#------------------------------------------------------------------------------ #$Date: 2021-09-03 23:27:52 +0300 (Fri, 03 Sep 2021) $ #$Revision: 268440 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519015.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519015 loop_ _publ_author_name 'Zheng, Zhiwei' 'Arai, Tsuyoshi' 'Takao, Koichiro' _publ_section_title ; Complexation-Distribution Separated Solvent Extraction Process Designed for Rapid and Efficient Recovery of Inert Platinum Group Metals. ; _journal_issue 33 _journal_name_full 'ACS omega' _journal_page_first 21809 _journal_page_last 21818 _journal_paper_doi 10.1021/acsomega.1c03565 _journal_volume 6 _journal_year 2021 _chemical_formula_moiety 'C18 H16 N4 O8 Ru, O' _chemical_formula_sum 'C20 H16 N2 O9 Ru' _chemical_formula_weight 529.42 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-03-23 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-07-21 deposited with the CCDC. 2021-07-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 116.707(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.9414(4) _cell_length_b 15.0754(3) _cell_length_c 12.8497(5) _cell_measurement_reflns_used 5727 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 30.2740 _cell_measurement_theta_min 2.3140 _cell_volume 2066.44(15) _computing_cell_refinement 'CrysAlisPro 1.171.40.60a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.60a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.60a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293 _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 0.942 _diffrn_measured_fraction_theta_max 0.871 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 10.00 110.00 0.50 95.00 -- 20.00 54.00-150.00 200 2 \w 52.00 100.00 0.50 95.00 -- 20.00 54.00 150.00 96 3 \w -38.00 -13.00 0.50 95.00 -- 20.00 54.00 0.00 50 4 \w -74.00 -29.00 0.50 95.00 -- 20.00 54.00 -90.00 90 5 \w 6.00 62.00 0.50 95.00 -- 20.00 54.00 -90.00 112 6 \w -61.00 -29.00 0.50 95.00 -- 20.00 54.00-150.00 64 ; _diffrn_measurement_device 'two-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Mini II' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0400 _diffrn_reflns_av_unetI/netI 0.0500 _diffrn_reflns_Laue_measured_fraction_full 0.942 _diffrn_reflns_Laue_measured_fraction_max 0.871 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 11272 _diffrn_reflns_point_group_measured_fraction_full 0.942 _diffrn_reflns_point_group_measured_fraction_max 0.871 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.852 _diffrn_reflns_theta_min 2.230 _exptl_absorpt_coefficient_mu 0.815 _exptl_absorpt_correction_T_max 0.958 _exptl_absorpt_correction_T_min 0.905 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.60a (Rigaku Oxford Diffraction, 2019) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) ; _exptl_crystal_colour brown _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.702 _exptl_crystal_description plate _exptl_crystal_F_000 1064 _exptl_crystal_size_max 0.314 _exptl_crystal_size_mid 0.225 _exptl_crystal_size_min 0.121 _refine_diff_density_max 1.015 _refine_diff_density_min -0.502 _refine_diff_density_rms 0.149 _refine_ls_extinction_coef 0.0026(6) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2017/1 (Sheldrick 2017)' _refine_ls_goodness_of_fit_ref 0.957 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 292 _refine_ls_number_reflns 5672 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.957 _refine_ls_R_factor_all 0.0601 _refine_ls_R_factor_gt 0.0387 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0719P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1017 _refine_ls_wR_factor_ref 0.1148 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4152 _reflns_number_total 5672 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao1c03565_si_002.cif _cod_data_source_block 200803_weber_ru-tbpda_a_ _cod_original_cell_volume 2066.44(14) _cod_database_code 4519015 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C8(H8A,H8B), C10(H10A,H10B) 2.b Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C14(H14), C16(H16), C5(H5), C15(H15) 2.c Idealised Me refined as rotating group: C9(H9A,H9B,H9C), C11(H11A,H11B,H11C) ; _shelx_res_file ; TITL 200803_weber_ru-tbpda_a__a.res in P2(1)/c 200803_weber_ru-tbpda_a_.res created by SHELXL-2017/1 at 10:08:24 on 23-Mar-2021 REM Old TITL 200803_Weber_Ru-TBPDA_a_ in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.094, Rweak 0.006, Alpha 0.050 REM 0.416 for 152 systematic absences, Orientation as input REM Formula found by SHELXT: C15 N3 O9 Ru CELL 0.71073 11.9414 15.0754 12.8497 90 116.707 90 ZERR 4 0.0004 0.0003 0.0005 0 0.005 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O Ru UNIT 80 64 8 36 4 L.S. 10 PLAN 20 MORE -1 BOND $H CONF fmap 2 acta REM REM REM WGHT 0.071900 EXTI 0.002607 FVAR 0.42065 RU1 5 0.371181 0.617482 0.689430 11.00000 0.03671 0.02917 = 0.03524 -0.00106 0.01738 0.00182 O2 4 0.467472 0.504557 0.733028 11.00000 0.05018 0.03540 = 0.04285 0.00359 0.01933 0.00836 O7 4 0.537070 0.674597 0.711228 11.00000 0.04523 0.04154 = 0.05002 -0.00523 0.02506 -0.00429 O5 4 0.240938 0.553978 0.726992 11.00000 0.04858 0.04679 = 0.05684 0.00083 0.03033 -0.00560 N4 3 0.449166 0.636231 0.858586 11.00000 0.04619 0.03157 = 0.03669 -0.00088 0.01807 0.00892 N2 3 0.314740 0.559149 0.521561 11.00000 0.03686 0.02761 = 0.04189 -0.00605 0.02203 -0.00500 O3 4 0.504884 0.376102 0.669991 11.00000 0.06805 0.03779 = 0.06630 0.00214 0.02942 0.01469 O8 4 0.716747 0.723718 0.852008 11.00000 0.04929 0.09796 = 0.08986 -0.02501 0.02689 -0.02312 O6 4 0.207095 0.520844 0.879441 11.00000 0.09149 0.06908 = 0.09750 0.00926 0.07065 -0.00397 O4 4 0.257436 0.743215 0.410108 11.00000 0.05015 0.03892 = 0.08168 -0.00020 0.02743 -0.00939 N1 3 0.291239 0.718136 0.656822 11.00000 0.04484 0.03839 = 0.03825 -0.00214 0.01717 0.00691 O1 4 0.240942 0.785442 0.638896 11.00000 0.08729 0.04882 = 0.06172 0.00278 0.02582 0.03052 N3 3 0.066856 0.693673 0.379637 11.00000 0.04474 0.04255 = 0.05826 0.00560 0.02602 0.00367 C2 1 0.368689 0.478688 0.529975 11.00000 0.03536 0.03095 = 0.04547 -0.00340 0.02160 -0.00467 C3 1 0.350253 0.428463 0.434481 11.00000 0.04700 0.03452 = 0.05476 -0.01020 0.02756 -0.00622 AFIX 43 H3 2 0.390454 0.374125 0.443509 11.00000 -1.20000 AFIX 0 C1 1 0.453887 0.447888 0.651231 11.00000 0.04098 0.03006 = 0.05062 0.00178 0.02535 -0.00007 C4 1 0.271392 0.459772 0.325252 11.00000 0.05943 0.04753 = 0.05573 -0.01746 0.03364 -0.01114 AFIX 43 H4 2 0.256628 0.426578 0.259325 11.00000 -1.20000 AFIX 0 C13 1 0.390727 0.601413 0.915988 11.00000 0.06054 0.03363 = 0.04742 0.00401 0.03193 0.01491 C17 1 0.563534 0.672170 0.906585 11.00000 0.04863 0.03300 = 0.04841 -0.00476 0.01438 0.00809 C7 1 0.186775 0.682546 0.402884 11.00000 0.04362 0.03571 = 0.03647 -0.00049 0.01613 -0.00384 C12 1 0.269451 0.555365 0.837918 11.00000 0.06719 0.04091 = 0.06931 0.00696 0.04649 0.00723 C14 1 0.448386 0.606053 1.035900 11.00000 0.08671 0.04504 = 0.04301 0.00732 0.03399 0.02557 AFIX 43 H14 2 0.409831 0.582811 1.078705 11.00000 -1.20000 AFIX 0 C16 1 0.623843 0.677993 1.027896 11.00000 0.05984 0.04736 = 0.04779 -0.00959 0.00217 0.00946 AFIX 43 H16 2 0.703184 0.703190 1.066126 11.00000 -1.20000 AFIX 0 C6 1 0.237423 0.589619 0.414781 11.00000 0.03442 0.03610 = 0.03847 -0.00157 0.01627 -0.00780 C5 1 0.214347 0.541397 0.314915 11.00000 0.04848 0.05252 = 0.03788 -0.00545 0.01809 -0.00925 AFIX 43 H5 2 0.161020 0.563817 0.241786 11.00000 -1.20000 AFIX 0 C18 1 0.611377 0.693414 0.819305 11.00000 0.04571 0.04239 = 0.06636 -0.00541 0.02459 -0.00099 C15 1 0.563627 0.645608 1.090645 11.00000 0.09907 0.05051 = 0.03694 0.00149 0.02146 0.02689 AFIX 43 H15 2 0.602282 0.650880 1.171366 11.00000 -1.20000 AFIX 0 C8 1 -0.021895 0.620234 0.364862 11.00000 0.04474 0.06378 = 0.06214 -0.00172 0.02291 -0.01013 AFIX 23 H8A 2 0.015633 0.564565 0.359037 11.00000 -1.20000 H8B 2 -0.097579 0.628858 0.292652 11.00000 -1.20000 AFIX 0 C10 1 0.016732 0.783991 0.356999 11.00000 0.06430 0.05669 = 0.09612 0.02375 0.04546 0.01947 AFIX 23 H10A 2 0.079367 0.824894 0.409462 11.00000 -1.20000 H10B 2 -0.056196 0.787480 0.371443 11.00000 -1.20000 AFIX 0 C9 1 -0.055724 0.614665 0.463116 11.00000 0.06579 0.06654 = 0.08551 0.00622 0.04187 -0.00243 AFIX 137 H9A 2 -0.115951 0.568129 0.448003 11.00000 -1.50000 H9B 2 -0.091080 0.670096 0.470505 11.00000 -1.50000 H9C 2 0.018077 0.602184 0.534108 11.00000 -1.50000 AFIX 0 C11 1 -0.019425 0.810095 0.232555 11.00000 0.06898 0.10146 = 0.10184 0.04856 0.03097 0.02398 AFIX 137 H11A 2 -0.086057 0.772464 0.180795 11.00000 -1.50000 H11B 2 0.051776 0.803712 0.217219 11.00000 -1.50000 H11C 2 -0.046993 0.870711 0.220491 11.00000 -1.50000 AFIX 0 O9 4 0.077545 0.434436 0.977944 11.00000 0.25596 0.44538 = 0.40306 0.25686 0.24190 0.06169 HKLF 4 REM 200803_weber_ru-tbpda_a__a.res in P2(1)/c REM R1 = 0.0387 for 4152 Fo > 4sig(Fo) and 0.0601 