5 0 2 100.59 21.10 -5 0 2 111.39 15.50 -5 0 2 120.39 27.40 5 0 -2 129.09 25.00 -6 0 2 513.45 59.19 -6 0 -2 509.75 52.79 -6 0 2 479.35 49.10 -6 0 -2 479.75 56.29 6 0 -2 506.65 52.79 -6 0 2 503.45 51.59 6 0 2 473.35 56.49 -6 0 -2 493.95 52.59 6 0 -2 570.84 61.19 -7 0 2 14.00 7.80 -7 0 2 3.80 5.20 7 0 2 11.70 10.50 -7 0 -2 10.00 7.90 -7 0 -2 19.20 9.50 7 0 -2 -7.50 6.20 7 0 -2 -1.80 12.00 -7 0 -2 0.50 7.20 8 0 -2 -2.30 6.90 -8 0 -2 -0.80 7.20 -8 0 2 3.60 5.60 -8 0 -2 -3.90 9.00 -8 0 -2 0.60 6.80 8 0 -2 9.10 12.70 -8 0 2 -7.70 5.60 8 0 2 -7.60 8.50 -8 0 -2 6.10 9.90 9 0 2 -8.80 9.60 9 0 -2 23.50 10.50 -9 0 -2 -4.10 11.90 -9 0 2 1.80 6.50 -9 0 -2 3.90 7.80 9 0 -2 10.60 16.60 10 0 -2 27.60 19.30 -10 0 -2 -25.40 13.10 -10 0 -2 12.60 11.60 -10 0 -2 15.70 13.20 0 0 3 2.00 2.90 0 0 -3 -0.80 2.50 0 0 -3 -1.80 3.50 0 0 3 2.70 4.20 1 0 3 -6.20 3.10 -1 0 3 -4.00 3.20 1 0 -3 0.10 4.60 -1 0 -3 -6.10 4.60 1 0 -3 -3.40 4.10 -1 0 3 -0.60 4.10 2 0 -3 -0.70 3.20 2 0 3 -3.80 2.60 2 0 3 -2.80 4.00 -2 0 -3 1.20 5.00 2 0 -3 -3.80 4.50 -2 0 3 0.90 4.70 2 0 -3 1.80 4.20 -2 0 3 -1.70 2.80 3 0 3 3.90 4.80 -3 0 -3 -3.20 2.80 -3 0 -3 2.10 5.60 3 0 -3 2.30 4.10 -3 0 3 -0.80 2.80 -3 0 3 10.10 7.10 3 0 -3 6.50 6.70 3 0 3 6.80 5.80 -4 0 3 1.00 6.40 -4 0 -3 -2.40 4.10 4 0 -3 -6.70 4.50 -4 0 -3 -2.90 2.00 4 0 3 7.00 5.80 -4 0 3 1.30 3.50 -4 0 -3 8.60 6.20 -4 0 3 1.20 3.90 4 0 3 5.30 5.50 4 0 -3 6.00 7.40 -4 0 -3 -4.10 3.60 5 0 -3 -2.80 6.90 -5 0 3 -8.20 5.80 5 0 3 -4.80 5.30 -5 0 -3 0.30 5.70 -5 0 -3 -2.50 5.50 -5 0 3 -5.20 3.40 -5 0 -3 5.30 5.80 5 0 -3 0.90 4.30 -5 0 3 -2.60 3.80 5 0 3 -3.10 7.20 -5 0 3 4.30 4.10 -6 0 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-3 0 4 103.09 20.00 3 0 -4 75.19 18.20 3 0 4 93.39 17.90 3 0 -4 79.09 14.80 -3 0 4 111.89 12.80 -3 0 -4 96.29 18.00 3 0 4 111.39 13.90 4 0 -4 33.70 13.70 -4 0 -4 26.30 8.50 4 0 4 24.90 8.40 -4 0 -4 41.70 10.70 -4 0 4 24.50 11.10 4 0 4 32.40 11.50 4 0 -4 22.10 8.00 -4 0 4 26.60 6.20 -5 0 4 72.39 18.00 5 0 -4 62.79 13.40 -5 0 4 58.69 9.50 -5 0 -4 60.49 8.00 5 0 4 57.39 13.90 5 0 4 75.99 18.20 -5 0 -4 54.59 13.00 -5 0 -4 70.59 15.90 -5 0 -4 64.89 7.70 5 0 -4 74.79 20.40 -6 0 -4 1.90 3.00 6 0 4 -0.90 7.10 6 0 4 19.20 15.00 -6 0 4 1.90 3.50 6 0 -4 -0.10 9.00 -6 