#------------------------------------------------------------------------------ #$Date: 2021-06-26 03:30:20 +0300 (Sat, 26 Jun 2021) $ #$Revision: 266702 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/88/4518838.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4518838 loop_ _publ_author_name 'Barman, Debasish' 'Gopikrishna, Peddaboodi' 'Iyer, Parameswar Krishnan' _publ_section_title ; Stimuli-Responsive Trimorphs and Charge-Transfer Complexes of a Twisted Molecular Donor. ; _journal_name_full 'Langmuir : the ACS journal of surfaces and colloids' _journal_paper_doi 10.1021/acs.langmuir.1c01172 _journal_year 2021 _chemical_formula_sum 'C34 H22' _chemical_formula_weight 430.52 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 10.7705(19) _cell_length_b 17.623(3) _cell_length_c 23.643(4) _cell_measurement_reflns_used 3470 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 28.417 _cell_measurement_theta_min 2.311 _cell_volume 4487.6(13) _computing_cell_refinement 'Bruker SMART' _computing_data_collection 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0688 _diffrn_reflns_av_unetI/netI 0.0344 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 70396 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.417 _diffrn_reflns_theta_min 2.311 _exptl_absorpt_coefficient_mu 0.072 _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.274 _exptl_crystal_description 'hexagonal blocks' _exptl_crystal_F_000 1808.0 _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.24 _exptl_crystal_size_min 0.16 _refine_diff_density_max 0.132 _refine_diff_density_min -0.189 _refine_diff_density_rms 0.037 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.878 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 307 _refine_ls_number_reflns 5645 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.878 _refine_ls_R_factor_all 0.0917 _refine_ls_R_factor_gt 0.0499 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.6519P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1338 _refine_ls_wR_factor_ref 0.1612 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3470 _reflns_number_total 5610 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file la1c01172_si_010.cif _cod_data_source_block TAH-Red _cod_database_code 4518838 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL GK-red_0m_a.res in Pbca GK-red_0m_a.res created by SHELXL-2016/6 at 16:50:49 on 02-Aug-2018 CELL 0.71073 10.7705 17.6230 23.6430 90.000 90.000 90.000 ZERR 12.000 0.0019 0.0029 0.0037 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H UNIT 264 240 REM Old TITL GK-red_0m in Pbca REM SHELXT solution in Pbca REM R1 0.163, Rweak 0.008, Alpha 0.023, Orientation as input REM Formula found by SHELXT: C34 L.S. 20 ACTA BOND $H FMAP 2 PLAN 2 TEMP 0.000 WGHT 0.100000 0.651920 FVAR 0.39893 C001 1 0.527085 0.311742 0.642696 11.00000 0.04588 0.04153 = 0.04127 0.00277 -0.00513 -0.00757 C002 1 0.651830 0.565154 0.536666 11.00000 0.04107 0.03907 = 0.05043 0.00111 0.00463 -0.00370 C003 1 0.538313 0.233323 0.665441 11.00000 0.04914 0.04164 = 0.04651 0.00350 -0.00653 -0.01014 C004 1 0.645609 0.429063 0.524604 11.00000 0.04534 0.03709 = 0.05245 -0.00222 0.00870 -0.00253 AFIX 43 H004 2 0.653896 0.387190 0.500964 11.00000 -1.20000 AFIX 0 C005 1 0.419695 0.345492 0.672844 11.00000 0.04530 0.04614 = 0.03852 0.00246 -0.00273 -0.00906 C006 1 0.734177 0.672947 0.474538 11.00000 0.04899 0.03349 = 0.04857 0.00078 -0.00492 -0.00389 C007 1 0.662112 0.500999 0.502549 11.00000 0.04817 0.04414 = 0.04459 0.00327 0.00796 -0.00422 AFIX 43 H007 2 0.680365 0.506664 0.464336 11.00000 -1.20000 AFIX 0 C008 1 0.845767 0.644055 0.444193 11.00000 0.04704 0.03853 = 0.04994 0.00135 -0.00258 -0.00775 C009 1 0.616857 0.417870 0.581421 11.00000 0.04074 0.04273 = 0.04783 0.00345 0.00432 -0.00489 C00A 1 0.714581 0.750536 0.451899 11.00000 0.05560 0.03443 = 0.04866 -0.00028 -0.00980 -0.00682 C00B 1 0.375052 0.291905 0.712263 11.00000 0.05137 0.05231 = 0.04139 0.00492 -0.00131 -0.00972 C00C 1 0.803253 0.766017 0.410161 11.00000 0.06098 0.03987 = 0.04951 0.00350 -0.01009 -0.01078 C00D 1 0.604262 0.340117 0.603053 11.00000 0.04988 0.04116 = 0.05142 0.00207 0.00308 -0.00449 AFIX 43 H00D 2 0.657921 0.304926 0.586877 11.00000 -1.20000 AFIX 0 C00E 1 0.450762 0.222988 0.708226 11.00000 0.05377 0.04622 = 0.04579 0.00645 -0.00659 -0.01071 C00F 1 0.660014 0.642521 0.514223 11.00000 0.04976 0.03812 = 0.05589 -0.00018 0.00316 -0.00041 AFIX 43 H00F 2 0.604098 0.676500 0.530251 11.00000 -1.20000 AFIX 0 C00G 1 0.622578 0.553897 0.593555 11.00000 0.05792 0.04330 = 0.05176 -0.00454 0.00666 -0.00812 AFIX 43 H00G 2 0.612875 0.595844 0.617009 11.00000 -1.20000 AFIX 0 C00H 1 0.886489 0.700306 0.405893 11.00000 0.05536 0.04470 = 0.04875 0.00199 -0.00359 -0.01153 C00I 1 0.607681 0.482148 0.615901 11.00000 0.06048 0.05022 = 0.04112 0.00112 0.00657 -0.01140 AFIX 43 H00I 2 0.591366 0.476451 0.654294 11.00000 -1.20000 AFIX 0 C00J 1 0.356010 0.413560 0.666514 11.00000 0.05654 0.05192 = 0.05009 0.00847 0.00115 -0.00205 AFIX 43 H00J 2 0.382528 0.449338 0.640244 11.00000 -1.20000 AFIX 0 C00K 1 0.914061 0.577531 0.449281 11.00000 0.04910 0.04282 = 0.06521 0.00628 0.00168 -0.00324 AFIX 43 H00K 2 0.889891 0.540271 0.474867 11.00000 -1.20000 AFIX 0 C00L 1 0.621943 0.802945 0.464152 11.00000 0.06481 0.03829 = 0.06514 -0.00273 -0.00902 -0.00073 AFIX 43 H00L 2 0.562581 0.792777 0.491694 11.00000 -1.20000 AFIX 0 C00M 1 0.620159 0.175201 0.651977 11.00000 0.05800 0.04753 = 0.06320 0.00133 -0.00270 -0.00371 AFIX 43 H00M 2 0.678473 0.181435 0.623342 11.00000 -1.20000 AFIX 0 C00N 1 0.800463 0.834177 0.380489 11.00000 0.08403 0.04813 = 0.05545 0.00930 -0.01270 -0.01840 AFIX 43 H00N 2 0.859020 0.844851 0.352698 11.00000 -1.20000 AFIX 0 C00O 1 0.271641 0.306730 0.744964 11.00000 0.06622 0.06943 = 0.05419 0.01363 0.01131 -0.00700 AFIX 43 H00O 2 0.243305 0.271178 0.771009 11.00000 -1.20000 AFIX 0 C00P 1 0.620062 0.870366 0.434538 11.00000 0.07966 0.03727 = 0.07388 -0.00147 -0.02238 0.00250 AFIX 43 H00P 2 0.558753 0.906048 0.442274 11.00000 -1.20000 AFIX 0 C00Q 1 0.252505 0.427535 0.699796 11.00000 0.06270 0.06353 = 0.06410 0.00566 0.00686 0.00845 AFIX 43 H00Q 2 0.210350 0.473295 0.695910 11.00000 -1.20000 AFIX 0 C00R 1 0.444353 0.155144 0.738152 11.00000 0.07396 0.05756 = 0.05887 0.01722 -0.00066 -0.01246 AFIX 43 H00R 2 0.385828 0.148390 0.766631 11.00000 -1.20000 AFIX 0 C00S 1 0.990377 0.688887 0.372412 11.00000 0.06458 0.06395 = 0.06136 0.00938 0.00882 -0.01417 AFIX 43 H00S 2 1.015761 0.725905 0.346874 11.00000 -1.20000 AFIX 0 C00T 1 0.707710 0.885579 0.393673 11.00000 0.09877 0.03673 = 0.06694 0.00846 -0.03103 -0.00568 AFIX 43 H00T 2 0.704496 0.931572 0.374442 11.00000 -1.20000 AFIX 0 C00U 1 0.526979 0.098053 0.724561 11.00000 0.08505 0.04979 = 0.07710 0.02156 -0.00889 -0.00665 AFIX 43 H00U 2 0.524424 0.052466 0.744342 11.00000 -1.20000 AFIX 0 C00V 1 0.613474 0.107761 0.681929 11.00000 0.06946 0.04749 = 0.08113 0.00681 -0.00991 0.00007 AFIX 43 H00V 2 0.667890 0.068476 0.673251 11.00000 -1.20000 AFIX 0 C00W 1 1.018793 0.567102 0.415830 11.00000 0.05339 0.05709 = 0.08072 0.00261 0.00544 0.00255 AFIX 43 H00W 2 1.064710 0.522655 0.419311 11.00000 -1.20000 AFIX 0 C00X 1 1.055729 0.621838 0.377450 11.00000 0.05656 0.07510 = 0.07763 0.00144 0.01521 -0.00432 AFIX 43 H00X 2 1.125084 0.613423 0.354874 11.00000 -1.20000 AFIX 0 C00Y 1 0.211057 0.375094 0.738385 11.00000 0.06411 0.07791 = 0.06201 0.00582 0.01750 0.00174 AFIX 43 H00Y 2 0.141491 0.385784 0.760282 11.00000 -1.20000 AFIX 0 HKLF 4 REM GK-red_0m_a.res in Pbca REM R1 = 0.0499 for 3470 Fo > 4sig(Fo) and 0.0917 for all 5610 data REM 307 parameters refined using 0 restraints END WGHT 0.0620 0.3732 REM Highest difference peak 0.132, deepest hole -0.189, 1-sigma level 0.037 Q1 1 0.7185 0.2872 0.5827 11.00000 0.05 0.13 Q2 1 0.5388 0.2657 0.6507 11.00000 0.05 0.12 ; _shelx_res_checksum 69730 _shelx_hkl_file ; 1 0 0 -0.60 0.60 -1 0 0 0.10 0.20 2 0 0 6.50 2.50 -2 0 0 8.60 1.10 -3 0 0 -0.10 1.10 3 0 0 4.40 3.70 -3 0 0 -0.10 0.70 -3 0 0 -0.10 0.60 -4 0 0 4700.73 141.19 4 0 0 4616.64 144.69 -4 0 0 4523.75 141.39 -4 0 0 4890.01 142.99 -5 0 0 0.80 1.90 -5 0 0 0.00 0.90 5 0 0 1.90 3.70 -5 0 0 0.20 