for all 5672 data REM 292 parameters refined using 0 restraints END WGHT 0.0718 0.0000 REM Highest difference peak 1.015, deepest hole -0.502, 1-sigma level 0.149 Q1 1 0.0779 0.4001 0.9449 11.00000 0.05 1.01 Q2 1 0.4413 0.6185 0.7263 11.00000 0.05 0.90 Q3 1 0.3000 0.6160 0.6522 11.00000 0.05 0.67 Q4 1 0.1441 0.4925 1.0529 11.00000 0.05 0.65 Q5 1 0.3562 0.6185 0.7363 11.00000 0.05 0.65 Q6 1 0.3911 0.6201 0.6456 11.00000 0.05 0.60 Q7 1 0.3691 0.5726 0.6891 11.00000 0.05 0.56 Q8 1 0.0032 0.4647 0.9382 11.00000 0.05 0.55 Q9 1 0.6899 0.6805 0.8469 11.00000 0.05 0.51 Q10 1 0.7260 0.7396 0.8126 11.00000 0.05 0.49 Q11 1 0.4732 0.6571 0.7034 11.00000 0.05 0.48 Q12 1 0.3701 0.6691 0.6868 11.00000 0.05 0.47 Q13 1 0.7139 0.6789 1.0358 11.00000 0.05 0.46 Q14 1 0.6210 0.6430 0.7729 11.00000 0.05 0.44 Q15 1 0.1910 0.3912 1.0968 11.00000 0.05 0.44 Q16 1 0.5622 0.6232 0.6926 11.00000 0.05 0.44 Q17 1 0.7082 0.7417 0.9055 11.00000 0.05 0.43 Q18 1 0.5774 0.6774 1.0682 11.00000 0.05 0.43 Q19 1 0.6809 0.7496 0.8331 11.00000 0.05 0.42 Q20 1 0.7125 0.7668 0.8685 11.00000 0.05 0.42 ; _shelx_res_checksum 5946 _shelx_hkl_file ; 0 0 2 2822.25 72.1387 4 0 0 -2 2795.18 72.0870 4 0 0 -2 2773.66 72.0439 6 0 0 3 2.08506 2.14774 4 0 0 -3 1.12359 1.88624 4 0 0 -3 0.40396 1.68927 6 0 0 -4 1405.46 36.8065 6 0 0 -4 1379.56 36.8327 4 0 0 4 1382.10 37.0407 4 0 0 5 0.74964 2.35177 4 0 0 -5 0.27018 2.05827 4 0 0 -5 0.12992 2.13315 6 0 0 -6 1116.49 30.7544 6 0 0 6 1149.20 31.2964 4 0 0 7-0.38626 2.71745 4 0 0 8 800.780 23.7064 4 0 0 9 1.22511 3.55196 4 0 0 10 200.190 9.21651 4 0 0 11 0.12761 4.39973 4 0 0 12 6.17447 4.66929 4 0 0 13 0.30578 4.76806 4 0 0 14 55.1923 6.63177 4 0 0 15 1.23119 5.53590 4 0 0 16 18.7545 6.42490 4 0 -1 1 266.228 8.68320 4 0 -1 1 382.109 8.67401 6 0 1 -2 477.316 13.1218 6 0 -1 2 489.039 13.1432 6 0 -1 2 485.546 13.3672 4 0 -1 -2 480.812 13.1558 4 0 1 2 510.017 13.2185 4 0 -1 3 3214.30 83.4034 6 0 1 -3 3245.54 83.3265 6 0 -1 -3 3132.79 83.3477 4 0 -1 3 3229.35 83.6367 4 0 1 3 3329.57 83.4971 4 0 1 -4 1734.91 46.1076 6 0 1 -4 1794.92 46.3189 4 0 -1 -4 1783.48 46.1945 4 0 1 4 1692.75 46.3258 4 0 -1 4 1787.93 46.5428 4 0 -1 -5 4377.96 114.683 6 0 1 -5 4379.45 114.528 6 0 1 -5 4467.27 114.719 4 0 -1 -5 4493.00 114.628 4 0 1 5 4348.06 114.887 4 0 -1 5 4506.00 115.066 4 0 1 -6 2386.66 64.8687 6 0 1 6 2499.78 65.4143 4 0 -1 6 2558.92 65.6115 4 0 -1 7 485.998 15.3908 4 0 1 7 490.707 15.2310 4 0 -1 8-0.18361 3.34933 4 0 1 8-1.30920 3.03880 4 0 1 9 9.07646 3.55366 4 0 -1 9 11.4880 3.78810 4 0 1 10 20.5512 4.45460 4 0 -1 10 17.9404 4.31742 4 0 -1 11 125.427 7.71726 4 0 1 11 127.982 7.56660 4 0 -1 12 83.6490 7.00706 4 0 1 12 89.1914 6.91107 4 0 -1 13 86.6570 7.41916 4 0 1 13 79.3297 7.17347 4 0 -1 14 39.2351 6.37699 4 0 1 14 39.7994 6.20842 4 0 -1 15 8.40302 5.70005 4 0 1 15 13.4773 5.85459 4 0 -1 16 3.39727 5.83747 4 0 -2 0 60.1083 1.82011 1 0 2 0 33.9143 1.60857 1 0 2 0 54.2835 1.95396 2 0 -2 0 66.6928 2.06516 2 0 -2 1 6007.55 20.3162 2 0 2 -1 5707.92 20.3154 2 0 -2 1 5485.95 19.5306 1 0 2 -1 5729.66 19.6179 1 0 -2 1 6113.01 20.4913 4 0 2 -1 5989.72 20.3389 4 0 -2 2 8.90379 1.58030 6 0 -2 2 6.37343 1.12268 2 0 2 -2 7.78463 1.12689 2 0 2 -2 7.35496 1.65247 4 0 -2 -2 6.62777 1.37674 4 0 -2 2 7.35797 1.85098 4 0 2 2 6.79726 1.48320 4 0 -2 3 3324.32 86.7506 6 0 2 -3 3369.74 86.6693 6 0 -2 3 3240.92 86.2066 2 0 2 3 3440.77 86.8237 4 0 -2 3 3543.98 87.1268 4 0 -2 -3 3439.17 86.7152 4 0 2 -4 1823.79 45.0887 6 0 -2 4 1806.47 45.2145 6 0 -2 4 1579.73 44.2492 2 0 2 4 1858.92 45.3461 4 0 -2 4 1788.37 45.6067 4 0 -2 -4 1771.65 45.1312 4 0 2 -5 224.269 7.22478 6 0 -2 5 203.761 6.06239 2 0 -2 -5 239.199 7.33177 4 0 2 5 237.727 7.61495 4 0 -2 5 233.320 7.90779 4 0 -2 -6 1.49867 2.11174 4 0 2 6 0.91593 2.52595 4 0 -2 6 1.11034 2.87672 4 0 2 -6 0.28513 2.15911 6 0 2 7 754.536 22.0227 4 0 -2 7 761.377 22.3569 4 0 2 8 40.4380 4.02746 4 0 -2 8 40.8871 4.24540 4 0 2 9 719.817 21.7361 4 0 -2 9 702.704 21.9958 4 0 2 10-0.98760 3.80345 4 0 -2 10 2.87024 4.04455 4 0 2 11 51.8330 5.55750 4 0 -2 11 53.8159 5.75165 4 0 -2 12-3.49207 4.92875 4 0 2 12-0.67368 4.57121 4 0 -2 13 8.21970 5.17725 4 0 2 13 4.70178 4.99511 4 0 2 14 9.51460 5.45425 4 0 -2 14 13.1082 5.61762 4 0 2 15 49.7525 6.91371 4 0 -2 15 48.8377 7.08982 4 0 -2 16 9.18128 6.11169 4 0 3 0 0.26074 1.70752 2 0 -3 0-1.62567 1.52848 1 0 3 0 0.01726 1.33906 1 0 3 -1 66.6104 2.68406 2 0 3 1 75.5852 3.05610 2 0 -3 1 64.1304 2.57795 2 0 3 1 54.6789 2.84707 1 0 3 -1 57.3907 2.24004 1 0 -3 1 57.0576 2.25573 1 0 -3 1 69.0373 2.37754 4 0 -3 -1 78.9542 3.17324 3 0 3 1 73.0390 2.85460 3 0 -3 2 428.822 8.57318 1 0 3 -2 423.598 8.68900 2 0 -3 2 433.467 8.61908 2 0 3 2 416.073 8.40958 4 0 -3 -2 426.085 8.34837 4 0 -3 2 437.032 9.01675 4 0 3 -2 443.903 8.91224 4 0 -3 3 1262.24 32.9850 6 0 3 -3 1193.22 32.6883 2 0 -3 3 1235.65 32.6492 2 0 3 3 1294.90 32.9820 4 0 -3 3 1273.08 33.3932 4 0 3 -3 1285.34 33.2508 4 0 -3 -3 1272.78 32.8700 4 0 -3 4 351.056 10.1892 6 0 -3 4 331.366 9.50394 2 0 3 4 346.084 10.2841 4 0 -3 4 359.293 10.7759 4 0 3 -4 362.981 10.4773 4 0 -3 -4 355.432 10.1144 4 0 -3 5 373.917 6.02751 6 0 3 -5 359.828 5.61646 6 0 -3 5 359.755 3.69050 2 0 -3 5 381.011 7.12626 4 0 3 5 382.328 6.30875 4 0 -3 -5 365.127 5.73052 4 0 -3 6 1386.95 38.3642 4 0 3 6 1417.12 37.9733 4 0 -3 -6 1399.41 37.5314 4 0 3 -6 1397.02 37.4633 6 0 -3 7 114.787 5.99071 4 0 3 7 111.576 5.44504 4 0 -3 8 106.168 6.23726 4 0 3 8 107.407 5.77627 4 0 3 9 8.90218 3.65751 4 0 -3 9 5.11939 4.12843 4 0 -3 10 61.6714 6.01911 4 0 3 10 67.8706 5.50960 4 0 -3 11 108.593 7.46413 4 0 3 11 113.455 7.01686 4 0 -3 12 240.405 11.1579 4 0 3 12 217.755 10.4992 4 0 3 13 81.4426 6.79257 4 0 -3 13 71.6188 7.24411 4 0 3 14 71.6082 6.89508 4 0 -3 14 70.1085 7.43770 4 0 -3 15 32.5495 6.65593 4 0 3 16 3.49669 6.37502 1 0 -3 16 5.42235 6.29247 4 0 4 0 2455.69 51.0836 1 0 4 0 2853.21 51.7436 2 0 -4 1 0.03878 1.22929 1 0 4 1-0.05861 1.72648 1 0 -4 -1 1.71838 1.89814 1 0 4 -1 1.77777 1.12450 1 0 -4 1 0.43458 1.16004 4 0 -4 -1 0.91577 2.07650 3 0 4 1 0.13756 1.90415 2 0 -4 1 2.18984 1.48901 2 0 4 1-0.99864 1.67661 3 0 4 -1-0.23943 1.68947 2 0 -4 2 263.832 6.11343 2 0 4 -2 247.974 6.20215 2 0 4 -2 254.877 5.92270 1 0 4 2 266.285 6.75968 2 0 -4 2 225.994 5.84260 1 0 -4 2 263.788 6.17934 4 0 -4 -2 247.603 5.41308 4 0 4 2 264.271 6.51401 3 0 -4 3 129.388 4.23414 1 0 -4 3 156.273 4.48954 6 0 4 -3 155.783 4.45951 2 0 -4 3 154.503 4.33846 2 0 4 3 158.619 4.34243 4 0 -4 3 156.398 4.95101 4 0 -4 -3 159.245 4.26371 4 0 -4 4 14.7427 1.76349 1 0 -4 4 18.8033 1.97978 6 0 -4 4 19.0978 1.56775 2 0 4 4 19.5843 2.08919 4 0 -4 -4 19.2466 1.90487 4 0 -4 4 16.6550 2.50719 4 0 -4 5 45.7181 2.97639 6 0 -4 5 47.1117 2.14577 2 0 -4 5 46.1945 3.55823 4 0 4 5 48.5423 3.07364 4 0 -4 -5 44.8817 2.84458 4 0 4 6 349.804 11.2906 4 0 -4 6 346.957 11.7796 4 0 -4 -6 365.244 10.9954 4 0 -4 6 375.711 11.2429 6 0 4 7 3.82197 2.59180 4 0 -4 7 4.28790 3.11693 4 0 4 7 1.92665 1.99689 2 0 -4 8 1244.70 35.5713 4 0 4 8 1261.83 34.9420 4 0 4 9 6.62859 3.53998 4 0 -4 9 1.88817 3.99862 4 0 4 10 353.106 12.9116 4 0 -4 10 362.988 13.6549 4 0 4 11 21.5333 4.61660 4 0 -4 11 15.6303 4.94013 4 0 4 12 9.62973 4.40747 4 0 -4 12 4.95273 4.79151 4 0 -4 13 5.85863 5.28014 4 0 -4 14 34.9742 6.43774 4 0 4 15 4.49535 6.21058 1 0 -4 15 6.32187 6.02165 4 0 4 16 14.4851 6.74676 1 0 -5 0 0.03522 0.70337 4 0 5 0-0.04049 1.94744 2 0 -5 0-0.44014 2.08502 3 0 5 1 804.474 11.3667 1 0 -5 1 779.880 10.4055 1 0 -5 1 1010.34 11.7106 2 0 5 -1 911.155 10.8275 1 0 -5 1 1007.00 10.3958 4 0 5 1 1002.63 11.7704 3 0 -5 -1 1048.78 12.2224 3 0 5 1 999.873 12.4926 2 0 5 -1 1019.96 12.1444 2 0 -5 2 420.333 12.0862 1 0 5 -2 403.674 12.0682 1 0 5 2 489.509 12.7112 3 0 -5 2 483.426 12.3511 4 0 -5 -2 449.907 11.5492 4 0 5 2 465.757 12.9738 2 0 -5 2 457.183 12.3835 2 0 5 -2 453.920 12.6102 2 0 5 -3 2070.09 50.3911 2 0 -5 3 2069.63 50.2263 2 0 5 3 2100.55 50.9616 2 0 -5 3 1889.36 50.0359 1 0 -5 -3 2008.48 49.7716 4 0 -5 3 2044.58 50.6319 4 0 -5 4 398.660 10.0154 1 0 -5 4 435.370 10.2631 6 0 -5 4 446.774 9.91849 2 0 5 4 453.116 10.9409 2 0 5 -4 447.396 10.1083 2 0 -5 4 467.085 11.0521 4 0 5 4 441.567 10.1329 4 0 -5 -4 430.805 9.87911 4 0 -5 5 659.961 19.3948 1 0 5 5 728.028 20.0755 2 0 -5 5 705.871 19.6689 6 0 -5 5 701.051 19.0503 2 0 5 5 727.365 19.6552 4 0 -5 5 719.423 20.4114 4 0 -5 -5 720.984 19.4428 4 0 -5 6 203.447 7.05431 1 0 -5 6 207.991 7.38515 6 0 5 6 211.847 7.54138 2 0 5 6 214.604 7.53742 4 0 -5 6 214.104 8.15932 4 0 -5 -6 220.496 7.12239 4 0 -5 7 5.21664 2.52674 6 0 -5 7 7.02534 3.30138 4 0 5 7 4.07829 2.48943 4 0 5 7 1.47597 2.04709 2 0 5 8 15.3333 3.32547 4 0 -5 8 10.9413 3.72709 4 0 5 9 119.968 6.46180 4 0 -5 9 127.426 7.11719 4 0 -5 10 96.1507 6.88441 4 0 5 10 88.4570 5.89007 4 0 -5 11 210.404 10.3071 4 0 -5 12 108.769 7.93848 4 0 -5 13 125.718 8.69626 4 0 5 14 13.7819 6.30839 1 0 -5 14 22.6240 6.13491 4 0 5 