0 4 -0.80 4.40 6 0 -4 1.50 6.40 -6 0 -4 -1.60 5.80 -6 0 -4 -4.30 5.80 7 0 -4 2.70 10.60 -7 0 -4 25.20 11.30 -7 0 -4 2.00 6.10 7 0 4 8.90 12.10 -7 0 -4 9.20 5.20 -7 0 -4 27.60 10.60 -7 0 4 2.40 4.10 7 0 4 2.00 12.90 7 0 -4 7.50 9.30 -8 0 -4 -3.90 7.60 8 0 -4 9.10 7.60 8 0 4 -7.60 8.30 8 0 -4 2.80 11.60 -8 0 -4 1.00 4.80 9 0 -4 -7.10 10.00 -9 0 -4 4.80 6.30 9 0 -4 -5.40 13.10 -9 0 -4 6.40 10.20 0 0 -5 2.40 3.60 0 0 5 6.90 5.20 0 0 -5 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131.49 17.60 -4 -3 8 83.49 22.10 -4 3 -8 135.59 26.80 4 3 8 133.79 17.70 4 3 -8 143.59 20.10 -4 3 8 146.99 20.30 4 3 -8 155.28 30.20 -4 -3 -8 91.49 22.10 5 -3 -8 35.20 15.00 -5 3 -8 47.00 16.30 5 3 8 45.50 11.80 5 -3 -8 21.00 14.90 -5 3 8 18.10 10.70 -5 -3 -8 31.70 16.60 5 3 -8 58.59 19.60 5 3 -8 54.89 14.30 6 -3 -8 -4.50 11.00 -6 3 -8 -3.40 7.70 6 -3 -8 -6.10 9.30 6 3 8 -5.80 6.10 -6 -3 -8 -6.30 10.30 -6 3 8 -5.20 7.70 6 3 -8 1.30 11.80 7 -3 -8 20.10 12.40 7 3 8 16.10 9.10 -7 3 -8 5.40 12.40 7 -3 -8 14.30 17.10 -7 3 8 8.50 8.30 7 3 -8 37.70 18.00 -7 -3 -8 5.30 12.50 7 3 -8 5.80 9.20 -8 3 -8 49.50 19.60 8 -3 -8 22.20 15.30 8 3 8 55.89 15.80 8 -3 -8 55.59 23.80 -8 -3 -8 22.80 16.80 8 3 -8 79.99 29.10 -8 3 8 39.80 10.20 8 3 -8 33.90 15.40 0 -3 -9 -1.80 7.30 0 3 -9 -11.70 6.40 0 3 -9 4.40 4.50 0 -3 9 -3.70 6.50 0 3 9 9.20 6.00 0 -3 9 9.80 8.80 0 3 9 -1.70 7.20 -1 -3 9 9.40 8.00 1 -3 -9 -1.70 7.10 1 3 9 16.40 9.70 -1 -3 9 10.60 6.60 1 3 9 -4.30 4.20 -1 3 -9 10.40 9.10 -1 -3 -9 14.30 10.10 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5 10 8 10.40 6.70 -5 10 -8 3.60 5.60 -5 -10 -8 40.70 17.40 5 -10 8 14.00 7.80 5 10 -8 20.30 14.70 -5 10 8 12.50 11.70 5 10 -8 5.10 6.40 -6 10 -8 -1.10 5.60 6 -10 -8 35.40 15.90 -6 10 -8 16.60 13.50 -6 10 -8 21.20 12.10 6 10 8 4.20 11.60 6 10 -8 1.70 7.60 -6 -10 -8 74.99 21.30 6 10 -8 13.60 18.00 -6 10 8 7.00 11.20 7 10 8 4.80 11.30 7 -10 -8 1.90 13.40 -7 10 -8 -7.60 8.60 -7 10 -8 1.90 12.40 -7 10 -8 10.80 9.70 -7 -10 -8 15.40 15.60 7 10 -8 5.00 17.40 -7 10 8 0.10 11.40 7 10 -8 0.90 6.00 8 -10 -8 -21.70 11.40 -8 10 -8 -5.30 7.20 -8 10 -8 33.90 16.50 8 10 8 5.40 16.50 -8 -10 -8 -0.30 14.70 8 10 -8 9.70 19.30 -8 10 8 1.90 14.20 0 10 -9 666.93 70.29 0 10 9 711.03 67.89 0 -10 -9 