#------------------------------------------------------------------------------ #$Date: 2021-06-26 00:36:02 +0300 (Sat, 26 Jun 2021) $ #$Revision: 266689 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/88/4518833.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4518833 loop_ _publ_author_name 'Gonz\'alez, Bruno' 'Fag\'undez, Catherine' 'Peixoto de Abreu Lima, Alejandro' 'Suescun, Leopoldo' 'Sellanes, Diver' 'Seoane, Gustavo A.' 'Carrera, Ignacio' _publ_section_title ; Efficient Access to the Iboga Skeleton: Optimized Procedure to Obtain Voacangine from Voacanga africana Root Bark ; _journal_name_full 'ACS Omega' _journal_paper_doi 10.1021/acsomega.1c00745 _journal_year 2021 _chemical_absolute_configuration rmad _chemical_formula_moiety 'C43 H57 N4 O5, 2.5(H2 O)' _chemical_formula_sum 'C43 H57 N4 O7.5' _chemical_formula_weight 749.92 _chemical_name_common voacamine _space_group_crystal_system orthorhombic _space_group_IT_number 18 _space_group_name_Hall 'P 2 2ab' _space_group_name_H-M_alt 'P 21 21 2' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.7939(10) _cell_length_b 22.4746(12) _cell_length_c 10.3719(5) _cell_measurement_reflns_used 9443 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 67.657 _cell_measurement_theta_min 3.65 _cell_volume 4380.9(4) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 298(2) _diffrn_detector_area_resol_mean 10.4167 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker D8 Venture/Photon 100 CMOS' _diffrn_measurement_method '\j and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0965 _diffrn_reflns_av_unetI/netI 0.0298 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 169742 _diffrn_reflns_point_group_measured_fraction_full 0.992 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 68.927 _diffrn_reflns_theta_min 3.065 _diffrn_source 'Cu Incoatec microsource' _exptl_absorpt_coefficient_mu 0.628 _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.6735 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour 'light pink' _exptl_crystal_density_diffrn 1.137 _exptl_crystal_description parallelepiped _exptl_crystal_F_000 1612 _exptl_crystal_size_max 0.310 _exptl_crystal_size_mid 0.283 _exptl_crystal_size_min 0.130 _refine_diff_density_max 0.540 _refine_diff_density_min -0.292 _refine_diff_density_rms 0.069 _refine_ls_abs_structure_details ; Flack x determined using 1746 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.01(13) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.071 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 874 _refine_ls_number_reflns 8023 _refine_ls_number_restraints 1572 _refine_ls_restrained_S_all 1.034 _refine_ls_R_factor_all 0.1552 _refine_ls_R_factor_gt 0.1276 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1657P)^2^+5.3190P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3400 _refine_ls_wR_factor_ref 0.3659 _reflns_Friedel_coverage 0.778 _reflns_Friedel_fraction_full 0.985 _reflns_Friedel_fraction_max 0.976 _reflns_number_gt 5663 _reflns_number_total 8023 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao1c00745_si_002.cif _cod_data_source_block voacamina_uy_paper _cod_original_formula_sum 'C43 H57 N4 O7.50' _cod_database_code 4518833 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.829 _shelx_estimated_absorpt_t_max 0.923 _shelx_res_file ; TITL cu_20180720_AP_BG_voacamina_0m_a.res in P2(1)2(1)2 voacamina_uy_paper.res created by SHELXL-2018/3 at 16:16:34 on 07-Dec-2020 REM Old TITL cu_20180720_AP_BG_voacangina_0 in P222 REM SHELXT solution in P2(1)2(1)2 REM R1 0.259, Rweak 0.149, Alpha 0.020, Orientation a'=b, b'=c, c'=a REM Flack x = 0.253 ( 0.118 ) from Parsons' quotients REM Formula found by SHELXT: C42 N5 O5 CELL 1.54178 18.7939 22.4746 10.3719 90.000 90.000 90.000 ZERR 4.000 0.0010 0.0012 0.0005 0.000 0.000 0.000 LATT -1 SYMM -X, -Y, Z SYMM 1/2-X, 1/2+Y, -Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N O UNIT 172 228 16 30 SIZE 0.130 .283 .310 TEMP 25 L.S. 50 BOND $H LIST 4 FMAP 2 PLAN 20 ACTA CONF HTAB HTAB C11 O15 HTAB N19 O1W HTAB C11' O15' HTAB N19' O1W' EQIV $2 -x+1/2, y+1/2, -z+1 EQIV $1 -x+1, -y+1, z HTAB CE' O3W'_$1 HTAB NQ OT'_$1 SIMU 0.005 C1 > Cs WGHT 0.165700 5.319000 FVAR 0.54601 0.51684 0.39127 PART 1 31 C1 1 0.050958 0.563262 0.136741 31.00000 0.09938 0.15040 = 0.07997 -0.01207 -0.01085 -0.01707 AFIX 137 H1A 2 0.024619 0.581270 0.067700 31.00000 -1.50000 H1B 2 0.061762 0.592779 0.200717 31.00000 -1.50000 H1C 2 0.023033 0.532152 0.174982 31.00000 -1.50000 AFIX 0 C2 1 0.117294 0.538207 0.086102 31.00000 0.09338 0.14455 = 0.07316 -0.00835 -0.00350 -0.02868 AFIX 43 H2 2 0.127008 0.543376 -0.001102 31.00000 -1.20000 AFIX 0 C3 1 0.166599 0.507241 0.159895 31.00000 0.08994 0.13937 = 0.07063 -0.00884 0.00069 -0.03021 N4 3 0.241963 0.428514 0.076186 31.00000 0.09102 0.13721 = 0.06624 -0.00810 0.00897 -0.03466 C16 1 0.311349 0.418367 0.020229 31.00000 0.09507 0.14030 = 0.06629 -0.00829 0.01475 -0.04074 AFIX 133 H16A 2 0.341594 0.399489 0.082600 31.00000 -1.50000 H16B 2 0.331821 0.455720 -0.005064 31.00000 -1.50000 H16C 2 0.306715 0.393154 -0.054011 31.00000 -1.50000 AFIX 0 C4 1 0.235974 0.494300 0.106927 31.00000 0.09127 0.13846 = 0.06769 -0.00786 0.00466 -0.03355 AFIX 23 H4A 2 0.272478 0.505377 0.168531 31.00000 -1.20000 H4B 2 0.243247 0.517400 0.029034 31.00000 -1.20000 AFIX 0 C5 1 0.224872 0.387415 0.187330 31.00000 0.08813 0.13311 = 0.06812 -0.00926 0.01035 -0.03338 AFIX 13 H5 2 0.221878 0.346636 0.154313 31.00000 -1.20000 AFIX 0 C6 1 0.284759 0.389939 0.291448 31.00000 0.08750 0.12935 = 0.07053 -0.00997 0.01132 -0.03279 AFIX 23 H6A 2 0.323281 0.364090 0.264307 31.00000 -1.20000 H6B 2 0.303299 0.430193 0.294522 31.00000 -1.20000 AFIX 0 C7 1 0.308012 0.264015 0.422708 31.00000 0.09829 0.13091 = 0.08389 -0.01859 0.00347 -0.02746 AFIX 43 H7 2 0.325398 0.263612 0.338764 31.00000 -1.20000 AFIX 0 C8 1 0.311230 0.214127 0.496489 31.00000 0.10225 0.13412 = 0.09070 -0.01726 0.00107 -0.02541 AFIX 43 H8 2 0.333858 0.180325 0.464964 31.00000 -1.20000 AFIX 0 C9 1 0.281560 0.213269 0.616264 31.00000 0.10245 0.13393 = 0.09090 -0.01473 0.00079 -0.02821 AFIX 43 H9 2 0.282609 0.177764 0.662278 31.00000 -1.20000 AFIX 0 C10 1 0.250997 0.260587 0.671482 31.00000 0.09954 0.13133 = 0.08532 -0.01431 0.00256 -0.02896 AFIX 43 H10 2 0.233632 0.259196 0.755391 31.00000 -1.20000 AFIX 0 C11 1 0.189448 0.460707 0.519759 31.00000 0.07975 0.12710 = 0.07163 -0.01563 0.00269 -0.02152 AFIX 13 H11 2 0.139419 0.453869 0.541898 31.00000 -1.20000 AFIX 0 C12 1 0.186665 0.494221 0.391975 31.00000 0.08121 0.13097 = 0.07233 -0.01480 0.00138 -0.02629 AFIX 23 H12A 2 0.235373 0.499241 0.363018 31.00000 -1.20000 H12B 2 0.168350 0.533683 0.410224 31.00000 -1.20000 AFIX 0 C13 1 0.144040 0.469692 0.277301 31.00000 0.08460 0.13476 = 0.07068 -0.01086 0.00298 -0.03002 AFIX 13 H13 2 0.093525 0.477405 0.293730 31.00000 -1.20000 AFIX 0 C14 1 0.151432 0.405726 0.236809 31.00000 0.08640 0.13450 = 0.07000 -0.00995 0.00741 -0.03283 AFIX 13 H14 2 0.123077 0.404828 0.157538 31.00000 -1.20000 AFIX 0 PART 1 31 C15 1 0.108812 0.365047 0.324585 31.00000 0.09029 0.13635 = 0.07501 -0.01000 0.00752 -0.03464 O15 4 0.067253 0.382645 0.403744 31.00000 0.08511 0.14072 = 0.08079 -0.00242 0.02083 -0.02846 O16 4 0.124585 0.308308 0.305232 31.00000 0.09237 0.13624 = 0.07954 -0.00820 0.00713 -0.03433 C21 1 0.087703 0.264854 0.385457 31.00000 0.09870 0.13992 = 0.09420 -0.00395 0.00236 -0.03744 AFIX 133 H21A 2 0.039854 0.259956 0.354846 31.00000 -1.50000 H21B 2 0.086795 0.278587 0.473085 31.00000 -1.50000 H21C 2 0.112180 0.227413 0.381253 31.00000 -1.50000 AFIX 0 C17 1 0.262837 0.372361 0.424405 31.00000 0.08830 0.12639 = 0.07262 -0.01344 0.00705 -0.03099 C18 1 0.278414 0.315891 0.473821 31.00000 0.09361 0.12758 = 0.07779 -0.01692 0.00499 -0.02964 N19 3 0.211977 0.362111 0.616965 31.00000 0.08985 0.12592 = 0.07244 -0.01635 0.00531 -0.02881 AFIX 43 H19 2 0.187309 0.370266 0.684529 31.00000 -1.20000 AFIX 0 C19 1 0.246511 0.311482 0.597933 31.00000 0.09459 0.12773 = 0.07749 -0.01592 0.00480 -0.02938 C20 1 0.221008 0.399934 0.513603 31.00000 0.08560 0.12519 = 0.07073 -0.01528 0.00479 -0.02782 PART 2 -31 SAME C1 > C20 C1' 1 0.062780 0.570288 0.188828 -31.00000 0.10675 0.15576 = 0.08827 -0.00591 -0.01084 -0.01334 AFIX 133 H1A' 2 0.065823 0.612566 0.200828 -31.00000 -1.50000 H1B' 2 0.057836 0.551177 0.271118 -31.00000 -1.50000 H1C' 2 0.022238 0.561128 0.136138 -31.00000 -1.50000 AFIX 0 C2' 1 0.127549 0.548915 0.125346 -31.00000 0.09445 0.14524 = 0.07460 -0.00650 -0.00373 -0.02839 AFIX 43 H2' 2 0.147954 0.573640 0.063683 -31.00000 -1.20000 AFIX 0 C3' 1 0.161826 0.493947 0.149567 -31.00000 0.09022 0.13915 = 0.07099 -0.00924 0.00126 -0.03090 N4' 3 0.236599 0.409713 0.067271 -31.00000 0.09117 0.13802 = 0.06558 -0.00670 0.01022 -0.03603 C16' 1 0.301633 0.394165 0.000290 -31.00000 0.09527 0.15111 = 0.07361 -0.00421 0.01866 -0.04005 AFIX 133 H16D 2 0.341439 0.412151 0.043250 -31.00000 -1.50000 H16E 2 0.299298 0.408331 -0.086927 -31.00000 -1.50000 H16F 2 0.307258 0.351710 0.000159 -31.00000 -1.50000 AFIX 0 C4' 1 0.226880 0.476473 0.082300 -31.00000 0.09113 0.13844 = 0.06773 -0.00644 0.00528 -0.03382 AFIX 23 H4A' 2 0.267385 0.492323 0.128991 -31.00000 -1.20000 H4B' 2 0.226757 0.494500 -0.002673 -31.00000 -1.20000 AFIX 0 C5' 1 0.227282 0.376121 0.190134 -31.00000 0.08803 0.13300 = 0.06812 -0.00909 0.01080 -0.03400 AFIX 13 H5' 2 0.226132 0.333762 0.167809 -31.00000 -1.20000 AFIX 0 C6' 1 0.287807 0.384525 0.289942 -31.00000 0.08728 0.12939 = 0.07074 -0.00945 0.01223 -0.03298 AFIX 23 H6A' 2 0.329017 0.362224 0.261043 -31.00000 -1.20000 H6B' 2 0.301001 0.426245 0.291513 -31.00000 -1.20000 AFIX 0 C7' 1 0.337625 0.264661 0.439332 -31.00000 0.10073 0.13200 = 0.08397 -0.01771 0.00241 -0.02675 AFIX 43 H7' 2 0.359995 0.265116 0.359358 -31.00000 -1.20000 AFIX 0 C8' 1 0.346020 0.218035 0.521285 -31.00000 0.10442 0.13355 = 0.09165 -0.01794 0.00133 -0.02524 AFIX 43 H8' 2 0.370947 0.185161 0.490859 -31.00000 -1.20000 AFIX 0 C9' 1 0.320729 0.215462 0.645319 -31.00000 0.10532 0.13594 = 0.09306 -0.01403 0.00150 -0.02645 AFIX 43 H9' 2 0.330614 0.182994 0.697941 -31.00000 -1.20000 AFIX 0 C10' 1 0.281293 0.261162 0.688590 -31.00000 0.10045 0.13194 = 0.08532 -0.01442 0.00231 -0.02817 AFIX 43 H10' 2 0.264085 0.261395 0.772658 -31.00000 -1.20000 AFIX 0 C11' 1 0.187454 0.449099 0.513940 -31.00000 0.07909 0.12696 = 0.07114 -0.01603 0.00309 -0.02195 AFIX 13 H11' 2 0.138005 0.438749 0.533838 -31.00000 -1.20000 AFIX 0 C12' 1 0.189231 0.482041 0.383987 -31.00000 0.08135 0.13147 = 0.07267 -0.01487 0.00079 -0.02628 AFIX 23 H12C 2 0.238370 0.483515 0.355560 -31.00000 -1.20000 H12D 2 0.174278 0.522736 0.399363 -31.00000 -1.20000 AFIX 0 C13' 1 0.144249 0.457429 0.271355 -31.00000 0.08433 0.13480 = 0.07066 -0.01102 0.00293 -0.03048 AFIX 13 H13' 2 0.094068 0.464335 0.292237 -31.00000 -1.20000 AFIX 0 C14' 1 0.152453 0.392757 0.238081 -31.00000 0.08590 0.13422 = 0.06936 -0.01043 0.00758 -0.03307 AFIX 13 H14' 2 0.121527 0.386843 0.163093 -31.00000 -1.20000 AFIX 0 C15' 1 0.124398 0.349293 0.339012 -31.00000 0.08989 0.13663 = 0.07529 -0.00983 0.00573 -0.03476 O15' 4 0.076886 0.360835 0.411822 -31.00000 0.09187 0.14077 = 0.08489 -0.00309 0.01580 -0.03961 O16' 4 0.146210 0.294657 0.318683 -31.00000 0.09322 0.13680 = 0.08035 -0.00851 0.00719 -0.03731 C21' 1 0.123776 0.248306 0.410498 -31.00000 0.10203 0.14348 = 0.09978 -0.00565 0.00451 -0.04085 AFIX 133 H21D 2 0.118504 0.211139 0.365893 -31.00000 -1.50000 H21E 2 0.079142 0.259357 0.448607 -31.00000 -1.50000 H21F 2 0.159063 0.244215 0.476832 -31.00000 -1.50000 AFIX 0 C17' 1 0.270285 0.365550 0.424242 -31.00000 0.08817 0.12633 = 0.07240 -0.01335 0.00674 -0.03128 C18' 1 0.294266 0.312097 0.478727 -31.00000 0.09433 0.12712 = 0.07791 -0.01774 0.00472 -0.03028 N19' 3 0.230238 0.357770 0.625088 -31.00000 0.08964 0.12614 = 0.07242 -0.01655 0.00547 -0.02956 AFIX 43 H19' 2 0.208833 0.366582 0.695842 -31.00000 -1.20000 AFIX 0 C19' 1 0.266787 0.307778 0.605917 -31.00000 0.09454 0.12793 = 0.07719 -0.01601 0.00373 -0.03003 C20' 1 0.231041 0.393779 0.516746 -31.00000 0.08507 0.12469 = 0.07045 -0.01521 0.00414 -0.02811 PART 0 DFIX 1.5 0.01 Ca Cb Ca' Cb' DFIX 1.48 0.01 Cb Cc cb' cc' PART 1 21 CA 1 0.561272 0.779061 0.972242 21.00000 0.13310 0.10775 = 0.13316 -0.02114 -0.02405 -0.00012 AFIX 133 HAA 2 0.610926 0.771673 0.957560 21.00000 -1.50000 HAB 2 0.553118 0.821179 0.976678 21.00000 -1.50000 HAC 2 0.533970 0.762484 0.902750 21.00000 -1.50000 AFIX 0 CB 1 0.539064 0.750668 1.096973 21.00000 0.12470 0.09772 = 0.12099 -0.02057 -0.02567 0.00551 AFIX 23 HBA 2 0.578095 0.752290 1.158062 21.00000 -1.20000 HBB 2 0.499169 0.772312 1.133321 21.00000 -1.20000 AFIX 0 CC 1 0.518369 0.687678 1.074381 21.00000 0.11882 0.09241 = 0.11534 -0.02209 -0.02270 0.00862 AFIX 13 HC 2 0.557775 0.665194 1.036230 21.00000 -1.20000 AFIX 0 CD 1 0.492482 0.657899 1.202147 21.00000 0.11900 0.09345 = 0.11377 -0.02206 -0.02088 0.00742 AFIX 23 HDA 2 0.476580 0.688753 1.260852 21.00000 -1.20000 HDB 2 0.532419 0.637745 1.242177 21.00000 -1.20000 AFIX 0 CE 1 0.430362 0.611865 1.182667 21.00000 0.11227 0.09242 = 0.11053 -0.01795 -0.02088 0.01171 AFIX 13 HE 2 0.421114 0.587689 1.259494 21.00000 -1.20000 AFIX 0 CF 1 0.446423 0.574043 1.061088 21.00000 0.10501 0.08838 = 0.10838 -0.01645 -0.02189 0.01342 AFIX 23 HFA 2 0.412376 0.541790 1.053603 21.00000 -1.20000 HFB 2 0.493820 0.557143 1.066503 21.00000 -1.20000 AFIX 0 CG 1 0.440746 0.616526 0.941395 21.00000 0.09817 0.08251 = 0.10491 -0.01852 -0.01682 0.01583 CT 1 0.502877 0.604715 0.852559 21.00000 0.09425 0.08430 = 0.10829 -0.01924 -0.01271 0.01273 OT 4 0.543496 0.563488 0.864318 21.00000 0.09420 0.08617 = 0.11270 -0.02427 -0.01288 0.02409 OU 4 0.512586 0.650531 0.768449 21.00000 0.09581 0.09501 = 0.10970 -0.01568 -0.00912 0.01013 CU 1 0.569360 0.644613 0.680483 21.00000 0.09925 0.11088 = 0.11824 -0.01865 0.00185 -0.00141 AFIX 133 HUA 2 0.563854 0.608354 0.632584 21.00000 -1.50000 HUB 2 0.613573 0.643663 0.726790 21.00000 -1.50000 HUC 2 0.569302 0.677793 0.622192 21.00000 -1.50000 AFIX 0 NH 3 0.390927 0.703628 1.066729 21.00000 0.11108 0.09047 = 0.10691 -0.02480 -0.01690 0.01738 CJ 1 0.334251 0.728106 0.980395 21.00000 0.10421 0.08512 = 0.10211 -0.02669 -0.01223 0.02227 AFIX 23 HJA 2 0.356040 0.744438 0.903355 21.00000 -1.20000 HJB 2 0.309564 0.760111 1.024395 21.00000 -1.20000 AFIX 0 CH 1 0.449893 0.682533 0.989602 21.00000 0.10928 0.08687 = 0.10909 -0.02300 -0.01914 0.01473 AFIX 13 HH 2 0.455117 0.708579 0.914419 21.00000 -1.20000 AFIX 0 CI 1 0.365281 0.652729 1.143824 21.00000 0.11252 0.09309 = 0.10733 -0.02330 -0.01774 0.01401 AFIX 23 HIA 2 0.331224 0.629841 1.094039 21.00000 -1.20000 HIB 2 0.341618 0.667098 1.220885 21.00000 -1.20000 AFIX 0 CK 1 0.281639 0.680836 0.942804 21.00000 0.09843 0.08334 = 0.09652 -0.02561 -0.01185 0.02658 AFIX 23 HKA 2 0.243760 0.700016 0.894760 21.00000 -1.20000 HKB 2 0.260676 0.665394 1.021442 21.00000 -1.20000 AFIX 0 PART 2 -21 SAME Ca > Ck CA' 1 0.584576 0.788927 1.061627 -21.00000 0.13485 0.11327 = 0.13281 -0.01902 -0.02450 -0.00294 AFIX 133 HAA' 2 0.607199 0.754775 1.099180 -21.00000 -1.50000 HAB' 2 0.580332 0.819696 1.125365 -21.00000 -1.50000 HAC' 2 0.612672 0.803147 0.990734 -21.00000 -1.50000 AFIX 0 CB' 1 0.511941 0.771988 1.014115 -21.00000 0.12397 0.09855 = 0.12136 -0.02018 -0.02333 0.00726 AFIX 23 HBA' 2 0.475457 0.786793 1.071967 -21.00000 -1.20000 HBB' 2 0.503557 0.788113 0.928707 -21.00000 -1.20000 AFIX 0 CC' 1 0.511550 0.705317 1.010979 -21.00000 0.11840 0.09216 = 0.11544 -0.02216 -0.02237 0.00964 AFIX 13 HC' 2 0.550848 0.689755 0.958825 -21.00000 -1.20000 AFIX 0 CD' 1 0.512510 0.679048 1.148783 -21.00000 0.11997 0.09318 = 0.11484 -0.02184 -0.02072 0.00630 AFIX 23 HDA' 2 0.506469 0.711213 1.210173 -21.00000 -1.20000 HDB' 2 0.558764 0.661285 1.164288 -21.00000 -1.20000 AFIX 0 CE' 1 0.454120 0.631360 1.173921 -21.00000 0.11168 0.09293 = 0.11058 -0.01863 -0.02130 0.01019 AFIX 13 HE' 2 0.459003 0.612062 1.258186 -21.00000 -1.20000 AFIX 0 CF' 1 0.457863 0.586721 1.060116 -21.00000 0.10448 0.08867 = 0.10843 -0.01626 -0.02194 0.01333 AFIX 23 HFA' 2 0.423154 0.555425 1.073978 -21.00000 -1.20000 HFB' 2 0.504642 0.568498 1.058700 -21.00000 -1.20000 AFIX 0 CG' 1 0.443494 0.616370 0.927622 -21.00000 0.09833 0.08286 = 0.10512 -0.01818 -0.01683 0.01563 CT' 1 0.501236 0.605963 0.828763 -21.00000 0.09392 0.08459 = 0.10856 -0.01885 -0.01272 0.01301 OT' 4 0.540904 0.564112 0.818374 -21.00000 0.10022 0.08118 = 0.10853 -0.03054 -0.00764 0.02067 OU' 4 0.496888 0.642517 0.725311 -21.00000 0.09677 0.09334 = 0.10841 -0.01908 -0.00732 0.00875 CU' 1 0.547832 0.635535 0.624214 -21.00000 0.09951 0.11076 = 0.11586 -0.01528 -0.00015 0.00798 AFIX 133 HUA' 2 0.594010 0.628613 0.660829 -21.00000 -1.50000 HUB' 2 0.549045 0.671003 0.572685 -21.00000 -1.50000 HUC' 2 0.534677 0.602296 0.571193 -21.00000 -1.50000 AFIX 0 NH' 3 0.378256 0.697540 1.039874 -21.00000 0.11148 0.09064 = 0.10609 -0.02498 -0.01689 0.01800 CJ' 1 0.308078 0.714426 0.997278 -21.00000 0.10627 0.08829 = 0.10389 -0.02810 -0.01300 0.02287 AFIX 23 HJA' 2 0.310185 0.755037 0.965846 -21.00000 -1.20000 HJB' 2 0.276584 0.714079 1.071367 -21.00000 -1.20000 AFIX 0 CH' 1 0.437426 0.685266 0.955912 -21.00000 0.10874 0.08688 = 0.10891 -0.02247 -0.01925 0.01527 AFIX 13 HH' 2 0.429424 0.705953 0.874009 -21.00000 -1.20000 AFIX 0 CI' 1 0.384283 0.668187 1.161453 -21.00000 0.11232 0.09188 = 0.10647 -0.02120 -0.01900 0.01428 AFIX 23 HIA' 2 0.343844 0.641884 1.172782 -21.00000 -1.20000 HIB' 2 0.382826 0.697679 1.229685 -21.00000 -1.20000 AFIX 0 CK' 1 0.276507 0.677334 0.896670 -21.00000 0.09962 0.08372 = 0.09756 -0.02560 -0.01227 0.02570 AFIX 23 HKA' 2 0.228624 0.667503 0.924321 -21.00000 -1.20000 HKB' 2 0.271962 0.701872 0.820176 -21.00000 -1.20000 AFIX 0 PART 0 CM 1 0.214855 0.496219 0.618510 11.00000 0.07275 0.12216 = 0.07360 -0.01634 0.00112 -0.00235 CL 1 0.194530 0.585456 0.742578 11.00000 0.06980 0.11182 = 0.07668 -0.00921 -0.00215 0.02793 AFIX 43 HL 2 0.163971 0.615265 0.770894 11.00000 -1.20000 AFIX 0 CO 1 0.170563 0.542814 0.663112 11.00000 0.06524 0.13325 = 0.08545 -0.00945 -0.00609 0.01813 OO 4 0.101837 0.540130 0.613481 11.00000 0.07385 0.17246 = 0.10861 -0.02156 -0.00510 0.01977 CV 1 0.052766 0.581451 0.660441 11.00000 0.07602 0.18895 = 0.16779 -0.01168 -0.01424 0.03283 AFIX 133 HVA 2 0.068288 0.620930 0.639049 11.00000 -1.50000 HVB 2 0.049197 0.577639 0.752403 11.00000 -1.50000 HVC 2 0.007079 0.574188 0.622154 11.00000 -1.50000 AFIX 0 CN 1 0.283756 0.492918 0.665299 11.00000 0.07292 0.10511 = 0.07861 -0.01799 -0.00530 0.00976 AFIX 43 HN 2 0.313377 0.461437 0.642808 11.00000 -1.20000 AFIX 0 CP 1 0.265802 0.584969 0.782852 11.00000 0.07325 0.08965 = 0.07359 -0.00759 -0.00636 0.02386 CQ 1 0.307461 0.537714 0.746496 11.00000 0.06880 0.08978 = 0.07423 -0.01271 -0.00873 0.01806 NQ 3 0.374485 0.546399 0.800190 11.00000 0.06909 0.08621 = 0.08828 -0.01528 -0.01416 0.02271 AFIX 43 HQ 2 0.410363 0.522918 0.792458 11.00000 -1.20000 AFIX 0 CR 1 0.373439 0.599244 0.868046 11.00000 0.08329 0.07665 = 0.09081 -0.01174 -0.01010 0.02256 CS 1 0.308506 0.625292 0.859750 11.00000 0.08609 0.08172 = 0.08564 -0.01674 -0.00637 0.02972 EADP O1W O1W' PART 1 31 O1W 4 0.099699 0.402678 0.857035 31.00000 0.09518 0.17663 = 0.05136 -0.01545 0.00326 -0.00815 PART 2 -31 O1W' 4 0.159046 0.378808 0.867057 -31.00000 0.09518 0.17663 = 0.05136 -0.01545 0.00326 -0.00815 PART 0 ISOR 0.005 O2W O3W O3W' PART 1 O2W 4 0.524255 0.505135 1.441855 10.50000 0.34097 0.34125 = 0.33228 -0.00301 0.00512 0.00327 EADP O3W O3W' O3W 4 0.646806 0.389266 1.482327 10.50000 0.29376 0.27873 = 0.27110 -0.00434 -0.01017 0.00141 PART 2 O3W' 4 0.573314 0.455849 1.458506 10.50000 0.29376 0.27873 = 0.27110 -0.00434 -0.01017 0.00141 PART 0 HKLF 4 REM cu_20180720_AP_BG_voacamina_0m_a.res in P2(1)2(1)2 REM wR2 = 0.3659, GooF = S = 1.071, Restrained GooF = 1.034 for all data REM R1 = 0.1276 for 5663 Fo > 4sig(Fo) and 0.1552 for all 8023 data REM 874 parameters refined using 1572 restraints END WGHT 0.1659 5.3186 REM Instructions for potential hydrogen bonds HTAB C11 O15 HTAB N19 O1W HTAB C11' O15' HTAB N19' O1W' HTAB CJ O16_$2 HTAB CE' O3W'_$1 HTAB NQ OT_$1 HTAB NQ OT' HTAB NQ OT'_$1 REM Highest difference peak 0.540, deepest hole -0.292, 1-sigma level 0.069 Q1 1 0.1413 0.4087 0.8425 11.00000 0.05 0.54 Q2 1 0.1460 0.3691 0.8692 11.00000 0.05 0.52 Q3 1 0.5333 0.4499 1.4514 11.00000 0.05 0.42 Q4 1 0.0860 0.4150 0.8955 11.00000 0.05 0.41 Q5 1 0.6219 0.4561 1.4205 11.00000 0.05 0.38 Q6 1 0.3569 0.6131 1.1692 11.00000 0.05 0.29 Q7 1 0.5792 0.5199 1.3719 11.00000 0.05 0.25 Q8 1 0.4974 0.7459 1.1597 11.00000 0.05 0.22 Q9 1 0.6048 0.3912 1.4913 11.00000 0.05 0.22 Q10 1 0.4969 0.6756 0.8322 11.00000 0.05 0.21 Q11 1 0.6426 0.4808 1.3440 11.00000 0.05 0.21 Q12 1 0.1008 0.4993 0.6287 11.00000 0.05 0.20 Q13 1 0.1186 0.5788 0.5629 11.00000 0.05 0.19 Q14 1 0.3075 0.6340 1.3261 11.00000 0.05 0.18 Q15 1 0.0444 0.3208 0.4739 11.00000 0.05 0.18 Q16 1 0.0226 0.3296 0.4549 11.00000 0.05 0.18 Q17 1 0.6991 0.3706 1.4717 11.00000 0.05 0.18 Q18 1 0.5873 0.7811 0.8781 11.00000 0.05 0.18 Q19 1 0.6831 0.4390 1.3635 11.00000 0.05 0.18 Q20 1 0.6782 0.3936 1.4143 11.00000 0.05 0.18 ; _shelx_res_checksum 93206 _shelx_hkl_file ; 0 0 1 872.73 55.47 0 0 1 811.26 55.56 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30.28 8.50 11 -2 0 34.25 10.43 11 2 0 35.00 6.77 11 2 0 38.74 10.09 11 -2 0 37.48 5.24 11 -2 0 89.65 37.84 -11 2 0 54.27 5.49 11 2 0 50.14 6.97 -11 2 0 54.13 7.12 -11 -2 0 40.00 5.46 -11 -2 0 33.74 7.61 -11 2 0 24.54 12.38 -11 2 0 52.01 6.95 -11 -2 0 36.24 10.24 11 2 0 46.71 6.78 -11 2 0 31.19 9.06 11 2 0 34.30 10.29 11 2 0 40.64 5.30 -11 2 0 49.66 19.76 -11 -2 0 48.21 5.45 -11 2 0 24.95 6.09 11 -2 0 31.43 8.01 -11 -2 0 44.53 6.48 -11 2 0 39.86 7.84 11 -2 0 41.25 8.07 -11 -2 0 46.18 6.00 -11 -2 0 64.93 7.55 -11 2 0 49.34 5.26 11 2 0 25.17 7.69 -11 2 0 13.36 13.78 11 -2 0 22.30 7.15 11 -2 0 33.50 10.71 11 -2 0 43.32 7.37 -11 2 1 68.89 7.72 11 2 -1 98.34 12.16 11 -2 1 85.34 7.15 11 2 -1 59.10 7.54 11 -2 1 75.70 9.91 -11 -2 -1 102.09 12.19 -11 -2 -1 72.63 9.53 11 2 -1 81.41 9.67 11 -2 1 81.46 9.01 11 2 -1 64.46 9.08 11 -2 1 118.25 47.39 11 2 -1 58.59 8.52 11 -2 1 76.23 7.86 -11 2 1 76.50 10.42 -11 -2 -1 99.56 27.75 -11 2 1 62.23 22.15 -11 -2 -1 49.61 15.84 -11 -2 -1 69.65 8.17 11 -2 1 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20.61 11 2 1 91.13 10.10 -11 -2 1 70.75 7.04 -11 -2 1 84.13 9.26 11 -2 -1 66.85 8.40 -11 -2 1 60.37 15.65 -11 2 -1 56.17 12.08 -11 -2 1 64.68 7.80 -11 2 2 62.81 10.71 11 2 -2 64.48 11.50 11 -2 2 82.95 13.49 -11 -2 -2 75.95 10.13 11 2 -2 74.01 9.57 -11 -2 -2 67.87 7.75 -11 2 2 84.69 6.93 11 2 -2 74.10 8.41 11 -2 2 85.98 7.21 -11 -2 -2 75.75 7.59 -11 -2 -2 83.31 9.13 11 2 -2 68.22 8.80 11 2 -2 68.29 8.22 -11 -2 -2 72.89 14.94 11 2 -2 71.91 7.66 -11 -2 -2 78.91 7.20 -11 2 2 80.41 7.42 11 -2 2 74.25 8.18 11 -2 2 64.55 7.84 -11 -2 -2 68.96 13.01 -11 2 2 55.35 10.40 11 -2 2 90.90 9.05 11 -2 2 81.81 11.26 -11 -2 -2 73.79 9.00 -11 2 2 69.67 9.38 11 2 -2 77.17 8.29 -11 2 2 72.67 15.63 11 -2 2 160.70 46.72 -11 2 2 56.18 8.20 -11 2 2 79.63 8.18 11 2 -2 82.15 8.29 -11 2 2 81.62 7.65 11 2 -2 72.52 10.19 -11 2 2 57.32 17.58 11 -2 -2 84.39 8.42 -11 -2 2 63.77 11.37 -11 -2 2 79.34 7.26 -11 2 -2 75.39 8.01 11 2 2 69.27 11.14 11 -2 -2 72.25 7.89 11 2 2 86.78 7.28 -11 2 -2 82.36 7.52 -11 2 -2 75.34 9.18 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79.89 7.82 10 -3 1 80.59 7.41 -10 3 1 78.53 7.82 -10 3 1 67.89 8.15 10 3 -1 79.95 9.63 10 -3 1 86.05 9.50 -10 -3 -1 80.95 8.16 10 -3 1 91.12 8.41 -10 -3 -1 70.79 20.94 10 -3 1 74.17 10.60 -10 3 1 87.14 11.17 -10 3 1 85.35 7.05 -10 -3 -1 81.93 9.11 -10 3 1 77.91 11.07 10 3 -1 91.10 8.87 -10 3 1 71.13 14.12 -10 -3 -1 86.15 9.73 10 -3 1 75.92 8.28 -10 -3 -1 76.78 10.38 10 3 -1 86.27 10.78 10 -3 -1 78.26 8.90 -10 -3 1 75.87 26.63 10 3 1 96.60 8.32 -10 -3 1 66.89 9.81 10 3 1 80.65 7.11 10 3 1 73.84 29.60 10 -3 -1 75.19 36.09 -10 -3 1 71.44 7.53 10 -3 -1 72.91 8.87 -10 3 -1 61.27 7.76 10 3 1 75.68 9.16 -10 3 -1 57.74 7.99 -10 -3 1 77.06 8.35 10 3 1 87.34 8.08 -10 -3 1 87.21 7.72 10 -3 -1 84.42 8.06 10 -3 -1 81.49 9.85 -10 3 -1 94.34 27.11 -10 -3 1 63.53 13.38 -10 3 -1 84.30 8.48 -10 3 -1 63.86 10.56 -10 3 -1 59.71 9.49 -10 -3 1 88.23 6.98 10 -3 -1 75.75 9.24 -10 3 2 102.44 11.50 10 -3 2 88.46 12.44 10 3 -2 87.22 14.71 -10 -3 -2 83.52 15.44 -10 3 2 97.83 8.66 10 -3 2 99.13 35.93 -10 -3 -2 80.99 8.69 10 3 -2 78.90 9.00 10 3 -2 98.78 9.50 -10 -3 -2 95.30 8.61 -10 3 2 76.77 15.85 -10 3 2 89.42 11.84 10 -3 2 96.13 8.24 -10 -3 -2 74.53 28.30 -10 3 2 96.92 9.64 10 3 -2 79.20 9.05 -10 3 2 101.46 8.03 10 3 -2 85.52 10.78 -10 -3 -2 93.74 10.63 -10 3 2 97.76 9.18 10 3 -2 105.46 10.31 10 3 -2 102.83 9.67 -10 -3 -2 99.41 9.32 -10 -3 -2 98.35 9.73 -10 3 2 80.42 33.89 -10 3 2 82.33 9.12 10 3 -2 96.05 10.56 10 3 -2 94.85 12.21 -10 3 2 105.98 8.70 10 -3 2 104.72 9.06 10 -3 2 101.96 9.41 -10 -3 -2 82.65 10.11 10 -3 2 101.99 10.58 10 -3 2 87.64 13.44 -10 -3 2 85.87 8.09 10 -3 -2 91.91 10.97 -10 -3 2 58.40 19.85 10 -3 -2 88.58 9.10 -10 -3 2 99.17 11.36 -10 -3 2 97.22 7.87 -10 -3 2 91.73 15.76 10 3 2 102.32 8.07 10 3 2 110.14 33.37 -10 3 -2 96.90 8.43 -10 -3 2 88.84 9.21 -10 3 -2 98.94 10.94 10 3 2 94.02 10.24 -10 3 -2 89.98 9.44 -10 3 -2 115.20 31.01 10 -3 -2 84.42 14.48 -10 -3 2 86.95 8.85 10 -3 -2 88.17 35.14 10 -3 -2 92.47 8.55 10 -3 -2 77.80 8.79 -10 3 -2 96.30 9.02 10 3 2 93.23 8.88 10 -3 -2 92.50 10.31 10 -3 -2 86.95 10.32 -10 3 -2 86.93 10.02 10 3 2 94.35 12.78 10 -3 -2 97.28 8.77 10 3 2 103.04 9.09 -10 -3 -3 81.77 9.74 10 3 -3 84.41 8.27 10 3 -3 100.27 13.96 -10 -3 -3 87.83 9.73 -10 3 3 86.07 7.31 10 3 -3 89.46 8.94 10 -3 3 91.45 7.58 -10 3 3 76.67 8.76 10 3 -3 79.69 10.48 10 -3 3 78.53 8.61 -10 3 3 81.06 9.88 -10 -3 -3 77.76 10.35 -10 -3 -3 85.33 9.47 -10 3 3 62.99 14.51 -10 3 3 88.23 8.45 10 -3 3 64.90 23.51 10 3 -3 83.59 10.12 10 -3 3 98.05 10.85 -10 3 3 82.66 7.97 10 3 -3 83.12 9.12 -10 3 3 69.32 18.60 10 -3 3 83.12 8.83 10 3 -3 76.09 10.20 -10 3 3 58.65 9.85 -10 3 3 85.16 8.64 10 -3 3 91.70 8.87 10 -3 3 71.62 13.34 -10 -3 -3 85.25 8.17 10 3 -3 85.97 8.91 -10 -3 -3 74.34 10.53 10 3 -3 73.69 7.81 10 3 3 94.12 7.53 10 -3 -3 91.37 10.60 -10 -3 3 78.50 8.23 10 3 3 59.38 12.79 10 -3 -3 65.34 9.72 -10 -3 3 94.78 7.41 -10 -3 3 74.97 11.11 -10 -3 3 80.24 9.08 -10 3 -3 88.07 8.42 10 3 3 97.87 8.59 -10 3 -3 86.01 7.96 -10 3 -3 73.83 10.28 -10 3 -3 77.78 9.54 10 -3 -3 78.31 9.34 10 3 3 72.24 11.69 -10 -3 3 87.62 16.98 -10 3 -3 87.28 11.39 -10 -3 3 118.21 15.97 10 -3 -3 80.49 8.77 10 -3 -3 78.36 8.31 10 -3 -3 86.79 8.88 10 3 3 86.19 13.70 -10 -3 3 85.45 8.83 10 -3 -3 81.21 8.16 10 3 3 78.10 13.36 -10 -3 3 94.09 8.11 -10 3 -3 71.10 12.05 10 3 -4 35.33 5.15 -10 3 4 35.13 6.56 10 3 -4 30.19 7.35 -10 -3 -4 38.82 6.81 -10 -3 -4 29.62 10.70 -10 3 4 44.10 12.35 -10 -3 -4 28.15 6.86 10 3 -4 32.93 9.06 -10 3 4 30.71 6.79 10 3 -4 33.28 5.70 10 3 -4 32.24 6.46 -10 3 4 32.98 5.62 -10 -3 -4 39.43 7.82 10 3 -4 24.24 6.00 10 -3 4 37.15 9.33 10 3 -4 43.12 6.63 10 -3 4 36.51 6.56 10 -3 4 10.95 13.21 -10 -3 -4 32.70 6.84 10 3 -4 29.56 8.34 -10 3 4 22.48 17.56 10 -3 4 21.70 8.09 10 -3 4 38.96 4.84 -10 -3 -4 43.81 6.99 -10 -3 -4 57.64 10.98 10 -3 4 38.55 7.02 -10 -3 -4 36.55 5.74 -10 3 4 40.28 4.53 10 -3 4 19.79 12.93 10 3 -4 25.63 6.66 -10 3 4 34.30 6.38 10 -3 4 34.03 11.01 10 -3 4 29.10 9.67 -10 3 4 27.16 10.92 -10 3 4 34.12 9.77 -10 -3 4 31.20 5.56 10 3 4 37.88 6.05 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2037.55 141.90 -5 -4 2 2022.26 141.40 -5 4 -2 1977.96 141.31 -5 -4 2 1885.13 141.06 -5 -4 2 1909.40 141.38 5 -4 -2 2018.21 141.97 5 4 2 1858.78 141.21 -5 4 -2 1786.89 144.65 5 4 2 1920.58 144.43 5 4 2 1876.82 141.05 -5 4 -2 1926.80 141.96 -5 4 -2 2002.77 142.05 5 4 2 2014.22 142.01 5 4 2 2019.12 141.43 -5 -4 2 2040.95 142.59 5 -4 -2 1972.14 141.32 5 4 2 1945.17 141.19 5 4 2 1974.50 141.49 -5 4 -2 1969.36 140.94 -5 -4 2 1854.82 144.46 -5 -4 2 1962.71 142.20 5 4 2 2018.34 141.84 5 -4 3 130.46 17.01 -5 -4 -3 138.63 11.93 5 -4 3 147.19 10.77 5 4 -3 143.47 11.41 5 -4 3 123.31 11.57 -5 4 3 137.62 11.91 5 4 -3 133.00 11.35 -5 4 3 153.56 10.64 -5 4 3 116.45 12.74 -5 4 3 125.13 12.93 5 -4 3 161.28 18.73 5 -4 3 130.63 10.32 -5 4 3 165.92 17.10 5 4 -3 121.67 16.96 -5 -4 -3 136.87 11.36 5 -4 3 126.80 16.34 -5 4 3 132.88 10.92 5 -4 3 129.83 11.17 5 4 -3 123.23 11.25 5 -4 -3 123.41 14.68 -5 -4 3 134.19 10.28 5 4 3 131.27 10.28 -5 -4 3 124.04 10.58 5 4 3 136.86 10.64 5 4 3 122.50 10.67 5 4 3 136.39 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42.45 7.85 10 -4 -4 29.96 5.75 -10 -4 4 44.08 7.36 -10 -4 4 42.64 12.29 -10 -4 4 42.68 4.89 -10 -4 4 49.93 9.96 10 -4 -4 38.90 7.95 10 4 4 31.86 14.81 10 4 4 40.00 7.03 -10 4 -4 31.90 5.96 -10 -4 4 35.07 5.85 -10 4 5 84.99 9.57 -10 -4 -5 108.14 11.37 10 4 -5 96.90 8.93 10 -4 5 72.08 9.82 -10 4 5 84.08 9.58 -10 -4 -5 61.33 13.49 10 4 -5 90.66 8.89 10 4 -5 79.42 10.56 -10 4 5 70.21 13.43 -10 4 5 70.70 17.66 10 -4 5 91.91 9.75 -10 4 5 93.80 10.61 -10 4 5 93.63 8.85 10 4 -5 85.74 11.55 -10 -4 -5 74.08 8.15 -10 4 5 86.91 7.75 -10 4 5 91.58 9.05 10 -4 5 88.06 10.16 10 -4 5 97.16 31.47 -10 -4 -5 85.45 10.04 10 -4 5 50.85 14.23 -10 -4 -5 79.11 10.60 10 -4 5 95.61 8.13 10 4 -5 90.68 8.69 10 4 -5 75.09 13.54 -10 -4 -5 79.10 9.47 10 4 -5 77.05 8.49 10 -4 5 85.68 13.13 -10 -4 5 93.96 11.82 10 -4 -5 74.96 8.40 -10 4 -5 83.18 8.53 -10 4 -5 76.48 11.62 10 -4 -5 84.67 8.52 -10 -4 5 96.74 8.69 10 4 5 119.49 15.17 10 -4 -5 94.24 11.25 -10 -4 5 99.52 8.93 -10 -4 5 83.70 15.62 10 -4 -5 80.12 9.96 -10 -4 5 85.44 8.10 -10 4 -5 112.43 12.39 10 -4 -5 100.61 10.69 10 -4 -5 87.11 11.04 -10 4 -5 100.76 9.97 10 -4 -5 94.03 9.49 -10 4 -5 91.73 12.45 -10 4 -5 94.56 9.90 -10 -4 5 80.19 10.28 -10 4 -5 71.91 14.01 10 4 5 95.73 8.25 10 4 5 83.84 9.54 -10 -4 5 86.43 10.03 10 4 5 107.65 9.99 10 -4 -5 94.70 13.35 -10 4 6 58.51 7.30 10 4 -6 33.19 16.86 10 4 -6 46.30 11.21 10 4 -6 48.71 6.61 -10 4 6 32.15 8.52 10 -4 6 61.99 8.71 10 -4 6 37.91 19.71 10 -4 6 18.33 23.25 -10 -4 -6 69.78 9.76 -10 -4 -6 59.63 8.62 -10 4 6 18.26 21.65 -10 4 6 50.73 16.66 -10 -4 -6 51.43 11.81 10 -4 6 37.68 10.52 -10 4 6 39.86 8.37 -10 -4 -6 64.56 12.50 -10 -4 -6 59.59 8.90 -10 -4 -6 63.62 9.11 -10 -4 -6 45.07 16.67 10 4 -6 40.50 6.46 10 -4 6 28.10 6.78 10 4 -6 65.80 7.92 10 4 -6 49.20 6.28 10 4 -6 55.64 6.92 10 -4 6 35.58 8.98 -10 -4 -6 33.42 6.57 -10 4 6 40.44 6.01 -10 -4 -6 44.25 9.69 -10 -4 -6 42.52 8.05 -10 -4 -6 49.44 7.33 -10 4 6 30.28 11.07 10 -4 -6 47.49 11.37 10 4 6 45.46 8.11 -10 -4 6 37.39 8.39 10 -4 -6 40.94 5.91 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15.60 4.46 -11 -4 0 24.92 5.28 11 4 0 12.62 7.42 -11 4 0 18.62 4.70 11 -4 0 18.29 30.88 11 -4 1 72.36 6.98 11 -4 1 74.82 9.55 11 -4 1 75.07 27.71 -11 4 1 48.88 18.62 11 4 -1 65.41 9.67 11 4 -1 73.27 10.39 11 4 -1 83.49 8.22 -11 -4 -1 83.98 9.88 -11 4 1 64.26 9.57 11 4 -1 85.92 9.91 -11 4 1 55.95 10.52 -11 -4 -1 84.08 47.13 11 -4 1 73.76 8.22 -11 -4 -1 69.89 7.69 -11 -4 -1 88.31 17.57 11 -4 1 64.94 12.37 -11 4 1 70.07 8.43 -11 -4 -1 76.48 11.85 -11 4 1 70.37 8.42 -11 4 1 67.53 18.05 -11 4 1 76.57 7.48 -11 4 1 70.85 6.63 11 4 -1 68.72 8.12 11 4 -1 73.89 7.66 -11 -4 -1 68.78 8.91 11 4 -1 68.23 7.55 11 4 -1 61.24 7.87 11 -4 1 86.39 9.28 -11 -4 -1 64.57 13.78 11 -4 1 70.36 10.82 11 -4 1 74.62 9.16 -11 -4 -1 67.02 7.00 11 4 -1 64.93 9.24 11 4 -1 56.25 22.94 11 -4 1 68.51 7.29 -11 -4 -1 75.44 8.40 11 4 -1 66.69 8.21 -11 4 1 73.54 7.06 11 4 -1 58.66 12.39 -11 4 1 66.07 9.90 -11 4 1 70.00 6.84 -11 -4 1 70.98 16.98 11 4 1 70.20 6.95 -11 4 -1 70.35 7.24 -11 -4 1 78.17 6.83 11 4 1 80.67 8.33 11 -4 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7.21 -11 4 -2 69.00 6.56 -11 4 -2 62.34 7.34 -11 -4 -3 18.25 5.45 -11 -4 -3 25.04 5.37 -11 -4 -3 28.60 5.32 11 4 -3 40.60 11.32 11 4 -3 18.46 5.65 11 -4 3 14.25 6.12 11 -4 3 24.80 5.70 -11 4 3 28.08 6.43 -11 4 3 5.57 18.79 11 4 -3 26.85 9.14 11 -4 3 32.37 9.96 -11 -4 -3 31.13 7.48 11 -4 3 19.14 5.75 -11 -4 -3 28.09 5.71 -11 4 3 20.74 12.27 11 4 -3 34.92 7.43 -11 4 3 26.51 8.95 11 -4 3 8.91 8.61 11 -4 3 29.87 7.15 -11 4 3 34.09 5.70 11 -4 3 -6.77 14.14 -11 4 3 16.61 12.23 -11 -4 -3 29.99 10.51 11 4 -3 36.08 5.76 11 4 -3 28.36 4.84 -11 4 3 27.56 4.21 11 4 -3 14.62 6.79 11 -4 3 11.30 11.65 -11 4 3 5.05 7.03 -11 4 3 28.73 5.45 11 -4 3 25.66 4.61 -11 4 3 30.18 8.34 11 4 -3 31.35 10.33 11 4 3 30.00 9.82 -11 -4 3 22.09 6.01 -11 -4 3 12.61 10.79 11 4 3 26.90 4.52 11 -4 -3 23.78 5.43 -11 -4 3 29.71 7.06 11 -4 -3 17.36 5.86 -11 4 -3 25.84 10.42 11 4 3 29.73 6.65 -11 4 -3 17.18 5.27 -11 -4 3 26.15 4.74 -11 -4 3 33.39 5.05 11 -4 -3 23.85 6.87 -11 4 -3 24.22 6.99 11 -4 -3 28.35 5.60 11 -4 -3 12.73 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259.98 23.44 7 -5 1 270.29 25.14 -7 -5 -1 297.40 26.76 7 5 -1 288.21 20.73 -7 -5 -1 278.62 20.99 -7 5 1 293.90 28.00 -7 5 1 272.21 21.25 7 5 -1 284.10 21.01 7 5 -1 283.78 21.49 7 5 -1 299.95 28.30 7 -5 1 271.11 21.95 7 5 -1 275.49 21.20 -7 -5 -1 282.13 21.73 7 5 -1 254.02 21.38 -7 5 1 278.00 20.86 -7 -5 -1 284.66 21.17 7 5 -1 257.28 26.64 -7 -5 -1 285.94 21.29 -7 5 1 276.53 22.15 -7 -5 -1 229.88 21.14 7 5 -1 292.08 21.08 7 -5 1 274.04 21.47 -7 5 1 295.65 20.95 -7 -5 -1 262.92 21.99 -7 -5 1 278.48 20.82 -7 -5 1 276.70 22.46 7 5 1 280.61 21.40 -7 5 -1 270.49 22.15 7 5 1 266.00 22.28 -7 5 -1 281.56 20.51 7 5 1 284.33 20.34 7 -5 -1 259.97 29.38 7 -5 -1 279.35 21.47 7 5 1 280.94 21.85 7 -5 -1 287.51 21.06 -7 -5 1 271.27 21.39 -7 -5 1 297.13 27.30 -7 -5 1 275.70 20.35 7 -5 -1 264.29 20.65 -7 5 -1 262.20 20.71 7 -5 -1 273.55 21.42 7 5 1 278.18 20.75 7 5 1 290.28 21.66 -7 5 -1 264.63 20.68 7 -5 -1 267.23 22.68 -7 5 -1 260.03 21.29 -7 5 -1 287.20 27.66 7 -5 -1 261.26 21.02 -7 -5 1 284.51 20.39 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6.94 3.08 7 -5 -11 3.02 1.90 -7 5 -11 11.14 3.46 7 -5 -11 1.63 2.63 -7 5 -11 10.73 4.11 -7 5 -11 10.62 3.62 7 -5 -11 0.75 2.48 -7 5 -11 1.31 2.10 -7 -5 11 4.49 5.83 7 -5 -11 3.99 2.44 7 -5 -11 5.89 2.35 -7 5 -11 2.67 2.70 -7 5 -11 3.64 2.90 7 -5 -11 0.69 1.65 -8 -5 0 24.15 4.12 8 5 0 17.04 5.26 8 -5 0 15.39 4.57 8 -5 0 21.06 5.01 8 5 0 19.08 5.76 -8 -5 0 15.16 3.78 8 -5 0 17.62 3.98 -8 -5 0 18.29 3.97 8 -5 0 9.72 14.40 8 5 0 20.11 3.75 -8 -5 0 21.55 7.73 -8 5 0 15.09 4.72 8 -5 0 16.61 5.78 8 -5 0 19.35 4.87 -8 -5 0 11.97 7.84 8 5 0 20.19 6.26 8 5 0 25.72 13.98 8 5 0 15.26 4.34 -8 5 0 14.79 19.97 -8 -5 0 17.67 5.91 -8 5 0 12.03 3.83 -8 5 0 18.53 4.61 -8 -5 0 18.35 4.99 -8 5 0 19.87 7.30 -8 5 0 20.92 4.72 -8 -5 -1 121.00 10.85 8 -5 1 131.31 12.69 8 5 -1 138.09 10.80 -8 5 1 131.59 10.63 -8 -5 -1 131.91 13.10 -8 5 1 116.41 14.83 -8 -5 -1 130.73 11.04 8 5 -1 131.96 11.22 -8 5 1 139.30 10.17 8 -5 1 136.04 11.57 -8 5 1 126.94 12.22 -8 5 1 129.61 10.99 -8 -5 -1 112.86 10.64 8 -5 1 131.42 11.08 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4.25 8 5 -4 4.26 5.63 -8 -5 -4 9.12 4.48 -8 -5 4 8.97 6.16 8 -5 -4 6.01 5.89 8 5 4 5.05 5.26 8 5 4 1.28 3.41 8 -5 -4 7.93 4.57 -8 -5 4 -4.71 4.44 8 -5 -4 1.98 4.48 8 -5 -4 7.71 4.11 8 -5 -4 1.05 3.64 -8 -5 4 15.85 9.93 8 -5 -4 3.71 5.73 8 5 4 7.76 3.20 -8 5 -4 -1.40 5.56 -8 -5 4 -3.93 6.82 -8 5 -4 4.37 3.90 8 5 4 -3.74 10.43 -8 5 -4 0.32 8.68 8 5 4 12.47 8.22 -8 5 -4 -1.23 7.47 8 -5 -4 -11.05 6.47 -8 -5 4 -3.61 12.18 -8 -5 4 0.97 2.91 8 -5 -4 -4.32 6.83 -8 5 -4 7.74 5.02 -8 -5 -5 22.84 6.14 -8 5 5 -5.91 20.20 -8 5 5 27.04 12.39 8 -5 5 32.20 14.44 8 5 -5 22.51 6.89 -8 -5 -5 22.71 6.71 8 5 -5 27.09 5.72 -8 -5 -5 25.61 8.81 -8 -5 -5 25.70 7.05 8 -5 5 31.14 14.15 -8 -5 -5 23.95 7.23 8 -5 5 9.78 12.73 -8 5 5 22.56 3.95 8 -5 5 2.62 12.11 8 -5 5 28.63 6.68 -8 -5 -5 21.23 6.41 8 5 -5 21.10 7.38 -8 -5 -5 21.24 9.93 -8 -5 -5 31.30 7.49 -8 5 5 25.62 5.55 8 -5 5 18.64 5.91 -8 -5 -5 41.16 11.85 8 5 -5 28.40 10.80 8 5 -5 27.77 5.83 8 5 -5 33.24 7.95 8 5 -5 20.91 6.14 8 -5 5 16.21 9.47 8 -5 5 27.06 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6.91 4.23 -8 -5 -7 14.36 5.08 -8 5 7 8.54 10.85 8 5 -7 16.02 4.83 -8 -5 -7 21.95 6.63 8 5 -7 26.52 8.58 8 5 -7 5.50 7.40 -8 5 7 -16.11 26.39 8 -5 7 21.20 4.91 8 5 7 9.17 18.63 -8 -5 7 12.76 4.43 -8 -5 7 29.95 12.32 -8 5 -7 15.76 6.78 8 -5 -7 4.96 6.05 -8 5 -7 21.27 6.69 -8 5 -7 18.69 5.27 -8 -5 7 18.98 4.77 8 5 7 7.87 6.82 -8 -5 7 -8.48 23.33 -8 5 -7 11.92 20.30 8 -5 -7 11.18 14.81 8 5 7 30.50 10.06 -8 5 -7 6.66 4.90 8 -5 -7 14.00 5.10 -8 5 -7 19.04 6.62 -8 5 -7 21.25 6.90 8 -5 -7 12.61 5.03 -8 -5 7 16.75 5.77 8 -5 -7 24.49 8.26 -8 5 -7 4.06 6.60 8 -5 -7 15.06 4.80 8 -5 -7 16.21 6.15 8 -5 -7 13.39 4.87 8 5 -8 0.23 5.34 -8 -5 -8 1.45 4.96 8 -5 8 -5.19 9.25 8 -5 8 -9.30 6.47 -8 5 8 3.04 3.86 8 5 -8 7.59 6.59 -8 -5 -8 2.00 5.54 -8 -5 -8 1.30 4.61 -8 5 8 13.47 22.65 -8 -5 -8 0.91 3.75 -8 -5 -8 0.71 3.12 -8 -5 -8 -3.28 3.89 8 5 -8 10.17 4.94 8 -5 8 4.93 4.04 -8 5 8 -0.91 6.02 -8 -5 -8 1.50 3.43 -8 -5 -8 -0.83 3.08 8 5 -8 3.33 3.11 8 5 -8 -0.38 5.15 8 5 -8 -5.67 12.51 -8 -5 -8 2.84 5.38 -8 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3.86 3.07 8 5 -9 5.20 8.65 -8 -5 -9 6.81 4.12 -8 -5 9 11.18 4.30 8 -5 -9 9.64 4.81 8 -5 -9 1.59 3.14 -8 5 -9 -0.23 3.20 8 -5 -9 0.15 4.50 -8 5 -9 3.28 4.31 8 -5 -9 3.74 3.55 -8 5 -9 3.03 3.94 -8 -5 9 9.41 4.77 8 -5 -9 2.40 4.96 8 -5 -9 5.21 3.74 -8 -5 9 8.50 5.57 8 -5 -9 12.74 3.89 -8 5 -9 17.72 5.55 8 5 9 2.45 5.83 -8 -5 9 -10.24 10.84 8 -5 -9 10.14 4.01 -8 5 -9 5.17 2.99 -8 5 -9 7.25 5.65 -8 5 -9 1.18 3.91 -8 5 -9 17.93 6.02 -8 5 -9 5.66 3.73 -8 -5 -10 9.87 6.33 -8 5 10 -4.66 5.09 -8 -5 -10 6.21 3.05 8 5 -10 10.16 2.98 8 5 -10 -0.43 3.56 -8 -5 -10 6.61 3.14 -8 -5 -10 11.76 3.82 -8 5 10 8.36 6.89 8 5 -10 2.29 3.21 -8 -5 -10 3.87 1.90 8 5 -10 7.90 2.97 8 5 -10 9.79 3.50 -8 -5 -10 1.16 3.25 8 -5 10 -5.48 5.66 -8 -5 -10 3.86 2.17 8 -5 10 5.01 8.34 -8 -5 -10 5.54 2.75 8 5 -10 2.54 3.65 8 5 -10 5.28 8.55 -8 5 -10 4.34 2.88 -8 5 -10 -0.69 3.08 -8 5 -10 7.01 3.22 -8 5 -10 0.47 2.56 -8 5 -10 4.08 2.39 8 -5 -10 2.15 2.30 8 -5 -10 5.73 2.76 8 -5 -10 6.02 2.95 -8 -5 10 1.55 4.95 -8 5 -10 -0.64 3.46 8 -5 -10 4.72 2.60 8 -5 -10 14.90 5.26 8 -5 -10 7.35 3.79 8 -5 -10 4.52 4.28 8 -5 -10 -0.05 2.99 -8 -5 10 5.61 3.68 -8 -5 10 -0.81 4.10 8 5 -11 3.95 2.73 8 5 -11 -4.84 3.11 -8 -5 -11 -0.21 2.32 -8 -5 -11 3.88 2.65 8 5 -11 1.93 1.88 8 5 -11 2.88 2.17 -8 -5 -11 0.67 1.59 -8 -5 -11 5.35 2.74 -8 -5 -11 3.75 2.33 8 5 -11 -2.29 2.53 -8 -5 -11 -0.31 1.46 -8 -5 -11 2.37 3.41 8 5 -11 2.87 2.74 -8 -5 11 6.95 5.39 -8 5 -11 -0.83 2.92 -8 5 -11 3.68 3.14 -8 5 -11 -0.65 2.26 8 -5 -11 3.03 2.46 8 -5 -11 5.23 3.20 8 -5 -11 -1.54 2.52 8 -5 -11 0.28 1.62 -8 5 -11 3.97 2.26 8 -5 -11 8.01 2.97 -8 5 -11 1.39 2.35 -8 5 -11 -2.26 2.55 8 -5 -11 1.80 2.12 8 -5 -11 2.92 1.85 -8 5 -11 -0.46 2.67 9 5 0 84.30 7.50 9 5 0 96.06 8.35 9 -5 0 70.40 8.91 9 -5 0 80.11 8.72 9 -5 0 77.43 15.01 -9 5 0 95.49 7.42 9 -5 0 81.45 9.11 -9 -5 0 79.19 8.36 -9 -5 0 86.28 7.71 9 5 0 72.58 10.01 9 5 0 130.52 34.10 -9 5 0 87.43 24.92 -9 5 0 95.70 8.41 -9 5 0 79.21 8.43 -9 -5 0 80.93 12.18 -9 5 0 81.59 10.44 9 -5 0 83.26 7.67 -9 -5 0 91.12 8.44 -9 5 0 92.35 8.24 -9 -5 0 77.80 7.97 -9 -5 0 91.59 9.84 9 -5 0 96.86 8.99 -9 5 0 66.27 8.64 -9 -5 0 77.99 32.56 9 -5 0 114.02 29.37 9 5 0 89.55 8.93 9 5 0 84.03 7.72 9 5 0 86.52 9.12 9 5 -1 9.10 4.91 -9 5 1 16.08 15.02 -9 -5 -1 15.46 4.94 9 5 -1 25.48 4.76 -9 5 1 17.49 5.45 9 -5 1 25.59 6.91 -9 -5 -1 23.15 8.87 9 -5 1 12.60 15.34 -9 5 1 23.64 5.14 9 -5 1 17.40 4.16 -9 -5 -1 22.52 6.05 -9 -5 -1 23.82 6.67 9 5 -1 19.10 5.96 9 5 -1 19.28 6.93 -9 5 1 24.07 7.36 9 -5 1 9.27 5.49 -9 -5 -1 9.03 5.66 9 -5 1 24.66 5.39 -9 -5 -1 20.96 7.14 -9 5 1 19.03 5.19 -9 5 1 22.71 6.07 9 5 -1 15.91 5.59 -9 5 1 25.32 11.85 9 -5 1 31.97 5.82 -9 5 1 20.60 4.59 9 -5 1 24.59 8.13 9 5 -1 4.01 12.30 -9 -5 -1 15.35 9.97 -9 5 -1 18.24 4.95 9 5 1 16.63 3.97 -9 5 -1 26.27 8.96 9 5 1 20.09 7.31 9 5 1 -0.41 12.83 -9 5 -1 19.90 5.45 -9 -5 1 20.47 11.08 9 -5 -1 17.00 6.22 9 5 1 17.76 13.19 -9 5 -1 23.98 5.03 9 -5 -1 -10.19 14.93 -9 5 -1 14.33 5.37 -9 -5 1 25.53 6.89 9 5 1 12.18 4.46 9 -5 -1 24.48 7.34 9 -5 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5 -3 37.42 8.31 9 -5 -3 44.73 7.77 -9 -5 3 48.49 8.69 9 5 3 46.36 6.62 9 -5 -3 7.55 22.98 9 -5 -3 39.96 6.06 9 5 3 36.17 4.51 9 5 3 43.91 11.53 -9 -5 3 36.71 5.93 9 5 3 47.06 19.59 -9 -5 3 44.11 14.24 9 5 3 38.07 7.63 -9 5 -3 44.84 10.43 -9 5 -3 33.00 6.21 -9 -5 3 32.58 4.40 9 5 3 36.51 5.37 9 -5 -3 30.01 5.69 9 -5 -3 35.32 6.08 -9 -5 3 37.46 5.95 -9 5 4 15.43 5.55 9 5 -4 20.54 6.22 -9 -5 -4 7.77 4.22 9 -5 4 18.40 4.05 -9 5 4 20.35 5.33 9 5 -4 19.13 8.63 -9 -5 -4 24.27 7.30 -9 -5 -4 24.59 5.92 9 5 -4 15.77 9.57 9 5 -4 13.13 4.32 9 5 -4 19.83 6.04 9 5 -4 14.78 4.07 -9 -5 -4 31.62 5.77 -9 5 4 17.37 3.68 9 5 -4 16.23 6.34 9 5 -4 20.99 6.50 -9 5 4 31.53 8.55 -9 -5 -4 16.53 6.36 9 -5 4 13.50 12.14 9 -5 4 15.10 7.62 9 -5 4 20.33 6.69 9 -5 4 28.12 9.59 -9 -5 -4 18.55 6.81 -9 5 4 24.69 10.40 9 -5 4 19.33 10.25 -9 -5 -4 15.92 5.18 -9 -5 -4 21.85 5.92 9 -5 4 15.53 5.88 9 -5 4 3.44 10.46 -9 5 4 14.64 16.43 -9 -5 -4 18.54 8.93 -9 5 4 19.11 11.00 -9 -5 -4 22.46 5.57 -9 -5 4 24.35 4.43 9 -5 -4 31.78 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52.94 14.57 -9 -5 -6 66.34 7.58 9 -5 6 56.91 9.43 -9 5 6 41.51 8.26 -9 -5 -6 70.85 12.36 -9 -5 -6 60.80 9.95 -9 -5 -6 79.64 8.20 -9 -5 -6 69.61 10.10 9 5 -6 57.78 10.62 -9 -5 -6 64.65 7.70 9 5 -6 71.08 8.71 -9 5 6 53.41 6.44 9 -5 -6 67.75 12.20 9 5 6 50.74 6.43 -9 5 -6 78.53 9.09 -9 5 -6 48.39 14.40 -9 -5 6 47.74 9.06 9 -5 -6 73.19 13.44 9 -5 -6 67.89 15.04 9 -5 -6 43.84 6.61 -9 -5 6 58.88 6.38 9 -5 -6 57.36 7.50 9 5 6 54.24 9.63 -9 5 -6 60.65 8.33 -9 5 -6 62.21 10.04 -9 -5 6 63.31 7.37 -9 5 -6 62.11 8.39 -9 -5 6 42.19 16.43 9 5 6 50.53 7.77 -9 5 -6 77.21 15.12 9 -5 -6 74.96 7.77 -9 5 -6 50.67 9.31 9 5 6 76.14 17.29 -9 5 -6 77.23 8.25 9 -5 -6 61.94 7.56 9 -5 -6 48.30 7.63 -9 -5 6 69.16 18.05 -9 -5 6 38.52 8.57 -9 -5 -7 48.63 7.41 -9 -5 -7 41.77 8.10 -9 5 7 9.13 57.47 9 5 -7 48.28 7.99 -9 5 7 35.57 11.44 9 5 -7 51.52 13.46 -9 5 7 36.79 5.19 -9 -5 -7 32.96 6.54 9 -5 7 41.73 8.44 -9 5 7 38.94 8.59 -9 -5 -7 47.16 7.04 9 5 -7 39.97 6.01 -9 -5 -7 29.79 11.72 9 5 -7 35.12 10.98 9 -5 7 44.48 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23.14 -10 -5 0 7.63 4.49 10 -5 0 18.31 7.26 -10 5 0 16.79 4.11 10 -5 0 52.27 25.99 10 5 0 8.51 5.20 -10 5 0 10.74 6.00 10 -5 0 22.17 6.41 10 5 0 9.09 3.23 -10 5 0 22.72 5.49 -10 -5 0 23.69 8.81 -10 -5 0 11.14 7.44 10 5 0 1.28 3.31 -10 -5 0 6.25 9.46 -10 -5 0 7.75 