#------------------------------------------------------------------------------ #$Date: 2021-09-03 22:47:39 +0300 (Fri, 03 Sep 2021) $ #$Revision: 268427 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519001.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519001 loop_ _publ_author_name 'Lohrey, Trevor D.' 'Cusumano, Alexander Q.' 'Goddard, William A.' 'Stoltz, Brian M.' _publ_section_title ; Identifying the Imperative Role of Metal--Olefin Interactions in Catalytic C--O Reductive Elimination from Nickel(II) ; _journal_issue 16 _journal_name_full 'ACS Catalysis' _journal_page_first 10208 _journal_page_last 10222 _journal_paper_doi 10.1021/acscatal.1c02790 _journal_volume 11 _journal_year 2021 _chemical_formula_moiety 'C36 H66 I Ni P2' _chemical_formula_sum 'C36 H66 I Ni P2' _chemical_formula_weight 746.43 _chemical_name_common 'NiI(PCy3)2 diethyl ether solvate' _space_group_crystal_system trigonal _space_group_IT_number 167 _space_group_name_Hall '-R 3 2"c' _space_group_name_H-M_alt 'R -3 c :H' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 18 _cell_length_a 29.259(3) _cell_length_b 29.259(3) _cell_length_c 23.165(2) _cell_measurement_reflns_used 9813 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 26.43 _cell_measurement_theta_min 2.30 _cell_volume 17174(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics ORTEP-32 _computing_publication_material WinGX _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution SHELXT _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0742 _diffrn_reflns_av_unetI/netI 0.0276 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 36 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_k_max 36 _diffrn_reflns_limit_k_min -36 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 85598 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 26.540 _diffrn_reflns_theta_min 1.933 _exptl_absorpt_coefficient_mu 1.423 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.5248 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.299 _exptl_crystal_description rod _exptl_crystal_F_000 7074 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.040 _exptl_crystal_size_min 0.030 _refine_diff_density_max 0.906 _refine_diff_density_min -0.610 _refine_diff_density_rms 0.087 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 182 _refine_ls_number_reflns 3978 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.067 _refine_ls_R_factor_all 0.0473 _refine_ls_R_factor_gt 0.0320 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0450P)^2^+47.1573P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0784 _refine_ls_wR_factor_ref 0.0861 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3186 _reflns_number_total 3978 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c02790_si_002.cif _cod_data_source_block PCy32NiI_2078295 _cod_depositor_comments ; The following automatic conversions were performed: data item '_atom_sites_solution_secondary' value 'diffmap' was changed to 'difmap'. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_original_cell_volume 17175(4) _cod_database_code 4519001 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL shelxt_a.res in R-3c CELL 0.71073 29.2592 29.2592 23.1653 90.000 90.000 120.000 ZERR 18.00 0.0031 0.0031 0.0021 0.000 0.000 0.000 LATT 3 SYMM - Y, X - Y, Z SYMM - X + Y, - X, Z SYMM Y, X, 1/2 - Z SYMM X - Y, - Y, 1/2 - Z SYMM - X, - X + Y, 1/2 - Z SFAC C H P NI I UNIT 648 1188 36 18 18 MERG 2 OMIT -1 2 0 OMIT 0 3 0 OMIT -3 6 0 ABIN FMAP 2 PLAN 20 ACTA 50.00 BOND $H LIST 4 WPDB -2 L.S. 5 0 15 TEMP -173.13 WGHT 0.045000 47.157299 FVAR 0.02020 C1 1 0.407883 0.329213 0.438262 11.00000 0.01461 0.01310 = 0.01885 -0.00177 -0.00045 0.00614 AFIX 13 H1 2 0.381415 0.329793 0.411413 11.00000 -1.20000 AFIX 0 C2 1 0.386339 0.327597 0.499269 11.00000 0.02295 0.01597 = 0.02009 0.00029 0.00349 0.00815 AFIX 23 H2A 2 0.352728 0.294057 0.504555 11.00000 -1.20000 H2B 2 0.411816 0.328877 0.528257 11.00000 -1.20000 AFIX 0 C3 1 0.377054 0.373938 0.508859 11.00000 0.02919 0.02276 = 0.02184 -0.00022 0.00685 0.01425 AFIX 23 H3A 2 0.349485 0.371125 0.481935 11.00000 -1.20000 H3B 2 0.364386 0.372732 0.548764 11.00000 -1.20000 AFIX 0 C4 1 0.427745 0.426163 0.499085 11.00000 0.02870 0.01656 = 0.02472 -0.00239 0.00023 0.01336 AFIX 23 H4A 2 0.420577 0.455623 0.503873 11.00000 -1.20000 H4B 2 0.454283 0.430368 0.528286 11.00000 -1.20000 AFIX 0 C5 1 0.449626 0.428423 0.439052 11.00000 0.02139 0.01526 = 0.02751 0.00225 0.00414 0.00783 AFIX 23 H5A 2 0.483397 0.461930 0.434462 11.00000 -1.20000 H5B 2 0.424558 0.427755 0.409899 11.00000 -1.20000 AFIX 0 C6 1 0.458757 0.381956 0.428647 11.00000 0.02207 0.01597 = 0.02720 0.00149 0.00581 0.00802 AFIX 23 H6A 2 0.486449 0.384581 0.455255 11.00000 -1.20000 H6B 2 0.471283 0.383480 0.388611 11.00000 -1.20000 AFIX 0 C7 1 0.450569 0.286837 0.354951 11.00000 0.01774 0.01374 = 0.01560 -0.00064 0.00091 0.00754 AFIX 13 H7 2 0.483382 0.320941 0.363643 11.00000 -1.20000 AFIX 0 C8 1 0.423266 0.296640 0.303688 11.00000 0.01891 0.01403 = 0.01829 0.00048 -0.00030 0.00708 AFIX 23 H8A 2 0.390213 0.263649 0.294374 11.00000 -1.20000 H8B 2 0.413936 0.323710 0.314439 11.00000 -1.20000 AFIX 0 C9 1 0.459037 0.315195 0.250519 11.00000 0.02115 0.01883 = 0.01651 0.00099 0.00060 0.00850 AFIX 23 H9A 2 0.439858 0.319549 0.217714 11.00000 -1.20000 H9B 2 0.490522 0.349923 0.258598 11.00000 -1.20000 AFIX 0 C10 1 0.476366 0.275897 0.234262 11.00000 0.02570 0.02068 = 0.02170 -0.00010 0.00565 0.01026 AFIX 23 H10A 2 0.501257 0.289911 0.201380 11.00000 -1.20000 H10B 2 0.445250 0.242373 0.221894 11.00000 -1.20000 AFIX 0 C11 1 0.502973 0.265350 0.284941 11.00000 0.02773 0.02158 = 0.02218 0.00159 0.00686 0.01519 AFIX 23 H11A 2 0.536262 0.298039 0.294417 11.00000 -1.20000 H11B 2 0.511873 0.238046 0.273851 11.00000 -1.20000 AFIX 0 C12 1 0.467415 0.246842 0.338098 11.00000 0.02349 0.01984 = 0.01874 0.00048 0.00175 0.01384 AFIX 23 H12A 2 0.486521 0.242097 0.370709 11.00000 -1.20000 H12B 2 0.435694 0.212317 0.329934 11.00000 -1.20000 AFIX 0 C13 1 0.447958 0.254159 0.473418 11.00000 0.01966 0.01543 = 0.01910 -0.00111 -0.00134 0.00901 AFIX 13 H13 2 0.451058 0.224653 0.455717 11.00000 -1.20000 AFIX 0 C14 1 0.419185 0.231282 0.530704 11.00000 0.02845 0.02392 = 0.01978 0.00345 0.00100 0.01356 AFIX 23 H14A 2 0.418075 0.259370 0.553421 11.00000 -1.20000 H14B 2 0.382421 0.203238 0.522938 11.00000 -1.20000 AFIX 0 C15 1 0.447663 0.208405 0.565258 11.00000 0.03992 0.02822 = 0.02091 0.00349 0.00047 0.01925 AFIX 23 H15A 2 0.429521 0.194887 0.602688 11.00000 -1.20000 H15B 2 0.446205 0.178452 0.543776 11.00000 -1.20000 AFIX 0 C16 1 0.505082 0.250049 0.576036 11.00000 0.04255 0.03200 = 0.02584 -0.00473 -0.00866 0.02556 AFIX 23 H16A 2 0.523124 0.233520 0.595924 11.00000 -1.20000 H16B 2 0.506425 0.277747 0.601705 11.00000 -1.20000 AFIX 0 C17 1 0.534161 0.275384 0.519888 11.00000 0.02805 0.03138 = 0.02704 -0.00174 -0.00949 0.01701 AFIX 23 H17A 2 0.537486 0.248774 0.496693 11.00000 -1.20000 H17B 2 0.570170 0.304365 0.528986 11.00000 -1.20000 AFIX 0 C18 1 0.505234 0.297257 0.484466 11.00000 0.02281 0.01866 = 0.02669 -0.00004 -0.00705 0.00766 AFIX 23 H18A 2 0.523565 0.310844 0.447141 11.00000 -1.20000 H18B 2 0.505731 0.326949 0.505517 11.00000 -1.20000 AFIX 0 P1 3 0.408568 0.267483 0.420495 11.00000 0.01534 0.01304 = 0.01550 -0.00028 0.00081 0.00688 NI1 4 0.333333 0.191025 0.416667 10.50000 0.01409 0.01320 = 0.02203 -0.00007 -0.00014 0.00704 I1 5 0.333333 0.106125 0.416667 10.50000 0.02133 0.01541 = 0.04111 0.00039 0.00078 0.01066 HKLF 4 REM shelxt_a.res in R-3c REM R1 = 0.0320 for 3186 Fo > 4sig(Fo) and 0.0473 for all 3978 data REM 182 parameters refined using 0 restraints END WGHT 0.0398 57.8438 REM Highest difference peak 0.906, deepest hole -0.610, 1-sigma level 0.087 Q1 1 0.5445 0.3333 0.5833 10.50000 0.05 0.91 Q2 1 0.5849 0.2966 0.5856 11.00000 0.05 0.66 Q3 1 0.4183 0.1902 0.4182 11.00000 0.05 0.65 Q4 1 0.5820 0.2487 0.5833 10.50000 0.05 0.61 Q5 1 0.3722 0.2259 0.4141 11.00000 0.05 0.51 Q6 1 0.4429 0.3587 0.2501 11.00000 0.05 0.44 Q7 1 0.2956 0.1437 0.4179 11.00000 0.05 0.42 Q8 1 0.3704 0.2618 0.4140 11.00000 0.05 0.39 Q9 1 0.3702 0.3020 0.4093 11.00000 0.05 0.38 Q10 1 0.5032 0.3333 0.5833 10.50000 0.05 0.38 Q11 1 0.5429 0.2468 0.5828 11.00000 0.05 0.38 Q12 1 