#------------------------------------------------------------------------------ #$Date: 2021-06-03 22:10:51 +0300 (Thu, 03 Jun 2021) $ #$Revision: 265722 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/87/4518762.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4518762 loop_ _publ_author_name 'Britton, Luke' 'Skrodzki, Maciej' 'Nichol, Gary S.' 'Dominey, Andrew P.' 'Pawlu\'c, Piotr' 'Docherty, Jamie H.' 'Thomas, Stephen P.' _publ_section_title ; Manganese-Catalyzed C(sp2)--H Borylation of Furan and Thiophene Derivatives ; _journal_name_full 'ACS Catalysis' _journal_page_first 6857 _journal_page_last 6864 _journal_paper_doi 10.1021/acscatal.1c01563 _journal_year 2021 _chemical_formula_moiety 'C18 H46 B Mn O2 P4' _chemical_formula_sum 'C18 H46 B Mn O2 P4' _chemical_formula_weight 484.18 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _audit_creation_date 2021-01-15 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6226) ; _cell_angle_alpha 90 _cell_angle_beta 101.606(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.1864(3) _cell_length_b 20.8702(7) _cell_length_c 13.5759(5) _cell_measurement_reflns_used 11832 _cell_measurement_temperature 120.00(10) _cell_measurement_theta_max 29.4870 _cell_measurement_theta_min 3.6630 _cell_volume 2549.58(15) _computing_cell_refinement 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 120.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.1574 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.890 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 2.00 63.00 1.00 10.00 -- 10.76-120.00 135.00 61 2 \w 22.00 86.00 1.00 10.00 -- 10.76-155.00 -21.00 64 3 \w -41.00 21.00 1.00 10.00 -- -9.35 77.00 0.00 62 4 \w -41.00 21.00 1.00 10.00 -- -9.35 77.00 60.00 62 5 \w -40.00 22.00 1.00 10.00 -- -9.35 -77.00 0.00 62 6 \w -48.00 29.00 1.00 10.00 -- 10.76 -57.00 60.00 77 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Rigaku Oxford Diffraction SuperNova' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0099408000 _diffrn_orient_matrix_UB_12 -0.0336988000 _diffrn_orient_matrix_UB_13 -0.0002667000 _diffrn_orient_matrix_UB_21 0.0457480000 _diffrn_orient_matrix_UB_22 0.0016225000 _diffrn_orient_matrix_UB_23 0.0487393000 _diffrn_orient_matrix_UB_31 -0.0634174000 _diffrn_orient_matrix_UB_32 -0.0041027000 _diffrn_orient_matrix_UB_33 0.0216937000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0341 _diffrn_reflns_av_unetI/netI 0.0347 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.890 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 28518 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.890 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.655 _diffrn_reflns_theta_min 3.305 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.779 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.75261 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.61a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'light brown' _exptl_crystal_density_diffrn 1.261 _exptl_crystal_description plate _exptl_crystal_F_000 1040 _exptl_crystal_recrystallization_method 'The material was recrystallised from hexane by slow evaporation in the freezer.' _exptl_crystal_size_max 0.436 _exptl_crystal_size_mid 0.287 _exptl_crystal_size_min 0.099 _refine_diff_density_max 0.352 _refine_diff_density_min -0.253 _refine_diff_density_rms 0.058 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.058 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 419 _refine_ls_number_reflns 6424 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.058 _refine_ls_R_factor_all 0.0398 _refine_ls_R_factor_gt 0.0323 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0240P)^2^+1.0177P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0651 _refine_ls_wR_factor_ref 0.0684 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5585 _reflns_number_total 6424 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c01563_si_003.cif _cod_data_source_block se21001 _cod_database_code 4518762 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C18 H46 B1 Mn1 O2 P4' _chemical_oxdiff_usercomment '@ 120 K LAB181' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.70 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; ; _shelx_res_file ; TITL se21001_a.res in P2(1)/c se21001.res created by SHELXL-2018/3 at 10:07:30 on 15-Jan-2021 REM Old TITL SE21001_refinalized in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.082, Rweak 0.029, Alpha 0.036 REM 0.920 for 158 systematic absences, Orientation as input REM Formula found by SHELXT: C17 B2 O2 P4 Mn CELL 0.71073 9.1864 20.8702 13.5759 90 101.606 90 ZERR 4 0.0003 0.0007 0.0005 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H B Mn O P UNIT 72 184 4 4 8 16 L.S. 16 PLAN 5 CONF BOND list 4 fmap 2 MORE -1 BOND $H ACTA REM REM REM WGHT 0.024000 1.017700 FVAR 0.37381 MN1 4 0.356034 0.391152 0.291658 11.00000 0.01184 0.01010 = 0.01181 0.00033 0.00222 0.00004 H1C 2 0.207539 0.424534 0.242818 11.00000 0.02522 H1D 2 0.408809 0.464206 0.304760 11.00000 0.02211 P1 6 0.284013 0.392126 0.439251 11.00000 0.01419 0.01377 = 0.01292 0.00003 0.00322 -0.00168 P2 6 0.226867 0.301457 0.264635 11.00000 0.01637 0.01213 = 0.01362 0.00036 0.00101 -0.00171 P3 6 0.445969 0.388437 0.151157 11.00000 0.01656 0.01716 = 0.01354 -0.00073 0.00450 0.00010 P4 6 0.579422 0.353893 0.358510 11.00000 0.01348 0.01462 = 0.01596 0.00030 0.00238 0.00174 O1 5 0.212323 0.528212 0.310032 11.00000 0.01958 0.01332 = 0.01473 0.00203 0.00343 0.00492 O2 5 0.256824 0.508986 0.151766 11.00000 0.02110 0.01307 = 0.01585 0.00227 0.00496 0.00390 C1 1 0.224795 0.310535 0.467365 11.00000 0.02295 0.01921 = 0.01646 0.00243 0.00464 -0.00338 H1A 2 0.172745 0.312706 0.521153 11.00000 0.02483 H1B 2 0.312364 0.285368 0.487719 11.00000 0.02282 C2 1 0.130912 0.283702 0.370394 11.00000 0.02362 0.01851 = 0.02082 0.00160 0.00590 -0.00830 H2A 2 0.037306 0.305005 0.355615 11.00000 0.02205 H2B 2 0.113683 0.238030 0.373811 11.00000 0.03113 C3 1 0.403173 0.413984 0.559539 11.00000 0.02144 0.02338 = 0.01690 -0.00311 0.00353 -0.00173 H3A 2 0.434304 0.456045 0.557926 11.00000 0.02868 H3B 2 0.489903 0.386497 0.574851 11.00000 0.02653 H3C 2 0.351642 0.409559 0.614014 11.00000 0.03066 C4 1 0.116482 0.436162 0.452825 11.00000 0.01897 0.02200 = 0.02235 0.00104 0.00890 0.00061 H4A 2 0.037204 0.426326 0.397762 11.00000 0.02481 H4B 2 0.084276 0.423478 0.513729 11.00000 0.03120 H4C 2 0.135485 0.479155 0.452528 11.00000 0.01712 C5 1 0.065596 0.300427 0.159278 11.00000 0.01973 0.02114 = 0.01966 0.00196 -0.00198 -0.00422 H5A 2 0.001766 0.264367 0.160861 11.00000 0.02837 H5B 2 0.007067 0.339279 0.161585 11.00000 0.03134 H5C 2 0.096590 0.299706 0.095867 11.00000 0.03559 C6 1 0.301458 0.220961 0.247920 11.00000 0.02854 0.01354 = 0.02587 -0.00164 0.00038 -0.00065 H6A 2 0.367306 0.209871 0.305209 11.00000 0.03849 H6B 2 0.226987 0.189143 0.237244 11.00000 0.02751 H6C 2 0.351027 0.220819 0.190858 11.00000 0.02644 C7 1 0.582939 0.322932 0.157933 11.00000 0.02497 0.02047 = 0.02264 -0.00318 0.01084 0.00312 H7A 2 0.636123 0.325954 0.103657 11.00000 0.02451 H7B 2 0.533864 0.283437 0.151179 11.00000 0.02609 C8 1 0.684929 0.325808 0.261439 11.00000 0.02048 0.02778 = 0.02640 0.00105 0.00910 0.00828 H8A 2 0.763059 0.356505 0.259090 11.00000 0.02409 H8B 2 0.729381 0.285065 0.282212 11.00000 0.03117 C9 1 0.333760 0.378964 0.023987 11.00000 0.02580 0.03614 = 0.01485 -0.00276 0.00373 -0.00168 H9A 2 0.283060 0.338771 0.017978 11.00000 0.03366 H9B 2 0.265489 0.412668 0.011865 11.00000 0.03515 H9C 2 0.397410 0.380216 -0.025101 11.00000 0.03984 C10 1 0.564733 0.455778 0.129248 11.00000 0.02186 0.02394 = 0.02463 0.00232 0.01067 -0.00139 H10A 2 0.609102 0.448145 0.072166 11.00000 0.02867 H10B 2 0.637644 0.460810 0.185005 11.00000 0.03129 H10C 2 0.506755 0.493616 0.118608 11.00000 0.03292 C11 1 0.617574 0.286548 0.448177 11.00000 0.02206 0.01900 = 0.02154 0.00270 0.00039 0.00449 H11A 2 0.720356 0.276416 0.463838 11.00000 0.02638 H11B 2 0.565432 0.250264 0.421501 11.00000 0.03169 H11C 2 0.589575 0.296674 0.507446 11.00000 0.02573 C12 1 0.715329 0.410364 0.427995 11.00000 0.01537 0.02387 = 0.02808 -0.00158 0.00106 -0.00258 H12A 2 0.722604 0.446906 0.383025 11.00000 0.03054 H12B 2 0.809126 0.391120 0.448438 11.00000 0.02738 H12C 2 0.681279 0.425043 0.485277 11.00000 0.03372 C13 1 0.124691 0.573188 0.242914 11.00000 0.02001 0.01626 = 0.01622 0.00249 0.00221 0.00621 C14 1 -0.033170 0.547165 0.213964 11.00000 0.01977 0.03278 = 0.02733 0.00193 0.00406 0.00458 H14A 2 -0.038993 0.507719 0.177734 11.00000 0.03128 H14B 2 -0.070734 0.539788 0.275965 11.00000 0.03181 H14C 2 -0.094507 0.576067 0.173049 11.00000 0.03168 C15 1 0.124450 0.636930 0.296995 11.00000 0.03679 0.01871 = 0.02321 -0.00003 0.00493 0.01112 H15A 2 0.220685 0.651833 0.327631 11.00000 0.03242 H15B 2 0.066734 0.632851 0.348815 11.00000 0.03406 H15C 2 0.075534 0.670337 0.248538 11.00000 0.03642 C16 1 0.206666 0.574259 0.153384 11.00000 0.02093 0.01348 = 0.01731 0.00332 0.00303 0.00413 C17 1 0.343342 0.617424 0.172897 11.00000 0.03049 0.01751 = 0.02847 0.00482 0.00718 -0.00094 H17A 2 0.319843 0.661353 0.175264 11.00000 0.03312 H17B 2 0.403197 0.607810 0.234768 11.00000 0.02393 H17C 2 0.399467 0.610486 0.119833 11.00000 0.03386 C18 1 0.109134 0.590330 0.052183 11.00000 0.03117 0.02801 = 0.01905 0.00562 0.00162 0.00881 H18A 2 0.068523 0.631132 0.054455 11.00000 0.03336 H18B 2 0.167302 0.590989 0.000260 11.00000 0.03896 H18C 2 0.029899 0.560578 0.030674 11.00000 0.02490 B1 3 0.271229 0.482477 0.250307 11.00000 0.01442 0.01397 = 0.01563 0.00161 0.00239 0.00013 HKLF 4 REM se21001_a.res in P2(1)/c REM wR2 = 0.0684, GooF = S = 1.058, Restrained GooF = 1.058 for all data REM R1 = 0.0323 for 5585 Fo > 4sig(Fo) and 0.0398 for all 6424 data REM 419 parameters refined using 0 restraints END WGHT 0.0240 1.0177 REM Highest difference peak 0.352, deepest hole -0.253, 1-sigma level 0.058 Q1 1 0.2560 0.5079 0.2886 11.00000 0.05 0.35 Q2 1 0.1996 0.4174 0.4563 11.00000 0.05 0.34 Q3 1 0.2552 0.3460 0.4641 11.00000 0.05 0.33 Q4 1 0.1703 0.5755 0.1962 11.00000 0.05 0.32 Q5 1 0.1497 0.2999 0.2039 11.00000 0.05 0.32 ; _shelx_res_checksum 34103 _shelx_hkl_file ; 0 0 3 0.12 1.24 0 0 4 265.16 10.14 0 0 5 4.98 2.40 0 0 6 104.52 7.84 0 0 7 11.24 3.54 0 0 8 48.99 6.14 0 0 9 2.61 3.24 0 0 -9 1.56 2.73 0 0 10 1665.93 45.20 0 0 -10 1785.88 46.42 0 0 11 -0.31 2.41 0 0 12 103.15 11.18 0 0 13 1.66 3.13 0 0 14 517.64 12.42 0 0 14 544.87 28.58 0 0 15 4.30 3.47 0 0 15 3.02 4.10 0 0 15 1.54 3.11 0 0 16 2.87 2.69 0 0 16 3.49 2.82 0 0 16 7.30 4.16 0 0 17 -0.33 2.21 0 -1 3 291.55 