5.48 10 5 0 20.64 6.67 10 5 0 23.33 8.80 10 5 0 10.50 5.05 10 -5 1 23.40 5.84 -10 5 1 18.82 14.22 10 5 -1 15.67 6.89 -10 5 1 22.84 5.08 -10 -5 -1 30.99 6.29 -10 5 1 22.68 5.27 -10 5 1 28.38 7.37 10 5 -1 23.83 5.32 10 5 -1 31.94 6.52 10 -5 1 25.56 4.15 -10 -5 -1 6.20 10.24 -10 -5 -1 27.83 5.77 10 5 -1 9.25 10.88 10 -5 1 29.97 6.62 10 5 -1 30.69 8.84 -10 5 1 27.47 5.75 -10 -5 -1 15.62 15.10 -10 5 1 26.90 5.72 10 5 -1 20.52 6.24 10 -5 1 32.04 10.20 10 5 -1 24.23 5.98 -10 -5 -1 27.89 6.47 -10 5 1 27.17 9.63 -10 -5 -1 30.52 8.95 10 -5 1 17.65 4.82 10 5 -1 19.66 4.92 10 -5 1 19.45 4.36 10 -5 1 -8.10 20.94 -10 5 1 35.11 13.79 -10 5 1 26.44 3.96 10 5 -1 23.94 5.75 10 5 -1 17.27 6.96 10 -5 1 23.93 6.59 -10 -5 -1 26.90 4.56 -10 -5 -1 25.81 6.85 10 5 -1 26.82 6.16 -10 5 1 26.10 9.33 10 -5 1 25.98 7.59 -10 5 1 32.79 6.97 10 -5 1 16.19 7.60 10 -5 1 28.17 9.43 10 5 1 28.20 5.99 10 -5 -1 8.54 6.14 10 5 1 14.72 17.60 10 5 1 20.95 9.79 -10 5 -1 30.50 10.34 10 -5 -1 33.86 7.48 -10 5 -1 22.37 9.09 10 -5 -1 26.66 7.81 10 5 1 16.79 4.86 10 -5 -1 20.78 4.99 -10 5 -1 23.96 5.64 10 -5 -1 21.40 7.78 10 -5 -1 27.98 8.14 -10 5 -1 22.96 5.96 -10 -5 1 25.61 5.21 -10 -5 1 25.88 4.75 -10 -5 1 25.82 3.90 -10 5 -1 21.07 5.84 -10 -5 1 32.97 9.30 -10 5 -1 17.52 17.30 10 -5 -1 32.28 22.16 -10 -5 1 36.03 10.17 10 -5 -1 20.22 6.26 -10 -5 1 21.07 5.00 -10 5 -1 23.93 7.32 -10 -5 1 22.54 4.74 10 5 1 19.71 6.75 10 -5 -1 26.35 5.60 -10 -5 1 30.73 16.35 -10 -5 1 22.10 6.01 10 5 1 17.62 5.98 10 5 1 20.98 5.45 -10 5 -1 22.21 5.99 10 5 1 27.82 4.23 -10 -5 1 32.60 12.60 -10 5 -1 26.78 6.97 -10 5 -1 22.88 6.83 10 -5 -1 20.81 6.03 10 -5 -1 20.25 9.07 10 -5 -1 24.55 8.86 -10 -5 -2 50.08 12.06 10 5 -2 72.87 8.50 -10 -5 -2 98.64 33.52 10 5 -2 64.39 8.08 -10 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81.42 7.86 10 -5 -2 61.73 8.26 10 5 2 73.01 7.96 -10 -5 2 79.42 7.76 -10 5 -2 68.75 11.13 -10 -5 2 80.05 7.32 -10 5 -2 80.98 10.71 -10 -5 2 96.94 9.19 -10 -5 2 101.24 38.76 10 5 2 75.05 7.18 10 5 2 65.96 12.85 -10 5 -2 85.49 8.26 10 5 2 111.43 15.45 -10 -5 2 68.21 10.13 10 -5 -2 68.95 11.67 10 -5 3 68.01 8.43 -10 5 3 50.22 10.78 10 5 -3 52.03 7.64 -10 5 3 65.65 12.53 10 -5 3 67.89 10.90 -10 -5 -3 54.82 7.95 -10 -5 -3 52.36 6.84 10 5 -3 49.19 8.77 -10 5 3 69.82 7.51 10 5 -3 70.83 6.50 10 5 -3 70.66 14.54 10 -5 3 63.53 10.99 10 -5 3 65.00 6.29 10 5 -3 49.76 8.45 10 5 -3 52.28 9.73 -10 -5 -3 60.52 7.89 -10 -5 -3 52.82 9.26 10 5 -3 72.20 7.27 -10 -5 -3 64.96 10.38 10 -5 3 80.32 7.97 10 -5 3 61.36 7.47 -10 5 3 62.93 6.04 -10 -5 -3 69.13 6.76 -10 -5 -3 45.47 7.95 10 5 -3 68.66 12.37 10 5 -3 66.70 8.71 -10 -5 -3 68.26 8.18 -10 5 3 62.62 7.62 10 -5 3 47.39 14.23 -10 5 3 35.72 16.49 10 5 -3 48.66 9.91 -10 -5 -3 58.23 8.85 -10 5 -3 46.34 17.31 10 5 3 84.40 11.28 -10 -5 3 62.32 6.24 10 5 3 66.89 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394.74 29.33 -7 6 0 406.41 28.94 -7 6 0 372.98 30.60 7 6 0 407.75 29.21 -7 -6 0 362.17 30.41 -7 -6 0 366.48 29.13 -7 -6 0 419.74 29.34 7 6 0 424.52 29.41 7 -6 0 357.33 30.20 7 -6 0 417.87 29.60 7 -6 0 388.32 29.92 -7 6 0 363.19 29.60 7 6 0 442.11 36.98 -7 6 0 418.35 29.53 -7 -6 -1 40.41 6.74 -7 6 1 45.16 4.49 7 -6 1 49.52 6.15 -7 -6 -1 51.28 6.05 -7 -6 -1 59.89 17.11 7 6 -1 36.73 5.23 -7 6 1 44.89 5.25 -7 -6 -1 46.60 6.30 7 6 -1 44.43 16.91 -7 -6 -1 53.14 7.34 7 -6 1 73.94 20.89 7 6 -1 47.21 5.93 -7 -6 -1 51.28 5.54 7 6 -1 48.48 6.59 -7 6 1 40.34 5.47 -7 6 1 44.64 4.99 7 6 -1 42.82 5.22 7 -6 1 49.09 5.64 7 6 -1 49.12 5.37 7 -6 1 37.88 5.37 7 -6 1 32.47 7.83 -7 6 1 38.43 6.98 7 -6 1 42.17 11.86 -7 -6 -1 37.72 5.86 -7 6 1 51.35 10.28 -7 6 -1 46.04 5.18 7 -6 -1 33.27 8.62 7 6 1 37.53 4.96 -7 6 -1 51.40 8.86 -7 -6 1 42.83 5.41 7 6 1 44.66 6.52 7 6 1 51.92 6.39 -7 -6 1 49.31 6.43 7 -6 -1 45.68 5.86 7 -6 -1 36.41 5.87 -7 6 -1 46.70 6.24 7 -6 -1 41.42 5.98 -7 -6 1 86.99 19.36 7 6 1 46.37 6.93 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317.79 24.21 7 -6 3 340.07 25.05 -7 -6 -3 305.47 25.37 7 -6 3 327.03 32.51 7 -6 3 303.06 24.52 7 6 -3 340.31 28.72 7 -6 3 296.28 39.28 7 -6 3 338.21 27.56 7 -6 3 337.05 26.24 -7 6 3 335.69 26.38 -7 6 3 320.33 28.28 7 6 -3 334.52 25.54 -7 6 3 344.53 24.78 7 -6 3 348.56 25.59 7 -6 3 329.33 24.66 -7 6 3 293.42 36.08 7 6 -3 314.15 36.51 -7 6 3 332.40 25.10 7 6 -3 332.16 24.43 -7 -6 -3 311.67 25.93 7 -6 3 336.07 24.29 -7 -6 3 330.18 24.53 7 -6 -3 339.33 26.22 -7 -6 3 333.24 24.35 -7 6 -3 318.20 26.23 -7 -6 3 348.00 26.37 -7 -6 3 338.76 25.01 -7 6 -3 312.06 35.74 7 6 3 324.60 25.39 -7 6 -3 329.97 24.97 7 6 3 294.36 24.98 7 6 3 320.60 35.83 7 -6 -3 322.12 24.92 7 -6 -3 297.35 39.48 -7 -6 3 333.72 28.01 -7 -6 3 333.66 26.30 7 6 3 341.37 26.05 7 6 3 347.51 24.76 -7 -6 -4 116.02 11.07 7 -6 4 91.34 22.08 -7 6 4 91.75 30.55 7 6 -4 90.02 33.51 7 6 -4 115.03 10.90 7 6 -4 107.79 10.18 7 6 -4 98.56 12.32 7 -6 4 124.06 10.29 7 -6 4 88.67 14.06 -7 6 4 84.08 17.04 7 -6 4 170.33 42.18 -7 -6 -4 108.49 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84.60 17.71 8 -6 2 95.09 30.29 -8 -6 -2 141.00 22.06 8 6 -2 94.31 9.64 -8 6 2 101.97 8.07 8 6 -2 139.02 31.12 -8 6 2 98.17 8.88 8 6 -2 91.13 10.20 8 -6 2 95.66 10.04 8 6 2 93.86 8.73 8 6 2 78.37 9.40 -8 6 -2 119.15 25.41 -8 -6 2 103.77 8.20 8 6 2 93.78 9.99 8 6 2 103.47 11.81 -8 6 -2 89.08 10.57 8 -6 -2 106.76 10.34 -8 -6 2 91.85 10.58 8 -6 -2 114.71 30.49 8 -6 -2 106.93 8.88 -8 -6 2 102.48 12.79 -8 -6 2 115.28 24.27 -8 6 -2 98.02 9.67 -8 6 -2 86.42 8.24 8 6 2 97.26 8.18 -8 -6 2 89.43 8.44 8 6 2 115.03 24.01 -8 6 3 156.21 15.07 8 6 -3 149.29 11.60 -8 6 3 109.33 17.39 8 6 -3 154.43 33.34 -8 -6 -3 153.40 12.84 8 -6 3 151.99 13.56 -8 -6 -3 149.88 12.05 8 -6 3 161.15 16.56 8 -6 3 129.31 12.47 8 -6 3 196.51 38.44 -8 -6 -3 161.70 13.33 8 -6 3 116.46 22.83 -8 6 3 142.20 11.37 8 6 -3 141.22 13.02 8 6 -3 151.07 12.33 -8 6 3 156.73 35.45 -8 6 3 165.46 12.32 8 6 -3 135.23 12.41 -8 -6 -3 140.04 13.81 -8 6 3 127.01 12.43 8 -6 3 151.05 11.52 8 6 -3 132.09 13.39 8 -6 3 161.65 12.73 -8 -6 -3 142.88 12.07 -8 -6 -3 128.63 12.65 8 -6 3 142.50 12.09 8 6 -3 150.27 13.06 8 6 3 128.92 12.54 8 6 3 162.38 14.02 -8 -6 3 160.62 11.35 8 -6 -3 126.26 13.70 8 6 3 137.54 14.88 -8 6 -3 139.75 12.02 8 6 3 149.05 11.35 8 -6 -3 129.89 13.55 -8 -6 3 127.30 17.34 8 6 3 130.33 30.04 -8 -6 3 144.93 11.67 8 -6 -3 135.51 11.85 -8 -6 3 134.70 14.08 -8 6 -3 145.17 12.24 8 -6 -3 135.87 11.79 8 -6 -3 150.15 12.21 -8 -6 3 157.59 12.48 -8 6 -3 172.32 31.75 8 6 3 148.77 11.88 -8 6 -3 146.31 14.17 -8 6 -3 146.65 12.22 8 -6 4 38.19 6.97 8 6 -4 25.38 7.54 -8 -6 -4 23.32 6.40 -8 6 4 33.10 5.57 8 -6 4 31.68 13.06 -8 6 4 36.12 14.26 -8 -6 -4 17.83 8.49 8 -6 4 35.66 6.34 8 6 -4 31.09 6.01 -8 -6 -4 32.74 7.42 -8 -6 -4 32.12 14.30 8 6 -4 36.48 8.07 -8 -6 -4 47.22 9.49 -8 6 4 28.08 15.44 8 -6 4 23.00 8.01 8 -6 4 28.89 8.35 -8 -6 -4 51.15 12.16 -8 -6 -4 29.95 5.93 -8 6 4 20.72 9.65 -8 -6 -4 27.77 6.91 -8 6 4 24.38 6.19 8 -6 4 39.84 12.73 -8 -6 -4 25.25 5.35 8 6 -4 19.78 4.78 -8 -6 -4 26.55 6.44 8 6 -4 22.50 4.57 8 6 -4 21.26 7.01 8 6 -4 23.11 6.97 8 6 -4 18.09 6.98 -8 6 4 26.42 4.06 8 -6 4 33.54 4.41 -8 -6 4 24.23 7.78 8 6 4 25.36 8.80 -8 6 -4 26.06 7.79 -8 -6 4 17.95 4.52 8 -6 -4 54.36 12.64 8 -6 -4 19.56 7.57 8 6 4 26.03 4.79 -8 -6 4 23.16 11.18 8 6 4 20.61 6.88 8 6 4 27.50 4.08 -8 6 -4 33.22 7.18 -8 6 -4 27.05 6.38 -8 -6 4 52.43 17.03 8 -6 -4 21.38 5.42 8 6 4 50.39 13.22 8 -6 -4 20.96 5.70 -8 6 -4 30.64 7.98 8 -6 -4 14.16 6.83 -8 -6 4 26.86 6.05 8 -6 -4 26.44 9.34 -8 6 -4 29.44 6.69 -8 -6 4 28.94 5.18 -8 6 -4 20.78 6.12 8 -6 -4 33.55 6.10 -8 -6 4 28.87 3.99 8 -6 -4 26.12 5.82 -8 6 -4 32.44 7.27 -8 6 -4 22.14 5.38 -8 6 -4 37.42 9.59 8 -6 -4 33.12 6.57 -8 -6 -5 35.59 7.26 -8 -6 -5 38.27 6.34 8 -6 5 27.13 6.84 8 -6 5 42.14 8.74 -8 -6 -5 36.94 9.00 8 -6 5 31.21 16.17 8 -6 5 21.20 8.03 8 6 -5 25.04 5.78 -8 6 5 4.47 12.38 8 6 -5 40.91 12.99 8 6 -5 39.98 6.55 -8 6 5 37.04 6.26 -8 -6 -5 44.81 8.28 -8 6 5 38.96 4.70 8 -6 5 38.22 5.05 8 -6 5 13.54 19.40 -8 -6 -5 33.39 5.91 -8 -6 -5 44.90 6.43 8 6 -5 30.17 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260.76 19.28 -10 -6 2 263.43 19.05 10 6 2 367.28 62.97 -10 6 3 34.32 12.81 10 -6 3 32.41 4.78 -10 -6 -3 33.23 8.34 -10 -6 -3 26.97 9.64 -10 -6 -3 37.65 5.55 -10 -6 -3 26.20 6.72 -10 -6 -3 35.08 6.93 -10 -6 -3 23.79 7.55 10 -6 3 42.32 7.32 10 -6 3 45.77 14.66 -10 -6 -3 21.22 5.61 -10 6 3 27.16 9.85 10 6 -3 24.81 9.58 -10 -6 -3 23.12 6.71 -10 -6 -3 28.63 6.83 -10 6 3 23.71 9.07 -10 6 3 7.89 17.06 10 -6 3 38.55 5.92 10 -6 3 41.47 7.58 10 6 -3 34.27 9.63 10 6 -3 31.41 6.41 10 -6 3 49.64 9.85 10 -6 3 19.78 10.23 10 -6 3 36.45 9.56 -10 6 3 28.00 5.81 -10 -6 -3 26.48 7.04 10 6 -3 19.47 7.12 -10 6 3 37.14 6.55 -10 6 3 35.54 4.48 10 6 -3 28.19 4.89 10 6 -3 43.22 10.32 10 6 -3 28.14 6.40 10 6 -3 38.99 7.80 10 6 -3 28.36 14.13 10 -6 3 14.80 12.32 10 6 -3 42.15 6.06 -10 6 -3 27.22 10.73 -10 -6 3 27.45 7.00 -10 -6 3 17.90 10.13 10 -6 -3 23.33 8.37 -10 6 -3 29.99 7.48 -10 -6 3 31.88 4.88 -10 6 -3 33.19 8.11 10 -6 -3 22.58 7.56 10 -6 -3 36.43 7.52 -10 -6 3 36.60 4.74 10 -6 -3 46.02 9.48 -10 6 -3 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357.76 25.14 -8 7 -1 323.22 25.51 8 -7 -1 407.65 42.10 8 7 1 346.50 25.56 -8 7 -1 305.51 26.09 8 -7 -1 330.26 25.44 8 7 1 340.09 26.35 -8 -7 1 338.47 25.11 -8 -7 1 320.36 27.90 8 7 1 346.79 27.11 8 -7 2 37.76 6.46 8 -7 2 12.27 16.85 8 7 -2 32.65 15.79 -8 7 2 27.50 11.38 -8 7 2 42.21 5.98 8 7 -2 42.71 8.37 -8 -7 -2 33.48 6.29 8 7 -2 65.74 8.38 8 -7 2 56.58 6.74 -8 7 2 49.39 9.22 8 7 -2 26.72 7.18 8 -7 2 38.04 4.89 -8 -7 -2 29.60 7.35 8 -7 2 42.56 6.66 8 7 -2 49.08 6.92 -8 7 2 32.06 5.47 -8 -7 -2 46.03 7.47 -8 7 2 43.78 4.61 8 -7 2 44.36 10.42 8 7 -2 47.86 7.87 -8 7 2 51.37 6.02 -8 -7 -2 47.55 6.89 8 -7 2 39.94 7.53 8 7 -2 26.36 6.87 -8 7 -2 47.32 7.17 -8 -7 2 30.30 6.42 8 7 2 39.28 6.72 -8 7 -2 31.97 6.98 -8 -7 2 27.95 5.49 -8 7 -2 34.06 5.62 8 7 2 39.66 9.87 -8 7 -2 43.04 20.30 -8 7 -2 43.38 8.31 -8 -7 2 30.34 7.75 8 7 2 47.88 7.32 -8 -7 2 37.72 4.51 8 -7 -2 43.80 5.93 8 7 2 29.24 5.00 8 -7 -2 87.75 31.43 8 7 2 10.40 12.81 -8 -7 2 37.25 11.79 -8 -7 2 44.93 5.42 8 7 2 46.12 7.46 8 -7 -2 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19.81 4.20 -7 -8 1 2.24 3.73 -7 8 -1 -9.97 15.50 -7 8 -1 5.39 5.07 -7 8 2 134.47 12.26 7 8 -2 107.75 11.03 7 8 -2 117.39 28.24 7 -8 2 127.99 11.77 7 8 -2 99.35 10.91 7 8 -2 113.73 10.92 7 -8 2 115.74 10.48 7 -8 2 107.72 13.07 -7 8 2 121.79 13.11 -7 -8 -2 130.76 12.04 7 8 -2 116.65 11.62 7 8 -2 131.19 30.00 7 -8 2 126.42 9.81 -7 -8 -2 122.45 11.16 -7 8 2 120.41 10.30 7 -8 2 81.84 32.81 7 -8 2 119.60 10.86 -7 8 2 122.82 9.66 7 -8 2 140.60 10.51 -7 8 2 112.20 28.11 7 -8 2 124.39 19.63 7 8 -2 100.41 13.34 -7 8 2 117.61 10.83 -7 8 -2 133.81 28.33 7 8 2 110.28 11.57 7 8 2 125.42 10.30 7 8 2 106.94 26.04 -7 8 -2 134.17 12.10 7 8 2 119.43 9.70 -7 -8 2 112.25 9.99 7 8 2 102.26 27.24 -7 8 -2 92.62 11.01 7 8 2 116.61 11.68 -7 -8 2 135.09 14.72 -7 -8 2 119.44 11.87 -7 8 -2 108.87 10.49 -7 -8 2 111.06 12.67 7 8 2 120.07 10.04 7 -8 -2 135.64 11.77 7 8 2 110.39 10.88 -7 -8 2 125.05 10.05 7 8 2 138.66 16.71 -7 8 3 15.60 8.03 7 8 -3 36.84 17.97 -7 8 3 -2.47 5.42 7 -8 3 12.90 9.76 -7 -8 -3 4.70 5.69 7 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11.76 4.79 7 -8 -8 24.31 17.36 -7 8 -8 19.22 5.61 7 -8 -8 5.87 6.24 -7 -8 8 19.73 7.02 -7 8 -8 30.09 7.03 -7 -8 8 12.36 4.44 -7 8 -8 10.82 6.20 7 -8 -8 10.41 4.41 7 8 8 14.04 5.21 -7 -8 8 3.34 9.97 7 -8 -8 1.86 5.32 -7 -8 8 18.28 5.83 -7 8 -8 23.29 6.50 7 -8 -8 17.29 5.77 -7 8 -8 10.05 5.01 -7 -8 -9 13.47 3.93 7 -8 9 13.49 4.68 7 8 -9 18.35 6.51 -7 -8 -9 26.61 4.75 -7 -8 -9 15.62 3.88 -7 8 9 11.45 4.62 7 8 -9 18.23 4.04 7 8 -9 21.08 5.18 -7 -8 -9 28.67 5.19 7 8 -9 30.59 4.79 7 8 -9 13.25 5.16 -7 -8 -9 22.81 7.19 7 8 -9 12.23 6.11 -7 -8 -9 22.14 5.47 -7 -8 -9 21.50 4.83 -7 8 9 30.07 8.55 7 8 -9 3.76 5.03 7 8 -9 17.84 5.93 7 -8 9 6.67 5.80 -7 -8 -9 27.65 8.95 7 -8 9 9.81 13.02 7 8 9 4.75 6.26 -7 8 -9 9.68 3.82 7 -8 -9 7.63 4.05 7 -8 -9 10.07 3.68 -7 8 -9 8.79 5.44 7 -8 -9 27.60 7.12 7 -8 -9 15.83 4.12 -7 8 -9 13.62 4.73 -7 -8 9 11.07 4.60 -7 8 -9 10.75 4.54 -7 8 -9 8.82 3.89 7 -8 -9 8.05 3.09 7 -8 -9 14.02 7.04 -7 -8 9 15.67 4.10 7 -8 -9 9.36 3.84 7 -8 -9 7.65 3.52 -7 -8 -10 4.42 3.43 7 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18.67 10.92 -5 -9 5 2.91 5.31 5 -9 -5 20.25 5.25 5 -9 -5 -2.81 7.75 5 -9 -5 9.30 5.28 5 -9 -5 19.92 5.98 -5 -9 5 -1.52 10.22 -5 9 -5 12.57 5.73 5 -9 -5 -5.51 8.03 5 9 5 4.88 3.79 5 -9 -5 16.24 8.57 -5 9 -5 4.81 9.55 -5 -9 5 10.05 9.42 -5 9 -5 16.32 4.86 -5 -9 5 7.24 10.24 5 9 5 5.70 7.61 5 -9 -5 18.06 5.78 -5 9 -5 14.42 6.37 5 -9 -5 8.29 4.02 5 9 5 26.16 13.79 5 -9 -5 15.18 3.74 -5 -9 5 6.89 6.72 -5 9 -5 9.95 4.91 5 9 5 8.45 3.75 -5 -9 5 10.23 4.00 -5 -9 5 5.59 4.00 5 -9 -5 3.58 3.68 -5 -9 5 7.29 3.38 5 9 5 21.67 10.32 -5 9 -5 19.46 6.42 -5 -9 -6 42.78 8.70 5 9 -6 41.66 7.86 5 -9 6 65.50 7.51 -5 9 6 70.39 11.95 -5 -9 -6 59.47 13.77 5 -9 6 53.79 8.37 5 -9 6 47.20 7.65 -5 9 6 44.99 6.97 -5 -9 -6 44.75 16.51 5 -9 6 62.51 6.23 -5 -9 -6 54.95 10.36 5 9 -6 51.24 10.84 -5 -9 -6 52.00 10.52 5 9 -6 58.45 10.44 -5 -9 -6 57.41 9.38 -5 -9 -6 73.45 9.31 5 -9 6 61.53 11.79 -5 -9 -6 54.79 7.25 -5 -9 -6 32.72 9.60 -5 -9 -6 56.14 7.25 5 9 -6 50.88 7.75 5 9 -6 63.86 7.20 -5 9 6 45.22 14.17 -5 -9 -6 52.69 7.29 5 -9 6 65.94 18.81 -5 -9 -6 54.70 10.91 5 -9 -6 46.04 8.19 5 -9 -6 64.72 5.76 -5 9 -6 47.62 6.72 -5 -9 6 64.27 8.45 5 9 6 52.31 6.08 5 9 6 56.16 6.79 5 -9 -6 74.03 9.07 -5 9 -6 64.49 10.77 5 -9 -6 41.10 6.80 -5 -9 6 48.25 11.54 -5 9 -6 42.53 9.16 -5 -9 6 18.49 18.10 -5 -9 6 55.47 8.26 -5 -9 6 71.72 16.68 5 -9 -6 67.21 7.61 -5 -9 6 69.13 17.34 5 -9 -6 53.08 6.96 -5 -9 6 49.99 7.73 -5 -9 6 48.15 5.88 -5 9 -6 54.39 11.51 -5 9 -6 39.08 12.65 5 -9 -6 84.17 12.51 5 9 6 61.80 14.80 -5 -9 6 54.19 7.13 5 -9 -6 70.68 11.85 -5 9 -6 32.48 10.22 -5 -9 -7 44.22 6.55 5 -9 7 49.20 7.47 5 -9 7 46.20 5.80 -5 -9 -7 38.93 7.53 -5 -9 -7 10.73 21.56 -5 9 7 23.84 20.83 -5 9 7 41.52 7.95 -5 -9 -7 50.89 9.22 5 -9 7 65.22 27.76 -5 -9 -7 43.47 5.49 -5 -9 -7 53.29 8.23 5 9 -7 43.04 6.83 -5 -9 -7 39.01 10.36 5 9 -7 35.38 16.84 -5 -9 -7 41.61 6.39 5 9 -7 36.53 6.23 -5 -9 -7 44.82 12.97 -5 9 