491.35 72.49 0 -10 9 624.54 72.29 0 10 -9 645.94 65.99 1 -10 -9 264.47 38.10 1 -10 -9 203.48 34.00 1 10 9 226.78 28.00 -1 10 -9 144.89 22.80 -1 10 -9 184.68 30.70 -1 10 9 270.17 31.40 1 10 -9 196.18 28.70 -1 10 9 158.68 31.20 -1 -10 -9 140.59 35.20 1 10 -9 188.28 27.70 1 -10 9 201.98 29.70 2 -10 -9 2.30 9.30 -2 10 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20.50 16.20 7 10 -9 17.70 8.80 7 10 -9 3.50 22.20 -7 -10 -9 9.00 16.40 -7 10 9 22.90 15.80 0 10 -10 54.09 17.00 0 10 -10 34.30 11.50 0 -10 -10 2.50 15.60 0 10 10 10.80 9.80 0 10 10 7.80 10.50 -1 10 -10 4.30 5.90 1 -10 -10 -0.50 11.00 1 -10 -10 8.50 16.60 -1 10 -10 -2.60 8.40 1 10 10 7.50 8.20 1 10 -10 15.50 11.80 1 10 -10 7.30 9.60 -1 10 10 9.90 10.30 -1 -10 -10 23.00 18.60 1 -10 10 1.80 10.00 2 10 10 49.50 12.90 2 -10 -10 31.00 16.30 -2 10 -10 53.19 17.70 2 10 -10 38.80 14.70 2 -10 10 32.50 14.40 -2 10 10 72.79 18.50 -2 -10 -10 49.70 21.40 2 10 -10 45.40 17.30 3 -10 -10 40.90 17.20 3 10 10 35.60 10.70 -3 10 -10 40.10 17.20 3 10 -10 21.40 10.70 -3 -10 -10 15.10 16.00 -3 10 10 4.70 10.50 3 10 -10 28.50 14.60 4 10 10 8.50 6.10 4 -10 -10 8.30 9.20 -4 10 -10 8.00 11.70 4 -10 10 16.20 9.10 -4 10 10 19.70 9.80 4 10 -10 10.40 8.20 4 10 -10 -0.30 12.10 -4 -10 -10 19.30 15.60 5 -10 -10 6.40 11.50 5 10 10 3.30 6.70 5 10 -10 -6.90 11.10 -5 -10 -10 -2.10 14.60 5 10 -10 13.60 7.60 5 -10 10 -5.90 7.00 6 -10 -10 -12.80 9.70 -6 10 -10 36.60 16.60 6 10 10 13.80 13.10 6 10 -10 25.80 10.80 -6 -10 -10 10.30 19.20 -6 10 10 -0.70 10.70 7 10 10 3.10 13.80 7 -10 -10 -15.20 13.60 -7 10 -10 13.90 13.80 -7 10 10 14.70 14.70 -7 -10 -10 -15.70 15.90 7 10 -10 -11.30 7.90 7 10 -10 12.50 15.40 0 10 11 706.23 77.79 0 10 -11 745.13 75.59 0 10 -11 782.42 82.49 1 -10 -11 34.90 15.10 -1 10 -11 12.90 6.70 1 10 11 15.80 9.50 1 10 11 -6.40 10.20 1 -10 -11 67.19 21.60 -1 10 -11 13.70 11.50 1 10 -11 4.70 9.90 -1 -10 -11 -9.60 11.40 1 10 -11 24.40 10.70 2 -10 -11 -7.70 15.30 2 -10 -11 -0.40 9.70 -2 10 -11 -4.70 8.60 2 10 -11 -9.50 6.10 2 10 -11 -10.10 7.50 -2 10 11 6.20 10.30 -2 -10 -11 -14.80 11.00 2 -10 11 -4.00 10.40 -3 10 -11 14.50 12.40 3 10 11 3.20 6.80 3 -10 -11 14.10 13.20 3 10 -11 -10.50 9.70 -3 10 11 10.30 9.80 3 10 -11 12.10 11.00 -3 -10 -11 13.00 15.90 3 -10 11 0.30 10.10 4 -10 -11 -2.20 11.30 4 10 11 -12.30 5.40 -4 -10 -11 26.20 17.20 4 10 -11 6.90 7.80 -4 10 11 5.70 10.10 4 10 -11 -8.10 11.20 4 -10 11 3.20 8.30 5 10 11 31.80 8.90 5 -10 -11 4.60 13.00 -5 10 -11 24.10 13.30 -5 10 11 33.40 16.10 5 10 -11 23.00 19.90 5 10 -11 18.40 10.10 -5 -10 -11 39.30 22.90 5 -10 11 40.60 10.20 6 -10 -11 10.40 15.90 6 10 11 14.90 12.50 -6 10 -11 7.10 12.60 6 10 -11 28.50 21.70 -6 10 11 26.20 14.30 6 10 -11 5.40 9.00 -6 -10 -11 20.70 18.70 0 10 12 2.00 10.00 0 10 -12 14.00 12.80 0 -10 -12 22.70 18.70 0 10 -12 6.20 7.00 1 -10 -12 34.30 21.90 1 10 12 34.20 15.10 -1 10 -12 39.40 16.90 -1 10 -12 45.30 9.30 1 10 12 34.60 12.50 -1 10 12 47.30 16.30 1 10 -12 38.70 13.20 -1 -10 -12 42.30 21.20 1 10 -12 29.20 15.10 -2 10 -12 26.90 15.60 2 -10 -12 9.20 17.80 2 10 12 20.10 12.90 2 10 12 24.10 11.10 2 -10 -12 21.30 14.60 -2 -10 -12 6.40 15.40 -2 10 12 7.90 10.80 2 10 -12 6.40 10.20 2 10 -12 59.39 17.90 3 -10 -12 6.00 13.40 3 10 12 18.20 9.40 -3 10 12 2.10 12.80 3 10 -12 -9.10 7.30 3 10 -12 1.30 9.30 3 -10 12 -13.20 10.20 4 10 12 9.90 6.90 4 -10 -12 8.30 13.70 -4 10 -12 19.10 15.00 4 10 -12 -12.90 11.40 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8.80 3 23 -5 8.80 9.60 3 23 -5 11.50 14.80 0 23 6 -14.60 11.30 0 23 -6 -25.70 14.30 0 23 -6 -41.40 16.10 0 -23 -6 9.20 12.40 -1 23 -6 11.50 15.20 -1 23 -6 3.10 18.00 1 23 6 1.40 11.20 1 23 -6 -9.30 13.30 1 23 -6 -5.90 14.90 -1 23 6 -9.20 11.40 -1 -23 -6 7.80 10.60 2 23 6 -20.20 11.70 2 -23 -6 13.70 13.50 -2 23 -6 -0.90 16.70 -2 23 -6 27.80 22.30 2 23 -6 11.10 15.00 -2 23 6 15.90 15.80 2 23 -6 -12.00 14.50 -2 -23 -6 4.90 11.10 2 23 -6 -8.80 15.20 0 23 -7 -15.20 14.60 0 23 -7 3.10 16.10 0 23 7 -12.50 14.00 1 -23 -7 15.40 13.60 -1 23 -7 -3.40 15.70 -1 23 -7 42.40 21.50 1 23 7 9.50 15.10 1 23 -7 1.40 16.30 1 23 -7 43.50 20.40 -1 23 7 15.00 15.80 -1 -23 -7 -1.10 11.40 0 -24 0 240.28 35.00 0 24 0 236.58 45.40 -1 24 0 -12.50 13.70 1 -24 0 5.00 11.50 1 24 0 -10.40 14.60 -1 -24 0 -11.60 8.70 -2 -24 0 30.30 13.60 -2 24 0 -5.30 11.70 2 -24 0 2.30 13.70 2 24 0 23.10 19.50 3 24 0 41.60 23.60 3 -24 0 6.10 13.50 -3 24 0 -12.60 12.70 0 -24 -1 5.10 13.20 0 24 -1 -19.30 11.60 0 24 1 -11.80 15.40 0 -24 1 5.00 12.50 -1 24 -1 26.10 