9.44 0 1 3 276.38 9.15 0 1 4 78.64 5.38 0 -1 -4 74.35 5.26 0 -1 4 88.38 5.81 0 -1 -5 215.86 10.09 0 -1 5 216.25 10.19 0 1 5 219.74 10.10 0 1 6 1125.70 28.21 0 -1 6 1101.87 28.25 0 1 7 3106.68 59.44 0 -1 7 3000.21 59.15 0 -1 8 389.63 17.48 0 1 8 384.94 17.24 0 1 9 118.68 9.93 0 -1 9 96.50 9.06 0 1 -9 111.80 9.68 0 -1 -9 114.56 9.77 0 1 10 324.32 17.88 0 -1 10 326.63 17.98 0 -1 -10 358.35 18.60 0 1 -10 319.17 17.51 0 1 11 42.04 7.26 0 -1 11 33.81 6.33 0 -1 12 288.76 18.83 0 1 12 307.76 19.25 0 -1 13 87.18 10.81 0 1 13 94.78 11.33 0 1 13 111.43 4.52 0 1 13 107.75 5.07 0 -1 14 74.25 10.40 0 1 14 59.43 9.52 0 -1 14 75.25 11.36 0 1 14 61.23 10.31 0 -1 14 75.05 8.87 0 -1 15 271.15 21.13 0 1 15 258.09 20.39 0 1 15 264.86 22.45 0 -1 15 306.69 24.33 0 -1 15 296.74 18.47 0 -1 16 2.76 2.94 0 1 16 2.73 2.81 0 -1 16 5.36 3.44 0 1 16 1.93 3.27 0 1 16 11.13 5.06 0 -1 16 1.41 2.89 0 1 17 13.12 4.56 0 -2 -2 14.89 1.78 0 2 2 15.12 1.90 0 2 -2 14.42 1.67 0 -2 2 15.22 1.94 0 2 3 387.76 11.49 0 -2 -3 399.75 11.51 0 -2 3 416.54 11.90 0 -2 4 123.86 6.93 0 -2 -4 108.34 6.35 0 2 4 119.21 6.62 0 2 5 15.48 2.89 0 -2 -5 10.54 2.43 0 -2 5 10.99 2.56 0 -2 6 80.21 6.83 0 2 6 69.90 6.24 0 2 7 43.61 5.34 0 -2 7 39.60 5.32 0 -2 8 443.20 18.85 0 2 8 435.73 18.31 0 -2 -8 427.35 18.42 0 2 9 253.00 14.76 0 -2 -9 256.58 14.98 0 -2 9 251.91 14.98 0 2 -9 255.73 14.79 0 2 10 60.39 7.76 0 -2 10 53.98 7.30 0 2 -10 63.26 7.81 0 -2 -10 53.85 7.18 0 2 10 59.32 3.37 0 -2 11 14.99 4.48 0 2 11 11.92 4.18 0 2 11 15.00 1.64 0 2 12 35.77 6.68 0 -2 12 29.88 6.48 0 2 12 33.75 2.25 0 -2 13 565.23 28.31 0 2 13 556.04 27.55 0 -2 13 477.29 27.75 0 2 13 492.70 28.09 0 -2 13 559.13 23.49 0 2 14 33.83 7.60 0 -2 14 40.19 8.26 0 -2 14 36.88 6.24 0 -2 14 47.13 9.39 0 2 14 28.41 7.29 0 -2 15 301.11 18.56 0 -2 15 312.70 22.55 0 2 15 283.89 21.32 0 2 15 297.77 23.63 0 -2 15 308.39 24.39 0 2 16 -2.92 3.67 0 -2 16 -1.72 2.93 0 2 16 6.41 3.39 0 -2 16 2.37 3.00 0 2 16 6.24 5.20 0 -2 16 11.12 6.06 0 2 -16 8.99 4.40 0 2 17 0.63 2.18 0 2 -17 -0.41 2.28 0 -3 1 781.33 14.06 0 -3 -2 600.84 13.79 0 -3 -2 637.33 10.75 0 3 -2 625.26 13.44 0 -3 2 616.51 13.56 0 -3 -3 326.68 10.49 0 3 3 320.69 10.29 0 3 3 324.39 6.28 0 -3 -3 332.35 6.69 0 3 -3 317.49 9.55 0 -3 3 347.27 10.93 0 3 4 51.73 4.45 0 -3 -4 53.87 4.55 0 3 4 52.55 1.98 0 3 -4 57.79 4.11 0 -3 4 50.80 4.64 0 3 5 62.46 5.49 0 -3 -5 69.88 5.77 0 3 5 62.86 2.28 0 -3 5 65.65 5.73 0 3 6 1011.66 26.51 0 -3 -6 1021.14 26.98 0 -3 6 1031.71 27.33 0 3 6 1015.71 16.41 0 -3 7 295.09 14.36 0 3 7 305.64 14.13 0 3 7 297.11 6.63 0 -3 -8 216.84 13.08 0 -3 8 230.88 13.46 0 3 8 228.51 13.14 0 3 8 217.92 5.58 0 3 9 337.82 17.03 0 -3 9 313.81 16.97 0 -3 -9 339.12 17.37 0 3 9 324.53 7.33 0 3 -9 314.16 16.65 0 3 10 38.43 6.31 0 -3 10 39.89 6.66 0 3 10 41.36 2.08 0 3 -10 34.95 5.86 0 -3 -10 36.13 6.11 0 3 11 730.77 28.88 0 -3 11 709.23 29.22 0 3 12 47.88 7.70 0 -3 12 36.33 7.23 0 -3 12 37.44 5.95 0 3 13 39.72 7.41 0 -3 13 43.92 7.99 0 -3 13 44.79 6.65 0 3 13 65.06 10.22 0 -3 13 42.19 8.34 0 -3 14 160.22 13.01 0 3 -14 148.67 13.30 0 -3 14 144.68 15.88 0 3 14 159.83 16.77 0 3 14 161.37 15.13 0 -3 14 146.57 14.94 0 3 -15 61.18 8.78 0 -3 15 64.65 8.73 0 -3 15 56.05 10.64 0 3 15 45.24 9.33 0 3 15 62.30 10.11 0 -3 15 53.13 9.56 0 3 -16 32.96 6.91 0 -3 16 34.37 6.72 0 3 16 31.73 8.31 0 -3 16 29.48 8.03 0 -3 16 47.92 9.50 0 3 16 31.85 7.60 0 3 17 5.56 3.40 0 3 -17 0.92 3.45 0 -4 0 5623.85 80.05 0 4 0 5705.90 79.89 0 -4 0 5738.74 84.70 0 -4 1 1969.67 31.12 0 4 -1 1981.45 31.14 0 4 -1 2038.36 33.73 0 -4 1 1920.51 33.16 0 -4 -2 23.80 2.58 0 -4 2 23.96 2.46 0 4 -2 19.89 2.30 0 4 -2 19.15 2.00 0 -4 2 21.54 2.09 0 -4 -2 22.17 1.65 0 -4 3 102.02 5.94 0 4 -3 97.63 5.25 0 -4 3 90.79 5.02 0 -4 3 96.50 4.94 0 4 3 93.92 5.39 0 -4 -3 98.28 5.61 0 -4 -3 97.08 3.37 0 4 -4 4.60 1.53 0 -4 4 4.10 1.78 0 -4 -4 7.24 2.08 0 4 4 2.70 1.40 0 4 4 6.66 0.82 0 -4 -4 7.02 0.97 0 4 5 15.58 2.94 0 -4 -5 7.53 2.34 0 4 5 11.25 0.97 0 4 -5 8.84 2.23 0 -4 5 10.90 3.04 0 -4 6 93.58 7.54 0 4 6 77.70 6.60 0 -4 -6 87.74 7.14 0 4 6 95.41 2.88 0 4 -6 81.88 6.16 0 4 7 4.79 2.38 0 4 7 4.75 0.64 0 -4 7 0.56 2.00 0 -4 -8 455.08 19.16 0 4 8 436.76 18.42 0 -4 8 431.92 19.08 0 -4 9 506.06 18.63 0 4 -9 513.08 19.72 0 4 -9 480.01 21.16 0 -4 9 499.21 21.90 0 -4 -9 517.63 21.79 0 4 9 516.58 21.38 0 4 10 21.01 4.70 0 -4 10 16.81 3.83 0 -4 -10 17.88 4.70 0 4 -10 21.15 4.38 0 -4 10 15.26 4.25 0 4 -10 19.84 4.67 0 4 -11 158.90 11.70 0 -4 11 127.99 12.16 0 4 11 136.27 11.93 0 -4 11 152.61 10.90 0 4 -12 208.55 14.39 0 -4 12 200.68 15.94 0 4 12 189.22 14.96 0 -4 12 188.54 12.95 0 -4 13 71.40 8.48 0 4 13 70.53 9.76 0 -4 13 55.35 8.74 0 4 -13 73.23 8.88 0 -4 13 73.39 10.76 0 4 13 68.45 10.44 0 -4 14 619.86 26.65 0 4 -14 648.07 28.50 0 -4 14 668.72 34.47 0 4 14 563.77 31.42 0 4 14 648.01 31.01 0 -4 14 614.85 31.47 0 4 -15 7.39 4.35 0 -4 15 1.18 2.58 0 -4 15 3.54 3.64 0 4 15 2.28 3.66 0 4 15 -0.31 2.73 0 -4 15 1.66 3.64 0 4 -16 41.13 7.75 0 -4 16 49.32 7.94 0 4 16 36.10 8.81 0 -4 16 49.80 10.47 0 -4 16 50.05 10.18 0 4 16 43.30 8.63 0 4 17 2.20 2.58 0 4 -17 0.08 2.55 0 -5 0 1.21 1.43 0 -5 0 0.72 1.02 0 5 0 0.71 1.11 0 5 -1 27.17 3.09 0 -5 1 33.73 3.11 0 -5 1 27.08 2.30 0 5 -1 33.20 2.44 0 -5 2 11.69 1.98 0 5 -2 17.60 2.36 0 -5 2 16.25 1.97 0 5 -2 15.16 1.91 0 -5 -2 15.27 1.55 0 -5 3 225.61 8.75 0 -5 -3 216.58 8.84 0 -5 -3 237.04 6.26 0 -5 3 222.24 8.07 0 5 -3 220.60 8.69 0 -5 4 82.44 5.41 0 -5 4 84.99 6.19 0 5 -4 79.23 5.39 0 -5 4 83.21 5.26 0 -5 -4 89.79 6.18 0 5 4 90.73 6.00 0 -5 -4 89.22 3.57 0 5 -5 23.68 3.31 0 -5 -5 25.28 1.92 0 -5 5 20.33 3.43 0 -5 -5 22.04 3.66 0 5 5 16.18 2.95 0 -5 6 13.12 3.36 0 5 -6 11.35 2.73 0 5 6 17.04 3.50 0 -5 -6 13.74 2.96 0 5 7 904.53 26.45 0 -5 7 928.21 27.85 0 -5 -8 29.04 4.97 0 -5 8 32.12 5.50 0 5 8 22.13 4.28 0 -5 9 17.32 3.50 0 -5 9 14.36 3.99 0 -5 -9 16.69 3.95 0 5 -9 13.50 3.38 0 5 9 17.94 4.24 0 -5 10 8.53 2.94 0 5 -10 7.43 2.63 0 -5 -10 8.74 3.37 0 -5 10 5.67 3.38 0 5 10 6.69 2.93 0 -5 11 25.68 4.72 0 -5 11 27.10 5.78 0 5 -11 36.00 5.91 0 5 11 40.72 6.72 0 -5 12 1.69 2.09 0 5 -12 10.10 3.78 0 5 12 10.91 4.67 0 -5 12 12.40 4.61 0 5 -13 56.18 7.88 0 -5 13 46.29 6.92 0 5 13 54.81 9.36 0 -5 13 56.91 9.72 0 5 13 49.21 8.12 0 -5 13 51.25 9.04 0 5 -14 82.20 10.80 0 5 14 56.68 9.14 0 -5 14 34.51 7.71 0 -5 14 46.97 7.29 0 -5 14 53.75 9.68 0 5 14 70.23 11.11 0 -5 15 559.88 26.39 0 5 -15 601.38 28.70 0 -5 15 551.60 32.68 0 5 15 512.77 31.49 0 -5 15 482.38 29.22 0 5 15 532.06 29.23 0 5 -16 23.29 6.12 0 -5 16 9.07 4.35 0 -5 16 14.97 5.95 0 5 16 23.63 7.80 0 5 16 24.36 6.78 0 -5 16 34.41 8.40 0 5 -17 48.16 8.59 0 -6 0 849.98 21.16 0 6 0 848.40 16.56 0 -6 0 832.83 16.78 0 6 -1 470.82 14.53 0 -6 1 494.01 14.27 0 6 1 482.25 11.26 0 -6 1 487.90 11.86 0 6 -1 482.15 11.59 0 -6 2 674.96 17.22 0 6 -2 684.13 15.61 0 6 -2 690.20 17.59 0 -6 2 704.52 15.73 0 -6 -2 695.69 14.49 0 -6 3 107.39 6.41 0 -6 -3 114.80 6.76 0 6 -3 128.31 7.07 0 6 -3 91.74 5.35 0 -6 3 118.86 6.19 0 -6 -3 101.51 4.40 0 -6 4 137.99 7.02 0 -6 -4 115.29 7.21 0 -6 -4 126.03 4.79 0 -6 4 131.13 8.07 0 6 -4 145.00 7.51 0 -6 4 140.02 7.60 0 6 5 92.24 6.84 0 -6 -5 88.18 6.83 0 -6 -5 92.66 4.07 0 6 -5 93.65 6.52 0 -6 5 106.78 7.85 0 6 6 301.77 13.35 0 -6 6 300.52 14.21 0 6 -6 289.09 12.42 0 6 7 285.74 13.99 0 -6 7 317.29 15.44 0 6 8 567.22 21.73 0 -6 8 572.33 22.73 0 -6 -8 570.24 22.48 0 6 -8 583.32 20.39 0 -6 9 131.08 9.43 0 6 -9 136.99 10.02 0 -6 -9 149.31 11.57 0 -6 9 124.03 10.95 0 6 9 117.29 10.08 0 6 10 12.09 3.84 0 -6 10 6.05 3.24 0 6 -10 9.28 3.44 0 -6 -10 11.85 3.65 0 -6 10 12.66 3.44 0 6 11 18.13 4.47 0 -6 11 20.10 4.14 0 -6 11 18.60 5.18 0 6 -11 28.71 5.27 0 -6 12 92.32 9.30 0 -6 12 98.90 11.30 0 6 12 90.26 10.49 0 6 -12 96.08 9.73 0 6 12 67.06 9.78 0 -6 12 81.92 10.81 0 -6 13 439.55 21.29 0 6 13 411.48 23.37 0 -6 13 398.73 24.08 0 6 -13 403.47 21.52 0 6 13 355.34 23.61 0 -6 13 430.24 25.90 0 -6 14 89.36 9.93 0 6 14 91.65 11.72 0 -6 14 85.85 11.57 0 6 -14 75.86 9.77 0 -6 14 77.56 11.97 0 6 14 72.83 11.31 0 -6 15 292.41 18.85 0 6 -15 303.76 20.36 0 -6 15 267.47 22.71 0 6 15 287.96 23.27 0 6 15 274.28 20.76 0 -6 15 303.36 22.84 0 6 -16 14.39 5.46 0 -6 16 6.45 3.27 0 6 16 13.47 6.39 0 -6 16 14.62 6.68 0 6 16 10.65 5.15 0 -6 16 5.16 4.70 0 6 -17 3.08 2.86 0 -7 0 -0.22 1.40 0 7 0 0.67 0.74 0 -7 1 268.81 8.62 0 7 -1 260.19 8.35 0 7 1 259.00 8.03 0 7 -1 265.88 11.25 0 -7 1 248.54 10.55 0 -7 2 686.41 16.00 0 7 -2 669.38 18.47 0 -7 2 656.70 18.03 0 7 -2 664.41 15.82 0 -7 -3 758.49 19.76 0 7 -3 788.41 20.24 0 7 -3 752.94 18.03 0 -7 3 737.36 19.60 0 -7 3 769.84 18.31 0 -7 -3 753.92 15.90 0 -7 -4 33.27 4.12 0 7 -4 29.52 3.80 0 -7 4 29.52 3.75 0 -7 4 33.90 3.64 0 -7 -4 31.03 2.61 0 -7 5 9.61 2.43 0 -7 5 14.71 3.37 0 7 -5 3.73 1.96 0 -7 -5 12.20 2.84 0 -7 -5 6.06 1.22 0 -7 -6 783.56 16.05 0 -7 6 788.38 24.99 0 -7 -7 77.59 7.59 0 7 7 80.08 7.29 0 -7 7 80.22 7.86 0 -7 8 396.55 16.16 0 -7 -8 397.61 18.55 0 7 8 405.08 17.81 0 -7 8 405.72 19.20 0 7 -8 406.13 16.77 0 7 -9 0.17 2.27 0 -7 -9 -0.75 1.69 0 7 9 2.68 2.23 0 -7 9 3.57 2.04 0 -7 9 7.54 3.79 0 -7 10 151.06 10.92 0 7 -10 156.72 11.31 0 7 10 141.01 11.78 0 -7 10 153.77 12.87 0 -7 -10 162.89 13.01 0 -7 11 4.14 2.53 0 7 -11 3.69 2.61 0 -7 11 11.63 4.25 0 7 11 4.91 3.18 0 7 -12 33.21 6.27 0 -7 12 26.35 6.25 0 -7 12 26.45 5.29 0 7 12 20.66 5.65 0 -7 12 27.40 6.57 0 7 12 27.37 5.98 0 7 -13 -0.13 2.18 0 7 13 1.57 2.99 0 -7 13 8.31 5.06 0 -7 13 -2.11 2.65 0 -7 13 1.05 3.34 0 7 13 0.41 2.75 0 -7 14 529.18 25.05 0 7 -14 569.76 27.12 0 -7 14 545.21 30.85 0 7 14 568.79 31.51 0 -7 14 546.84 30.20 0 7 14 544.15 28.13 0 7 -15 99.96 12.10 0 7 15 72.61 10.83 0 -7 15 63.47 10.89 0 -7 15 79.18 9.98 0 -7 15 80.42 12.39 0 7 15 63.76 10.95 0 7 -16 55.75 8.97 0 -7 16 53.59 10.34 0 7 16 45.66 8.94 0 -7 16 56.01 8.85 0 -7 16 30.85 8.52 0 7 16 36.25 9.15 0 7 -17 72.68 10.60 0 -8 0 178.94 7.12 0 8 0 181.33 6.87 0 -8 0 173.56 9.70 0 -8 1 867.19 18.85 0 8 -1 862.62 18.52 0 8 1 838.96 17.88 0 -8 1 829.31 22.56 0 -8 2 51.02 4.05 0 -8 2 50.92 3.25 0 8 2 53.47 3.23 0 -8 2 54.92 5.03 0 8 -2 53.24 4.04 0 8 -2 49.81 5.09 0 8 -3 45.91 4.89 0 -8 3 37.69 4.25 0 8 -3 47.05 4.05 0 -8 3 48.61 4.20 0 -8 -3 41.52 3.31 0 -8 -4 443.00 15.88 0 8 -4 476.63 15.92 0 -8 4 436.00 15.38 0 -8 4 437.06 14.30 0 -8 -4 452.36 11.76 0 -8 -5 144.11 9.21 0 -8 5 140.87 8.69 0 -8 5 159.12 10.02 0 -8 5 155.93 8.52 0 -8 -5 142.58 6.14 0 8 -5 168.72 9.33 0 -8 6 407.66 17.52 0 -8 6 466.70 16.21 0 -8 -6 416.66 11.16 0 -8 7 337.07 14.36 0 -8 -7 327.66 9.31 0 -8 -7 326.22 16.00 0 -8 7 337.10 16.78 0 -8 8 285.86 13.85 0 -8 -8 289.74 15.86 0 8 -8 280.50 14.09 0 -8 8 292.01 16.28 0 -8 9 484.04 19.27 0 -8 -9 482.15 22.01 0 8 9 505.65 21.49 0 -8 9 486.26 22.63 0 8 -9 466.82 19.41 0 8 -10 66.39 7.42 0 -8 -10 68.52 8.48 0 8 10 56.06 7.27 0 -8 10 55.98 6.75 0 -8 10 61.79 8.57 0 -8 11 74.63 8.10 0 8 11 78.97 9.25 0 -8 11 93.51 10.75 0 8 -11 80.19 8.77 0 -8 11 81.41 10.21 0 8 11 87.03 10.21 0 -8 12 105.66 10.09 0 8 12 100.07 10.83 0 -8 12 116.50 12.88 0 8 -12 100.67 10.23 0 8 12 109.36 12.60 0 -8 12 111.99 12.35 0 -8 13 164.47 13.18 0 8 13 179.09 15.41 0 -8 13 172.34 16.35 0 8 -13 166.55 13.94 0 -8 13 186.28 17.14 0 8 13 176.39 16.45 0 -8 14 354.67 20.51 0 8 14 334.08 22.06 0 -8 14 353.81 24.13 0 8 14 298.33 22.63 0 -8 14 366.72 25.37 0 8 -14 353.19 21.02 0 8 -15 33.47 6.78 0 -8 15 61.90 10.93 0 8 15 43.57 8.51 0 -8 15 41.22 7.25 0 8 15 44.58 9.30 0 -8 15 33.74 8.56 0 8 -16 11.52 4.83 0 8 16 10.75 5.32 0 8 16 11.43 5.12 0 -8 16 10.29 5.46 0 8 -17 59.09 9.54 0 9 0 1.48 1.34 0 -9 0 1.78 2.45 0 9 -1 69.40 4.54 0 9 1 65.11 4.25 0 -9 1 67.70 4.63 0 -9 1 61.57 6.02 0 -9 2 41.20 3.88 0 9 -2 40.69 3.74 0 -9 2 44.77 5.09 0 9 -2 48.15 5.28 0 -9 2 45.12 2.97 0 9 2 46.92 2.96 0 9 -3 5.92 2.72 0 -9 3 1.86 1.77 0 -9 -3 4.85 1.57 0 -9 3 5.27 1.86 0 9 -3 6.83 2.17 0 9 3 4.31 1.80 0 -9 3 5.22 1.82 0 -9 -4 2.84 1.53 0 -9 4 4.74 1.77 0 -9 -4 6.65 1.55 0 9 -4 7.02 2.58 0 -9 4 4.90 2.07 0 -9 5 206.54 11.85 0 -9 5 196.43 10.67 0 -9 -5 190.12 7.59 0 -9 5 203.64 10.01 0 -9 6 968.16 26.94 0 -9 6 999.06 29.74 0 -9 6 994.25 26.03 0 -9 -6 942.04 20.19 0 -9 7 2393.57 53.21 0 -9 -7 2283.46 38.62 0 9 -7 2374.55 49.22 0 -9 -7 2282.40 51.82 0 -9 7 2304.18 47.72 0 -9 -8 252.51 14.94 0 -9 8 244.82 15.22 0 9 -8 250.39 13.44 0 -9 8 243.63 13.01 0 -9 -9 250.60 15.85 0 -9 9 260.65 14.04 0 -9 9 254.36 16.37 0 9 -9 271.83 14.70 0 9 -10 50.36 6.73 0 -9 10 51.34 7.73 0 9 10 48.02 7.29 0 -9 10 47.65 6.45 0 -9 10 48.25 7.82 0 9 -11 10.80 3.60 0 -9 11 27.66 6.16 0 9 11 25.82 6.02 0 -9 11 24.33 5.04 0 -9 11 35.49 7.02 0 -9 12 -3.36 3.03 0 9 12 8.86 3.65 0 9 -12 2.70 2.75 0 -9 12 3.55 2.60 0 -9 12 8.36 4.19 0 9 12 4.94 3.75 0 -9 13 62.49 9.94 0 9 13 56.13 8.60 0 -9 13 66.10 8.40 0 -9 13 53.55 9.28 0 9 13 56.69 9.30 0 9 -13 57.79 8.19 0 9 14 -1.39 3.22 0 -9 14 0.23 3.40 0 9 -14 -2.32 3.09 0 -9 14 -1.72 2.65 0 -9 14 2.25 3.80 0 9 14 5.48 4.57 0 9 -15 227.51 17.63 0 9 15 225.14 18.88 0 -9 15 206.54 19.49 0 -9 15 242.19 17.62 0 9 15 217.84 20.14 0 -9 15 198.81 19.34 0 -9 16 48.27 10.28 0 9 16 50.48 11.21 0 9 -16 60.02 9.37 0 9 -17 24.68 6.50 0 10 0 4061.42 62.92 0 -10 0 3969.86 72.57 0 10 -1 119.42 6.34 0 -10 1 121.40 6.59 0 10 1 118.80 5.99 0 -10 1 116.25 8.52 0 -10 2 132.99 7.20 0 10 -2 131.80 6.93 0 10 2 122.90 6.28 0 -10 2 125.42 4.80 0 10 2 128.11 4.86 0 -10 2 106.22 7.91 0 10 -2 118.33 8.63 0 -10 -3 108.71 6.08 0 10 -3 111.07 6.73 0 -10 3 105.44 7.80 0 -10 3 115.56 6.87 0 -10 3 119.34 5.93 0 10 3 110.21 5.89 0 -10 4 476.26 14.84 0 10 4 486.37 15.07 0 -10 -4 480.81 17.57 0 -10 4 489.80 16.00 0 -10 4 502.86 17.97 0 -10 -4 479.69 13.63 0 -10 5 13.46 3.26 0 -10 -5 9.52 1.90 0 -10 5 10.47 2.54 0 10 5 11.58 2.69 0 -10 -6 141.11 10.12 0 -10 6 157.72 10.12 0 -10 6 150.15 10.78 0 10 -6 149.56 9.93 0 -10 6 149.71 9.30 0 -10 -6 153.99 6.89 0 -10 7 3.24 2.39 0 -10 -7 4.22 1.39 0 10 -7 7.58 2.67 0 -10 7 2.97 2.22 0 -10 -7 1.36 1.98 0 -10 -8 231.15 14.54 0 -10 8 209.62 14.49 0 -10 -8 218.61 8.01 0 10 -8 205.63 12.65 0 -10 8 245.46 13.23 0 10 8 221.69 13.76 0 -10 9 44.06 7.00 0 -10 -9 74.64 8.70 0 10 -9 59.26 7.06 0 -10 9 56.48 6.69 0 10 9 44.42 7.00 0 -10 9 55.01 7.43 0 10 -10 114.03 10.22 0 -10 10 101.66 11.22 0 -10 10 111.39 9.78 0 10 10 111.50 11.06 0 -10 10 114.36 11.27 0 10 -11 6.68 3.03 0 -10 11 0.66 3.07 0 10 11 -0.54 2.13 0 -10 11 6.11 2.94 0 -10 11 7.49 3.72 0 10 -12 1.68 2.20 0 -10 12 -0.67 2.29 0 -10 12 1.29 2.52 0 10 12 3.37 2.26 0 -10 12 2.33 3.07 0 10 -13 233.30 16.54 0 -10 13 215.81 18.55 0 -10 13 204.88 15.17 0 10 13 217.11 18.12 0 -10 13 209.09 18.07 0 10 -14 42.67 7.32 0 10 14 43.16 8.65 0 -10 14 38.73 8.34 0 -10 14 53.07 8.19 0 -10 14 50.67 9.67 0 10 -15 30.84 6.69 0 -10 15 28.67 7.60 0 -10 15 31.83 6.61 0 10 15 33.44 8.33 0 -10 15 37.54 8.55 0 -10 16 2.65 3.74 0 10 16 4.73 3.82 0 10 -16 12.81 4.83 0 10 -17 3.11 3.28 0 11 0 14.21 2.45 0 -11 0 18.05 4.40 0 11 1 8.06 1.79 0 11 -1 6.92 1.93 0 -11 1 4.01 1.56 0 11 2 3.59 1.50 0 -11 2 0.15 1.05 0 11 -2 1.14 1.43 0 -11 2 2.01 0.79 0 11 2 2.57 0.77 0 -11 2 3.50 2.19 0 -11 -3 454.38 13.96 0 -11 3 447.94 15.11 0 11 3 429.91 12.25 0 -11 3 454.53 12.44 0 11 -3 430.79 14.46 0 -11 3 417.58 16.83 0 -11 -4 8.72 1.95 0 11 -4 9.07 2.22 0 -11 4 8.99 2.33 0 -11 4 14.03 2.46 0 11 4 12.34 2.31 0 -11 4 18.79 3.74 0 -11 -5 24.57 2.97 0 -11 5 23.06 3.92 0 11 -5 29.14 4.67 0 -11 5 24.35 3.74 0 -11 5 23.47 3.50 0 11 5 29.92 4.01 0 11 6 1339.59 33.33 0 -11 6 1308.13 33.04 0 -11 6 1386.27 35.55 0 -11 6 1419.75 38.11 0 -11 -6 1344.06 36.23 0 11 -6 1380.65 35.70 0 -11 6 1375.81 33.39 0 -11 -6 1380.97 27.84 0 -11 7 726.85 24.40 0 11 7 746.41 25.04 0 -11 -7 754.47 26.74 0 -11 7 727.68 27.19 0 11 -7 777.22 25.48 0 -11 7 734.78 23.60 0 -11 -7 746.45 18.21 0 -11 -8 973.38 31.97 0 -11 8 939.40 32.63 0 -11 -8 907.02 20.57 0 11 -8 974.49 29.88 0 -11 8 918.68 28.19 0 -11 8 913.20 29.90 0 11 8 852.41 29.20 0 -11 9 112.82 11.36 0 11 9 123.08 10.98 0 -11 9 116.08 10.60 0 11 -9 114.83 10.01 0 -11 9 113.62 9.60 0 -11 -9 121.70 11.23 0 11 -10 35.52 5.76 0 -11 10 42.12 6.96 0 11 10 35.90 6.45 0 -11 10 36.93 5.87 0 -11 10 34.67 6.41 0 11 -11 1.12 2.74 0 11 11 -1.97 2.16 0 -11 11 2.57 3.06 0 -11 11 4.33 2.69 0 -11 11 2.75 2.63 0 11 -12 15.10 4.36 0 11 12 19.15 5.42 0 -11 12 16.11 5.45 0 -11 12 19.39 4.65 0 -11 12 16.20 5.81 0 11 -13 5.67 3.78 0 11 13 6.42 3.97 0 -11 13 4.31 3.13 0 -11 13 2.65 3.85 0 -11 13 5.13 3.14 0 11 14 105.65 13.31 0 -11 14 92.25 12.73 0 -11 14 111.97 11.70 0 11 -14 123.34 12.70 0 -11 14 97.87 13.36 0 11 -15 2.91 2.57 0 -11 15 -1.02 2.81 0 -11 15 -1.55 2.88 0 11 15 9.81 5.31 0 -11 15 1.13 3.38 0 11 -16 13.08 4.78 0 11 16 23.58 7.48 0 -11 16 25.88 7.78 0 12 0 872.26 20.70 0 -12 0 869.00 28.03 0 -12 1 1466.40 30.59 0 12 1 1429.78 28.83 0 12 -1 1421.23 29.41 0 -12 -1 1337.61 37.43 0 -12 1 1368.92 36.26 0 -12 -2 327.39 12.35 0 -12 2 327.70 15.52 0 12 -2 342.52 12.44 0 -12 2 335.48 7.59 0 -12 2 345.14 12.96 0 12 2 348.16 11.84 0 12 2 327.89 7.30 0 -12 -3 649.77 18.23 0 12 -3 663.21 19.01 0 -12 3 658.64 22.61 0 -12 3 664.33 19.59 0 12 3 665.41 17.80 0 -12 3 684.35 15.88 0 12 3 635.20 15.37 0 -12 4 73.74 7.15 0 -12 -4 65.89 5.15 0 12 -4 73.72 7.57 0 12 -4 72.61 6.12 0 -12 4 74.71 6.33 0 12 4 64.45 5.05 0 -12 4 67.08 5.10 0 12 5 908.18 23.94 0 -12 5 942.32 24.23 0 -12 5 874.10 27.26 0 -12 -5 892.54 27.61 0 12 -5 903.04 28.21 0 -12 5 916.19 25.38 0 -12 -5 891.99 22.04 0 12 6 8.91 2.86 0 -12 6 5.99 2.14 0 -12 6 7.59 3.04 0 -12 6 10.54 3.07 0 -12 -6 6.05 2.41 0 12 -6 9.96 3.56 0 -12 6 7.60 2.78 0 -12 -6 9.13 2.16 0 12 7 0.81 1.70 0 -12 7 0.83 1.96 0 -12 -7 4.09 2.70 0 -12 7 2.91 2.50 0 -12 7 2.03 3.22 0 12 -7 2.55 2.58 0 -12 7 1.26 2.13 0 -12 -7 0.44 1.01 0 -12 -8 0.66 1.82 0 -12 8 -0.51 2.02 0 -12 -8 1.51 1.16 0 12 -8 0.85 2.62 0 -12 8 -1.49 2.19 0 -12 8 0.45 2.10 0 12 8 1.58 2.16 0 -12 9 24.43 5.50 0 -12 -9 32.81 5.81 0 12 -9 29.75 5.51 0 -12 9 29.81 5.42 0 -12 9 21.04 4.75 0 12 9 15.55 4.02 0 12 -10 10.75 3.56 0 -12 10 14.46 4.27 0 12 10 12.47 3.86 0 -12 10 14.53 3.84 0 -12 10 10.00 4.31 0 12 -11 10.84 3.53 0 -12 11 9.95 3.75 0 12 11 8.03 4.01 0 -12 11 10.13 3.85 0 -12 11 5.80 4.17 0 12 -12 53.96 7.88 0 -12 12 60.69 9.35 0 12 12 66.74 9.76 0 -12 12 68.36 8.58 0 -12 12 58.74 9.89 0 12 -13 17.94 4.95 0 -12 13 24.46 6.08 0 12 13 20.32 5.73 0 -12 13 21.17 5.11 0 -12 13 20.86 6.61 0 12 -14 3.58 3.22 0 12 14 17.15 6.23 0 -12 14 14.37 5.39 0 -12 14 7.18 3.17 0 -12 14 16.16 5.90 0 -12 15 30.37 7.69 0 12 15 43.60 9.62 0 12 -15 38.39 8.00 0 12 16 4.94 4.29 0 -12 16 6.71 3.97 0 12 -16 5.05 3.86 0 13 0 11.51 2.36 0 -13 0 16.80 4.33 0 13 -1 0.93 1.38 0 13 1 1.55 1.40 0 -13 1 2.46 1.51 0 -13 -1 0.04 2.00 0 -13 1 2.43 2.32 0 13 -2 7.63 2.04 0 13 2 7.48 1.85 0 -13 2 6.11 2.06 0 -13 -2 4.85 2.07 0 -13 2 5.71 2.65 0 13 3 14.67 2.51 0 -13 -3 14.65 2.70 0 13 -3 18.40 3.18 0 -13 3 10.63 2.51 0 13 3 16.64 1.97 0 -13 3 18.36 2.09 0 -13 3 19.63 3.92 0 13 -3 15.39 3.84 0 -13 -4 11.84 2.46 0 13 -4 10.85 3.38 0 -13 4 15.26 3.59 0 13 -4 12.65 2.69 0 -13 4 11.60 2.62 0 -13 4 14.77 2.48 0 13 4 18.58 2.76 0 -13 5 458.30 15.72 0 13 5 439.20 15.50 0 -13 5 466.58 19.54 0 -13 -5 451.46 19.17 0 13 -5 452.28 19.95 0 -13 5 431.72 16.95 0 -13 -5 456.67 15.10 0 13 6 234.89 12.14 0 -13 6 240.84 12.23 0 -13 6 235.60 13.92 0 -13 6 250.68 15.27 0 -13 -6 216.46 13.51 0 13 -6 259.67 14.99 0 -13 6 234.66 12.62 0 -13 -6 222.18 9.99 0 -13 7 1586.93 38.78 0 13 7 1521.26 38.39 0 -13 7 1510.29 40.71 0 -13 7 1561.69 44.12 0 -13 -7 1562.42 42.26 0 13 -7 1532.41 41.36 0 -13 7 1557.57 38.77 0 -13 -7 1503.34 31.80 0 -13 8 123.67 10.19 0 13 8 125.98 10.49 0 -13 -8 138.64 11.79 0 -13 8 127.47 12.07 0 13 -8 144.03 11.61 0 -13 8 119.97 9.89 0 -13 -8 119.94 7.06 0 -13 9 196.72 15.53 0 -13 -9 187.16 8.49 0 13 -9 197.27 13.88 0 -13 9 179.58 12.72 0 -13 9 187.11 13.52 0 13 9 205.29 14.37 0 13 -10 16.16 4.37 0 -13 10 16.63 5.44 0 -13 10 11.99 3.77 0 -13 10 26.02 5.50 0 13 10 22.13 5.24 0 13 -11 11.82 4.20 0 -13 11 6.74 4.37 0 -13 11 6.61 3.24 0 13 11 12.31 4.39 0 -13 11 8.38 3.92 0 13 -12 9.97 3.90 0 -13 12 12.15 5.03 0 -13 12 16.08 4.40 0 13 12 12.65 4.12 0 -13 12 16.21 5.00 0 13 -13 19.86 5.53 0 -13 13 26.19 7.21 0 -13 13 18.89 5.21 0 -13 13 19.05 5.96 0 13 13 9.97 4.63 0 13 -14 23.71 6.14 0 -13 14 22.99 7.68 0 -13 14 17.63 5.37 0 -13 14 22.29 6.58 0 13 14 18.29 6.73 0 13 15 1.59 2.52 0 -13 15 -1.83 2.55 0 13 -15 2.11 2.79 0 13 -16 11.09 4.24 0 -14 0 450.65 20.73 0 14 0 453.67 14.73 0 -14 1 365.23 18.14 0 -14 -1 382.33 19.33 0 -14 1 390.79 14.50 0 14 1 387.35 13.19 0 14 -1 412.65 14.01 0 14 -2 78.14 6.12 0 -14 2 78.78 8.17 0 -14 2 90.17 6.81 0 14 2 85.45 5.91 0 -14 -2 80.89 6.46 0 -14 -3 3.98 1.97 0 14 3 5.68 1.77 0 14 -3 3.46 0.87 0 -14 3 4.01 2.12 0 14 -3 3.06 1.71 0 -14 3 3.00 1.94 0 14 3 3.82 1.02 0 -14 3 4.18 1.01 0 -14 4 92.87 8.69 0 14 -4 91.96 7.18 0 14 -4 95.79 9.34 0 -14 -4 96.16 6.85 0 -14 4 101.99 7.78 0 14 4 95.09 6.52 0 14 4 95.32 5.75 0 -14 4 96.74 5.87 0 -14 5 55.22 5.12 0 14 5 52.05 4.92 0 -14 -5 53.22 6.64 0 -14 5 48.99 6.38 0 14 -5 57.46 7.46 0 -14 5 59.67 6.25 0 -14 -5 50.71 4.99 0 -14 6 0.54 1.27 0 14 6 -0.03 1.31 0 -14 6 1.39 1.66 0 -14 -6 0.02 2.39 0 14 -6 -0.61 2.20 0 -14 6 -0.82 1.98 0 -14 -6 2.34 1.57 0 -14 7 14.27 3.64 0 14 7 13.80 3.44 0 -14 7 17.70 5.14 0 -14 7 17.00 4.29 0 -14 -7 15.16 4.28 0 14 -7 13.06 