0.4480 0.3495 0.4218 11.00000 0.05 0.37 Q13 1 0.3338 0.1480 0.3968 11.00000 0.05 0.36 Q14 1 0.4567 0.2276 0.4164 11.00000 0.05 0.35 Q15 1 0.5927 0.2749 0.6230 11.00000 0.05 0.34 Q16 1 0.4093 0.3020 0.4266 11.00000 0.05 0.34 Q17 1 0.4348 0.3557 0.4424 11.00000 0.05 0.33 Q18 1 0.4289 0.2591 0.4585 11.00000 0.05 0.33 Q19 1 0.2955 0.0630 0.4176 11.00000 0.05 0.32 Q20 1 0.5828 0.2936 0.4922 11.00000 0.05 0.31 ; _shelx_res_checksum 10577 _shelx_hkl_file ; -2 1 0 0.15 2.60 1 1 0 2.10 2.72 -1 2 0 2.16 2.52 -1 -1 0 -1.66 2.61 2 -1 0 9.83 2.95 3 0 0 46.45 2.73 3 0 0 47.60 2.71 0 -3 0 48.87 2.73 -3 3 0 49.71 2.73 0 -3 0 50.91 2.73 3 0 0 49.46 2.72 0 -3 0 47.16 2.72 -3 3 0 48.87 2.72 -3 3 0 48.33 2.74 0 3 0 49.12 2.72 0 3 0 45.55 2.72 3 -3 0 47.00 2.73 3 -3 0 46.60 2.71 -3 0 0 45.79 2.71 -3 0 0 44.36 2.71 -4 2 0 70.61 4.13 2 2 0 70.25 4.13 -4 2 0 75.71 4.12 2 -4 0 77.45 4.13 2 -4 0 71.68 4.14 2 2 0 73.75 4.14 -4 2 0 71.25 4.15 2 2 0 71.69 4.13 2 -4 0 72.72 4.14 -2 -2 0 75.03 4.15 -2 -2 0 73.15 4.13 4 -2 0 69.21 4.13 4 -2 0 77.08 4.12 -2 4 0 71.82 4.13 -2 4 0 73.28 4.14 -2 4 0 78.30 4.13 4 -2 0 72.56 4.14 4 -5 0 0.32 0.40 1 4 0 0.16 0.36 4 -5 0 0.22 0.37 -5 1 0 0.46 0.36 1 4 0 -0.02 0.34 -5 1 0 0.39 0.37 1 4 0 0.34 0.34 1 4 0 0.17 0.33 4 -5 0 0.39 0.37 5 -1 0 0.43 0.36 -4 5 0 0.12 0.41 -1 -4 0 0.43 0.40 5 -1 0 0.42 0.34 -4 5 0 0.74 0.38 -4 5 0 0.33 0.39 -1 -4 0 0.35 0.39 -1 -4 0 0.28 0.40 5 -1 0 0.17 0.34 -1 -4 0 -0.61 0.43 1 -5 0 0.06 0.38 -5 4 0 0.05 0.39 1 -5 0 -0.06 0.39 -5 4 0 0.77 0.41 4 1 0 0.33 0.33 -5 4 0 -0.04 0.37 4 1 0 0.32 0.38 4 1 0 0.29 0.34 1 -5 0 0.18 0.40 5 -4 0 0.37 0.36 -4 -1 0 0.27 0.37 -1 5 0 0.10 0.35 -1 5 0 0.19 0.37 -4 -1 0 0.51 0.43 -4 -1 0 0.26 0.41 5 -4 0 0.16 0.36 -1 5 0 0.28 0.32 5 -4 0 0.06 0.38 3 -6 0 3.46 0.54 3 3 0 2.97 0.50 -6 3 0 3.50 0.57 3 -6 0 3.04 0.51 3 3 0 1.93 0.46 3 -6 0 2.54 0.47 -6 3 0 2.55 0.50 3 3 0 1.87 0.45 3 3 0 2.21 0.49 -6 3 0 2.39 0.47 -3 -3 0 1.92 0.52 -3 6 0 3.13 0.55 6 -3 0 4.51 0.70 -3 -3 0 2.51 0.58 6 -3 0 3.23 0.53 -3 6 0 3.03 0.51 -3 -3 0 1.80 0.50 -3 -3 0 2.25 0.51 6 -3 0 2.68 0.48 0 -6 0 18.70 1.38 6 0 0 18.49 1.37 6 0 0 18.01 1.31 0 -6 0 19.59 1.39 -6 6 0 17.58 1.31 6 0 0 18.92 1.39 -6 6 0 17.74 1.44 -6 6 0 17.40 1.45 6 0 0 16.94 1.35 0 6 0 17.97 1.33 0 6 0 17.75 1.36 -6 0 0 17.06 1.30 6 -6 0 15.65 1.32 6 -6 0 16.75 1.34 6 -6 0 16.46 1.43 0 6 0 19.46 1.30 -7 2 0 291.94 16.58 2 5 0 290.24 16.59 5 -7 0 304.52 16.59 2 5 0 287.70 16.60 5 -7 0 311.01 16.61 -7 2 0 296.99 16.61 5 -7 0 306.51 16.62 2 5 0 321.75 16.61 2 5 0 282.71 16.59 -5 7 0 295.94 16.58 7 -2 0 288.87 16.61 -5 7 0 297.30 16.61 7 -2 0 275.03 16.57 -5 7 0 305.73 16.60 -2 -5 0 295.90 16.60 -2 -5 0 311.88 16.60 -2 -5 0 298.43 16.62 -2 -5 0 317.56 16.62 7 -2 0 303.18 16.60 5 2 0 312.74 16.61 5 2 0 270.01 16.60 5 2 0 296.65 16.59 2 -7 0 306.91 16.62 2 -7 0 308.75 16.60 -7 5 0 319.94 16.59 2 -7 0 315.02 16.63 -7 5 0 295.18 16.61 -7 5 0 305.90 16.62 5 2 0 275.11 16.59 -5 -2 0 280.65 16.69 -5 -2 0 307.76 16.60 -2 7 0 310.97 16.60 -2 7 0 294.55 16.58 -5 -2 0 289.11 16.60 -2 7 0 289.44 16.60 7 -5 0 286.18 16.59 7 -5 0 305.14 16.61 7 -5 0 285.66 16.49 -5 -2 0 312.71 16.63 7 -5 0 312.06 16.59 -8 1 0 117.61 6.27 1 7 0 105.73 6.25 7 -8 0 114.29 6.30 7 -8 0 109.94 6.27 1 7 0 114.69 6.27 7 -8 0 108.22 6.25 1 7 0 102.92 6.39 1 7 0 106.12 6.25 1 7 0 104.24 6.25 -8 1 0 115.79 6.25 -7 8 0 110.22 6.25 -7 8 0 110.97 6.27 8 -1 0 104.70 6.25 8 -1 0 112.63 6.25 -1 -7 0 114.23 6.29 8 -1 0 110.09 6.29 -7 8 0 106.73 6.30 4 4 0 91.23 5.68 4 4 0 99.09 5.68 4 -8 0 101.59 5.70 4 4 0 94.96 5.68 4 -8 0 106.76 5.72 4 4 0 95.94 5.67 -8 4 0 99.97 5.66 4 -8 0 100.91 5.67 -8 4 0 97.84 5.70 -8 4 0 107.89 5.70 -4 8 0 103.31 5.68 8 -4 0 103.66 5.72 -4 8 0 96.78 5.70 -4 -4 0 96.03 5.68 -4 8 0 102.29 5.66 -4 -4 0 91.30 5.70 -4 -4 0 94.93 5.69 8 -4 0 107.19 5.70 8 -4 0 97.01 5.66 7 1 0 104.98 6.27 -8 7 0 111.72 6.30 1 -8 0 107.98 6.29 -8 7 0 106.46 6.25 7 1 0 115.66 6.26 7 1 0 109.71 6.27 1 -8 0 115.00 6.30 1 -8 0 116.97 6.28 -8 7 0 116.29 6.27 7 1 0 101.16 6.23 -7 -1 0 102.74 6.29 8 -7 0 112.21 6.30 8 -7 0 106.11 6.26 -1 8 0 108.89 6.24 -1 8 0 117.54 6.28 8 -7 0 110.78 6.25 -7 -1 0 112.28 6.28 -7 -1 0 108.54 6.29 -7 -1 0 103.14 6.24 -9 3 0 27.87 1.84 3 6 0 29.43 1.84 -9 3 0 25.22 1.85 3 6 0 29.34 1.87 3 6 0 28.19 1.83 6 -9 0 28.86 1.88 -9 3 0 25.88 1.90 3 6 0 25.73 1.81 -3 -6 0 27.15 1.93 -6 9 0 29.80 1.82 -6 9 0 26.78 1.92 -3 -6 0 28.38 1.88 -3 -6 0 24.76 1.91 -6 9 0 26.83 1.84 9 -3 0 27.56 1.88 9 -3 0 26.50 1.89 -3 -6 0 27.77 1.93 9 -3 0 23.00 1.81 6 3 0 27.91 1.89 6 3 0 28.06 1.88 -9 6 0 30.28 1.85 3 -9 0 24.09 1.93 -9 6 0 31.42 1.89 3 -9 0 26.13 1.88 6 3 0 26.85 1.86 3 -9 0 27.44 1.93 6 3 0 24.81 1.84 -9 6 0 30.04 1.95 9 -6 0 28.54 1.90 9 -6 0 27.05 1.84 9 -6 0 28.56 1.95 -6 -3 0 28.88 1.96 -6 -3 0 29.96 1.93 -6 -3 0 28.41 1.89 -3 9 0 22.80 1.98 -3 9 0 26.80 1.81 -3 9 0 26.48 1.84 -6 -3 0 23.74 1.92 -9 9 0 333.29 18.28 9 0 0 317.82 18.25 9 0 0 323.35 18.26 0 -9 0 330.46 18.28 9 0 0 333.27 18.25 -9 9 0 353.75 18.25 -9 9 0 332.05 18.26 0 -9 0 318.16 18.26 9 0 0 337.09 18.29 9 0 0 321.80 18.24 0 9 0 326.23 18.24 0 9 0 320.69 18.25 0 9 0 342.87 18.24 9 -9 0 325.66 18.27 -9 0 0 322.16 18.23 0 9 0 334.67 18.28 -9 0 0 346.67 18.27 0 9 0 317.84 18.25 9 -9 0 315.20 18.24 9 -9 0 310.27 18.28 8 -10 0 -0.10 0.55 8 -10 0 0.23 0.53 2 8 0 -0.29 0.43 -10 2 0 -0.81 0.48 2 8 0 -0.37 0.47 2 8 0 -0.20 0.42 2 8 0 0.16 0.48 -10 2 0 -0.16 0.55 -10 2 0 0.05 0.55 2 8 0 -0.51 0.42 8 -10 0 0.54 0.52 -8 10 0 0.08 0.51 -2 -8 0 -0.32 0.59 10 -2 0 -0.27 0.45 10 -2 0 -0.15 0.48 -2 -8 0 -0.23 0.57 -8 10 0 -0.34 0.46 -8 10 0 -0.06 0.52 10 -2 0 -0.52 0.45 5 5 0 19.37 1.61 5 -10 0 24.44 1.69 5 -10 0 25.26 1.74 5 5 0 21.33 1.67 -10 5 0 23.20 1.61 5 5 0 21.15 1.67 -10 5 0 25.40 1.71 -10 5 0 23.93 1.72 5 -10 0 22.87 1.67 5 5 0 19.26 1.62 -5 -5 0 22.59 1.67 10 -5 0 24.15 1.74 -5 10 0 23.48 1.59 -5 10 0 21.78 1.81 10 -5 0 22.71 1.62 -5 -5 0 20.02 1.74 -5 -5 0 21.01 1.68 10 -5 0 22.63 1.68 -5 -5 0 17.83 1.69 -5 10 0 25.97 1.66 8 2 0 0.79 0.50 2 -10 0 0.58 0.58 2 -10 0 -0.10 0.56 8 2 0 -0.14 0.44 -10 8 0 -0.04 0.51 8 2 0 -0.74 0.45 2 -10 0 -0.26 0.56 8 2 0 -0.02 0.47 -10 8 0 -0.02 0.50 -10 8 0 0.30 0.57 10 -8 0 -0.02 0.50 -2 10 0 0.16 0.45 -8 -2 0 -0.20 0.50 -2 10 0 0.08 0.43 -8 -2 0 -0.11 0.58 10 -8 0 -0.42 0.52 10 -8 0 -0.02 0.27 -8 -2 0 0.20 0.55 10 -8 0 0.06 0.53 -2 10 0 0.45 0.47 -8 -2 0 0.19 0.62 10 -11 0 68.79 4.47 1 10 0 72.31 4.44 10 -11 0 72.81 4.45 1 10 0 77.91 4.43 10 -11 0 71.56 4.51 1 10 0 74.40 4.45 -11 1 0 74.87 4.43 1 10 0 79.65 4.45 1 10 0 78.50 4.49 -11 1 0 82.61 4.49 -1 -10 0 73.76 4.49 11 -1 0 77.11 4.49 -10 11 0 66.95 4.62 11 -1 0 76.50 4.46 11 -1 0 68.67 4.43 -10 11 0 78.49 4.44 11 -1 0 81.33 4.46 -1 -10 0 76.54 4.52 -10 11 0 74.67 4.49 11 -1 0 77.36 4.45 7 -11 0 141.90 8.24 -11 4 0 145.96 8.19 4 7 0 141.41 8.18 7 -11 0 139.82 8.19 -11 4 0 153.85 8.23 4 7 0 144.11 8.21 -11 4 0 147.06 8.24 4 7 0 137.44 8.18 7 -11 0 139.91 8.21 4 7 0 151.50 8.22 -4 -7 0 143.13 8.21 -7 11 0 155.78 8.21 -7 11 0 147.21 8.18 -4 -7 0 136.88 8.22 11 -4 0 152.91 8.21 11 -4 0 150.03 8.23 -4 -7 0 145.32 8.25 11 -4 0 137.41 8.17 -4 -7 0 132.07 8.24 4 -11 0 152.21 8.39 7 4 0 144.15 8.35 7 4 0 140.73 8.32 4 -11 0 141.48 8.35 4 -11 0 149.19 8.39 7 4 0 131.01 8.32 7 4 0 144.04 8.34 -11 7 0 148.20 8.33 -11 7 0 156.69 8.36 -11 7 0 150.81 8.38 11 -7 0 146.45 8.17 -7 -4 0 150.61 8.36 -7 -4 0 133.24 8.36 -4 11 0 145.74 8.34 11 -7 0 146.03 8.35 -4 11 0 155.20 8.33 -4 11 0 151.84 8.37 -7 -4 0 150.04 8.39 -7 -4 0 144.88 8.39 11 -7 0 153.46 8.34 11 -7 0 152.68 8.39 -11 10 0 72.23 4.45 10 1 0 72.82 4.41 10 1 0 69.60 4.43 1 -11 0 76.07 4.52 10 1 0 83.44 4.46 1 -11 0 73.61 4.47 10 1 0 76.82 4.43 -11 10 0 71.73 4.49 10 1 0 75.18 4.49 -11 10 0 79.25 4.43 1 -11 0 78.00 4.52 -1 11 0 75.95 4.46 11 -10 0 68.62 4.46 -1 11 0 75.73 4.44 -10 -1 0 76.91 4.42 11 -10 0 77.12 4.27 -1 11 0 80.22 4.42 11 -10 0 71.96 4.43 11 -10 0 68.74 4.47 3 9 0 19.95 1.57 -12 3 0 19.72 1.62 -12 3 0 23.42 1.71 3 9 0 21.20 1.57 9 -12 0 20.51 1.70 9 -12 0 20.93 1.73 9 -12 0 19.02 1.61 3 9 0 22.49 1.61 -12 3 0 24.47 1.74 3 9 0 19.49 1.61 -9 12 0 20.01 2.04 -9 12 0 22.32 1.63 -9 12 0 20.23 1.57 -3 -9 0 17.52 1.72 12 -3 0 20.61 1.65 12 -3 0 18.97 1.63 12 -3 0 19.61 1.59 -3 -9 0 19.11 1.78 -12 6 0 22.05 1.79 -12 6 0 24.14 1.72 