0.80 -6 0 0 3.90 1.70 6 0 0 -0.70 4.00 -6 0 0 0.80 1.80 -6 0 0 1.20 1.40 7 0 0 -4.20 4.50 -7 0 0 -2.20 1.40 -7 0 0 -0.70 2.30 -7 0 0 -0.20 1.10 8 0 0 669.93 32.20 -8 0 0 735.63 27.70 -8 0 0 687.03 26.80 -8 0 0 684.13 29.00 -9 0 0 0.60 3.20 -9 0 0 -0.40 2.20 -9 0 0 -3.00 1.90 9 0 0 7.90 7.40 10 0 0 6.90 6.80 -10 0 0 17.60 5.90 -10 0 0 18.20 4.50 -10 0 0 13.00 4.00 11 0 0 -4.00 6.70 -11 0 0 0.40 3.60 -11 0 0 1.80 3.40 -11 0 0 -1.10 2.60 -12 0 0 59.89 10.30 -12 0 0 51.49 8.60 12 0 0 74.59 13.30 -12 0 0 55.39 8.70 -13 0 0 2.40 5.50 -13 0 0 7.50 4.40 -14 0 0 -2.40 4.80 -14 0 0 6.40 4.60 0 -1 0 0.20 0.10 0 -1 0 0.60 0.30 0 1 0 0.60 0.20 0 1 0 0.20 0.20 -1 -1 0 -0.10 0.20 1 -1 0 0.20 0.40 -1 1 0 0.30 0.30 -1 1 0 -0.10 0.20 1 1 0 -1.70 0.70 -2 -1 0 4.40 0.90 2 -1 0 7.50 2.10 -2 1 0 4.50 1.30 -2 1 0 5.20 0.90 2 1 0 3.90 2.40 -3 -1 0 1.10 0.80 3 -1 0 6.40 3.50 -3 -1 0 -0.60 1.30 -3 -1 0 0.00 0.50 -3 1 0 -0.50 0.70 -3 1 0 -1.00 1.10 -3 1 0 -0.70 0.60 3 1 0 2.30 3.80 -4 -1 0 55.99 5.30 4 -1 0 57.49 6.70 -4 -1 0 46.70 4.10 -4 -1 0 48.00 3.40 -4 1 0 53.79 4.40 -4 1 0 43.00 4.00 -4 1 0 35.00 4.20 4 1 0 51.99 6.80 -5 -1 0 0.50 1.50 -5 -1 0 -0.70 1.10 5 -1 0 -2.90 3.30 -5 -1 0 -0.80 0.90 -5 1 0 2.60 1.70 -5 1 0 0.30 1.20 -5 1 0 0.70 1.00 5 1 0 6.20 4.30 -5 1 0 0.30 1.60 6 -1 0 55.09 8.40 -6 -1 0 34.80 4.20 -6 -1 0 33.50 5.20 -6 -1 0 36.20 4.30 -6 1 0 39.70 4.60 -6 1 0 44.10 4.40 -6 1 0 43.50 5.70 -6 1 0 41.10 4.80 6 1 0 58.29 8.90 -7 -1 0 0.30 2.30 -7 -1 0 0.60 1.30 7 -1 0 -5.90 5.50 -7 -1 0 0.80 2.00 -7 1 0 1.10 2.90 -7 1 0 -1.90 1.10 7 1 0 3.30 6.00 -7 1 0 0.90 1.70 -8 -1 0 11.90 3.90 -8 -1 0 16.20 3.70 -8 -1 0 20.30 4.10 8 -1 0 25.20 8.10 -8 1 0 15.40 4.40 -8 1 0 22.30 4.10 8 1 0 24.90 7.90 -8 1 0 24.80 4.30 -9 -1 0 -1.00 2.60 -9 -1 0 -0.20 2.80 -9 -1 0 -0.80 2.20 9 -1 0 -4.10 7.10 -9 1 0 1.00 2.40 9 1 0 -1.70 6.80 -9 1 0 -0.70 2.10 -9 1 0 -0.50 3.00 -10 -1 0 1.60 2.70 -10 -1 0 6.40 4.30 10 -1 0 -6.40 5.30 -10 -1 0 6.30 3.40 -10 1 0 7.60 3.60 10 1 0 10.00 7.10 -10 1 0 3.70 3.20 -10 1 0 -1.60 4.10 -11 -1 0 3.30 3.40 11 -1 0 10.30 8.00 -11 -1 0 -0.10 3.30 -11 -1 0 1.50 4.40 -11 1 0 -1.20 4.10 11 1 0 14.80 7.10 -11 1 0 -1.80 2.70 -11 1 0 0.90 3.00 -12 -1 0 160.18 16.60 -12 -1 0 133.09 13.20 -12 -1 0 145.29 13.90 -12 1 0 137.59 13.30 12 1 0 160.68 19.60 -12 1 0 162.68 14.60 -12 1 0 140.19 15.20 -13 -1 0 -0.50 3.30 -13 -1 0 4.70 5.50 -13 1 0 -0.80 4.30 -13 1 0 5.40 5.10 -14 -1 0 3.40 4.00 14 -1 0 -2.10 5.40 -14 -1 0 -0.70 5.50 -14 1 0 3.10 5.30 -14 1 0 -1.10 4.90 0 -2 0 4128.99 120.99 0 2 0 4013.50 121.49 1 -2 0 0.20 0.30 -1 -2 0 0.30 0.40 -1 2 0 0.00 0.40 1 2 0 0.60 1.10 -2 -2 0 33.50 2.20 -2 -2 0 37.80 2.10 2 -2 0 37.20 2.80 -2 2 0 31.00 2.30 -2 2 0 27.70 2.80 2 2 0 32.70 4.60 -2 2 0 31.70 2.30 -3 -2 0 0.70 1.20 3 -2 0 -2.00 2.20 -3 -2 0 -0.90 0.60 -3 -2 0 -0.40 0.60 -3 2 0 -1.20 0.90 -3 2 0 -0.60 0.60 -3 2 0 -1.60 1.10 3 2 0 6.00 3.90 -3 2 0 0.00 0.90 -4 -2 0 1601.04 49.10 -4 -2 0 1574.94 50.39 4 -2 0 1588.64 51.29 -4 -2 0 1518.25 48.40 -4 2 0 1540.55 49.30 -4 2 0 1502.45 49.00 4 2 0 1544.15 53.09 -4 2 0 1548.95 49.30 -4 2 0 1536.05 50.29 5 -2 0 3.60 3.60 -5 -2 0 -0.40 1.60 -5 -2 0 -0.40 0.80 -5 -2 0 -1.30 0.80 -5 2 0 0.40 1.80 -5 2 0 -0.50 1.10 5 2 0 0.10 4.20 -5 2 0 -0.40 1.70 -5 2 0 0.10 1.20 -6 -2 0 100.69 6.50 6 -2 0 133.59 11.90 -6 -2 0 83.89 8.10 -6 -2 0 105.09 6.40 6 2 0 92.19 10.80 -6 2 0 95.69 6.60 -6 2 0 102.29 9.00 -6 2 0 110.89 6.60 -6 2 0 93.29 6.40 7 -2 0 -1.90 4.80 -7 -2 0 -1.10 2.10 -7 -2 0 5.70 2.30 -7 -2 0 1.00 1.70 -7 2 0 -2.90 2.30 -7 2 0 0.30 1.90 -7 2 0 -0.30 1.50 -7 2 0 1.80 2.10 7 2 0 -2.30 5.00 -8 -2 0 24.70 5.10 8 -2 0 54.29 10.30 -8 -2 0 27.80 4.60 -8 -2 0 37.30 5.20 -8 2 0 36.40 6.50 8 2 0 34.50 8.90 -8 2 0 21.10 4.20 -8 2 0 26.80 4.90 -9 -2 0 3.00 3.50 -9 -2 0 -1.20 1.60 9 -2 0 5.60 7.20 -9 -2 0 -1.60 1.90 -9 2 0 2.30 2.00 -9 2 0 -1.50 2.70 -9 2 0 -2.10 2.00 9 2 0 -3.30 6.10 10 -2 0 2.60 6.60 -10 -2 0 13.30 4.00 -10 -2 0 14.70 4.40 -10 -2 0 19.60 5.70 -10 2 0 6.20 4.40 10 2 0 19.70 7.20 -10 2 0 5.90 3.20 -10 2 0 18.20 4.90 -11 -2 0 5.60 3.30 -11 -2 0 2.40 3.90 -11 -2 0 2.70 3.40 11 -2 0 -3.20 6.80 -11 2 0 -2.00 4.40 -11 2 0 0.20 3.20 11 2 0 -11.80 6.30 -11 2 0 0.40 3.30 -12 -2 0 75.99 10.10 -12 -2 0 58.49 10.30 -12 -2 0 70.19 9.80 -12 2 0 51.99 8.60 -12 2 0 64.19 10.30 12 2 0 72.49 13.30 -12 2 0 84.19 10.20 -13 -2 0 1.60 3.90 13 -2 0 -6.00 5.40 -13 -2 0 1.00 5.10 -13 2 0 -6.60 4.40 -13 2 0 -5.00 3.80 13 2 0 9.00 7.80 -14 -2 0 3.20 5.20 -14 -2 0 2.30 5.60 14 -2 0 0.60 6.40 -14 2 0 -2.70 5.20 -14 2 0 -1.70 4.60 0 -3 0 1.50 0.60 0 3 0 1.00 0.90 -1 -3 0 0.40 0.60 -1 -3 0 0.50 0.40 1 -3 0 0.10 0.30 -1 3 0 0.00 0.40 -1 3 0 -0.50 0.60 1 3 0 0.90 1.50 -2 -3 0 11.10 1.80 -2 -3 0 15.70 1.70 2 -3 0 18.80 2.50 -2 -3 0 11.80 1.50 2 -3 0 14.50 1.70 2 -3 0 18.60 2.10 -2 3 0 14.70 2.20 -2 3 0 13.90 1.80 -2 3 0 12.90 1.80 -2 3 0 15.20 2.70 2 3 0 11.80 3.90 -3 -3 0 0.40 1.00 3 -3 0 0.50 1.70 -3 -3 0 -0.20 0.70 3 -3 0 0.10 1.30 -3 -3 0 0.20 0.60 -3 3 0 0.90 1.70 -3 3 0 0.60 1.10 -3 3 0 0.20 0.90 3 3 0 -3.00 3.10 -3 3 0 0.60 0.80 -4 -3 0 27.20 3.80 -4 -3 0 23.00 2.80 4 -3 0 29.20 4.40 -4 -3 0 23.00 2.70 -4 3 0 21.20 3.00 4 3 0 24.30 5.50 -4 3 0 23.10 3.40 -4 3 0 30.70 3.30 -4 3 0 21.70 3.50 -5 -3 0 1.60 1.50 5 -3 0 -4.00 3.10 -5 -3 0 1.10 1.20 -5 -3 0 2.30 1.30 5 3 0 -1.60 3.60 -5 3 0 0.60 1.50 -5 3 0 -0.80 1.20 -5 3 0 -0.80 1.80 -5 3 0 0.60 1.20 -6 -3 0 95.39 6.20 -6 -3 0 117.89 7.10 6 -3 0 110.29 10.80 -6 -3 0 108.19 8.00 -6 3 0 110.99 9.40 -6 3 0 98.99 6.80 6 3 0 130.49 12.80 -6 3 0 117.39 7.20 -6 3 0 112.09 7.20 7 -3 0 5.70 5.80 -7 -3 0 0.50 2.30 -7 -3 0 1.30 1.60 -7 -3 0 -0.10 1.40 -7 3 0 -0.30 1.80 -7 3 0 -3.40 2.00 -7 3 0 -5.10 1.90 -7 3 0 0.60 1.60 7 3 0 6.30 6.20 8 -3 0 311.07 19.60 -8 -3 0 338.37 17.60 -8 -3 0 335.57 15.20 -8 -3 0 323.87 15.50 -8 3 0 318.07 17.30 8 3 0 307.57 20.50 -8 3 0 343.77 15.90 -8 3 0 300.27 15.30 -9 -3 0 0.40 2.90 9 -3 0 9.30 7.80 -9 -3 0 0.30 1.90 -9 -3 0 2.80 2.30 9 3 0 11.10 6.70 -9 3 0 1.20 2.30 -9 3 0 -4.00 2.20 -9 3 0 -1.90 2.00 -10 -3 0 1.90 3.00 -10 -3 0 11.90 3.90 10 -3 0 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0 3.80 4.20 -11 -5 0 1.40 2.90 -11 5 0 2.80 3.90 11 5 0 8.90 7.80 -11 5 0 -2.70 3.80 -11 5 0 0.90 2.90 12 -5 0 13.00 5.60 -12 -5 0 2.50 4.80 -12 -5 0 6.90 4.90 -12 -5 0 -0.50 3.50 -12 5 0 0.70 4.00 12 5 0 -0.20 7.10 -12 5 0 1.80 4.80 -12 5 0 4.70 3.80 -13 -5 0 -2.90 3.40 13 -5 0 -2.60 4.60 -13 -5 0 1.10 5.20 -13 5 0 0.20 4.60 -13 5 0 2.40 5.50 -14 -5 0 5.70 5.10 -14 5 0 -0.20 4.90 0 -6 0 23.30 2.60 0 -6 0 18.70 2.20 0 -6 0 20.70 2.30 0 6 0 19.40 2.50 0 6 0 16.00 2.80 0 6 0 16.60 3.20 -1 -6 0 -0.20 0.70 -1 -6 0 -1.50 0.50 -1 -6 0 0.50 1.00 1 -6 0 -1.70 0.80 1 -6 0 0.40 0.70 1 -6 0 0.70 0.90 -1 6 0 0.40 1.00 1 6 0 0.70 1.90 -1 6 0 -1.90 1.30 1 6 0 0.90 1.50 -1 6 0 -0.10 0.90 -1 6 0 -0.10 0.80 2 -6 0 8.90 1.60 -2 -6 0 6.40 1.60 2 -6 0 8.90 2.00 -2 -6 0 6.90 1.50 -2 -6 0 10.30 1.80 2 -6 0 9.40 1.80 -2 6 0 9.10 2.00 2 6 0 7.60 2.10 -2 6 0 9.10 1.90 -2 6 0 9.00 1.90 2 6 0 9.60 3.60 -2 6 0 4.10 2.30 -3 -6 0 -0.60 0.80 3 -6 0 -0.10 0.70 -3 -6 0 -0.10 1.30 -3 -6 0 1.60 1.50 -3 -6 0 -0.40 0.90 3 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3.50 -8 -6 0 2.40 2.10 8 -6 0 7.90 6.10 -8 -6 0 6.20 2.60 -8 -6 0 1.10 3.40 -8 6 0 5.30 4.10 -8 6 0 0.70 2.60 -8 6 0 5.90 2.60 -8 6 0 0.50 3.20 8 6 0 6.10 6.70 9 -6 0 -2.30 2.70 -9 -6 0 -1.00 2.00 -9 -6 0 0.00 2.20 -9 -6 0 -3.90 3.00 -9 6 0 -1.40 2.20 9 6 0 8.60 6.30 -9 6 0 -0.90 3.40 -9 6 0 3.40 2.40 -10 -6 0 4.30 4.70 -10 -6 0 3.40 3.10 -10 -6 0 15.50 4.50 10 -6 0 21.40 6.50 10 6 0 15.60 8.50 -10 6 0 5.90 3.50 -10 6 0 3.50 3.20 -10 6 0 4.60 4.50 -11 -6 0 2.50 3.30 -11 -6 0 1.70 3.10 11 -6 0 -3.40 4.60 -11 -6 0 -1.20 3.00 -11 6 0 -2.00 4.20 -11 6 0 4.50 3.70 -11 6 0 0.20 2.80 11 6 0 -3.10 5.90 -12 -6 0 29.10 7.90 -12 -6 0 13.50 5.00 12 -6 0 50.29 9.90 -12 -6 0 24.90 5.90 -12 6 0 33.10 7.10 12 6 0 26.20 10.20 -12 6 0 14.50 6.50 -12 6 0 29.20 6.50 13 -6 0 -3.00 4.30 -13 -6 0 -0.20 4.30 -13 -6 0 -10.10 4.40 -13 6 0 -1.40 4.50 -13 6 0 2.50 5.30 0 -7 0 -0.90 0.90 0 -7 0 0.00 0.90 0 -7 0 -0.40 0.90 0 7 0 -1.00 0.90 0 7 0 0.20 1.50 0 7 0 0.00 1.70 1 -7 0 -0.10 1.00 -1 -7 0 0.40 0.90 1 -7 0 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1.80 -5 7 0 -1.10 1.10 6 -7 0 5.00 3.60 -6 -7 0 2.10 1.60 -6 -7 0 3.30 1.70 6 -7 0 2.20 2.70 -6 -7 0 0.70 2.10 6 -7 0 1.10 1.60 -6 7 0 1.30 2.20 -6 7 0 -0.10 1.50 -6 7 0 -0.30 1.60 -6 7 0 3.50 3.50 6 7 0 -4.40 4.30 7 -7 0 2.10 4.70 7 -7 0 -4.20 2.80 7 -7 0 -1.30 1.50 -7 -7 0 1.90 2.10 -7 -7 0 4.50 2.80 -7 -7 0 3.40 1.80 -7 7 0 1.00 3.40 -7 7 0 1.10 3.00 -7 7 0 1.70 1.90 7 7 0 0.20 5.70 -7 7 0 0.10 1.90 8 -7 0 1.40 3.40 -8 -7 0 -0.20 1.70 -8 -7 0 0.20 1.90 -8 -7 0 -4.20 2.70 8 -7 0 -1.40 1.70 -8 7 0 -2.20 3.70 -8 7 0 -0.20 2.20 -8 7 0 0.50 3.00 8 7 0 4.80 6.80 -8 7 0 0.60 2.10 -9 -7 0 1.00 2.20 9 -7 0 -1.10 2.10 9 -7 0 -1.20 3.50 -9 -7 0 2.40 3.30 -9 -7 0 1.70 2.50 -9 7 0 1.20 3.80 9 7 0 0.40 5.40 -9 7 0 0.90 3.10 -9 7 0 -1.00 2.50 -10 -7 0 1.80 2.90 -10 -7 0 5.10 3.80 10 -7 0 2.40 2.70 10 -7 0 3.60 4.30 -10 -7 0 -1.60 3.20 -10 7 0 3.10 4.00 10 7 0 -1.70 5.60 -10 7 0 -1.20 2.70 -10 7 0 -4.70 2.60 -11 -7 0 -0.10 2.40 11 -7 0 2.00 2.80 11 -7 0 2.20 4.80 -11 -7 0 -2.70 2.40 -11 -7 0 0.70 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85.19 10.70 -8 15 0 75.49 9.90 -8 15 0 93.09 11.20 -8 15 0 92.19 13.70 -9 -15 0 5.30 3.40 9 -15 0 0.00 3.20 9 -15 0 5.50 4.60 9 -15 0 4.00 4.20 -9 15 0 2.40 3.80 -9 15 0 -4.70 6.40 -9 15 0 -1.80 3.00 -9 15 0 1.70 4.40 10 -15 0 17.10 7.00 10 -15 0 7.80 4.10 -10 -15 0 9.00 4.30 -10 15 0 12.60 6.80 -10 15 0 4.20 5.00 11 -15 0 4.90 6.00 -11 -15 0 0.70 3.10 11 -15 0 3.10 4.90 -11 15 0 3.80 4.60 0 -16 0 173.18 10.20 0 -16 0 177.08 10.80 0 16 0 162.48 10.90 0 16 0 151.18 15.60 1 -16 0 0.80 2.30 1 -16 0 -1.50 1.50 -1 -16 0 1.80 2.60 -1 -16 0 1.80 2.30 -1 16 0 -2.20 3.50 1 16 0 3.60 4.40 -1 16 0 1.40 2.70 2 -16 0 59.29 6.90 2 -16 0 67.49 7.80 -2 -16 0 60.49 7.20 -2 -16 0 76.39 9.60 -2 -16 0 68.89 7.20 -2 16 0 76.99 8.80 2 16 0 79.79 10.90 2 16 0 77.19 10.90 -2 16 0 68.29 10.20 -3 -16 0 -0.70 2.60 3 -16 0 -5.20 2.30 3 -16 0 1.60 2.40 3 -16 0 1.10 2.00 -3 -16 0 2.30 4.30 -3 -16 0 3.40 2.50 3 16 0 1.20 4.10 3 16 0 0.30 4.50 -3 16 0 -2.40 4.50 -3 16 0 1.40 2.60 -4 -16 0 17.80 4.30 4 -16 0 9.30 3.60 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11.10 3.80 -8 11 3 9.30 4.30 -8 11 3 6.50 3.10 8 11 -3 20.00 8.80 -8 11 3 6.40 4.60 -7 -11 3 2.60 2.30 7 -11 -3 6.20 2.50 7 -11 -3 5.90 3.10 -7 -11 3 5.60 2.80 -7 -11 3 1.90 3.20 7 -11 -3 1.80 3.40 -7 11 3 4.00 5.10 -7 11 3 8.10 4.00 -7 11 3 -1.70 2.80 -7 11 3 3.80 2.60 7 11 -3 4.30 6.80 6 -11 -3 147.99 10.30 6 -11 -3 147.29 9.00 -6 -11 3 137.89 8.50 -6 -11 3 137.19 9.10 6 -11 -3 152.08 9.40 -6 -11 3 145.89 12.50 -6 11 3 143.99 9.60 -6 11 3 142.79 9.80 6 11 -3 147.89 17.20 -6 11 3 114.69 12.50 -6 11 3 151.88 10.60 5 -11 -3 12.30 3.80 -5 -11 3 11.80 3.00 5 -11 -3 3.80 2.30 -5 -11 3 10.40 4.60 -5 -11 3 11.80 3.00 -5 -11 3 2.10 2.80 5 -11 -3 10.10 3.20 5 -11 -3 7.90 2.60 -5 11 3 16.90 4.90 5 11 -3 14.30 6.80 -5 11 3 15.70 3.40 -5 11 3 10.90 3.50 -5 11 3 11.10 3.80 -4 -11 3 95.29 6.60 4 -11 -3 99.89 7.10 4 -11 -3 108.49 7.60 4 -11 -3 104.59 6.80 -4 -11 3 91.09 8.80 -4 -11 3 103.29 7.10 -4 11 3 100.69 11.40 4 11 -3 106.19 8.20 -4 11 3 97.19 7.30 4 11 -3 106.49 12.70 -4 11 3 101.39 7.40 -4 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3.20 3.60 -9 5 4 4.70 3.80 -9 5 4 2.60 2.60 -9 5 4 5.80 4.80 9 5 -4 3.90 7.20 8 -5 -4 2.70 6.40 -8 -5 4 2.60 3.30 -8 -5 4 5.10 2.50 -8 -5 4 13.80 3.30 -8 5 4 11.30 3.50 8 5 -4 8.20 7.50 -8 5 4 1.80 2.70 -8 5 4 2.00 2.20 7 -5 -4 3.20 4.80 -7 -5 4 2.10 2.80 -7 -5 4 3.80 1.90 -7 -5 4 4.70 2.20 -7 5 4 2.90 3.00 7 5 -4 4.70 7.40 -7 5 4 5.70 3.00 -7 5 4 2.20 1.90 -7 5 4 5.30 2.50 6 -5 -4 121.39 11.10 -6 -5 4 103.39 6.30 -6 -5 4 111.19 9.90 -6 5 4 103.79 7.10 -6 5 4 105.09 7.50 -6 5 4 122.29 7.50 -6 5 4 119.39 8.60 6 5 -4 119.89 14.00 5 -5 -4 6.20 3.10 -5 -5 4 1.70 1.20 -5 -5 4 2.40 2.00 -5 -5 4 4.50 1.60 -5 5 4 6.20 2.70 -5 5 4 4.40 1.50 -5 5 4 0.70 2.00 5 5 -4 2.50 5.40 -5 5 4 0.60 1.60 4 -5 -4 1.80 1.20 -4 -5 4 1.20 1.10 -4 -5 4 0.30 1.60 4 -5 -4 1.40 2.20 -4 -5 4 1.00 1.20 -4 5 4 -0.80 1.90 -4 5 4 -1.20 1.70 -4 5 4 1.70 1.40 -4 5 4 2.20 1.40 4 5 -4 3.10 4.80 3 -5 -4 50.89 3.30 -3 -5 4 46.20 5.10 -3 -5 4 49.90 3.60 3 -5 -4 49.30 4.90 -3 -5 4 48.80 3.20 3 5 -4 56.79 7.80 3 5 -4 53.59 4.60 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12.40 5.20 -9 7 4 14.90 4.40 -9 7 4 7.20 3.10 -9 7 4 13.40 5.20 9 7 -4 16.50 8.70 8 -7 -4 15.40 6.90 -8 -7 4 14.20 3.60 8 -7 -4 15.90 5.10 -8 -7 4 11.00 4.10 8 -7 -4 13.40 3.40 -8 -7 4 11.60 3.40 -8 7 4 14.10 4.10 8 7 -4 8.80 7.40 -8 7 4 8.60 3.10 -8 7 4 17.20 5.00 7 -7 -4 -0.30 1.50 7 -7 -4 2.70 3.40 -7 -7 4 0.80 2.10 -7 -7 4 2.70 3.20 7 -7 -4 12.00 5.20 -7 -7 4 -0.90 1.70 -7 7 4 0.00 2.50 -7 7 4 5.80 3.20 -7 7 4 3.60 2.60 7 7 -4 -0.20 6.70 -7 7 4 5.40 2.20 -6 -7 4 30.40 4.30 6 -7 -4 36.30 5.70 6 -7 -4 25.60 3.60 -6 -7 4 43.70 6.60 -6 -7 4 36.70 4.30 6 -7 -4 32.50 6.20 6 7 -4 28.00 9.20 -6 7 4 26.30 4.50 -6 7 4 27.80 4.40 -6 7 4 26.90 5.10 -6 7 4 26.10 4.70 -5 -7 4 1.10 2.10 -5 -7 4 1.70 1.30 5 -7 -4 0.00 1.30 5 -7 -4 0.10 2.10 5 -7 -4 1.00 2.10 -5 -7 4 -1.10 1.10 -5 7 4 -1.80 1.60 -5 7 4 0.60 1.40 5 7 -4 0.20 5.40 -5 7 4 3.60 2.80 -5 7 4 0.80 1.70 -4 -7 4 0.00 1.10 -4 -7 4 0.30 1.60 -4 -7 4 -0.80 0.70 4 -7 -4 -0.60 1.90 4 -7 -4 0.00 1.70 4 -7 -4 0.00 1.10 4 -7 -4 0.20 1.10 -4 7 4 0.60 1.30 4 7 -4 -7.90 3.80 -4 7 4 0.30 1.20 4 7 -4 0.90 1.50 -4 7 4 -0.90 1.60 -4 7 4 -0.20 2.00 3 -7 -4 91.89 4.90 3 -7 -4 81.19 5.00 -3 -7 4 80.29 4.60 3 -7 -4 73.89 5.20 -3 -7 4 70.99 6.40 -3 -7 4 69.59 4.90 -3 7 4 80.79 7.70 -3 7 4 75.79 5.10 -3 7 4 73.79 5.30 -3 7 4 77.89 5.00 3 7 -4 69.89 8.90 3 7 -4 76.69 5.80 2 -7 -4 1986.70 60.69 2 -7 -4 1909.61 62.39 2 -7 -4 1963.10 60.09 2 -7 -4 1949.10 60.49 -2 -7 4 1917.11 60.69 -2 -7 4 1959.50 61.79 -2 -7 4 1917.21 60.29 2 7 -4 1996.90 62.89 -2 7 4 1946.51 61.09 -2 7 4 1893.11 63.69 -2 7 4 1870.61 60.29 -2 7 4 1955.70 60.49 2 7 -4 1942.31 64.99 -1 -7 4 1.70 1.20 -1 -7 4 0.60 1.00 1 -7 -4 2.00 1.00 1 -7 -4 2.10 1.30 1 -7 -4 1.50 1.10 1 -7 -4 0.50 2.20 -1 -7 4 2.30 1.30 -1 7 4 2.30 1.20 -1 7 4 3.40 1.60 1 7 -4 0.40 1.00 -1 7 4 0.90 2.10 1 7 -4 -0.40 2.40 1 7 -4 0.20 1.90 0 -7 -4 -1.80 1.60 0 -7 4 0.40 0.90 0 -7 -4 1.00 1.20 0 -7 -4 -0.40 0.60 0 -7 4 0.50 0.80 0 -7 4 -1.00 1.00 0 7 -4 0.10 1.90 0 7 -4 0.00 1.10 0 7 4 0.40 1.10 0 7 -4 0.90 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2.00 2.10 -4 -10 4 1.90 1.70 -4 10 4 5.40 2.20 -4 10 4 7.30 2.70 4 10 -4 5.20 2.90 4 10 -4 -2.40 4.80 -4 10 4 4.90 3.10 -4 10 4 4.30 2.10 3 -10 -4 405.96 16.30 -3 -10 4 391.26 16.40 3 -10 -4 395.56 16.40 -3 -10 4 408.26 17.60 -3 -10 4 380.86 15.90 3 -10 -4 413.06 15.90 -3 10 4 394.16 19.80 -3 10 4 440.66 16.70 3 10 -4 404.06 20.80 -3 10 4 411.76 16.40 -3 10 4 399.56 17.10 3 10 -4 423.96 18.60 2 -10 -4 34.30 3.90 -2 -10 4 41.20 4.50 2 -10 -4 32.00 4.10 -2 -10 4 34.00 4.10 2 -10 -4 31.50 3.50 -2 -10 4 35.70 4.50 2 10 -4 42.70 7.10 2 10 -4 33.90 5.50 -2 10 4 33.90 4.40 -2 10 4 33.80 5.90 -2 10 4 32.80 3.70 -1 -10 4 4.40 1.70 1 -10 -4 1.30 1.30 1 -10 -4 2.60 2.80 1 -10 -4 0.10 1.20 1 -10 -4 2.20 1.60 -1 -10 4 2.60 1.60 -1 -10 4 1.30 1.40 -1 10 4 2.90 3.30 1 10 -4 0.30 1.40 -1 10 4 -0.80 1.60 1 10 -4 3.40 2.80 1 10 -4 0.00 2.70 0 -10 4 1.90 1.60 0 -10 -4 1.20 1.10 0 -10 -4 -1.20 2.20 0 -10 -4 0.00 1.50 0 -10 4 1.90 1.70 0 -10 -4 0.40 1.00 0 -10 4 0.40 1.00 0 10 -4 -1.60 2.20 0 10 4 -1.40 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2.40 -5 -10 -4 2.80 2.30 -5 -10 -4 2.80 2.00 5 -10 4 5.80 2.20 -5 10 -4 8.60 3.00 5 10 4 10.40 5.60 5 10 4 7.60 2.60 -5 10 -4 5.60 3.00 -5 10 -4 6.30 4.40 -5 10 -4 1.60 2.20 6 -10 4 3.40 3.30 -6 -10 -4 2.90 2.20 6 -10 4 1.20 2.10 -6 -10 -4 2.50 2.10 -6 -10 -4 4.90 2.30 -6 10 -4 5.40 3.10 6 10 4 0.20 4.70 -6 10 -4 2.30 4.60 -6 10 -4 8.60 3.40 -6 10 -4 2.90 2.50 6 10 4 2.00 3.40 -7 -10 -4 34.80 5.10 7 -10 4 19.10 4.00 7 -10 4 28.20 6.20 -7 -10 -4 27.20 4.60 -7 10 -4 32.30 5.90 7 10 4 23.10 7.30 -7 10 -4 15.30 5.20 -7 10 -4 27.00 7.10 -7 10 -4 32.70 5.70 -8 -10 -4 1.00 2.60 -8 -10 -4 -2.00 1.90 8 -10 4 0.70 2.20 8 -10 4 8.20 4.20 -8 10 -4 -1.00 2.30 -8 10 -4 1.70 5.00 8 10 4 -2.30 4.60 -8 10 -4 5.50 3.50 -8 10 -4 0.90 2.50 9 -10 4 6.70 4.70 -9 -10 -4 1.90 3.00 9 -10 4 0.10 2.40 -9 -10 -4 5.80 3.20 -9 10 -4 -3.00 2.40 9 10 4 