19.60 -1 -24 1 34.80 13.60 1 -24 -1 13.80 16.70 1 24 1 9.80 15.50 1 -24 1 25.50 15.60 -1 -24 -1 24.60 15.50 -1 24 1 16.00 15.40 1 24 -1 59.09 25.80 2 -24 -1 56.49 21.90 -2 24 -1 10.40 14.80 2 24 1 -30.30 10.70 2 -24 1 1.00 12.90 -2 -24 -1 -2.00 8.70 -2 24 1 -6.10 12.00 2 24 -1 -17.60 12.50 3 24 1 9.00 15.10 -3 24 -1 8.10 13.60 3 -24 -1 -6.60 12.20 -3 -24 -1 -0.80 8.20 3 -24 1 -4.60 13.00 -3 24 1 -9.10 12.30 3 24 -1 4.50 15.80 0 24 2 42.10 19.30 0 -24 -2 47.10 18.40 0 24 -2 52.99 24.40 1 -24 -2 -17.50 13.30 1 24 2 11.20 16.40 -1 24 -2 -6.20 13.80 1 24 -2 19.40 18.40 -1 24 2 2.80 10.80 -1 -24 -2 -11.70 11.70 1 -24 2 9.40 12.50 -2 24 -2 4.20 13.80 2 -24 2 -4.40 14.90 -2 -24 -2 -16.20 9.90 2 24 -2 26.30 19.10 -2 24 2 17.00 15.40 3 24 2 -11.00 21.00 3 -24 -2 13.00 15.90 -3 24 -2 -1.10 17.30 -3 24 2 -7.90 12.50 3 -24 2 41.60 19.70 3 24 -2 23.30 21.60 -3 -24 -2 31.20 12.90 0 24 -3 66.39 25.00 0 -24 -3 21.30 15.20 0 24 3 8.40 12.50 -1 24 -3 9.00 19.20 1 24 3 -9.80 13.80 1 -24 -3 6.20 12.80 -1 -24 -3 9.50 12.10 -1 24 3 11.60 13.20 1 24 -3 14.10 17.80 2 24 3 -15.90 16.10 2 -24 -3 -18.00 10.90 -2 24 -3 13.40 18.50 2 24 -3 -8.00 11.90 -2 24 3 -9.10 13.30 -2 -24 -3 3.00 8.60 2 24 -3 -32.00 16.20 3 24 3 25.10 19.40 3 -24 -3 -6.00 12.70 -3 24 -3 -9.70 15.30 3 24 -3 -13.20 13.30 -3 24 3 -19.30 12.00 -3 -24 -3 7.70 10.50 0 24 -4 119.69 34.40 0 -24 -4 103.29 25.80 0 24 4 127.09 28.20 1 -24 -4 70.79 20.30 1 24 4 31.70 22.20 -1 24 -4 69.19 27.00 1 24 -4 34.40 19.00 -1 -24 -4 46.70 17.10 -1 24 4 32.70 19.50 2 24 4 22.20 16.70 -2 24 -4 9.40 16.50 2 -24 -4 2.60 14.50 -2 24 4 -8.20 7.90 -2 -24 -4 -8.90 9.20 2 24 -4 9.30 16.60 2 24 -4 12.50 16.10 0 24 -5 43.10 27.60 0 24 5 16.40 17.90 0 -24 -5 50.79 18.80 0 24 -5 33.20 22.90 -1 24 -5 25.50 21.80 -1 24 -5 45.90 21.20 1 -24 -5 -11.00 15.60 1 24 5 15.40 20.40 -1 24 5 56.89 22.10 -1 -24 -5 39.70 16.00 1 24 -5 -0.10 17.80 -2 24 -5 1.10 18.90 2 24 -5 -7.70 14.10 0 -25 0 0.90 12.10 0 25 0 -24.00 13.10 -1 25 0 -22.00 12.30 1 -25 0 2.60 12.10 1 25 0 -0.80 18.80 -1 -25 0 -14.30 9.60 -2 -25 0 98.09 20.70 2 25 0 44.20 24.90 2 -25 0 96.19 26.30 -2 25 0 58.29 25.80 0 -25 -1 0.10 12.90 0 25 -1 -7.40 13.60 0 25 1 6.40 14.00 0 -25 1 -4.90 12.00 -1 25 -1 -8.10 12.80 1 -25 -1 17.80 