15 13.8080 6.46014 1 0 -5 15 38.1224 7.07191 4 0 5 16 15.3725 6.74611 1 0 6 0 128.024 4.26016 1 0 -6 0 147.025 3.13127 5 0 6 0 143.330 4.95936 2 0 -6 0 151.824 3.18469 4 0 -6 0 146.615 4.93503 3 0 6 -1 145.431 4.73269 2 0 6 1 147.936 4.91565 2 0 6 1 114.390 4.30841 1 0 6 -1 134.703 3.91696 1 0 -6 1 150.546 3.50426 4 0 -6 -1 152.181 4.83228 3 0 6 2 75.7942 4.00350 2 0 6 -2 69.1047 3.48626 2 0 -6 2 73.1873 3.25579 2 0 6 2 41.8133 3.54547 1 0 6 -2 67.2222 2.96138 1 0 -6 2 58.3919 2.90591 1 0 -6 2 74.5101 3.07812 4 0 6 2 76.3422 3.69369 3 0 6 -3 97.0477 3.61134 1 0 -6 3 93.8002 3.48687 1 0 6 -3 97.7882 4.05448 2 0 -6 3 98.9768 3.76168 2 0 6 3 100.101 4.57049 2 0 -6 3 93.3049 3.83606 4 0 6 3 101.887 4.33818 3 0 -6 -3 92.4719 2.92241 4 0 -6 4 46.0947 2.57537 1 0 -6 4 46.1767 2.76122 6 0 6 -4 46.3604 2.75775 2 0 -6 4 47.0165 2.60175 2 0 6 4 50.4793 3.51124 2 0 -6 4 52.5627 3.25639 4 0 -6 -4 45.3045 2.24229 4 0 -6 5 161.557 5.10650 6 0 6 5 153.386 5.63552 2 0 -6 5 156.050 5.76329 4 0 6 5 146.986 4.82117 4 0 -6 5 139.146 4.60912 1 0 -6 6 110.701 4.62311 6 0 6 6 114.007 5.05275 2 0 6 6 113.432 4.68652 4 0 -6 6 113.813 5.51184 4 0 6 7 349.128 11.0669 4 0 -6 7 342.074 11.8944 4 0 -6 7 331.788 10.8742 6 0 6 7 331.918 11.0358 2 0 -6 8 174.688 8.18311 4 0 -6 9 498.276 16.8918 4 0 -6 10-0.25631 4.37489 4 0 6 11 15.5395 5.82106 1 0 -6 11 98.5576 6.95077 4 0 6 12 10.1972 5.60685 1 0 -6 12 8.01115 5.07815 4 0 6 13 9.75660 5.86816 1 0 -6 13 5.16361 5.04170 4 0 6 14 8.76028 6.24065 1 0 -6 14 4.99703 5.68560 4 0 6 15 13.5501 6.74361 1 0 -6 15 59.4365 7.47036 4 0 -7 0-1.36070 2.56530 3 0 7 0-0.05808 2.33717 2 0 -7 0-0.03608 1.72012 1 0 7 0-0.12253 1.72899 1 0 -7 0-0.07982 0.69493 5 0 -7 0-0.12870 0.79833 4 0 7 1 7.93426 2.72024 2 0 7 -1 5.79923 2.38828 2 0 -7 1 1.63980 1.62908 1 0 7 1 7.88708 2.29220 1 0 -7 -1 0.04025 2.02463 1 0 7 -1 6.37042 1.75837 1 0 -7 -1 10.1707 2.86216 3 0 -7 1 7.42957 1.35520 4 0 7 -2 575.304 17.6690 1 0 -7 2 603.231 17.6519 1 0 7 -2 672.835 18.5644 2 0 7 2 678.708 18.9503 2 0 7 2 659.838 18.5965 1 0 -7 2 703.870 17.8235 4 0 7 2 684.012 18.3817 3 0 -7 3 537.833 14.1164 2 0 -7 3 464.969 13.6691 1 0 7 -3 469.747 13.7537 1 0 7 -3 521.758 14.4091 2 0 7 3 520.449 14.9673 2 0 -7 3 530.415 14.1884 4 0 7 3 535.994 14.5210 3 0 7 4 844.849 26.1589 1 0 -7 4 976.066 25.2250 2 0 7 -4 918.154 25.4630 2 0 7 4 957.456 26.2472 2 0 -7 4 998.820 25.7830 4 0 -7 4 867.812 24.9706 1 0 -7 5 666.497 12.8806 6 0 7 -5 633.469 12.8138 2 0 7 5 653.308 14.0633 2 0 -7 5 686.574 14.0346 4 0 -7 6 152.895 5.67823 6 0 -7 6 157.388 6.61695 4 0 7 6 154.931 6.29062 2 0 7 7 2.67724 2.65783 2 0 -7 7 2.01670 3.10063 4 0 7 7 1.55604 3.86611 1 0 -7 8 3.54537 3.69799 4 0 7 8 1.95605 4.17568 1 0 -7 9 14.6329 4.25478 4 0 7 9 6.96532 5.01586 1 0 7 10 8.57780 5.30494 1 0 -7 10 134.038 7.30277 4 0 -7 11 19.5852 5.06772 4 0 7 11 8.85284 5.29485 1 0 7 12 20.8446 6.32540 1 0 -7 12 226.611 9.69078 4 0 -7 13 41.3424 6.32219 4 0 7 13 19.1691 6.32220 1 0 7 14 35.8677 7.17302 1 0 -7 14 91.4737 8.11641 4 0 7 15 4.22972 6.52370 1 0 -7 15 5.70792 6.24031 4 0 8 0 556.614 8.98409 1 0 8 0 643.699 10.7190 2 0 -8 0 646.561 6.40422 4 0 -8 0 643.923 10.4411 3 0 8 -1 57.9330 3.03693 1 0 8 1 67.0475 4.06145 2 0 8 -1 71.3682 3.97189 2 0 8 1 57.0120 3.52371 1 0 -8 1 48.3592 2.70542 1 0 -8 1 73.9973 2.52109 4 0 -8 -1 74.5218 4.24276 3 0 8 -2 623.775 17.1823 2 0 8 2 612.324 17.4906 2 0 -8 2 504.043 15.9930 1 0 8 2 527.466 16.8778 1 0 -8 2 633.359 16.1085 4 0 8 -2 581.922 16.2065 1 0 8 -3 42.3833 3.17829 2 0 8 3 43.9974 3.69861 2 0 8 3 20.0061 3.46362 1 0 -8 3 37.0232 2.68721 4 0 8 -3 39.4912 2.51965 1 0 8 4 12.9231 3.07165 2 0 8 -4 10.9198 2.34398 2 0 8 4 8.77824 3.10120 1 0 -8 4 11.4874 2.34105 4 0 -8 5 64.6901 4.04602 4 0 8 5 63.2713 4.46365 2 0 8 -5 60.3433 3.63968 2 0 8 5 57.3566 4.64832 1 0 -8 6 318.635 10.3813 4 0 8 6 317.869 10.4655 2 0 -8 7 208.496 8.54869 4 0 8 7 206.554 8.23524 2 0 8 7 169.089 8.66783 1 0 -8 8 486.555 15.2285 4 0 8 8 465.970 14.3322 2 0 8 9 61.8275 6.37667 1 0 -8 9 78.5280 6.02106 4 0 8 10 57.0724 6.54624 1 0 -8 10 89.5542 6.61915 4 0 8 11 9.60763 5.46169 1 0 -8 11 4.62558 4.86846 4 0 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94.3769 5.69071 2 0 9 8 68.4755 6.46436 1 0 9 9 40.3324 5.72628 1 0 -9 9 49.4449 5.30640 4 0 9 10 34.3336 6.16345 1 0 -9 10 57.9055 5.86714 4 0 9 11 88.6594 8.28978 1 0 -9 11 189.820 9.34738 4 0 -9 12 47.1597 6.33447 4 0 9 12 23.9623 6.48021 1 0 9 13 48.8644 7.40878 1 0 -9 13 92.2123 7.83981 4 0 9 14 6.12047 6.44997 1 0 -9 14 6.52523 5.66556 4 0 10 0 373.981 12.3008 2 0 -10 0 379.169 12.1084 3 0 10 0 334.629 11.1547 1 0 10 1 620.629 17.9372 2 0 10 -1 623.768 17.7448 2 0 10 1 493.560 16.7114 1 0 10 -1 527.667 16.4412 1 0 -10 -1 635.880 17.6113 3 0 10 -2 82.7718 4.82653 2 0 10 2 75.2576 4.98716 2 0 10 2 62.9954 4.40322 1 0 10 3 96.3106 5.69192 2 0 10 -3 93.9657 5.18093 2 0 10 3 97.1548 5.42820 1 0 10 4 2.22383 2.99583 2 0 10 -4 0.53021 2.62734 2 0 10 4-0.90556 3.40511 1 0 -10 5 277.170 9.55025 4 0 10 5 280.478 10.5551 2 0 10 5 258.601 10.4807 1 0 10 6 6.52120 3.51165 2 0 10 6 9.02529 4.22533 1 0 -10 6 5.03027 3.09601 4 0 -10 7 205.972 8.73959 4 0 10 7 209.899 8.92827 2 0 10 7 192.125 9.43345 1 0 -10 8 48.8646 4.93361 4 0 10 8 43.9939 4.68457 2 0 10 8 37.2012 5.72053 1 0 10 9 106.820 8.31474 1 0 -10 9 192.596 8.66046 4 0 10 10 15.3785 5.73118 1 0 -10 10 34.7629 5.36861 4 0 10 11 18.4803 5.96773 1 0 -10 11 30.6756 5.63180 4 0 10 12 6.68027 6.15757 1 0 -10 12 12.5611 5.42961 4 0 10 13 3.53207 6.10781 1 0 -10 13 7.50852 5.49365 4 0 10 14 1.56188 6.30802 1 0 -10 14 14.3179 6.29453 4 0 11 0 1.24165 3.00623 2 0 11 0 1.60100 2.21646 1 0 -11 0-0.76480 3.31523 3 0 11 1 30.4354 3.90336 2 0 -11 1 33.5996 4.05323 3 0 11 -1 36.2177 4.07686 2 0 11 1 25.4258 3.30213 1 0 -11 -1 36.5267 4.22947 3 0 11 2 140.065 7.10550 1 0 11 2 194.157 8.18166 2 0 11 -2 193.787 7.80098 2 0 11 3 10.6610 3.48563 1 0 11 3 10.7802 3.47089 2 0 11 -3 13.1379 3.29198 2 0 11 4 827.718 25.5861 1 0 11 4 895.381 26.0914 2 0 11 -4 880.800 25.3052 2 0 11 5 151.987 8.00537 1 0 11 5 163.012 7.87224 2 0 11 6 178.785 8.95797 1 0 11 6 203.076 8.84689 2 0 11 7-2.77949 4.74178 1 0 11 7-1.36357 3.55067 2 0 11 8 3.15266 4.74109 1 0 11 8 3.57754 3.65633 2 0 11 9 31.3854 5.93151 1 0 11 10 114.662 8.29378 1 0 11 11 19.6984 6.26153 1 0 11 12 48.8712 7.71550 1 0 -11 12 84.9196 7.31918 4 0 11 13 9.69085 6.23344 1 0 -11 13 14.3181 5.77746 4 0 -11 14 40.8336 6.90321 4 0 -12 0 1148.01 32.3811 3 0 12 0 1113.83 32.7087 2 0 -12 1 161.378 7.67895 3 0 -12 -1 164.291 7.77551 3 0 12 1 163.607 7.91499 2 0 12 -1 159.103 7.66369 2 0 12 2 475.505 16.5341 1 0 12 2 571.101 17.7993 2 0 12 -2 568.725 17.3682 2 0 12 3 118.312 6.73072 1 0 12 3 138.728 7.39709 2 0 12 -3 147.083 6.86147 2 0 12 4 57.8246 5.17184 1 0 12 -4 62.8770 4.90158 2 0 12 4 61.9538 5.39128 2 0 12 5 16.2316 4.44510 1 0 12 5 26.9660 4.45525 2 0 12 6 717.741 23.2393 1 0 12 6 759.771 23.3068 2 0 12 7 0.92450 4.72703 1 0 12 7 5.29887 3.84055 2 0 12 8 196.493 9.99429 1 0 12 8 201.291 9.30499 2 0 12 9 202.414 10.5927 1 0 12 10 13.9471 5.67704 1 0 12 11 4.53709 5.80898 1 0 12 12 2.76868 6.00719 1 0 12 13-5.61927 6.46105 1 0 -13 0 3.25282 4.07057 3 0 13 0 2.87668 3.60596 2 0 -13 -1 126.679 7.26189 3 0 -13 1 121.935 7.13722 3 0 13 1 131.699 7.30606 2 0 13 -1 140.213 7.28518 2 0 -13 2 58.9341 5.54390 3 0 13 -2 75.4785 5.43449 2 0 13 2 75.0855 5.70486 2 0 13 3 795.402 25.1792 1 0 13 -3 902.270 25.8022 2 0 13 3 871.121 26.3052 2 0 13 4 54.7060 5.12450 1 0 13 -4 58.8375 4.94640 2 0 13 4 55.2239 5.48907 2 0 13 5 363.834 13.7810 1 0 13 5 400.779 14.3657 2 0 13 6 0.38245 4.28417 1 0 13 6 1.30883 3.88036 2 0 13 7 11.6994 4.80062 1 0 13 7 18.3282 4.55386 2 0 13 8 27.0914 5.57536 1 0 13 8 27.7994 4.81318 2 0 13 9 9.19012 5.21411 1 0 13 10 11.6507 5.88188 1 0 13 11 80.3533 8.15512 1 0 13 12 9.04549 6.31680 1 0 13 13 58.1523 8.18619 1 0 -14 0 329.714 12.3529 3 0 14 0 308.474 12.3929 2 0 -14 1 215.091 9.58887 3 0 -14 -1 214.701 9.53839 3 0 14 -1 212.147 9.60912 2 0 14 1 220.969 9.89360 2 0 14 2 46.9297 5.41029 2 0 -14 2 37.9535 5.09024 3 0 14 -2 38.3462 4.67109 2 0 14 -3 59.2252 5.21864 2 0 14 3 62.1752 5.84200 2 0 14 4 8.16239 4.25166 2 0 14 5 2.83073 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3.40282 1.96536 2 1 5 6 5.50704 3.78473 1 1 -5 6 5.98959 3.00228 4 1 5 6 7.38680 2.19373 2 1 5 7 35.2951 4.77779 1 1 -5 7 57.3558 4.67812 4 1 5 8 34.2799 5.41515 1 1 -5 8 81.6862 5.67068 4 1 5 9 171.418 10.2348 1 1 -5 9 430.441 12.5600 4 1 -5 10 34.2072 5.42562 4 1 5 10 20.2397 5.03151 1 1 5 11 168.003 10.5405 1 1 -5 11 381.742 12.8835 4 1 -5 12 48.4780 6.34438 4 1 5 12 18.0506 5.81860 1 1 -5 13 40.7967 6.43453 4 1 5 13 13.2495 5.98787 1 1 5 14 12.4400 6.25561 1 1 -5 14 6.22107 5.72680 4 1 5 15-1.86324 6.21653 1 -1 -6 16 4.85722 5.97084 4 -1 6 16 7.76446 6.62311 1 -1 -6 15-0.18433 5.55432 4 -1 6 15 8.52241 6.38841 1 -1 -6 14 3.11594 5.27281 4 -1 -6 13 94.1564 7.63330 4 -1 -6 12 16.3140 5.18413 4 -1 -6 11 283.211 11.9809 4 -1 -6 10 7.84459 4.12390 4 -1 -6 9 280.908 10.8964 4 -1 -6 9 262.503 9.87273 6 -1 -6 8 117.188 6.36864 4 -1 -6 8 109.354 5.45981 6 -1 6 7 75.0387 3.98076 4 -1 -6 7 73.4360 4.87230 4 -1 -6 7 67.8902 4.18815 6 -1 -6 6 7.69240 2.32811 6 -1 -6 6 9.84404 1.95929 1 -1 -6 6 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74.0188 4.08809 2 1 6 7 334.024 13.8504 1 1 -6 7 489.384 14.3977 4 1 -6 8-0.54531 3.67088 4 1 6 8 1.74499 4.28422 1 1 -6 9 4.14752 4.48172 4 1 6 9 4.21340 4.72506 1 1 -6 10 18.3618 4.83866 4 1 6 10 16.5636 5.25618 1 1 -6 11 36.9904 5.74161 4 1 6 11 11.2997 5.41694 1 1 -6 12 14.9474 5.46057 4 1 6 12 13.6033 5.72067 1 1 -6 13 54.8497 7.04997 4 1 6 13 24.5072 6.44728 1 1 6 14 10.5772 6.37161 1 1 -6 14 14.7514 6.26882 4 1 6 15 24.6015 6.93893 1 -1 -7 15 16.3356 6.21481 4 -1 7 15 5.48227 6.51918 1 -1 7 14 27.3844 6.86438 1 -1 -7 14 85.8714 7.75915 4 -1 -7 13 22.1108 5.56698 4 -1 7 13 15.4543 6.06877 1 -1 -7 12 88.1386 7.27021 4 -1 -7 11 2.47289 4.34407 4 -1 -7 10 6.22797 4.34601 4 -1 -7 9 96.5283 6.28937 4 -1 -7 8 332.784 11.1870 6 -1 -7 8 334.224 12.1094 4 -1 -7 7 195.395 7.57600 6 -1 -7 7 209.728 8.34908 4 -1 -7 6 800.167 22.5992 6 -1 -7 6 800.281 23.1481 4 -1 -7 5 802.450 11.7273 1 -1 -7 5 849.830 13.0586 4 -1 -7 5 851.877 11.7858 2 1 7 -4 321.951 9.02625 1 -1 -7 4 316.290 8.77978 1 -1 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466.497 9.16862 5 1 -7 2 501.597 10.2813 4 1 7 2 494.693 10.6833 3 -1 7 -2 493.680 10.0192 4 1 7 2 473.950 11.4680 2 -1 7 -2 482.392 10.8811 2 -1 7 -3 14.8756 2.17408 2 1 7 3 13.2227 2.72174 2 1 7 3 6.44836 3.18929 1 1 -7 3 17.4704 2.27529 4 -1 7 -3 14.0319 2.11351 4 1 7 3 14.7398 2.47094 3 1 7 4 280.409 11.2031 1 1 -7 4 339.834 9.89769 6 1 -7 4 344.151 10.9571 4 -1 7 -4 350.946 10.5287 4 1 7 4 349.219 11.1729 2 -1 7 -4 341.114 10.3228 2 1 -7 5 125.032 5.69706 4 1 7 5 90.1326 5.94107 1 1 7 5 120.268 5.49541 2 1 7 6 10.7262 3.88546 1 1 -7 6 12.3208 3.42058 4 1 7 6 14.7895 2.90892 2 1 7 7 32.8199 4.93339 1 1 -7 7 32.9503 4.39030 4 1 7 7 39.7831 3.65940 2 1 7 8 237.504 12.1773 1 1 -7 8 476.197 13.7402 4 1 -7 9 40.7084 5.23175 4 1 7 9 16.2442 5.36953 1 1 7 10 99.1588 8.56446 1 1 -7 10 245.431 10.0341 4 1 -7 11 48.0315 6.11135 4 1 7 11 38.0411 6.31803 1 1 -7 12 56.6301 6.67801 4 1 7 12 34.7260 6.54705 1 1 -7 13 20.7481 5.94156 4 1 7 13 3.19263 6.05337 1 1 7 14 5.04440 6.12330 1 1 -7 14 7.23222 5.85991 4 -1 -8 15 7.08332 5.85209 4 -1 8 15 1.92629 6.40177 1 -1 -8 14 0.70299 5.29588 4 -1 8 14 7.31574 6.27771 1 -1 -8 13-0.65615 5.01081 4 -1 8 13 6.19862 5.86443 1 -1 8 12 29.1166 6.50716 1 -1 -8 12 119.602 7.70842 4 -1 -8 11 39.3625 5.52821 4 -1 8 11 12.5283 5.31281 1 -1 8 10 17.4239 6.11076 1 -1 -8 10 327.641 10.1162 4 -1 8 9 5.01407 5.11638 1 -1 -8 9 102.399 6.06301 4 -1 8 8 179.871 6.74091 2 -1 -8 8 186.630 7.37775 4 -1 8 7 47.8428 4.20804 2 -1 -8 7 43.6966 4.09261 4 -1 -8 6 87.6062 4.34129 6 -1 8 6 93.9403 5.08320 2 -1 -8 6 90.8034 4.84034 4 1 8 -5 53.9860 3.49988 2 -1 8 5 32.6640 3.95823 1 -1 -8 5 58.1821 3.67482 4 1 8 -4 666.630 17.6289 2 -1 8 4 700.843 18.3316 2 1 8 -4 596.594 16.9601 1 -1 -8 4 689.816 17.3195 4 1 8 -3 191.223 6.84671 2 -1 8 3 184.337 7.20475 2 -1 8 3 142.922 6.34594 1 1 8 -3 159.252 6.10013 1 -1 -8 3 159.991 5.95371 1 -1 -8 3 182.974 6.00899 4 -1 8 2 2291.78 57.1739 2 1 8 -2 2260.22 56.9117 2 -1 8 2 2072.07 56.2057 1 1 8 -2 2112.42 56.2154 1 1 -8 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27.3771 3.63039 2 1 -8 7 30.6017 4.28176 4 1 8 7 27.5536 4.89627 1 1 8 8 89.1053 7.03331 1 1 -8 8 109.256 6.64342 4 1 -8 9 5.51292 4.17908 4 1 8 9 5.27230 4.82893 1 1 -8 10 2.90240 4.53611 4 1 8 10 0.60002 4.99671 1 1 -8 11 9.36054 5.07385 4 1 8 11 6.76709 5.63014 1 1 8 12 36.9839 6.87962 1 1 -8 12 86.1432 7.50266 4 1 -8 13 14.5535 5.71984 4 1 8 13 1.09254 6.14227 1 1 8 14 41.9073 7.60028 1 1 -8 14 92.8809 8.29338 4 -1 -9 15 53.2500 7.19458 4 -1 9 15 20.9843 7.16416 1 -1 -9 14 4.41392 5.56941 4 -1 9 14 8.77788 6.27329 1 -1 9 13 10.2305 6.22129 1 -1 -9 13 71.3422 7.09190 4 -1 -9 12 5.50944 4.77255 4 -1 9 12 11.2377 5.81664 1 -1 -9 11 45.2707 5.68509 4 -1 9 11 6.76215 5.21408 1 -1 -9 10 7.29258 4.39088 4 -1 9 10 5.53833 5.27740 1 -1 -9 9 253.104 9.54151 4 -1 9 9 118.963 8.36246 1 -1 -9 8 154.017 7.34805 4 -1 9 8 157.083 7.20533 2 -1 -9 7 514.503 12.3603 4 -1 9 7 511.394 12.6469 2 -1 -9 6 136.166 5.87777 4 -1 9 6 125.836 6.27207 2 1 9 -5 658.989 16.8578 2 -1 9 5 658.977 17.6748 2 -1 -9 5 675.571 16.7878 4 -1 9 4 50.3677 4.15535 2 1 9 -4 43.2251 3.66203 2 -1 9 4 40.7234 4.02320 1 1 9 -4 38.9761 3.00468 1 -1 -9 4 50.1478 3.26464 4 1 9 -3 288.431 10.0597 2 -1 9 3 302.002 10.4880 2 -1 9 3 258.294 9.67060 1 1 9 -3 291.648 9.39791 1 -1 -9 3 302.946 9.11290 4 1 9 -2 121.013 5.55747 2 -1 9 2 128.515 5.90119 2 -1 9 2 96.3819 4.81306 1 -1 -9 2 68.9539 4.41427 1 1 9 -2 107.204 4.70030 1 -1 -9 2 120.226 4.16016 4 1 -9 -2 136.799 5.99661 3 1 9 -1 221.230 7.15868 2 -1 9 1 226.139 7.32165 2 -1 9 1 175.141 5.77907 1 1 9 -1 202.406 6.28273 1 -1 -9 1 206.967 6.78609 3 1 -9 -1 222.524 7.27450 3 -1 9 0 86.7309 4.74086 2 1 9 0 91.4593 4.89032 2 -1 -9 0 36.5168 3.25864 1 1 9 0 75.4900 4.16887 1 -1 9 0 81.6268 3.53533 1 -1 -9 0 95.6218 4.62823 3 1 -9 0 88.9802 4.97753 3 1 9 1 799.253 21.7174 2 -1 9 -1 773.244 21.3501 2 1 9 1 677.303 20.9625 1 -1 9 -1 665.285 19.8342 1 -1 -9 -1 795.912 21.1616 3 1 -9 2 72.5951 3.40757 4 -1 9 -2 72.7581 4.26566 2 1 9 2 69.1448 4.62215 2 1 9 2 57.8271 4.36591 1 1 -9 3 1265.35 33.2745 4 -1 9 -3 1196.17 33.7122 2 1 9 3 1231.86 34.4079 2 1 9 3 1192.87 34.3094 1 1 -9 4 77.4061 4.30455 4 1 9 4 79.0572 5.08851 2 -1 9 -4 73.9294 4.18480 2 1 9 4 57.3287 5.08628 1 1 -9 5 79.7774 4.82656 4 1 9 5 74.9234 5.04918 2 1 9 5 78.1481 5.73041 1 1 9 6 2.02317 3.08214 2 1 9 6 5.50792 4.22784 1 1 -9 6 5.13445 3.35761 4 1 -9 7 41.4436 4.71808 4 1 9 7 38.0264 4.26253 2 1 9 7 33.0192 5.19192 1 1 -9 8 0.68291 3.91242 4 1 9 8 1.33504 4.71669 1 1 9 9 289.850 12.9488 1 1 -9 9 335.351 12.6820 4 1 9 10 41.8357 6.34670 1 1 -9 10 52.4265 6.03124 4 1 9 11 130.583 9.19491 1 1 -9 11 157.842 8.97746 4 1 -9 12 26.9546 6.00315 4 1 9 12 10.2610 6.07672 1 1 9 13 16.4350 6.30813 1 1 -9 13 19.7011 6.06408 4 1 9 14 5.66911 6.28723 1 -1 -10 15 7.65185 5.95152 4 -1 -10 14 1.59091 5.31074 4 -1 10 14 6.28806 6.41419 1 -1 -10 13 15.7508 5.50357 4 -1 10 13 6.50022 6.08949 1 -1 -10 12 20.0163 5.24547 4 -1 10 12 3.90462 5.60384 1 -1 -10 11 115.751 7.60757 4 -1 10 11 75.0752 7.48602 1 -1 -10 10 133.819 7.57651 4 -1 10 10 78.4157 7.22095 1 -1 -10 9 204.570 9.02909 4 -1 10 9 159.448 9.04358 1 -1 -10 8 170.873 7.69611 4 -1 10 8 176.425 7.79507 2 -1 10 7 12.0577 3.73752 2 -1 10 7 1.35268 4.28689 1 -1 -10 7 9.82994 3.49381 4 -1 10 6 3.29636 3.51928 2 -1 10 6 0.50932 3.68104 1 -1 -10 6-0.15959 2.64498 4 -1 -10 5 167.667 6.72131 4 1 10 -5 162.620 6.98307 2 -1 10 5 175.891 7.77045 2 -1 10 5 138.040 7.18574 1 1 10 -4 869.024 24.5179 2 -1 10 4 865.504 25.1822 2 -1 10 4 799.527 24.3747 1 1 10 -3 1098.97 32.1786 1 1 10 -3 1261.87 33.2783 2 -1 10 3 1267.71 33.6962 2 -1 10 3 1145.17 32.7637 1 -1 10 2 687.894 20.0113 2 1 10 -2 673.208 19.7145 2 -1 10 2 586.623 18.7243 1 1 -10 -2 703.879 19.8548 3 1 10 -2 631.414 18.7012 1 -1 10 1 155.734 6.86008 2 1 10 -1 151.777 6.76704 2 1 10 -1 131.230 5.89039 1 -1 10 1 131.577 5.62697 1 -1 -10 1 163.496 6.53667 3 1 -10 -1 157.599 6.90330 3 1 -10 0 29.4983 3.79337 3 1 10 0 31.8086 3.74025 2 -1 10 0 30.5715 3.50923 2 1 10 0 25.9012 3.10583 1 -1 -10 0 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42.4110 4.40206 2 -1 12 4 44.1311 4.90631 2 -1 12 4 29.6841 4.23831 1 -1 12 3 254.772 10.5670 2 1 12 -3 268.159 10.2498 2 1 -12 -2 969.894 27.8698 3 -1 -12 2 935.107 27.5115 3 -1 12 2 923.528 28.0014 2 1 12 -2 944.305 27.8260 2 -1 -12 1 254.715 9.70421 3 1 -12 -1 246.277 10.0980 3 -1 12 1 250.179 10.1253 2 1 12 -1 245.975 10.0321 2 -1 12 0 134.977 6.98239 2 1 12 0 137.234 7.13544 2 1 -12 0 140.658 7.28890 3 -1 -12 0 146.796 6.88049 3 1 12 0 117.031 6.07210 1 1 12 1 175.187 8.23108 2 -1 12 -1 176.326 7.97951 2 -1 -12 -1 186.782 7.97186 3 1 -12 1 182.682 8.41650 3 1 12 1 152.742 7.22667 1 1 12 2 49.3194 4.53367 1 1 12 2 44.3857 4.79637 2 -1 12 -2 48.3480 4.53876 2 -1 12 -3 90.3839 5.47047 2 1 12 3 86.2361 5.94491 2 1 12 3 81.0677 5.85507 1 1 12 4 161.321 7.98234 2 1 12 4 140.830 7.74127 1 1 12 5 99.0703 6.49602 2 1 12 5 99.0573 6.68144 1 1 12 6 481.338 16.5459 2 1 12 6 470.217 16.9389 1 1 12 7 20.4560 4.32341 2 1 12 7 14.0983 5.16016 1 1 12 8 134.449 8.73326 1 1 12 9 40.1958 6.25067 1 1 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8.48786 6 -5 -2 10 40.9045 4.94688 6 -5 -2 9 1032.40 30.2023 6 -5 2 9 1067.07 30.3277 6 -5 2 8 321.557 11.3333 6 -5 -2 8 327.189 11.4390 6 -5 2 7 525.867 15.9254 6 -5 -2 7 507.521 16.0591 6 -5 2 6 21.1955 