2.00 5.20 -9 10 -4 5.10 3.50 -9 10 -4 -1.70 5.00 -9 10 -4 1.90 4.20 -10 -10 -4 4.20 4.00 -10 -10 -4 12.70 4.70 10 -10 4 5.30 3.30 10 -10 4 2.80 4.80 10 10 4 13.70 7.60 -10 10 -4 2.30 3.70 -10 10 -4 5.50 4.50 -10 10 -4 8.20 5.30 11 -10 4 -1.40 5.00 -11 -10 -4 0.60 3.80 11 -10 4 0.00 4.70 -11 -10 -4 0.20 2.90 -11 10 -4 10.40 5.30 -11 10 -4 6.30 4.10 11 10 4 6.60 8.10 -11 10 -4 10.90 5.40 12 -10 4 2.10 5.20 -12 -10 -4 -0.50 3.80 -12 10 -4 0.50 3.80 -12 10 -4 0.40 4.10 12 -11 -4 12.40 6.60 -12 -11 4 0.10 4.00 -12 -11 4 -0.90 5.90 -12 11 4 -0.50 4.00 -12 11 4 -1.00 4.10 -11 -11 4 6.30 6.10 11 -11 -4 8.20 4.40 11 -11 -4 11.20 5.60 -11 -11 4 4.80 3.90 -11 11 4 3.60 4.80 -11 11 4 11.10 5.70 -11 11 4 2.70 3.70 -10 -11 4 19.80 4.80 10 -11 -4 17.40 4.40 10 -11 -4 11.50 5.50 -10 -11 4 7.10 3.80 -10 -11 4 13.70 5.70 -10 11 4 14.70 4.70 -10 11 4 8.60 5.80 10 11 -4 12.50 7.90 -10 11 4 13.60 5.10 -9 -11 4 42.50 6.60 9 -11 -4 37.00 7.60 -9 -11 4 40.70 7.80 -9 -11 4 40.50 6.10 9 -11 -4 27.90 5.60 9 11 -4 21.30 9.20 -9 11 4 48.40 8.80 -9 11 4 46.00 7.30 -9 11 4 38.20 6.80 -8 -11 4 12.40 3.60 8 -11 -4 9.60 3.30 8 -11 -4 10.70 3.40 -8 -11 4 3.50 2.70 -8 -11 4 3.80 3.70 8 -11 -4 11.00 4.40 8 11 -4 17.10 8.20 -8 11 4 11.30 5.50 -8 11 4 14.10 4.40 -8 11 4 9.30 3.80 -8 11 4 2.70 2.80 -7 -11 4 1.70 2.20 -7 -11 4 -0.50 3.30 7 -11 -4 -2.00 2.90 7 -11 -4 1.00 2.30 7 -11 -4 0.50 2.10 -7 -11 4 0.00 1.90 -7 11 4 0.50 4.10 7 11 -4 3.10 6.60 -7 11 4 -0.30 2.20 -7 11 4 2.20 3.10 -7 11 4 1.20 2.50 6 -11 -4 171.18 11.30 -6 -11 4 168.88 10.10 6 -11 -4 174.08 10.10 -6 -11 4 151.78 11.30 6 -11 -4 162.18 10.90 6 -11 -4 167.48 9.60 -6 -11 4 162.08 9.20 6 11 -4 171.38 18.30 -6 11 4 160.58 11.00 -6 11 4 160.48 10.30 -6 11 4 162.38 10.60 -6 11 4 161.88 12.60 -5 -11 4 2.30 2.50 -5 -11 4 15.60 3.50 5 -11 -4 11.60 3.10 5 -11 -4 7.70 3.30 -5 -11 4 11.10 2.80 5 -11 -4 20.60 4.10 5 -11 -4 18.20 4.30 -5 11 4 9.50 3.60 -5 11 4 6.10 3.00 -5 11 4 15.50 4.90 -5 11 4 14.60 3.60 5 11 -4 23.90 8.00 -4 -11 4 72.29 7.90 4 -11 -4 90.49 7.80 -4 -11 4 82.89 6.90 4 -11 -4 86.09 7.30 4 -11 -4 72.69 6.40 -4 -11 4 67.09 6.60 -4 11 4 62.69 8.90 4 11 -4 66.09 10.80 -4 11 4 66.79 6.80 -4 11 4 89.39 7.50 4 11 -4 92.99 8.80 -4 11 4 78.99 7.60 3 -11 -4 0.70 2.00 -3 -11 4 -1.10 1.20 3 -11 -4 0.90 1.40 -3 -11 4 5.30 2.70 -3 -11 4 2.00 1.60 3 -11 -4 0.30 2.10 -3 11 4 2.70 1.60 -3 11 4 0.20 1.80 3 11 -4 1.70 4.80 -3 11 4 4.20 1.90 3 11 -4 0.80 2.70 -3 11 4 3.70 3.40 -2 -11 4 2.50 1.70 2 -11 -4 4.10 2.20 2 -11 -4 -0.60 1.00 -2 -11 4 2.80 2.00 -2 -11 4 1.90 1.90 2 -11 -4 2.40 1.50 2 11 -4 2.70 4.10 -2 11 4 0.50 2.90 2 11 -4 4.60 3.30 -2 11 4 2.00 1.60 -2 11 4 2.10 2.00 -1 -11 4 72.69 5.50 1 -11 -4 79.59 4.80 1 -11 -4 84.19 5.90 -1 -11 4 74.99 6.30 1 -11 -4 61.99 7.40 1 -11 -4 84.29 5.40 1 11 -4 78.29 6.90 -1 11 4 77.39 6.80 -1 11 4 66.49 8.40 1 11 -4 72.49 8.50 1 11 -4 71.79 8.20 0 -11 -4 0.60 2.90 0 -11 -4 -1.00 0.80 0 -11 4 -0.60 1.00 0 -11 4 2.60 1.90 0 -11 -4 1.60 1.10 0 -11 -4 -0.70 1.50 0 -11 4 -1.00 1.30 0 11 -4 0.20 1.60 0 11 4 1.10 1.60 0 11 4 0.50 2.60 0 11 -4 0.30 2.70 0 11 -4 0.80 2.40 1 -11 4 84.79 6.00 1 -11 4 84.79 5.70 -1 -11 -4 74.49 5.10 1 -11 4 78.39 6.80 -1 -11 -4 80.49 6.70 -1 -11 -4 68.29 7.30 -1 11 -4 67.29 6.80 1 11 4 74.29 8.30 -1 11 -4 80.09 9.60 -1 11 -4 75.79 5.90 -2 -11 -4 0.30 1.30 2 -11 4 1.30 1.60 2 -11 4 0.80 1.70 2 -11 4 5.60 2.70 -2 -11 -4 4.70 2.00 -2 -11 -4 -4.00 1.90 -2 11 -4 0.00 2.90 2 11 4 4.70 3.90 -2 11 -4 0.60 1.90 2 11 4 2.00 2.90 -3 -11 -4 1.60 1.70 -3 -11 -4 2.00 1.90 3 -11 4 0.60 1.40 3 -11 4 2.40 1.90 3 -11 4 6.20 2.80 -3 -11 -4 1.50 3.00 -3 11 -4 1.90 1.80 -3 11 -4 2.40 3.50 3 11 4 1.10 2.80 -3 11 -4 0.20 1.80 3 11 4 6.90 4.10 4 -11 4 74.29 7.70 4 -11 4 67.79 6.50 -4 -11 -4 74.29 7.00 -4 -11 -4 81.69 6.80 -4 -11 -4 78.09 6.70 4 -11 4 72.49 7.10 -4 11 -4 76.29 7.80 4 11 4 83.69 8.20 4 11 4 85.19 11.10 -4 11 -4 64.79 9.20 -4 11 -4 82.59 7.80 -4 11 -4 86.49 8.50 -5 -11 -4 8.70 2.80 -5 -11 -4 7.00 2.50 5 -11 4 10.70 3.00 5 -11 4 8.70 3.00 5 -11 4 11.70 4.20 -5 -11 -4 13.00 3.60 -5 11 -4 7.80 4.40 -5 11 -4 10.20 3.60 5 11 4 11.10 3.20 -5 11 -4 6.30 2.90 5 11 4 9.90 5.60 -5 11 -4 17.20 3.90 -6 -11 -4 157.88 9.70 6 -11 4 175.88 11.80 6 -11 4 177.18 10.30 -6 -11 -4 160.28 9.40 -6 -11 -4 178.98 10.00 6 11 4 170.18 17.10 -6 11 -4 140.09 14.50 -6 11 -4 156.38 11.10 -6 11 -4 181.68 11.80 -6 11 -4 162.18 10.80 -7 -11 -4 1.40 2.40 7 -11 4 -2.00 2.90 7 -11 4 -1.90 2.00 -7 -11 -4 1.50 2.40 7 11 4 0.80 4.10 -7 11 -4 1.60 2.90 -7 11 -4 -2.00 2.10 -7 11 -4 2.90 3.50 -7 11 -4 -1.10 4.00 8 -11 4 9.30 4.40 -8 -11 -4 12.50 3.60 8 -11 4 5.80 3.20 -8 -11 -4 7.90 3.70 -8 11 -4 0.90 2.80 -8 11 -4 7.00 5.60 -8 11 -4 4.90 3.40 8 11 4 11.50 6.70 -8 11 -4 1.80 3.60 9 -11 4 40.50 6.60 -9 -11 -4 33.50 6.00 -9 -11 -4 35.00 6.10 9 -11 4 36.90 7.50 -9 11 -4 34.30 6.80 -9 11 -4 35.50 6.70 -9 11 -4 21.60 5.60 9 11 4 38.50 9.70 -9 11 -4 31.00 8.80 10 -11 4 17.80 6.10 10 -11 4 13.60 4.50 -10 -11 -4 19.60 5.10 -10 -11 -4 6.30 3.80 -10 11 -4 7.30 5.00 -10 11 -4 12.30 5.20 -10 11 -4 15.30 5.20 10 11 4 8.20 8.50 11 -11 4 0.80 4.10 -11 -11 -4 12.90 4.70 -11 11 -4 3.80 4.00 -11 11 -4 7.90 5.60 12 -11 4 0.60 4.90 -12 -11 -4 2.50 3.90 -12 11 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22.20 9.20 -7 12 4 47.90 7.10 -7 12 4 34.60 7.10 -6 -12 4 2.90 3.30 -6 -12 4 -1.10 1.80 6 -12 -4 0.80 2.20 6 -12 -4 -0.60 1.90 6 -12 -4 0.60 3.20 -6 -12 4 2.20 2.10 -6 12 4 1.30 2.60 6 12 -4 3.70 6.10 -6 12 4 2.00 2.40 -6 12 4 2.60 4.00 -6 12 4 -3.80 2.30 5 -12 -4 96.29 8.80 5 -12 -4 95.39 8.80 -5 -12 4 93.49 10.00 5 -12 -4 75.99 7.00 -5 -12 4 90.89 7.70 -5 -12 4 81.09 7.60 5 -12 -4 89.49 8.10 -5 12 4 105.49 9.80 -5 12 4 106.19 9.40 5 12 -4 88.39 13.30 -5 12 4 106.19 8.90 -5 12 4 99.89 11.30 -4 -12 4 30.80 4.70 -4 -12 4 46.40 5.40 4 -12 -4 33.00 4.50 4 -12 -4 40.00 5.30 -4 -12 4 29.90 5.30 4 -12 -4 31.20 4.80 -4 12 4 34.60 5.50 -4 12 4 43.80 5.70 4 12 -4 36.90 6.00 4 12 -4 36.50 8.40 -4 12 4 38.90 7.30 -4 12 4 36.70 5.00 -3 -12 4 132.39 8.10 3 -12 -4 127.19 8.30 -3 -12 4 132.99 8.30 3 -12 -4 132.39 8.00 3 -12 -4 122.69 7.50 -3 -12 4 134.29 9.00 -3 12 4 131.39 7.90 3 12 -4 132.49 10.10 -3 12 4 137.79 9.00 3 12 -4 140.09 14.20 -3 12 4 137.09 13.20 -2 -12 4 -0.70 1.50 2 -12 -4 -4.50 2.80 -2 -12 4 5.60 2.20 2 -12 -4 0.50 1.40 -2 -12 4 -0.80 1.20 2 -12 -4 0.00 1.70 2 -12 -4 0.70 1.50 2 12 -4 2.10 3.30 -2 12 4 2.20 3.00 -2 12 4 1.20 2.00 2 12 -4 -4.80 3.70 -1 -12 4 7.70 2.40 -1 -12 4 13.10 3.00 1 -12 -4 5.50 4.40 1 -12 -4 5.40 2.20 1 -12 -4 6.60 2.10 -1 -12 4 12.20 2.90 1 12 -4 8.40 2.90 -1 12 4 7.80 4.10 1 12 -4 8.10 4.00 -1 12 4 6.80 2.90 1 12 -4 -2.10 3.00 0 -12 -4 -0.10 1.60 0 -12 4 2.10 1.80 0 -12 -4 0.80 2.80 0 -12 4 1.00 1.90 0 -12 -4 -0.90 1.00 0 -12 4 -1.50 1.10 0 12 -4 3.70 2.30 0 12 -4 0.40 2.40 0 12 4 -1.70 2.80 0 12 4 -0.10 1.70 0 12 -4 1.40 3.20 1 -12 4 8.70 2.20 -1 -12 -4 3.40 1.80 -1 -12 -4 3.80 2.30 1 -12 4 6.50 2.50 -1 -12 -4 11.60 4.40 1 -12 4 9.70 2.70 1 12 4 1.70 3.50 -1 12 -4 4.20 2.40 -1 12 -4 6.20 4.00 2 -12 4 -0.50 1.40 2 -12 4 0.70 1.70 -2 -12 -4 -2.10 1.50 -2 -12 -4 -1.80 2.40 -2 -12 -4 0.20 1.50 2 -12 4 1.10 1.90 -2 12 -4 -1.70 1.90 -2 12 -4 1.70 3.30 2 12 4 -1.40 2.60 2 12 4 3.80 3.40 -3 -12 -4 138.09 8.10 3 -12 4 129.99 8.50 3 -12 4 134.29 8.30 -3 -12 -4 116.19 8.90 -3 -12 -4 138.09 7.90 3 -12 4 141.59 9.10 -3 12 -4 141.19 9.30 3 12 4 127.89 13.50 -3 12 -4 118.59 8.30 -3 12 -4 135.79 13.90 3 12 4 128.49 9.70 -4 -12 -4 34.30 5.40 -4 -12 -4 41.80 5.10 4 -12 4 30.40 4.90 4 -12 4 38.90 5.20 4 -12 4 36.30 5.60 -4 -12 -4 35.00 4.90 4 12 4 41.30 6.10 4 12 4 40.80 8.80 -4 12 -4 42.10 6.20 -4 12 -4 38.40 5.50 -4 12 -4 39.30 8.40 -5 -12 -4 90.49 7.00 5 -12 4 111.69 10.20 -5 -12 -4 80.99 7.30 -5 -12 -4 91.19 8.10 5 -12 4 90.29 8.10 5 -12 4 86.49 8.30 5 12 4 81.69 8.20 -5 12 -4 103.49 12.60 -5 12 -4 93.79 9.30 5 12 4 67.89 11.10 -5 12 -4 102.09 9.50 -5 12 -4 96.89 9.40 -6 -12 -4 0.30 2.30 6 -12 4 -0.30 1.50 6 -12 4 1.80 2.60 6 -12 4 -1.40 2.70 -6 -12 -4 2.20 2.50 -6 12 -4 1.20 3.10 -6 12 -4 -1.90 1.40 -6 12 -4 -0.10 4.30 6 12 4 -2.50 4.40 -6 12 -4 3.40 3.00 7 -12 4 37.80 7.00 -7 -12 -4 37.70 5.60 7 -12 4 26.10 5.00 -7 -12 -4 35.00 5.80 -7 12 -4 40.70 7.00 7 12 4 32.30 8.80 -7 12 -4 