6 -12 0 18.97 1.81 6 6 0 26.67 1.75 6 6 0 25.84 1.73 -12 6 0 21.11 1.80 6 -12 0 21.08 1.77 6 -12 0 21.53 1.81 -6 12 0 22.94 1.70 -6 -6 0 25.10 1.86 12 -6 0 21.27 1.71 12 -6 0 22.06 1.84 12 -6 0 22.28 1.69 -6 12 0 22.91 1.74 -6 12 0 21.44 1.78 -6 -6 0 29.11 1.97 -6 -6 0 27.72 1.85 9 3 0 20.38 1.62 -12 9 0 20.94 1.69 9 3 0 21.89 1.62 -12 9 0 20.41 1.76 9 3 0 19.88 1.59 3 -12 0 20.73 1.74 -12 9 0 19.60 1.61 3 -12 0 20.67 1.73 9 3 0 21.65 1.64 3 -12 0 21.82 1.68 12 -9 0 21.55 1.35 -3 12 0 22.54 1.67 -9 -3 0 21.93 1.78 -9 -3 0 19.40 1.63 12 -9 0 21.38 1.72 -9 -3 0 21.08 1.73 12 -9 0 22.29 1.70 -3 12 0 22.68 1.63 -3 12 0 21.01 1.57 -9 -3 0 18.70 1.72 12 -9 0 20.25 1.63 12 0 0 68.71 4.03 -12 12 0 64.75 4.40 -12 12 0 64.76 3.99 -12 12 0 71.04 3.98 12 0 0 62.05 4.10 12 0 0 62.14 3.93 0 -12 0 62.83 4.04 12 0 0 66.56 3.95 12 0 0 69.42 4.01 12 -12 0 63.72 4.04 -12 0 0 67.34 3.97 0 12 0 62.60 3.96 0 12 0 64.81 3.96 0 12 0 67.40 3.93 -12 0 0 67.34 4.01 0 12 0 62.10 4.10 0 12 0 65.53 4.00 12 -12 0 64.89 4.00 2 11 0 121.83 6.99 -13 2 0 124.87 7.00 2 11 0 123.58 7.00 2 11 0 119.61 7.04 11 -13 0 122.49 7.07 -13 2 0 136.45 7.06 2 11 0 118.73 7.01 11 -13 0 115.26 7.02 -11 13 0 121.91 6.99 -11 13 0 119.57 7.02 13 -2 0 122.81 7.02 13 -2 0 117.98 6.99 13 -2 0 127.76 6.99 -11 13 0 117.48 7.04 13 -2 0 120.78 7.00 13 -2 0 115.45 7.02 -2 -11 0 117.14 7.05 -13 5 0 23.65 1.75 -13 5 0 21.43 1.63 5 8 0 20.39 1.63 8 -13 0 18.84 1.70 5 8 0 16.89 1.60 5 8 0 19.51 1.63 5 8 0 19.32 1.60 8 -13 0 17.67 1.66 -13 5 0 20.84 1.72 13 -5 0 19.73 1.59 -5 -8 0 19.24 1.76 -8 13 0 22.26 1.62 -8 13 0 20.14 1.70 -5 -8 0 18.65 1.78 13 -5 0 19.91 1.60 -8 13 0 21.50 1.57 -5 -8 0 18.99 1.68 13 -5 0 22.26 1.72 5 -13 0 23.00 1.73 8 5 0 19.60 1.62 8 5 0 18.63 1.60 8 5 0 19.64 1.63 -13 8 0 23.02 1.64 5 -13 0 20.71 1.70 8 5 0 22.32 1.68 -13 8 0 18.34 1.71 -13 8 0 20.04 1.73 -8 -5 0 18.75 1.74 -8 -5 0 20.05 1.69 13 -8 0 18.03 1.64 -8 -5 0 19.76 1.76 13 -8 0 21.15 1.68 -8 -5 0 18.14 1.75 13 -8 0 21.19 1.32 -5 13 0 22.19 1.64 -5 13 0 22.49 1.58 13 -8 0 20.87 1.72 -5 13 0 22.14 1.73 11 2 0 122.39 6.98 2 -13 0 123.49 7.03 11 2 0 113.69 7.02 11 2 0 124.36 7.01 -13 11 0 121.43 7.00 -13 11 0 125.93 6.98 2 -13 0 107.57 7.42 11 2 0 116.65 6.98 2 -13 0 124.31 7.07 -2 13 0 124.16 7.01 -2 13 0 128.21 6.97 13 -11 0 124.78 6.80 13 -11 0 121.56 7.04 -11 -2 0 117.04 7.01 13 -11 0 126.51 7.15 13 -11 0 116.88 7.00 -2 13 0 122.81 7.00 -11 -2 0 115.56 6.98 13 -14 0 37.86 2.64 1 13 0 35.18 2.51 1 13 0 36.63 2.56 1 13 0 37.38 2.79 13 -14 0 37.90 2.62 -14 1 0 37.65 2.53 13 -14 0 33.74 3.25 -14 1 0 40.58 2.65 1 13 0 37.48 2.49 -13 14 0 37.19 2.64 -13 14 0 40.02 2.67 14 -1 0 37.09 2.57 14 -1 0 37.17 2.55 14 -1 0 36.91 2.57 14 -1 0 39.26 2.52 -1 -13 0 35.72 2.74 14 -1 0 38.96 2.58 -13 14 0 40.18 2.54 -14 4 0 1.90 0.73 10 -14 0 1.43 0.69 4 10 0 2.63 0.71 4 10 0 2.06 0.59 -14 4 0 4.40 0.74 10 -14 0 2.02 0.74 -14 4 0 3.47 0.74 10 -14 0 3.10 0.80 4 10 0 1.57 0.58 4 10 0 1.17 0.59 -10 14 0 3.47 0.68 -4 -10 0 1.95 0.84 14 -4 0 2.99 0.67 14 -4 0 3.76 0.69 -10 14 0 2.64 0.67 -4 -10 0 1.76 0.86 14 -4 0 2.85 0.73 -10 14 0 3.94 0.72 7 -14 0 215.08 12.45 7 -14 0 223.54 12.48 7 7 0 236.46 12.45 7 7 0 211.70 12.42 -14 7 0 228.18 12.44 7 7 0 227.66 12.41 -14 7 0 224.92 12.41 -14 7 0 211.17 12.46 7 -14 0 201.54 12.54 7 7 0 196.04 12.53 -7 -7 0 220.87 12.44 14 -7 0 228.69 12.46 -7 14 0 224.61 12.43 14 -7 0 225.66 12.43 -7 14 0 225.62 12.45 -7 -7 0 213.07 12.42 -7 -7 0 194.79 12.65 14 -7 0 226.78 12.44 -7 -7 0 222.48 12.47 -7 14 0 244.37 12.42 -14 10 0 2.11 0.67 10 4 0 1.68 0.59 10 4 0 1.87 0.61 10 4 0 1.87 0.68 4 -14 0 1.64 0.68 4 -14 0 1.46 0.93 -14 10 0 1.67 0.67 10 4 0 1.17 0.62 -14 10 0 2.21 0.99 14 -10 0 1.09 0.68 14 -10 0 2.44 0.38 14 -10 0 1.99 0.65 -4 14 0 3.78 0.69 -10 -4 0 1.54 0.88 14 -10 0 2.13 0.65 -10 -4 0 1.76 0.73 -10 -4 0 1.49 0.68 -10 -4 0 2.33 0.78 13 1 0 37.34 2.54 13 1 0 39.29 2.60 -14 13 0 38.27 2.64 1 -14 0 36.80 2.79 13 1 0 38.65 2.61 1 -14 0 42.34 2.83 13 1 0 38.35 2.59 -14 13 0 37.87 2.72 -14 13 0 36.54 2.58 13 1 0 39.40 2.60 -1 14 0 40.38 2.62 -1 14 0 40.65 2.55 -13 -1 0 36.22 2.55 -1 14 0 39.87 2.61 -1 14 0 42.29 2.70 -1 14 0 39.95 2.60 14 -13 0 34.07 2.63 14 -13 0 33.64 2.63 -13 -1 0 35.78 2.67 14 -13 0 37.85 2.33 3 12 0 18.92 1.81 3 12 0 19.83 1.81 3 12 0 21.75 2.12 -15 3 0 26.86 1.98 3 12 0 18.73 1.70 -15 3 0 23.29 1.77 12 -15 0 26.57 2.30 12 -15 0 23.30 1.88 12 -15 0 20.85 1.89 3 12 0 20.70 1.78 15 -3 0 26.38 1.83 15 -3 0 24.28 1.85 -12 15 0 21.92 1.91 -3 -12 0 17.39 2.07 -12 15 0 21.60 1.72 15 -3 0 22.30 1.81 -12 15 0 23.72 1.87 9 -15 0 34.08 2.51 6 9 0 37.18 2.48 -15 6 0 34.66 2.59 6 9 0 35.30 2.49 6 9 0 37.78 2.43 -15 6 0 36.66 2.54 -15 6 0 35.61 2.46 9 -15 0 35.23 2.56 6 9 0 38.12 2.51 15 -6 0 34.52 2.50 -9 15 0 36.18 2.41 15 -6 0 35.69 2.49 -9 15 0 36.35 2.47 -6 -9 0 37.21 2.53 15 -6 0 34.50 2.42 -6 -9 0 38.40 2.64 -6 -9 0 36.53 2.70 -6 -9 0 39.00 2.64 -9 15 0 33.17 2.52 6 -15 0 33.93 2.65 6 -15 0 36.55 2.58 9 6 0 36.07 2.53 -15 9 0 36.71 2.43 9 6 0 38.32 2.47 -15 9 0 35.81 2.55 9 6 0 40.47 2.45 9 6 0 38.86 2.46 -15 9 0 32.59 2.93 -6 15 0 34.97 2.50 15 -9 0 38.01 2.14 15 -9 0 34.70 2.44 -9 -6 0 31.88 2.63 -9 -6 0 37.64 2.49 -9 -6 0 34.95 2.63 -9 -6 0 36.84 2.56 15 -9 0 32.71 2.47 -6 15 0 35.34 2.40 15 -9 0 36.24 2.52 -6 15 0 32.84 2.46 -15 12 0 22.69 1.80 3 -15 0 27.99 1.98 3 -15 0 25.08 2.08 12 3 0 17.37 1.80 12 3 0 21.90 1.89 -15 12 0 22.76 1.99 3 -15 0 25.47 2.10 12 3 0 21.46 1.79 12 3 0 19.92 1.79 -15 12 0 25.82 1.90 15 -12 0 22.47 1.53 15 -12 0 19.66 1.86 -12 -3 0 20.23 1.80 -3 15 0 26.07 1.84 -3 15 0 25.91 1.77 -3 15 0 25.04 1.90 -12 -3 0 20.59 1.91 15 -12 0 21.31 1.91 15 0 0 71.50 4.74 15 0 0 81.74 4.80 15 0 0 79.31 4.77 -15 15 0 82.26 4.79 0 -15 0 78.65 4.90 15 0 0 73.18 4.70 -15 15 0 75.80 4.84 -15 15 0 79.95 4.74 15 0 0 78.11 4.98 0 -15 0 72.37 4.90 0 15 0 81.76 4.82 0 15 0 81.22 4.73 15 -15 0 85.20 4.55 -15 0 0 73.84 4.82 -15 0 0 78.20 4.76 0 15 0 73.17 4.73 0 15 0 80.65 4.77 0 15 0 80.41 4.79 15 -15 0 77.93 4.83 15 -15 0 83.28 4.83 15 -15 0 77.51 4.84 2 14 0 59.75 4.17 -16 2 0 65.93 4.23 2 14 0 66.16 4.12 14 -16 0 73.38 4.29 2 14 0 64.80 4.14 14 -16 0 74.53 3.98 -16 2 0 65.30 4.17 14 -16 0 67.98 4.23 14 -16 0 64.66 4.25 2 14 0 67.62 4.20 2 14 0 59.93 4.17 -14 16 0 73.38 4.21 -2 -14 0 60.35 4.34 -14 16 0 68.56 4.15 16 -2 0 69.69 4.14 16 -2 0 71.59 4.47 -14 16 0 75.34 4.31 -2 -14 0 66.94 4.37 16 -2 0 61.12 4.17 16 -2 0 69.15 4.17 16 -2 0 69.01 4.19 -16 5 0 86.06 5.32 -16 5 0 99.10 5.40 11 -16 0 88.30 5.36 11 -16 0 94.41 5.40 5 11 0 90.40 5.41 11 -16 0 89.77 5.44 5 11 0 87.13 5.35 5 11 0 90.79 5.33 5 11 0 89.40 5.29 -11 16 0 92.23 5.40 16 -5 0 86.28 5.32 16 -5 0 85.20 5.34 -5 -11 0 85.92 5.75 -11 16 0 90.82 5.30 16 -5 0 79.82 5.37 -11 16 0 100.25 5.38 -5 -11 0 85.12 5.46 8 8 0 5.01 0.83 8 8 0 4.97 0.75 -16 8 0 5.05 0.88 8 8 0 4.06 0.94 8 -16 0 3.37 0.82 8 8 0 5.05 0.82 -16 8 0 4.91 0.78 8 -16 0 3.30 0.95 8 -16 0 3.05 0.88 -8 16 0 4.33 0.80 16 -8 0 4.25 0.82 16 -8 0 5.24 0.82 -8 -8 0 2.13 1.09 16 -8 0 3.89 0.83 -8 16 0 4.25 0.81 -8 -8 0 2.66 0.78 -8 16 0 5.26 0.77 -8 -8 0 3.93 1.02 -8 -8 0 4.41 0.89 5 -16 0 87.56 5.38 -16 11 0 95.78 5.30 5 -16 0 87.66 5.37 -16 11 0 90.91 5.35 -16 11 0 90.61 5.38 11 5 0 80.53 5.49 11 5 0 91.09 5.32 11 5 0 94.63 5.34 11 5 0 87.16 5.27 5 -16 0 90.19 5.41 -11 -5 0 89.07 5.46 -11 -5 0 87.66 5.32 16 -11 0 93.61 5.04 -11 -5 0 85.73 5.39 -11 -5 0 77.25 5.47 16 -11 0 84.00 5.96 -5 16 0 85.74 5.34 16 -11 0 89.72 5.32 -5 16 0 88.38 5.24 -5 16 0 90.27 5.30 16 -11 0 95.77 5.36 14 2 0 61.59 4.19 14 2 0 61.85 4.18 2 -16 0 69.96 4.38 14 2 0 58.61 4.13 -16 14 0 74.64 4.33 -16 14 0 71.28 4.29 -16 14 0 73.45 4.21 14 2 0 65.20 4.28 14 2 0 66.96 4.19 2 -16 0 68.13 4.33 16 -14 0 68.44 4.33 16 -14 0 62.15 4.23 -14 -2 0 64.59 4.19 -2 16 0 71.44 4.16 -14 -2 0 61.85 4.23 -2 16 0 72.63 4.24 16 -14 0 74.84 3.96 16 -14 0 68.55 4.24 -2 16 0 72.66 4.23 16 -17 0 33.33 2.69 16 -17 0 34.84 2.28 1 16 0 33.87 2.47 1 16 0 34.93 2.66 16 -17 0 34.93 2.82 16 -17 0 35.63 2.60 1 16 0 34.10 2.58 -17 1 0 36.01 2.64 1 16 0 30.39 3.01 -1 -16 0 32.35 2.84 -16 17 0 41.08 2.70 -16 17 0 36.53 2.71 17 -1 0 36.75 2.51 17 -1 0 37.29 2.68 -1 -16 0 32.73 2.89 17 -1 0 39.59 2.55 17 -1 0 35.26 2.60 4 13 0 16.43 1.62 4 13 0 17.49 1.47 -17 4 0 13.60 1.62 -17 4 0 10.04 1.53 