3.96 0 -14 7 15.78 3.75 0 -14 -7 11.96 2.57 0 -14 8 595.52 23.18 0 14 8 543.08 22.65 0 -14 -8 582.72 25.47 0 -14 8 566.13 26.60 0 14 -8 609.26 25.17 0 -14 8 572.64 22.69 0 -14 -8 566.05 17.29 0 -14 9 93.11 10.83 0 -14 -9 102.80 6.59 0 14 -9 101.05 10.21 0 -14 9 90.62 9.21 0 -14 9 107.41 10.40 0 14 9 93.26 9.65 0 14 -10 167.81 13.50 0 -14 10 189.24 16.48 0 -14 10 173.98 13.16 0 14 10 163.65 13.87 0 -14 10 193.98 14.51 0 14 -11 21.61 5.32 0 -14 11 15.33 5.96 0 -14 11 24.38 5.22 0 -14 11 16.32 5.11 0 14 11 24.00 5.71 0 14 -12 73.84 9.67 0 -14 12 63.49 10.51 0 -14 12 64.74 8.67 0 14 12 73.78 10.35 0 -14 12 70.05 9.80 0 14 -13 1.09 2.53 0 -14 13 4.23 4.40 0 -14 13 3.21 3.00 0 -14 13 0.61 2.58 0 14 13 2.63 2.58 0 14 -14 80.53 10.79 0 -14 14 107.80 14.57 0 -14 14 101.65 11.78 0 14 14 82.16 12.05 0 -14 14 99.05 13.00 0 -14 15 10.89 4.62 0 14 15 -1.81 3.23 0 -14 15 2.27 2.29 0 14 -15 5.24 4.23 0 14 -16 18.59 5.69 0 -15 0 3.81 2.43 0 15 0 3.11 1.54 0 -15 1 31.02 5.74 0 -15 -1 18.91 4.66 0 15 1 22.12 3.15 0 15 -1 19.36 3.36 0 -15 2 162.46 12.31 0 15 -2 187.75 9.78 0 -15 -2 171.28 13.33 0 15 2 179.24 8.99 0 -15 2 187.46 10.36 0 -15 -2 191.86 10.41 0 -15 -3 17.20 3.34 0 -15 -3 20.08 1.75 0 15 -3 18.44 1.34 0 -15 3 25.39 4.96 0 -15 3 16.20 3.44 0 15 3 20.91 3.05 0 15 -3 30.76 4.08 0 15 3 21.60 1.73 0 -15 3 20.64 1.76 0 -15 4 2.95 2.65 0 15 -4 -0.76 3.06 0 -15 -4 3.88 1.77 0 15 4 1.12 0.89 0 15 -4 0.68 1.30 0 -15 4 0.59 1.40 0 15 4 1.36 0.92 0 -15 4 2.10 1.07 0 -15 5 65.75 5.54 0 15 5 56.27 5.07 0 -15 -5 62.13 7.26 0 -15 5 58.31 7.17 0 15 -5 44.83 7.00 0 -15 5 59.68 6.37 0 -15 -5 49.13 5.08 0 -15 6 1318.39 32.30 0 15 6 1300.59 32.23 0 -15 6 1302.51 38.30 0 -15 -6 1351.09 38.83 0 15 -6 1320.76 40.00 0 -15 6 1344.48 35.48 0 -15 -6 1308.45 30.85 0 -15 7 235.41 13.18 0 15 7 251.51 13.58 0 -15 7 247.16 15.61 0 -15 7 248.39 16.89 0 -15 -7 221.49 14.99 0 15 -7 225.80 15.57 0 -15 7 246.76 14.22 0 -15 -7 220.23 10.98 0 -15 -8 872.67 23.04 0 -15 8 863.57 33.83 0 15 -8 812.40 30.78 0 -15 8 814.15 28.44 0 15 8 892.27 29.08 0 -15 8 821.93 28.16 0 -15 9 12.69 4.71 0 -15 -9 16.60 2.84 0 15 -9 18.55 4.70 0 -15 9 13.95 3.93 0 -15 9 15.33 4.42 0 15 9 13.71 3.91 0 15 -10 4.67 3.19 0 15 10 5.60 3.39 0 -15 10 1.96 1.80 0 -15 10 4.20 2.75 0 -15 10 4.43 4.01 0 15 -11 76.39 9.48 0 -15 11 53.15 8.19 0 15 11 65.17 9.05 0 -15 11 74.63 9.02 0 -15 11 51.66 9.20 0 -15 12 120.25 14.24 0 15 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13.81 2.92 0 -16 -6 17.85 4.52 0 16 -6 19.05 4.99 0 -16 6 18.18 4.16 0 -16 -6 14.08 3.11 0 -16 -7 327.04 14.08 0 -16 7 356.04 20.91 0 16 -7 356.54 20.20 0 -16 7 335.22 17.31 0 16 7 337.94 15.53 0 -16 7 346.99 15.71 0 -16 8 30.29 6.65 0 -16 -8 21.18 3.55 0 16 -8 30.15 6.20 0 -16 8 18.03 3.97 0 16 8 32.20 5.03 0 -16 8 32.52 5.29 0 -16 -9 209.65 10.45 0 -16 9 179.56 15.93 0 16 -9 188.66 15.00 0 -16 9 211.11 14.43 0 16 9 207.73 14.18 0 -16 9 219.81 14.50 0 -16 10 3.69 2.85 0 -16 -10 8.92 2.36 0 16 -10 5.65 3.36 0 -16 10 0.97 2.12 0 16 10 3.42 2.90 0 -16 10 4.84 2.47 0 16 -11 25.45 5.85 0 -16 11 19.16 5.09 0 16 11 13.15 4.58 0 -16 11 20.04 5.19 0 -16 11 24.55 6.97 0 16 -12 25.55 6.12 0 -16 12 23.21 5.88 0 16 12 16.48 4.92 0 -16 12 19.60 5.38 0 -16 12 26.80 7.12 0 16 -13 234.60 18.56 0 -16 13 272.09 22.93 0 -16 13 277.22 19.31 0 -16 13 235.36 18.84 0 16 13 237.27 18.98 0 -16 14 24.86 6.77 0 16 14 22.37 6.65 0 16 -14 30.12 7.18 0 -16 15 58.71 8.36 0 -16 15 51.11 10.00 0 16 15 59.05 10.15 0 16 -15 64.18 10.41 0 -17 0 6.69 3.51 0 17 0 3.76 1.98 0 -17 1 147.62 12.65 0 -17 -1 142.50 9.87 0 17 -1 158.72 9.14 0 17 1 152.43 8.64 0 -17 2 13.44 3.95 0 -17 -2 10.69 3.01 0 -17 2 11.28 2.71 0 17 -2 10.75 2.55 0 17 2 14.93 2.80 0 -17 3 360.72 19.60 0 17 -3 373.06 15.47 0 -17 3 355.66 15.90 0 17 3 391.81 14.41 0 -17 -3 390.00 16.17 0 -17 -4 2.64 1.63 0 17 4 2.18 1.49 0 -17 4 1.47 1.52 0 17 4 2.50 0.85 0 -17 4 3.70 0.92 0 -17 -4 1.90 0.77 0 17 -4 3.83 0.86 0 17 5 6.75 1.75 0 -17 5 6.63 1.81 0 -17 -5 6.63 2.65 0 -17 5 7.79 2.84 0 17 5 7.97 2.11 0 -17 -5 12.31 2.96 0 -17 6 475.38 16.76 0 17 6 509.87 17.08 0 -17 -6 483.38 22.80 0 17 -6 493.92 24.62 0 -17 6 505.06 21.02 0 -17 -6 473.91 17.96 0 -17 -7 436.13 17.03 0 17 -7 422.81 23.06 0 -17 7 458.97 24.42 0 -17 7 441.25 20.27 0 17 7 462.03 18.12 0 -17 7 436.38 17.81 0 -17 -8 223.67 11.58 0 -17 8 218.20 17.48 0 17 -8 223.15 16.89 0 -17 8 216.73 14.46 0 -17 8 230.64 13.74 0 17 8 234.48 13.77 0 -17 9 41.90 7.73 0 -17 -9 31.46 4.35 0 17 -9 29.46 6.21 0 -17 9 27.55 5.50 0 -17 9 23.34 4.84 0 17 9 24.38 4.90 0 17 -10 18.33 5.28 0 17 10 11.28 3.43 0 -17 10 24.07 5.34 0 -17 10 27.65 5.87 0 -17 10 19.76 6.33 0 17 -11 36.62 7.45 0 -17 11 30.31 6.03 0 17 11 36.41 7.04 0 -17 11 39.48 7.11 0 -17 11 37.05 8.11 0 17 -12 22.96 6.16 0 17 12 9.09 3.82 0 -17 12 13.94 4.72 0 -17 12 20.48 5.32 0 -17 12 9.94 5.48 0 17 -13 121.82 13.56 0 -17 13 113.55 13.01 0 17 13 120.70 13.60 0 -17 13 130.13 13.37 0 -17 13 119.07 15.61 0 -17 14 281.82 18.52 0 17 14 236.93 19.90 0 -17 14 256.49 20.52 0 17 -14 304.17 22.11 0 17 15 7.72 4.03 0 18 0 252.22 11.72 0 18 -1 309.81 13.53 0 18 1 339.46 13.46 0 -18 -1 282.85 14.57 0 18 2 6.42 1.94 0 18 -2 8.11 2.32 0 -18 -2 5.90 2.35 0 18 -3 10.92 3.22 0 18 3 8.65 2.27 0 -18 3 8.80 2.91 0 -18 -3 6.64 2.82 0 -18 4 3.56 2.12 0 -18 -4 10.01 2.86 0 18 4 7.73 2.11 0 -18 -4 6.62 0.97 0 -18 -4 3.87 0.84 0 -18 -5 81.90 7.53 0 18 -5 79.97 4.30 0 -18 -5 84.32 4.98 0 18 5 92.46 7.19 0 -18 5 77.39 8.11 0 -18 5 78.65 5.05 0 18 5 75.68 4.87 0 -18 -6 12.86 3.21 0 18 6 12.18 2.87 0 18 -6 9.95 4.19 0 -18 6 19.61 4.44 0 -18 6 17.27 3.02 0 18 6 11.01 2.36 0 -18 -7 1.29 1.84 0 18 -7 1.93 3.68 0 -18 7 7.65 4.22 0 -18 7 2.15 2.01 0 -18 7 1.35 1.60 0 18 7 1.55 1.89 0 -18 -8 131.58 9.12 0 -18 8 136.14 14.09 0 18 -8 142.16 13.91 0 -18 8 138.03 11.66 0 -18 8 135.92 10.18 0 18 8 121.58 9.61 0 -18 9 24.61 6.79 0 -18 -9 13.93 2.92 0 18 -9 22.38 5.76 0 -18 9 16.93 4.33 0 18 9 12.97 3.43 0 -18 9 13.66 3.46 0 18 -10 19.76 5.71 0 -18 10 16.80 5.49 0 -18 10 12.65 4.22 0 18 10 17.98 4.47 0 -18 10 16.72 4.42 0 18 -11 13.25 5.10 0 -18 11 21.63 6.57 0 -18 11 31.70 6.43 0 18 11 14.16 4.33 0 -18 11 21.26 5.15 0 18 -12 85.04 11.75 0 -18 12 84.38 12.89 0 -18 12 78.18 10.22 0 -18 12 76.59 10.10 0 18 12 93.65 10.91 0 18 13 78.25 10.96 0 18 -13 72.97 10.99 0 18 -14 146.15 15.53 0 -19 0 6.60 2.70 0 19 0 7.84 2.46 0 19 -1 63.88 6.11 0 19 1 41.69 4.75 0 -19 -1 60.49 6.90 0 19 2 2.78 1.74 0 19 -2 6.78 2.36 0 -19 -2 1.93 1.78 0 19 -3 1.43 1.18 0 19 3 1.30 1.38 0 -19 -3 1.62 2.05 0 -19 3 4.55 2.56 0 19 4 1.72 1.48 0 -19 4 2.97 2.51 0 -19 -4 1.14 1.86 0 19 -5 28.40 2.00 0 -19 -5 23.95 2.43 0 -19 5 27.74 4.92 0 19 5 31.98 4.39 0 19 5 30.96 2.59 0 19 -5 27.07 2.02 0 -19 5 30.89 2.64 0 -19 -5 28.44 4.70 0 -19 -6 84.14 7.82 0 19 6 77.04 6.80 0 -19 6 88.62 8.99 0 -19 6 84.67 5.99 0 19 6 83.43 5.94 0 -19 -7 339.48 15.74 0 19 -7 318.48 21.23 0 -19 7 316.69 21.28 0 -19 7 319.64 17.81 0 19 7 330.45 14.93 0 -19 7 315.81 13.71 0 19 7 295.48 13.20 0 -19 -8 35.83 5.04 0 -19 8 42.05 8.21 0 19 -8 32.01 7.00 0 -19 8 33.20 5.99 0 19 8 30.12 4.67 0 -19 8 34.09 5.01 0 -19 9 8.79 4.70 0 -19 -9 12.85 3.24 0 19 -9 5.71 4.30 0 -19 9 10.28 3.64 0 19 9 8.28 2.76 0 -19 9 9.86 3.10 0 19 -10 43.21 8.18 0 -19 10 42.06 6.43 0 19 10 60.09 7.74 0 -19 10 57.26 8.23 0 -19 10 29.51 7.68 0 19 -11 50.62 10.35 0 19 11 44.39 7.21 0 -19 11 58.20 8.69 0 -19 11 56.06 10.65 0 -19 12 51.79 8.44 0 19 -12 55.10 9.41 0 -19 12 59.56 11.07 0 19 -13 -0.50 2.97 0 20 0 318.86 14.01 0 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169.45 15.64 -2 -15 14 182.94 14.19 -2 -15 13 85.04 12.24 2 15 -13 78.05 11.57 -2 -15 13 97.56 10.16 -2 -15 13 90.19 11.22 -2 15 13 91.14 11.53 -2 -15 13 88.20 11.19 -2 15 12 375.52 22.26 -2 -15 12 361.05 21.63 -2 -15 12 416.69 25.66 2 15 -12 430.16 25.07 -2 -15 12 394.09 22.56 -2 -15 12 404.98 20.36 -2 -15 11 12.18 3.61 -2 -15 11 8.52 4.46 2 15 -11 8.52 3.83 -2 -15 11 2.78 2.51 -2 -15 11 3.13 2.42 -2 15 11 12.47 4.27 -2 -15 10 8.05 3.12 -2 -15 10 14.25 4.93 2 -15 -10 10.22 1.69 -2 -15 10 4.60 3.21 -2 15 10 7.73 3.04 -2 -15 10 7.46 3.35 2 -15 -9 141.61 7.06 -2 -15 9 148.08 11.46 -2 -15 9 145.28 13.10 2 15 -9 149.13 13.44 -2 -15 9 143.07 12.32 -2 15 9 154.43 11.71 -2 -15 9 141.11 11.22 2 -15 -8 24.14 3.06 -2 -15 8 18.28 3.98 -2 -15 8 19.36 4.97 2 15 -8 24.48 3.89 2 15 -8 36.01 6.79 -2 -15 8 26.35 5.10 -2 15 8 23.61 4.41 -2 -15 8 26.85 4.81 -2 -15 7 1.02 1.59 2 -15 -7 0.87 1.34 -2 -15 7 5.75 3.27 2 -15 -7 0.95 1.16 2 15 -7 5.63 3.70 -2 -15 7 1.24 2.26 -2 15 7 2.34 1.83 -2 -15 7 -0.97 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8.47 -5 -5 14 87.75 7.65 5 5 -13 31.06 6.73 -5 -5 13 28.18 6.42 -5 -5 13 28.45 4.43 -5 -5 13 26.90 5.84 -5 5 13 36.27 5.35 -5 5 13 26.12 6.58 -5 -5 13 26.95 6.80 5 5 -12 6.59 3.87 -5 -5 12 11.63 4.24 -5 -5 12 2.34 1.49 -5 -5 12 6.89 3.39 -5 5 12 2.99 1.98 -5 5 12 2.09 2.86 -5 -5 12 4.95 3.91 -5 5 11 339.78 21.20 -5 -5 11 343.24 21.27 5 5 -11 335.83 19.90 -5 -5 11 361.46 20.22 -5 5 11 349.05 15.27 -5 -5 11 338.66 18.13 -5 -5 11 318.82 15.23 -5 5 10 16.91 4.86 -5 -5 10 15.77 4.43 5 5 -10 10.37 4.03 5 5 -10 13.05 3.69 -5 -5 10 6.07 3.21 -5 -5 10 11.82 3.25 -5 -5 10 10.21 3.29 5 -5 -10 8.86 1.57 -5 5 9 0.67 2.03 -5 -5 9 4.45 2.85 5 -5 -9 0.86 1.80 5 5 -9 6.43 3.70 -5 -5 9 3.23 3.01 5 -5 -9 6.93 3.39 5 5 -9 3.14 3.28 5 5 -9 0.26 1.55 5 -5 -9 3.89 2.30 -5 -5 9 1.72 1.59 5 5 -9 1.39 1.85 5 5 -9 4.52 2.52 -5 -5 9 5.27 2.79 5 -5 -9 1.33 0.91 5 -5 -8 3.36 2.91 5 5 -8 2.38 2.13 -5 5 8 5.03 3.37 -5 -5 8 3.16 2.49 -5 -5 8 1.85 2.13 5 -5 -8 0.62 1.56 5 5 -8 2.47 1.82 -5 -5 8 2.05 1.59 5 -5 -8 2.73 2.23 5 5 -8 0.04 1.64 5 -5 -8 0.80 0.83 5 5 -8 0.28 2.14 -5 -5 8 1.77 2.37 -5 5 8 1.50 1.22 5 5 -8 1.67 1.75 5 5 -8 0.68 1.04 -5 5 7 99.47 9.30 -5 -5 7 82.03 8.45 5 -5 -7 86.03 9.17 5 5 -7 79.93 9.06 5 5 -7 76.07 7.20 -5 -5 7 88.41 7.63 5 -5 -7 98.14 9.34 5 5 -7 75.65 7.85 5 -5 -7 81.79 8.21 5 5 -7 90.18 8.44 5 -5 -7 90.79 6.53 -5 -5 7 79.03 7.60 5 5 -7 90.70 7.75 -5 5 7 81.93 5.67 5 5 -7 83.89 6.72 -5 -5 7 86.69 7.50 5 5 -6 7.41 2.75 -5 5 6 3.43 2.31 -5 -5 6 6.91 3.25 5 -5 -6 6.72 2.68 5 5 -6 5.62 2.82 5 -5 -6 4.00 2.04 -5 -5 6 6.39 2.16 5 5 -6 5.76 2.22 5 -5 -6 7.86 2.79 -5 -5 6 7.78 2.94 5 -5 -6 9.03 2.53 5 5 -6 4.47 2.55 5 5 -6 6.02 2.28 5 -5 -6 5.39 1.44 5 5 -6 7.80 2.24 -5 -5 6 6.73 2.75 -5 5 5 498.82 20.03 -5 -5 5 513.83 20.18 5 -5 -5 524.44 21.72 5 5 -5 511.97 21.33 5 -5 -5 553.29 21.04 -5 -5 5 504.23 16.08 5 5 -5 517.43 16.70 5 5 -5 532.73 19.53 -5 -5 5 516.35 19.61 -5 -5 5 497.43 18.92 5 5 -5 513.89 17.84 5 -5 -5 513.34 13.36 5 5 -5 496.33 18.78 5 -5 -5 537.27 20.11 5 5 -5 526.45 