59.19 10.20 -7 12 -4 25.50 5.40 -7 12 -4 23.40 5.40 -8 -12 -4 12.70 4.00 8 -12 4 5.10 3.10 8 -12 4 3.30 3.90 -8 -12 -4 2.00 2.40 8 12 4 6.20 5.80 -8 12 -4 1.30 6.10 -8 12 -4 6.80 3.90 -8 12 -4 4.70 3.80 -8 12 -4 1.20 3.60 9 -12 4 11.60 4.40 -9 -12 -4 9.20 4.20 -9 -12 -4 3.90 3.30 9 -12 4 5.70 4.30 -9 12 -4 11.30 5.30 9 12 4 8.20 6.50 -9 12 -4 6.30 4.00 -9 12 -4 4.30 4.10 -9 12 -4 9.10 6.70 -10 -12 -4 35.40 6.80 -10 -12 -4 34.30 6.70 10 -12 4 41.50 8.20 10 -12 4 32.00 6.30 -10 12 -4 26.30 7.40 -10 12 -4 20.40 6.30 10 12 4 24.90 9.00 -10 12 -4 29.10 6.50 -11 -12 -4 -1.20 3.20 11 -12 4 4.40 4.30 -11 12 -4 -3.20 3.90 -11 12 -4 -7.60 3.00 12 -12 4 8.30 6.00 -12 -12 -4 4.80 4.30 -12 12 -4 1.60 4.40 -12 12 -4 4.90 6.10 -11 -13 4 2.40 3.60 11 -13 -4 11.30 5.00 11 -13 -4 3.30 5.60 -11 13 4 16.00 7.10 -11 13 4 12.10 5.60 10 -13 -4 15.70 5.50 10 -13 -4 19.80 6.50 10 -13 -4 5.10 3.80 -10 -13 4 17.60 5.20 -10 -13 4 10.80 6.20 -10 13 4 13.80 4.60 -10 13 4 6.70 5.00 -10 13 4 16.70 5.40 -9 -13 4 -1.40 3.60 9 -13 -4 1.10 3.30 -9 -13 4 0.60 3.00 -9 -13 4 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-4 -13 4 0.50 2.20 4 -13 -4 2.90 2.70 -4 -13 4 6.10 2.50 4 -13 -4 2.20 1.90 4 13 -4 3.90 3.40 -4 13 4 4.10 2.60 -4 13 4 4.30 2.20 -4 13 4 2.50 3.90 4 13 -4 -1.10 5.60 -4 13 4 0.40 2.60 -3 -13 4 36.50 5.60 3 -13 -4 35.30 4.50 -3 -13 4 35.40 5.00 3 -13 -4 30.80 4.40 -3 -13 4 36.10 5.00 3 -13 -4 29.60 4.70 -3 13 4 28.90 6.60 3 13 -4 46.90 8.80 -3 13 4 27.10 4.80 3 13 -4 41.40 6.80 -3 13 4 37.20 4.80 2 -13 -4 55.79 5.40 2 -13 -4 80.59 9.30 -2 -13 4 58.79 6.30 -2 -13 4 62.39 6.90 -2 -13 4 75.99 7.00 2 -13 -4 65.19 6.60 -2 13 4 59.69 6.80 2 13 -4 77.09 10.00 -2 13 4 53.69 8.80 2 13 -4 62.99 8.80 1 -13 -4 16.00 2.90 1 -13 -4 18.30 3.70 -1 -13 4 15.40 3.70 1 -13 -4 9.40 4.50 -1 -13 4 13.00 3.20 -1 -13 4 8.90 2.60 1 13 -4 10.60 3.10 -1 13 4 10.10 4.70 1 13 -4 23.00 5.70 -1 13 4 9.10 3.10 1 13 -4 18.40 5.30 0 -13 -4 1.80 1.60 0 -13 -4 -1.30 3.40 0 -13 4 1.70 2.20 0 -13 4 0.20 1.40 0 -13 -4 1.40 2.10 0 -13 4 3.00 2.20 0 13 4 -2.40 3.60 0 13 -4 -1.00 2.60 0 13 -4 1.00 2.00 0 13 -4 0.20 3.10 1 -13 4 16.00 3.60 1 -13 4 13.10 3.30 -1 -13 -4 7.50 2.90 -1 -13 -4 8.90 4.50 1 -13 4 11.20 3.00 -1 -13 -4 8.10 2.40 -1 13 -4 6.70 4.30 -1 13 -4 9.60 3.00 1 13 4 9.20 4.50 2 -13 4 61.99 6.80 2 -13 4 69.29 6.70 -2 -13 -4 70.39 6.70 2 -13 4 66.39 6.90 -2 -13 -4 59.19 5.90 -2 -13 -4 60.49 7.50 -2 13 -4 78.79 8.10 2 13 4 70.09 9.90 -2 13 -4 55.69 9.20 2 13 4 74.39 9.10 3 -13 4 39.50 5.30 -3 -13 -4 37.20 4.70 3 -13 4 28.80 5.00 -3 -13 -4 45.10 5.50 3 -13 4 36.10 5.50 -3 -13 -4 55.29 7.10 -3 13 -4 33.10 7.80 -3 13 -4 28.60 5.30 3 13 4 35.00 6.10 3 13 4 34.60 7.80 -4 -13 -4 2.60 3.00 4 -13 4 2.50 2.30 -4 -13 -4 -2.20 1.90 4 -13 4 3.80 2.90 -4 -13 -4 4.40 2.50 4 -13 4 -0.60 1.90 -4 13 -4 3.20 2.80 -4 13 -4 -1.70 3.30 4 13 4 0.70 3.60 4 13 4 -3.60 3.50 -4 13 -4 0.80 2.40 -5 -13 -4 9.90 4.20 -5 -13 -4 9.80 3.20 5 -13 4 15.00 3.60 -5 -13 -4 13.90 3.30 5 -13 4 9.10 3.50 5 -13 4 16.80 4.50 -5 13 -4 13.70 4.40 -5 13 -4 7.10 3.00 5 13 4 19.30 7.00 -5 13 -4 17.10 6.30 -5 13 -4 7.60 3.60 5 13 4 14.80 4.30 6 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0.80 4.20 10 -14 -4 13.50 5.30 10 -14 -4 12.20 6.30 10 -14 -4 21.20 6.80 -10 -14 4 20.20 5.40 -10 14 4 7.20 5.70 -10 14 4 9.30 5.00 -10 14 4 19.20 6.50 -9 -14 4 9.30 9.40 9 -14 -4 22.00 4.90 -9 -14 4 36.80 6.70 9 -14 -4 16.60 6.20 9 -14 -4 28.60 5.90 -9 -14 4 19.00 5.10 -9 14 4 21.20 6.30 -9 14 4 28.30 7.00 9 14 -4 21.40 10.20 -9 14 4 25.50 7.30 -8 -14 4 -2.90 2.00 8 -14 -4 2.30 4.70 8 -14 -4 -3.00 3.20 -8 -14 4 0.60 2.80 8 -14 -4 0.30 2.60 8 -14 -4 2.80 3.20 -8 -14 4 -2.40 3.90 -8 14 4 6.40 4.10 -8 14 4 1.00 3.20 -8 14 4 1.70 3.90 -8 14 4 -1.60 5.80 8 14 -4 -2.60 6.20 7 -14 -4 3.00 2.70 -7 -14 4 -2.50 2.10 7 -14 -4 6.90 3.90 7 -14 -4 4.50 3.50 -7 -14 4 3.90 3.90 -7 -14 4 3.10 2.30 -7 14 4 -0.60 4.70 -7 14 4 4.80 3.10 -7 14 4 0.20 3.10 7 14 -4 14.80 7.80 -7 14 4 -0.60 2.90 6 -14 -4 97.29 10.10 6 -14 -4 110.79 9.40 6 -14 -4 106.89 10.20 -6 -14 4 111.09 8.10 -6 -14 4 115.49 10.20 -6 -14 4 117.09 11.90 -6 14 4 119.79 11.00 -6 14 4 118.59 10.60 6 14 -4 119.79 15.90 -6 14 4 97.59 10.60 -6 14 4 129.79 14.70 -5 -14 4 2.10 3.80 5 -14 -4 15.20 4.50 -5 -14 4 1.00 2.40 5 -14 -4 7.70 3.30 -5 -14 4 9.10 3.10 5 -14 -4 7.70 2.80 -5 14 4 12.70 4.30 5 14 -4 12.70 6.90 -5 14 4 5.70 3.00 -5 14 4 10.90 5.80 -5 14 4 10.70 4.10 -4 -14 4 87.49 9.50 4 -14 -4 93.49 8.90 -4 -14 4 97.79 8.40 -4 -14 4 90.79 8.30 4 -14 -4 102.79 7.40 -4 14 4 91.79 12.00 -4 14 4 108.49 10.20 4 14 -4 105.49 13.60 -4 14 4 103.99 9.10 4 14 -4 94.19 10.40 3 -14 -4 0.40 1.70 -3 -14 4 2.70 2.40 -3 -14 4 1.20 2.00 -3 -14 4 -1.70 1.70 3 -14 -4 -0.90 2.20 -3 14 4 3.90 2.60 3 14 -4 4.10 3.40 -3 14 4 0.60 4.30 3 14 -4 2.90 4.90 -2 -14 4 0.30 2.30 2 -14 -4 2.90 4.20 2 -14 -4 -0.70 2.20 -2 -14 4 -0.10 1.90 -2 -14 4 -0.70 1.70 2 -14 -4 0.60 1.80 -2 14 4 2.30 3.50 2 14 -4 3.90 3.50 2 14 -4 14.50 5.60 -2 14 4 1.00 2.40 1 -14 -4 299.57 16.90 -1 -14 4 306.67 14.40 1 -14 -4 294.97 13.40 -1 -14 4 279.47 14.10 -1 -14 4 292.77 14.00 -1 14 4 295.77 14.80 1 14 -4 303.17 14.80 1 14 -4 307.77 16.70 -1 14 4 314.87 18.50 1 14 -4 281.17 17.50 0 -14 4 378.16 16.80 0 -14 -4 377.46 15.70 0 -14 -4 335.17 18.70 0 -14 4 350.06 16.20 0 -14 -4 392.16 16.70 0 -14 4 360.66 16.30 0 14 -4 381.16 17.20 0 14 -4 363.26 17.70 0 14 4 385.56 20.70 0 14 -4 386.36 21.10 -1 -14 -4 282.27 16.20 -1 -14 -4 339.57 14.80 1 -14 4 303.57 14.50 1 -14 4 262.37 14.00 1 -14 4 305.57 14.40 -1 -14 -4 291.47 13.60 -1 14 -4 302.07 15.20 -1 14 -4 327.97 19.40 1 14 4 319.47 18.10 2 -14 4 1.50 2.30 -2 -14 -4 0.00 2.00 -2 -14 -4 2.50 3.80 2 -14 4 -0.50 2.30 -2 -14 -4 -2.60 1.50 2 -14 4 -0.40 1.60 2 14 4 0.80 4.00 2 14 4 -3.20 3.70 -2 14 -4 7.30 4.70 -2 14 -4 5.30 3.10 3 -14 4 1.60 2.60 -3 -14 -4 5.00 3.90 3 -14 4 2.00 2.60 -3 -14 -4 -0.80 1.60 3 -14 4 0.60 1.70 -3 -14 -4 -2.20 2.10 3 14 4 -1.10 2.70 -3 14 -4 1.00 2.60 3 14 4 2.70 4.30 -3 14 -4 -0.80 4.00 -4 -14 -4 105.79 7.60 4 -14 4 85.79 8.90 4 -14 4 113.69 10.10 4 -14 4 96.69 8.60 -4 -14 -4 90.69 9.30 -4 -14 -4 105.59 8.90 -4 14 -4 92.89 12.50 -4 14 -4 100.49 10.00 4 14 4 105.39 10.60 -4 14 -4 115.59 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15.10 5.90 -6 -13 10 9.00 3.50 6 -13 -10 -2.30 3.00 6 -13 -10 5.30 4.50 -6 -13 10 -0.50 3.70 -6 13 10 4.00 3.20 6 13 -10 6.10 7.40 -6 13 10 11.50 6.10 -5 -13 10 2.60 3.80 5 -13 -10 6.00 2.90 5 -13 -10 4.60 3.30 -5 -13 10 5.60 2.60 5 -13 -10 5.20 4.80 -5 -13 10 4.50 2.80 -5 13 10 2.30 4.20 5 13 -10 1.40 7.10 -5 13 10 8.10 3.60 4 -13 -10 6.60 4.50 -4 -13 10 5.30 3.80 -4 -13 10 11.30 3.60 -4 -13 10 1.70 2.30 4 -13 -10 8.90 3.40 -4 13 10 10.30 5.00 4 13 -10 5.80 6.50 -4 13 10 6.60 3.30 -3 -13 10 -0.80 1.90 -3 -13 10 10.30 4.30 -3 -13 10 -0.50 2.00 3 -13 -10 2.20 4.30 3 -13 -10 0.50 2.50 -3 13 10 2.30 2.40 -3 13 10 -0.60 3.00 3 13 -10 -1.30 5.80 3 13 -10 1.70 4.20 -2 -13 10 64.69 8.00 -2 -13 10 70.99 6.80 2 -13 -10 68.99 8.40 2 -13 -10 56.69 6.50 -2 -13 10 57.79 6.50 -2 13 10 65.99 9.50 2 13 -10 66.59 9.90 2 13 -10 80.99 10.40 -1 -13 10 7.10 2.70 -1 -13 10 8.10 2.80 1 -13 -10 5.80 3.90 -1 -13 10 2.20 2.50 1 -13 -10 4.60 2.90 1 13 -10 11.10 5.80 -1 13 10 0.50 3.60 1 13 -10 8.20 2.90 0 -13 10 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14 13.40 7.30 10 -6 -14 10.60 8.80 -10 -6 14 10.20 4.90 -10 6 14 14.50 7.00 10 6 -14 30.60 11.60 -9 -6 14 18.90 6.60 9 -6 -14 14.70 8.50 -9 -6 14 4.30 3.20 9 6 -14 18.80 11.00 -9 6 14 6.80 5.20 -8 -6 14 4.80 3.70 8 -6 -14 -2.90 5.10 -8 -6 14 1.00 2.70 8 6 -14 8.00 10.60 -8 6 14 6.10 4.20 -7 -6 14 57.79 6.50 7 -6 -14 60.09 10.30 -7 -6 14 60.29 9.10 -7 6 14 57.89 8.80 7 6 -14 34.60 10.60 6 -6 -14 314.57 19.10 -6 -6 14 337.57 15.30 -6 -6 14 315.67 18.90 6 -6 -14 320.27 14.80 -6 6 14 316.37 17.30 6 6 -14 311.37 22.80 -6 6 14 327.97 14.80 5 -6 -14 359.76 15.50 -5 -6 14 343.77 19.20 5 -6 -14 334.57 18.70 -5 -6 14 331.07 15.10 -5 6 14 370.36 15.80 5 6 -14 326.37 23.40 -5 6 14 372.56 17.80 -4 -6 14 53.89 5.30 4 -6 -14 52.39 7.70 4 -6 -14 44.60 5.50 -4 -6 14 48.30 7.40 -4 6 14 47.50 6.40 4 6 -14 28.20 9.00 -4 6 14 43.60 5.30 4 6 -14 50.59 7.10 -3 -6 14 40.10 4.30 3 -6 -14 53.29 7.50 3 -6 -14 41.70 