2.40855 5 -5 2 6 20.9407 3.10368 6 5 2 -5 1923.86 52.6939 1 -5 2 5 2097.75 52.1157 3 -5 2 5 2008.43 52.1927 5 -5 2 5 1999.98 52.4385 6 -5 -2 5 2050.31 52.4093 5 -5 2 4 218.136 5.94354 1 5 2 -4 212.194 6.75374 1 -5 2 4 242.886 6.10970 3 5 2 -4 224.335 6.85972 5 -5 2 4 228.933 6.27973 5 -5 2 4 219.042 6.31396 6 -5 -2 4 227.030 6.48851 5 5 -2 -4 216.920 6.55620 5 -5 -2 3 3257.26 84.9342 1 5 2 -3 3201.83 85.2445 1 -5 2 3 3125.34 84.4330 1 -5 2 3 3249.08 84.9169 5 -5 -2 3 3318.57 85.0553 5 5 -2 -3 3442.66 84.8099 3 5 -2 -3 3193.79 85.1763 5 5 2 -3 3373.36 85.4088 5 -5 2 2 29.5551 2.03793 1 -5 -2 2 29.5593 2.69020 1 5 -2 -2 32.9030 2.27435 1 5 2 -2 30.3244 2.95392 1 5 2 -2 35.5535 3.12891 5 5 -2 -2 34.3530 3.22108 5 -5 -2 2 39.0053 3.04945 5 -5 2 2 44.0075 3.01366 5 5 -2 -2 33.3703 2.70738 3 -5 -2 1 2077.36 52.4239 1 -5 2 1 2008.38 51.6926 1 5 2 -1 1996.80 52.6743 1 5 -2 -1 2097.38 52.8899 5 -5 -2 1 2095.19 52.5810 5 5 2 -1 2031.11 52.8796 5 -5 -2 0 35.0313 2.89888 1 -5 2 0 32.9771 2.20638 1 5 2 0 40.8672 3.59586 5 5 -2 0 42.2944 3.75235 5 5 -2 0 35.3194 2.21019 1 5 2 0 36.0713 3.23865 1 -5 -2 -1 73.5474 3.42908 2 5 2 1 93.1637 4.97188 5 -5 2 -1 58.9328 3.09818 1 -5 -2 -1 82.3029 4.06856 1 5 2 1 83.3177 4.30600 1 5 -2 1 77.2731 3.35933 1 5 -2 2 1.46392 1.75316 1 5 2 2 3.72242 2.56139 1 5 2 3 272.284 9.77885 1 5 -2 3 276.696 8.78009 1 5 2 4 44.3556 4.12067 1 5 2 5 1187.37 33.5729 1 5 2 6-1.49009 3.88708 1 5 2 7 102.782 6.59073 1 5 2 8 11.3882 4.50954 1 -5 -3 17 0.92685 5.47882 4 -5 -3 16 32.4455 6.23794 4 -5 -3 15 52.1717 6.42574 4 -5 3 14 135.697 8.07050 4 -5 -3 14 139.126 8.68373 4 -5 -3 13 31.7329 5.18810 4 -5 3 13 29.8606 4.77158 4 -5 -3 13 32.6080 5.31921 6 -5 3 12 32.1751 4.52985 4 -5 -3 12 31.6308 5.11414 4 -5 -3 12 30.1336 5.08692 6 -5 3 11 1.22303 3.46036 4 -5 -3 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101.745 6.45281 6 -5 -6 9 303.887 11.5096 6 5 6 -6 33.5026 3.65948 1 5 6 -5 287.988 10.3373 1 5 -6 -5 298.875 9.20994 6 5 6 -4 34.2656 3.44331 1 5 -6 -4 39.8293 3.87067 3 5 -6 -4 32.2532 2.58427 5 5 6 -3 786.942 24.1731 1 5 -6 -3 901.689 24.3569 3 5 6 -3 850.965 23.7996 5 5 -6 -3 829.914 23.2056 5 -5 -6 3 855.035 23.4379 5 5 6 -2 242.137 9.11449 1 -5 -6 2 251.051 8.26580 5 5 -6 -2 241.712 8.28327 5 5 -6 -2 267.356 9.23879 3 5 6 -2 258.349 8.64896 5 5 6 -1 2016.61 52.5681 5 5 -6 -1 1965.74 52.3797 5 -5 -6 1 1975.60 52.1640 5 5 6 -1 1920.11 53.1939 1 5 6 0 9.66669 2.51870 5 5 6 0 8.08462 3.23278 1 5 6 1 192.114 7.53927 5 5 6 1 208.473 8.28929 1 5 6 2 35.9575 4.01117 1 5 6 2 36.2187 3.75457 5 5 6 3 125.682 6.94342 1 5 6 3 135.729 6.36192 5 5 6 4 0.98136 3.61439 1 5 6 5 450.192 15.7812 1 5 6 6-2.40179 4.60290 1 5 6 7 451.921 16.5095 1 5 6 8 31.9496 5.77023 1 5 6 9 26.4394 5.88221 1 5 6 10-2.61849 5.57413 1 5 6 11 1.03310 5.65088 1 5 6 12-2.87379 6.12234 1 -5 -7 16 62.0456 7.29704 4 -5 -7 15 30.8579 6.07349 4 -5 -7 14 157.150 9.36071 4 -5 -7 14 162.430 9.10820 6 -5 -7 13 32.9126 5.53755 4 -5 -7 13 28.6271 5.29637 6 -5 -7 12 97.2465 7.12380 4 -5 -7 12 104.014 7.00666 6 -5 -7 11 10.7649 4.46183 4 -5 -7 11 12.5193 4.26946 6 -5 -7 10-3.51494 4.21660 4 -5 -7 10-0.33751 3.78102 6 -5 -7 9 39.9513 4.63315 6 5 7 -7 256.504 9.80882 1 5 7 -6 1250.05 35.1596 1 5 7 -5 59.6985 4.36130 1 5 -7 -4 475.685 13.6948 5 5 -7 -4 493.038 15.3090 3 5 7 -4 454.283 15.0093 1 5 -7 -3 61.3414 3.22870 5 5 7 -3 59.7783 4.42118 1 5 -7 -3 67.0943 4.75542 3 5 -7 -2 15.4613 3.32263 3 5 -7 -2 11.3800 2.17233 5 -5 -7 2 17.6077 2.28938 5 5 7 -2 14.2818 2.49066 5 5 7 -2 14.8376 3.21934 1 5 -7 -1 10.9256 2.59351 5 5 7 -1 10.4707 2.36138 5 -5 -7 1 14.9676 2.28651 5 5 7 -1 12.2065 3.24117 1 5 7 0 375.344 11.6858 5 5 -7 0 363.107 11.7716 5 5 7 0 365.198 12.5751 1 5 7 1 125.646 5.57995 5 5 7 1 125.840 6.49522 1 5 7 2 1135.76 31.8832 1 5 7 2 1075.84 30.7122 5 5 7 3 150.267 7.83947 1 5 7 3 163.783 7.17070 5 5 7 4 526.334 17.5913 1 5 7 4 520.247 16.5185 5 5 7 5 42.8109 5.16900 1 5 7 6 8.13366 4.45343 1 5 7 7 83.2513 7.26086 1 5 7 8 66.3925 6.97160 1 5 7 9 54.6363 6.81107 1 5 7 10 78.0218 7.78380 1 5 7 11 3.38660 5.80614 1 5 7 12 46.3511 7.40897 1 -5 -8 16 6.83741 5.82415 4 -5 -8 15 7.16299 5.39584 4 -5 -8 14 14.0971 5.39165 4 -5 -8 13 16.9539 5.11574 4 -5 -8 13 18.3932 5.06843 6 -5 -8 12 207.232 10.2285 4 -5 -8 12 215.715 9.94077 6 -5 -8 11 44.1196 5.30531 4 -5 -8 11 39.9689 5.10359 6 -5 -8 10 468.310 16.0042 4 -5 -8 10 445.220 15.7054 6 -5 -8 9 80.0259 5.70070 6 5 8 -7 28.8307 3.96206 1 5 8 -6 18.1420 3.47315 1 5 8 -5 297.601 10.7916 1 5 8 -4 207.777 8.53195 1 5 -8 -4 221.393 8.92063 3 5 8 -3 23.4611 3.47357 1 5 -8 -3 28.4759 3.86324 3 5 8 -2 775.492 23.7720 1 5 -8 -2 819.886 23.9794 3 5 8 -2 822.918 22.8288 5 5 8 -1 101.918 4.88220 5 5 8 -1 111.406 5.94092 1 5 -8 -1 107.476 4.87225 5 5 8 0 220.050 7.77247 5 5 8 0 213.330 8.92470 1 5 -8 0 217.461 7.93826 5 5 8 1 39.2959 4.29047 1 5 8 1 35.5326 3.25402 5 5 8 2 156.040 7.79075 1 5 8 2 160.284 7.21460 2 5 8 3 1.49964 3.87697 1 5 8 3 2.59654 3.09686 2 5 8 4 167.740 8.64888 1 5 8 4 175.737 7.64605 2 5 8 5 25.5213 5.06065 1 5 8 6 231.321 11.0895 1 5 8 7 48.9875 6.09257 1 5 8 8 56.9234 6.67733 1 5 8 9 15.2443 5.89700 1 5 8 10-0.70447 5.94672 1 5 8 11-3.68117 6.16131 1 5 8 12 4.58080 6.25986 1 -5 -9 16 10.9395 5.71384 4 -5 -9 15 79.9763 7.68347 4 -5 -9 14 4.95752 5.02472 4 -5 -9 13 144.161 8.94629 4 -5 -9 12 25.8734 5.18514 4 -5 -9 12 25.1642 4.93640 6 -5 -9 11 17.9186 4.72840 4 -5 -9 11 18.8766 4.41840 6 -5 -9 10 20.6657 4.39548 4 -5 -9 10 12.1440 4.13109 6 5 9 -7 600.213 18.9083 1 5 9 -6 149.284 7.14706 1 5 9 -5 823.653 24.4953 1 5 9 -4 125.672 6.57850 1 5 -9 -4 143.154 7.16690 3 5 9 -3 0.66577 3.10141 1 5 -9 -3 6.41662 3.73936 3 5 9 -2 23.4605 3.59456 1 5 -9 -2 23.6315 4.16457 3 5 9 -1 232.828 9.85354 1 5 -9 -1 290.471 10.5557 3 5 9 0 58.4786 4.96704 1 5 9 0 64.2251 4.87015 2 5 9 1 687.489 21.7007 1 5 9 1 704.149 21.4123 2 5 9 2 94.5061 6.29795 1 5 9 2 107.125 5.95152 2 5 9 3 84.2849 5.44548 2 5 9 3 63.4558 6.02216 1 5 9 4 8.74384 3.40318 2 5 9 4 10.0285 4.32342 1 5 9 5 19.1252 4.85685 1 5 9 6 4.27129 4.56906 1 5 9 7 49.8324 6.37558 1 5 9 8 10.5690 5.22820 1 5 9 9 86.5919 7.77367 1 5 9 10 45.1736 6.57882 1 5 9 11 39.6432 6.62254 1 -5 -10 16 6.12264 5.85222 4 -5 -10 15 0.35246 5.25146 4 -5 -10 14 15.9379 5.49995 4 -5 -10 13 28.7146 5.54807 4 -5 -10 12 9.23409 4.68936 4 -5 -10 11 249.561 11.0149 4 -5 -10 10 84.3316 6.26525 4 -5 -10 10 86.1895 6.35362 6 -5 -10 9 354.539 13.0735 4 5 10 -7 30.7243 4.19058 1 5 10 -6-0.71879 3.33605 1 5 10 -5 50.5938 4.57357 1 5 -10 -4 138.591 7.52332 3 5 10 -4 119.962 6.58572 1 5 -10 -3 546.418 17.2830 3 5 10 -3 485.091 16.5401 1 5 -10 -2 9.13294 4.04162 3 5 10 -2 10.5619 3.60869 1 5 -10 -1 618.869 19.6049 3 5 10 -1 595.043 19.2514 1 5 10 0 158.528 7.85965 1 5 10 0 162.116 7.75839 2 5 10 1 8.68468 3.50058 2 5 10 1 14.1116 3.99729 1 5 10 2 1.50477 3.32098 2 5 10 2 0.61367 3.79217 1 5 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8.41459 1 5 11 4 144.609 7.57867 2 5 11 5 18.8995 5.16895 1 5 11 6 8.36592 5.04972 1 5 11 7 7.11588 5.36941 1 5 11 8 94.2541 8.08879 1 5 11 9 8.54997 5.77385 1 5 11 10 57.0592 7.53898 1 -5 12 15 3.69573 6.46284 1 -5 12 14 8.56601 6.04954 1 5 12 -7 26.2852 4.12159 1 5 12 -6 33.0617 4.47773 1 5 12 -5 10.1722 3.76544 1 5 12 -4 350.120 13.0697 1 5 -12 -4 378.871 14.0286 3 5 12 -3 35.3835 4.52865 1 5 -12 -3 37.4844 5.54179 3 5 12 -2 417.798 15.2801 1 5 -12 -2 475.115 16.1526 3 5 12 -1 216.716 9.63662 1 5 -12 -1 222.073 10.2431 3 5 12 -1 225.836 9.96249 2 5 12 0 80.2774 6.16595 1 5 -12 0 83.9867 6.60876 3 5 12 0 77.9518 6.08033 2 -5 12 0 83.4520 5.69805 2 5 12 1 34.1317 4.98830 1 5 12 1 42.2143 4.97457 2 5 12 2 1.23152 4.27223 1 5 12 2 5.29406 3.95012 2 5 12 3 14.5159 4.61840 1 5 12 3 23.3540 4.56232 2 5 12 4 79.2099 6.72881 1 5 12 4 81.2126 6.15056 2 5 12 5 99.6182 7.92439 1 5 12 6 140.567 9.19486 1 5 12 7 114.666 8.54342 1 5 12 8 30.8479 6.36530 1 5 12 9 7.08085 5.72286 1 5 12 10 10.3058 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136.686 8.48608 3 -5 14 2 136.607 7.77341 2 5 14 -1 461.259 17.3520 1 5 -14 -1 520.759 18.3887 3 5 14 -1 525.699 18.0567 2 -5 14 1 540.928 17.7750 2 5 14 0 146.329 8.24888 1 5 -14 0 147.125 9.11548 3 5 14 0 159.694 8.71063 2 5 14 1-2.44927 4.07458 1 5 -14 1-5.25115 5.59478 3 5 14 1 1.44489 4.35361 2 5 14 2 11.1342 4.84425 1 5 14 2 18.4074 4.76782 2 5 14 3 23.4132 5.28233 1 5 14 3 29.7465 5.14574 2 5 14 4 90.5396 7.60578 1 5 14 4 100.251 7.29194 2 5 14 5 84.5686 7.56193 1 5 14 6 63.1791 7.24976 1 5 14 7 43.1567 6.67766 1 5 14 8 22.3043 6.31062 1 -5 15 12 11.2255 5.42832 2 -5 15 11 2.41050 5.00993 2 -5 15 10 3.41035 5.00403 2 -5 15 9 5.72192 5.06252 2 -5 15 8 80.9860 7.20073 2 -5 15 7 8.90968 4.91498 2 -5 15 6 303.679 13.0257 2 -5 15 5 1.23339 4.54273 2 -5 15 4 171.097 9.30529 2 5 15 -3 2.62155 3.74188 1 5 -15 -3 6.04213 5.42200 3 -5 15 3 6.83746 4.65872 2 5 15 -2 1.21160 3.89645 