4 13 0 15.83 1.58 13 -17 0 12.08 1.78 13 -17 0 13.06 1.54 4 13 0 17.03 1.47 13 -17 0 11.95 1.74 4 13 0 17.71 1.71 -13 17 0 11.15 1.43 17 -4 0 13.15 1.46 -4 -13 0 19.00 1.96 17 -4 0 16.68 1.71 -13 17 0 14.29 1.54 -13 17 0 13.01 1.64 -4 -13 0 14.49 1.95 17 -4 0 10.03 1.54 7 10 0 4.02 0.84 -17 7 0 4.52 1.16 7 10 0 4.23 0.79 7 10 0 3.28 0.71 -17 7 0 3.00 0.78 10 -17 0 4.02 0.75 10 -17 0 2.29 0.90 -17 7 0 4.39 0.85 10 -17 0 4.56 1.01 7 10 0 4.24 0.87 17 -7 0 4.06 0.77 -7 -10 0 3.26 1.00 -10 17 0 3.85 0.82 17 -7 0 3.89 0.86 -10 17 0 4.60 0.79 -7 -10 0 2.18 1.02 -7 -10 0 4.68 1.16 -10 17 0 4.50 0.81 -7 -10 0 2.93 0.88 7 -17 0 3.11 0.93 10 7 0 4.71 0.85 -17 10 0 3.90 0.86 10 7 0 4.69 0.77 10 7 0 4.88 0.81 7 -17 0 2.99 1.01 10 7 0 4.20 0.86 7 -17 0 3.66 0.84 -17 10 0 2.93 0.76 -17 10 0 4.10 0.87 -7 17 0 3.72 0.79 -10 -7 0 3.41 1.01 -7 17 0 4.50 0.81 -7 17 0 4.97 0.85 17 -10 0 4.57 0.61 -10 -7 0 3.12 0.89 17 -10 0 5.41 1.04 17 -10 0 3.65 0.77 17 -10 0 4.81 0.91 -10 -7 0 3.36 0.88 4 -17 0 12.30 1.54 4 -17 0 12.19 1.89 13 4 0 16.70 1.64 -17 13 0 13.34 1.52 13 4 0 17.48 1.48 -17 13 0 13.67 1.67 13 4 0 18.25 1.52 -17 13 0 14.20 1.61 13 4 0 18.73 1.80 4 -17 0 13.29 1.83 17 -13 0 15.13 1.56 -13 -4 0 17.76 1.77 -13 -4 0 18.32 1.69 17 -13 0 12.47 1.70 -13 -4 0 18.28 1.99 -13 -4 0 18.98 2.00 17 -13 0 14.26 1.12 -4 17 0 15.13 1.56 -4 17 0 11.39 1.39 17 -13 0 12.70 1.70 -4 17 0 11.33 1.56 1 -17 0 36.83 2.91 16 1 0 36.49 2.56 1 -17 0 32.57 2.83 16 1 0 34.19 2.64 -17 16 0 36.68 2.69 16 1 0 33.04 2.67 -17 16 0 36.57 2.75 16 1 0 35.33 2.46 -1 17 0 33.76 2.58 -1 17 0 38.26 2.61 17 -16 0 35.38 2.24 -1 17 0 34.90 2.59 17 -16 0 34.00 2.69 17 -16 0 34.75 2.60 -16 -1 0 36.07 2.71 -1 17 0 34.63 2.49 17 -16 0 37.46 2.74 3 15 0 12.41 1.72 -18 3 0 14.93 1.87 3 15 0 14.34 1.65 15 -18 0 13.81 1.35 3 15 0 15.19 1.68 3 15 0 15.34 1.50 15 -18 0 15.76 1.98 15 -18 0 11.94 1.77 15 -18 0 15.57 1.63 18 -3 0 15.78 1.68 -15 18 0 16.18 1.63 18 -3 0 13.47 1.80 -3 -15 0 12.20 2.01 -3 -15 0 14.39 2.12 18 -3 0 14.56 1.54 -15 18 0 14.25 1.82 18 -3 0 15.22 1.55 12 -18 0 3.48 0.75 6 12 0 3.82 0.88 -18 6 0 4.95 0.99 6 12 0 4.92 0.79 12 -18 0 3.93 1.01 -18 6 0 4.98 0.93 6 12 0 4.28 0.90 12 -18 0 4.26 1.10 -6 -12 0 2.99 1.14 18 -6 0 4.45 0.89 18 -6 0 7.05 1.21 18 -6 0 4.63 0.99 -12 18 0 4.36 0.90 -12 18 0 4.31 0.81 -6 -12 0 4.07 1.13 -12 18 0 6.41 0.93 9 9 0 97.64 6.03 9 9 0 101.44 6.00 9 9 0 107.57 6.07 -18 9 0 104.65 6.07 9 -18 0 100.58 6.10 9 -18 0 101.27 6.14 9 -18 0 101.31 6.13 9 9 0 102.65 6.07 -18 9 0 105.47 6.11 -9 18 0 95.95 5.98 18 -9 0 98.70 6.08 -9 -9 0 108.02 6.25 -9 -9 0 106.51 6.14 18 -9 0 94.95 6.02 -9 18 0 104.24 6.05 18 -9 0 94.07 6.04 -9 -9 0 95.07 6.16 -9 18 0 103.46 6.08 -9 -9 0 105.11 6.21 12 6 0 5.35 0.93 12 6 0 4.07 0.81 12 6 0 4.33 0.93 6 -18 0 4.85 1.12 -18 12 0 3.85 0.80 6 -18 0 2.11 1.05 -18 12 0 5.20 0.96 6 -18 0 3.77 0.84 18 -12 0 3.22 0.94 -12 -6 0 4.54 0.98 -12 -6 0 3.48 1.12 -12 -6 0 3.32 1.18 -6 18 0 4.12 0.79 18 -12 0 4.07 0.75 18 -12 0 4.00 0.97 -6 18 0 4.16 0.86 18 -12 0 4.77 0.52 -6 18 0 5.69 0.86 15 3 0 12.26 1.65 -18 15 0 15.08 1.71 15 3 0 13.25 1.47 3 -18 0 10.69 1.53 15 3 0 12.86 1.75 3 -18 0 17.23 2.06 15 3 0 12.55 1.52 -18 15 0 15.58 1.80 -15 -3 0 12.60 1.76 18 -15 0 15.21 1.92 -3 18 0 14.70 1.65 -3 18 0 15.85 1.50 18 -15 0 13.70 1.74 18 -15 0 12.98 1.57 18 -15 0 15.58 1.16 -18 18 0 34.46 2.83 18 0 0 32.70 2.65 18 0 0 31.61 2.55 18 0 0 30.85 2.46 18 0 0 31.52 2.41 -18 18 0 34.54 2.75 0 -18 0 25.80 2.83 0 -18 0 33.86 2.87 18 -18 0 36.68 2.81 18 -18 0 34.45 2.19 0 18 0 32.30 2.53 0 18 0 32.89 2.59 18 -18 0 39.19 2.62 -18 0 0 30.53 2.70 0 18 0 31.64 2.57 18 -18 0 36.11 2.75 2 17 0 1.04 0.80 17 -19 0 1.60 1.09 2 17 0 0.51 0.75 -19 2 0 1.44 0.92 17 -19 0 1.26 1.03 2 17 0 2.01 0.87 17 -19 0 0.82 0.72 -2 -17 0 1.31 1.20 19 -2 0 2.66 0.79 19 -2 0 1.99 0.94 -17 19 0 1.99 0.85 -2 -17 0 0.59 1.24 19 -2 0 1.08 0.64 19 -2 0 1.39 0.91 14 -19 0 3.14 0.88 5 14 0 2.91 0.89 5 14 0 3.50 0.90 5 14 0 2.07 0.85 14 -19 0 1.47 1.01 5 14 0 1.87 0.77 14 -19 0 0.79 1.00 -19 5 0 1.14 0.87 -14 19 0 2.41 0.79 19 -5 0 1.67 0.82 -5 -14 0 2.42 1.14 19 -5 0 2.24 0.90 19 -5 0 2.25 0.67 -5 -14 0 1.52 1.21 -14 19 0 3.49 0.89 -19 8 0 1.50 0.82 11 -19 0 1.45 1.07 8 11 0 1.13 0.80 11 -19 0 1.24 0.73 8 11 0 1.31 0.78 11 -19 0 1.67 1.01 -19 8 0 1.58 0.86 8 11 0 0.09 0.63 -8 -11 0 0.82 1.10 19 -8 0 1.64 0.87 19 -8 0 1.32 0.67 -8 -11 0 0.92 0.97 -8 -11 0 -0.01 0.99 -11 19 0 2.23 0.80 -11 19 0 2.26 0.80 19 -8 0 0.38 0.78 8 -19 0 0.64 0.70 8 -19 0 2.01 1.03 8 -19 0 0.49 0.98 11 8 0 1.11 0.62 -19 11 0 2.20 0.90 -19 11 0 1.78 0.77 11 8 0 0.82 0.78 11 8 0 1.19 0.75 -8 19 0 2.08 0.76 -11 -8 0 1.89 1.10 -11 -8 0 0.98 1.10 19 -11 0 2.59 0.76 19 -11 0 0.62 0.85 19 -11 0 0.98 0.84 -11 -8 0 0.30 0.85 -8 19 0 1.80 0.77 14 5 0 2.17 0.87 5 -19 0 0.27 0.73 -19 14 0 2.20 0.85 14 5 0 0.93 1.25 14 5 0 2.15 0.73 -19 14 0 0.68 0.71 5 -19 0 2.63 1.14 5 -19 0 2.22 1.12 -14 -5 0 3.15 0.99 -14 -5 0 2.01 1.12 -5 19 0 1.41 0.71 19 -14 0 2.64 0.46 -14 -5 0 1.88 1.19 19 -14 0 1.22 0.94 19 -14 0 2.58 0.73 19 -14 0 2.17 0.93 17 2 0 2.04 0.91 -19 17 0 0.18 0.84 2 -19 0 0.48 1.17 2 -19 0 1.45 1.20 17 2 0 1.08 0.64 17 2 0 1.55 0.91 17 2 0 0.68 0.69 -19 17 0 1.29 0.81 -2 19 0 1.93 0.80 19 -17 0 0.79 1.02 19 -17 0 1.61 1.04 -17 -2 0 2.16 0.97 19 -17 0 1.46 0.45 -2 19 0 2.38 0.84 19 -17 0 1.84 0.69 -2 19 0 1.41 0.86 19 -20 0 17.22 2.38 19 -20 0 17.76 2.29 1 19 0 14.62 2.02 1 19 0 14.04 1.98 1 19 0 15.01 1.91 19 -20 0 15.57 1.84 20 -1 0 21.52 1.80 -19 20 0 20.60 2.27 -1 -19 0 15.08 2.59 -1 -19 0 17.00 2.48 20 -1 0 20.39 2.01 20 -1 0 19.73 2.14 -20 4 0 43.12 2.99 4 16 0 33.52 2.81 16 -20 0 38.91 2.94 16 -20 0 42.04 2.86 16 -20 0 40.26 3.02 4 16 0 33.57 2.79 4 16 0 36.43 2.76 -4 -16 0 34.90 3.14 -4 -16 0 32.61 3.06 -16 20 0 37.27 2.91 20 -4 0 36.65 2.65 20 -4 0 36.32 2.92 20 -4 0 38.33 2.72 20 -4 0 34.72 2.75 13 -20 0 0.90 1.05 13 -20 0 1.91 1.09 7 13 0 1.90 0.76 13 -20 0 0.06 0.65 -20 7 0 3.42 1.02 7 13 0 0.65 0.83 -20 7 0 1.68 0.85 7 13 0 1.37 0.82 20 -7 0 0.53 0.87 -7 -13 0 0.13 1.16 -13 20 0 2.26 0.89 20 -7 0 0.75 0.85 20 -7 0 1.76 0.71 -7 -13 0 1.19 1.16 10 -20 0 94.84 5.74 10 -20 0 89.53 5.69 -20 10 0 91.77 5.65 10 10 0 86.24 5.55 -20 10 0 93.65 5.60 10 10 0 86.16 5.48 10 -20 0 95.76 5.63 10 10 0 91.20 5.58 -10 -10 0 83.26 5.74 -10 -10 0 97.60 5.78 20 -10 0 93.40 5.59 -10 -10 0 90.91 5.69 -10 20 0 93.63 5.63 20 -10 0 89.20 5.62 20 -10 0 95.95 5.61 7 -20 0 1.47 1.05 7 -20 0 0.55 1.11 13 7 0 0.59 0.81 13 7 0 1.04 0.72 -20 13 0 2.18 0.89 -20 13 0 -0.63 0.73 13 7 0 0.04 0.79 7 -20 0 0.13 0.79 20 -13 0 0.53 0.41 -13 -7 0 1.06 0.93 20 -13 0 -0.11 0.87 -13 -7 0 0.12 1.14 20 -13 0 1.67 0.74 20 -13 0 -0.27 0.87 -13 -7 0 -0.20 1.04 -7 20 0 1.32 0.82 16 4 0 36.43 2.83 16 4 0 32.67 2.65 -20 16 0 38.23 3.08 4 -20 0 38.00 3.07 16 4 0 38.04 2.72 -20 16 0 38.25 2.94 4 -20 0 36.51 3.17 16 4 0 35.27 2.83 20 -16 0 40.41 2.91 20 -16 0 39.81 2.37 20 -16 0 39.43 3.01 20 -16 0 41.18 2.80 -4 20 0 37.75 2.83 -16 -4 0 34.32 2.99 1 -20 0 15.99 2.57 19 1 0 16.95 2.18 1 -20 0 18.08 2.42 19 1 0 13.59 1.65 19 1 0 13.31 2.03 -20 19 0 16.97 2.22 -1 20 0 18.74 2.00 20 -19 0 16.55 2.09 -1 20 0 20.44 2.00 20 -19 0 17.66 1.88 -1 20 0 20.92 2.11 20 -19 0 16.25 2.21 18 -21 0 5.74 1.36 3 18 0 5.98 1.16 3 18 0 4.42 1.14 18 -21 0 4.11 0.86 3 18 0 5.59 1.11 18 -21 0 4.77 1.34 21 -3 0 4.93 1.14 -3 -18 0 2.91 1.40 -3 -18 0 3.76 1.56 21 -3 0 4.97 1.14 21 -3 0 5.12 0.86 -18 21 0 6.95 1.23 6 15 0 3.21 0.95 15 -21 0 1.78 0.76 15 -21 0 1.52 1.24 6 15 0 3.82 1.03 -21 6 0 2.60 0.94 6 15 0 3.90 1.03 15 -21 0 1.09 1.13 21 -6 0 1.55 0.94 -15 21 0 3.22 1.02 21 -6 0 2.27 0.74 21 -6 0 0.85 0.94 -6 -15 0 2.21 1.34 -6 -15 0 2.47 1.42 12 -21 0 43.57 2.95 9 12 0 40.47 2.88 12 -21 0 34.46 3.05 -21 9 0 39.34 2.99 12 -21 0 39.21 3.21 9 12 0 39.98 2.97 9 12 0 41.24 2.94 -21 9 0 43.25 3.02 21 -9 0 39.59 2.83 -9 -12 0 37.42 3.25 -9 -12 0 36.13 3.40 21 -9 0 40.42 2.96 21 -9 0 36.44 2.87 -12 21 0 36.38 2.97 -9 -12 0 37.01 3.25 9 -21 0 37.87 3.08 12 9 0 39.71 2.83 9 -21 0 36.85 3.18 9 -21 0 36.11 2.92 12 9 0 42.53 2.92 -21 12 0 43.39 3.04 12 9 0 39.78 2.88 -21 12 0 41.97 2.98 -12 -9 0 38.07 3.18 -12 -9 0 36.95 3.02 21 -12 0 37.25 2.83 21 -12 0 39.58 3.02 -12 -9 0 44.96 3.26 21 -12 0 35.81 2.98 -9 21 0 41.21 2.98 -21 15 0 1.37 0.89 6 -21 0 1.84 1.27 6 -21 0 0.88 1.25 15 6 0 1.64 0.95 15 6 0 3.43 1.03 15 6 0 2.66 0.88 6 -21 0 1.73 1.26 -15 -6 0 2.68 1.20 21 -15 0 1.62 0.69 21 -15 0 2.63 1.04 21 -15 0 1.81 0.46 -6 21 0 0.64 0.82 -15 -6 0 1.52 1.31 -15 -6 0 3.97 1.32 21 -15 0 1.72 1.04 3 -21 0 3.43 1.49 18 3 0 4.77 0.90 18 3 0 4.68 1.17 18 3 0 1.86 1.14 3 -21 0 4.80 1.47 -21 18 0 6.74 1.18 21 -18 0 6.44 1.26 21 -18 0 5.15 1.34 21 -18 0 5.44 0.67 21 -18 0 5.87 1.09 -3 21 0 5.49 1.10 -3 21 0 5.50 1.06 -3 21 0 4.73 1.13 21 0 0 76.90 4.99 -21 21 0 82.15 5.13 0 -21 0 80.77 5.35 0 -21 0 67.50 5.20 21 0 0 76.01 4.85 21 0 0 76.72 4.96 0 21 0 76.58 4.92 21 -21 0 77.19 5.17 21 -21 0 73.87 5.01 0 21 0 75.67 4.91 21 -21 0 78.12 4.95 0 21 0 71.43 4.93 2 20 0 20.90 2.20 2 20 0 23.60 2.36 20 -22 0 19.14 2.09 2 20 0 22.71 2.20 20 -22 0 15.10 2.35 20 -22 0 19.06 2.73 22 -2 0 18.48 2.29 -20 22 0 19.52 2.50 -2 -20 0 20.62 2.84 22 -2 0 19.20 2.38 -2 -20 0 17.56 2.91 22 -2 0 19.61 1.95 5 17 0 31.82 2.71 17 -22 0 30.05 2.90 5 17 0 28.77 2.67 17 -22 0 31.08 2.53 17 -22 0 31.64 2.80 5 17 0 27.83 2.61 -5 -17 0 32.97 3.15 22 -5 0 36.23 2.52 -5 -17 0 26.20 3.04 22 -5 0 32.58 2.80 22 -5 0 33.15 2.66 -17 22 0 33.63 2.81 -22 8 0 10.16 1.79 14 -22 0 8.46 1.32 8 14 0 7.96 1.22 8 14 0 9.26 1.35 14 -22 0 7.78 1.52 14 -22 0 7.82 1.48 -8 -14 0 9.67 1.65 22 -8 0 8.35 1.25 -8 -14 0 7.62 1.64 -14 22 0 10.55 1.85 22 -8 0 10.47 1.41 22 -8 0 11.43 1.51 11 11 0 0.18 0.84 11 -22 0 -1.47 0.81 -22 11 0 -0.02 0.85 -22 11 0 -0.20 0.97 11 -22 0 0.19 1.15 11 11 0 0.15 0.83 11 -22 0 -0.84 1.15 22 -11 0 1.01 0.92 -11 22 0 0.07 0.80 22 -11 0 -0.31 0.97 -11 -11 0 -0.23 1.18 -11 -11 0 -1.15 1.28 22 -11 0 -0.29 0.63 14 8 0 8.60 1.26 8 -22 0 7.64 1.56 8 -22 0 7.10 1.63 14 8 0 9.96 1.32 -22 14 0 8.17 1.22 8 -22 0 8.93 1.52 -14 -8 0 8.39 1.54 22 -14 0 9.13 0.97 -8 22 0 11.00 1.79 22 -14 0 7.86 1.10 22 -14 0 7.81 1.35 -14 -8 0 9.78 1.70 22 -14 0 7.69 1.42 17 5 0 27.69 2.39 5 -22 0 28.97 2.95 17 5 0 29.47 2.79 5 -22 0 33.92 2.97 17 5 0 28.73 2.71 -22 17 0 33.11 2.73 22 -17 0 28.01 2.45 22 -17 0 30.70 2.69 22 -17 0 29.95 2.81 22 -17 0 32.45 2.04 -5 22 0 31.70 2.67 -22 20 0 20.04 2.46 20 2 0 21.83 2.36 2 -22 0 16.52 2.63 20 2 0 20.30 2.18 20 2 0 21.69 1.91 2 -22 0 13.96 2.12 -2 22 0 13.66 2.01 22 -20 0 18.04 2.44 22 -20 0 17.79 2.04 22 -20 0 14.07 2.39 -2 22 0 16.04 2.10 -2 22 0 18.08 2.15 22 -23 0 11.67 1.88 22 -23 0 10.78 1.78 1 22 0 13.72 2.00 1 22 0 11.98 2.06 22 -23 0 11.19 1.85 -1 -22 0 12.56 2.17 -1 -22 0 10.75 2.12 23 -1 0 13.74 2.09 23 -1 0 11.94 1.65 23 -1 0 13.62 1.72 -22 23 0 16.20 1.88 4 19 0 18.71 2.12 19 -23 0 19.65 2.54 19 -23 0 22.86 2.24 4 19 0 19.55 2.30 19 -23 0 24.56 2.70 4 19 0 24.76 2.46 -4 -19 0 25.13 3.05 23 -4 0 26.15 2.19 23 -4 0 25.04 2.54 -19 23 0 26.55 2.59 -4 -19 0 17.39 2.90 23 -4 0 20.31 2.38 16 -23 0 47.00 3.69 7 16 0 43.31 3.28 7 16 0 44.09 3.43 16 -23 0 46.04 3.50 7 16 0 40.98 3.21 16 -23 0 46.84 3.29 -16 23 0 48.71 3.44 23 -7 0 42.74 3.18 23 -7 0 44.02 3.36 -7 -16 0 45.41 3.80 23 -7 0 42.74 3.35 -7 -16 0 41.00 3.69 13 -23 0 7.08 1.54 10 13 0 7.59 1.28 10 13 0 5.16 1.18 13 -23 0 6.23 1.46 -23 10 0 7.84 1.36 23 -10 0 8.25 1.34 -10 -13 0 5.25 1.67 23 -10 0 9.53 1.36 -13 23 0 8.83 1.31 -10 -13 0 4.85 1.65 23 -10 0 9.33 1.51 13 10 0 6.17 1.19 13 10 0 5.41 1.17 10 -23 0 11.56 2.14 10 -23 0 8.59 1.52 -23 13 0 7.73 1.31 10 -23 0 5.54 1.56 -13 -10 0 4.58 1.54 23 -13 0 8.59 1.36 23 -13 0 8.63 1.21 -13 -10 0 5.02 1.63 23 -13 0 7.16 1.46 -10 23 0 8.94 1.32 16 7 0 44.89 3.47 7 -23 0 44.61 3.67 7 -23 0 45.97 3.75 16 7 0 41.31 3.38 -23 16 0 46.86 3.44 7 -23 0 43.99 3.76 -7 23 0 43.89 3.41 23 -16 0 46.53 3.45 23 -16 0 45.42 3.24 23 -16 0 46.97 2.81 23 -16 0 49.32 3.49 -16 -7 0 43.50 3.60 -16 -7 0 42.44 3.86 19 4 0 25.18 2.15 -23 19 0 23.43 2.60 19 4 0 21.67 2.47 4 -23 0 21.79 2.83 19 4 0 25.06 2.53 4 -23 0 25.75 2.91 23 -19 0 26.56 2.30 -4 23 0 22.41 2.47 23 -19 0 23.18 2.48 -4 23 0 25.23 2.44 23 -19 0 23.99 2.76 -4 23 0 22.00 2.29 22 1 0 13.25 1.65 22 1 0 15.19 2.27 -23 22 0 13.18 1.66 1 -23 0 8.04 1.93 22 1 0 11.26 1.58 1 -23 0 10.69 2.02 23 -22 0 12.50 1.92 -1 23 0 9.86 1.49 23 -22 0 10.63 1.81 -1 23 0 11.25 1.48 23 -22 0 10.80 1.78 -1 23 0 11.72 1.57 3 21 0 7.84 1.44 21 -24 0 8.74 1.77 21 -24 0 6.39 1.62 3 21 0 7.91 1.36 -3 -21 0 6.00 2.17 24 -3 0 10.09 1.50 24 -3 0 8.71 1.45 -21 24 0 9.70 1.64 24 -3 0 12.52 1.61 18 -24 0 1.61 1.45 18 -24 0 -0.76 0.95 6 18 0 2.84 1.15 18 -24 0 1.46 1.38 6 18 0 2.73 1.15 -6 -18 0 2.67 1.59 24 -6 0 2.15 0.79 24 -6 0 0.80 1.08 24 -6 0 1.20 1.15 -18 24 0 1.40 1.12 -6 -18 0 1.49 1.77 9 15 0 42.87 3.24 9 15 0 47.32 3.43 -24 9 0 43.45 3.41 15 -24 0 45.16 3.71 15 -24 0 34.53 3.49 15 -24 0 43.22 3.51 24 -9 0 49.57 3.21 24 -9 0 37.88 3.21 -15 24 0 44.44 3.41 24 -9 0 47.29 3.43 -9 -15 0 42.41 3.90 -9 -15 0 39.79 3.71 12 -24 0 60.53 4.52 12 12 0 61.86 4.35 12 -24 0 77.97 5.45 12 12 0 62.96 4.27 -24 12 0 70.99 4.50 12 -24 0 59.58 4.57 -12 -12 0 63.62 4.70 24 -12 0 67.21 4.27 -12 24 0 63.48 4.43 24 -12 0 56.98 4.27 -12 -12 0 60.84 4.72 24 -12 0 69.95 4.43 9 -24 0 40.86 3.62 -24 15 0 44.59 3.53 9 -24 0 46.82 3.77 15 9 0 39.84 3.24 9 -24 0 44.76 3.58 15 9 0 46.54 3.36 24 -15 0 43.94 3.46 24 -15 0 47.08 3.20 24 -15 0 43.18 3.45 -15 -9 0 49.49 3.88 -9 24 0 42.81 3.31 -15 -9 0 37.65 3.65 18 6 0 4.24 0.94 -24 18 0 1.88 1.23 18 6 0 3.53 1.11 6 -24 0 2.60 1.56 6 -24 0 1.63 1.50 18 6 0 2.26 1.11 24 -18 0 2.58 0.62 24 -18 0 2.04 0.81 -6 24 0 2.02 1.05 24 -18 0 3.57 1.25 24 -18 0 3.36 1.38 21 3 0 6.74 1.36 -24 21 0 8.32 1.49 21 3 0 8.64 1.50 3 -24 0 10.75 1.99 21 3 0 7.12 1.36 3 -24 0 6.63 1.92 24 -21 0 8.53 1.60 -3 24 0 9.71 1.39 -3 24 0 5.21 1.16 24 -21 0 11.82 1.49 24 -21 0 7.32 1.56 -3 24 0 9.62 1.47 24 0 0 0.55 1.19 24 0 0 2.24 0.81 0 -24 0 1.38 1.76 -24 24 0 4.93 1.35 0 -24 0 2.12 1.90 24 0 0 3.07 1.45 0 24 0 0.51 1.08 24 -24 0 -0.57 0.99 24 -24 0 2.11 1.49 24 -24 0 1.12 1.54 0 24 0 1.32 1.13 2 23 0 146.50 8.83 2 23 0 145.02 8.89 23 -25 0 146.98 9.09 23 -25 0 142.39 9.42 23 -25 0 154.44 8.98 25 -2 0 148.50 8.85 25 -2 0 149.78 8.78 -23 25 0 144.59 8.96 -2 -23 0 141.71 9.20 25 -2 0 152.38 9.15 -2 -23 0 136.45 9.21 20 -25 0 0.04 1.42 20 -25 0 1.49 1.17 5 20 0 0.35 1.03 20 -25 0 0.76 1.42 5 20 0 0.73 1.14 25 -5 0 0.69 1.12 25 -5 0 1.06 1.16 -5 -20 0 1.08 1.86 -20 25 0 2.37 1.28 25 -5 0 0.76 0.83 -5 -20 0 2.33 1.69 8 17 0 1.39 1.10 17 -25 0 0.14 1.40 17 -25 0 0.52 1.58 17 -25 0 1.11 1.47 8 17 0 0.39 0.99 25 -8 0 2.05 1.15 25 -8 0 -0.89 1.05 -8 -17 0 1.87 1.77 -17 25 0 1.68 1.14 -8 -17 0 -0.81 1.53 25 -8 0 0.37 0.76 14 -25 0 58.01 4.20 14 -25 0 50.61 4.29 11 14 0 58.72 3.95 11 14 0 53.77 3.86 -25 11 0 59.17 4.05 25 -11 0 51.78 3.85 -11 -14 0 57.99 4.52 -14 25 0 52.12 4.01 25 -11 0 51.47 4.01 25 -11 0 55.90 3.79 -11 -14 0 47.25 4.17 -25 14 0 54.56 3.97 14 11 0 54.80 3.83 14 11 0 59.13 4.00 11 -25 0 50.58 4.06 11 -25 0 49.76 4.28 11 -25 0 53.15 4.24 25 -14 0 53.55 3.91 -14 -11 0 59.66 4.40 25 -14 0 51.52 3.69 -14 -11 0 53.94 4.29 -11 25 0 53.92 3.96 25 -14 0 53.75 4.05 8 -25 0 -0.28 1.43 -25 17 0 1.53 1.19 17 8 0 0.18 0.99 8 -25 0 1.80 1.59 8 -25 0 -1.71 1.48 17 8 0 0.17 1.02 25 -17 0 -0.03 1.22 25 -17 0 0.12 1.18 25 -17 0 -0.09 0.56 -17 -8 0 -0.35 1.45 -8 25 0 1.93 1.05 25 -17 0 0.68 0.80 -25 20 0 1.04 1.34 20 5 0 1.60 0.72 5 -25 0 0.26 1.58 20 5 0 0.91 1.10 20 5 0 0.99 1.10 5 -25 0 -0.17 1.66 25 -20 0 -0.07 1.29 -5 25 0 1.86 0.92 25 -20 0 0.64 1.29 -5 25 0 0.24 1.01 25 -20 0 1.08 0.92 -5 25 0 1.31 1.09 23 2 0 134.48 8.63 -25 23 0 150.00 8.90 2 -25 0 146.28 9.10 23 2 0 142.15 9.24 2 -25 0 132.28 9.01 23 2 0 135.23 8.66 25 -23 0 149.75 8.95 25 -23 0 149.17 8.80 -2 25 0 143.89 8.68 -2 25 0 150.05 8.74 25 -23 0 151.09 8.79 25 -26 0 20.06 2.92 25 -26 0 18.85 3.05 1 25 0 20.80 2.63 1 25 0 22.44 2.67 26 -1 0 23.78 2.91 -1 -25 0 15.97 2.55 26 -1 0 18.56 2.12 -1 -25 0 20.51 2.89 26 -1 0 20.79 2.70 4 22 0 39.37 3.09 22 -26 0 32.70 3.36 22 -26 0 32.14 3.44 4 22 0 36.30 3.17 22 -26 0 42.45 4.00 26 -4 0 33.56 3.17 -4 -22 0 39.76 4.00 -4 -22 0 37.30 3.91 26 -4 0 30.99 3.14 -22 26 0 33.10 3.26 26 -4 0 28.34 2.69 7 19 0 -0.17 1.05 7 19 0 -0.29 1.12 19 -26 0 -0.16 1.56 19 -26 0 0.35 1.49 -7 -19 0 0.81 1.90 26 -7 0 0.01 1.16 -19 26 0 1.98 1.32 26 -7 0 0.31 1.20 26 -7 0 2.11 0.82 -7 -19 0 -0.34 1.63 16 -26 0 19.94 2.92 16 -26 0 10.37 2.03 10 16 0 14.72 2.17 10 16 0 16.34 2.31 16 -26 0 17.75 