16.50 1 25 1 36.30 21.10 1 25 -1 -9.10 14.30 -1 -25 -1 41.30 16.00 1 -25 1 4.20 12.40 -1 25 1 6.20 15.10 2 -25 -1 4.70 14.40 2 25 1 11.00 15.80 -2 25 -1 0.20 16.50 2 25 -1 34.90 22.00 -2 25 1 -3.90 13.30 -2 -25 -1 6.90 10.90 2 -25 1 20.20 19.70 0 25 -2 30.90 17.90 0 -25 -2 11.50 13.50 0 25 2 -4.60 17.30 -1 25 -2 -9.20 13.80 1 -25 -2 6.60 12.00 1 25 2 -1.40 13.60 -1 -25 -2 5.00 12.70 1 25 -2 1.20 16.30 -1 25 2 34.40 15.70 1 -25 2 2.80 13.70 2 25 2 -28.30 16.20 -2 25 -2 25.70 16.10 -2 25 2 5.10 11.40 2 25 -2 4.70 15.50 0 25 3 8.90 15.60 0 25 -3 11.70 16.10 1 -25 -3 38.90 19.70 1 25 3 0.50 16.70 -1 25 -3 46.20 29.00 1 25 -3 22.90 20.60 -1 25 3 42.50 17.50 -1 -25 -3 30.90 15.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 65835 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.3348(3) 0.67030(13) 0.4577(2) 0.0343(8) Uani 1 1 d . . . . . H001 H 0.4179 0.6813 0.4307 0.051 Uiso 1 1 calc R . . . . O002 O 0.6489(3) 0.77618(14) 0.4163(2) 0.0413(8) Uani 1 1 d . . . . . H002 H 0.7103 0.7984 0.4487 0.062 Uiso 1 1 calc GR . . . . N003 N 0.4664(3) 0.71305(15) 0.3007(2) 0.0282(8) Uani 1 1 d . . . . . C004 C 0.2878(4) 0.62807(17) 0.2992(3) 0.0261(10) Uani 1 1 d . . . . . C005 C 0.5605(4) 0.75906(17) 0.2564(3) 0.0263(10) Uani 1 1 d . . . . . C006 C 0.2083(4) 0.58076(18) 0.2413(3) 0.0300(10) Uani 1 1 d . . . . . C007 C 0.6533(4) 0.79328(18) 0.3205(3) 0.0298(10) Uani 1 1 d . . . . . C008 C 0.3871(4) 0.66997(17) 0.2536(3) 0.0274(10) Uani 1 1 d . . . . . H008 H 0.3986 0.6674 0.1845 0.033 Uiso 1 1 calc R . . . . C009 C 0.5628(4) 0.77176(19) 0.1571(3) 0.0325(10) Uani 1 1 d . . . . . H009 H 0.5015 0.7478 0.1134 0.039 Uiso 1 1 calc R . . . . C00A C 0.7428(5) 0.84221(18) 0.2844(3) 0.0322(10) Uani 1 1 d . . . . . H00A H 0.8035 0.8667 0.3277 0.039 Uiso 1 1 calc R . . . . C00B C 0.7425(5) 0.85476(19) 0.1853(3) 0.0355(11) Uani 1 1 d . . . . . H00B H 0.8035 0.8880 0.1606 0.043 Uiso 1 1 calc R . . . . C00C C 0.1123(5) 0.53748(19) 0.2898(3) 0.0338(11) Uani 1 1 d . . . . . C00D C 0.2658(4) 0.63017(18) 0.4036(3) 0.0303(10) Uani 1 1 d . . . . . C00E C 0.6542(4) 0.8194(2) 0.1212(3) 0.0368(11) Uani 1 1 d . . . . . H00E H 0.6566 0.8278 0.0529 0.044 Uiso 1 1 calc R . . . . C00F C 0.1616(5) 0.5860(2) 0.4466(3) 