5.30 -3 -6 14 41.70 6.10 -3 6 14 50.19 5.90 3 6 -14 61.79 8.00 -3 6 14 46.20 5.50 3 6 -14 45.20 10.20 -2 -6 14 10.10 3.20 -2 -6 14 21.10 3.00 2 -6 -14 21.00 4.10 2 6 -14 26.60 7.40 2 6 -14 17.60 5.20 -1 -6 14 34.40 3.40 1 -6 -14 43.20 5.40 1 -6 -14 36.60 3.50 -1 -6 14 40.90 4.20 -1 -6 14 44.90 5.80 1 6 -14 44.00 7.80 1 6 -14 31.50 7.00 0 -6 -14 1.50 1.20 0 -6 -14 3.10 2.70 0 -6 14 1.70 1.50 0 -6 14 2.60 1.50 0 -6 14 1.50 2.00 0 6 -14 -0.10 3.90 0 6 -14 -2.70 4.40 0 6 -14 -0.40 1.30 -1 -6 -14 44.90 4.10 1 -6 14 41.00 4.20 1 -6 14 43.20 5.60 -1 -6 -14 51.59 5.90 -1 6 -14 47.60 6.20 -1 6 -14 40.30 7.60 -1 6 -14 50.29 4.90 2 -6 14 19.30 3.30 -2 -6 -14 20.90 3.00 2 -6 14 20.00 4.20 -2 -6 -14 22.10 4.50 -2 6 -14 17.50 5.90 -2 6 -14 18.40 3.40 3 -6 14 42.90 5.80 3 -6 14 41.20 4.60 -3 -6 -14 52.19 6.10 -3 -6 -14 46.50 4.80 -3 6 -14 46.00 8.50 -3 6 -14 43.90 5.00 -3 6 -14 47.90 5.50 -4 -6 -14 41.80 5.10 -4 -6 -14 36.30 5.70 4 -6 14 45.10 5.20 4 -6 14 35.80 5.80 -4 6 -14 44.40 5.30 -4 6 -14 39.00 5.30 -4 6 -14 41.60 8.50 -5 -6 -14 348.17 15.80 5 -6 14 336.07 17.40 5 -6 14 401.46 16.30 -5 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44.80 8.70 -10 8 -14 31.50 7.30 -10 8 -14 34.70 7.50 -11 -8 -14 7.80 4.10 11 -8 14 12.20 6.80 -11 8 -14 7.80 4.90 11 8 14 12.00 10.10 -11 8 -14 13.90 6.40 -11 -9 14 1.40 5.50 -11 9 14 2.20 5.30 10 -9 -14 26.90 11.90 -10 -9 14 36.30 7.00 -10 -9 14 22.80 8.20 -10 9 14 28.40 7.70 -9 -9 14 21.60 7.20 -9 -9 14 31.80 6.10 9 -9 -14 20.80 9.60 -9 9 14 45.20 8.50 9 9 -14 21.70 12.70 8 -9 -14 1.40 5.10 -8 -9 14 6.90 5.10 -8 -9 14 2.30 2.50 -8 9 14 11.20 5.80 8 9 -14 -6.40 7.80 -7 -9 14 1.50 2.80 7 -9 -14 4.60 5.00 -7 -9 14 2.00 3.30 7 9 -14 5.10 8.90 6 -9 -14 2.90 3.30 -6 -9 14 3.40 3.80 6 -9 -14 4.50 4.10 -6 -9 14 1.50 2.60 6 9 -14 3.10 9.50 -6 9 14 -3.40 2.80 -5 -9 14 7.40 2.80 -5 -9 14 1.20 3.30 5 -9 -14 8.70 5.00 5 -9 -14 5.50 3.30 5 9 -14 8.60 8.40 -5 9 14 5.00 3.20 -4 -9 14 0.80 2.90 4 -9 -14 -2.10 3.10 -4 -9 14 1.40 2.00 4 -9 -14 6.30 3.50 4 9 -14 6.30 8.60 -4 9 14 -1.20 3.10 -3 -9 14 190.58 10.10 3 -9 -14 172.58 10.70 -3 -9 14 192.38 12.60 3 9 -14 190.88 13.40 3 9 -14 178.78 18.00 -3 9 14 180.08 11.70 2 -9 -14 95.09 7.50 -2 -9 14 90.89 9.60 -2 -9 14 86.79 7.30 2 9 -14 113.49 12.30 -2 9 14 70.69 8.00 2 9 -14 91.69 12.50 1 -9 -14 66.29 7.10 1 -9 -14 51.89 4.70 -1 -9 14 64.79 5.60 -1 -9 14 61.69 5.90 -1 -9 14 60.49 7.50 1 9 -14 58.19 9.60 1 9 -14 57.39 5.40 -1 9 14 55.29 7.00 1 9 -14 65.99 9.60 0 -9 14 2.00 1.70 0 -9 14 1.10 1.80 0 -9 -14 0.70 1.90 0 -9 14 0.40 2.40 0 -9 -14 0.30 2.70 0 9 14 -0.20 2.60 0 9 -14 -3.10 4.50 0 9 -14 -1.40 1.40 1 -9 14 49.70 5.30 -1 -9 -14 44.90 4.70 1 -9 14 50.79 5.40 1 -9 14 67.69 7.40 -1 -9 -14 56.59 6.80 1 9 14 54.19 6.70 -1 9 -14 54.39 9.50 -1 9 -14 53.09 5.80 -2 -9 -14 102.09 8.90 2 -9 14 87.39 7.70 2 -9 14 96.29 9.10 -2 -9 -14 77.99 5.70 2 -9 14 76.39 6.90 -2 9 -14 109.59 13.20 -2 9 -14 74.39 7.50 3 -9 14 177.08 11.30 3 -9 14 181.78 10.10 -3 -9 -14 176.28 9.40 -3 -9 -14 171.08 10.70 -3 9 -14 184.18 10.70 -3 9 -14 176.58 17.10 -4 -9 -14 3.30 2.60 -4 -9 -14 3.70 3.40 4 -9 14 0.60 2.10 4 -9 14 1.50 2.80 -4 9 -14 4.90 2.60 -4 9 -14 6.30 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-2 -28 -4.30 5.70 -1 2 -28 14.40 8.00 -2 -2 -28 3.20 6.40 -2 2 -28 17.40 7.40 -3 -2 -28 -1.70 5.00 -3 2 -28 2.80 6.60 -4 -2 -28 5.90 7.20 -4 2 -28 3.10 7.00 -5 -2 -28 11.20 7.60 -5 2 -28 -2.90 8.00 -6 -2 -28 3.60 8.40 -6 2 -28 8.30 9.60 -6 -3 28 0.60 6.10 -5 -3 28 2.90 7.10 -4 -3 28 2.40 6.30 4 3 -28 -5.70 6.60 3 -3 -28 8.90 6.50 -3 -3 28 2.50 6.50 2 -3 -28 5.00 6.10 2 -3 -28 2.00 6.10 2 3 -28 18.70 8.60 1 -3 -28 -5.50 6.00 1 -3 -28 4.70 4.90 1 3 -28 1.10 7.30 0 -3 -28 0.90 4.10 0 -3 -28 -2.10 6.30 0 3 -28 2.70 7.30 -1 -3 -28 2.60 5.40 -1 -3 -28 3.80 6.30 -1 3 -28 2.60 7.90 -2 -3 -28 4.20 6.80 -2 3 -28 2.30 6.20 -3 -3 -28 10.00 7.10 -3 3 -28 1.60 8.00 -4 -3 -28 -1.80 5.80 -4 3 -28 -5.30 5.80 -5 -3 -28 1.80 7.30 -5 3 -28 3.10 7.90 -6 -3 -28 3.40 6.80 -6 3 -28 -5.90 7.90 -6 -4 28 17.90 8.60 -5 -4 28 -1.90 5.60 -4 -4 28 2.80 5.60 -3 -4 28 2.60 5.20 3 -4 -28 11.30 7.00 2 -4 -28 -6.80 5.30 2 -4 -28 6.80 6.20 -2 -4 28 -4.40 5.00 2 4 -28 -6.90 7.00 1 -4 -28 7.40 5.50 1 -4 -28 2.00 5.20 -1 -4 28 15.40 7.20 1 4 -28 0.90 7.40 0 -4 28 -0.20 5.60 0 -4 -28 6.20 5.10 0 -4 -28 -3.20 5.90 0 4 -28 1.60 7.00 -1 -4 -28 4.70 4.30 -1 -4 -28 5.30 6.20 -1 4 -28 -15.80 6.20 -2 -4 -28 -11.40 3.70 -2 4 -28 -1.40 7.20 -3 -4 -28 8.90 6.50 -3 4 -28 -5.30 5.80 -4 -4 -28 7.10 7.10 -4 4 -28 18.20 9.00 -5 -4 -28 -1.60 5.90 -5 4 -28 8.60 7.60 -6 -4 -28 3.80 8.20 -6 4 -28 9.90 8.10 -5 -5 28 -0.70 6.40 -4 -5 28 0.90 5.80 -3 -5 28 4.60 6.00 3 -5 -28 24.70 8.10 -2 -5 28 12.30 6.00 2 -5 -28 4.40 6.30 2 5 -28 17.40 8.50 1 -5 -28 1.60 4.60 -1 -5 28 2.90 5.60 1 -5 -28 7.90 6.50 1 5 -28 7.10 8.20 0 -5 28 2.60 4.80 0 -5 -28 -3.50 4.90 0 -5 -28 1.00 3.90 0 5 -28 9.30 7.30 1 -5 28 -0.30 4.90 -1 -5 -28 -5.00 4.60 -1 -5 -28 3.60 4.80 -1 5 -28 5.80 7.60 2 -5 28 7.90 5.50 -2 -5 -28 12.60 4.30 -2 -5 -28 6.90 6.60 -2 5 -28 15.70 8.30 -3 -5 -28 8.60 7.10 -3 5 -28 14.70 8.80 -4 -5 -28 -3.30 5.80 -4 5 -28 6.60 7.40 -5 -5 -28 6.40 6.70 -5 5 -28 7.50 9.20 -6 -5 -28 13.00 8.20 -6 5 -28 -14.90 8.00 -5 -6 28 3.20 7.00 4 -6 -28 -9.50 4.30 -4 -6 28 -9.00 5.70 -3 -6 28 3.30 6.90 3 -6 -28 -4.30 5.80 2 -6 -28 9.70 5.90 -2 -6 28 -8.70 5.10 2 6 -28 -1.40 6.70 -1 -6 28 15.90 7.00 1 -6 -28 6.50 5.90 1 6 -28 3.40 8.30 0 -6 -28 19.00 7.50 0 -6 28 15.30 6.50 0 6 -28 20.20 9.50 1 -6 28 7.70 5.90 -1 -6 -28 10.60 6.60 -1 -6 -28 8.00 4.80 -1 6 -28 1.70 6.90 -2 -6 -28 -1.80 5.00 2 -6 28 4.10 4.90 -2 6 -28 4.20 7.30 -3 -6 -28 1.50 5.20 3 -6 28 5.20 4.90 -3 6 -28 1.20 8.10 4 -6 28 2.90 6.30 -4 -6 -28 -2.10 5.80 -4 6 -28 -0.50 7.90 -5 -6 -28 -4.10 5.50 -5 6 -28 9.10 8.10 -5 -7 28 18.90 7.60 -4 -7 28 3.60 7.50 4 -7 -28 4.80 6.00 -3 -7 28 0.20 5.80 3 -7 -28 4.50 5.30 2 -7 -28 -3.00 5.50 -2 -7 28 -1.50 5.10 2 7 -28 5.70 8.10 1 -7 -28 0.00 5.80 -1 -7 28 4.20 5.00 1 7 -28 2.60 6.80 0 -7 -28 -1.10 5.20 0 -7 28 5.00 5.50 0 7 -28 0.50 6.50 1 -7 28 -6.20 4.90 -1 -7 -28 -8.20 4.60 -1 7 -28 -0.40 6.70 -2 -7 -28 5.70 5.30 2 -7 28 4.90 5.60 -2 7 -28 11.60 7.70 -3 -7 -28 6.10 6.40 3 -7 28 0.30 4.30 -3 7 -28 7.90 7.80 4 -7 28 7.90 5.10 -4 -7 -28 7.40 6.50 -4 7 -28 9.50 8.00 -5 -7 -28 -1.40 5.60 -5 7 -28 17.60 8.20 4 -8 -28 -5.80 5.00 -4 -8 28 -2.90 6.20 3 -8 -28 5.20 5.40 -3 -8 28 -0.20 5.50 2 -8 -28 -0.10 5.80 -2 -8 28 -0.10 4.50 -1 -8 28 -4.10 5.40 1 -8 -28 3.10 5.80 1 8 -28 15.20 8.10 0 -8 28 3.70 5.30 0 -8 -28 2.40 5.30 0 8 -28 10.40 8.50 1 -8 28 -3.30 5.30 -1 -8 -28 -2.50 6.00 -1 8 -28 10.00 7.40 2 -8 28 5.30 5.90 -2 -8 -28 -2.40 4.80 -2 8 -28 7.40 7.60 -3 -8 -28 2.00 6.20 3 -8 28 6.10 5.00 -3 8 -28 10.20 6.90 4 -8 28 3.10 5.90 -4 -8 -28 3.30 5.80 -4 8 -28 5.90 7.60 3 -9 -28 2.50 5.20 -3 -9 28 2.50 5.90 2 -9 -28 13.50 7.20 -2 -9 28 3.70 5.50 1 -9 -28 4.20 5.70 -1 -9 28 2.20 5.90 1 9 -28 18.60 9.00 0 -9 -28 4.30 6.20 0 -9 28 -3.50 5.20 0 9 -28 2.50 7.60 -1 -9 -28 -1.80 4.70 1 -9 28 1.20 5.60 -1 9 -28 5.50 7.20 -2 -9 -28 2.20 5.10 2 -9 28 8.70 5.60 -2 9 -28 -1.00 8.40 3 -9 28 11.80 5.90 -3 -9 -28 6.50 6.10 -3 9 -28 3.80 6.60 -2 -10 28 9.10 6.70 2 -10 -28 -1.50 5.00 1 -10 -28 12.40 7.50 -1 -10 28 19.20 7.90 1 10 -28 17.50 9.60 0 -10 28 36.60 9.70 0 -10 -28 26.20 7.80 0 10 -28 20.30 9.90 1 -10 28 19.40 8.20 -1 -10 -28 4.30 6.50 -1 10 -28 11.70 8.80 -2 -10 -28 11.40 7.00 2 -10 28 3.70 4.80 -2 10 -28 19.30 10.50 0 11 -28 4.70 8.80 3 0 -29 -1.20 7.50 3 0 -29 11.80 7.00 2 0 -29 6.30 5.60 2 0 -29 5.50 6.80 1 0 -29 14.90 7.90 0 0 -29 1.50 6.10 -1 0 -29 3.70 6.70 -2 0 -29 1.80 6.20 -3 0 -29 3.70 6.70 -4 0 -29 -4.70 5.70 -5 0 -29 1.10 7.20 3 -1 -29 -1.90 6.10 3 1 -29 -5.10 5.60 2 -1 -29 -1.70 5.60 2 -1 -29 -0.30 6.10 2 1 -29 -8.60 6.50 1 -1 -29 20.60 8.90 1 1 -29 7.10 7.20 0 -1 -29 4.10 7.00 0 1 -29 5.00 7.30 -1 -1 -29 8.30 7.10 -1 1 -29 22.70 10.00 -2 -1 -29 5.20 6.20 -2 1 -29 1.50 6.60 -3 -1 -29 1.80 6.50 -3 1 -29 -3.10 5.70 -4 -1 -29 8.10 7.90 -4 1 -29 4.50 6.40 -5 -1 -29 8.40 8.20 -5 1 -29 -6.20 6.80 3 -2 -29 0.50 6.10 2 -2 -29 3.00 5.80 2 -2 -29 20.30 7.70 2 2 -29 11.80 8.10 1 -2 -29 5.80 6.30 1 -2 -29 1.30 5.30 1 2 -29 4.40 6.80 0 -2 -29 15.30 7.80 0 2 -29 26.10 