2.61 -26 10 0 19.53 2.44 -16 26 0 15.88 1.96 -10 -16 0 16.95 2.42 -10 -16 0 13.55 2.18 26 -10 0 15.98 1.92 26 -10 0 16.80 2.23 26 -10 0 17.70 2.47 13 13 0 13.70 2.04 13 13 0 13.65 2.12 -26 13 0 11.23 1.70 13 -26 0 7.00 1.80 13 -26 0 10.77 1.83 -13 26 0 10.51 1.60 -13 -13 0 10.77 1.89 -13 -13 0 19.30 3.07 26 -13 0 11.68 1.71 26 -13 0 9.42 1.62 26 -13 0 8.94 1.52 16 10 0 16.01 2.10 -26 16 0 14.21 2.51 10 -26 0 12.30 1.91 10 -26 0 18.43 2.90 10 -26 0 12.20 2.13 16 10 0 13.86 1.73 26 -16 0 16.06 2.28 -10 26 0 14.02 2.35 26 -16 0 14.00 1.84 26 -16 0 15.93 1.82 -16 -10 0 14.23 2.06 -16 -10 0 17.94 2.45 19 7 0 0.92 1.10 7 -26 0 0.21 1.59 7 -26 0 1.15 1.71 -26 19 0 1.37 1.39 19 7 0 1.19 1.09 19 7 0 -0.46 0.70 -7 26 0 1.19 0.95 26 -19 0 1.52 1.36 26 -19 0 1.45 1.30 22 4 0 36.61 3.72 4 -26 0 29.47 3.65 4 -26 0 25.85 3.67 22 4 0 37.70 2.96 -26 22 0 29.73 3.06 22 4 0 34.45 2.62 -4 26 0 26.89 2.81 26 -22 0 32.80 3.31 26 -22 0 29.35 2.81 -4 26 0 28.79 2.93 26 -22 0 30.54 3.07 25 1 0 23.84 2.71 1 -26 0 18.77 2.66 1 -26 0 14.71 2.69 25 1 0 17.29 2.04 25 1 0 17.04 2.69 -1 26 0 22.96 2.47 26 -25 0 23.37 3.24 -1 26 0 24.12 2.56 26 -25 0 18.51 2.90 24 -27 0 7.79 1.78 24 -27 0 7.17 1.91 24 -27 0 9.20 1.99 3 24 0 8.43 1.64 3 24 0 8.37 1.58 27 -3 0 12.50 1.75 27 -3 0 10.04 1.37 -3 -24 0 6.93 2.40 -3 -24 0 9.29 2.24 27 -3 0 11.80 1.75 21 -27 0 8.37 1.86 21 -27 0 7.30 1.91 6 21 0 7.24 1.44 6 21 0 7.62 1.50 21 -27 0 7.17 1.90 27 -6 0 6.40 1.11 -21 27 0 6.23 1.36 27 -6 0 4.88 1.33 -6 -21 0 8.24 2.28 27 -6 0 9.66 1.60 -6 -21 0 4.78 2.00 9 18 0 14.44 2.29 9 18 0 13.49 2.12 18 -27 0 12.58 2.09 18 -27 0 9.99 1.99 18 -27 0 13.85 2.13 27 -9 0 13.38 1.88 27 -9 0 11.40 1.63 -9 -18 0 12.81 2.42 -9 -18 0 9.91 2.06 27 -9 0 15.79 1.85 -18 27 0 16.78 2.57 12 15 0 5.97 1.30 -27 12 0 9.11 1.63 15 -27 0 4.77 1.67 12 15 0 5.62 1.37 15 -27 0 3.59 1.72 15 -27 0 8.07 1.84 27 -12 0 4.65 1.37 -12 -15 0 4.09 1.77 -15 27 0 6.46 1.41 27 -12 0 6.21 1.45 -12 -15 0 3.47 2.02 15 12 0 7.04 1.38 12 -27 0 4.72 1.79 15 12 0 6.17 1.30 12 -27 0 1.91 1.73 -27 15 0 5.42 1.39 12 -27 0 5.57 1.74 27 -15 0 6.95 1.54 27 -15 0 3.38 1.36 -15 -12 0 6.81 1.81 -15 -12 0 5.42 2.04 27 -15 0 6.29 1.15 -12 27 0 8.27 1.36 18 9 0 14.00 2.42 18 9 0 14.39 2.15 9 -27 0 10.00 2.17 9 -27 0 11.29 2.14 -27 18 0 18.64 2.61 27 -18 0 16.30 2.69 27 -18 0 16.70 2.42 27 -18 0 19.71 1.50 -9 27 0 18.93 2.07 27 -18 0 13.61 1.90 21 6 0 8.99 1.57 6 -27 0 5.70 1.93 -27 21 0 4.46 1.34 21 6 0 6.60 1.09 21 6 0 5.47 1.38 6 -27 0 3.46 1.89 -6 27 0 6.79 1.32 27 -21 0 4.02 1.21 27 -21 0 7.91 1.61 -6 27 0 6.60 1.39 27 -21 0 7.20 1.62 3 -27 0 12.88 2.29 3 -27 0 12.44 2.48 24 3 0 10.43 1.74 24 3 0 10.23 1.54 24 3 0 11.36 1.75 -3 27 0 16.10 2.35 27 -24 0 9.75 1.90 27 -24 0 13.33 2.44 -3 27 0 14.33 1.79 27 -24 0 8.60 1.97 27 0 0 76.26 5.18 0 -27 0 68.04 5.78 27 0 0 67.97 5.08 27 0 0 71.90 4.81 0 -27 0 68.79 5.75 0 27 0 76.51 5.02 27 -27 0 70.41 5.55 0 27 0 68.70 5.02 27 -27 0 72.57 5.29 26 -28 0 0.57 1.89 2 26 0 1.20 1.35 2 26 0 1.34 1.30 26 -28 0 1.99 1.76 26 -28 0 3.97 1.91 28 -2 0 2.06 1.46 -2 -26 0 0.44 2.44 28 -2 0 0.49 0.79 28 -2 0 2.95 1.49 -2 -26 0 1.37 2.12 23 -28 0 1.70 1.79 23 -28 0 1.94 1.81 23 -28 0 -0.71 1.70 5 23 0 5.39 1.39 5 23 0 2.88 1.39 -5 -23 0 2.00 2.28 -5 -23 0 3.27 1.99 28 -5 0 3.46 1.40 28 -5 0 1.66 0.94 28 -5 0 1.55 1.28 8 20 0 14.95 2.19 20 -28 0 9.84 2.07 20 -28 0 7.32 1.98 20 -28 0 7.10 1.95 8 20 0 13.91 1.79 28 -8 0 15.23 2.55 28 -8 0 9.05 1.60 28 -8 0 10.98 1.80 -8 -20 0 8.21 2.11 -8 -20 0 11.38 2.52 17 -28 0 -0.99 1.59 11 17 0 -0.10 1.07 11 17 0 1.77 1.18 17 -28 0 -0.64 1.71 17 -28 0 2.54 1.71 -28 11 0 -0.42 1.18 28 -11 0 -0.11 1.16 -11 -17 0 -0.19 1.70 28 -11 0 1.70 1.25 28 -11 0 1.06 0.77 -17 28 0 1.97 1.26 -11 -17 0 1.35 2.04 14 14 0 8.47 1.47 14 -28 0 4.13 1.87 14 14 0 9.39 1.43 14 -28 0 7.63 1.89 -28 14 0 5.55 1.31 14 -28 0 6.75 1.87 -14 -14 0 4.44 1.85 28 -14 0 8.96 1.32 -14 -14 0 5.38 2.17 28 -14 0 7.49 1.50 28 -14 0 7.03 1.71 11 -28 0 0.87 1.83 11 -28 0 -0.48 1.73 17 11 0 0.93 1.09 -28 17 0 -0.22 1.03 17 11 0 2.16 1.21 11 -28 0 -1.38 1.61 -17 -11 0 -0.95 1.57 28 -17 0 0.56 1.31 28 -17 0 -0.03 1.32 -17 -11 0 -0.98 1.89 28 -17 0 -0.36 0.67 -11 28 0 0.66 0.90 8 -28 0 7.03 2.22 20 8 0 14.27 2.27 20 8 0 15.21 2.36 20 8 0 13.12 1.72 8 -28 0 8.93 2.12 28 -20 0 9.96 1.79 28 -20 0 10.26 1.79 28 -20 0 10.97 1.50 23 5 0 5.51 1.44 23 5 0 2.34 0.83 23 5 0 2.17 1.34 5 -28 0 6.86 2.07 5 -28 0 2.38 2.14 -5 28 0 4.95 1.37 28 -23 0 2.73 1.53 28 -23 0 1.15 1.54 -5 28 0 1.58 1.22 28 -23 0 2.14 1.29 2 -28 0 0.62 2.03 2 -28 0 0.22 2.18 26 2 0 1.58 1.35 26 2 0 2.21 1.48 26 2 0 0.67 0.98 -2 28 0 2.13 1.26 28 -26 0 2.00 1.89 -2 28 0 2.88 1.31 28 -26 0 4.38 1.54 28 -26 0 1.05 1.76 28 -29 0 25.36 3.88 28 -29 0 25.30 3.76 1 28 0 17.69 2.91 1 28 0 17.52 2.75 28 -29 0 22.74 3.41 -1 -28 0 16.68 3.05 -1 -28 0 16.34 3.07 29 -1 0 26.15 3.18 4 25 0 14.03 1.95 25 -29 0 20.21 3.43 4 25 0 13.51 2.00 25 -29 0 18.76 2.66 25 -29 0 23.25 3.33 29 -4 0 17.83 2.84 -4 -25 0 13.02 2.60 29 -4 0 12.56 1.99 29 -4 0 20.10 3.03 -4 -25 0 8.39 2.80 22 -29 0 1.00 1.84 7 22 0 2.51 1.31 22 -29 0 2.48 1.95 22 -29 0 1.97 1.79 7 22 0 2.13 1.37 -7 -22 0 1.69 2.33 29 -7 0 1.01 1.37 -7 -22 0 -0.76 1.86 29 -7 0 -0.51 0.90 29 -7 0 1.96 1.37 10 19 0 2.60 1.24 19 -29 0 1.49 1.77 19 -29 0 1.97 1.80 19 -29 0 2.61 1.75 10 19 0 3.05 1.29 29 -10 0 1.34 0.90 -10 -19 0 1.05 1.88 -10 -19 0 -1.91 2.05 29 -10 0 0.62 1.28 29 -10 0 1.76 1.35 16 -29 0 -0.46 1.76 16 -29 0 -2.39 1.62 13 16 0 0.96 1.18 16 -29 0 -0.35 1.78 13 16 0 0.36 1.15 29 -13 0 -1.31 0.85 -13 -16 0 -0.66 1.62 -13 -16 0 -2.60 1.98 29 -13 0 0.46 1.24 29 -13 0 0.00 1.29 13 -29 0 -1.09 1.67 13 -29 0 0.86 1.76 13 -29 0 -2.39 1.64 16 13 0 -0.15 1.10 16 13 0 -0.81 1.08 29 -16 0 0.56 1.33 29 -16 0 0.17 1.32 -16 -13 0 -0.17 1.69 -16 -13 0 0.54 2.03 29 -16 0 -0.94 0.67 10 -29 0 -0.71 1.82 10 -29 0 2.94 1.85 10 -29 0 0.17 1.79 19 10 0 1.45 1.20 19 10 0 1.63 1.18 29 -19 0 1.07 1.03 29 -19 0 1.50 1.40 29 -19 0 2.30 1.46 29 -19 0 0.12 0.84 7 -29 0 1.54 2.18 22 7 0 1.89 1.30 22 7 0 0.51 0.87 22 7 0 1.02 1.27 7 -29 0 1.34 1.92 -7 29 0 3.12 1.28 29 -22 0 1.17 1.55 29 -22 0 1.92 1.21 29 -22 0 1.83 1.54 -7 29 0 -0.18 1.27 4 -29 0 15.44 2.62 25 4 0 15.93 2.65 25 4 0 14.48 2.09 4 -29 0 11.81 2.65 29 -25 0 20.79 3.24 -4 29 0 20.49 2.63 -4 29 0 16.11 2.46 29 -25 0 17.68 2.69 1 -29 0 22.13 3.34 28 1 0 23.99 3.08 1 -29 0 18.99 3.03 28 1 0 19.54 3.03 29 -28 0 21.96 3.57 -1 29 0 25.97 3.12 29 -28 0 25.64 3.59 -1 29 0 25.09 2.93 29 -28 0 22.75 3.71 3 27 0 -0.01 1.39 27 -30 0 -0.59 1.88 27 -30 0 0.14 1.80 3 27 0 0.96 1.38 27 -30 0 -2.23 1.85 -3 -27 0 0.86 2.59 30 -3 0 0.15 1.46 -3 -27 0 1.47 2.32 30 -3 0 2.65 1.61 24 -30 0 21.25 3.50 6 24 0 23.62 2.78 24 -30 0 14.45 2.77 24 -30 0 15.28 2.31 30 -6 0 11.62 2.08 -6 -24 0 18.31 2.95 30 -6 0 19.02 3.00 9 21 0 13.74 1.85 21 -30 0 9.08 2.40 21 -30 0 10.38 2.22 9 21 0 12.55 1.81 21 -30 0 11.41 2.27 -9 -21 0 13.07 2.40 30 -9 0 12.05 1.98 -9 -21 0 16.76 2.86 30 -9 0 14.13 1.95 30 -9 0 16.95 2.68 18 -30 0 0.23 1.85 18 -30 0 0.81 1.86 18 -30 0 1.53 1.95 12 18 0 0.92 1.24 12 18 0 0.19 1.19 30 -12 0 2.71 1.45 30 -12 0 1.55 1.39 -12 -18 0 0.00 2.32 -12 -18 0 0.25 1.86 30 -12 0 0.21 0.87 15 -30 0 1.62 2.03 15 -30 0 1.44 1.89 15 15 0 -0.42 1.14 15 -30 0 -0.48 1.79 15 15 0 -0.82 1.11 30 -15 0 0.45 1.39 30 -15 0 0.58 1.32 -15 -15 0 -0.54 1.74 -15 -15 0 1.08 2.24 12 -30 0 0.36 1.93 12 -30 0 1.97 2.08 18 12 0 1.19 1.20 12 -30 0 0.98 1.87 18 12 0 0.97 1.26 -18 -12 0 -0.25 1.78 -18 -12 0 -0.80 2.25 30 -18 0 0.27 0.81 30 -18 0 2.93 1.50 30 -18 0 3.35 1.44 21 9 0 16.77 2.40 9 -30 0 8.87 2.23 9 -30 0 12.93 2.52 21 9 0 9.17 1.39 21 9 0 11.79 1.80 30 -21 0 11.23 2.03 30 -21 0 10.01 1.54 30 -21 0 12.67 2.00 6 -30 0 13.29 2.76 24 6 0 21.46 2.71 24 6 0 13.61 2.09 6 -30 0 13.09 2.63 30 -24 0 15.43 2.21 -6 30 0 15.81 2.46 -6 30 0 12.54 1.90 3 -30 0 2.23 2.35 3 -30 0 -1.80 2.52 27 3 0 -0.68 1.34 27 3 0 -0.90 1.35 30 -27 0 -1.28 1.85 30 -27 0 1.29 1.93 -3 30 0 -0.75 1.44 30 -27 0 -0.23 1.74 -3 30 0 -0.20 1.29 30 0 0 27.84 3.61 0 -30 0 21.29 4.16 0 -30 0 27.34 4.50 30 0 0 29.77 3.33 30 -30 0 31.55 4.83 0 30 0 30.43 3.42 0 30 0 28.58 3.17 30 -30 0 18.69 2.93 2 29 0 1.28 1.67 29 -31 0 -3.78 2.06 2 29 0 -0.27 1.47 31 -2 0 2.55 1.65 -2 -29 0 0.60 4.35 -2 -29 0 -2.30 2.29 31 -2 0 -0.24 1.62 