7 38.28 9.41 5 9 -7 47.96 7.37 5 9 -7 26.27 8.12 -5 9 7 33.05 10.08 -5 -9 -7 45.15 6.21 5 9 -7 36.24 8.63 -5 -9 -7 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12.13 4.18 -5 9 -9 6.86 4.10 -5 9 -9 5.16 4.74 5 -9 -9 8.61 3.98 5 9 -10 -1.70 3.40 -5 -9 -10 4.21 3.66 -5 -9 -10 4.67 3.21 5 9 -10 -1.98 3.31 5 9 -10 3.13 3.44 -5 -9 -10 1.46 1.98 -5 -9 -10 0.31 3.33 -5 -9 -10 4.42 2.14 5 -9 10 -4.45 5.78 -5 -9 -10 2.20 2.73 5 9 -10 5.56 2.82 5 -9 10 -0.07 4.65 -5 -9 -10 3.81 3.28 5 9 -10 -6.04 3.43 5 9 -10 3.44 3.89 5 9 -10 1.01 0.78 -5 -9 -10 1.31 2.83 -5 9 -10 -3.04 2.89 5 -9 -10 0.82 2.20 5 -9 -10 1.74 2.66 5 -9 -10 3.97 2.95 -5 9 -10 -1.66 2.94 -5 -9 10 -6.86 4.65 5 -9 -10 0.14 3.35 5 -9 -10 4.95 3.74 5 -9 -10 2.72 3.26 -5 -9 10 -4.23 3.87 5 -9 -10 8.61 5.27 5 -9 -10 -0.68 5.30 -5 9 -10 -5.67 3.27 -5 9 -10 4.28 3.67 -5 9 -10 0.45 3.71 5 -9 -10 2.01 2.91 -5 9 -10 -1.99 3.49 5 -9 -10 0.10 2.72 -5 9 -10 2.22 3.40 -5 -9 10 -4.58 3.78 -5 -9 -11 -1.00 4.70 5 9 -11 0.81 3.34 5 9 -11 2.56 2.32 5 9 -11 4.22 2.70 -5 -9 -11 -2.90 4.38 5 9 -11 2.95 2.32 5 9 -11 0.41 0.51 -5 -9 -11 2.10 2.33 -5 -9 -11 0.91 1.39 5 9 -11 0.09 2.55 5 9 -11 -0.45 3.19 -5 -9 -11 0.97 2.52 5 -9 11 -15.73 9.64 5 -9 -11 3.12 1.80 5 -9 -11 1.49 2.70 5 -9 -11 2.18 2.48 -5 9 -11 0.78 2.50 5 -9 -11 2.44 3.13 5 -9 -11 3.88 2.39 -5 9 -11 -0.27 1.98 5 -9 -11 1.09 2.82 -5 -9 11 3.25 5.66 5 -9 -11 -1.27 1.45 -5 9 -11 2.81 3.17 -5 9 -11 1.11 2.59 -5 9 -11 0.07 2.32 -5 -9 11 -2.25 3.46 -6 9 0 287.69 23.47 6 9 0 286.77 22.78 6 -9 0 307.50 23.15 6 9 0 302.43 24.00 6 9 0 279.79 22.87 6 -9 0 299.76 23.22 6 -9 0 311.10 46.68 6 -9 0 275.78 26.26 6 9 0 297.94 22.90 6 -9 0 312.94 22.46 -6 -9 0 280.08 22.86 -6 9 0 327.16 22.36 -6 -9 0 312.28 24.05 -6 -9 0 305.78 23.74 6 9 0 299.99 23.45 6 9 0 311.51 33.32 -6 9 0 289.86 22.82 -6 -9 0 312.63 23.06 6 9 0 344.61 24.14 6 9 0 297.92 22.45 6 -9 0 292.11 22.94 6 -9 0 301.97 23.79 -6 -9 0 279.14 22.37 6 9 0 286.47 34.62 6 -9 1 5.60 4.78 -6 9 1 14.57 11.32 6 -9 1 23.25 3.73 6 9 -1 26.64 5.15 6 9 -1 16.87 4.52 -6 9 1 16.38 3.52 -6 9 1 8.55 4.63 -6 9 1 14.15 6.05 6 -9 1 13.99 7.20 -6 9 1 27.49 5.72 -6 -9 -1 10.00 4.72 6 9 -1 15.67 6.87 6 -9 1 11.27 4.88 6 9 -1 18.23 6.04 -6 -9 -1 10.92 5.95 -6 -9 -1 13.51 4.45 6 9 -1 19.27 15.98 -6 9 1 11.85 7.55 6 9 -1 16.40 5.33 6 -9 1 20.15 5.19 6 9 -1 30.47 25.32 6 9 -1 15.89 5.32 -6 -9 1 23.13 4.40 6 9 1 31.99 7.69 -6 -9 1 25.34 7.82 -6 -9 1 35.04 6.20 -6 9 -1 19.18 4.06 6 9 1 14.80 4.60 -6 -9 1 12.81 3.75 -6 9 -1 20.87 5.62 6 -9 -1 12.58 5.73 6 -9 -1 22.98 10.13 6 -9 -1 20.99 5.75 -6 9 -1 10.56 9.26 6 9 1 18.52 6.97 6 -9 -1 31.82 19.68 -6 9 -1 17.56 5.46 6 9 1 18.53 5.43 -6 -9 1 16.85 4.30 -6 9 -1 19.73 4.56 6 -9 -1 22.37 5.62 6 9 1 17.96 6.09 6 9 1 -0.33 17.05 6 9 1 22.43 11.83 6 -9 -1 31.34 6.56 -6 -9 1 12.69 7.57 6 -9 2 164.06 16.22 -6 9 2 187.01 13.85 6 -9 2 172.08 21.71 -6 9 2 156.63 15.70 -6 -9 -2 180.28 14.64 -6 9 2 139.66 13.86 6 -9 2 181.49 13.63 6 9 -2 189.71 14.63 6 9 -2 177.94 14.26 6 9 -2 150.59 13.94 6 -9 2 174.40 14.28 6 -9 2 172.86 36.42 6 9 -2 202.99 30.82 -6 9 2 161.77 15.26 6 9 -2 157.55 14.15 6 9 -2 159.28 14.57 -6 9 2 179.84 31.11 6 -9 2 178.33 13.18 -6 -9 -2 151.47 14.65 -6 9 2 176.08 13.07 -6 9 2 165.83 13.70 6 9 2 213.73 32.53 -6 9 -2 215.01 37.80 -6 9 -2 141.47 14.27 -6 -9 2 178.98 17.52 6 9 2 181.82 13.71 6 -9 -2 167.72 35.31 6 -9 -2 165.90 14.84 -6 9 -2 184.99 14.37 -6 -9 2 158.85 15.79 6 9 2 165.76 17.01 6 9 2 177.35 13.25 -6 -9 2 166.41 14.89 -6 -9 2 168.23 13.50 -6 -9 2 185.04 13.32 6 9 2 164.12 15.01 -6 -9 2 172.18 13.58 6 9 2 152.30 14.23 -6 9 -2 162.91 14.92 -6 -9 2 160.09 14.04 6 9 2 181.36 15.51 6 -9 -2 173.61 14.16 -6 9 3 47.33 9.44 -6 -9 -3 31.05 7.51 -6 -9 -3 32.41 5.63 -6 -9 -3 29.50 8.93 6 9 -3 29.46 7.29 -6 -9 -3 44.44 6.74 6 -9 3 33.81 9.67 6 9 -3 72.84 25.00 -6 -9 -3 36.09 8.55 6 9 -3 93.23 32.16 6 -9 3 44.67 4.75 6 -9 3 37.58 6.10 -6 9 3 42.07 6.39 -6 9 3 38.15 6.59 6 9 -3 39.96 6.46 -6 -9 -3 30.29 8.19 6 9 -3 32.76 6.60 -6 9 3 59.43 19.38 -6 9 3 37.94 8.55 -6 -9 -3 37.94 6.14 6 -9 3 50.65 6.88 -6 9 3 47.58 4.53 -6 9 3 44.00 5.45 6 -9 3 20.53 14.02 6 9 -3 48.03 7.07 6 9 -3 34.28 8.90 6 -9 3 40.97 9.73 -6 -9 -3 55.17 8.71 6 -9 -3 36.00 7.68 6 9 3 50.65 17.51 -6 -9 3 37.94 8.07 -6 -9 3 40.85 4.62 6 9 3 30.50 9.98 -6 9 -3 20.94 15.69 6 -9 -3 42.56 6.66 -6 -9 3 56.53 6.65 6 9 3 43.70 8.58 6 -9 -3 38.45 21.76 -6 9 -3 39.32 7.04 6 -9 -3 36.82 10.07 -6 -9 3 35.01 9.15 6 9 3 37.96 7.30 6 9 3 47.79 5.43 -6 9 -3 40.23 6.26 -6 -9 3 36.64 5.82 -6 -9 3 37.33 5.64 6 -9 -3 37.64 7.69 6 9 3 64.50 19.07 -6 9 -3 28.17 6.98 -6 9 -3 31.20 6.97 6 -9 -3 43.09 5.98 -6 -9 3 48.48 13.40 -6 -9 3 39.92 9.48 -6 -9 3 36.54 5.91 6 9 3 51.95 8.26 6 9 3 42.21 4.74 -6 9 -3 40.39 8.60 6 9 -4 42.66 7.18 -6 -9 -4 41.25 8.18 6 -9 4 45.90 12.26 -6 -9 -4 43.95 6.65 -6 -9 -4 56.64 15.11 6 9 -4 45.68 9.83 6 -9 4 30.69 6.99 6 9 -4 48.78 10.50 -6 -9 -4 45.30 8.26 6 -9 4 29.75 10.37 6 9 -4 39.40 8.66 -6 9 4 42.46 5.73 6 9 -4 42.76 7.40 -6 -9 -4 36.92 7.14 6 9 -4 36.13 5.43 -6 9 4 53.13 11.14 -6 -9 -4 59.16 8.22 6 9 -4 54.30 6.73 6 -9 4 50.34 4.96 -6 -9 -4 34.48 8.15 6 9 -4 41.81 7.39 -6 9 4 36.44 9.22 -6 -9 -4 49.19 6.49 -6 9 4 46.46 7.18 -6 -9 -4 35.09 5.89 -6 -9 -4 44.35 10.07 6 -9 -4 38.01 6.12 -6 -9 4 63.61 11.18 -6 -9 4 53.07 6.74 6 -9 -4 20.73 8.06 6 -9 -4 47.27 7.12 6 9 4 32.64 8.19 6 9 4 42.29 5.13 -6 -9 4 26.81 9.80 6 9 4 66.39 13.30 6 9 4 43.00 9.29 6 -9 -4 43.65 7.60 -6 9 -4 32.33 8.12 -6 9 -4 47.76 9.57 -6 9 -4 53.66 8.04 6 -9 -4 47.39 6.92 -6 9 -4 35.39 6.15 -6 -9 4 61.92 17.97 -6 -9 4 58.90 11.62 -6 9 -4 50.28 7.17 6 -9 -4 46.92 9.07 -6 -9 4 49.98 7.00 -6 -9 4 44.41 4.92 6 -9 -4 43.55 6.23 6 9 4 47.22 9.80 6 -9 -4 32.97 10.08 6 9 4 42.87 5.66 -6 9 -4 46.35 7.26 -6 9 -4 39.56 10.23 -6 -9 4 30.77 6.15 -6 -9 4 54.29 5.99 6 9 -5 1.25 4.45 -6 -9 -5 9.73 4.29 -6 -9 -5 -0.95 4.69 6 -9 5 6.41 3.67 -6 9 5 8.12 4.57 -6 9 5 11.29 12.72 -6 9 5 1.32 8.41 6 9 -5 10.99 4.98 6 -9 5 8.06 4.69 6 -9 5 -3.11 4.61 -6 9 5 2.24 5.44 -6 9 5 -5.59 13.19 6 -9 5 -4.26 6.75 -6 -9 -5 3.86 4.32 6 9 -5 -1.92 21.56 6 9 -5 -3.48 4.27 -6 -9 -5 10.96 8.11 -6 -9 -5 0.77 3.69 -6 9 5 4.03 3.25 6 -9 5 6.95 6.09 6 -9 5 -5.01 14.60 6 9 -5 2.99 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13.35 10 -9 -1 55.78 8.15 -10 -9 1 64.16 18.63 10 -9 -1 62.82 6.84 10 9 1 52.85 10.78 -10 -9 1 53.07 7.80 -10 9 -1 63.47 10.30 -10 9 -1 57.29 6.45 -10 -9 1 67.40 6.88 -10 -9 1 40.39 12.36 -10 9 -1 56.52 7.75 -10 9 -1 56.11 10.87 -10 -9 1 54.87 6.62 10 -9 -1 53.82 7.41 -10 9 -1 48.18 11.46 10 9 1 65.39 7.98 10 9 1 69.14 6.52 10 9 1 54.05 7.11 -10 -9 1 51.48 6.11 10 9 1 64.92 15.76 -10 9 -1 53.75 6.49 -10 -9 1 57.14 10.62 -10 9 -1 78.58 17.05 -10 -9 1 47.81 7.68 -10 9 -1 80.29 36.29 -10 -9 1 54.11 7.25 10 -9 2 38.90 10.82 10 -9 2 19.58 4.91 10 9 -2 42.63 11.30 10 9 -2 25.39 4.83 -10 9 2 24.40 11.90 10 9 -2 19.98 7.44 -10 -9 -2 19.88 8.34 10 9 -2 18.65 8.23 -10 -9 -2 10.63 8.01 -10 9 2 25.91 4.34 -10 -9 -2 17.48 5.47 10 -9 2 3.87 11.97 -10 -9 -2 27.77 5.77 10 -9 2 2.92 12.57 10 -9 2 19.96 5.05 -10 -9 -2 24.13 6.16 -10 9 2 23.71 5.92 10 -9 2 18.75 6.76 -10 -9 -2 24.68 9.75 10 -9 2 27.88 6.62 -10 9 2 40.93 7.56 -10 -9 -2 22.71 6.51 10 -9 2 30.00 8.72 -10 -9 -2 23.44 7.25 -10 -9 -2 21.13 4.93 -10 9 2 20.00 8.62 10 9 -2 21.92 6.72 10 9 -2 28.63 6.36 10 9 -2 12.68 8.75 -10 -9 -2 21.19 5.07 10 -9 2 28.29 7.10 10 -9 2 34.49 9.17 -10 9 2 27.22 13.97 -10 9 2 27.80 9.16 -10 9 2 30.68 6.60 10 9 -2 16.49 6.44 10 -9 2 31.27 4.97 10 9 -2 11.98 6.55 -10 -9 2 16.57 4.72 -10 9 -2 24.75 9.98 -10 -9 2 27.35 5.82 10 9 2 20.10 4.57 10 -9 -2 19.13 7.44 -10 -9 2 14.83 5.69 10 9 2 18.15 6.58 10 -9 -2 17.08 7.09 -10 -9 2 7.21 11.82 10 -9 -2 17.87 10.51 10 9 2 29.23 6.21 10 -9 -2 29.44 5.73 -10 -9 2 25.32 4.79 -10 9 -2 26.70 5.22 -10 -9 2 30.13 5.05 10 -9 -2 27.53 5.38 -10 9 -2 16.52 11.76 -10 9 -2 26.34 5.68 10 9 2 27.31 10.15 -10 -9 2 31.87 18.56 -10 9 -2 29.91 7.93 -10 9 -2 26.21 5.25 10 9 2 3.37 15.79 10 -9 -2 12.65 6.97 -10 9 -2 40.13 8.90 -10 -9 2 10.51 7.96 10 9 2 23.54 6.58 10 9 2 30.49 7.05 -10 -9 2 18.88 8.11 10 9 2 18.75 5.92 10 -9 -2 29.34 7.96 10 -9 -2 34.87 6.32 10 -9 -2 15.76 8.04 -10 -9 2 20.35 5.96 10 -9 3 27.80 5.04 -10 -9 -3 9.87 10.39 10 9 -3 23.52 7.33 -10 9 3 27.89 12.75 -10 9 3 35.59 6.03 -10 9 3 20.25 8.95 10 9 -3 26.21 4.67 10 -9 3 19.84 16.14 -10 9 3 35.04 6.07 -10 -9 -3 28.05 6.05 10 9 -3 23.07 9.15 10 9 -3 20.91 6.58 -10 9 3 4.37 14.88 10 9 -3 30.58 10.53 -10 9 3 17.23 6.56 10 -9 3 9.50 17.96 -10 -9 -3 24.18 5.14 10 9 -3 19.42 6.27 -10 9 3 26.43 4.57 -10 -9 -3 29.24 6.64 -10 9 3 45.60 9.83 10 -9 3 30.16 8.65 10 9 -3 33.91 5.98 10 -9 3 45.63 8.69 10 -9 3 26.87 5.09 -10 9 3 27.03 8.05 -10 -9 -3 23.25 7.15 -10 -9 -3 21.49 6.62 -10 -9 -3 19.70 4.22 10 9 -3 37.00 9.14 -10 -9 -3 26.74 6.77 -10 -9 -3 30.02 10.08 10 -9 3 46.77 9.63 -10 -9 3 21.71 4.79 -10 9 -3 17.54 4.64 -10 9 -3 21.25 5.63 10 -9 -3 34.73 10.64 -10 -9 3 24.69 5.59 -10 9 -3 36.89 5.74 -10 9 -3 0.93 12.13 -10 -9 3 33.14 8.48 -10 -9 3 22.48 7.28 -10 -9 3 37.03 34.62 10 -9 -3 25.95 5.85 10 -9 -3 25.58 9.47 -10 9 -3 22.25 6.06 10 9 3 17.67 6.46 10 -9 -3 33.75 7.40 10 -9 -3 34.63 7.48 10 9 3 20.63 4.67 10 9 3 37.93 11.69 10 9 3 24.88 6.67 -10 9 -3 29.21 7.50 10 -9 -3 37.49 8.47 -10 9 -3 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52.31 9.46 5 -12 0 36.91 8.25 5 12 0 53.97 11.37 5 -12 0 25.92 17.72 5 12 0 59.44 7.21 5 12 0 62.09 9.03 5 -12 0 37.24 8.27 -5 12 0 49.03 7.63 -5 -12 0 51.60 7.18 -5 12 0 52.89 6.32 5 -12 0 42.49 6.99 5 12 -1 38.15 6.29 -5 -12 -1 43.55 7.72 5 12 -1 45.80 20.50 -5 12 1 49.79 13.42 -5 12 1 43.52 4.89 5 -12 1 49.99 5.27 -5 -12 -1 43.43 7.99 5 12 -1 39.25 5.81 5 12 -1 54.54 7.34 5 -12 1 42.80 9.38 5 -12 1 52.94 7.17 5 12 -1 31.76 6.88 5 12 -1 46.63 7.31 -5 12 1 40.14 6.33 -5 -12 -1 34.33 6.23 -5 12 1 26.73 8.18 -5 -12 -1 25.71 6.99 -5 -12 -1 45.41 7.12 5 12 -1 54.08 8.84 5 -12 1 43.81 5.33 5 12 -1 4.16 15.73 5 12 -1 40.56 10.04 -5 -12 -1 41.59 6.29 5 -12 1 29.48 6.03 -5 12 1 42.76 5.98 5 12 -1 35.07 8.11 5 -12 1 45.00 6.87 5 -12 1 29.18 10.12 -5 12 1 11.19 18.58 5 12 -1 57.80 33.97 5 -12 1 48.97 8.33 5 12 -1 44.43 6.63 5 -12 1 45.87 6.74 5 12 -1 42.32 9.37 5 12 -1 41.56 9.78 -5 -12 -1 29.84 7.75 5 12 1 21.21 7.86 5 -12 -1 46.20 6.27 -5 -12 1 43.58 7.48 -5 12 -1 37.10 10.27 -5 12 -1 57.07 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26 0 -4.41 2.99 -4 26 0 1.01 3.20 -4 -26 0 -0.23 2.08 4 -26 0 2.41 1.87 4 -26 0 -0.66 2.41 4 26 0 3.45 4.17 -4 -26 0 0.19 2.23 4 26 0 4.39 2.75 -4 26 0 4.51 2.23 4 26 0 0.58 2.47 -4 26 0 -0.71 2.36 4 26 -1 2.74 3.31 4 26 -1 -2.12 2.31 4 -26 1 0.10 1.94 4 26 -1 -3.15 3.50 -4 26 1 -1.23 2.16 -4 -26 -1 0.38 1.93 -4 -26 -1 -1.33 2.01 4 -26 1 -1.03 2.30 -4 26 -1 2.26 2.60 4 -26 -1 0.63 1.84 4 26 1 3.01 3.60 4 26 1 -3.24 2.45 -4 26 -1 1.09 2.13 -4 -26 1 -2.64 2.22 4 26 1 -3.96 2.46 -4 -26 1 0.12 2.25 -4 26 2 1.53 2.04 4 -26 2 2.33 4.09 -4 -26 -2 -0.61 1.83 -4 26 2 -0.92 2.27 4 -26 2 -0.29 2.10 -4 -26 -2 1.08 1.73 4 26 -2 -2.69 2.41 4 -26 2 -1.22 2.30 4 26 -2 -1.45 2.62 4 26 2 2.53 3.29 -4 -26 2 -1.07 2.24 -4 -26 2 -5.77 4.83 -4 -26 2 0.15 4.05 4 -26 -2 1.30 1.64 4 26 2 -1.59 2.49 -4 -26 2 0.65 2.13 -4 26 -2 -3.62 2.31 -4 26 -2 -1.97 2.11 4 26 2 -0.45 1.79 5 26 0 -1.44 3.21 5 -26 0 0.01 2.19 5 26 0 -0.46 2.68 -5 26 0 6.58 3.73 5 -26 0 -0.31 1.78 -5 26 0 0.47 2.01 -5 -26 0 1.40 2.09 5 26 0 -0.96 4.21 5 -26 1 -0.27 1.84 -5 26 1 0.06 2.17 5 26 -1 0.55 2.13 5 26 -1 -0.12 2.85 -5 -26 -1 1.15 1.97 5 -26 1 -1.91 1.96 5 26 -1 3.42 4.51 -5 -26 -1 -3.12 1.74 5 26 1 -1.28 2.63 -5 -26 1 0.20 2.20 5 26 1 -1.54 2.39 5 26 1 3.51 3.06 5 -26 -1 -0.45 1.85 -5 -26 1 1.33 2.12 -5 26 -1 1.44 2.05 -5 26 -1 -0.56 3.16 5 -26 2 -5.48 4.66 5 -26 2 -0.65 2.09 5 26 -2 -0.55 3.34 5 26 -2 -0.17 2.36 -5 -26 -2 0.76 1.73 -5 26 2 2.60 2.22 -5 26 -2 0.63 3.33 5 -26 -2 3.64 2.19 5 26 2 -3.08 2.08 5 26 2 -1.44 2.30 5 26 2 1.42 3.01 -5 26 -2 0.47 2.29 5 -26 -2 6.25 2.15 -5 -26 2 -3.33 3.18 6 26 0 -2.03 2.29 -6 26 0 2.38 3.65 6 -26 0 2.35 1.91 6 -26 0 -0.70 2.15 6 26 0 1.09 3.19 -6 26 0 4.28 3.77 -6 26 0 -1.86 1.92 6 26 0 3.94 4.64 -6 -26 0 0.70 2.05 -6 26 1 1.26 2.82 6 -26 1 1.62 1.88 -6 -26 -1 0.17 1.80 6 26 -1 -4.42 2.64 -6 26 -1 -3.33 2.46 6 -26 -1 -1.11 1.58 -6 -26 1 2.43 2.28 -6 26 -1 4.34 4.14 0 27 0 3.66 2.57 0 27 0 1.02 2.18 0 27 0 4.65 2.97 0 27 0 -0.04 3.81 0 -27 0 1.17 1.70 1 27 0 0.05 3.53 -1 -27 0 -0.23 1.69 -1 27 0 -4.29 3.77 -1 27 0 1.47 3.43 -1 27 0 3.30 2.40 -1 27 0 4.99 4.25 1 -27 0 0.42 1.87 1 27 0 -7.74 4.23 1 27 0 -0.56 2.67 1 27 0 -1.41 2.27 0 0 0 0.00 0.00 _chemical_name_common voacamine _chemical_formula_moiety 'C43 H57 N4 O5, 2.5(H2 O)' _cell_measurement_reflns_used 9443 _cell_measurement_theta_min 3.65 _cell_measurement_theta_max 67.657 _exptl_crystal_description parallelepiped _exptl_crystal_colour 'light pink' _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.6735 _exptl_special_details _diffrn_ambient_temperature 298(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source 'Cu Incoatec microsource' _diffrn_measurement_device_type 'Bruker D8 Venture/Photon 100 CMOS' _diffrn_measurement_method '\j and \w scans' _diffrn_detector_area_resol_mean 10.4167 _chemical_absolute_configuration rmad _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 97985 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.0510(16) 0.5633(19) 0.137(3) 0.110(5) Uani 0.391(9) 1 d D U P A 1 H1A H 0.024619 0.581270 0.067700 0.165 Uiso 0.391(9) 1 calc R U P A 1 H1B H 0.061762 0.592779 0.200717 0.165 Uiso 0.391(9) 1 calc R U P A 1 H1C H 0.023033 0.532152 0.174982 0.165 Uiso 0.391(9) 1 calc R U P A 1 C2 C 0.1173(14) 0.5382(15) 0.086(3) 0.104(3) Uani 0.391(9) 1 d D U P A 1 H2 H 0.127008 0.543376 -0.001102 0.124 Uiso 0.391(9) 1 calc R U P A 1 C3 C 0.1666(15) 0.5072(13) 0.160(3) 0.100(2) Uani 0.391(9) 1 d D U P A 1 N4 N 0.2420(14) 0.4285(12) 0.076(2) 0.098(2) Uani 0.391(9) 1 d D U P A 1 C16 C 0.3113(15) 0.4184(16) 0.020(3) 0.101(5) Uani 0.391(9) 1 d D U P A 1 H16A H 0.341594 0.399489 0.082600 0.151 Uiso 0.391(9) 1 calc R U P A 1 H16B H 0.331821 0.455720 -0.005064 0.151 Uiso 0.391(9) 1 calc R U P A 1 H16C H 0.306715 0.393154 -0.054011 0.151 Uiso 