0.0375(11) Uani 1 1 d . . . . . H00F H 0.1413 0.5878 0.5150 0.045 Uiso 1 1 calc R . . . . C00G C 0.0921(5) 0.5422(2) 0.3918(3) 0.0391(12) Uani 1 1 d . . . . . H00G H 0.0262 0.5131 0.4235 0.047 Uiso 1 1 calc R . . . . C00H C 0.2212(5) 0.5756(2) 0.1393(3) 0.0370(11) Uani 1 1 d . . . . . H00H H 0.2813 0.6051 0.1042 0.044 Uiso 1 1 calc R . . . . C00I C 0.0380(5) 0.49018(19) 0.2365(4) 0.0420(12) Uani 1 1 d . . . . . H00I H -0.0271 0.4614 0.2696 0.050 Uiso 1 1 calc R . . . . C00J C 0.0585(5) 0.4852(2) 0.1378(4) 0.0475(13) Uani 1 1 d . . . . . H00J H 0.0113 0.4522 0.1026 0.057 Uiso 1 1 calc R . . . . C00K C 0.1485(5) 0.5286(2) 0.0892(4) 0.0458(12) Uani 1 1 d . . . . . H00K H 0.1602 0.5258 0.0202 0.055 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0322(15) 0.0380(18) 0.0327(17) -0.0036(14) 0.0020(13) -0.0024(13) O002 0.0475(19) 0.042(2) 0.0347(18) -0.0032(15) -0.0063(14) -0.0106(14) N003 0.0226(17) 0.0231(19) 0.039(2) -0.0018(16) -0.0010(15) 0.0036(14) C004 0.022(2) 0.022(2) 0.034(3) -0.0031(17) -0.0022(18) 0.0079(17) C005 0.020(2) 0.026(2) 0.033(2) -0.0006(19) 0.0000(17) 0.0020(17) C006 0.025(2) 0.029(2) 0.036(3) -0.001(2) -0.0052(18) 0.0084(18) C007 0.028(2) 0.024(2) 0.037(3) 0.0015(19) -0.0003(19) 0.0061(18) C008 0.026(2) 0.027(2) 0.029(2) -0.0017(19) -0.0035(18) 0.0062(18) C009 0.029(2) 0.031(3) 0.038(3) -0.002(2) -0.0027(19) 0.0012(19) C00A 0.031(2) 0.023(2) 0.043(3) -0.0038(19) 0.000(2) 0.0042(19) C00B 0.032(2) 0.024(2) 0.050(3) 0.005(2) 0.004(2) -0.0007(19) C00C 0.032(2) 0.024(2) 0.046(3) 0.004(2) -0.010(2) 0.0045(19) C00D 0.029(2) 0.025(2) 0.037(3) -0.0012(19) -0.0022(19) 0.0006(19) C00E 0.037(2) 0.035(3) 0.039(3) 0.004(2) -0.002(2) 0.003(2) C00F 0.039(2) 0.039(3) 0.035(3) 0.006(2) 0.002(2) 0.001(2) C00G 0.035(2) 0.035(3) 0.047(3) 0.008(2) -0.003(2) -0.004(2) C00H 0.034(2) 0.038(3) 0.039(3) -0.006(2) -0.002(2) 0.002(2) C00I 0.043(3) 0.026(2) 0.058(3) 0.003(2) -0.017(2) -0.002(2) C00J 0.048(3) 0.032(3) 0.063(4) -0.011(2) -0.025(2) 0.003(2) C00K 0.049(3) 0.040(3) 0.049(3) -0.013(2) -0.013(2) 0.005(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00D O001 H001 109.5 . . ? C007 O002 H002 109.5 . . ? C008 N003 C005 125.5(3) . . ? C008 C004 C006 120.0(4) . . ? C008 C004 C00D 120.2(4) . . ? C00D