26 -31 0 14.79 2.63 5 26 0 14.51 2.10 26 -31 0 17.64 2.58 5 26 0 15.86 2.15 26 -31 0 13.58 2.39 31 -5 0 18.27 2.90 31 -5 0 20.06 3.14 -5 -26 0 11.25 2.75 -5 -26 0 12.73 3.18 8 23 0 5.09 1.55 23 -31 0 1.96 2.33 23 -31 0 4.24 2.09 31 -8 0 5.88 1.69 31 -8 0 2.51 1.05 31 -8 0 5.42 1.62 -8 -23 0 0.65 2.51 11 20 0 0.18 1.25 20 -31 0 1.49 1.97 11 20 0 1.62 1.36 20 -31 0 0.19 2.06 20 -31 0 0.94 2.12 31 -11 0 2.71 1.53 31 -11 0 0.85 0.89 -11 -20 0 1.58 2.05 -11 -20 0 1.13 2.44 14 17 0 1.40 1.24 14 17 0 2.56 1.35 17 -31 0 5.29 2.04 17 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0.00 -16 17 24 -1.99 0.00 -13 17 24 -0.84 0.00 -10 17 24 -0.11 0.00 -7 17 24 -0.11 0.00 -4 17 24 -1.31 0.00 -1 17 24 -2.05 0.00 -18 18 24 -2.34 0.00 -15 18 24 -1.97 0.00 -12 18 24 -1.27 0.00 -9 18 24 -0.59 0.00 -6 18 24 -0.81 0.00 -3 18 24 -1.66 0.00 0 18 24 -1.19 0.00 -14 19 24 -1.79 0.00 -11 19 24 -1.27 0.00 -8 19 24 -0.80 0.00 -5 19 24 -1.20 0.00 -13 20 24 -1.38 0.00 -10 20 24 -1.04 0.00 -7 20 24 -0.94 0.00 -2 3 25 -0.01 0.00 -1 4 25 -0.03 0.00 -3 5 25 0.11 0.00 -5 6 25 0.39 0.00 -2 6 25 -0.14 0.00 -4 7 25 0.56 0.00 -1 7 25 -0.43 0.00 -6 8 25 1.67 0.00 -3 8 25 -0.40 0.00 -8 9 25 1.73 0.00 -5 9 25 1.39 0.00 -2 9 25 -1.55 0.00 -7 10 25 3.64 0.00 -4 10 25 -0.82 0.00 -1 10 25 -1.53 0.00 -9 11 25 4.29 0.00 -6 11 25 2.19 0.00 -3 11 25 -3.08 0.00 -11 12 25 2.67 0.00 -8 12 25 5.27 0.00 -5 12 25 -1.41 0.00 -2 12 25 -3.54 0.00 -10 13 25 6.16 0.00 -7 13 25 2.33 0.00 -4 13 25 -4.40 0.00 -1 13 25 -2.06 0.00 -12 14 25 4.56 0.00 -9 14 25 5.47 0.00 -6 14 25 -2.09 0.00 -3 14 25 -4.94 0.00 -14 15 25 1.97 0.00 -11 15 25 6.15 0.00 -8 15 25 1.54 0.00 -5 15 25 -4.99 0.00 -2 15 25 -3.38 0.00 -13 16 25 4.65 0.00 -10 16 25 4.08 0.00 -7 16 25 -2.65 0.00 -4 16 25 -5.13 0.00 -1 16 25 -1.33 0.00 -15 17 25 2.46 0.00 -12 17 25 4.48 0.00 -9 17 25 0.23 0.00 -6 17 25 -4.68 0.00 -3 17 25 -3.47 0.00 -11 18 25 2.02 0.00 -8 18 25 -2.79 0.00 -5 18 25 -4.26 0.00 0 1 26 -5.38 0.00 -2 2 26 -4.07 0.00 -1 3 26 -3.86 0.00 -3 4 26 -0.82 0.00 0 4 26 -2.99 0.00 -5 5 26 3.25 0.00 -2 5 26 -1.25 0.00 -4 6 26 2.68 0.00 -1 6 26 -1.14 0.00 -6 7 26 5.86 0.00 -3 7 26 1.69 0.00 0 7 26 0.44 0.00 -8 8 26 6.15 0.00 -5 8 26 4.95 0.00 -2 8 26 1.66 0.00 -7 9 26 5.89 0.00 -4 9 26 4.18 0.00 -1 9 26 3.24 0.00 -9 10 26 3.75 0.00 -6 10 26 5.46 0.00 -3 10 26 4.53 0.00 0 10 26 5.62 0.00 -11 11 26 0.14 0.00 -8 11 26 3.99 0.00 -5 11 26 5.52 0.00 -2 11 26 5.92 0.00 -10 12 26 0.56 0.00 -7 12 26 4.58 0.00 -4 12 26 6.22 0.00 -1 12 26 7.17 0.00 -12 13 26 -2.58 0.00 -9 13 26 1.66 0.00 -6 13 26 5.41 0.00 -3 13 26 6.92 0.00 0 13 26 7.08 0.00 -14 14 26 -3.67 0.00 -11 14 26 -1.57 0.00 -8 14 26 3.05 0.00 -5 14 26 5.99 0.00 -2 14 26 6.76 0.00 -13 15 26 -3.22 0.00 -10 15 26 0.03 0.00 -7 15 26 4.09 0.00 -4 15 26 5.76 0.00 -9 16 26 1.57 0.00 -6 16 26 4.21 0.00 -1 2 27 0.04 0.00 -2 4 27 0.23 0.00 -4 5 27 0.31 0.00 -1 5 27 0.13 0.00 -3 6 27 0.51 0.00 -5 7 27 0.95 0.00 -2 7 27 0.02 0.00 -7 8 27 0.91 0.00 -4 8 27 0.74 0.00 -1 8 27 -0.43 0.00 -6 9 27 1.84 0.00 -3 9 27 -0.49 0.00 -8 10 27 2.26 0.00 -5 10 27 0.92 0.00 -2 10 27 -1.50 0.00 -10 11 27 1.43 0.00 -7 11 27 2.76 0.00 -4 11 27 -1.08 0.00 -1 11 27 -1.26 0.00 -9 12 27 3.41 0.00 -6 12 27 1.17 0.00 -3 12 27 -2.52 0.00 -8 13 27 3.33 0.00 -5 13 27 -1.23 0.00 -1 1 28 5.14 0.00 0 2 28 5.47 0.00 -2 3 28 6.36 0.00 -4 4 28 8.02 0.00 -1 4 28 6.00 0.00 -3 5 28 7.42 0.00 0 5 28 5.18 0.00 -5 6 28 8.50 0.00 -2 6 28 5.85 0.00 -7 7 28 7.58 0.00 -4 7 28 6.94 0.00 -1 7 28 3.89 0.00 -6 8 28 6.77 0.00 -3 8 28 4.58 0.00 0 8 28 2.12 0.00 -8 9 28 4.67 0.00 -5 9 28 4.81 0.00 -2 9 28 2.37 0.00 -4 10 28 2.66 0.00 -1 3 29 0.16 0.00 -7 35 0 -0.57 0.00 -17 37 0 -3.32 0.00 -2 33 1 0.47 0.00 -11 36 1 -0.66 0.00 -19 37 1 -0.63 0.00 -32 32 2 -2.80 0.00 -25 36 2 -1.28 0.00 -29 34 3 -0.16 0.00 -5 34 3 0.99 0.00 -24 36 3 -2.17 0.00 -12 36 3 -2.19 0.00 -27 35 4 1.02 0.00 -23 36 4 -4.56 0.00 -6 34 5 1.69 0.00 -26 35 5 -2.28 0.00 -22 36 5 -1.04 0.00 -13 36 5 0.32 0.00 -25 35 6 0.09 0.00 -10 35 6 -1.32 0.00 -21 36 6 -0.14 0.00 -15 36 6 4.45 0.00 -30 32 7 2.35 0.00 -7 34 7 1.56 0.00 -24 35 7 -0.79 0.00 -28 33 8 -0.83 0.00 -23 35 8 0.69 0.00 -27 33 9 5.76 0.00 -6 33 9 0.84 0.00 -19 35 9 0.05 0.00 -16 35 9 2.14 0.00 -26 33 10 -0.65 0.00 -1 30 11 -1.10 0.00 -3 31 11 -2.76 0.00 -21 34 11 0.43 0.00 -15 34 11 -2.86 0.00 -25 32 12 -1.36 0.00 -7 32 12 1.95 0.00 -9 32 13 0.37 0.00 -20 33 13 -1.50 0.00 -17 33 13 -3.97 0.00 -14 33 13 -1.86 0.00 0 28 14 2.83 0.00 -2 29 14 1.86 0.00 -4 30 14 -0.24 0.00 -24 31 14 -1.13 0.00 -20 32 14 1.65 0.00 -11 32 14 0.53 0.00 -24 30 15 2.70 0.00 -6 30 15 1.63 0.00 -25 28 16 4.53 0.00 -24 29 16 2.77 0.00 -8 30 16 -1.43 0.00 -16 31 16 0.03 0.00 -25 27 17 -0.08 0.00 -8 29 17 0.52 0.00 -16 30 17 0.78 0.00 -13 30 17 -0.25 0.00 -16 29 18 4.51 0.00 -13 29 18 4.54 0.00 -20 27 19 -0.68 0.00 -16 28 19 4.53 0.00 -13 28 19 2.83 0.00 -21 25 20 1.95 0.00 -13 27 20 1.49 0.00 -17 25 21 -1.21 0.00 -8 25 21 -2.48 0.00 -18 23 22 2.86 0.00 -14 24 22 0.03 0.00 -8 24 22 1.39 0.00 -6 22 23 2.43 0.00 -11 23 23 0.37 0.00 -17 19 24 -2.08 0.00 -2 19 24 -1.10 0.00 -16 20 24 -1.42 0.00 -4 20 24 -0.93 0.00 -12 21 24 -0.91 0.00 -9 21 24 -0.86 0.00 -14 18 25 3.36 0.00 -13 19 25 2.33 0.00 -10 19 25 -0.78 0.00 -7 19 25 -3.66 0.00 -1 15 26 5.38 0.00 -12 16 26 -2.07 0.00 -3 16 26 4.56 0.00 -8 17 26 2.35 0.00 -11 13 27 2.42 0.00 -2 13 27 -2.42 0.00 -10 14 27 3.66 0.00 -7 14 27 1.44 0.00 -4 14 27 -2.76 0.00 -7 10 28 3.63 0.00 -1 10 28 0.88 0.00 -6 11 28 2.19 0.00 -3 4 29 0.28 0.00 -2 5 29 0.58 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 200618) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 -0.004 426 161 ' ' 2 0.333 0.667 0.235 432 162 ' ' 3 0.667 0.333 0.902 432 162 ' ' _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL shelx R -3 c :h R = 0.05 CELL 29.2590 29.2590 23.1650 90.00 90.00 120.00 SPGR R-3c # Solvent Accessible Volume = 1290 # Electrons Found in S.A.V. = 482 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 1.000 1.000 0.500 ! 4.95 eA-3 C102 1.000 0.998 0.453 ! 3.36 eA-3 C103 0.992 0.977 0.402 ! 2.68 eA-3 Q104 0.437 0.438 0.250 ! 1.82 eA-3 Q105 1.000 0.477 0.250 ! 1.30 eA-3 Q106 0.455 0.790 0.912 ! 1.29 eA-3 C107 1.000 1.000 0.250 ! 1.04 eA-3 C108 1.001 1.000 0.351 ! 0.98 eA-3 Q109 0.666 0.367 0.085 ! 0.87 eA-3 Q110 0.710 0.298 0.084 ! 0.87 eA-3 Q111 0.938 0.751 0.413 ! 0.87 eA-3 Q112 0.916 1.000 0.749 ! 0.83 eA-3 C113 0.651 0.369 0.436 ! 0.77 eA-3 Q114 0.956 0.014 0.403 ! 0.75 eA-3 Q115 0.858 0.750 0.413 ! 0.70 eA-3 C116 0.975 0.945 0.943 ! 0.65 eA-3 Q117 0.046 1.000 0.250 ! 0.60 eA-3 Q118 0.983 0.961 0.171 ! 0.59 eA-3 Q119 0.649 0.361 0.998 ! 0.59 eA-3 C120 0.310 0.689 0.833 ! 0.58 eA-3 Q121 0.229 0.775 0.078 ! 0.56 eA-3 C122 0.047 0.022 0.719 ! 0.53 eA-3 Q123 0.387 0.673 0.007 ! 0.53 eA-3 Q124 0.116 0.088 0.133 ! 0.53 eA-3 Q125 0.596 0.318 0.122 ! 0.53 eA-3 Q126 0.704 0.815 0.577 ! 0.51 eA-3 Q127 0.149 0.811 0.608 ! 0.50 eA-3 C128 0.578 0.288 0.397 ! 0.50 eA-3 ) ; _shelx_fab_checksum 63195 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z+1/2' 'x-y, -y, -z+1/2' '-x, -x+y, -z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+5/6' 'x-y+2/3, -y+1/3, -z+5/6' '-x+2/3, -x+y+1/3, -z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+7/6' 'x-y+1/3, -y+2/3, -z+7/6' '-x+1/3, -x+y+2/3, -z+7/6' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z-1/2' '-x+y, y, z-1/2' 'x, x-y, z-1/2' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z-1/6' '-x+y+2/3, y+1/3, z-1/6' 'x+2/3, x-y+1/3, z-1/6' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+1/6' '-x+y+1/3, y+2/3, z+1/6' 'x+1/3, x-y+2/3, z+1/6' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.40788(10) 0.32921(10) 0.43826(11) 0.0159(5) Uani 1 1 d . . . . . H1 H 0.3814 0.3298 0.4114 0.019 Uiso 1 1 calc R U . . . C2 C 0.38634(11) 0.32760(11) 0.49927(11) 0.0204(6) Uani 1 1 d . . . . . H2A H 0.3527 0.2941 0.5046 0.024 Uiso 1 1 calc R U . . . H2B H 0.4118 0.3289 0.5283 0.024 Uiso 1 1 calc R U . . . C3 C 0.37705(11) 0.37394(11) 0.50886(12) 0.0240(6) Uani 1 1 d . . . . . H3A H 0.3495 0.3711 0.4819 0.029 Uiso 1 1 calc R U . . . H3B H 0.3644 0.3727 0.5488 0.029 Uiso 1 1 calc R U . . . C4 C 0.42775(11) 0.42616(11) 0.49909(12) 0.0224(6) Uani 1 1 d . . . . . H4A H 0.4206 0.4556 0.5039 0.027 Uiso 1 1 calc R U . . . H4B H 0.4543 