1 5 -15 -2 1.51314 5.18963 3 -5 15 2 4.36275 4.28664 2 5 15 -1 31.4363 5.29006 1 5 -15 -1 44.7244 6.26882 3 5 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145.884 8.39788 1 9 6 3 146.015 8.40758 5 9 -6 3 158.332 8.93073 5 9 6 4 48.5195 6.11087 5 9 6 4 34.5608 5.41545 1 9 6 5 51.1507 6.43643 5 9 6 5 46.9380 5.78150 1 -9 -7 17 20.7402 6.17268 4 -9 -7 17 17.5280 6.47682 6 -9 -7 16 54.1791 7.12643 4 -9 -7 16 61.2080 7.38869 6 -9 -7 15 7.02691 5.24919 4 -9 -7 15 8.69891 5.55846 6 -9 -7 14 162.202 9.69736 6 -9 -7 13 17.2879 5.39308 6 -9 -7 12 0.76557 4.77515 6 -9 -7 11 8.94328 4.89276 6 9 7 -8 436.406 15.6555 1 9 7 -7 106.665 6.81895 1 9 7 -6 312.892 12.3128 1 9 7 -5 31.1569 4.42086 5 9 -7 -5 37.5621 4.82173 3 9 7 -5 28.1450 4.68785 1 9 -7 -4 148.228 7.19573 5 9 7 -4 161.510 7.75564 5 9 -7 -4 160.482 7.65313 3 9 7 -4 145.681 7.98736 1 9 7 -3 42.2928 4.70207 5 9 -7 -3 44.4986 4.41108 5 9 7 -3 42.7596 5.07178 1 9 -7 -3 41.0347 4.87313 3 9 -7 -2 14.6500 4.03473 5 9 7 -2 19.5791 4.03718 5 9 7 -2 20.5400 4.34536 1 9 -7 -2 17.2835 4.25135 3 9 -7 -1 1.07937 3.89537 5 9 7 -1 4.79660 3.80240 5 9 7 -1 0.25372 3.75746 1 9 7 0 512.465 17.3109 5 9 7 0 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24.6358 6.54450 5 13 -5 2 30.2785 6.71353 5 13 5 3 20.9940 6.43453 5 13 -5 3 21.5153 6.75658 5 -13 -6 15-3.47850 5.90914 6 -13 -6 14 6.00688 5.89402 6 -13 -6 13 55.5734 7.12366 6 -13 -6 12-0.17673 5.54733 6 13 6 -9 24.1010 5.27747 1 13 6 -8-1.42537 4.42807 1 13 6 -7 1.24629 4.24399 1 13 6 -7 2.52789 4.53802 5 13 6 -6 1.99421 4.43014 1 13 6 -6 1.88748 4.47323 5 13 6 -5 17.9300 4.78004 1 13 6 -5 17.8233 5.08090 5 13 -6 -5 14.9881 4.66579 5 13 6 -4 4.53500 4.30937 1 13 6 -4 3.81496 4.51626 5 13 -6 -4 2.36936 4.44044 5 13 6 -3 54.1116 6.02440 1 13 6 -3 56.7096 6.26521 5 13 -6 -3 63.0450 6.24997 5 13 6 -2 9.49839 4.77821 5 13 -6 -2 12.7264 4.89447 5 13 6 -1 80.6118 7.22960 5 13 -6 -1 76.0667 7.36221 5 13 -6 0-1.17919 5.56091 5 13 6 0 3.91512 4.88918 5 13 -6 1 0.17462 5.83157 5 13 6 1 6.96038 5.15982 5 13 -6 2 11.9440 6.15016 5 13 6 2 9.25154 5.99442 5 13 -6 3 13.8668 6.49979 5 -13 -7 15 22.0998 6.53348 6 -13 -7 14 59.0940 7.44008 6 -13 -7 13 4.45646 5.70562 6 13 7 -9 1.50609 4.49746 1 13 7 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18.1775 5.52337 1 13 9 -7 163.218 9.74226 1 13 9 -6 14.0518 5.22352 1 13 9 -5 26.0767 5.69239 1 13 9 -4 6.73428 5.02157 1 13 9 -3-0.34634 4.78551 1 13 9 -2-2.08846 4.86057 1 13 9 -1 48.2323 6.55010 1 13 9 0 5.31100 5.10306 1 13 10 -10 15.8045 5.55526 1 13 10 -9 58.9840 6.93690 1 13 10 -8 14.5679 5.56920 1 13 10 -7 1.08466 4.87049 1 13 10 -6 45.1520 6.50848 1 13 10 -5 22.9613 5.60438 1 13 10 -4 18.8445 5.49769 1 13 10 -3 73.9887 7.31254 1 13 10 -2 19.1877 5.64561 1 13 10 -1 26.4459 6.14668 1 13 10 0 5.69988 5.14274 1 13 10 1-0.74224 5.12793 1 13 11 -10 12.0054 5.61730 1 13 11 -9 4.71787 5.25322 1 13 11 -8 53.6299 6.76017 1 13 11 -7 1.30623 5.18716 1 13 11 -6 48.9017 6.74230 1 13 11 -5 15.7848 5.85872 1 13 11 -4 18.7723 5.65901 1 13 11 -3-1.11974 5.07152 1 13 11 -2 7.12719 5.23493 1 13 11 -1 0.75543 5.18816 1 13 11 0 57.6764 7.18123 1 13 12 -10 41.0672 6.42008 1 13 12 -9 12.9591 5.73208 1 13 12 -8 23.1199 5.96509 1 13 12 -7-1.92001 5.10846 1 13 12 -6 14.1872 5.66628 1 13 12 -5 7.66374 5.43377 1 13 12 -4 44.1500 6.66892 1 13 12 -3 26.2074 6.06340 1 13 12 -2 18.0216 6.02167 1 13 13 -9 29.8446 6.27842 1 13 13 -8-2.76027 5.25269 1 13 13 -7 65.8156 7.62055 1 13 13 -6 0.39400 5.26779 1 13 13 -5 12.0244 5.68222 1 13 13 -4 1.38258 5.26164 1 -14 0 16 24.4898 6.65789 6 -14 0 15 1.79626 5.63317 6 -14 0 14 94.0453 8.00051 6 14 0 -8 13.1087 5.02581 5 14 0 -7-2.95458 4.74580 5 14 0 -6 201.366 10.5233 5 14 0 -5-1.50933 4.88468 5 14 0 -4 201.387 10.7649 5 14 0 -3 4.33259 5.00042 5 14 0 -2 76.5716 7.40614 5 14 0 -1 5.06698 5.35559 5 14 0 0-3.89626 6.28528 5 14 0 1-10.4639 6.57985 5 14 0 2 60.2488 7.84824 5 -14 1 16 20.2571 6.30954 6 -14 -1 16 26.7564 6.86868 6 -14 -1 15 14.4354 5.90722 6 -14 -1 14 12.1107 5.80689 6 -14 -1 13 2.68985 5.40123 6 -14 -1 12 11.5827 5.36660 6 14 -1 -8 53.4607 6.11410 5 14 1 -8 55.4286 6.24972 5 14 -1 -7 55.7523 6.33012 5 14 1 -7 47.1981 6.11399 5 14 1 -6 22.8325 5.49273 5 14 -1 -6 27.0807 5.66012 5 14 1 -5 1.68627 4.89644 5 14 -1 -5 4.66274 4.89196 5 14 1 -4 0.68448 4.93658 5 14 -1 -4 3.72399 4.78719 5 14 1 -3 29.7599 5.70445 5 14 -1 -3 32.4242 5.94512 5 14 1 -2 53.0152 6.62345 5 14 -1 -2 48.6490 6.68713 5 14 -1 -1 75.2690 7.45117 5 14 1 -1 74.3375 7.35068 5 14 -1 0 22.6071 6.42434 5 14 1 0 7.98227 6.08377 5 14 1 1 27.7561 6.82994 5 14 -1 1 27.3745 6.73363 5 14 1 2-2.72407 6.21816 5 14 -1 2-0.19506 6.15063 5 -14 -2 15 41.0964 6.86038 6 -14 -2 14 4.47457 5.53634 6 -14 -2 13 90.1716 7.86685 6 -14 -2 12 1.32178 5.07107 6 -14 -2 11 129.721 8.53543 6 14 -2 -8-1.28016 4.38554 5 14 2 -8-0.83481 4.68420 5 14 2 -7 93.2716 7.62320 5 14 -2 -7 106.137 7.72386 5 14 2 -6-0.83819 4.97026 5 14 -2 -6 5.52658 4.93640 5 14 2 -5 190.825 10.3472 5 14 -2 -5 197.412 10.3928 5 14 2 -4 1.54589 5.08750 5 14 -2 -4 3.19526 4.91414 5 14 2 -3 57.9449 6.68808 5 14 -2 -3 57.0771 6.65396 5 14 2 -2 4.79674 4.99071 5 14 -2 -2 2.27916 4.94750 5 14 2 -1 10.8761 5.55623 5 14 -2 -1 4.31440 5.59930 5 14 -2 0-7.20052 6.21438 5 14 2 0 9.45086 5.60540 5 14 2 1 16.5008 6.53235 5 14 -2 1 21.4474 6.62085 5 14 2 2-4.65302 6.20149 5 14 -2 2-0.77927 6.25894 5 -14 -3 15 20.4122 6.35759 6 -14 -3 14-3.10219 5.60125 6 -14 -3 13-4.92735 5.44365 6 -14 -3 12 5.08740 5.27551 6 -14 -3 11 9.15857 5.29569 6 14 3 -8 83.5467 7.24480 5 14 -3 -8 83.4468 7.12703 5 14 3 -7 24.5083 5.67146 5 14 -3 -7 21.5808 5.30511 5 14 3 -6 5.55660 4.93714 5 14 -3 -6 4.66101 4.62810 5 14 3 -5 8.66527 4.95405 5 14 -3 -5 9.32164 4.98601 5 14 3 -4 20.6607 5.58826 5 14 -3 -4 26.9921 5.66743 5 14 3 -3 16.9453 5.36346 5 14 -3 -3 16.6661 5.32099 5 14 3 -2 54.7124 6.73714 5 14 -3 -2 48.7839 6.58383 5 14 3 -1 45.4535 6.49880 5 14 -3 -1 41.8628 6.57776 5 14 -3 0 49.6364 7.22500 5 14 3 0 60.2627 6.97380 5 14 -3 1 11.1541 6.27714 5 14 3 1 9.63454 6.11158 5 14 3 2 0.38560 6.12860 5 14 -3 2-0.19424 6.11915 5 -14 -4 15 9.20871 6.08109 6 -14 -4 14 86.8460 8.29969 6 -14 -4 13 1.07912 5.58306 6 -14 -4 12 76.2088 7.40042 6 14 4 -8 35.4507 5.41697 1 14 4 -8 36.6985 5.88254 5 14 -4 -8 40.3653 5.65281 5 14 4 -7 4.89025 4.68466 5 14 4 -7 8.65640 4.53064 1 14 -4 -7 5.00800 4.65672 5 14 -4 -6 76.7817 6.82976 5 14 4 -6 69.6276 6.85657 5 14 4 -5 7.49064 5.12259 5 14 -4 -5 7.43444 4.75589 5 14 4 -4 90.4681 7.63292 5 14 -4 -4 98.9388 7.57751 5 14 4 -3 7.51064 5.18135 5 14 -4 -3 6.40642 4.90834 5 14 4 -2 9.93864 5.31933 5 14 -4 -2 6.56748 4.96821 5 14 4 -1 3.79268 4.98514 5 14 -4 -1-1.95351 5.64525 5 14 -4 0-4.75002 5.96620 5 14 4 0 12.3308 5.72961 5 14 -4 1 3.76147 6.04972 5 14 4 1 9.57860 5.71725 5 14 4 2 21.2441 6.68541 5 -14 -5 15 20.2618 6.66052 6 -14 -5 14 4.35511 5.88441 6 -14 -5 13-4.04241 5.59171 6 -14 -5 12 11.5895 5.69052 6 14 5 -9 58.8180 6.44645 1 14 5 -8 42.8155 5.83799 1 14 -5 -8 40.8471 5.61375 5 14 5 -7 8.80174 4.95436 5 14 5 -7 9.82418 4.68798 1 14 -5 -7 3.69162 4.46011 5 14 5 -6 13.6548 4.77010 1 14 5 -6 13.3801 5.15932 5 14 -5 -6 12.6523 4.77847 5 14 5 -5 2.21379 4.75061 5 14 -5 -5 3.03004 4.57084 5 14 5 -4 0.68824 4.76040 5 14 -5 -4-0.81452 4.53882 5 14 -5 -3 64.4834 6.72158 5 14 5 -3 64.8673 6.91752 5 14 5 -2 20.3559 5.51571 5 14 -5 -2 17.4518 5.33785 5 14 5 -1 68.8574 7.27406 5 14 -5 -1 55.1126 7.18587 5 14 -5 0 1.08748 5.85060 5 14 5 0 12.2556 5.56836 5 14 -5 1 22.0212 6.55549 5 14 5 1 29.8075 6.21099 5 -14 -6 14 4.81314 5.95525 6 -14 -6 13 82.1796 8.25363 6 14 6 -9 5.90548 4.89580 1 14 6 -8 2.97774 4.66826 1 14 6 -7 71.7372 6.92562 1 14 6 -7 74.7951 6.93209 5 14 6 -6 22.6190 5.20212 1 14 6 -6 21.5135 5.42842 5 14 6 -5 50.0555 6.11418 1 14 6 -5 42.8885 6.13730 5 14 6 -4 4.80487 4.94482 5 14 -6 -4 13.4776 5.02303 5 14 6 -3 14.4182 5.52931 5 14 -6 -3 19.5868 5.30569 5 14 6 -2 0.17610 5.10798 5 14 -6 -2 6.76494 5.14152 5 14 6 -1 3.39468 5.26978 5 14 -6 -1-2.08970 5.50585 5 14 -6 0-5.74021 6.23153 5 14 6 0 8.70602 5.37738 5 14 -6 1 18.1094 6.29966 5 14 6 1 26.1903 6.09482 5 -14 -7 14 9.00725 6.14478 6 -14 -7 13-3.44399 5.90659 6 14 7 -9 22.7025 5.64493 1 14 7 -8 30.7226 5.65442 1 14 7 -7 27.4015 5.67134 1 14 7 -7 20.6929 5.31480 5 14 7 -6 6.68973 4.94464 1 14 7 -6 3.38506 4.79338 5 14 7 -5 0.66374 4.62864 1 14 7 -5-0.84795 4.76329 5 14 7 -4 9.75744 4.91004 1 14 7 -4 1.36638 4.79926 5 14 7 -3-0.34551 4.77966 5 14 7 -2 58.1925 6.93788 5 14 7 -1 15.9411 5.43587 5 -14 -8 13 3.50584 5.94983 6 14 8 -9 5.40795 5.24108 1 14 8 -8 16.5334 5.36232 1 14 8 -7 24.2359 5.56207 1 14 8 -6 112.709 8.26639 1 14 8 -6 112.099 8.13439 5 14 8 -5 14.8763 5.37461 1 14 8 -5 10.9675 5.11937 5 14 8 -4 42.4053 6.11414 1 14 8 -4 47.4935 6.35880 5 14 8 -3 0.51735 4.61718 1 14 8 -3 1.02724 4.97602 5 14 9 -10-0.18816 5.03143 1 14 9 -9 64.8883 7.16731 1 14 9 -8 