0.391(9) 1 calc R U P A 1 C4 C 0.2360(14) 0.4943(13) 0.107(3) 0.099(3) Uani 0.391(9) 1 d D U P A 1 H4A H 0.272478 0.505377 0.168531 0.119 Uiso 0.391(9) 1 calc R U P A 1 H4B H 0.243247 0.517400 0.029034 0.119 Uiso 0.391(9) 1 calc R U P A 1 C5 C 0.2249(18) 0.3874(15) 0.187(3) 0.096(2) Uani 0.391(9) 1 d D U P A 1 H5 H 0.221878 0.346636 0.154313 0.116 Uiso 0.391(9) 1 calc R U P A 1 C6 C 0.285(2) 0.390(3) 0.291(3) 0.096(2) Uani 0.391(9) 1 d D U P A 1 H6A H 0.323281 0.364090 0.264307 0.115 Uiso 0.391(9) 1 calc R U P A 1 H6B H 0.303299 0.430193 0.294522 0.115 Uiso 0.391(9) 1 calc R U P A 1 C7 C 0.3080(17) 0.2640(13) 0.423(3) 0.104(3) Uani 0.391(9) 1 d D U P A 1 H7 H 0.325398 0.263612 0.338764 0.125 Uiso 0.391(9) 1 calc R U P A 1 C8 C 0.3112(19) 0.2141(14) 0.496(3) 0.109(3) Uani 0.391(9) 1 d D U P A 1 H8 H 0.333858 0.180325 0.464964 0.131 Uiso 0.391(9) 1 calc R U P A 1 C9 C 0.2816(18) 0.2133(14) 0.616(3) 0.109(3) Uani 0.391(9) 1 d D U P A 1 H9 H 0.282609 0.177764 0.662278 0.131 Uiso 0.391(9) 1 calc R U P A 1 C10 C 0.2510(17) 0.2606(13) 0.671(3) 0.105(3) Uani 0.391(9) 1 d D U P A 1 H10 H 0.233632 0.259196 0.755391 0.126 Uiso 0.391(9) 1 calc R U P A 1 C11 C 0.189(2) 0.4607(14) 0.520(3) 0.093(2) Uani 0.391(9) 1 d D U P A 1 H11 H 0.139419 0.453869 0.541898 0.111 Uiso 0.391(9) 1 calc R U P A 1 C12 C 0.187(3) 0.4942(15) 0.392(3) 0.095(2) Uani 0.391(9) 1 d D U P A 1 H12A H 0.235373 0.499241 0.363018 0.114 Uiso 0.391(9) 1 calc R U P A 1 H12B H 0.168350 0.533683 0.410224 0.114 Uiso 0.391(9) 1 calc R U P A 1 C13 C 0.1440(19) 0.4697(12) 0.277(3) 0.097(2) Uani 0.391(9) 1 d D U P A 1 H13 H 0.093525 0.477405 0.293730 0.116 Uiso 0.391(9) 1 calc R U P A 1 C14 C 0.1514(18) 0.4057(12) 0.237(3) 0.097(2) Uani 0.391(9) 1 d D U P A 1 H14 H 0.123077 0.404828 0.157538 0.116 Uiso 0.391(9) 1 calc R U P A 1 C15 C 0.1088(18) 0.3650(14) 0.325(3) 0.101(3) Uani 0.391(9) 1 d D U P A 1 O15 O 0.0673(17) 0.3826(13) 0.404(3) 0.102(5) Uani 0.391(9) 1 d D U P A 1 O16 O 0.1246(13) 0.3083(12) 0.305(3) 0.103(3) Uani 0.391(9) 1 d D U P A 1 C21 C 0.0877(19) 0.2649(16) 0.385(3) 0.111(5) Uani 0.391(9) 1 d D U P A 1 H21A H 0.039854 0.259956 0.354846 0.166 Uiso 0.391(9) 1 calc R U P A 1 H21B H 0.086795 0.278587 0.473085 0.166 Uiso 0.391(9) 1 calc R U P A 1 H21C H 0.112180 0.227413 0.381253 0.166 Uiso 0.391(9) 1 calc R U P A 1 C17 C 0.263(3) 0.3724(17) 0.424(3) 0.096(2) Uani 0.391(9) 1 d D U P A 1 C18 C 0.278(2) 0.3159(14) 0.474(3) 0.100(2) Uani 0.391(9) 1 d D U P A 1 N19 N 0.2120(15) 0.3621(13) 0.617(3) 0.096(2) Uani 0.391(9) 1 d D U P A 1 H19 H 0.187309 0.370266 0.684529 0.115 Uiso 0.391(9) 1 calc R U P A 1 C19 C 0.2465(17) 0.3115(13) 0.598(3) 0.100(2) Uani 0.391(9) 1 d D U P A 1 C20 C 0.221(3) 0.3999(16) 0.514(4) 0.094(2) Uani 0.391(9) 1 d D U P A 1 C1' C 0.0628(12) 0.5703(13) 0.189(2) 0.117(5) Uani 0.609(9) 1 d D U P A 2 H1A' H 0.065823 0.612566 0.200828 0.175 Uiso 0.609(9) 1 calc R U P A 2 H1B' H 0.057836 0.551177 0.271118 0.175 Uiso 0.609(9) 1 calc R U P A 2 H1C' H 0.022238 0.561128 0.136138 0.175 Uiso 0.609(9) 1 calc R U P A 2 C2' C 0.1275(10) 0.5489(10) 0.1253(18) 0.105(3) Uani 0.609(9) 1 d D U P A 2 H2' H 0.147954 0.573640 0.063683 0.126 Uiso 0.609(9) 1 calc R U P A 2 C3' C 0.1618(10) 0.4939(9) 0.1496(19) 0.100(2) Uani 0.609(9) 1 d D U P A 2 N4' N 0.2366(9) 0.4097(8) 0.0673(16) 0.098(2) Uani 0.609(9) 1 d D U P A 2 C16' C 0.3016(11) 0.3942(11) 0.000(2) 0.107(4) Uani 0.609(9) 1 d D U P A 2 H16D H 0.341439 0.412151 0.043250 0.160 Uiso 0.609(9) 1 calc R U P A 2 H16E H 0.299298 0.408331 -0.086927 0.160 Uiso 0.609(9) 1 calc R U P A 2 H16F H 0.307258 0.351710 0.000159 0.160 Uiso 0.609(9) 1 calc R U P A 2 C4' C 0.2269(10) 0.4765(9) 0.0823(18) 0.099(2) Uani 0.609(9) 1 d D U P A 2 H4A' H 0.267385 0.492323 0.128991 0.119 Uiso 0.609(9) 1 calc R U P A 2 H4B' H 0.226757 0.494500 -0.002673 0.119 Uiso 0.609(9) 1 calc R U P A 2 C5' C 0.2273(12) 0.3761(10) 0.190(2) 0.096(2) Uani 0.609(9) 1 d D U P A 2 H5' H 0.226132 0.333762 0.167809 0.116 Uiso 0.609(9) 1 calc R U P A 2 C6' C 0.2878(14) 0.3845(18) 0.290(2) 0.096(2) Uani 0.609(9) 1 d D U P A 2 H6A' H 0.329017 0.362224 0.261043 0.115 Uiso 0.609(9) 1 calc R U P A 2 H6B' H 0.301001 0.426245 0.291513 0.115 Uiso 0.609(9) 1 calc R U P A 2 C7' C 0.3376(12) 0.2647(10) 0.4393(19) 0.106(3) Uani 0.609(9) 1 d D U P A 2 H7' H 0.359995 0.265116 0.359358 0.127 Uiso 0.609(9) 1 calc R U P A 2 C8' C 0.3460(12) 0.2180(10) 0.5213(18) 0.110(3) Uani 0.609(9) 1 d D U P A 2 H8' H 0.370947 0.185161 0.490859 0.132 Uiso 0.609(9) 1 calc R U P A 2 C9' C 0.3207(12) 0.2155(10) 0.6453(19) 0.111(3) Uani 0.609(9) 1 d D U P A 2 H9' H 0.330614 0.182994 0.697941 0.134 Uiso 0.609(9) 1 calc R U P A 2 C10' C 0.2813(11) 0.2612(9) 0.6886(19) 0.106(3) Uani 0.609(9) 1 d D U P A 2 H10' H 0.264085 0.261395 0.772658 0.127 Uiso 0.609(9) 1 calc R U P A 2 C11' C 0.1875(16) 0.4491(9) 0.514(2) 0.092(2) Uani 0.609(9) 1 d D U P A 2 H11' H 0.138005 0.438749 0.533838 0.111 Uiso 0.609(9) 1 calc R U P A 2 C12' C 0.1892(18) 0.4820(10) 0.384(2) 0.095(2) Uani 0.609(9) 1 d D U P A 2 H12C H 0.238370 0.483515 0.355560 0.114 Uiso 0.609(9) 1 calc R U P A 2 H12D H 0.174278 0.522736 0.399363 0.114 Uiso 0.609(9) 1 calc R U P A 2 C13' C 0.1442(13) 0.4574(9) 0.2714(18) 0.097(2) Uani 0.609(9) 1 d D U P A 2 H13' H 0.094068 0.464335 0.292237 0.116 Uiso 0.609(9) 1 calc R U P A 2 C14' C 0.1525(12) 0.3928(9) 0.238(2) 0.096(2) Uani 0.609(9) 1 d D U P A 2 H14' H 0.121527 0.386843 0.163093 0.116 Uiso 0.609(9) 1 calc R U P A 2 C15' C 0.1244(12) 0.3493(10) 0.339(2) 0.101(3) Uani 0.609(9) 1 d D U P A 2 O15' O 0.0769(11) 0.3608(8) 0.412(2) 0.106(4) Uani 0.609(9) 1 d D U P A 2 O16' O 0.1462(8) 0.2947(7) 0.3187(17) 0.103(3) Uani 0.609(9) 1 d D U P A 2 C21' C 0.1238(13) 0.2483(11) 0.410(2) 0.115(5) Uani 0.609(9) 1 d D U P A 2 H21D H 0.118504 0.211139 0.365893 0.173 Uiso 0.609(9) 1 calc R U P A 2 H21E H 0.079142 0.259357 0.448607 0.173 Uiso 0.609(9) 1 calc R U P A 2 H21F H 0.159063 0.244215 0.476832 0.173 Uiso 0.609(9) 1 calc R U P A 2 C17' C 0.2703(18) 0.3656(11) 0.424(2) 0.096(2) Uani 0.609(9) 1 d D U P A 2 C18' C 0.2943(12) 0.3121(10) 0.479(2) 0.100(2) Uani 0.609(9) 1 d D U P A 2 N19' N 0.2302(9) 0.3578(9) 0.6251(18) 0.096(2) Uani 0.609(9) 1 d D U P A 2 H19' H 0.208833 0.366582 0.695842 0.115 Uiso 0.609(9) 1 calc R U P A 2 C19' C 0.2668(11) 0.3078(10) 0.6059(19) 0.100(2) Uani 0.609(9) 1 d D U P A 2 C20' C 0.2310(16) 0.3938(11) 0.517(2) 0.093(2) Uani 0.609(9) 1 d D U P A 2 CA C 0.5613(17) 0.7791(12) 0.972(2) 0.125(4) Uani 0.517(11) 1 d D U P B 1 HAA H 0.610926 0.771673 0.957560 0.187 Uiso 0.517(11) 1 calc R U P B 1 HAB H 0.553118 0.821179 0.976678 0.187 Uiso 0.517(11) 1 calc R U P B 1 HAC H 0.533970 0.762484 0.902750 0.187 Uiso 0.517(11) 1 calc R U P B 1 CB C 0.5391(15) 0.7507(8) 1.097(2) 0.114(3) Uani 0.517(11) 1 d D U P B 1 HBA H 0.578095 0.752290 1.158062 0.137 Uiso 0.517(11) 1 calc R U P B 1 HBB H 0.499169 0.772312 1.133321 0.137 Uiso 0.517(11) 1 calc R U P B 1 CC C 0.5184(12) 0.6877(9) 1.074(3) 0.109(2) Uani 0.517(11) 1 d D U P B 1 HC H 0.557775 0.665194 1.036230 0.131 Uiso 0.517(11) 1 calc R U P B 1 CD C 0.4925(15) 0.6579(12) 1.202(2) 0.109(3) Uani 0.517(11) 1 d D U P B 1 HDA H 0.476580 0.688753 1.260852 0.130 Uiso 0.517(11) 1 calc R U P B 1 HDB H 0.532419 0.637745 1.242177 0.130 Uiso 0.517(11) 1 calc R U P B 1 CE C 0.4304(13) 0.6119(10) 1.183(2) 0.105(2) Uani 0.517(11) 1 d D U P B 1 HE H 0.421114 0.587689 1.259494 0.126 Uiso 0.517(11) 1 calc R U P B 1 CF C 0.4464(16) 0.5740(9) 1.061(2) 0.101(2) Uani 0.517(11) 1 d D U P B 1 HFA H 0.412376 0.541790 1.053603 0.121 Uiso 0.517(11) 1 calc R U P B 1 HFB H 0.493820 0.557143 1.066503 0.121 Uiso 0.517(11) 1 calc R U P B 1 CG C 0.4407(14) 0.6165(10) 0.941(2) 0.0952(19) Uani 0.517(11) 1 d D U P B 1 CT C 0.5029(18) 0.6047(12) 0.853(3) 0.096(2) Uani 0.517(11) 1 d D U P B 1 OT O 0.5435(15) 0.5635(11) 0.864(2) 0.098(4) Uani 0.517(11) 1 d D U P B 1 OU O 0.5126(9) 0.6505(8) 0.7684(18) 0.100(3) Uani 0.517(11) 1 d D U P B 1 CU C 0.5694(13) 0.6446(13) 0.680(3) 0.109(5) Uani 0.517(11) 1 d D U P B 1 HUA H 0.563854 0.608354 0.632584 0.164 Uiso 0.517(11) 1 calc R U P B 1 HUB H 0.613573 0.643663 0.726790 0.164 Uiso 0.517(11) 1 calc R U P B 1 HUC H 0.569302 0.677793 0.622192 0.164 Uiso 0.517(11) 1 calc R U P B 1 NH N 0.3909(10) 0.7036(9) 1.0667(19) 0.103(2) Uani 0.517(11) 1 d D U P B 1 CJ C 0.3343(13) 0.7281(9) 0.980(2) 0.097(2) Uani 0.517(11) 1 d D U P B 1 HJA H 0.356040 0.744438 0.903355 0.117 Uiso 0.517(11) 1 calc R U P B 1 HJB H 0.309564 0.760111 1.024395 0.117 Uiso 0.517(11) 1 calc R U P B 1 CH C 0.4499(11) 0.6825(10) 0.990(2) 0.102(2) Uani 0.517(11) 1 d D U P B 1 HH H 0.455117 0.708579 0.914419 0.122 Uiso 0.517(11) 1 calc R U P B 1 CI C 0.3653(12) 0.6527(9) 1.144(2) 0.104(2) Uani 0.517(11) 1 d D U P B 1 HIA H 0.331224 0.629841 1.094039 0.125 Uiso 0.517(11) 1 calc R U P B 1 HIB H 0.341618 0.667098 1.220885 0.125 Uiso 0.517(11) 1 calc R U P B 1 CK C 0.2816(13) 0.6808(11) 0.943(3) 0.093(3) Uani 0.517(11) 1 d D U P B 1 HKA H 0.243760 0.700016 0.894760 0.111 Uiso 0.517(11) 1 calc R U P B 1 HKB H 0.260676 0.665394 1.021442 0.111 Uiso 0.517(11) 1 calc R U P B 1 CA' C 0.5846(14) 0.7889(13) 1.062(3) 0.127(5) Uani 0.483(11) 1 d D U P B 2 HAA' H 0.607199 0.754775 1.099180 0.190 Uiso 0.483(11) 1 calc R U P B 2 HAB' H 0.580332 0.819696 1.125365 0.190 Uiso 0.483(11) 1 calc R U P B 2 HAC' H 0.612672 0.803147 0.990734 0.190 Uiso 0.483(11) 1 calc R U P B 2 CB' C 0.5119(14) 0.7720(9) 1.014(3) 0.115(3) Uani 0.483(11) 1 d D U P B 2 HBA' H 0.475457 0.786793 1.071967 0.138 Uiso 0.483(11) 1 calc R U P B 2 HBB' H 0.503557 0.788113 0.928707 0.138 Uiso 0.483(11) 1 calc R U P B 2 CC' C 0.5115(12) 0.7053(9) 1.011(3) 0.109(2) Uani 0.483(11) 1 d D U P B 2 HC' H 0.550848 0.689755 0.958825 0.130 Uiso 0.483(11) 1 calc R U P B 2 CD' C 0.5125(15) 0.6790(12) 1.149(3) 0.109(3) Uani 0.483(11) 1 d D U P B 2 HDA' H 0.506469 0.711213 1.210173 0.131 Uiso 0.483(11) 1 calc R U P B 2 HDB' H 0.558764 0.661285 1.164288 0.131 Uiso 0.483(11) 1 calc R U P B 2 CE' C 0.4541(13) 0.6314(11) 1.174(2) 0.105(2) Uani 0.483(11) 1 d D U P B 2 HE' H 0.459003 0.612062 1.258186 0.126 Uiso 0.483(11) 1 calc R U P B 2 CF' C 0.4579(17) 0.5867(10) 1.060(2) 0.101(2) Uani 0.483(11) 1 d D U P B 2 HFA' H 0.423154 0.555425 1.073978 0.121 Uiso 0.483(11) 1 calc R U P B 2 HFB' H 0.504642 0.568498 1.058700 0.121 Uiso 0.483(11) 1 calc R U P B 2 CG' C 0.4435(15) 0.6164(11) 0.928(2) 0.0954(19) Uani 0.483(11) 1 d D U P B 2 CT' C 0.501(2) 0.6060(13) 0.829(3) 0.096(2) Uani 0.483(11) 1 d D U P B 2 OT' O 0.5409(16) 0.5641(12) 0.818(2) 0.097(4) Uani 0.483(11) 1 d D U P B 2 OU' O 0.4969(11) 0.6425(9) 0.7253(18) 0.100(3) Uani 0.483(11) 1 d D U P B 2 CU' C 0.5478(15) 0.6355(14) 0.624(3) 0.109(5) Uani 0.483(11) 1 d D U P B 2 HUA' H 0.594010 0.628613 0.660829 0.163 Uiso 0.483(11) 1 calc R U P B 2 HUB' H 0.549045 0.671003 0.572685 0.163 Uiso 0.483(11) 1 calc R U P B 2 HUC' H 0.534677 0.602296 0.571193 0.163 Uiso 0.483(11) 1 calc R U P B 2 NH' N 0.3783(10) 0.6975(10) 1.0399(19) 0.103(2) Uani 0.483(11) 1 d D U P B 2 CJ' C 0.3081(13) 0.7144(12) 0.997(3) 0.099(2) Uani 0.483(11) 1 d D U P B 2 HJA' H 0.310185 0.755037 0.965846 0.119 Uiso 0.483(11) 1 calc R U P B 2 HJB' H 0.276584 0.714079 1.071367 0.119 Uiso 0.483(11) 1 calc R U P B 2 CH' C 0.4374(11) 0.6853(10) 0.956(2) 0.102(2) Uani 0.483(11) 1 d D U P B 2 HH' H 0.429424 0.705953 0.874009 0.122 Uiso 0.483(11) 1 calc R U P B 2 CI' C 0.3843(13) 0.6682(11) 1.161(2) 0.104(2) Uani 0.483(11) 1 d D U P B 2 HIA' H 0.343844 0.641884 1.172782 0.124 Uiso 0.483(11) 1 calc R U P B 2 HIB' H 0.382826 0.697679 1.229685 0.124 Uiso 0.483(11) 1 calc R U P B 2 CK' C 0.2765(15) 0.6773(12) 0.897(3) 0.094(3) Uani 0.483(11) 1 d D U P B 2 HKA' H 0.228624 0.667503 0.924321 0.112 Uiso 0.483(11) 1 calc R U P B 2 HKB' H 0.271962 0.701872 0.820176 0.112 Uiso 0.483(11) 1 calc R U P B 2 CM C 0.2149(5) 0.4962(5) 0.6185(9) 0.0895(18) Uani 1 1 d . U . . . CL C 0.1945(5) 0.5855(5) 0.7426(9) 0.086(2) Uani 1 1 d . U . . . HL H 0.163971 0.615265 0.770894 0.103 Uiso 1 1 calc R U . . . CO C 0.1706(5) 0.5428(6) 0.6631(11) 0.095(2) Uani 1 1 d . U . . . OO O 0.1018(4) 0.5401(5) 0.6135(8) 0.118(2) Uani 1 1 d . U . . . CV C 0.0528(7) 0.5815(8) 0.6604(18) 0.144(5) Uani 1 1 d . U . . . HVA H 0.068288 0.620930 0.639049 0.216 Uiso 1 1 calc R U . . . HVB H 0.049197 0.577639 0.752403 0.216 Uiso 1 1 calc R U . . . HVC H 0.007079 0.574188 0.622154 0.216 Uiso 1 1 calc R U . . . CN C 0.2838(5) 0.4929(5) 0.6653(9) 0.086(2) Uani 1 1 d . U . . . HN H 0.313377 0.461437 0.642808 0.103 Uiso 1 1 calc R U . . . CP C 0.2658(5) 0.5850(4) 0.7829(9) 0.0788(18) Uani 1 1 d . U . . . CQ C 0.3075(5) 0.5377(4) 0.7465(9) 0.0776(18) Uani 1 1 d . U . . . NQ N 0.3745(4) 0.5464(3) 0.8002(8) 0.0812(18) Uani 1 1 d . U . . . HQ H 0.410363 0.522918 0.792458 0.097 Uiso 1 1 calc R U . . . CR C 0.3734(5) 0.5992(4) 0.8680(10) 0.0836(18) Uani 1 1 d . U . . . CS C 0.3085(5) 0.6253(4) 0.8597(10) 0.0845(18) Uani 1 1 d . U . . . O1W O 0.0997(11) 0.4027(11) 0.8570(15) 0.108(4) Uani 0.391(9) 1 d . . P A 1 O1W' O 0.1590(7) 0.3788(7) 0.8671(10) 0.108(4) Uani 0.609(9) 1 d . . P A 2 O2W O 0.524(3) 0.505(4) 1.442(5) 0.34(3) Uani 0.5 1 d . U P C 1 O3W O 0.647(3) 0.389(2) 1.482(5) 0.281(14) Uani 0.5 1 d . U P D 1 O3W' O 0.573(3) 0.456(2) 1.459(5) 0.281(14) Uani 0.5 1 d . U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.099(9) 0.150(9) 0.080(9) -0.012(9) -0.011(9) -0.017(9) C2 0.093(5) 0.145(6) 0.073(5) -0.008(5) -0.003(5) -0.029(5) C3 0.090(4) 0.139(5) 0.071(4) -0.009(4) 0.001(3) -0.030(4) N4 0.091(4) 0.137(5) 0.066(4) -0.008(4) 0.009(3) -0.035(5) C16 0.095(8) 0.140(10) 0.066(8) -0.008(9) 0.015(7) -0.041(9) C4 0.091(4) 0.138(5) 0.068(4) -0.008(5) 0.005(4) -0.034(5) C5 0.088(3) 0.133(5) 0.068(3) -0.009(4) 0.010(3) -0.033(4) C6 0.087(4) 0.129(5) 0.071(4) -0.010(4) 0.011(4) -0.033(4) C7 0.098(6) 0.131(5) 0.084(4) -0.019(4) 0.003(5) -0.027(5) C8 0.102(6) 0.134(5) 0.091(5) -0.017(4) 0.001(5) -0.025(6) C9 0.102(6) 0.134(5) 0.091(5) -0.015(4) 0.001(5) -0.028(6) C10 0.100(6) 0.131(5) 0.085(4) -0.014(4) 0.003(5) -0.029(5) C11 0.080(4) 0.127(4) 0.072(3) -0.016(4) 0.003(3) -0.022(4) C12 0.081(4) 0.131(5) 0.072(4) -0.015(4) 