0.4304 0.5283 0.027 Uiso 1 1 calc R U . . . C5 C 0.44963(11) 0.42842(11) 0.43905(12) 0.0220(6) Uani 1 1 d . . . . . H5A H 0.4834 0.4619 0.4345 0.026 Uiso 1 1 calc R U . . . H5B H 0.4246 0.4278 0.4099 0.026 Uiso 1 1 calc R U . . . C6 C 0.45876(11) 0.38196(10) 0.42865(12) 0.0224(6) Uani 1 1 d . . . . . H6A H 0.4864 0.3846 0.4553 0.027 Uiso 1 1 calc R U . . . H6B H 0.4713 0.3835 0.3886 0.027 Uiso 1 1 calc R U . . . C7 C 0.45057(10) 0.28684(10) 0.35495(10) 0.0158(5) Uani 1 1 d . . . . . H7 H 0.4834 0.3209 0.3636 0.019 Uiso 1 1 calc R U . . . C8 C 0.42327(10) 0.29664(10) 0.30369(11) 0.0176(5) Uani 1 1 d . . . . . H8A H 0.3902 0.2636 0.2944 0.021 Uiso 1 1 calc R U . . . H8B H 0.4139 0.3237 0.3144 0.021 Uiso 1 1 calc R U . . . C9 C 0.45904(11) 0.31520(11) 0.25052(11) 0.0195(6) Uani 1 1 d . . . . . H9A H 0.4399 0.3195 0.2177 0.023 Uiso 1 1 calc R U . . . H9B H 0.4905 0.3499 0.2586 0.023 Uiso 1 1 calc R U . . . C10 C 0.47637(11) 0.27590(11) 0.23426(12) 0.0233(6) Uani 1 1 d . . . . . H10A H 0.5013 0.2899 0.2014 0.028 Uiso 1 1 calc R U . . . H10B H 0.4453 0.2424 0.2219 0.028 Uiso 1 1 calc R U . . . C11 C 0.50297(11) 0.26535(11) 0.28494(11) 0.0226(6) Uani 1 1 d . . . . . H11A H 0.5363 0.2980 0.2944 0.027 Uiso 1 1 calc R U . . . H11B H 0.5119 0.2380 0.2739 0.027 Uiso 1 1 calc R U . . . C12 C 0.46742(11) 0.24684(10) 0.33810(11) 0.0194(6) Uani 1 1 d . . . . . H12A H 0.4865 0.2421 0.3707 0.023 Uiso 1 1 calc R U . . . H12B H 0.4357 0.2123 0.3299 0.023 Uiso 1 1 calc R U . . . C13 C 0.44796(10) 0.25416(10) 0.47342(11) 0.0180(5) Uani 1 1 d . . . . . H13 H 0.4511 0.2247 0.4557 0.022 Uiso 1 1 calc R U . . . C14 C 0.41918(12) 0.23128(11) 0.53070(11) 0.0238(6) Uani 1 1 d . . . . . H14A H 0.4181 0.2594 0.5534 0.029 Uiso 1 1 calc R U . . . H14B H 0.3824 0.2032 0.5229 0.029 Uiso 1 1 calc R U . . . C15 C 0.44766(13) 0.20840(12) 0.56526(12) 0.0287(7) Uani 1 1 d . . . . . H15A H 0.4295 0.1949 0.6027 0.034 Uiso 1 1 calc R U . . . H15B H 0.4462 0.1785 0.5438 0.034 Uiso 1 1 calc R U . . . C16 C 0.50508(13) 0.25005(13) 0.57604(12) 0.0304(7) Uani 1 1 d . . . . . H16A H 0.5231 0.2335 0.5959 0.036 Uiso 1 1 calc R U . . . H16B H 0.5064 0.2777 0.6017 0.036 Uiso 1 1 calc R U . . . C17 C 0.53416(12) 0.27538(12) 0.51989(12) 0.0279(7) Uani 1 1 d . . . . . H17A H 0.5375 0.2488 0.4967 0.033 Uiso 1 1 calc R U . . . H17B H 0.5702 0.3044 0.5290 0.033 Uiso 1 1 calc R U . . . C18 C 0.50523(11) 0.29726(11) 0.48447(12) 0.0239(6) Uani 1 1 d . . . . . H18A H 0.5236 0.3108 0.4471 0.029 Uiso 1 1 calc R U . . . H18B H 0.5057 0.3269 0.5055 0.029 Uiso 1 1 calc R U . . . P1 P 0.40857(3) 0.26748(3) 0.42049(3) 0.01472(15) Uani 1 1 d . . . . . Ni1 Ni 0.3333 0.19103(2) 0.4167 0.01634(12) Uani 1 2 d S T P . . I1 I 0.3333 0.10612(2) 0.4167 0.02529(10) Uani 1 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0146(13) 0.0131(13) 0.0188(13) -0.0018(10) -0.0005(10) 0.0061(11) C2 0.0230(14) 0.0160(14) 0.0201(14) 0.0003(10) 0.0035(11) 0.0082(12) C3 0.0292(16) 0.0228(15) 0.0218(14) -0.0002(11) 0.0068(11) 0.0142(13) C4 0.0287(16) 0.0166(14) 0.0247(14) -0.0024(11) 0.0002(11) 0.0134(12) C5 0.0214(14) 0.0153(14) 0.0275(15) 0.0022(11) 0.0041(11) 0.0078(12) C6 0.0221(15) 0.0160(14) 0.0272(15) 0.0015(11) 0.0058(11) 0.0080(12) C7 0.0177(13) 0.0137(12) 0.0156(12) -0.0006(9) 0.0009(10) 0.0075(11) C8 0.0189(14) 0.0140(13) 0.0183(13) 0.0005(10) -0.0003(10) 0.0071(11) C9 0.0212(14) 0.0188(14) 0.0165(13) 0.0010(10) 0.0006(10) 0.0085(12) C10 0.0257(15) 0.0207(14) 0.0217(14) -0.0001(11) 0.0056(11) 0.0103(13) C11 0.0277(15) 0.0216(15) 0.0222(14) 0.0016(11) 0.0069(11) 0.0152(13) C12 0.0235(14) 0.0198(14) 0.0187(13) 0.0005(10) 0.0018(11) 0.0138(12) C13 0.0197(14) 0.0154(13) 0.0191(13) -0.0011(10) -0.0013(10) 0.0090(11) C14 0.0285(16) 0.0239(15) 0.0198(14) 0.0035(11) 0.0010(11) 0.0136(13) C15 0.0399(18) 0.0282(16) 0.0209(14) 0.0035(12) 0.0005(12) 0.0193(15) C16 0.0425(19) 0.0320(17) 0.0258(15) -0.0047(13) -0.0087(13) 0.0256(16) C17 0.0281(16) 0.0314(17) 0.0270(15) -0.0017(12) -0.0095(12) 0.0170(14) C18 0.0228(15) 0.0187(14) 0.0267(15) 0.0000(11) -0.0071(11) 0.0077(12) P1 0.0153(3) 0.0130(3) 0.0155(3) -0.0003(2) 0.0008(2) 0.0069(3) Ni1 0.0141(3) 0.01320(19) 0.0220(3) -0.00007(9) -0.00014(18) 0.00704(13) I1 0.02133(15) 0.01541(12) 0.04111(18) 0.00039(5) 0.00078(11) 0.01066(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 C1 C2 109.9(2) . . ? C6 C1 P1 117.93(18) . . ? C2 C1 P1 112.09(18) . . ? C6 C1 H1 105.2 . . ? C2 C1 H1 105.2 . . ? P1 C1 H1 105.2 . . ? C3 C2 C1 111.0(2) . . ? C3 C2 H2A 109.4 . . ? C1 C2 H2A 109.4 . . ? C3 C2 H2B 109.4 . . ? C1 C2 H2B 109.4 . . ? H2A C2 H2B 108.0 . . ? C4 C3 C2 110.7(2) . . ? C4 C3 H3A 109.5 . . ? C2 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C2 C3 H3B 109.5 . . ? H3A C3 H3B 108.1 . . ? C5 C4 C3 111.0(2) . . ? C5 C4 H4A 109.4 . . ? C3 C4 H4A 109.4 . . ? C5 C4 H4B 109.4 . . ? C3 C4 H4B 109.4 . . ? H4A C4 H4B 108.0 . . ? C4 C5 C6 111.3(2) . . ? C4 C5 H5A 109.4 . . ? C6 C5 H5A 109.4 . . ? C4 C5 H5B 109.4 . . ? C6 C5 H5B 109.4 . . ? H5A C5 H5B 108.0 . . ? C5 C6 C1 111.0(2) . . ? C5 C6 H6A 109.4 . . ? C1 C6 H6A 109.4 . . ? C5 C6 H6B 109.4 . . ? C1 C6 H6B 109.4 . . ? H6A C6 H6B 108.0 . . ? C12 C7 C8 110.0(2) . . ? C12 C7 P1 113.14(17) . . ? C8 C7 P1 111.27(17) . . ? C12 C7 H7 107.4 . . ? C8 C7 H7 107.4 . . ? P1 C7 H7 107.4 . . ? C9 C8 C7 111.2(2) . . ? C9 C8 H8A 109.4 . . ? C7 C8 H8A 109.4 . . ? C9 C8 H8B 109.4 . . ? C7 C8 H8B 109.4 . . ? H8A C8 H8B 108.0 . . ? C10 C9 C8 111.1(2) . . ? C10 C9 H9A 109.4 . . ? C8 C9 H9A 109.4 . . ? C10 C9 H9B 109.4 . . ? C8 C9 H9B 109.4 . . ? H9A C9 H9B 108.0 . . ? C9 C10 C11 111.1(2) . . ? C9 C10 H10A 109.4 . . ? C11 C10 H10A 109.4 . . ? C9 C10 H10B 109.4 . . ? C11 C10 H10B 109.4 . . ? H10A C10 H10B 108.0 . . ? C10 C11 C12 111.5(2) . . ? C10 C11 H11A 109.3 . . ? C12 C11 H11A 109.3 . . ? C10 C11 H11B 109.3 . . ? C12 C11 H11B 109.3 . . ? H11A C11 H11B 108.0 . . ? C11 C12 C7 111.0(2) . . ? C11 C12 H12A 109.4 . . ? C7 C12 H12A 109.4 . . ? C11 C12 H12B 109.4 . . ? C7 C12 H12B 109.4 . . ? H12A C12 H12B 108.0 . . ? C14 C13 C18 110.5(2) . . ? C14 C13 P1 113.62(19) . . ? C18 C13 P1 118.46(18) . . ? C14 C13 H13 104.2 . . ? C18 C13 H13 104.2 . . ? P1 C13 H13 104.2 . . ? C15 C14 C13 110.1(2) . . ? C15 C14 H14A 109.6 . . ? C13 C14 H14A 109.6 . . ? C15 C14 H14B 109.6 . . ? C13 C14 H14B 109.6 . . ? H14A C14 H14B 108.2 . . ? C16 C15 C14 111.1(2) . . ? C16 C15 H15A 109.4 . . ? C14 C15 H15A 109.4 . . ? C16 C15 H15B 109.4 . . ? C14 C15 H15B 109.4 . . ? H15A C15 H15B 108.0 . . ? C15 C16 C17 111.9(2) . . ? C15 C16 H16A 109.2 . . ? C17 C16 H16A 109.2 . . ? C15 C16 H16B 109.2 . . ? C17 C16 H16B 109.2 . . ? H16A C16 H16B 107.9 . . ? C16 C17 C18 111.7(3) . . ? C16 C17 H17A 109.3 . . ? C18 C17 H17A 109.3 . . ? C16 C17 H17B 109.3 . . ? C18 C17 H17B 109.3 . . ? H17A C17 H17B 107.9 . . ? C17 C18 C13 110.6(2) . . ? C17 C18 H18A 109.5 . . ? C13 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 108.1 . . ? C13 P1 C7 102.65(12) . . ? C13 P1 C1 111.55(12) . . ? C7 P1 C1 102.21(11) . . ? C13 P1 Ni1 102.83(9) . . ? C7 P1 Ni1 116.52(8) . . ? C1 P1 Ni1 119.99(8) . . ? P1 Ni1 P1 118.45(4) . 12 ? P1 Ni1 I1 120.77(2) . . ? P1 Ni1 I1 120.78(2) 12 . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C6 1.533(4) . ? C1 C2 1.539(4) . ? C1 P1 1.862(3) . ? C1 H1 1.0000 . ? C2 C3 1.526(4) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.523(4) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C4 C5 1.519(4) . ? C4 H4A 0.9900 . ? C4 H4B 0.9900 . ? C5 C6 1.530(4) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C12 1.530(3) . ? C7 C8 1.536(3) . ? C7 P1 1.855(3) . ? C7 H7 1.0000 . ? C8 C9 1.529(3) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 C10 1.518(4) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C10 C11 1.523(4) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 C12 1.526(4) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C14 1.534(4) . ? C13 C18 1.533(4) . ? C13 P1 1.853(3) . ? C13 H13 1.0000 . ? C14 C15 1.530(4) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 C16 1.524(4) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C16 C17 1.528(4) . ? C16 H16A 0.9900 . ? C16 H16B 0.9900 . ? C17 C18 1.530(4) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? P1 Ni1 2.2212(7) . ? Ni1 P1 2.2214(7) 12 ? Ni1 I1 2.4841(6) . ?