9.10 -1 -2 -29 -8.70 6.20 -1 2 -29 6.10 6.70 -2 -2 -29 12.90 6.90 -2 2 -29 13.60 8.00 -3 -2 -29 3.60 5.90 -3 2 -29 16.60 9.30 -4 -2 -29 7.90 7.20 -4 2 -29 4.90 7.90 -5 -2 -29 0.90 7.20 -5 2 -29 -4.80 7.60 -5 -3 29 13.70 10.10 3 -3 -29 6.20 7.50 2 -3 -29 10.70 8.00 2 3 -29 23.40 10.40 1 -3 -29 6.90 6.60 1 -3 -29 -0.40 4.10 1 3 -29 8.40 8.50 0 -3 -29 5.70 6.70 0 -3 -29 3.20 4.70 0 3 -29 -3.60 6.50 -1 -3 -29 3.80 6.10 -1 3 -29 1.60 7.50 -2 -3 -29 14.90 7.50 -2 3 -29 1.10 7.90 -3 -3 -29 -3.30 5.80 -3 3 -29 0.70 6.30 -4 -3 -29 -3.80 5.00 -4 3 -29 -8.20 5.30 -5 -3 -29 10.40 7.80 -5 3 -29 3.10 6.80 -5 -4 29 9.30 7.70 -4 -4 29 9.40 7.80 -3 -4 29 15.20 7.80 3 -4 -29 22.90 8.40 -2 -4 29 -9.10 6.90 2 -4 -29 -9.20 5.70 2 4 -29 -3.80 6.10 1 -4 -29 8.20 6.60 1 4 -29 9.00 8.10 0 -4 -29 4.30 4.90 0 -4 -29 -3.50 5.40 0 4 -29 -2.70 6.70 -1 -4 -29 2.80 3.80 -1 -4 -29 4.50 6.50 -1 4 -29 -15.70 6.60 -2 -4 -29 -1.20 5.40 -2 4 -29 5.70 8.90 -3 -4 -29 5.90 6.60 -3 4 -29 13.50 8.00 -4 -4 -29 8.20 8.00 -4 4 -29 5.30 8.10 -5 -4 -29 6.00 7.70 -5 4 -29 8.90 8.70 -4 -5 29 12.40 7.70 -3 -5 29 4.20 6.30 3 -5 -29 1.20 6.90 -2 -5 29 -0.10 5.00 2 -5 -29 0.80 6.70 2 5 -29 -1.20 7.40 1 -5 -29 -5.40 5.00 -1 -5 29 0.20 6.30 1 5 -29 -1.30 6.80 0 -5 -29 2.80 6.60 0 -5 29 -3.70 5.40 0 5 -29 -2.10 7.30 -1 -5 -29 1.80 6.30 -1 5 -29 -4.40 6.00 -2 -5 -29 -2.60 6.00 -2 5 -29 5.00 7.10 -3 -5 -29 6.30 5.80 -3 5 -29 -5.00 6.00 -4 -5 -29 1.90 7.00 -4 5 -29 -1.00 6.10 -4 -6 29 5.40 6.90 -3 -6 29 1.60 6.90 3 -6 -29 9.60 6.60 2 -6 -29 3.30 6.10 -2 -6 29 2.70 6.30 2 6 -29 -4.90 7.70 1 -6 -29 1.90 5.30 -1 -6 29 12.50 6.90 1 6 -29 5.40 9.00 0 -6 29 5.00 5.50 0 -6 -29 10.60 6.40 0 6 -29 15.80 9.00 1 -6 29 5.30 6.50 -1 -6 -29 2.00 5.70 -1 6 -29 4.10 8.30 -2 -6 -29 8.50 6.40 2 -6 29 1.30 5.80 -2 6 -29 -5.10 7.10 -3 -6 -29 -6.00 4.80 -3 6 -29 -0.30 6.50 -4 -6 -29 -3.30 5.80 -4 6 -29 4.40 7.00 3 -7 -29 -2.70 6.10 -3 -7 29 4.00 7.50 -2 -7 29 2.90 6.80 2 -7 -29 -0.50 5.00 1 -7 -29 -3.40 5.60 -1 -7 29 3.40 6.10 1 7 -29 5.80 7.80 0 -7 29 -3.70 5.20 0 -7 -29 -4.30 4.90 0 7 -29 5.00 7.30 1 -7 29 1.10 6.00 -1 -7 -29 3.10 5.40 -1 7 -29 2.50 7.20 -2 -7 -29 -1.40 5.30 2 -7 29 4.90 5.70 -2 7 -29 -1.00 7.80 -3 -7 -29 2.70 5.50 3 -7 29 3.90 5.30 -3 7 -29 6.30 7.90 2 -8 -29 3.20 5.70 -2 -8 29 0.90 6.80 -1 -8 29 7.80 6.50 1 -8 -29 -5.50 4.80 1 8 -29 10.90 7.70 0 -8 -29 -13.80 5.30 0 -8 29 1.20 5.90 0 8 -29 0.90 6.10 1 -8 29 -3.10 5.70 -1 -8 -29 3.80 6.70 -1 8 -29 8.40 7.40 2 -8 29 9.70 6.30 -2 -8 -29 -5.80 3.80 -2 8 -29 6.80 8.20 -3 8 -29 11.10 7.60 -1 -9 29 -2.10 5.50 1 -9 -29 7.00 5.40 1 9 -29 20.40 9.30 0 -9 29 3.40 6.80 0 -9 -29 -2.30 5.40 0 9 -29 7.10 7.40 1 -9 29 -4.90 5.50 -1 -9 -29 8.30 6.60 -1 9 -29 5.80 7.60 2 0 -30 8.10 8.10 1 0 -30 0.00 7.30 0 0 -30 -0.80 5.90 -1 0 -30 8.90 8.40 -2 0 -30 5.30 7.90 -3 0 -30 0.20 6.50 -4 0 -30 6.00 7.20 3 -1 -30 -0.20 7.10 2 -1 -30 5.80 6.90 2 1 -30 -2.70 6.00 1 -1 -30 35.60 10.50 1 1 -30 71.59 13.40 0 -1 -30 4.00 8.10 0 1 -30 4.00 6.80 -1 -1 -30 16.30 7.80 -1 1 -30 24.90 9.80 -2 -1 -30 1.20 7.40 -2 1 -30 8.70 7.20 -3 -1 -30 3.20 7.00 -3 1 -30 20.20 7.90 -4 -1 -30 4.70 6.70 -4 1 -30 6.70 7.20 3 -2 -30 12.00 7.60 2 -2 -30 34.20 10.30 2 2 -30 20.90 8.50 1 -2 -30 15.00 8.40 1 2 -30 9.70 8.80 0 -2 -30 -0.10 7.30 0 2 -30 9.10 7.50 -1 -2 -30 2.70 6.50 -1 2 -30 -4.90 7.60 -2 -2 -30 19.00 8.90 -2 2 -30 18.60 9.10 -3 -2 -30 4.10 7.30 -3 2 -30 -7.50 6.00 -4 -2 -30 4.60 6.90 -4 2 -30 -2.80 6.20 3 -3 -30 -2.70 6.90 2 -3 -30 47.40 11.00 2 3 -30 40.50 11.90 1 -3 -30 9.10 8.40 1 3 -30 7.50 9.00 0 -3 -30 -7.90 6.70 0 3 -30 -13.00 6.90 -1 -3 -30 3.60 7.00 -1 3 -30 -9.50 6.60 -2 -3 -30 26.00 8.40 -2 3 -30 36.90 12.70 -3 -3 -30 2.20 5.40 -3 3 -30 0.60 7.90 -4 -3 -30 1.10 7.50 -4 3 -30 -1.80 7.90 3 -4 -30 -5.00 7.60 2 -4 -30 -5.70 6.40 2 4 -30 9.90 9.10 1 -4 -30 2.00 6.50 1 4 -30 5.50 8.80 0 -4 -30 -11.50 4.70 0 4 -30 5.10 8.40 -1 -4 -30 2.20 7.00 -1 4 -30 -7.70 6.50 -2 -4 -30 -0.90 6.10 -2 4 -30 10.00 7.40 -3 -4 -30 9.10 7.30 -3 4 -30 4.70 8.70 3 -5 -30 -3.10 6.90 -3 -5 30 1.40 6.40 2 -5 -30 -3.50 6.30 -2 -5 30 0.40 7.00 2 5 -30 -7.20 8.00 1 -5 -30 1.50 6.40 1 5 -30 0.70 8.20 0 -5 -30 2.00 6.80 0 5 -30 8.60 7.70 -1 -5 -30 -7.40 4.70 -1 5 -30 10.50 8.50 -2 -5 -30 5.70 7.70 -2 5 -30 -2.30 7.70 -3 -5 -30 3.20 6.60 -3 5 -30 0.10 7.90 2 -6 -30 9.30 6.80 -2 -6 30 3.00 6.40 1 -6 -30 1.60 5.80 -1 -6 30 15.80 7.10 1 6 -30 12.20 9.80 0 -6 30 -7.50 4.90 0 -6 -30 -0.90 6.30 0 6 -30 -8.50 6.40 -1 -6 -30 2.10 6.10 -1 6 -30 6.00 8.20 -2 -6 -30 -1.30 6.60 -2 6 -30 -9.20 8.50 1 -7 -30 4.90 6.50 -1 -7 30 8.60 7.00 1 7 -30 27.10 10.10 0 -7 -30 -8.20 4.90 0 -7 30 -0.50 5.90 0 7 -30 0.50 8.20 -1 -7 -30 7.40 6.30 1 -7 30 7.40 6.80 -1 7 -30 14.50 10.00 2 0 -31 3.20 8.90 1 0 -31 -7.30 7.00 0 0 -31 -5.40 6.50 -1 0 -31 -0.20 6.80 -2 0 -31 -7.40 6.70 2 -1 -31 -1.70 6.20 2 1 -31 2.20 7.40 1 -1 -31 11.70 7.80 1 1 -31 -5.20 5.80 0 -1 -31 -1.60 6.30 0 1 -31 -1.80 7.60 -1 -1 -31 -5.50 6.90 -1 1 -31 8.90 7.40 -2 -1 -31 6.40 7.30 -2 1 -31 5.50 7.10 2 -2 -31 -3.90 6.30 2 2 -31 9.50 8.10 1 -2 -31 13.40 7.90 1 2 -31 -9.30 6.90 0 -2 -31 5.20 6.50 0 2 -31 8.50 9.40 -1 -2 -31 4.40 7.40 -1 2 -31 -0.70 7.50 -2 -2 -31 -0.70 6.50 -2 2 -31 -4.40 7.60 2 -3 -31 5.20 6.80 2 3 -31 -5.60 7.80 1 -3 -31 14.00 7.50 1 3 -31 14.60 9.70 0 -3 -31 11.30 8.40 0 3 -31 -10.20 7.00 -1 -3 -31 14.70 8.80 -1 3 -31 1.20 10.10 -2 -3 -31 16.00 9.30 -2 3 -31 8.00 8.90 1 -4 -31 19.60 9.50 1 4 -31 8.70 8.00 0 -4 -31 -1.20 7.00 0 4 -31 16.50 10.30 -1 -4 -31 -0.50 6.60 -1 4 -31 0.40 7.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 59877 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C001 C 0.52709(13) 0.31174(8) 0.64270(7) 0.0429(4) Uani 1 1 d . . . . . C002 C 0.65183(13) 0.56515(8) 0.53667(7) 0.0435(4) Uani 1 1 d . . . . . C003 C 0.53831(14) 0.23332(8) 0.66544(7) 0.0458(4) Uani 1 1 d . . . . . C004 C 0.64561(13) 0.42906(8) 0.52460(7) 0.0450(4) Uani 1 1 d . . . . . H004 H 0.653896 0.387190 0.500964 0.054 Uiso 1 1 calc R U . . . C005 C 0.41970(14) 0.34549(8) 0.67284(6) 0.0433(4) Uani 1 1 d . . . . . C006 C 0.73418(14) 0.67295(7) 0.47454(7) 0.0437(4) Uani 1 1 d . . . . . C007 C 0.66211(14) 0.50100(8) 0.50255(7) 0.0456(4) Uani 1 1 d . . . . . H007 H 0.680365 0.506664 0.464336 0.055 Uiso 1 1 calc R U . . . C008 C 0.84577(14) 0.64405(8) 0.44419(7) 0.0452(4) Uani 1 1 d . . . . . C009 C 0.61686(13) 0.41787(8) 0.58142(7) 0.0438(4) Uani 1 1 d . . . . . C00A C 0.71458(14) 0.75054(8) 0.45190(7) 0.0462(4) Uani 1 1 d . . . . . C00B C 0.37505(15) 0.29191(9) 0.71226(7) 0.0484(4) Uani 1 1 d . . . . . C00C C 0.80325(15) 0.76602(8) 0.41016(7) 0.0501(4) Uani 1 1 d . . . . . C00D C 0.60426(14) 0.34012(8) 0.60305(7) 0.0475(4) Uani 1 1 d . . . . . H00D H 0.657921 0.304926 0.586877 0.057 Uiso 1 1 calc R U . . . C00E C 0.45076(15) 0.22299(8) 0.70823(7) 0.0486(4) Uani 1 1 d . . . . . C00F C 0.66001(14) 0.64252(8) 0.51422(7) 0.0479(4) Uani 1 1 d . . . . . H00F H 0.604098 0.676500 0.530251 0.058 Uiso 1 1 calc R U . . . C00G C 0.62258(15) 0.55390(8) 0.59355(7) 0.0510(4) Uani 1 1 d . . . . . H00G H 0.612875 0.595844 0.617009 0.061 Uiso 1 1 calc R U . . . C00H C 0.88649(15) 0.70031(8) 0.40589(7) 0.0496(4) Uani 1 1 d . . . . . C00I C 0.60768(15) 0.48215(8) 0.61590(7) 0.0506(4) Uani 1 1 d . . . . . H00I H 0.591366 0.476451 0.654294 0.061 Uiso 1 1 calc R U . . . C00J C 0.35601(16) 0.41356(9) 0.66651(7) 0.0529(4) Uani 1 1 d . . . . . H00J H 0.382528 0.449338 0.640244 0.063 Uiso 1 1 calc R U . . . C00K C 0.91406(15) 0.57753(8) 0.44928(8) 0.0524(4) Uani 1 1 d . . . . . H00K H 0.889891 0.540271 0.474867 0.063 Uiso 1 1 calc R U . . . C00L C 0.62194(17) 0.80295(8) 0.46415(8) 0.0561(4) Uani 1 1 d . . . . . H00L H 0.562581 0.792777 0.491694 0.067 Uiso 1 1 calc R U . . . C00M C 0.62016(16) 0.17520(9) 0.65198(8) 0.0562(4) Uani 1 1 d . . . . . H00M H 0.678473 0.181435 0.623342 0.067 Uiso 1 1 calc R U . . . C00N C 0.80046(19) 0.83418(9) 0.38049(8) 0.0625(5) Uani 1 1 d . . . . . H00N H 0.859020 0.844851 0.352698 0.075 Uiso 1 1 calc R U . . . C00O C 0.27164(17) 0.30673(11) 0.74496(8) 0.0633(5) Uani 1 1 d . . . . . H00O H 0.243305 0.271178 0.771009 0.076 Uiso 1 1 calc R U . . . C00P C 0.62006(18) 0.87037(9) 0.43454(8) 0.0636(5) Uani 1 1 d . . . . . H00P H 0.558753 