19.58 5 -5 -4 111.32 9.29 5 5 -4 109.48 9.31 5 5 -4 118.78 6.60 -5 5 4 103.08 8.19 -5 -5 4 116.70 8.54 -5 -5 4 106.81 8.50 5 5 -4 103.78 8.19 5 -5 -4 98.04 7.95 5 5 -4 103.67 8.04 5 5 -4 122.99 8.83 5 -5 -4 108.03 5.41 5 5 -4 109.73 7.90 5 5 -3 1049.17 28.17 5 5 -3 1071.61 30.64 5 -5 -3 1026.84 30.28 5 -5 -3 1057.64 28.46 5 5 -3 1089.47 21.71 -5 -5 3 1098.14 28.02 -5 5 3 1084.09 28.50 -5 -5 3 1025.40 28.09 -5 -5 3 1030.17 29.27 5 5 -3 1126.27 28.65 5 -5 -3 1034.94 21.93 5 5 -3 1055.66 29.09 5 5 -3 1110.01 28.55 5 5 -2 370.35 16.33 5 -5 -2 378.87 15.40 5 5 -2 398.86 9.23 -5 -5 2 394.24 14.92 -5 -5 2 363.35 15.27 -5 5 2 356.70 15.00 5 5 -2 357.38 14.73 5 5 -2 353.82 15.54 5 5 -2 366.06 15.24 -5 -5 1 321.11 12.94 5 5 -1 325.58 13.81 -5 5 1 321.23 14.11 -5 -5 1 327.71 14.48 5 -5 -1 320.34 14.16 5 5 -1 330.32 14.58 -5 5 0 -0.02 1.59 -5 -5 0 3.15 2.16 -5 -5 0 2.46 1.57 5 5 0 3.98 2.11 5 5 0 6.13 2.37 -5 -5 -1 2012.88 39.57 -5 5 -1 1984.82 43.36 -5 -5 -1 1977.24 43.48 5 5 1 2037.51 44.73 -5 -5 -2 33.93 4.11 5 5 2 30.24 4.66 -5 5 -2 30.60 4.62 -5 -5 -2 32.05 4.82 5 5 2 28.89 2.19 5 5 3 709.48 16.29 -5 -5 -3 672.88 20.42 -5 -5 -3 728.27 24.49 -5 5 -3 752.70 24.38 5 5 3 706.11 23.84 -5 -5 -4 26.36 3.94 5 5 4 29.23 4.49 -5 5 -4 20.44 4.32 5 5 4 24.76 3.08 -5 -5 -5 335.46 15.40 5 5 5 363.34 13.46 5 5 5 366.12 16.81 5 5 6 18.39 3.93 5 5 6 17.12 3.27 5 -5 6 22.31 4.75 5 -5 7 65.24 8.28 -5 5 -7 72.62 3.68 5 5 7 62.09 6.51 5 5 7 71.94 7.59 -5 5 -8 46.81 3.55 5 5 8 30.04 4.91 5 -5 8 43.15 7.02 5 5 8 43.53 5.87 5 -5 9 156.90 13.73 -5 5 -9 138.18 7.04 5 5 9 128.81 10.69 5 5 9 146.15 10.86 5 5 10 50.79 6.40 -5 5 -10 51.54 4.76 5 -5 10 61.26 9.09 5 5 10 42.91 6.76 5 -5 11 69.52 10.04 5 5 11 46.77 7.46 5 -5 12 14.57 5.88 5 5 12 16.62 4.70 5 -5 13 10.29 4.93 5 5 13 17.71 5.16 5 -5 14 -1.15 3.49 5 5 14 0.94 2.21 5 5 15 1.29 3.00 -5 -6 16 3.29 4.59 -5 -6 16 3.59 3.12 -5 6 16 2.78 2.25 -5 6 16 12.88 5.77 -5 -6 16 2.39 3.41 5 6 -16 6.30 3.78 -5 -6 15 39.71 8.18 5 6 -15 52.08 8.98 -5 -6 15 51.66 8.34 -5 6 15 53.13 7.05 -5 6 15 36.24 8.13 -5 -6 15 36.13 8.38 5 6 -14 -2.83 2.67 -5 -6 14 0.29 2.27 -5 -6 14 0.49 1.44 -5 -6 14 2.85 2.71 -5 6 14 1.27 1.64 -5 6 14 1.48 3.55 -5 -6 14 1.60 2.75 -5 6 13 191.24 17.23 -5 -6 13 208.40 17.88 -5 -6 13 219.50 17.15 5 6 -13 186.11 15.98 -5 -6 13 190.33 14.64 -5 6 13 205.51 12.50 -5 -6 13 191.21 11.92 -5 -6 12 12.57 4.40 -5 -6 12 7.74 2.75 5 6 -12 7.62 3.82 -5 -6 12 7.31 3.48 -5 6 12 8.74 2.83 -5 6 12 6.93 3.59 -5 -6 12 8.44 4.21 5 6 -11 538.36 25.82 -5 -6 11 547.13 25.18 -5 6 11 512.34 26.30 -5 -6 11 541.19 27.05 -5 6 11 538.13 18.86 -5 -6 11 533.70 23.57 -5 -6 11 555.46 20.75 -5 6 10 220.79 16.18 -5 -6 10 223.11 14.96 5 6 -10 206.00 15.08 5 6 -10 221.28 14.75 -5 -6 10 198.86 15.47 -5 -6 10 225.40 14.67 -5 -6 10 225.37 12.71 5 -6 -10 226.66 7.91 -5 -6 9 104.48 10.56 -5 6 9 107.25 10.73 5 -6 -9 128.91 12.31 5 6 -9 117.92 11.83 -5 -6 9 127.81 10.59 5 6 -9 133.85 11.51 5 6 -9 111.32 9.85 5 -6 -9 119.35 10.31 5 6 -9 142.05 11.54 -5 -6 9 133.21 10.77 5 -6 -9 130.31 6.76 -5 -6 9 126.54 9.46 5 -6 -8 49.23 7.44 5 6 -8 30.27 5.98 -5 6 8 49.07 6.94 -5 -6 8 37.85 6.06 5 -6 -8 43.66 6.90 -5 -6 8 44.38 5.91 5 6 -8 46.68 5.90 5 -6 -8 49.91 6.56 5 6 -8 49.86 6.48 -5 -6 8 41.27 5.54 5 6 -8 50.95 6.86 -5 -6 8 37.02 5.50 5 6 -8 39.03 5.27 -5 6 8 42.77 4.21 5 -6 -8 44.15 4.35 -5 6 7 29.98 5.40 -5 -6 7 28.82 5.42 5 -6 -7 20.96 4.62 5 6 -7 40.94 6.41 -5 -6 7 22.93 4.15 5 -6 -7 21.76 4.81 5 6 -7 21.85 3.86 5 -6 -7 18.97 3.99 5 -6 -7 21.38 3.23 -5 -6 7 26.38 4.43 5 6 -7 24.29 4.56 5 6 -7 25.33 4.85 5 6 -7 29.40 4.76 -5 -6 7 24.21 4.52 -5 6 7 16.25 2.55 5 6 -7 26.66 3.85 -5 -6 6 240.82 13.90 -5 6 6 248.31 14.08 5 -6 -6 229.74 14.65 5 6 -6 258.22 15.50 5 -6 -6 252.20 14.79 -5 -6 6 234.75 11.43 5 6 -6 249.47 11.84 5 6 -6 222.53 13.07 5 -6 -6 249.90 13.74 5 6 -6 251.06 13.65 -5 -6 6 217.87 12.77 5 6 -6 228.78 12.64 -5 -6 6 237.51 12.84 5 6 -6 259.36 12.29 -5 6 5 1556.46 38.27 -5 -6 5 1536.92 38.04 5 -6 -5 1436.95 39.25 5 6 -5 1500.52 40.07 5 -6 -5 1525.78 39.25 -5 -6 5 1456.92 31.68 5 6 -5 1472.06 36.93 5 6 -5 1410.63 31.81 5 6 -5 1518.18 36.90 5 -6 -5 1584.30 37.80 5 -6 -5 1465.99 26.43 5 6 -5 1530.23 37.06 -5 -6 5 1439.27 36.92 5 6 -5 1484.46 34.57 -5 -6 5 1514.16 36.97 5 -6 -4 96.44 8.87 5 6 -4 80.48 8.00 -5 -6 4 79.95 5.25 5 6 -4 83.13 5.31 -5 -6 4 84.40 7.44 -5 -6 4 82.42 7.22 5 -6 -4 92.22 7.81 5 6 -4 92.92 7.71 -5 6 4 89.71 7.50 5 6 -4 76.68 7.16 5 6 -4 83.75 7.50 5 -6 -4 85.68 4.38 -5 -6 4 94.80 8.04 5 6 -4 98.96 7.43 5 6 -3 728.14 22.25 5 6 -3 690.18 15.42 -5 -6 3 713.81 22.25 -5 -6 3 674.49 23.08 -5 -6 3 669.39 21.73 -5 6 3 673.17 21.65 5 6 -3 728.03 22.89 5 -6 -3 691.12 15.54 5 6 -3 712.54 23.16 5 -6 -3 712.00 22.23 5 6 -3 713.28 22.23 5 -6 -3 682.25 23.62 5 6 -3 708.84 24.09 5 6 -2 19.82 3.68 5 6 -2 12.13 2.82 -5 -6 2 22.37 3.67 5 6 -2 17.30 3.64 -5 6 2 19.47 3.47 -5 -6 2 24.09 4.13 5 -6 -2 21.49 3.66 5 6 -2 16.51 3.62 5 6 -1 19.12 3.95 -5 -6 1 19.30 3.36 -5 6 1 20.36 3.54 5 -6 -1 20.90 3.62 5 6 -1 19.11 3.69 -5 -6 1 18.86 3.56 5 6 -1 15.97 3.41 5 6 -1 17.60 3.44 -5 -6 0 299.90 12.77 -5 6 0 286.34 13.42 -5 -6 0 294.48 13.76 5 6 0 311.68 14.27 -5 -6 -1 195.92 10.28 -5 -6 -1 201.10 12.68 -5 6 -1 196.09 11.16 -5 -6 -1 209.68 11.57 5 6 1 207.41 11.77 -5 -6 -2 85.44 7.59 -5 6 -2 75.88 7.17 5 6 2 88.39 7.64 -5 -6 -2 76.50 6.48 5 6 3 792.13 16.58 -5 6 -3 785.01 25.79 -5 -6 -3 854.51 26.77 5 6 3 855.04 26.09 -5 -6 -3 836.24 24.20 5 6 4 135.06 6.68 -5 -6 -4 136.55 10.45 -5 6 -4 118.33 9.64 5 6 4 133.53 9.79 -5 -6 -4 129.22 9.17 5 6 5 86.60 6.30 5 6 5 87.72 8.07 -5 -6 -5 85.84 7.93 5 -6 6 92.11 9.47 5 6 6 90.23 6.96 5 6 6 89.12 8.21 -5 6 -7 22.39 2.07 5 6 7 30.51 4.96 5 6 7 32.00 4.61 5 -6 7 25.19 5.46 5 -6 8 89.59 10.22 -5 6 -8 95.84 5.15 5 6 8 105.63 8.80 5 6 8 101.06 8.87 -5 6 -9 14.14 2.26 5 6 9 12.95 3.35 5 -6 9 11.29 4.94 5 6 9 20.10 4.53 -5 6 -10 10.93 2.32 5 6 10 14.97 3.67 5 6 10 9.87 3.30 5 -6 10 2.53 2.57 5 6 11 13.01 4.10 5 -6 11 4.13 3.19 5 6 12 -1.51 2.81 5 -6 12 5.14 5.22 5 6 13 15.08 4.84 5 -6 13 13.72 5.50 5 6 14 0.33 2.44 5 6 15 31.79 7.32 -5 -7 16 85.31 12.10 -5 -7 16 68.15 9.86 -5 7 16 64.67 7.87 -5 7 16 68.38 11.73 -5 -7 16 83.90 12.87 -5 -7 15 65.59 10.29 5 7 -15 86.16 11.68 -5 -7 15 77.09 10.04 -5 7 15 81.06 8.49 -5 7 15 77.86 11.84 -5 -7 15 75.63 11.48 -5 -7 14 11.71 4.69 5 7 -14 2.78 2.62 -5 -7 14 7.23 2.55 -5 -7 14 7.87 4.21 -5 7 14 2.84 1.80 -5 7 14 4.64 3.81 -5 -7 14 -0.41 3.48 -5 -7 13 -0.25 2.14 -5 -7 13 2.08 1.94 5 7 -13 2.67 3.50 -5 -7 13 2.81 2.71 -5 7 13 4.02 2.03 -5 7 13 2.29 2.66 -5 -7 13 0.66 3.14 -5 7 12 702.59 32.32 -5 -7 12 710.65 32.42 -5 -7 12 734.02 30.99 5 7 -12 700.68 30.83 -5 -7 12 675.67 28.31 -5 7 12 671.59 22.15 -5 -7 12 669.59 23.99 -5 -7 11 4.60 3.87 -5 -7 11 0.35 1.57 5 7 -11 1.02 3.32 -5 -7 11 0.50 1.96 -5 7 11 0.74 1.39 -5 7 11 -2.60 3.16 -5 -7 11 4.79 3.67 -5 -7 10 349.25 20.41 -5 7 10 358.53 20.89 -5 -7 10 340.32 18.77 5 7 -10 378.71 20.61 5 7 -10 376.28 19.31 -5 -7 10 353.65 18.68 5 -7 -10 372.09 10.59 -5 -7 10 365.67 16.91 -5 -7 9 4.43 2.89 5 7 -9 0.53 1.70 5 -7 -9 4.81 2.51 5 7 -9 -1.44 2.29 -5 -7 9 1.52 2.13 5 -7 -9 0.47 1.00 5 7 -9 3.63 3.02 -5 7 9 -0.32 0.94 -5 -7 9 1.27 1.68 5 7 -9 1.14 2.27 -5 7 9 -2.02 2.38 -5 -7 9 1.08 3.21 5 -7 -8 3.22 2.45 -5 -7 8 0.05 1.80 5 7 -8 5.08 2.61 -5 -7 8 -0.29 1.63 5 -7 -8 0.12 1.77 5 7 -8 -1.07 1.70 5 -7 -8 1.93 1.31 5 7 -8 3.75 2.59 -5 -7 8 -0.66 1.99 -5 7 8 0.24 0.97 5 7 -8 -0.39 1.23 5 -7 -8 -3.45 2.65 5 7 -8 0.16 1.71 -5 7 8 0.75 1.94 -5 -7 8 0.13 1.80 -5 -7 7 346.82 17.49 -5 7 7 334.02 17.39 5 -7 -7 300.96 17.23 -5 -7 7 300.19 14.26 5 7 -7 332.12 14.76 5 7 -7 323.88 16.67 5 -7 -7 293.36 17.40 5 7 -7 314.57 17.91 5 -7 -7 317.00 13.54 5 7 -7 330.18 16.48 5 -7 -7 311.43 16.18 5 7 -7 304.68 15.35 -5 -7 7 318.38 16.23 -5 7 7 301.12 10.29 5 7 -7 307.40 13.81 -5 -7 7 301.98 14.84 -5 7 6 98.87 8.85 -5 -7 6 112.82 9.48 5 -7 -6 111.36 10.18 5 7 -6 98.74 9.47 5 -7 -6 103.00 9.74 -5 -7 6 116.47 8.00 5 7 -6 107.01 7.68 5 7 -6 114.23 9.53 5 -7 -6 114.34 9.22 5 7 -6 114.34 9.06 -5 -7 6 102.61 8.99 5 7 -6 116.96 9.12 5 7 -6 110.41 8.10 -5 -7 6 103.56 8.51 5 7 -5 5.53 2.27 5 -7 -5 6.53 2.44 5 -7 -5 8.11 3.18 5 7 -5 5.46 2.48 -5 -7 5 5.81 1.80 5 7 -5 3.22 1.63 -5 -7 5 7.30 2.70 5 7 -5 3.81 2.34 5 7 -5 10.68 3.19 5 7 -5 4.50 1.64 -5 -7 5 7.08 3.36 5 7 -4 2706.10 54.42 5 -7 -4 2767.52 58.55 5 7 -4 2707.20 58.79 -5 -7 4 2858.73 47.38 -5 -7 4 2778.89 56.71 5 7 -4 2757.30 47.03 5 -7 -4 2769.30 55.08 -5 7 4 2637.67 53.83 -5 -7 4 2727.85 54.63 5 7 -4 2768.17 56.66 5 -7 -4 2825.92 42.34 5 7 -4 2753.45 56.55 -5 -7 4 2737.47 56.57 5 7 -4 2798.14 54.40 -5 -7 3 258.64 13.71 5 7 -3 254.34 12.62 -5 -7 3 243.65 12.77 -5 7 3 261.41 12.62 -5 -7 3 246.91 12.39 5 7 -3 255.30 13.45 5 -7 -3 253.56 7.53 5 7 -3 245.73 13.30 5 -7 -3 257.73 13.85 5 7 -3 240.92 13.46 5 7 -3 249.65 12.44 5 -7 -3 246.53 12.30 5 7 -2 300.64 13.83 -5 -7 2 292.74 13.66 -5 7 2 285.66 13.12 -5 -7 2 272.65 13.08 5 7 -2 300.82 14.63 5 7 -2 286.36 14.58 5 7 -2 288.12 14.39 5 -7 -2 307.73 13.68 5 7 -1 127.94 9.00 -5 -7 1 136.47 9.05 5 7 -1 132.74 9.65 5 -7 -1 131.42 8.87 5 7 -1 127.72 9.26 5 7 -1 137.43 9.98 -5 7 1 136.12 8.83 -5 -7 1 119.95 8.52 -5 -7 0 107.53 7.94 -5 -7 0 100.47 7.87 -5 7 0 104.52 7.85 5 7 0 105.10 8.21 -5 -7 -1 1.46 1.60 5 -7 1 0.95 0.75 -5 -7 -1 -0.14 1.84 -5 -7 -1 -1.81 2.18 -5 7 -1 1.86 1.95 5 7 1 -0.75 1.20 -5 7 -2 669.09 22.40 -5 -7 -2 699.01 22.91 5 7 2 701.97 23.15 -5 -7 -2 669.52 21.72 -5 7 -3 47.03 5.95 -5 -7 -3 42.84 5.77 5 7 3 37.42 5.19 -5 -7 -3 41.62 5.38 5 7 4 126.69 6.12 -5 7 -4 129.16 9.98 -5 -7 -4 127.38 10.11 5 7 4 123.85 9.54 -5 -7 -4 142.45 10.13 5 7 5 33.23 3.80 -5 -7 -5 38.63 6.37 -5 7 -5 32.88 5.75 -5 -7 -5 27.15 4.69 5 7 5 29.09 4.46 5 7 6 339.01 16.27 5 7 6 321.18 13.39 5 7 7 146.05 9.74 5 -7 7 152.26 12.96 5 7 7 172.86 11.54 -5 7 -8 7.25 1.70 5 7 8 5.16 2.46 5 -7 8 3.74 2.93 5 7 8 6.80 2.36 -5 7 -9 18.14 2.60 5 7 9 15.81 3.84 5 -7 9 20.73 5.50 5 7 9 14.23 3.69 5 7 10 453.68 21.31 -5 7 -10 457.99 14.89 5 -7 10 450.03 25.59 5 7 11 2.65 2.31 5 -7 11 -0.86 2.95 5 7 12 3.49 2.83 5 -7 12 1.07 2.78 5 7 13 -0.20 2.90 5 -7 13 0.64 2.72 5 7 14 12.12 4.41 -5 -8 16 33.00 7.89 -5 8 16 40.91 8.91 -5 -8 16 39.40 9.50 -5 -8 15 93.87 12.31 5 8 -15 109.62 13.50 -5 -8 15 94.33 11.29 -5 8 15 84.37 8.40 -5 8 15 83.38 12.42 -5 -8 15 96.88 13.12 -5 -8 14 33.73 7.94 -5 -8 14 28.80 4.99 5 8 -14 30.35 7.33 -5 -8 14 38.98 7.31 -5 8 14 34.23 5.09 -5 8 14 28.90 7.31 -5 -8 14 42.85 8.74 -5 8 13 157.28 15.55 -5 -8 13 122.90 13.62 -5 -8 13 142.73 14.15 -5 -8 13 133.54 12.69 -5 8 13 149.54 10.03 -5 -8 13 148.37 11.08 