11.0217 5.36905 1 14 9 -7 35.6366 6.16776 1 14 9 -6 27.2479 5.74237 1 14 9 -5 3.95215 5.03515 1 14 9 -4 0.17933 4.79529 1 14 9 -3 26.1914 5.92529 1 14 9 -2 6.47365 4.98966 1 14 10 -10 3.66705 5.41552 1 14 10 -9 0.95539 5.17983 1 14 10 -8 3.40750 5.17007 1 14 10 -7 49.7793 6.91973 1 14 10 -6 17.3583 5.80002 1 14 10 -5 81.8652 7.80102 1 14 10 -4 12.0779 5.54555 1 14 10 -3 21.2157 5.73199 1 14 10 -2-1.30515 5.15261 1 14 10 -1 6.17051 5.45420 1 14 11 -10 56.2775 7.15224 1 14 11 -9 4.50842 5.46265 1 14 11 -8 48.0787 6.95130 1 14 11 -7 3.28876 5.32150 1 14 11 -6-0.96259 5.28245 1 14 11 -5-0.19207 5.20666 1 14 11 -4 3.83954 5.31862 1 14 11 -3 3.46090 5.19371 1 15 0 -8 50.9309 6.44805 5 15 0 -7 0.70587 4.89386 5 15 0 -6 156.194 9.66259 5 15 0 -5 1.62293 5.03602 5 15 0 -4 10.4174 5.48003 5 15 0 -3 2.59666 5.21586 5 15 0 -2 4.52969 5.46327 5 15 0 -1 0.57683 5.33852 5 15 0 0 49.8049 7.02350 5 -15 -1 15 4.98363 5.86863 6 15 -1 -9 17.0195 5.30707 5 15 1 -8 4.60639 5.00597 5 15 -1 -8 4.86737 4.88403 5 15 1 -7 2.66796 5.04184 5 15 -1 -7 4.02279 5.07330 5 15 1 -6 9.85779 5.46257 5 15 -1 -6 14.8514 5.42520 5 15 1 -5 37.8880 6.18284 5 15 -1 -5 37.9657 6.25452 5 15 1 -4 22.7630 5.90864 5 15 -1 -4 21.2563 5.84313 5 15 1 -3 32.2072 6.20632 5 15 -1 -3 29.8902 6.00047 5 15 1 -2 35.5650 6.44735 5 15 -1 -2 27.2620 6.25756 5 15 1 -1 45.0355 6.78926 5 15 -1 -1 35.8633 6.67228 5 15 1 0 11.7709 6.04798 5 15 -1 0 14.8819 6.04241 5 -15 -2 15 69.4440 7.87537 6 -15 -2 14 4.54896 5.79542 6 -15 -2 13 24.0470 6.05082 6 15 -2 -9 54.1219 6.45290 5 15 2 -8-1.60701 4.93438 5 15 -2 -8 0.17181 4.82583 5 15 2 -7 97.3753 8.07616 5 15 -2 -7 90.5095 7.67199 5 15 2 -6-3.42188 5.21250 5 15 -2 -6-1.92737 5.13621 5 15 2 -5 33.6659 6.12363 5 15 -2 -5 31.7844 6.04881 5 15 2 -4-5.52511 5.31844 5 15 -2 -4 4.68845 5.10517 5 15 2 -3 8.76271 5.43144 5 15 -2 -3 0.55022 5.09350 5 15 2 -2 14.5779 5.93538 5 15 -2 -2 11.4059 5.70431 5 15 2 -1 26.5626 6.18638 5 15 -2 -1 16.8063 5.96479 5 15 2 0 8.02726 5.82946 5 15 -2 0 1.36541 5.77229 5 -15 -3 14 22.0998 6.21158 6 -15 -3 13 13.1217 5.74385 6 -15 -3 12 46.1064 6.82525 6 15 -3 -9 20.0764 5.33944 5 15 -3 -8 0.67751 4.60278 5 15 3 -8 0.71871 4.90055 5 15 3 -7-5.57561 5.09266 5 15 -3 -7-1.19614 4.89250 5 15 3 -6 16.0935 5.68030 5 15 -3 -6 16.1206 5.49585 5 15 3 -5 25.3720 5.90512 5 15 -3 -5 25.6819 5.72749 5 15 3 -4 71.7499 7.35204 5 15 -3 -4 81.2897 7.47612 5 15 3 -3 48.3242 6.72416 5 15 -3 -3 42.0401 6.50436 5 15 3 -2 28.1855 6.16614 5 15 -3 -2 27.8483 6.17514 5 15 3 -1 5.18526 5.41479 5 15 -3 -1 7.21387 5.50799 5 15 3 0 13.8491 5.67812 5 15 -3 0-0.58194 6.15225 5 -15 -4 14 35.2523 6.81337 6 -15 -4 13 1.28817 5.69652 6 -15 -4 12 16.9681 5.98917 6 15 -4 -9 3.98171 4.77128 5 15 4 -8 64.0334 6.95438 5 15 -4 -8 61.0125 6.48296 5 15 4 -7 6.49611 5.02863 5 15 -4 -7 1.68452 4.80212 5 15 -4 -6 65.3410 6.99129 5 15 4 -6 67.5596 7.25027 5 15 4 -5 3.46869 5.28904 5 15 -4 -5-2.60761 4.87154 5 15 4 -4 11.6091 5.60200 5 15 -4 -4 16.6054 5.53119 5 15 4 -3 19.7595 5.68792 5 15 -4 -3 13.6977 5.73486 5 15 4 -2 19.4365 5.89758 5 15 -4 -2 21.7269 5.91781 5 15 4 -1 8.03324 5.71675 5 15 -4 -1 12.0534 5.84636 5 -15 -5 13 10.1604 6.05538 6 -15 -5 12 30.7999 6.45465 6 15 5 -7 2.34917 5.03480 5 15 -5 -7-2.65027 4.83474 5 15 5 -6-3.62474 5.32946 5 15 -5 -6-2.35702 4.74012 5 15 5 -5 14.0432 5.47122 5 15 -5 -5 10.7960 5.22861 5 15 5 -4-1.10361 5.13667 5 15 -5 -4 0.69788 5.17784 5 15 -5 -3 65.0097 7.13019 5 15 5 -3 47.8045 6.83117 5 15 5 -2 15.2163 5.70678 5 15 -5 -2 26.3956 5.85654 5 15 5 -1 41.2876 6.91814 5 15 -5 -1 50.5429 6.97208 5 -15 -6 13 22.2870 6.56816 6 15 6 -9 24.0622 5.52717 1 15 6 -8-1.02686 4.78502 1 15 6 -7 94.2965 7.68648 1 15 6 -7 98.9966 8.01645 5 15 6 -6 1.80904 5.20735 5 15 6 -5 15.6424 5.41274 5 15 6 -4-1.46710 5.22106 5 15 6 -3 2.03457 5.18974 5 15 -6 -3 4.38834 5.17796 5 15 6 -2 5.41767 5.39243 5 15 -6 -2 9.70664 5.44599 5 15 6 -1 34.1499 6.52619 5 15 -6 -1 32.5747 6.19869 5 15 7 -9 7.03481 5.16120 1 15 7 -8 10.6394 5.16091 1 15 7 -7 8.04694 5.14996 1 15 7 -7 0.18037 5.07863 5 15 7 -6 26.6464 5.76952 1 15 7 -6 22.5364 5.75505 5 15 7 -5-1.08588 5.17530 5 15 7 -4 20.2299 5.76976 5 15 7 -3 8.80906 5.47885 5 15 7 -2 33.5073 6.29924 5 15 8 -9 0.93061 5.03312 1 15 8 -8 80.5394 7.64743 1 15 8 -7 19.2173 5.54865 1 15 8 -6 93.3510 7.92555 1 15 8 -6 86.9465 7.83459 5 15 8 -5 5.35144 5.03363 1 15 8 -5 0.53881 5.13076 5 15 8 -4 11.1939 5.36579 5 15 9 -10 12.6164 5.57798 1 15 9 -9 60.5227 7.36109 1 15 9 -8 2.83886 5.27356 1 15 9 -7 4.30973 5.38291 1 15 9 -6 5.95092 5.18960 1 15 9 -5 27.7236 6.16199 1 15 9 -4 2.39444 5.28469 1 15 10 -8 29.6090 6.21604 1 15 10 -7 55.4226 7.15313 1 15 10 -6 11.5107 5.57763 1 16 0 -9-6.70689 5.34775 5 16 0 -8 45.9667 6.68624 5 16 0 -7 0.18800 5.21982 5 16 0 -6 2.46636 5.21223 5 16 0 -5-0.95783 5.28765 5 16 0 -4 21.6745 6.17637 5 16 0 -3-1.56788 5.57970 5 16 -1 -9-0.92136 5.11633 5 16 1 -8-1.88324 5.20448 5 16 -1 -8 5.54890 5.20716 5 16 1 -7 18.3668 5.93811 5 16 -1 -7 26.6659 6.15661 5 16 1 -6 35.2835 6.40930 5 16 -1 -6 34.2602 6.27699 5 16 1 -5 25.7975 6.18556 5 16 -1 -5 28.3463 6.22432 5 16 1 -4 29.1649 6.35523 5 16 -1 -4 21.9396 6.09186 5 16 1 -3 4.71927 5.60627 5 16 -1 -3 6.82487 5.55339 5 16 -2 -9 46.0150 6.54580 5 16 -2 -8-1.46363 5.09154 5 16 2 -8 0.18946 5.13586 5 16 2 -7 23.3966 6.06108 5 16 -2 -7 32.2846 6.13600 5 16 2 -6 1.14944 5.50826 5 16 -2 -6-0.55924 5.12709 5 16 2 -5 1.73789 5.44217 5 16 -2 -5-0.18858 5.29060 5 16 2 -4 4.67701 5.45623 5 16 -2 -4 5.34494 5.44208 5 16 2 -3 64.3549 7.52823 5 16 -2 -3 62.2186 7.52829 5 16 -3 -9 0.89613 5.11382 5 16 -3 -8 4.51173 5.15077 5 16 3 -8 5.33188 5.30706 5 16 3 -7 17.1825 5.87523 5 16 -3 -7 10.3886 5.35314 5 16 3 -6 25.9324 6.02121 5 16 -3 -6 29.5025 6.13267 5 16 3 -5 14.1267 5.73732 5 16 -3 -5 6.90386 5.40053 5 16 3 -4 36.2673 6.57529 5 16 -3 -4 46.9102 6.71349 5 16 3 -3 10.0373 5.86094 5 16 -3 -3 14.2183 5.85999 5 -16 -4 13-7.86083 6.01078 6 16 -4 -9-1.93854 4.85883 5 16 -4 -8 44.9139 6.29407 5 16 4 -8 50.5914 6.83857 5 16 4 -7-1.33901 5.31104 5 16 -4 -7 0.35925 4.95798 5 16 4 -6 2.88256 5.24179 5 16 -4 -6 3.09356 5.31199 5 16 4 -5-0.19343 5.26933 5 16 -4 -5 1.10539 5.17457 5 16 4 -4 11.6948 5.78837 5 16 -4 -4 14.5894 5.68440 5 16 -4 -3 7.98483 5.51160 5 -16 -5 12 6.17585 6.00900 6 16 5 -8 6.11889 5.29893 5 16 5 -7 33.0997 6.22021 5 16 5 -6 4.41375 5.42443 5 16 -5 -6 11.4573 5.46129 5 16 -5 -5 65.5605 7.28674 5 16 5 -5 60.7999 7.37600 5 16 5 -4 1.16526 5.59670 5 16 -5 -4 4.42740 5.35639 5 16 6 -7 6.86933 5.40496 5 16 6 -6 2.86871 5.19758 5 16 6 -5 1.15302 5.42834 5 16 7 -9 4.61061 5.21078 1 16 7 -7 12.9225 5.75211 5 16 7 -6 35.3741 6.31687 5 16 8 -8 76.8590 7.71264 1 0 0 0 0.00 0.00 0 TITL 200803_Weber_Ru-TBPDA_a_ in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 11.941411 15.075454 12.849704 90.0000 116.7075 90.0000 ZERR 7.00 0.000430 0.000294 0.000500 0.0000 0.0050 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Ru UNIT 126.00 112.00 28.00 63.00 7.00 TREF HKLF 4 END ; _shelx_hkl_checksum 86686 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.37118(2) 0.61748(2) 0.68943(2) 0.03325(9) Uani 1 1 d . . . . . O2 O 0.4675(2) 0.50456(13) 0.73303(19) 0.0434(5) Uani 1 1 d . . . . . O7 O 0.5371(2) 0.67460(14) 0.7112(2) 0.0442(5) Uani 1 1 d . . . . . O5 O 0.2409(2) 0.55398(15) 0.7270(2) 0.0482(5) Uani 1 1 d . . . . . N4 N 0.4492(2) 0.63623(15) 0.8586(2) 0.0384(5) Uani 1 1 d . . . . . N2 N 0.3147(2) 0.55915(14) 0.5216(2) 0.0338(5) Uani 1 1 d . . . . . O3 O 0.5049(2) 0.37610(14) 0.6700(2) 0.0577(7) Uani 1 1 d . . . . . O8 O 0.7167(2) 0.7237(2) 0.8520(3) 0.0807(9) Uani 1 1 d . . . . . O6 O 0.2071(3) 0.52084(19) 0.8794(3) 0.0754(8) Uani 1 1 d . . . . . O4 O 0.2574(2) 0.74321(15) 0.4101(2) 0.0577(7) Uani 1 1 d . . . . . N1 N 0.2912(2) 0.71814(16) 0.6568(2) 0.0411(6) Uani 1 1 d . . . . . O1 O 0.2409(3) 0.78544(16) 0.6389(2) 0.0688(8) Uani 1 1 d . . . . . N3 N 0.0669(2) 0.69367(17) 0.3796(3) 0.0474(7) Uani 1 1 d . . . . . C2 C 0.3687(3) 0.47869(17) 0.5300(3) 0.0360(6) Uani 1 1 d . . . . . C3 C 0.3503(3) 0.4285(2) 0.4345(3) 0.0437(7) Uani 1 1 d . . . . . H3 H 0.390454 0.374125 0.443509 0.052 Uiso 1 1 calc R . . . . C1 C 0.4539(3) 0.44789(18) 0.6512(3) 0.0388(6) Uani 1 1 d . . . . . C4 C 0.2714(3) 0.4598(2) 0.3253(3) 0.0513(8) Uani 1 1 d . . . . . H4 H 0.256628 0.426578 0.259325 0.062 Uiso 1 1 calc R . . . . C13 C 0.3907(3) 0.60141(19) 0.9160(3) 0.0443(7) Uani 1 1 d . . . . . C17 C 0.5635(3) 0.6722(2) 0.9066(3) 0.0461(8) Uani 1 1 d . . . . . C7 C 0.1868(3) 0.68255(19) 0.4029(3) 0.0393(6) Uani 1 1 d . . . . . C12 C 0.2695(3) 0.5554(2) 0.8379(4) 0.0532(9) Uani 1 1 d . . . . . C14 C 0.4484(4) 0.6061(2) 1.0359(3) 0.0564(10) Uani 1 1 d . . . . . H14 H 0.409831 0.582811 1.078705 0.068 Uiso 1 1 calc R . . . . C16 C 0.6238(4) 0.6780(2) 1.0279(3) 0.0599(10) Uani 1 1 d . . . . . H16 H 0.703184 0.703190 1.066126 0.072 Uiso 1 1 calc