0.906048 0.442274 0.076 Uiso 1 1 calc R U . . . C00Q C 0.25250(18) 0.42754(10) 0.69980(8) 0.0634(5) Uani 1 1 d . . . . . H00Q H 0.210350 0.473295 0.695910 0.076 Uiso 1 1 calc R U . . . C00R C 0.44435(18) 0.15514(10) 0.73815(8) 0.0635(5) Uani 1 1 d . . . . . H00R H 0.385828 0.148390 0.766631 0.076 Uiso 1 1 calc R U . . . C00S C 0.99038(17) 0.68889(10) 0.37241(8) 0.0633(5) Uani 1 1 d . . . . . H00S H 1.015761 0.725905 0.346874 0.076 Uiso 1 1 calc R U . . . C00T C 0.7077(2) 0.88558(9) 0.39367(8) 0.0675(6) Uani 1 1 d . . . . . H00T H 0.704496 0.931572 0.374442 0.081 Uiso 1 1 calc R U . . . C00U C 0.52698(19) 0.09805(10) 0.72456(9) 0.0706(6) Uani 1 1 d . . . . . H00U H 0.524424 0.052466 0.744342 0.085 Uiso 1 1 calc R U . . . C00V C 0.61347(18) 0.10776(10) 0.68193(9) 0.0660(5) Uani 1 1 d . . . . . H00V H 0.667890 0.068476 0.673251 0.079 Uiso 1 1 calc R U . . . C00W C 1.01879(16) 0.56710(10) 0.41583(9) 0.0637(5) Uani 1 1 d . . . . . H00W H 1.064710 0.522655 0.419311 0.076 Uiso 1 1 calc R U . . . C00X C 1.05573(18) 0.62184(11) 0.37745(9) 0.0698(5) Uani 1 1 d . . . . . H00X H 1.125084 0.613423 0.354874 0.084 Uiso 1 1 calc R U . . . C00Y C 0.21106(18) 0.37509(11) 0.73839(8) 0.0680(5) Uani 1 1 d . . . . . H00Y H 0.141491 0.385784 0.760282 0.082 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C001 0.0459(8) 0.0415(7) 0.0413(9) 0.0028(6) -0.0051(7) -0.0076(6) C002 0.0411(8) 0.0391(7) 0.0504(10) 0.0011(6) 0.0046(7) -0.0037(6) C003 0.0491(8) 0.0416(8) 0.0465(9) 0.0035(6) -0.0065(7) -0.0101(6) C004 0.0453(8) 0.0371(7) 0.0525(10) -0.0022(6) 0.0087(7) -0.0025(6) C005 0.0453(8) 0.0461(8) 0.0385(9) 0.0025(6) -0.0027(6) -0.0091(6) C006 0.0490(8) 0.0335(7) 0.0486(9) 0.0008(6) -0.0049(7) -0.0039(6) C007 0.0482(8) 0.0441(8) 0.0446(10) 0.0033(6) 0.0080(7) -0.0042(6) C008 0.0470(8) 0.0385(7) 0.0499(10) 0.0014(6) -0.0026(7) -0.0078(6) C009 0.0407(8) 0.0427(7) 0.0478(10) 0.0035(6) 0.0043(7) -0.0049(6) C00A 0.0556(9) 0.0344(7) 0.0487(10) -0.0003(6) -0.0098(7) -0.0068(6) C00B 0.0514(9) 0.0523(9) 0.0414(9) 0.0049(7) -0.0013(7) -0.0097(7) C00C 0.0610(10) 0.0399(7) 0.0495(10) 0.0035(7) -0.0101(8) -0.0108(7) C00D 0.0499(9) 0.0412(8) 0.0514(10) 0.0021(7) 0.0031(7) -0.0045(6) C00E 0.0538(9) 0.0462(8) 0.0458(10) 0.0064(7) -0.0066(7) -0.0107(7) C00F 0.0498(9) 0.0381(7) 0.0559(10) -0.0002(7) 0.0032(8) -0.0004(6) C00G 0.0579(10) 0.0433(8) 0.0518(10) -0.0045(7) 0.0067(8) -0.0081(7) C00H 0.0554(9) 0.0447(8) 0.0487(10) 0.0020(7) -0.0036(8) -0.0115(7) C00I 0.0605(10) 0.0502(8) 0.0411(9) 0.0011(7) 0.0066(8) -0.0114(7) C00J 0.0565(10) 0.0519(9) 0.0501(10) 0.0085(7) 0.0011(8) -0.0021(7) C00K 0.0491(9) 0.0428(8) 0.0652(12) 0.0063(7) 0.0017(8) -0.0032(6) C00L 0.0648(10) 0.0383(8) 0.0651(12) -0.0027(7) -0.0090(8) -0.0007(7) C00M 0.0580(10) 0.0475(9) 0.0632(12) 0.0013(8) -0.0027(8) -0.0037(7) C00N 0.0840(13) 0.0481(9) 0.0555(11) 0.0093(8) -0.0127(10) -0.0184(9) C00O 0.0662(11) 0.0694(11) 0.0542(11) 0.0136(9) 0.0113(9) -0.0070(9) C00P 0.0797(13) 0.0373(8) 0.0739(14) -0.0015(8) -0.0224(11) 0.0025(8) C00Q 0.0627(11) 0.0635(11) 0.0641(12) 0.0057(9) 0.0069(9) 0.0084(8) C00R 0.0740(12) 0.0576(10) 0.0589(12) 0.0172(8) -0.0007(10) -0.0125(9) C00S 0.0646(11) 0.0639(11) 0.0614(12) 0.0094(9) 0.0088(9) -0.0142(9) C00T 0.0988(15) 0.0367(8) 0.0669(13) 0.0085(8) -0.0310(12) -0.0057(9) C00U 0.0850(14) 0.0498(10) 0.0771(14) 0.0216(9) -0.0089(11) -0.0067(9) C00V 0.0695(12) 0.0475(9) 0.0811(14) 0.0068(9) -0.0099(11) 0.0001(8) C00W 0.0534(10) 0.0571(10) 0.0807(14) 0.0026(9) 0.0054(10) 0.0026(8) C00X 0.0566(11) 0.0751(12) 0.0776(14) 0.0014(10) 0.0152(10) -0.0043(9) C00Y 0.0641(11) 0.0779(13) 0.0620(13) 0.0058(10) 0.0175(9) 0.0017(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00D C001 C005 131.75(14) . . ? C00D C001 C003 123.05(14) . . ? C005 C001 C003 105.20(12) . . ? C007 C002 C00G 117.42(13) . . ? C007 C002 C00F 122.72(14) . . ? C00G C002 C00F 119.65(14) . . ? C00M C003 C00E 119.95(14) . . ? C00M C003 C001 130.84(15) . . ? C00E C003 C001 109.17(14) . . ? C007 C004 C009 121.49(14) . . ? C007 C004 H004 119.3 . . ? C009 C004 H004 119.3 . . ? C00J C005 C00B 118.72(15) . . ? C00J C005 C001 132.78(14) . . ? C00B C005 C001 108.35(13) . . ? C00F C006 C00A 122.35(14) . . ? C00F C006 C008 132.81(13) . . ? C00A C006 C008 104.84(13) . . ? C004 C007 C002 121.04(15) . . ? C004 C007 H007 119.5 . . ? C002 C007 H007 119.5 . . ? C00K C008 C00H 118.91(15) . . ? C00K C008 C006 132.38(14) . . ? C00H C008 C006 108.63(13) . . ? C004 C009 C00I 117.59(13) . . ? C004 C009 C00D 119.25(13) . . ? C00I C009 C00D 123.08(15) . . ? C00L C00A C00C 120.46(14) . . ? C00L C00A C006 129.74(16) . . ? C00C C00A C006 109.69(14) . . ? C00O C00B C005 121.20(16) . . ? C00O C00B C00E 129.93(15) . . ? C005 C00B C00E 108.78(14) . . ? C00N C00C C00A 120.59(16) . . ? C00N C00C C00H 131.27(17) . . ? C00A C00C C00H 108.14(13) . . ? C001 C00D C009 130.14(14) . . ? C001 C00D H00D 114.9 . . ? C009 C00D H00D 114.9 . . ? C00R C00E C003 120.97(16) . . ? C00R C00E C00B 130.65(16) . . ? C003 C00E C00B 108.37(13) . . ? C006 C00F C002 131.28(14) . . ? C006 C00F H00F 114.4 . . ? C002 C00F H00F 114.4 . . ? C00I C00G C002 121.71(14) . . ? C00I C00G H00G 119.1 . . ? C002 C00G H00G 119.1 . . ? C00S C00H C008 121.01(15) . . ? C00S C00H C00C 130.33(15) . . ? C008 C00H C00C 108.66(14) . . ? C00G C00I C009 120.71(15) . . ? C00G C00I H00I 119.6 . . ? C009 C00I H00I 119.6 . . ? C00Q C00J C005 119.27(15) . . ? C00Q C00J H00J 120.4 . . ? C005 C00J H00J 120.4 . . ? C008 C00K C00W 119.48(16) . . ? C008 C00K H00K 120.3 . . ? C00W C00K H00K 120.3 . . ? C00P C00L C00A 118.50(18) . . ? C00P C00L H00L 120.8 . . ? C00A C00L H00L 120.8 . . ? C00V C00M C003 118.86(17) . . ? C00V C00M H00M 120.6 . . ? C003 C00M H00M 120.6 . . ? C00T C00N C00C 117.84(18) . . ? C00T C00N H00N 121.1 . . ? C00C C00N H00N 121.1 . . ? C00Y C00O C00B 118.94(16) . . ? C00Y C00O H00O 120.5 . . ? C00B C00O H00O 120.5 . . ? C00T C00P C00L 120.92(17) . . ? C00T C00P H00P 119.5 . . ? C00L C00P H00P 119.5 . . ? C00Y C00Q C00J 121.26(17) . . ? C00Y C00Q H00Q 119.4 . . ? C00J C00Q H00Q 119.4 . . ? C00U C00R C00E 118.41(18) . . ? C00U C00R H00R 120.8 . . ? C00E C00R H00R 120.8 . . ? C00X C00S C00H 119.13(17) . . ? C00X C00S H00S 120.4 . . ? C00H C00S H00S 120.4 . . ? C00P C00T C00N 121.69(16) . . ? C00P C00T H00T 119.2 . . ? C00N C00T H00T 119.2 . . ? C00R C00U C00V 120.89(17) . . ? C00R C00U H00U 119.6 . . ? C00V C00U H00U 119.6 . . ? C00U C00V C00M 120.91(18) . . ? C00U C00V H00V 119.5 . . ? C00M C00V H00V 119.5 . . ? C00X C00W C00K 120.97(17) . . ? C00X C00W H00W 119.5 . . ? C00K C00W H00W 119.5 . . ? C00S C00X C00W 120.46(18) . . ? C00S C00X H00X 119.8 . . ? C00W C00X H00X 119.8 . . ? C00Q C00Y C00O 120.60(17) . . ? C00Q C00Y H00Y 119.7 . . ? C00O C00Y H00Y 119.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C001 C00D 1.349(2) . ? C001 C005 1.483(2) . ? C001 C003 1.488(2) . ? C002 C007 1.393(2) . ? C002 C00G 1.396(2) . ? C002 C00F 1.4657(19) . ? C003 C00M 1.388(2) . ? C003 C00E 1.395(2) . ? C004 C007 1.3823(19) . ? C004 C009 1.393(2) . ? C004 H004 0.9300 . ? C005 C00J 1.390(2) . ? C005 C00B 1.411(2) . ? C006 C00F 1.344(2) . ? C006 C00A 1.4835(19) . ? C006 C008 1.489(2) . ? C007 H007 0.9300 . ? C008 C00K 1.389(2) . ? C008 C00H 1.412(2) . ? C009 C00I 1.399(2) . ? C009 C00D 1.4689(19) . ? C00A C00L 1.390(2) . ? C00A C00C 1.400(2) . ? C00B C00O 1.381(2) . ? C00B C00E 1.466(2) . ? C00C C00N 1.391(2) . ? C00C C00H 1.468(2) . ? C00D H00D 0.9300 . ? C00E C00R 1.391(2) . ? C00F H00F 0.9300 . ? C00G C00I 1.380(2) . ? C00G H00G 0.9300 . ? C00H C00S 1.385(2) . ? C00I H00I 0.9300 . ? C00J C00Q 1.387(2) . ? C00J H00J 0.9300 . ? C00K C00W 1.390(2) . ? C00K H00K 0.9300 . ? C00L C00P 1.379(2) . ? C00L H00L 0.9300 . ? C00M C00V 1.385(2) . ? C00M H00M 0.9300 . ? C00N C00T 1.384(3) . ? C00N H00N 0.9300 . ? C00O C00Y 1.379(2) . ? C00O H00O 0.9300 . ? C00P C00T 1.377(3) . ? C00P H00P 0.9300 . ? C00Q C00Y 1.373(2) . ? C00Q H00Q 0.9300 . ? C00R C00U 1.381(3) . ? C00R H00R 0.9300 . ? C00S C00X 1.381(3) . ? C00S H00S 0.9300 . ? C00T H00T 0.9300 . ? C00U C00V 1.383(3) . ? C00U H00U 0.9300 . ? C00V H00V 0.9300 . ? C00W C00X 1.383(3) . ? C00W H00W 0.9300 . ? C00X H00X 0.9300 . ? C00Y H00Y 0.9300 . ?