5 8 -13 150.35 14.84 -5 8 12 205.52 17.11 -5 -8 12 231.97 18.02 -5 -8 12 237.06 17.24 5 8 -12 222.06 17.20 -5 -8 12 225.35 16.17 -5 8 12 224.85 11.85 -5 -8 12 243.09 14.13 -5 8 11 40.03 7.60 -5 -8 11 44.00 7.89 -5 -8 11 49.19 7.67 -5 -8 11 49.32 6.30 5 8 -11 39.67 7.53 -5 -8 11 42.32 6.97 5 -8 -11 44.51 2.07 -5 8 10 384.63 21.48 -5 -8 10 394.28 21.81 -5 -8 10 390.21 20.19 5 8 -10 451.21 22.82 5 8 -10 439.06 20.87 -5 -8 10 369.56 19.70 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6.11 -6 -6 13 10.83 4.46 6 6 -13 19.43 5.43 -6 -6 13 12.04 3.19 -6 -6 13 5.11 2.94 -6 6 13 11.98 3.07 -6 6 13 9.74 4.42 -6 -6 13 10.22 4.64 -6 -6 12 34.19 6.72 -6 -6 12 35.12 5.45 6 6 -12 35.08 6.95 -6 -6 12 35.87 6.44 -6 6 12 33.00 4.81 -6 6 12 39.41 7.75 -6 -6 12 39.88 7.63 -6 6 11 133.76 13.37 -6 -6 11 122.56 12.91 -6 -6 11 146.32 12.67 6 6 -11 132.60 12.73 -6 -6 11 116.50 9.90 -6 6 11 130.49 9.08 -6 -6 11 131.08 12.04 6 -6 -11 126.96 6.57 -6 -6 10 10.57 3.21 6 6 -10 5.77 3.06 -6 -6 10 3.13 2.23 6 6 -10 10.86 3.98 -6 6 10 11.47 4.30 -6 -6 10 5.55 3.25 -6 -6 10 6.45 3.19 6 -6 -10 9.45 2.24 -6 -6 9 10.45 3.91 6 6 -9 7.99 3.24 6 -6 -9 2.07 1.54 -6 -6 9 6.19 2.72 6 6 -9 4.42 3.71 -6 6 9 8.44 4.07 -6 -6 9 8.00 3.98 -6 -6 9 4.72 2.94 6 6 -9 5.47 2.44 -6 6 8 245.74 16.22 -6 -6 8 249.79 16.14 -6 -6 8 242.98 13.50 6 6 -8 256.14 15.90 6 6 -8 262.54 14.29 -6 -6 8 240.11 14.28 -6 -6 8 241.97 15.15 6 6 -8 257.63 13.20 6 -6 -8 256.36 12.31 -6 6 7 6.38 3.00 6 -6 -7 7.08 2.91 6 6 -7 6.14 2.99 -6 -6 7 2.10 2.61 6 -6 -7 3.37 2.21 6 6 -7 3.29 2.77 -6 -6 7 3.56 2.17 6 -6 -7 4.36 2.69 6 6 -7 1.52 1.56 -6 -6 7 2.43 2.02 6 -6 -7 5.63 2.30 6 6 -7 1.72 2.44 6 6 -7 0.24 1.39 6 6 -7 7.33 2.28 -6 -6 7 9.28 3.67 6 -6 -6 74.68 8.72 6 6 -6 70.60 8.56 -6 -6 6 89.45 6.95 6 -6 -6 79.70 8.69 6 6 -6 87.63 6.96 6 6 -6 89.27 8.63 -6 -6 6 93.19 8.59 6 -6 -6 100.13 9.20 6 6 -6 73.27 7.73 6 -6 -6 79.09 7.59 6 -6 -6 80.22 4.91 6 6 -6 85.50 8.28 6 6 -6 78.72 7.27 6 -6 -5 1242.45 37.96 6 6 -5 1269.30 38.81 6 -6 -5 1286.41 36.84 6 6 -5 1309.45 29.11 6 -6 -5 1336.30 36.25 -6 -6 5 1241.55 35.71 -6 6 5 1259.37 34.78 -6 -6 5 1240.42 34.87 6 6 -5 1309.08 35.47 6 6 -5 1288.51 34.97 6 6 -5 1268.99 35.14 6 -6 -5 1273.28 25.42 6 6 -5 1300.16 33.84 6 -6 -4 48.78 6.69 6 6 -4 53.05 6.95 6 6 -4 42.42 5.42 6 6 -4 56.06 4.33 -6 -6 4 52.91 6.73 -6 6 4 46.55 5.92 -6 -6 4 31.96 5.45 6 6 -4 40.76 5.75 6 -6 -4 43.72 3.68 6 6 -4 48.59 6.03 6 -6 -4 48.74 6.09 6 6 -4 48.69 6.09 6 6 -3 1993.82 44.83 6 6 -3 1949.96 32.87 -6 -6 3 1888.94 43.03 -6 6 3 2002.92 45.13 -6 -6 3 1901.54 44.71 -6 -6 3 1921.65 47.10 6 6 -3 2033.69 44.97 6 -6 -3 1907.64 35.77 6 6 -3 1996.99 46.17 6 -6 -3 1944.01 47.80 6 6 -3 1905.62 44.64 6 6 -3 1933.01 48.30 6 -6 -3 1988.00 45.32 6 6 -2 182.86 11.64 -6 -6 2 203.55 11.30 -6 -6 2 197.02 12.10 -6 -6 2 221.50 13.75 -6 6 2 190.53 11.75 6 6 -2 216.22 12.38 6 6 -2 188.81 12.30 6 -6 -2 188.08 12.40 6 6 -2 186.84 12.58 6 -6 -2 201.18 12.09 6 6 -2 190.37 11.77 -6 -6 1 296.65 13.47 -6 -6 1 271.45 15.69 -6 6 1 314.30 15.27 -6 -6 1 306.63 15.13 6 6 -1 282.58 14.41 6 -6 -1 303.45 15.99 6 6 -1 311.91 16.20 6 6 -1 293.36 15.03 6 -6 -1 297.83 15.14 6 6 -1 305.82 15.91 6 6 -1 327.60 15.81 -6 6 0 284.00 14.65 -6 -6 0 286.76 15.06 6 -6 0 278.24 7.09 -6 -6 0 279.25 12.80 6 6 0 292.77 15.21 -6 6 -1 2.26 1.90 -6 -6 -1 6.48 2.55 6 6 1 4.78 2.44 -6 -6 -1 3.33 1.64 -6 -6 -2 272.72 15.14 -6 6 -2 278.36 15.12 6 6 2 289.92 15.43 -6 -6 -2 292.72 12.97 6 6 3 92.89 4.33 -6 6 -3 110.49 9.65 -6 -6 -3 110.44 9.70 6 6 3 93.56 8.80 -6 -6 -3 82.71 6.97 6 6 4 151.18 7.07 -6 -6 -4 135.65 9.26 -6 6 -4 163.06 12.00 -6 -6 -4 146.89 11.62 6 6 4 173.22 12.13 6 6 5 27.27 5.01 -6 -6 -5 22.77 4.19 6 6 5 24.06 3.30 -6 6 -5 23.90 5.16 -6 -6 -5 22.63 5.18 -6 -6 -6 71.44 7.29 6 6 6 80.63 6.67 6 -6 6 70.99 8.67 -6 6 -6 84.13 9.28 -6 -6 -6 89.26 9.76 -6 -6 -7 42.69 5.97 6 6 7 41.59 5.22 -6 6 -7 47.03 7.53 6 -6 7 39.65 6.55 6 -6 8 -2.00 3.11 6 6 8 0.30 1.44 6 -6 9 50.48 8.21 6 6 9 34.64 5.43 6 -6 10 4.29 3.75 6 6 10 5.03 2.90 6 -6 11 74.86 10.97 6 6 11 83.06 9.46 6 -6 12 1.85 4.07 6 6 12 2.53 2.41 6 -6 13 15.44 6.09 -6 -7 16 14.75 5.81 -6 -7 15 0.84 2.57 6 7 -15 1.56 2.94 -6 -7 15 0.17 2.75 -6 7 15 1.79 4.16 -6 -7 15 1.89 3.07 -6 -7 14 3.26 2.04 6 7 -14 -1.43 2.94 -6 7 14 2.91 2.15 -6 -7 14 -1.86 3.60 -6 -7 14 3.51 3.32 -6 7 14 2.76 1.67 -6 -7 14 5.35 5.15 -6 -7 13 62.85 9.31 -6 7 13 55.09 9.68 -6 -7 13 71.21 10.59 6 7 -13 61.17 9.42 -6 7 13 58.79 6.54 -6 -7 13 53.54 8.23 -6 -7 13 68.14 7.93 -6 7 12 190.86 16.71 -6 -7 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5.35 7 -7 -7 34.06 5.59 7 7 -7 30.43 4.45 7 -7 -6 40.16 3.54 7 7 -6 55.84 7.30 -7 -7 6 51.75 7.13 7 -7 -6 50.71 6.90 7 7 -6 40.61 4.68 7 7 -5 5.99 3.03 -7 7 5 8.88 3.53 -7 -7 5 5.38 2.76 -7 -7 5 8.85 3.74 7 -7 -5 2.28 0.98 7 7 -5 4.80 1.89 7 7 -4 1429.16 26.86 -7 7 4 1432.04 39.51 -7 -7 4 1351.28 39.08 -7 -7 4 1429.31 41.83 7 7 -4 1472.62 39.86 7 -7 -4 1384.17 28.82 7 -7 -4 1457.69 43.12 7 7 -4 1460.18 43.15 7 -7 -4 1520.05 40.71 7 7 -4 1441.25 39.76 7 -7 -3 4.69 2.67 7 7 -3 1.93 1.99 -7 -7 3 3.52 2.52 -7 7 3 2.38 2.44 -7 -7 3 1.58 2.79 -7 -7 3 1.50 1.89 7 7 -3 3.68 3.30 7 -7 -3 3.02 1.35 7 -7 -3 2.17 2.12 7 7 -3 -4.68 2.92 -7 -7 2 153.41 10.49 -7 7 2 155.68 11.61 -7 -7 2 148.73 12.55 -7 -7 2 169.03 12.18 7 -7 -2 167.96 8.92 7 7 -2 162.73 11.86 7 -7 -2 155.53 11.65 7 7 -2 163.88 12.02 7 -7 -2 159.52 12.53 7 7 -2 166.13 12.86 7 7 -1 18.11 4.18 7 -7 -1 21.32 2.41 -7 -7 1 23.46 4.05 7 7 -1 15.72 4.35 -7 7 1 16.59 4.35 -7 -7 1 20.54 4.65 7 -7 -1 23.88 4.91 -7 -7 0 103.70 8.24 -7 7 0 107.38 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4.59 8 4 3 20.11 2.76 -8 -4 -3 19.24 2.84 8 4 4 640.67 18.28 -8 4 -4 649.41 28.58 -8 -4 -4 611.27 28.09 -8 -4 -4 601.30 16.81 8 4 5 11.61 2.75 -8 4 -5 9.08 3.52 -8 -4 -5 10.65 4.01 8 -4 5 16.06 4.66 8 4 6 46.72 5.49 -8 4 -6 44.80 7.90 -8 -4 -6 52.64 8.57 8 -4 6 52.50 7.78 8 4 7 23.44 3.98 8 -4 7 25.01 5.85 -8 4 -7 9.76 4.62 -8 -4 -7 24.86 6.50 8 -4 8 -3.90 3.56 -8 4 -8 5.29 3.57 -8 -4 -8 2.29 2.49 8 -4 9 8.27 4.67 -8 4 -9 11.64 5.14 -8 -4 -9 5.93 3.43 8 -4 10 49.26 8.63 8 -4 11 51.65 9.13 -8 -5 15 194.32 17.02 -8 5 14 5.37 4.00 -8 -5 14 4.22 4.39 -8 -5 14 -3.82 3.23 8 5 -14 -0.15 3.11 -8 5 13 20.08 6.41 -8 -5 13 6.63 4.06 -8 -5 13 7.24 3.55 8 5 -13 11.21 4.92 -8 -5 12 65.25 9.27 -8 5 12 60.47 10.13 -8 -5 12 77.05 11.12 8 5 -12 64.64 9.90 8 5 -11 101.97 11.85 -8 5 11 115.52 13.10 -8 -5 11 119.39 13.32 -8 -5 11 101.78 11.20 8 5 -10 1.30 2.45 -8 5 10 5.68 4.01 8 5 -9 22.79 5.59 8 -5 -9 9.37 2.95 8 -5 -9 15.76 3.04 8 5 -9 19.69 4.30 8 -5 -8 52.82 5.13 8 5 -8 49.63 7.41 8 -5 -8 41.76 6.11 8 5 -8 51.04 6.45 8 5 -7 43.11 6.78 8 -5 -7 48.88 6.66 8 -5 -7 43.77 4.62 8 5 -7 40.07 5.43 8 5 -6 15.89 3.97 -8 5 6 18.93 4.88 -8 -5 6 22.73 5.33 8 -5 -6 16.38 4.30 8 -5 -6 16.45 2.90 8 5 -6 13.60 2.94 8 -5 -5 7.63 2.62 8 5 -5 8.63 2.41 -8 5 5 5.14 2.77 -8 -5 5 8.10 3.59 8 5 -5 3.08 2.05 8 -5 -5 10.00 2.32 8 -5 -5 9.63 3.48 8 5 -4 0.76 2.53 -8 5 4 1.11 1.90 -8 -5 4 4.72 2.86 8 -5 -4 3.74 1.69 8 5 -4 1.14 1.04 8 -5 -4 1.21 1.75 8 -5 -3 282.24 11.98 -8 5 3 293.05 17.24 -8 -5 3 251.66 16.41 8 5 -3 284.84 15.38 8 -5 -3 284.88 13.36 8 5 -3 286.93 9.63 8 5 -2 12.52 3.55 8 -5 -2 17.70 2.53 -8 5 2 10.22 3.48 -8 -5 2 17.25 4.77 8 5 -2 12.31 1.56 8 -5 -2 14.51 3.46 8 -5 -1 84.90 4.17 -8 -5 1 78.50 9.00 -8 5 1 79.09 9.08 -8 -5 0 231.93 11.63 -8 5 0 235.99 15.81 -8 -5 0 234.27 15.90 -8 -5 -1 12.86 2.74 -8 5 -1 16.99 4.61 -8 -5 -1 17.20 4.67 8 5 2 229.39 6.24 -8 -5 -2 242.04 11.17 -8 5 -2 229.98 15.95 -8 -5 -2 241.84 16.40 8 5 3 68.79 4.12 -8 -5 -3 61.88 8.74 -8 5 -3 61.97 8.73 -8 -5 -3 68.72 5.75 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8 7 -5 199.80 14.21 -8 7 5 176.70 13.76 -8 -7 5 177.40 13.84 8 -7 -5 195.82 9.14 8 7 -5 196.22 8.60 8 7 -4 184.94 13.42 8 -7 -4 188.75 9.44 -8 7 4 180.57 13.66 -8 -7 4 200.33 14.45 8 7 -3 169.67 12.74 -8 7 3 166.22 12.92 -8 -7 3 163.74 12.94 8 -7 -3 157.55 9.20 8 -7 -3 153.68 8.71 8 7 -2 482.19 21.78 8 -7 -2 460.38 17.25 -8 -7 2 470.52 19.50 8 -7 -2 495.11 14.42 -8 7 2 518.28 23.28 -8 -7 2 501.01 23.22 8 -7 -1 160.89 5.57 -8 -7 1 166.12 11.00 -8 7 1 159.97 12.53 -8 -7 1 152.39 12.63 -8 -7 0 7.98 2.71 -8 7 0 5.80 2.62 -8 -7 0 2.34 2.60 -8 -7 -1 18.64 3.72 -8 7 -1 14.51 4.06 -8 -7 -1 20.63 4.89 -8 -7 -2 81.97 7.24 -8 7 -2 87.65 9.71 -8 -7 -2 92.53 10.27 -8 -7 -3 10.82 2.73 -8 7 -3 5.96 3.63 -8 -7 -3 7.24 3.87 -8 7 -4 32.66 6.27 -8 -7 -4 47.31 7.87 -8 7 -5 292.94 19.09 -8 -7 -5 288.68 19.58 -8 7 -6 102.44 11.68 -8 -7 -6 101.41 11.93 8 -7 6 106.49 11.82 -8 -7 -7 85.10 11.16 -8 7 -7 93.47 11.33 8 -7 7 78.22 10.55 -8 7 -8 8.02 3.97 -8 -7 -8 3.30 3.80 8 -7 8 4.81 4.46 -8 7 -9 24.03 6.55 -8 -7 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12 90.39 10.81 -8 -9 12 76.89 9.50 8 9 -12 84.27 11.63 -8 -9 12 76.30 10.62 -8 -9 12 78.31 11.21 -8 9 12 75.41 10.95 -8 -9 11 34.34 6.81 -8 -9 11 35.13 7.61 8 9 -11 37.11 7.58 -8 -9 10 3.21 2.90 8 9 -10 1.85 2.89 8 -9 -9 0.83 1.80 -8 -9 9 -1.36 2.15 8 9 -9 -3.24 2.75 8 -9 -8 0.32 1.68 -8 -9 8 2.15 2.39 8 9 -8 1.78 3.21 -8 -9 7 -2.73 2.32 8 9 -7 0.25 2.88 -8 -9 6 111.02 11.73 8 -9 -6 92.55 4.91 8 9 -6 95.63 10.51 8 9 -5 58.50 8.33 -8 9 5 53.03 7.54 -8 -9 5 48.76 7.40 -8 -9 5 52.91 8.34 8 -9 -5 48.24 3.68 8 9 -4 330.04 19.35 8 -9 -4 303.05 10.59 -8 9 4 300.86 17.79 -8 -9 4 288.85 17.55 -8 -9 4 297.48 19.46 8 9 -3 775.02 30.57 -8 -9 3 817.57 30.47 -8 9 3 783.14 29.40 -8 -9 3 749.18 32.23 8 -9 -3 777.57 20.19 -8 -9 3 827.89 28.79 8 9 -2 295.43 18.11 -8 9 2 319.76 18.11 -8 -9 2 334.87 18.88 -8 -9 2 308.31 16.64 8 -9 -2 318.32 12.87 -8 9 1 167.08 12.88 -8 -9 1 160.87 12.79 8 -9 -1 166.52 6.31 -8 -9 1 172.86 12.15 -8 9 0 43.53 6.82 -8 -9 0 41.00 6.56 -8 -9 0 35.25 5.43 -8 9 -1 9.99 3.39 -8 -9 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-10 14 2 140.20 13.51 -10 -14 2 136.65 13.47 -10 14 1 4.08 3.16 -10 -14 1 5.06 3.68 -10 14 0 126.73 12.96 -10 -14 0 146.36 14.06 -10 -14 -1 12.42 4.55 -10 14 -1 11.12 4.15 -10 14 -2 59.16 9.08 -10 -14 -2 56.08 9.20 -10 14 -3 16.92 5.15 -10 -14 -3 14.59 5.00 10 15 -7 4.43 4.14 10 15 -6 15.18 6.04 -10 15 4 22.18 5.51 -10 -15 4 22.24 5.93 -10 15 3 8.73 3.99 -10 -15 3 -1.18 2.35 -10 -15 2 12.26 4.37 -10 15 2 4.99 3.06 -10 15 1 69.09 9.49 -10 -15 1 67.11 9.60 -10 15 0 4.77 3.18 -10 -15 0 0.13 3.10 -10 -15 -1 55.66 8.76 -10 15 -1 42.53 7.87 -10 15 -2 6.55 3.66 -10 -15 -2 10.72 4.21 -10 15 -3 60.64 9.31 -10 16 3 7.02 3.49 -10 -16 3 14.73 4.73 -10 16 2 5.85 3.21 -10 -16 2 6.35 2.96 -10 16 1 149.58 13.89 -10 -16 1 163.48 14.78 -10 -16 0 24.73 5.84 -10 16 0 22.57 5.68 -10 -16 -1 20.28 