C004 C006 119.8(4) . . ? C007 C005 N003 115.5(4) . . ? C009 C005 N003 124.4(4) . . ? C009 C005 C007 120.1(4) . . ? C00C C006 C004 118.8(4) . . ? C00H C006 C004 123.8(4) . . ? C00H C006 C00C 117.4(4) . . ? O002 C007 C005 116.3(4) . . ? O002 C007 C00A 124.1(4) . . ? C005 C007 C00A 119.6(4) . . ? N003 C008 C004 123.9(4) . . ? N003 C008 H008 118.1 . . ? C004 C008 H008 118.1 . . ? C005 C009 H009 119.9 . . ? C005 C009 C00E 120.1(4) . . ? C00E C009 H009 119.9 . . ? C007 C00A H00A 120.2 . . ? C00B C00A C007 119.6(4) . . ? C00B C00A H00A 120.2 . . ? C00A C00B H00B 119.6 . . ? C00A C00B C00E 120.7(4) . . ? C00E C00B H00B 119.6 . . ? C00G C00C C006 119.3(4) . . ? C00G C00C C00I 120.5(4) . . ? C00I C00C C006 120.2(4) . . ? O001 C00D C004 122.0(4) . . ? O001 C00D C00F 120.1(4) . . ? C00F C00D C004 117.9(4) . . ? C009 C00E C00B 119.8(4) . . ? C009 C00E H00E 120.1 . . ? C00B C00E H00E 120.1 . . ? C00D C00F H00F 119.4 . . ? C00G C00F C00D 121.1(4) . . ? C00G C00F H00F 119.4 . . ? C00C C00G H00G 118.5 . . ? C00F C00G C00C 123.1(4) . . ? C00F C00G H00G 118.5 . . ? C006 C00H H00H 119.4 . . ? C00K C00H C006 121.1(4) . . ? C00K C00H H00H 119.4 . . ? C00C C00I H00I 119.7 . . ? C00J C00I C00C 120.6(4) . . ? C00J C00I H00I 119.7 . . ? C00I C00J H00J 120.2 . . ? C00I C00J C00K 119.6(4) . . ? C00K C00J H00J 120.2 . . ? C00H C00K C00J 121.0(5) . . ? C00H C00K H00K 119.5 . . ? C00J C00K H00K 119.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 H001 0.8400 . ? O001 C00D 1.283(4) . ? O002 H002 0.8400 . ? O002 C007 1.360(5) . ? N003 C005 1.417(5) . ? N003 C008 1.320(5) . ? C004 C006 1.461(5) . ? C004 C008 1.391(5) . ? C004 C00D 1.437(6) . ? C005 C007 1.397(5) . ? C005 C009 1.383(6) . ? C006 C00C 1.412(6) . ? C006 C00H 1.401(6) . ? C007 C00A 1.397(5) . ? C008 H008 0.9500 . ? C009 H009 0.9500 . ? C009 C00E 1.384(6) . ? C00A H00A 0.9500 . ? C00A C00B 1.380(6) . ? C00B H00B 0.9500 . ? C00B C00E 1.388(6) . ? C00C C00G 1.407(6) . ? C00C C00I 1.407(6) . ? C00D C00F 1.434(6) . ? C00E H00E 0.9500 . ? C00F H00F 0.9500 . ? C00F C00G 1.346(6) . ? C00G H00G 0.9500 . ? C00H H00H 0.9500 . ? C00H C00K 1.374(6) . ? C00I H00I 0.9500 . ? C00I C00J 1.363(7) . ? C00J H00J 0.9500 . ? C00J C00K 1.384(7) . ? C00K H00K 0.9500 . ?