R . . . . C6 C 0.2374(3) 0.5896(2) 0.4148(3) 0.0364(6) Uani 1 1 d . . . . . C5 C 0.2143(3) 0.5414(2) 0.3149(3) 0.0468(7) Uani 1 1 d . . . . . H5 H 0.161020 0.563817 0.241786 0.056 Uiso 1 1 calc R . . . . C18 C 0.6114(3) 0.6934(2) 0.8193(3) 0.0517(9) Uani 1 1 d . . . . . C15 C 0.5636(4) 0.6456(3) 1.0906(3) 0.0656(11) Uani 1 1 d . . . . . H15 H 0.602282 0.650880 1.171366 0.079 Uiso 1 1 calc R . . . . C8 C -0.0219(3) 0.6202(2) 0.3649(4) 0.0573(9) Uani 1 1 d . . . . . H8A H 0.015633 0.564565 0.359037 0.069 Uiso 1 1 calc R . . . . H8B H -0.097579 0.628858 0.292652 0.069 Uiso 1 1 calc R . . . . C10 C 0.0167(4) 0.7840(3) 0.3570(4) 0.0688(12) Uani 1 1 d . . . . . H10A H 0.079367 0.824894 0.409462 0.083 Uiso 1 1 calc R . . . . H10B H -0.056196 0.787480 0.371443 0.083 Uiso 1 1 calc R . . . . C9 C -0.0557(4) 0.6147(3) 0.4631(4) 0.0697(12) Uani 1 1 d . . . . . H9A H -0.115951 0.568129 0.448003 0.104 Uiso 1 1 calc GR . . . . H9B H -0.091080 0.670096 0.470505 0.104 Uiso 1 1 calc GR . . . . H9C H 0.018077 0.602184 0.534108 0.104 Uiso 1 1 calc GR . . . . C11 C -0.0194(4) 0.8101(3) 0.2326(5) 0.0935(16) Uani 1 1 d . . . . . H11A H -0.086057 0.772464 0.180795 0.140 Uiso 1 1 calc GR . . . . H11B H 0.051776 0.803712 0.217219 0.140 Uiso 1 1 calc GR . . . . H11C H -0.046993 0.870711 0.220491 0.140 Uiso 1 1 calc GR . . . . O9 O 0.0775(8) 0.4344(7) 0.9779(9) 0.333(6) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.03671(14) 0.02917(12) 0.03524(14) -0.00106(9) 0.01738(11) 0.00182(9) O2 0.0502(12) 0.0354(10) 0.0428(12) 0.0036(9) 0.0193(11) 0.0084(9) O7 0.0452(12) 0.0415(11) 0.0500(14) -0.0052(10) 0.0251(11) -0.0043(9) O5 0.0486(12) 0.0468(12) 0.0568(14) 0.0008(11) 0.0303(12) -0.0056(10) N4 0.0462(14) 0.0316(11) 0.0367(13) -0.0009(10) 0.0181(12) 0.0089(10) N2 0.0369(12) 0.0276(10) 0.0419(14) -0.0061(10) 0.0220(11) -0.0050(9) O3 0.0681(16) 0.0378(12) 0.0663(17) 0.0021(11) 0.0294(15) 0.0147(10) O8 0.0493(15) 0.098(2) 0.090(2) -0.0250(18) 0.0269(16) -0.0231(15) O6 0.091(2) 0.0691(18) 0.097(2) 0.0093(16) 0.071(2) -0.0040(15) O4 0.0501(13) 0.0389(11) 0.0817(19) -0.0002(12) 0.0274(14) -0.0094(10) N1 0.0448(13) 0.0384(13) 0.0382(14) -0.0021(11) 0.0172(12) 0.0069(11) O1 0.0873(19) 0.0488(14) 0.0617(17) 0.0028(13) 0.0258(16) 0.0305(13) N3 0.0447(14) 0.0426(14) 0.0583(18) 0.0056(13) 0.0260(14) 0.0037(11) C2 0.0354(13) 0.0310(12) 0.0455(17) -0.0034(12) 0.0216(14) -0.0047(11) C3 0.0470(16) 0.0345(14) 0.055(2) -0.0102(14) 0.0276(16) -0.0062(13) C1 0.0410(15) 0.0301(13) 0.0506(18) 0.0018(13) 0.0253(15) -0.0001(11) C4 0.059(2) 0.0475(18) 0.056(2) -0.0175(16) 0.0336(19) -0.0111(15) C13 0.0605(19) 0.0336(14) 0.0474(18) 0.0040(13) 0.0319(17) 0.0149(13) C17 0.0486(17) 0.0330(14) 0.0484(19) -0.0048(13) 0.0144(16) 0.0081(12) C7 0.0436(15) 0.0357(14) 0.0365(16) -0.0005(12) 0.0161(14) -0.0038(12) C12 0.067(2) 0.0409(16) 0.069(2) 0.0070(17) 0.046(2) 0.0072(15) C14 0.087(3) 0.0450(18) 0.0430(19) 0.0073(15) 0.034(2) 0.0256(18) C16 0.060(2) 0.0474(18) 0.048(2) -0.0096(16) 0.0022(19) 0.0095(16) C6 0.0344(13) 0.0361(13) 0.0385(16) -0.0016(13) 0.0163(13) -0.0078(11) C5 0.0485(17) 0.0525(18) 0.0379(17) -0.0054(14) 0.0181(15) -0.0093(14) C18 0.0457(18) 0.0424(17) 0.066(2) -0.0054(16) 0.0246(19) -0.0010(14) C15 0.099(3) 0.0505(19) 0.0369(18) 0.0015(17) 0.021(2) 0.027(2) C8 0.0447(18) 0.064(2) 0.062(2) -0.0017(18) 0.0229(19) -0.0101(16) C10 0.064(2) 0.057(2) 0.096(3) 0.024(2) 0.045(3) 0.0195(18) C9 0.066(2) 0.067(3) 0.086(3) 0.006(2) 0.042(3) -0.0024(19) C11 0.069(3) 0.101(4) 0.102(4) 0.049(3) 0.031(3) 0.024(3) O9 0.256(8) 0.445(13) 0.403(15) 0.257(12) 0.242(11) 0.062(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 4 18 -10 0.1293 -5 17 11 0.0956 -6 -13 14 0.1406 5 -17 -11 0.1264 7 16 -11 0.1128 -14 2 -2 0.0815 -7 -16 11 0.1560 13 -4 3 0.0267 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Ru1 O7 85.45(8) . . ? O2 Ru1 O5 86.45(9) . . ? O2 Ru1 N2 79.18(9) . . ? O7 Ru1 N2 99.03(8) . . ? O5 Ru1 O7 160.63(9) . . ? O5 Ru1 N2 96.68(9) . . ? N4 Ru1 O2 83.39(9) . . ? N4 Ru1 O7 80.83(10) . . ? N4 Ru1 O5 80.78(10) . . ? N4 Ru1 N2 162.52(9) . . ? N1 Ru1 O2 177.63(11) . . ? N1 Ru1 O7 93.34(10) . . ? N1 Ru1 O5 94.09(11) . . ? N1 Ru1 N4 94.41(11) . . ? N1 Ru1 N2 103.03(11) . . ? C1 O2 Ru1 119.08(19) . . ? C18 O7 Ru1 112.9(2) . . ? C12 O5 Ru1 113.2(2) . . ? C13 N4 Ru1 116.8(2) . . ? C13 N4 C17 125.9(3) . . ? C17 N4 Ru1 116.6(2) . . ? C2 N2 Ru1 111.4(2) . . ? C6 N2 Ru1 130.50(19) . . ? C6 N2 C2 118.1(2) . . ? O1 N1 Ru1 177.8(3) . . ? C7 N3 C8 124.5(3) . . ? C7 N3 C10 117.6(3) . . ? C10 N3 C8 117.6(3) . . ? N2 C2 C3 122.9(3) . . ? N2 C2 C1 115.8(3) . . ? C3 C2 C1 121.2(3) . . ? C2 C3 H3 120.5 . . ? C2 C3 C4 119.0(3) . . ? C4 C3 H3 120.5 . . ? O2 C1 C2 114.4(2) . . ? O3 C1 O2 123.7(3) . . ? O3 C1 C2 121.9(3) . . ? C3 C4 H4 120.5 . . ? C3 C4 C5 119.0(3) . . ? C5 C4 H4 120.5 . . ? N4 C13 C12 113.5(3) . . ? N4 C13 C14 118.5(4) . . ? C14 C13 C12 127.9(3) . . ? N4 C17 C16 116.7(3) . . ? N4 C17 C18 113.2(3) . . ? C16 C17 C18 129.9(3) . . ? O4 C7 N3 124.0(3) . . ? O4 C7 C6 117.2(3) . . ? N3 C7 C6 118.7(3) . . ? O5 C12 C13 115.7(3) . . ? O6 C12 O5 124.2(4) . . ? O6 C12 C13 120.1(4) . . ? C13 C14 H14 120.7 . . ? C15 C14 C13 118.6(4) . . ? C15 C14 H14 120.7 . . ? C17 C16 H16 120.5 . . ? C15 C16 C17 119.0(4) . . ? C15 C16 H16 120.5 . . ? N2 C6 C7 118.8(3) . . ? N2 C6 C5 121.6(3) . . ? C5 C6 C7 119.3(3) . . ? C4 C5 C6 119.4(3) . . ? C4 C5 H5 120.3 . . ? C6 C5 H5 120.3 . . ? O7 C18 C17 116.4(3) . . ? O8 C18 O7 123.5(4) . . ? O8 C18 C17 120.0(4) . . ? C14 C15 C16 121.2(4) . . ? C14 C15 H15 119.4 . . ? C16 C15 H15 119.4 . . ? N3 C8 H8A 109.1 . . ? N3 C8 H8B 109.1 . . ? N3 C8 C9 112.5(3) . . ? H8A C8 H8B 107.8 . . ? C9 C8 H8A 109.1 . . ? C9 C8 H8B 109.1 . . ? N3 C10 H10A 109.6 . . ? N3 C10 H10B 109.6 . . ? N3 C10 C11 110.5(4) . . ? H10A C10 H10B 108.1 . . ? C11 C10 H10A 109.6 . . ? C11 C10 H10B 109.6 . . ? C8 C9 H9A 109.5 . . ? C8 C9 H9B 109.5 . . ? C8 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 O2 1.9887(19) . ? Ru1 O7 2.060(2) . ? Ru1 O5 2.060(2) . ? Ru1 N4 1.963(3) . ? Ru1 N2 2.139(2) . ? Ru1 N1 1.741(2) . ? O2 C1 1.307(4) . ? O7 C18 1.300(4) . ? O5 C12 1.308(4) . ? N4 C13 1.330(4) . ? N4 C17 1.335(4) . ? N2 C2 1.355(3) . ? N2 C6 1.344(4) . ? O3 C1 1.212(3) . ? O8 C18 1.222(4) . ? O6 C12 1.211(4) . ? O4 C7 1.219(3) . ? N1 O1 1.148(3) . ? N3 C7 1.335(4) . ? N3 C8 1.485(4) . ? N3 C10 1.463(4) . ? C2 C3 1.373(4) . ? C2 C1 1.501(4) . ? C3 H3 0.9300 . ? C3 C4 1.375(5) . ? C4 H4 0.9300 . ? C4 C5 1.384(5) . ? C13 C12 1.510(5) . ? C13 C14 1.378(5) . ? C17 C16 1.395(5) . ? C17 C18 1.504(5) . ? C7 C6 1.506(4) . ? C14 H14 0.9300 . ? C14 C15 1.369(6) . ? C16 H16 0.9300 . ? C16 C15 1.388(6) . ? C6 C5 1.390(4) . ? C5 H5 0.9300 . ? C15 H15 0.9300 . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C8 C9 1.491(6) . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 C11 1.509(6) . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C11 H11A 0.9600 . ? C11 H11B 0.9600 . ? C11 H11C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ru1 O2 C1 O3 -177.1(2) . . . . ? Ru1 O2 C1 C2 2.8(3) . . . . ? Ru1 O7 C18 O8 176.4(3) . . . . ? Ru1 O7 C18 C17 -1.0(4) . . . . ? Ru1 O5 C12 O6 -178.8(3) . . . . ? Ru1 O5 C12 C13 -0.7(3) . . . . ? Ru1 N4 C13 C12 -2.1(3) . . . . ? Ru1 N4 C13 C14 174.1(2) . . . . ? Ru1 N4 C17 C16 -174.2(2) . . . . ? Ru1 N4 C17 C18 1.0(3) . . . . ? Ru1 N2 C2 C3 -178.3(2) . . . . ? Ru1 N2 C2 C1 0.1(3) . . . . ? Ru1 N2 C6 C7 6.0(4) . . . . ? Ru1 N2 C6 C5 178.9(2) . . . . ? N4 C13 C12 O5 1.8(4) . . . . ? N4 C13 C12 O6 -180.0(3) . . . . ? N4 C13 C14 C15 -0.5(4) . . . . ? N4 C17 C16 C15 0.9(5) . . . . ? N4 C17 C18 O7 0.1(4) . . . . ? N4 C17 C18 O8 -177.4(3) . . . . ? N2 C2 C3 C4 -1.6(4) . . . . ? N2 C2 C1 O2 -1.9(3) . . . . ? N2 C2 C1 O3 178.0(3) . . . . ? N2 C6 C5 C4 0.5(5) . . . . ? O4 C7 C6 N2 76.9(4) . . . . ? O4 C7 C6 C5 -96.1(4) . . . . ? N3 C7 C6 N2 -106.3(3) . . . . ? N3 C7 C6 C5 80.7(4) . . . . ? C2 N2 C6 C7 -174.0(2) . . . . ? C2 N2 C6 C5 -1.1(4) . . . . ? C2 C3 C4 C5 0.8(5) . . . . ? C3 C2 C1 O2 176.6(3) . . . . ? C3 C2 C1 O3 -3.5(4) . . . . ? C3 C4 C5 C6 -0.3(5) . . . . ? C1 C2 C3 C4 -179.9(3) . . . . ? C13 N4 C17 C16 -3.8(4) . . . . ? C13 N4 C17 C18 171.4(3) . . . . ? C13 C14 C15 C16 -2.1(5) . . . . ? C17 N4 C13 C12 -172.5(3) . . . . ? C17 N4 C13 C14 3.7(4) . . . . ? C17 C16 C15 C14 1.9(5) . . . . ? C7 N3 C8 C9 109.8(4) . . . . ? C7 N3 C10 C11 81.3(4) . . . . ? C7 C6 C5 C4 173.3(3) . . . . ? C12 C13 C14 C15 175.0(3) . . . . ? C14 C13 C12 O5 -173.9(3) . . . . ? C14 C13 C12 O6 4.3(5) . . . . ? C16 C17 C18 O7 174.5(3) . . . . ? C16 C17 C18 O8 -3.0(6) . . . . ? C6 N2 C2 C3 1.7(4) . . . . ? C6 N2 C2 C1 -179.9(2) . . . . ? C18 C17 C16 C15 -173.3(3) . . . . ? C8 N3 C7 O4 176.9(3) . . . . ? C8 N3 C7 C6 0.3(5) . . . . ? C8 N3 C10 C11 -93.4(4) . . . . ? C10 N3 C7 O4 2.5(5) . . . . ? C10 N3 C7 C6 -174.0(3) . . . . ? C10 N3 C8 C9 -75.9(4) . . . . ?