5.72 -10 16 -1 16.73 4.97 -10 -16 -2 -0.10 2.33 -10 16 -2 4.98 2.66 -10 17 3 19.08 5.38 -10 -17 3 6.50 3.14 -10 -17 2 5.12 3.02 -10 -17 1 41.79 7.80 -10 -17 0 26.99 6.33 -10 -17 -1 -0.06 2.35 11 0 -12 0.02 2.24 11 0 -11 0.22 2.28 11 0 -10 114.22 12.51 11 0 -9 4.43 3.55 11 0 -8 696.76 29.40 11 0 -7 5.33 3.34 -11 0 6 38.66 8.05 -11 0 5 -2.44 2.68 -11 0 4 10.68 4.88 -11 0 3 5.27 4.42 -11 0 2 25.20 6.45 -11 0 1 4.50 3.65 -11 0 0 4.74 3.94 -11 0 -1 5.55 3.97 11 -1 -12 54.78 9.18 11 1 -12 62.49 10.06 11 -1 -11 42.88 8.31 11 1 -11 32.61 7.16 11 1 -10 181.47 15.85 11 -1 -10 149.38 14.28 11 -1 -9 -1.26 2.59 11 1 -9 4.63 2.77 11 -1 -8 20.02 4.86 11 1 -8 16.76 5.12 11 -1 -7 225.70 15.17 11 1 -7 210.45 15.26 11 1 -6 65.78 8.37 -11 1 6 90.93 12.28 -11 -1 6 61.23 10.22 -11 1 5 7.61 4.17 -11 -1 5 10.17 4.11 -11 1 4 -0.11 3.61 -11 -1 4 -1.68 3.27 -11 1 3 12.59 5.03 -11 -1 3 7.78 4.17 -11 1 2 2.06 2.97 -11 -1 2 -0.49 2.88 -11 1 1 14.62 6.09 -11 -1 1 1.83 2.52 -11 1 0 2.70 3.53 -11 -1 0 0.08 3.22 -11 1 -1 5.14 3.69 -11 -1 -1 3.79 3.45 11 -2 -12 2.85 2.93 11 2 -12 1.71 2.67 11 -2 -11 19.69 5.47 11 2 -11 34.67 7.53 11 -2 -10 10.92 4.00 11 2 -10 10.32 4.28 11 -2 -9 546.05 26.37 11 2 -9 491.28 25.86 11 -2 -8 36.44 6.27 11 2 -8 35.87 6.74 11 2 -7 270.75 17.54 11 2 -6 66.99 8.40 -11 2 6 53.13 9.19 -11 -2 6 48.90 9.01 -11 2 5 18.14 5.72 -11 -2 5 10.52 4.44 -11 2 4 3.14 2.79 -11 -2 4 2.70 3.26 -11 2 3 -1.72 3.13 -11 -2 3 0.91 2.56 -11 2 2 37.50 7.87 -11 -2 2 42.16 8.95 -11 -2 1 239.36 19.58 -11 2 1 295.86 21.59 -11 2 0 134.23 14.67 -11 -2 0 168.79 16.53 -11 2 -1 -0.79 2.61 -11 -2 -1 0.34 3.19 11 -3 -12 8.75 4.40 11 -3 -11 108.58 12.45 11 3 -11 116.43 13.46 11 -3 -10 3.75 2.63 11 3 -10 6.08 3.57 11 -3 -9 41.27 7.38 11 3 -9 34.74 7.04 11 -3 -8 223.19 15.47 11 3 -8 167.50 14.49 11 3 -7 24.62 5.62 11 3 -6 218.27 15.50 -11 3 6 216.36 18.59 -11 -3 6 195.07 17.82 11 3 -5 31.77 6.15 -11 3 5 18.81 6.05 -11 -3 5 30.47 7.39 -11 3 4 5.31 3.56 -11 -3 4 2.16 3.33 -11 3 3 -2.72 3.07 -11 -3 3 -7.59 4.97 -11 3 2 185.04 16.95 -11 -3 2 160.55 15.97 -11 -3 1 1.55 4.12 -11 3 1 2.76 3.32 -11 3 0 7.34 4.29 -11 -3 0 14.51 5.30 -11 3 -1 4.15 4.07 -11 -3 -1 18.74 6.21 11 -4 -12 0.60 2.88 11 -4 -11 39.12 7.35 11 4 -11 41.38 8.27 11 -4 -10 28.14 6.36 11 4 -10 45.37 8.08 11 -4 -9 -3.52 3.23 11 4 -9 -1.75 2.87 11 4 -8 239.39 17.65 11 4 -7 17.06 4.74 -11 4 6 23.37 6.69 -11 -4 6 19.84 6.37 11 4 -6 13.82 4.53 -11 4 5 15.31 5.37 -11 -4 5 14.26 4.77 11 4 -5 5.70 3.42 -11 4 4 10.83 4.58 -11 -4 4 1.89 3.30 -11 4 3 5.76 4.14 -11 -4 3 5.49 2.83 -11 4 2 105.15 12.80 -11 -4 2 100.18 12.63 -11 4 1 324.82 22.54 -11 -4 1 326.17 23.06 -11 4 0 122.75 13.97 -11 -4 0 146.48 15.29 -11 4 -1 223.71 19.14 -11 -4 -1 282.76 21.52 11 -5 -11 3.78 2.60 11 5 -11 4.95 3.81 11 -5 -10 14.44 4.61 11 5 -10 16.77 5.52 11 5 -9 29.55 6.80 11 5 -8 34.29 6.91 11 5 -7 296.84 19.54 11 5 -6 70.58 9.35 -11 5 6 74.84 10.92 -11 -5 6 77.51 11.13 11 5 -5 24.10 5.29 -11 5 5 11.19 4.17 -11 -5 5 14.33 5.25 -11 5 4 22.14 5.87 -11 -5 4 27.14 7.03 -11 5 3 52.18 8.94 -11 -5 3 36.80 7.96 -11 5 2 6.65 3.55 -11 -5 2 0.65 2.47 -11 -5 1 52.55 9.42 -11 5 1 69.34 10.53 -11 5 0 7.11 4.38 -11 -5 0 5.57 4.30 -11 5 -1 9.43 4.05 -11 -5 -1 5.40 4.84 11 -6 -11 36.92 7.28 11 6 -11 35.34 7.84 11 6 -10 0.97 4.42 11 6 -9 46.70 8.36 11 6 -8 13.06 5.12 11 6 -7 47.13 7.93 11 6 -6 0.49 1.78 -11 6 6 8.27 4.12 -11 -6 6 4.61 3.81 -11 6 5 2.77 3.20 -11 -6 5 -0.91 2.81 11 6 -4 42.46 7.31 -11 6 4 37.02 7.75 -11 -6 4 42.18 8.49 -11 6 3 20.17 6.13 -11 -6 3 9.90 4.27 -11 6 2 -3.85 3.66 -11 -6 2 -2.12 2.89 -11 6 1 356.52 23.48 -11 -6 1 343.82 23.41 -11 6 0 216.63 18.41 -11 -6 0 187.24 17.37 -11 6 -1 46.10 8.42 11 7 -10 19.26 5.70 11 7 -9 26.96 6.79 11 7 -8 290.96 20.74 11 7 -7 19.37 5.49 11 7 -6 198.24 16.30 -11 7 6 182.16 16.94 -11 -7 6 186.93 17.46 11 7 -5 11.63 4.07 -11 7 5 1.60 2.55 -11 -7 5 11.41 5.11 11 7 -4 -4.92 3.83 -11 -7 4 3.92 2.95 -11 7 4 3.71 2.63 -11 7 3 14.78 5.63 -11 -7 3 19.20 6.47 -11 7 2 83.85 11.34 -11 -7 2 102.21 12.64 -11 7 1 3.51 3.60 -11 -7 1 11.71 4.92 -11 7 0 54.96 9.30 -11 -7 0 50.17 9.31 -11 7 -1 4.91 4.03 11 8 -10 8.71 5.41 11 8 -9 29.09 7.47 11 8 -8 101.41 12.50 11 8 -7 56.38 9.24 11 8 -6 5.49 2.99 -11 8 6 1.56 2.93 -11 -8 6 1.62 3.03 11 8 -5 3.57 2.58 -11 8 5 5.41 2.95 -11 -8 5 4.63 3.16 11 8 -4 53.65 8.61 -11 8 4 41.60 8.32 -11 -8 4 66.06 10.48 -11 8 3 26.94 6.72 -11 -8 3 30.66 6.93 -11 8 2 303.70 21.58 -11 -8 2 309.95 22.16 -11 8 1 137.51 14.60 -11 -8 1 112.59 13.51 -11 8 0 327.95 22.64 -11 -8 0 354.26 23.79 11 9 -9 91.09 12.40 11 9 -8 1.47 2.89 11 9 -7 156.19 15.59 11 9 -6 38.98 7.57 -11 -9 6 38.28 8.10 11 9 -5 0.31 2.77 -11 9 5 1.34 3.14 -11 -9 5 -2.44 3.77 -11 9 4 49.14 8.49 -11 -9 4 52.12 8.88 -11 9 3 2.67 3.63 -11 -9 3 -1.74 2.78 -11 9 2 43.60 8.51 -11 -9 2 38.72 7.81 -11 9 1 209.58 17.80 -11 -9 1 219.22 18.51 -11 9 0 42.16 8.32 11 10 -9 2.34 2.93 11 10 -8 177.96 17.83 11 10 -7 41.51 8.51 11 10 -6 122.51 13.97 11 10 -5 7.35 3.51 -11 10 5 17.62 5.95 -11 -10 5 12.63 5.12 -11 10 4 68.46 10.33 -11 -10 4 73.76 10.78 -11 10 3 2.73 2.65 -11 -10 3 5.12 3.76 -11 10 2 4.88 3.30 -11 -10 2 6.53 3.80 -11 10 1 73.94 10.50 -11 -10 1 68.54 10.38 -11 10 0 170.84 16.22 11 11 -8 35.50 8.11 11 11 -7 4.58 4.01 11 11 -6 2.33 2.79 11 11 -5 58.71 9.98 -11 11 5 61.97 9.78 -11 -11 5 60.87 9.99 -11 11 4 -7.67 3.90 -11 -11 4 0.72 3.31 -11 -11 3 19.91 5.59 -11 11 3 23.95 6.18 -11 11 2 71.18 10.29 -11 -11 2 68.37 10.49 -11 11 1 44.99 8.20 -11 -11 1 43.31 8.39 11 12 -8 22.39 6.75 11 12 -7 8.79 4.20 11 12 -6 3.37 4.39 -11 12 5 78.14 10.91 -11 12 4 6.10 3.45 -11 -12 4 4.35 3.14 -11 12 3 115.73 13.30 -11 -12 3 135.24 14.23 -11 12 2 9.38 4.16 -11 12 1 69.95 10.24 11 13 -7 18.18 6.91 11 13 -6 1.69 3.61 -11 13 4 2.61 3.51 -11 13 3 46.11 8.47 -11 13 2 145.45 14.67 0 0 0 0.00 0.00 TITL SE21001_refinalized in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 9.186444 20.870163 13.575934 90.0000 101.6061 90.0000 ZERR 5.00 0.000329 0.000679 0.000452 0.0000 0.0034 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H B O P Mn UNIT 90.00 230.00 5.00 10.00 20.00 5.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 20675 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems Cryostream 700+' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a MITIGEN holder in perfluoroether oil' _olex2_submission_original_sample_id LAB181 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.306 _oxdiff_exptl_absorpt_empirical_full_min 0.734 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mn1 Mn 0.35603(2) 0.39115(2) 0.29166(2) 0.01127(6) Uani 1 1 d . . . . . H1C H 0.208(2) 0.4245(8) 0.2428(14) 0.025(5) Uiso 1 1 d . . . . . H1D H 0.4088(19) 0.4642(8) 0.3048(13) 0.022(4) Uiso 1 1 d . . . . . P1 P 0.28401(4) 0.39213(2) 0.43925(3) 0.01356(9) Uani 1 1 d . . . . . P2 P 0.22687(4) 0.30146(2) 0.26463(3) 0.01432(9) Uani 1 1 d . . . . . P3 P 0.44597(4) 0.38844(2) 0.15116(3) 0.01554(9) Uani 1 1 d . . . . . P4 P 0.57942(4) 0.35389(2) 0.35851(3) 0.01477(9) Uani 1 1 d . . . . . O1 O 0.21232(12) 0.52821(5) 0.31003(7) 0.0159(2) Uani 1 1 d . . . . . O2 O 0.25682(12) 0.50899(5) 0.15177(8) 0.0165(2) Uani 1 1 d . . . . . C1 C 0.22480(19) 0.31053(8) 0.46736(12) 0.0194(3) Uani 1 1 d . . . . . H1A H 0.173(2) 0.3127(8) 0.5212(14) 0.025(5) Uiso 1 1 d . . . . . H1B H 0.312(2) 0.2854(9) 0.4877(14) 0.023(5) Uiso 1 1 d . . . . . C2 C 0.1309(2) 0.28370(8) 0.37039(12) 0.0208(3) Uani 1 1 d . . . . . H2A H 0.037(2) 0.3050(8) 0.3556(13) 0.022(5) Uiso 1 1 d . . . . . H2B H 0.114(2) 0.2380(10) 0.3738(14) 0.031(5) Uiso 1 1 d . . . . . C3 C 0.4032(2) 0.41398(9) 0.55954(12) 0.0206(3) Uani 1 1 d . . . . . H3A H 0.434(2) 0.4560(10) 0.5579(14) 0.029(5) Uiso 1 1 d . . . . . H3B H 0.490(2) 0.3865(9) 0.5749(14) 0.027(5) Uiso 1 1 d . . . . . H3C H 0.352(2) 0.4096(9) 0.6140(15) 0.031(5) Uiso 1 1 d . . . . . C4 C 0.11648(19) 0.43616(8) 0.45282(13) 0.0204(3) Uani 1 1 d . . . . . H4A H 0.037(2) 0.4263(9) 0.3978(15) 0.025(5) Uiso 1 1 d . . . . . H4B H 0.084(2) 0.4235(9) 0.5137(15) 0.031(5) Uiso 1 1 d . . . . . H4C H 0.1355(19) 0.4792(9) 0.4525(13) 0.017(4) Uiso 1 1 d . . . . . C5 C 0.06560(19) 0.30043(8) 0.15928(12) 0.0210(3) Uani 1 1 d . . . . . H5A H 0.002(2) 0.2644(9) 0.1609(14) 0.028(5) Uiso 1 1 d . . . . . H5B H 0.007(2) 0.3393(10) 0.1616(14) 0.031(5) Uiso 1 1 d . . . . . H5C H 0.097(2) 0.2997(9) 0.0959(16) 0.036(5) Uiso 1 1 d . . . . . C6 C 0.3015(2) 0.22096(8) 0.24792(14) 0.0234(4) Uani 1 1 d . . . . . H6A H 0.367(2) 0.2099(10) 0.3052(17) 0.038(6) Uiso 1 1 d . . . . . H6B H 0.227(2) 0.1891(9) 0.2372(14) 0.028(5) Uiso 1 1 d . . . . . H6C H 0.351(2) 0.2208(9) 0.1909(15) 0.026(5) Uiso 1 1 d . . . . . C7 C 0.5829(2) 0.32293(8) 0.15793(12) 0.0218(3) Uani 1 1 d . . . . . H7A H 0.636(2) 0.3260(8) 0.1037(14) 0.025(5) Uiso 1 1 d . . . . . H7B H 0.534(2) 0.2834(9) 0.1512(14) 0.026(5) Uiso 1 1 d . . . . . C8 C 0.6849(2) 0.32581(9) 0.26144(13) 0.0243(4) Uani 1 1 d . . . . . H8A H 0.763(2) 0.3565(9) 0.2591(14) 0.024(5) Uiso 1 1 d . . . . . H8B H 0.729(2) 0.2851(10) 0.2822(15) 0.031(5) Uiso 1 1 d . . . . . C9 C 0.3338(2) 0.37896(10) 0.02399(12) 0.0256(4) Uani 1 1 d . . . . . H9A H 0.283(2) 0.3388(10) 0.0180(15) 0.034(5) Uiso 1 1 d . . . . . H9B H 0.265(2) 0.4127(10) 0.0119(15) 0.035(6) Uiso 1 1 d . . . . . H9C H 0.397(2) 0.3802(9) -0.0251(17) 0.040(6) Uiso 1 1 d . . . . . C10 C 0.5647(2) 0.45578(8) 0.12925(14) 0.0226(4) Uani 1 1 d . . . . . H10A H 0.609(2) 0.4481(9) 0.0722(15) 0.029(5) Uiso 1 1 d . . . . . H10B H 0.638(2) 0.4608(9) 0.1850(16) 0.031(5) Uiso 1 1 d . . . . . H10C H 0.507(2) 0.4936(10) 0.1186(15) 0.033(5) Uiso 1 1 d . . . . . C11 C 0.6176(2) 0.28655(8) 0.44818(13) 0.0214(3) Uani 1 1 d . . . . . H11A H 0.720(2) 0.2764(9) 0.4638(14) 0.026(5) Uiso 1 1 d . . . . . H11B H 0.565(2) 0.2503(10) 0.4215(15) 0.032(5) Uiso 1 1 d . . . . . H11C H 0.590(2) 0.2967(9) 0.5074(15) 0.026(5) Uiso 1 1 d . . . . . C12 C 0.71533(19) 0.41036(9) 0.42799(14) 0.0229(3) Uani 1 1 d . . . . . H12A H 0.723(2) 0.4469(9) 0.3830(15) 0.031(5) Uiso 1 1 d . . . . . H12B H 0.809(2) 0.3911(9) 0.4484(15) 0.027(5) Uiso 1 1 d . . . . . H12C H 0.681(2) 0.4250(9) 0.4853(16) 0.034(5) Uiso 1 1 d . . . . . C13 C 0.12469(17) 0.57319(7) 0.24291(11) 0.0177(3) Uani 1 1 d . . . . . C14 C -0.0332(2) 0.54716(10) 0.21396(14) 0.0267(4) Uani 1 1 d . . . . . H14A H -0.039(2) 0.5077(10) 0.1777(15) 0.031(5) Uiso 1 1 d . . . . . H14B H -0.071(2) 0.5398(9) 0.2760(15) 0.032(5) Uiso 1 1 d . . . . . H14C H -0.095(2) 0.5761(10) 0.1730(15) 0.032(5) Uiso 1 1 d . . . . . C15 C 0.1245(2) 0.63693(8) 0.29700(14) 0.0264(4) Uani 1 1 d . . . . . H15A H 0.221(2) 0.6518(9) 0.3276(15) 0.032(5) Uiso 1 1 d . . . . . H15B H 0.067(2) 0.6329(9) 0.3488(16) 0.034(5) Uiso 1 1 d . . . . . H15C H 0.076(2) 0.6703(10) 0.2485(16) 0.036(5) Uiso 1 1 d . . . . . C16 C 0.20667(17) 0.57426(7) 0.15338(11) 0.0174(3) Uani 1 1 d . . . . . C17 C 0.3433(2) 0.61742(8) 0.17290(14) 0.0253(4) Uani 1 1 d . . . . . H17A H 0.320(2) 0.6614(10) 0.1753(15) 0.033(5) Uiso 1 1 d . . . . . H17B H 0.403(2) 0.6078(8) 0.2348(15) 0.024(5) Uiso 1 1 d . . . . . H17C H 0.399(2) 0.6105(9) 0.1198(16) 0.034(5) Uiso 1 1 d . . . . . C18 C 0.1091(2) 0.59033(9) 0.05218(13) 0.0266(4) Uani 1 1 d . . . . . H18A H 0.069(2) 0.6311(10) 0.0545(15) 0.033(5) Uiso 1 1 d . . . . . H18B H 0.167(2) 0.5910(10) 0.0003(16) 0.039(6) Uiso 1 1 d . . . . . H18C H 0.030(2) 0.5606(9) 0.0307(14) 0.025(5) Uiso 1 1 d . . . . . B1 B 0.27123(19) 0.48248(8) 0.25031(12) 0.0148(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Mn1 0.01184(12) 0.01010(12) 0.01181(11) 0.00033(8) 0.00222(8) 0.00004(8) P1 0.0142(2) 0.01377(19) 0.01292(18) 0.00003(13) 0.00322(15) -0.00168(14) P2 0.0164(2) 0.01213(19) 0.01362(18) 0.00036(13) 0.00101(15) -0.00171(15) P3 0.0166(2) 0.0172(2) 0.01354(18) -0.00073(14) 0.00450(15) 0.00010(15) P4 0.01348(19) 0.01462(19) 0.01596(19) 0.00030(14) 0.00238(15) 0.00174(15) O1 0.0196(6) 0.0133(5) 0.0147(5) 0.0020(4) 0.0034(4) 0.0049(4) O2 0.0211(6) 0.0131(5) 0.0158(5) 0.0023(4) 0.0050(4) 0.0039(4) C1 0.0230(9) 0.0192(8) 0.0165(8) 0.0024(6) 0.0046(7) -0.0034(7) C2 0.0236(9) 0.0185(9) 0.0208(8) 0.0016(6) 0.0059(7) -0.0083(7) C3 0.0214(9) 0.0234(9) 0.0169(8) -0.0031(6) 0.0035(7) -0.0017(7) C4 0.0190(9) 0.0220(9) 0.0224(8) 0.0010(6) 0.0089(7) 0.0006(7) C5 0.0197(9) 0.0211(9) 0.0197(8) 0.0020(6) -0.0020(7) -0.0042(7) C6 0.0285(10) 0.0135(8) 0.0259(9) -0.0016(6) 0.0004(8) -0.0007(7) C7 0.0250(9) 0.0205(9) 0.0226(8) -0.0032(6) 0.0108(7) 0.0031(7) C8 0.0205(9) 0.0278(10) 0.0264(9) 0.0010(7) 0.0091(7) 0.0083(8) C9 0.0258(10) 0.0361(11) 0.0149(8) -0.0028(7) 0.0037(7) -0.0017(8) C10 0.0219(9) 0.0239(9) 0.0246(9) 0.0023(7) 0.0107(8) -0.0014(7) C11 0.0221(9) 0.0190(9) 0.0215(8) 0.0027(6) 0.0004(7) 0.0045(7) C12 0.0154(9) 0.0239(9) 0.0281(9) -0.0016(7) 0.0011(7) -0.0026(7) C13 0.0200(8) 0.0163(8) 0.0162(7) 0.0025(6) 0.0022(6) 0.0062(6) C14 0.0198(9) 0.0328(11) 0.0273(9) 0.0019(8) 0.0041(7) 0.0046(8) C15 0.0368(11) 0.0187(9) 0.0232(9) 0.0000(7) 0.0049(8) 0.0111(8) C16 0.0209(8) 0.0135(7) 0.0173(7) 0.0033(5) 0.0030(6) 0.0041(6) C17 0.0305(10) 0.0175(9) 0.0285(10) 0.0048(7) 0.0072(8) -0.0009(7) C18 0.0312(10) 0.0280(10) 0.0190(8) 0.0056(7) 0.0016(7) 0.0088(8) B1 0.0144(8) 0.0140(8) 0.0156(8) 0.0016(6) 0.0024(6) 0.0001(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -1 0 0.0281 0 1 0 0.0712 -3 -2 19 0.1777 -12 -4 11 0.1967 -7 -1 -14 0.1307 8 3 -17 0.2031 11 3 5 0.1526 6 1 15 0.1526 -7 24 6 0.1181 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1C Mn1 H1D 80.8(9) . . ? P1 Mn1 H1C 89.2(6) . . ? P1 Mn1 H1D 91.7(6) . . ? P2 Mn1 H1C 85.0(6) . . ? P2 Mn1 H1D 165.5(6) . . ? P2 Mn1 P1 84.862(15) . . ? P2 Mn1 P3 96.646(16) . . ? P2 Mn1 P4 101.154(17) . . ? P3 Mn1 H1C 95.2(6) . . ? P3 Mn1 H1D 87.9(6) . . ? P3 Mn1 P1 175.456(18) . . ? P4 Mn1 H1C 173.6(6) . . ? P4 Mn1 H1D 93.1(6) . . ? P4 Mn1 P1 93.035(16) . . ? P4 Mn1 P3 82.473(16) . . ? B1 Mn1 H1C 39.7(6) . . ? B1 Mn1 H1D 41.4(6) . . ? B1 Mn1 P1 94.07(5) . . ? B1 Mn1 P2 124.70(5) . . ? B1 Mn1 P3 88.60(5) . . ? B1 Mn1 P4 134.03(5) . . ? C1 P1 Mn1 109.22(5) . . ? C3 P1 Mn1 124.79(6) . . ? C3 P1 C1 101.13(8) . . ? C3 P1 C4 98.56(8) . . ? C4 P1 Mn1 120.07(6) . . ? C4 P1 C1 98.80(8) . . ? C2 P2 Mn1 111.21(5) . . ? C5 P2 Mn1 117.44(6) . . ? C5 P2 C2 99.47(8) . . ? C5 P2 C6 98.89(8) . . ? C6 P2 Mn1 126.30(6) . . ? C6 P2 C2 99.11(8) . . ? C7 P3 Mn1 110.03(5) . . ? C9 P3 Mn1 125.01(6) . . ? C9 P3 C7 102.43(8) . . ? C9 P3 C10 99.75(9) . . ? C10 P3 Mn1 116.96(6) . . ? C10 P3 C7 98.81(8) . . ? C8 P4 Mn1 112.87(6) . . ? C11 P4 Mn1 125.15(6) . . ? C11 P4 C8 99.71(8) . . ? C12 P4 Mn1 117.68(6) . . ? C12 P4 C8 99.63(8) . . ? C12 P4 C11 97.52(8) . . ? B1 O1 C13 107.74(11) . . ? B1 O2 C16 108.77(11) . . ? P1 C1 H1A 109.2(11) . . ? P1 C1 H1B 107.5(11) . . ? H1A C1 H1B 109.2(15) . . ? C2 C1 P1 107.34(11) . . ? C2 C1 H1A 113.3(11) . . ? C2 C1 H1B 110.2(11) . . ? P2 C2 H2A 106.9(11) . . ? P2 C2 H2B 109.8(11) . . ? C1 C2 P2 108.54(11) . . ? C1 C2 H2A 109.8(11) . . ? C1 C2 H2B 112.9(12) . . ? H2A C2 H2B 108.7(15) . . ? P1 C3 H3A 110.3(12) . . ? P1 C3 H3B 111.2(11) . . ? P1 C3 H3C 111.4(12) . . ? H3A C3 H3B 108.8(16) . . ? H3A C3 H3C 108.2(16) . . ? H3B C3 H3C 106.8(16) . . ? P1 C4 H4A 109.7(11) . . ? P1 C4 H4B 110.8(11) . . ? P1 C4 H4C 109.1(10) . . ? H4A C4 H4B 107.1(15) . . ? H4A C4 H4C 108.9(15) . . ? H4B C4 H4C 111.3(15) . . ? P2 C5 H5A 113.1(11) . . ? P2 C5 H5B 109.1(12) . . ? P2 C5 H5C 111.1(12) . . ? H5A C5 H5B 108.0(15) . . ? H5A C5 H5C 107.5(16) . . ? H5B C5 H5C 107.8(16) . . ? P2 C6 H6A 108.9(13) . . ? P2 C6 H6B 112.6(11) . . ? P2 C6 H6C 110.2(11) . . ? H6A C6 H6B 106.7(17) . . ? H6A C6 H6C 109.9(16) . . ? H6B C6 H6C 108.4(15) . . ? P3 C7 H7A 111.0(11) . . ? P3 C7 H7B 109.7(11) . . ? H7A C7 H7B 106.9(15) . . ? C8 C7 P3 107.62(11) . . ? C8 C7 H7A 112.9(11) . . ? C8 C7 H7B 108.6(12) . . ? P4 C8 H8A 107.9(11) . . ? P4 C8 H8B 108.6(11) . . ? C7 C8 P4 110.51(11) . . ? C7 C8 H8A 108.5(11) . . ? C7 C8 H8B 112.4(12) . . ? H8A C8 H8B 108.8(16) . . ? P3 C9 H9A 110.3(12) . . ? P3 C9 H9B 108.3(13) . . ? P3 C9 H9C 109.9(13) . . ? H9A C9 H9B 110.3(17) . . ? H9A C9 H9C 108.4(16) . . ? H9B C9 H9C 109.5(17) . . ? P3 C10 H10A 111.5(11) . . ? P3 C10 H10B 108.3(12) . . ? P3 C10 H10C 109.1(12) . . ? H10A C10 H10B 109.3(16) . . ? H10A C10 H10C 109.4(16) . . ? H10B C10 H10C 109.1(17) . . ? P4 C11 H11A 111.4(11) . . ? P4 C11 H11B 110.4(12) . . ? P4 C11 H11C 110.7(11) . . ? H11A C11 H11B 108.5(16) . . ? H11A C11 H11C 107.3(16) . . ? H11B C11 H11C 108.4(16) . . ? P4 C12 H12A 107.6(11) . . ? P4 C12 H12B 111.5(11) . . ? P4 C12 H12C 109.1(12) . . ? H12A C12 H12B 109.9(15) . . ? H12A C12 H12C 109.4(16) . . ? H12B C12 H12C 109.3(17) . . ? O1 C13 C14 108.26(13) . . ? O1 C13 C15 108.70(13) . . ? O1 C13 C16 101.98(11) . . ? C14 C13 C16 112.91(13) . . ? C15 C13 C14 110.04(14) . . ? C15 C13 C16 114.42(13) . . ? C13 C14 H14A 113.1(12) . . ? C13 C14 H14B 108.3(12) . . ? C13 C14 H14C 110.7(12) . . ? H14A C14 H14B 108.2(16) . . ? H14A C14 H14C 106.7(17) . . ? H14B C14 H14C 109.8(16) . . ? C13 C15 H15A 114.0(12) . . ? C13 C15 H15B 109.2(12) . . ? C13 C15 H15C 109.7(12) . . ? H15A C15 H15B 108.0(17) . . ? H15A C15 H15C 108.3(16) . . ? H15B C15 H15C 107.5(16) . . ? O2 C16 C13 101.85(11) . . ? O2 C16 C17 107.87(13) . . ? O2 C16 C18 109.12(13) . . ? C17 C16 C13 112.61(13) . . ? C18 C16 C13 114.85(13) . . ? C18 C16 C17 110.00(14) . . ? C16 C17 H17A 113.2(12) . . ? C16 C17 H17B 110.3(11) . . ? C16 C17 H17C 108.8(12) . . ? H17A C17 H17B 106.1(16) . . ? H17A C17 H17C 109.1(16) . . ? H17B C17 H17C 109.3(16) . . ? C16 C18 H18A 109.8(13) . . ? C16 C18 H18B 110.5(13) . . ? C16 C18 H18C 114.0(11) . . ? H18A C18 H18B 107.1(17) . . ? H18A C18 H18C 108.5(17) . . ? H18B C18 H18C 106.6(16) . . ? Mn1 B1 H1C 48.0(8) . . ? Mn1 B1 H1D 49.8(7) . . ? H1C B1 H1D 97.5(11) . . ? O1 B1 Mn1 128.30(11) . . ? O1 B1 H1C 115.9(7) . . ? O1 B1 H1D 106.9(7) . . ? O1 B1 O2 107.37(12) . . ? O2 B1 Mn1 124.27(11) . . ? O2 B1 H1C 108.8(8) . . ? O2 B1 H1D 120.6(7) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Mn1 H1C 1.556(18) . ? Mn1 H1D 1.599(17) . ? Mn1 P1 2.2330(4) . ? Mn1 P2 2.2072(4) . ? Mn1 P3 2.2267(4) . ? Mn1 P4 2.2114(5) . ? Mn1 B1 2.0926(17) . ? P1 C1 1.8506(16) . ? P1 C3 1.8314(17) . ? P1 C4 1.8334(16) . ? P2 C2 1.8668(16) . ? P2 C5 1.8408(17) . ? P2 C6 1.8455(17) . ? P3 C7 1.8477(17) . ? P3 C9 1.8347(18) . ? P3 C10 1.8397(17) . ? P4 C8 1.8798(16) . ? P4 C11 1.8462(17) . ? P4 C12 1.8340(17) . ? O1 C13 1.4368(18) . ? O1 B1 1.4275(19) . ? O2 C16 1.4396(18) . ? O2 B1 1.4290(19) . ? C1 H1A 0.951(18) . ? C1 H1B 0.954(19) . ? C1 C2 1.528(2) . ? C2 H2A 0.953(19) . ? C2 H2B 0.97(2) . ? C3 H3A 0.92(2) . ? C3 H3B 0.97(2) . ? C3 H3C 0.959(19) . ? C4 H4A 0.96(2) . ? C4 H4B 0.97(2) . ? C4 H4C 0.914(18) . ? C5 H5A 0.96(2) . ? C5 H5B 0.98(2) . ? C5 H5C 0.96(2) . ? C6 H6A 0.91(2) . ? C6 H6B 0.94(2) . ? C6 H6C 0.974(19) . ? C7 H7A 0.965(18) . ? C7 H7B 0.935(19) . ? C7 C8 1.525(2) . ? C8 H8A 0.967(19) . ? C8 H8B 0.96(2) . ? C9 H9A 0.95(2) . ? C9 H9B 0.93(2) . ? C9 H9C 0.97(2) . ? C10 H10A 0.959(19) . ? C10 H10B 0.91(2) . ? C10 H10C 0.95(2) . ? C11 H11A 0.949(19) . ? C11 H11B 0.93(2) . ? C11 H11C 0.917(19) . ? C12 H12A 0.99(2) . ? C12 H12B 0.94(2) . ? C12 H12C 0.95(2) . ? C13 C14 1.524(2) . ? C13 C15 1.520(2) . ? C13 C16 1.553(2) . ? C14 H14A 0.95(2) . ? C14 H14B 0.98(2) . ? C14 H14C 0.93(2) . ? C15 H15A 0.95(2) . ? C15 H15B 0.97(2) . ? C15 H15C 1.00(2) . ? C16 C17 1.525(2) . ? C16 C18 1.519(2) . ? C17 H17A 0.94(2) . ? C17 H17B 0.93(2) . ? C17 H17C 0.98(2) . ? C18 H18A 0.93(2) . ? C18 H18B 0.97(2) . ? C18 H18C 0.957(19) . ? B1 H1C 1.338(17) . ? B1 H1D 1.383(17) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Mn1 P1 C1 C2 -43.22(13) . . . . ? Mn1 P2 C2 C1 -30.63(13) . . . . ? Mn1 P3 C7 C8 -45.39(13) . . . . ? Mn1 P4 C8 C7 -10.76(14) . . . . ? P1 C1 C2 P2 45.01(14) . . . . ? P3 C7 C8 P4 33.56(15) . . . . ? O1 C13 C16 O2 34.25(14) . . . . ? O1 C13 C16 C17 -81.03(15) . . . . ? O1 C13 C16 C18 152.02(14) . . . . ? C3 P1 C1 C2 -176.41(12) . . . . ? C4 P1 C1 C2 83.00(13) . . . . ? C5 P2 C2 C1 -155.09(12) . . . . ? C6 P2 C2 C1 104.23(13) . . . . ? C9 P3 C7 C8 179.73(12) . . . . ? C10 P3 C7 C8 77.63(13) . . . . ? C11 P4 C8 C7 124.16(13) . . . . ? C12 P4 C8 C7 -136.42(13) . . . . ? C13 O1 B1 Mn1 -161.12(12) . . . . ? C13 O1 B1 O2 16.37(16) . . . . ? C14 C13 C16 O2 -81.70(15) . . . . ? C14 C13 C16 C17 163.02(14) . . . . ? C14 C13 C16 C18 36.07(19) . . . . ? C15 C13 C16 O2 151.40(13) . . . . ? C15 C13 C16 C17 36.12(19) . . . . ? C15 C13 C16 C18 -90.83(18) . . . . ? C16 O2 B1 Mn1 -175.15(11) . . . . ? C16 O2 B1 O1 7.23(16) . . . . ? B1 O1 C13 C14 88.07(14) . . . . ? B1 O1 C13 C15 -152.41(13) . . . . ? B1 O1 C13 C16 -31.21(15) . . . . ? B1 O2 C16 C13 -25.56(15) . . . . ? B1 O2 C16 C17 93.15(14) . . . . ? B1 O2 C16 C18 -147.38(14) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.0000 -1.0001 -0.0000 0.0337 -0.0016 0.0041 0.0000 1.0001 0.0000 -0.0337 0.0016 -0.0041 -3.0728 -1.6857 19.0961 0.0212 0.7874 0.6160 -11.6436 -3.5958 11.3727 0.0024 0.0158 0.9999 -6.7390 -1.1400 -13.9765 -0.0248 -0.9914 0.1288 8.4357 2.9888 -16.6198 -0.0124 -0.4193 -0.9078 11.4586 2.7912 5.1353 0.0185 0.7790 -0.6267 5.6656 0.8026 15.1545 0.0252 0.9991 -0.0338 -6.9698 23.9539 6.1845 -0.8782 0.0214 0.4779