0.001(4) -0.026(4) C13 0.085(3) 0.135(5) 0.071(3) -0.011(4) 0.003(3) -0.030(4) C14 0.086(3) 0.134(5) 0.070(3) -0.010(4) 0.007(3) -0.033(4) C15 0.090(5) 0.136(5) 0.075(4) -0.010(4) 0.008(4) -0.035(5) O15 0.085(8) 0.141(10) 0.081(7) -0.002(9) 0.021(7) -0.028(8) O16 0.092(6) 0.136(6) 0.080(5) -0.008(5) 0.007(5) -0.034(5) C21 0.099(10) 0.140(10) 0.094(9) -0.004(9) 0.002(9) -0.037(9) C17 0.088(4) 0.126(4) 0.073(3) -0.013(3) 0.007(3) -0.031(4) C18 0.094(5) 0.128(4) 0.078(3) -0.017(3) 0.005(4) -0.030(4) N19 0.090(5) 0.126(4) 0.072(4) -0.016(4) 0.005(4) -0.029(4) C19 0.095(5) 0.128(4) 0.077(4) -0.016(4) 0.005(4) -0.029(4) C20 0.086(4) 0.125(4) 0.071(3) -0.015(3) 0.005(3) -0.028(4) C1' 0.107(8) 0.156(9) 0.088(9) -0.006(9) -0.011(8) -0.013(8) C2' 0.094(5) 0.145(6) 0.075(5) -0.006(5) -0.004(5) -0.028(5) C3' 0.090(4) 0.139(5) 0.071(4) -0.009(4) 0.001(3) -0.031(4) N4' 0.091(4) 0.138(5) 0.066(3) -0.007(4) 0.010(3) -0.036(4) C16' 0.095(7) 0.151(9) 0.074(7) -0.004(8) 0.019(6) -0.040(8) C4' 0.091(4) 0.138(5) 0.068(4) -0.006(4) 0.005(4) -0.034(5) C5' 0.088(3) 0.133(5) 0.068(3) -0.009(4) 0.011(3) -0.034(4) C6' 0.087(4) 0.129(5) 0.071(3) -0.009(4) 0.012(3) -0.033(4) C7' 0.101(5) 0.132(5) 0.084(4) -0.018(4) 0.002(5) -0.027(5) C8' 0.104(6) 0.134(5) 0.092(5) -0.018(4) 0.001(5) -0.025(5) C9' 0.105(6) 0.136(5) 0.093(5) -0.014(4) 0.002(5) -0.026(5) C10' 0.100(6) 0.132(5) 0.085(4) -0.014(4) 0.002(5) -0.028(5) C11' 0.079(4) 0.127(4) 0.071(3) -0.016(4) 0.003(3) -0.022(4) C12' 0.081(4) 0.131(5) 0.073(4) -0.015(4) 0.001(3) -0.026(4) C13' 0.084(3) 0.135(5) 0.071(3) -0.011(4) 0.003(3) -0.030(4) C14' 0.086(3) 0.134(5) 0.069(3) -0.010(4) 0.008(3) -0.033(4) C15' 0.090(4) 0.137(5) 0.075(4) -0.010(4) 0.006(4) -0.035(4) O15' 0.092(6) 0.141(9) 0.085(6) -0.003(7) 0.016(5) -0.040(7) O16' 0.093(6) 0.137(6) 0.080(4) -0.009(5) 0.007(5) -0.037(5) C21' 0.102(9) 0.143(9) 0.100(8) -0.006(8) 0.005(8) -0.041(8) C17' 0.088(4) 0.126(4) 0.072(3) -0.013(3) 0.007(3) -0.031(4) C18' 0.094(5) 0.127(4) 0.078(3) -0.018(3) 0.005(4) -0.030(4) N19' 0.090(5) 0.126(4) 0.072(4) -0.017(4) 0.005(4) -0.030(4) C19' 0.095(5) 0.128(4) 0.077(3) -0.016(3) 0.004(4) -0.030(4) C20' 0.085(4) 0.125(4) 0.070(3) -0.015(3) 0.004(3) -0.028(4) CA 0.133(8) 0.108(8) 0.133(8) -0.021(8) -0.024(8) 0.000(8) CB 0.125(5) 0.098(5) 0.121(5) -0.021(5) -0.026(5) 0.006(5) CC 0.119(4) 0.092(4) 0.115(5) -0.022(4) -0.023(4) 0.009(4) CD 0.119(5) 0.093(5) 0.114(5) -0.022(5) -0.021(5) 0.007(4) CE 0.112(4) 0.092(4) 0.111(4) -0.018(4) -0.021(4) 0.012(4) CF 0.105(4) 0.088(4) 0.108(4) -0.016(4) -0.022(4) 0.013(4) CG 0.098(3) 0.083(3) 0.105(4) -0.019(3) -0.017(3) 0.016(3) CT 0.094(4) 0.084(4) 0.108(5) -0.019(4) -0.013(4) 0.013(4) OT 0.094(6) 0.086(6) 0.113(9) -0.024(8) -0.013(8) 0.024(6) OU 0.096(5) 0.095(5) 0.110(6) -0.016(5) -0.009(5) 0.010(4) CU 0.099(9) 0.111(8) 0.118(10) -0.019(9) 0.002(8) -0.001(8) NH 0.111(4) 0.090(4) 0.107(4) -0.025(4) -0.017(4) 0.017(3) CJ 0.104(5) 0.085(4) 0.102(5) -0.027(4) -0.012(4) 0.022(4) CH 0.109(4) 0.087(4) 0.109(4) -0.023(4) -0.019(4) 0.015(3) CI 0.113(5) 0.093(4) 0.107(4) -0.023(4) -0.018(4) 0.014(4) CK 0.098(5) 0.083(4) 0.097(5) -0.026(5) -0.012(5) 0.027(4) CA' 0.135(9) 0.113(9) 0.133(9) -0.019(9) -0.025(9) -0.003(8) CB' 0.124(6) 0.099(5) 0.121(6) -0.020(5) -0.023(5) 0.007(5) CC' 0.118(4) 0.092(4) 0.115(5) -0.022(4) -0.022(4) 0.010(4) CD' 0.120(5) 0.093(5) 0.115(5) -0.022(4) -0.021(5) 0.006(4) CE' 0.112(4) 0.093(4) 0.111(4) -0.019(4) -0.021(4) 0.010(4) CF' 0.104(4) 0.089(4) 0.108(4) -0.016(4) -0.022(4) 0.013(4) CG' 0.098(3) 0.083(3) 0.105(4) -0.018(3) -0.017(3) 0.016(3) CT' 0.094(4) 0.085(4) 0.109(5) -0.019(4) -0.013(4) 0.013(4) OT' 0.100(7) 0.081(6) 0.109(9) -0.031(8) -0.008(8) 0.021(6) OU' 0.097(5) 0.093(5) 0.108(6) -0.019(5) -0.007(5) 0.009(4) CU' 0.100(9) 0.111(9) 0.116(10) -0.015(9) 0.000(8) 0.008(8) NH' 0.111(4) 0.091(4) 0.106(4) -0.025(4) -0.017(4) 0.018(4) CJ' 0.106(5) 0.088(4) 0.104(5) -0.028(4) -0.013(4) 0.023(4) CH' 0.109(4) 0.087(4) 0.109(4) -0.022(4) -0.019(4) 0.015(3) CI' 0.112(5) 0.092(4) 0.106(4) -0.021(4) -0.019(4) 0.014(4) CK' 0.100(5) 0.084(4) 0.098(5) -0.026(5) -0.012(5) 0.026(4) CM 0.073(3) 0.122(4) 0.074(3) -0.016(3) 0.001(3) -0.002(3) CL 0.070(4) 0.112(5) 0.077(4) -0.009(4) -0.002(3) 0.028(4) CO 0.065(3) 0.133(5) 0.085(4) -0.009(4) -0.006(3) 0.018(4) OO 0.074(4) 0.172(6) 0.109(5) -0.022(5) -0.005(3) 0.020(4) CV 0.076(6) 0.189(11) 0.168(10) -0.012(10) -0.014(7) 0.033(7) CN 0.073(4) 0.105(4) 0.079(4) -0.018(4) -0.005(4) 0.010(4) CP 0.073(3) 0.090(4) 0.074(3) -0.008(3) -0.006(3) 0.024(3) CQ 0.069(3) 0.090(4) 0.074(4) -0.013(3) -0.009(3) 0.018(3) NQ 0.069(3) 0.086(4) 0.088(4) -0.015(3) -0.014(3) 0.023(3) CR 0.083(3) 0.077(3) 0.091(4) -0.012(3) -0.010(3) 0.023(3) CS 0.086(4) 0.082(3) 0.086(4) -0.017(3) -0.006(3) 0.030(3) O1W 0.095(6) 0.177(11) 0.051(4) -0.015(6) 0.003(5) -0.008(7) O1W' 0.095(6) 0.177(11) 0.051(4) -0.015(6) 0.003(5) -0.008(7) O2W 0.34(3) 0.34(3) 0.33(3) -0.003(15) 0.005(14) 0.003(15) O3W 0.294(16) 0.279(16) 0.271(16) -0.004(10) -0.010(10) 0.001(10) O3W' 0.294(16) 0.279(16) 0.271(16) -0.004(10) -0.010(10) 0.001(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? H1A C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C3 C2 C1 124(2) . . ? C3 C2 H2 117.9 . . ? C1 C2 H2 117.9 . . ? C2 C3 C4 120(2) . . ? C2 C3 C13 122(2) . . ? C4 C3 C13 116(2) . . ? C16 N4 C5 114(2) . . ? C16 N4 C4 108(2) . . ? C5 N4 C4 114.8(19) . . ? N4 C16 H16A 109.5 . . ? N4 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? N4 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C3 C4 N4 110(2) . . ? C3 C4 H4A 109.6 . . ? N4 C4 H4A 109.6 . . ? C3 C4 H4B 109.6 . . ? N4 C4 H4B 109.6 . . ? H4A C4 H4B 108.2 . . ? N4 C5 C14 106.5(19) . . ? N4 C5 C6 111(2) . . ? C14 C5 C6 114(2) . . ? N4 C5 H5 108.5 . . ? C14 C5 H5 108.5 . . ? C6 C5 H5 108.5 . . ? C17 C6 C5 116(3) . . ? C17 C6 H6A 108.4 . . ? C5 C6 H6A 108.4 . . ? C17 C6 H6B 108.4 . . ? C5 C6 H6B 108.4 . . ? H6A C6 H6B 107.5 . . ? C8 C7 C18 120(2) . . ? C8 C7 H7 120.2 . . ? C18 C7 H7 120.2 . . ? C7 C8 C9 120(3) . . ? C7 C8 H8 119.8 . . ? C9 C8 H8 119.8 . . ? C10 C9 C8 124(3) . . ? C10 C9 H9 118.1 . . ? C8 C9 H9 118.1 . . ? C9 C10 C19 117(2) . . ? C9 C10 H10 121.6 . . ? C19 C10 H10 121.6 . . ? CM C11 C20 115(3) . . ? CM C11 C12 112(2) . . ? C20 C11 C12 115(2) . . ? CM C11 H11 104.4 . . ? C20 C11 H11 104.4 . . ? C12 C11 H11 104.4 . . ? C11 C12 C13 121(2) . . ? C11 C12 H12A 107.1 . . ? C13 C12 H12A 107.1 . . ? C11 C12 H12B 107.1 . . ? C13 C12 H12B 107.1 . . ? H12A C12 H12B 106.8 . . ? C14 C13 C12 121(2) . . ? C14 C13 C3 106.1(18) . . ? C12 C13 C3 106(2) . . ? C14 C13 H13 107.9 . . ? C12 C13 H13 107.9 . . ? C3 C13 H13 107.9 . . ? C13 C14 C15 111.1(19) . . ? C13 C14 C5 116(2) . . ? C15 C14 C5 121(2) . . ? C13 C14 H14 101.8 . . ? C15 C14 H14 101.8 . . ? C5 C14 H14 101.8 . . ? O15 C15 O16 125(2) . . ? O15 C15 C14 124(3) . . ? O16 C15 C14 112(2) . . ? C15 O16 C21 117(2) . . ? O16 C21 H21A 109.5 . . ? O16 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? O16 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C20 C17 C18 106.5(18) . . ? C20 C17 C6 132(3) . . ? C18 C17 C6 121(2) . . ? C7 C18 C17 135(2) . . ? C7 C18 C19 117(2) . . ? C17 C18 C19 107.8(19) . . ? C19 N19 C20 110.7(19) . . ? C19 N19 H19 124.7 . . ? C20 N19 H19 124.7 . . ? N19 C19 C10 131(2) . . ? N19 C19 C18 106.3(19) . . ? C10 C19 C18 122(2) . . ? C17 C20 N19 108.6(19) . . ? C17 C20 C11 132(2) . . ? N19 C20 C11 119(2) . . ? C2' C1' H1A' 109.5 . . ? C2' C1' H1B' 109.5 . . ? H1A' C1' H1B' 109.5 . . ? C2' C1' H1C' 109.5 . . ? H1A' C1' H1C' 109.5 . . ? H1B' C1' H1C' 109.5 . . ? C3' C2' C1' 125.8(19) . . ? C3' C2' H2' 117.1 . . ? C1' C2' H2' 117.1 . . ? C2' C3' C4' 122.0(16) . . ? C2' C3' C13' 120.8(16) . . ? C4' C3' C13' 115.3(16) . . ? C16' N4' C5' 112.7(15) . . ? C16' N4' C4' 112.9(14) . . ? C5' N4' C4' 113.5(13) . . ? N4' C16' H16D 109.5 . . ? N4' C16' H16E 109.5 . . ? H16D C16' H16E 109.5 . . ? N4' C16' H16F 109.5 . . ? H16D C16' H16F 109.5 . . ? H16E C16' H16F 109.5 . . ? C3' C4' N4' 114.5(14) . . ? C3' C4' H4A' 108.6 . . ? N4' C4' H4A' 108.6 . . ? C3' C4' H4B' 108.6 . . ? N4' C4' H4B' 108.6 . . ? H4A' C4' H4B' 107.6 . . ? N4' C5' C14' 105.1(14) . . ? N4' C5' C6' 115.0(14) . . ? C14' C5' C6' 115.2(15) . . ? N4' C5' H5' 107.0 . . ? C14' C5' H5' 107.0 . . ? C6' C5' H5' 107.0 . . ? C17' C6' C5' 115.2(18) . . ? C17' C6' H6A' 108.5 . . ? C5' C6' H6A' 108.5 . . ? C17' C6' H6B' 108.5 . . ? C5' C6' H6B' 108.5 . . ? H6A' C6' H6B' 107.5 . . ? C8' C7' C18' 118.1(17) . . ? C8' C7' H7' 120.9 . . ? C18' C7' H7' 120.9 . . ? C7' C8' C9' 125(2) . . ? C7' C8' H8' 117.3 . . ? C9' C8' H8' 117.3 . . ? C10' C9' C8' 118(2) . . ? C10' C9' H9' 120.9 . . ? C8' C9' H9' 120.9 . . ? C9' C10' C19' 118.8(18) . . ? C9' C10' H10' 120.6 . . ? C19' C10' H10' 120.6 . . ? C20' C11' C12' 114.0(16) . . ? C20' C11' CM 111(2) . . ? C12' C11' CM 105.6(15) . . ? C20' C11' H11' 108.6 . . ? C12' C11' H11' 108.6 . . ? CM C11' H11' 108.6 . . ? C11' C12' C13' 118.6(16) . . ? C11' C12' H12C 107.7 . . ? C13' C12' H12C 107.7 . . ? C11' C12' H12D 107.7 . . ? C13' C12' H12D 107.7 . . ? H12C C12' H12D 107.1 . . ? C14' C13' C3' 107.7(13) . . ? C14' C13' C12' 117.7(17) . . ? C3' C13' C12' 108.2(14) . . ? C14' C13' H13' 107.6 . . ? C3' C13' H13' 107.6 . . ? C12' C13' H13' 107.6 . . ? C13' C14' C15' 115.2(14) . . ? C13' C14' C5' 113.8(14) . . ? C15' C14' C5' 112.5(16) . . ? C13' C14' H14' 104.6 . . ? C15' C14' H14' 104.6 . . ? C5' C14' H14' 104.6 . . ? O15' C15' O16' 122.5(17) . . ? O15' C15' C14' 123.5(19) . . ? O16' C15' C14' 112.4(15) . . ? C15' O16' C21' 117.9(15) . . ? O16' C21' H21D 109.5 . . ? O16' C21' H21E 109.5 . . ? H21D C21' H21E 109.5 . . ? O16' C21' H21F 109.5 . . ? H21D C21' H21F 109.5 . . ? H21E C21' H21F 109.5 . . ? C20' C17' C18' 106.8(14) . . ? C20' C17' C6' 129.9(19) . . ? C18' C17' C6' 123.3(18) . . ? C17' C18' C7' 136.1(16) . . ? C17' C18' C19' 108.4(15) . . ? C7' C18' C19' 115.5(17) . . ? C19' N19' C20' 111.5(14) . . ? C19' N19' H19' 124.3 . . ? C20' N19' H19' 124.3 . . ? N19' C19' C10' 130.5(16) . . ? N19' C19' C18' 105.6(16) . . ? C10' C19' C18' 123.8(18) . . ? C17' C20' N19' 107.7(15) . . ? C17' C20' C11' 132.1(16) . . ? N19' C20' C11' 119.9(15) . . ? CB CA HAA 109.5 . . ? CB CA HAB 109.5 . . ? HAA CA HAB 109.5 . . ? CB CA HAC 109.5 . . ? HAA CA HAC 109.5 . . ? HAB CA HAC 109.5 . . ? CC CB CA 110.0(19) . . ? CC CB HBA 109.7 . . ? CA CB HBA 109.7 . . ? CC CB HBB 109.7 . . ? CA CB HBB 109.7 . . ? HBA CB HBB 108.2 . . ? CB CC CD 111(2) . . ? CB CC CH 112.0(19) . . ? CD CC CH 100.9(17) . . ? CB CC HC 110.9 . . ? CD CC HC 110.9 . . ? CH CC HC 110.9 . . ? CC CD CE 113.8(16) . . ? CC CD HDA 108.8 . . ? CE CD HDA 108.8 . . ? CC CD HDB 108.8 . . ? CE CD HDB 108.8 . . ? HDA CD HDB 107.7 . . ? CF CE CD 108.7(19) . . ? CF CE CI 105.2(17) . . ? CD CE CI 103.0(17) . . ? CF CE HE 113.1 . . ? CD CE HE 113.1 . . ? CI CE HE 113.1 . . ? CE CF CG 107.2(15) . . ? CE CF HFA 110.3 . . ? CG CF HFA 110.3 . . ? CE CF HFB 110.3 . . ? CG CF HFB 110.3 . . ? HFA CF HFB 108.5 . . ? CT CG CR 107.0(19) . . ? CT CG CF 108.8(17) . . ? CR CG CF 107.2(19) . . ? CT CG CH 105.9(18) . . ? CR CG CH 119.2(17) . . ? CF CG CH 108.3(16) . . ? OT CT OU 124(2) . . ? OT CT CG 124(2) . . ? OU CT CG 111.2(16) . . ? CT OU CU 116.4(17) . . ? OU CU HUA 109.5 . . ? OU CU HUB 109.5 . . ? HUA CU HUB 109.5 . . ? OU CU HUC 109.5 . . ? HUA CU HUC 109.5 . . ? HUB CU HUC 109.5 . . ? CH NH CI 107.2(16) . . ? CH NH CJ 109.6(17) . . ? CI NH CJ 112.1(17) . . ? NH CJ CK 111.3(17) . . ? NH CJ HJA 109.4 . . ? CK CJ HJA 109.4 . . ? NH CJ HJB 109.4 . . ? CK CJ HJB 109.4 . . ? HJA CJ HJB 108.0 . . ? NH CH CC 107.2(16) . . ? NH CH CG 113.6(17) . . ? CC CH CG 109.8(16) . . ? NH CH HH 108.7 . . ? CC CH HH 108.7 . . ? CG CH HH 108.7 . . ? NH CI CE 109.6(17) . . ? NH CI HIA 109.8 . . ? CE CI HIA 109.8 . . ? NH CI HIB 109.8 . . ? CE CI HIB 109.8 . . ? HIA CI HIB 108.2 . . ? CJ CK CS 119(2) . . ? CJ CK HKA 107.6 . . ? CS CK HKA 107.6 . . ? CJ CK HKB 107.6 . . ? CS CK HKB 107.6 . . ? HKA CK HKB 107.0 . . ? CB' CA' HAA' 109.5 . . ? CB' CA' HAB' 109.5 . . ? HAA' CA' HAB' 109.5 . . ? CB' CA' HAC' 109.5 . . ? HAA' CA' HAC' 109.5 . . ? HAB' CA' HAC' 109.5 . . ? CC' CB' CA' 105.4(19) . . ? CC' CB' HBA' 110.7 . . ? CA' CB' HBA' 110.7 . . ? CC' CB' HBB' 110.7 . . ? CA' CB' HBB' 110.7 . . ? HBA' CB' HBB' 108.8 . . ? CB' CC' CD' 111(2) . . ? CB' CC' CH' 107.4(18) . . ? CD' CC' CH' 103.7(19) . . ? CB' CC' HC' 111.4 . . ? CD' CC' HC' 111.4 . . ? CH' CC' HC' 111.4 . . ? CC' CD' CE' 114.2(17) . . ? CC' CD' HDA' 108.7 . . ? CE' CD' HDA' 108.7 . . ? CC' CD' HDB' 108.7 . . ? CE' CD' HDB' 108.7 . . ? HDA' CD' HDB' 107.6 . . ? CF' CE' CD' 106.6(19) . . ? CF' CE' CI' 108.6(18) . . ? CD' CE' CI' 102.4(18) . . ? CF' CE' HE' 112.8 . . ? CD' CE' HE' 112.8 . . ? CI' CE' HE' 112.8 . . ? CE' CF' CG' 112.9(16) . . ? CE' CF' HFA' 109.0 . . ? CG' CF' HFA' 109.0 . . ? CE' CF' HFB' 109.0 . . ? CG' CF' HFB' 109.0 . . ? HFA' CF' HFB' 107.8 . . ? CR CG' CT' 108(2) . . ? CR CG' CF' 114(2) . . ? CT' CG' CF' 114.2(19) . . ? CR CG' CH' 105.3(18) . . ? CT' CG' CH' 109.2(18) . . ? CF' CG' CH' 105.6(16) . . ? OT' CT' OU' 116(2) . . ? OT' CT' CG' 129(2) . . ? OU' CT' CG' 113.6(18) . . ? CT' OU' CU' 118.3(18) . . ? OU' CU' HUA' 109.5 . . ? OU' CU' HUB' 109.5 . . ? HUA' CU' HUB' 109.5 . . ? OU' CU' HUC' 109.5 . . ? HUA' CU' HUC' 109.5 . . ? HUB' CU' HUC' 109.5 . . ? CI' NH' CH' 112.6(16) . . ? CI' NH' CJ' 118(2) . . ? CH' NH' CJ' 124.9(18) . . ? NH' CJ' CK' 116.1(19) . . ? NH' CJ' HJA' 108.3 . . ? CK' CJ' HJA' 108.3 . . ? NH' CJ' HJB' 108.3 . . ? CK' CJ' HJB' 108.3 . . ? HJA' CJ' HJB' 107.4 . . ? NH' CH' CC' 114.2(18) . . ? NH' CH' CG' 110.9(17) . . ? CC' CH' CG' 106.5(16) . . ? NH' CH' HH' 108.4 . . ? CC' CH' HH' 108.4 . . ? CG' CH' HH' 108.4 . . ? NH' CI' CE' 112.7(19) . . ? NH' CI' HIA' 109.1 . . ? CE' CI' HIA' 109.1 . . ? NH' CI' HIB' 109.1 . . ? CE' CI' HIB' 109.1 . . ? HIA' CI' HIB' 107.8 . . ? CS CK' CJ' 121(2) . . ? CS CK' HKA' 107.2 . . ? CJ' CK' HKA' 107.2 . . ? CS CK' HKB' 107.2 . . ? CJ' CK' HKB' 107.2 . . ? HKA' CK' HKB' 106.8 . . ? C11 CM CN 123.5(19) . . ? C11 CM CO 117.8(18) . . ? CN CM CO 118.4(9) . . ? CN CM C11' 120.2(13) . . ? CO CM C11' 121.4(12) . . ? CO CL CP 119.8(9) . . ? CO CL HL 120.1 . . ? CP CL HL 120.1 . . ? CL CO OO 124.7(9) . . ? CL CO CM 122.1(9) . . ? OO CO CM 113.1(10) . . ? CO OO CV 117.1(10) . . ? OO CV HVA 109.5 . . ? OO CV HVB 109.5 . . ? HVA CV HVB 109.5 . . ? OO CV HVC 109.5 . . ? HVA CV HVC 109.5 . . ? HVB CV HVC 109.5 . . ? CM CN CQ 118.3(9) . . ? CM CN HN 120.8 . . ? CQ CN HN 120.8 . . ? CQ CP CL 118.0(9) . . ? CQ CP CS 108.6(8) . . ? CL CP CS 133.4(8) . . ? CP CQ CN 123.1(8) . . ? CP CQ NQ 107.3(8) . . ? CN CQ NQ 129.5(8) . . ? CR NQ CQ 108.2(7) . . ? CR NQ HQ 125.9 . . ? CQ NQ HQ 125.9 . . ? CS CR NQ 110.6(9) . . ? CS CR CG' 134.7(12) . . ? NQ CR CG' 114.6(11) . . ? CS CR CG 131.9(11) . . ? NQ CR CG 117.5(10) . . ? CR CS CK' 138.2(14) . . ? CR CS CP 105.3(8) . . ? CK' CS CP 116.4(12) . . ? CR CS CK 126.0(12) . . ? CP CS CK 127.6(11) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.47(3) . ? C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? C2 C3 1.39(3) . ? C2 H2 0.9300 . ? C3 C4 1.44(2) . ? C3 C13 1.54(2) . ? N4 C16 1.45(2) . ? N4 C5 1.51(2) . ? N4 C4 1.52(2) . ? C16 H16A 0.9600 . ? C16 H16B 0.9600 . ? C16 H16C 0.9600 . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C5 C14 1.53(2) . ? C5 C6 1.56(2) . ? C5 H5 0.9800 . ? C6 C17 1.49(2) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C7 C8 1.36(3) . ? C7 C18 1.40(3) . ? C7 H7 0.9300 . ? C8 C9 1.36(3) . ? C8 H8 0.9300 . ? C9 C10 1.34(3) . ? C9 H9 0.9300 . ? C10 C19 1.38(2) . ? C10 H10 0.9300 . ? C11 CM 1.38(4) . ? C11 C20 1.49(2) . ? C11 C12 1.53(2) . ? C11 H11 0.9800 . ? C12 C13 1.54(2) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C13 C14 1.50(2) . ? C13 H13 0.9800 . ? C14 C15 1.52(2) . ? C14 H14 0.9800 . ? C15 O15 1.20(2) . ? C15 O16 1.32(2) . ? O16 C21 1.46(2) . ? C21 H21A 0.9600 . ? C21 H21B 0.9600 . ? C21 H21C 0.9600 . ? C17 C20 1.36(2) . ? C17 C18 1.40(2) . ? C18 C19 1.42(2) . ? N19 C19 1.32(2) . ? N19 C20 1.38(2) . ? N19 H19 0.8600 . ? C1' C2' 1.46(2) . ? C1' H1A' 0.9600 . ? C1' H1B' 0.9600 . ? C1' H1C' 0.9600 . ? C2' C3' 1.42(2) . ? C2' H2' 0.9300 . ? C3' C4' 1.46(2) . ? C3' C13' 1.542(19) . ? N4' C16' 1.449(18) . ? N4' C5' 1.491(18) . ? N4' C4' 1.52(2) . ? C16' H16D 0.9600 . ? C16' H16E 0.9600 . ? C16' H16F 0.9600 . ? C4' H4A' 0.9700 . ? C4' H4B' 0.9700 . ? C5' C14' 1.538(19) . ? C5' C6' 1.550(19) . ? C5' H5' 0.9800 . ? C6' C17' 1.494(17) . ? C6' H6A' 0.9700 . ? C6' H6B' 0.9700 . ? C7' C8' 1.36(2) . ? C7' C18' 1.40(2) . ? C7' H7' 0.9300 . ? C8' C9' 1.37(2) . ? C8' H8' 0.9300 . ? C9' C10' 1.34(2) . ? C9' H9' 0.9300 . ? C10' C19' 1.38(2) . ? C10' H10' 0.9300 . ? C11' C20' 1.49(2) . ? C11' C12' 1.538(19) . ? C11' CM 1.60(2) . ? C11' H11' 0.9800 . ? C12' C13' 1.544(18) . ? C12' H12C 0.9700 . ? C12' H12D 0.9700 . ? C13' C14' 1.50(2) . ? C13' H13' 0.9800 . ? C14' C15' 1.53(2) . ? C14' H14' 0.9800 . ? C15' O15' 1.198(18) . ? C15' O16' 1.31(2) . ? O16' C21' 1.473(19) . ? C21' H21D 0.9600 . ? C21' H21E 0.9600 . ? C21' H21F 0.9600 . ? C17' C20' 1.366(18) . ? C17' C18' 1.40(2) . ? C18' C19' 1.420(19) . ? N19' C19' 1.33(2) . ? N19' C20' 1.385(18) . ? N19' H19' 0.8600 . ? CA CB 1.502(13) . ? CA HAA 0.9600 . ? CA HAB 0.9600 . ? CA HAC 0.9600 . ? CB CC 1.487(12) . ? CB HBA 0.9700 . ? CB HBB 0.9700 . ? CC CD 1.56(3) . ? CC CH 1.56(3) . ? CC HC 0.9800 . ? CD CE 1.57(3) . ? CD HDA 0.9700 . ? CD HDB 0.9700 . ? CE CF 1.55(2) . ? CE CI 1.58(2) . ? CE HE 0.9800 . ? CF CG 1.57(2) . ? CF HFA 0.9700 . ? CF HFB 0.9700 . ? CG CT 1.51(2) . ? CG CR 1.53(3) . ? CG CH 1.57(2) . ? CT OT 1.207(18) . ? CT OU 1.36(2) . ? OU CU 1.41(2) . ? CU HUA 0.9600 . ? CU HUB 0.9600 . ? CU HUC 0.9600 . ? NH CH 1.45(2) . ? NH CI 1.48(2) . ? NH CJ 1.50(2) . ? CJ CK 1.50(2) . ? CJ HJA 0.9700 . ? CJ HJB 0.9700 . ? CH HH 0.9800 . ? CI HIA 0.9700 . ? CI HIB 0.9700 . ? CK CS 1.60(2) . ? CK HKA 0.9700 . ? CK HKB 0.9700 . ? CA' CB' 1.500(13) . ? CA' HAA' 0.9600 . ? CA' HAB' 0.9600 . ? CA' HAC' 0.9600 . ? CB' CC' 1.499(13) . ? CB' HBA' 0.9700 . ? CB' HBB' 0.9700 . ? CC' CD' 1.55(3) . ? CC' CH' 1.57(3) . ? CC' HC' 0.9800 . ? CD' CE' 1.56(3) . ? CD' HDA' 0.9700 . ? CD' HDB' 0.9700 . ? CE' CF' 1.55(2) . ? CE' CI' 1.56(2) . ? CE' HE' 0.9800 . ? CF' CG' 1.55(2) . ? CF' HFA' 0.9700 . ? CF' HFB' 0.9700 . ? CG' CR 1.50(3) . ? CG' CT' 1.51(2) . ? CG' CH' 1.58(2) . ? CT' OT' 1.205(18) . ? CT' OU' 1.35(2) . ? OU' CU' 1.43(2) . ? CU' HUA' 0.9600 . ? CU' HUB' 0.9600 . ? CU' HUC' 0.9600 . ? NH' CI' 1.43(2) . ? NH' CH' 1.44(2) . ? NH' CJ' 1.44(2) . ? CJ' CK' 1.46(2) . ? CJ' HJA' 0.9700 . ? CJ' HJB' 0.9700 . ? CH' HH' 0.9800 . ? CI' HIA' 0.9700 . ? CI' HIB' 0.9700 . ? CK' CS 1.37(3) . ? CK' HKA' 0.9700 . ? CK' HKB' 0.9700 . ? CM CN 1.385(13) . ? CM CO 1.415(15) . ? CL CO 1.342(15) . ? CL CP 1.403(13) . ? CL HL 0.9300 . ? CO OO 1.392(12) . ? OO CV 1.396(16) . ? CV HVA 0.9600 . ? CV HVB 0.9600 . ? CV HVC 0.9600 . ? CN CQ 1.386(13) . ? CN HN 0.9300 . ? CP CQ 1.372(12) . ? CP CS 1.450(14) . ? CQ NQ 1.391(11) . ? NQ CR 1.381(12) . ? NQ HQ 0.8600 . ? CR CS 1.356(13) . ? O2W O2W 0.94(12) 2_665 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C11 H11 O15 0.98 2.54 3.13(6) 118.6 . yes N19 H19 O1W 0.86 2.54 3.39(3) 170.1 . yes C11' H11' O15' 0.98 2.45 3.06(3) 120.4 . yes N19' H19' O1W' 0.86 2.03 2.88(2) 174.4 . yes CE' HE' O3W' 0.98 2.65 3.58(6) 158.9 2_665 yes NQ HQ OT' 0.86 2.18 2.96(2) 150.4 2_665 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C2 C3 C4 -168(3) . . . . ? C1 C2 C3 C13 31(5) . . . . ? C2 C3 C4 N4 -108(3) . . . . ? C13 C3 C4 N4 54(3) . . . . ? C16 N4 C4 C3 178(2) . . . . ? C5 N4 C4 C3 -54(3) . . . . ? C16 N4 C5 C14 178(2) . . . . ? C4 N4 C5 C14 53(3) . . . . ? C16 N4 C5 C6 54(3) . . . . ? C4 N4 C5 C6 -71(3) . . . . ? N4 C5 C6 C17 156(3) . . . . ? C14 C5 C6 C17 36(4) . . . . ? C18 C7 C8 C9 4(5) . . . . ? C7 C8 C9 C10 -3(5) . . . . ? C8 C9 C10 C19 4(5) . . . . ? CM C11 C12 C13 -165(3) . . . . ? C20 C11 C12 C13 61(5) . . . . ? C11 C12 C13 C14 -48(5) . . . . ? C11 C12 C13 C3 -168(3) . . . . ? C2 C3 C13 C14 107(4) . . . . ? C4 C3 C13 C14 -54(3) . . . . ? C2 C3 C13 C12 -124(3) . . . . ? C4 C3 C13 C12 75(3) . . . . ? C12 C13 C14 C15 79(4) . . . . ? C3 C13 C14 C15 -161(3) . . . . ? C12 C13 C14 C5 -64(3) . . . . ? C3 C13 C14 C5 56(3) . . . . ? N4 C5 C14 C13 -57(3) . . . . ? C6 C5 C14 C13 66(3) . . . . ? N4 C5 C14 C15 164(3) . . . . ? C6 C5 C14 C15 -73(4) . . . . ? C13 C14 C15 O15 10(5) . . . . ? C5 C14 C15 O15 150(4) . . . . ? C13 C14 C15 O16 -169(3) . . . . ? C5 C14 C15 O16 -28(4) . . . . ? O15 C15 O16 C21 1(5) . . . . ? C14 C15 O16 C21 179(3) . . . . ? C5 C6 C17 C20 -71(7) . . . . ? C5 C6 C17 C18 101(5) . . . . ? C8 C7 C18 C17 -175(5) . . . . ? C8 C7 C18 C19 -6(5) . . . . ? C20 C17 C18 C7 168(4) . . . . ? C6 C17 C18 C7 -6(8) . . . . ? C20 C17 C18 C19 -2(5) . . . . ? C6 C17 C18 C19 -176(4) . . . . ? C20 N19 C19 C10 -178(4) . . . . ? C20 N19 C19 C18 -2(4) . . . . ? C9 C10 C19 N19 170(4) . . . . ? C9 C10 C19 C18 -6(5) . . . . ? C7 C18 C19 N19 -170(3) . . . . ? C17 C18 C19 N19 2(4) . . . . ? C7 C18 C19 C10 7(5) . . . . ? C17 C18 C19 C10 179(4) . . . . ? C18 C17 C20 N19 1(6) . . . . ? C6 C17 C20 N19 174(4) . . . . ? C18 C17 C20 C11 178(5) . . . . ? C6 C17 C20 C11 -9(10) . . . . ? C19 N19 C20 C17 0(5) . . . . ? C19 N19 C20 C11 -177(4) . . . . ? CM C11 C20 C17 -115(6) . . . . ? C12 C11 C20 C17 18(8) . . . . ? CM C11 C20 N19 61(6) . . . . ? C12 C11 C20 N19 -166(4) . . . . ? C1' C2' C3' C4' -179.4(19) . . . . ? C1' C2' C3' C13' -16(3) . . . . ? C2' C3' C4' N4' -151.5(19) . . . . ? C13' C3' C4' N4' 44(2) . . . . ? C16' N4' C4' C3' -180.0(16) . . . . ? C5' N4' C4' C3' -50(2) . . . . ? C16' N4' C5' C14' -173.4(16) . . . . ? C4' N4' C5' C14' 56.6(18) . . . . ? C16' N4' C5' C6' 59(2) . . . . ? C4' N4' C5' C6' -71(2) . . . . ? N4' C5' C6' C17' 164(2) . . . . ? C14' C5' C6' C17' 41(3) . . . . ? C18' C7' C8' C9' -6(3) . . . . ? C7' C8' C9' C10' 4(3) . . . . ? C8' C9' C10' C19' 1(3) . . . . ? C20' C11' C12' C13' 77(3) . . . . ? CM C11' C12' C13' -160(2) . . . . ? C2' C3' C13' C14' 148(2) . . . . ? C4' C3' C13' C14' -47(2) . . . . ? C2' C3' C13' C12' -84(2) . . . . ? C4' C3' C13' C12' 81(2) . . . . ? C11' C12' C13' C14' -51(3) . . . . ? C11' C12' C13' C3' -174(2) . . . . ? C3' C13' C14' C15' -169.4(19) . . . . ? C12' C13' C14' C15' 68(2) . . . . ? C3' C13' C14' C5' 59(2) . . . . ? C12' C13' C14' C5' -64(2) . . . . ? N4' C5' C14' C13' -64.0(19) . . . . ? C6' C5' C14' C13' 64(2) . . . . ? N4' C5' C14' C15' 162.6(18) . . . . ? C6' C5' C14' C15' -70(2) . . . . ? C13' C14' C15' O15' 28(3) . . . . ? C5' C14' C15' O15' 161(2) . . . . ? C13' C14' C15' O16' -166.3(19) . . . . ? C5' C14' C15' O16' -34(3) . . . . ? O15' C15' O16' C21' -15(3) . . . . ? C14' C15' O16' C21' 179.1(18) . . . . ? C5' C6' C17' C20' -78(4) . . . . ? C5' C6' C17' C18' 103(4) . . . . ? C20' C17' C18' C7' -177(3) . . . . ? C6' C17' C18' C7' 2(5) . . . . ? C20' C17' C18' C19' 2(3) . . . . ? C6' C17' C18' C19' -179(2) . . . . ? C8' C7' C18' C17' -177(3) . . . . ? C8' C7' C18' C19' 4(3) . . . . ? C20' N19' C19' C10' 178(2) . . . . ? C20' N19' C19' C18' 1(3) . . . . ? C9' C10' C19' N19' -179(2) . . . . ? C9' C10' C19' C18' -3(3) . . . . ? C17' C18' C19' N19' -2(3) . . . . ? C7' C18' C19' N19' 177.5(19) . . . . ? C17' C18' C19' C10' -178(2) . . . . ? C7' C18' C19' C10' 1(3) . . . . ? C18' C17' C20' N19' -1(4) . . . . ? C6' C17' C20' N19' 180(3) . . . . ? C18' C17' C20' C11' -174(3) . . . . ? C6' C17' C20' C11' 6(6) . . . . ? C19' N19' C20' C17' 0(3) . . . . ? C19' N19' C20' C11' 174(2) . . . . ? C12' C11' C20' C17' -3(5) . . . . ? CM C11' C20' C17' -122(4) . . . . ? C12' C11' C20' N19' -176(2) . . . . ? CM C11' C20' N19' 65(3) . . . . ? CA CB CC CD -178(2) . . . . ? CA CB CC CH -66(3) . . . . ? CB CC CD CE 145(2) . . . . ? CH CC CD CE 26(2) . . . . ? CC CD CE CF 42(2) . . . . ? CC CD CE CI -69(2) . . . . ? CD CE CF CG -68(2) . . . . ? CI CE CF CG 42(2) . . . . ? CE CF CG CT 136(2) . . . . ? CE CF CG CR -108.9(19) . . . . ? CE CF CG CH 21(2) . . . . ? CR CG CT OT -106(4) . . . . ? CF CG CT OT 10(4) . . . . ? CH CG CT OT 126(3) . . . . ? CR CG CT OU 82(3) . . . . ? CF CG CT OU -162(2) . . . . ? CH CG CT OU -46(3) . . . . ? OT CT OU CU 8(4) . . . . ? CG CT OU CU 180(2) . . . . ? CH NH CJ CK 90(2) . . . . ? CI NH CJ CK -28(3) . . . . ? CI NH CH CC -86(2) . . . . ? CJ NH CH CC 152.3(17) . . . . ? CI NH CH CG 36(2) . . . . ? CJ NH CH CG -86(2) . . . . ? CB CC CH NH -70(2) . . . . ? CD CC CH NH 48(2) . . . . ? CB CC CH CG 167(2) . . . . ? CD CC CH CG -75.4(19) . . . . ? CT CG CH NH 174.4(18) . . . . ? CR CG CH NH 54(2) . . . . ? CF CG CH NH -69(2) . . . . ? CT CG CH CC -66(2) . . . . ? CR CG CH CC 173.8(18) . . . . ? CF CG CH CC 51(2) . . . . ? CH NH CI CE 35(2) . . . . ? CJ NH CI CE 154.9(17) . . . . ? CF CE CI NH -79(2) . . . . ? CD CE CI NH 34(2) . . . . ? NH CJ CK CS -63(3) . . . . ? CA' CB' CC' CD' 70(3) . . . . ? CA' CB' CC' CH' -178(2) . . . . ? CB' CC' CD' CE' 129(2) . . . . ? CH' CC' CD' CE' 14(2) . . . . ? CC' CD' CE' CF' 49(2) . . . . ? CC' CD' CE' CI' -65(2) . . . . ? CD' CE' CF' CG' -61(3) . . . . ? CI' CE' CF' CG' 49(3) . . . . ? CE' CF' CG' CR -109(2) . . . . ? CE' CF' CG' CT' 126(3) . . . . ? CE' CF' CG' CH' 6(3) . . . . ? CR CG' CT' OT' -99(4) . . . . ? CF' CG' CT' OT' 29(5) . . . . ? CH' CG' CT' OT' 147(4) . . . . ? CR CG' CT' OU' 67(3) . . . . ? CF' CG' CT' OU' -166(3) . . . . ? CH' CG' CT' OU' -48(3) . . . . ? OT' CT' OU' CU' -11(5) . . . . ? CG' CT' OU' CU' -178(2) . . . . ? CI' NH' CJ' CK' -104(3) . . . . ? CH' NH' CJ' CK' 49(4) . . . . ? CI' NH' CH' CC' -60(3) . . . . ? CJ' NH' CH' CC' 145(2) . . . . ? CI' NH' CH' CG' 60(3) . . . . ? CJ' NH' CH' CG' -95(3) . . . . ? CB' CC' CH' NH' -68(3) . . . . ? CD' CC' CH' NH' 50(2) . . . . ? CB' CC' CH' CG' 169(2) . . . . ? CD' CC' CH' CG' -73(2) . . . . ? CR CG' CH' NH' 58(2) . . . . ? CT' CG' CH' NH' 174(2) . . . . ? CF' CG' CH' NH' -63(2) . . . . ? CR CG' CH' CC' -176.8(18) . . . . ? CT' CG' CH' CC' -61(3) . . . . ? CF' CG' CH' CC' 62(2) . . . . ? CH' NH' CI' CE' 1(3) . . . . ? CJ' NH' CI' CE' 158.0(19) . . . . ? CF' CE' CI' NH' -56(3) . . . . ? CD' CE' CI' NH' 57(3) . . . . ? NH' CJ' CK' CS 9(4) . . . . ? C20 C11 CM CN 32(4) . . . . ? C12 C11 CM CN -102(3) . . . . ? C20 C11 CM CO -155(3) . . . . ? C12 C11 CM CO 71(3) . . . . ? C20' C11' CM CN 22(2) . . . . ? C12' C11' CM CN -102.3(18) . . . . ? C20' C11' CM CO -159.7(15) . . . . ? C12' C11' CM CO 76(2) . . . . ? CP CL CO OO -177.6(11) . . . . ? CP CL CO CM 0.7(17) . . . . ? C11 CM CO CL -169(2) . . . . ? CN CM CO CL 4.1(17) . . . . ? C11' CM CO CL -174.4(14) . . . . ? C11 CM CO OO 10(2) . . . . ? CN CM CO OO -177.5(10) . . . . ? C11' CM CO OO 4.0(18) . . . . ? CL CO OO CV -6.8(19) . . . . ? CM CO OO CV 174.9(12) . . . . ? C11 CM CN CQ 168(2) . . . . ? CO CM CN CQ -4.4(15) . . . . ? C11' CM CN CQ 174.1(13) . . . . ? CO CL CP CQ -4.8(15) . . . . ? CO CL CP CS 175.6(11) . . . . ? CL CP CQ CN 4.5(15) . . . . ? CS CP CQ CN -175.9(10) . . . . ? CL CP CQ NQ -178.5(9) . . . . ? CS CP CQ NQ 1.2(12) . . . . ? CM CN CQ CP 0.2(16) . . . . ? CM CN CQ NQ -176.2(11) . . . . ? CP CQ NQ CR -0.5(12) . . . . ? CN CQ NQ CR 176.3(11) . . . . ? CQ NQ CR CS -0.4(12) . . . . ? CQ NQ CR CG' -177.5(13) . . . . ? CQ NQ CR CG 177.0(13) . . . . ? CT' CG' CR CS -131.9(17) . . . . ? CF' CG' CR CS 100(2) . . . . ? CH' CG' CR CS -15(3) . . . . ? CT' CG' CR NQ 44.3(19) . . . . ? CF' CG' CR NQ -83.8(17) . . . . ? CH' CG' CR NQ 160.9(13) . . . . ? CT CG CR CS -139.0(15) . . . . ? CF CG CR CS 104.4(18) . . . . ? CH CG CR CS -19(3) . . . . ? CT CG CR NQ 44.3(19) . . . . ? CF CG CR NQ -72.3(17) . . . . ? CH CG CR NQ 164.3(15) . . . . ? NQ CR CS CK' -175(2) . . . . ? CG' CR CS CK' 2(3) . . . . ? NQ CR CS CP 1.1(12) . . . . ? CG' CR CS CP 177.4(17) . . . . ? CG CR CS CP -175.8(15) . . . . ? NQ CR CS CK 169.2(15) . . . . ? CG CR CS CK -8(3) . . . . ? CJ' CK' CS CR -19(4) . . . . ? CJ' CK' CS CP 166(2) . . . . ? CQ CP CS CR -1.4(12) . . . . ? CL CP CS CR 178.2(11) . . . . ? CQ CP CS CK' 175.5(17) . . . . ? CL CP CS CK' -5(2) . . . . ? CQ CP CS CK -169.3(15) . . . . ? CL CP CS CK 10(2) . . . . ? CJ CK CS CR 34(3) . . . . ? CJ CK CS CP -160.5(16) . . . . ?