#------------------------------------------------------------------------------ #$Date: 2021-10-03 22:07:01 +0300 (Sun, 03 Oct 2021) $ #$Revision: 269462 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519035.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519035 loop_ _publ_author_name 'Zhang, Zong-Hui' 'Fang, Han' 'Xue, Dong-Xu' 'Bai, Junfeng' _publ_section_title ; Tuning Open Metal Site-Free ncb Type of Metal-Organic Frameworks for Simultaneously High Gravimetric and Volumetric Methane Storage Working Capacities. ; _journal_issue 37 _journal_name_full 'ACS applied materials & interfaces' _journal_page_first 44956 _journal_page_last 44963 _journal_paper_doi 10.1021/acsami.1c13757 _journal_volume 13 _journal_year 2021 _chemical_formula_moiety 'C60 H39 Fe3 N6 O16' _chemical_formula_sum 'C60 H39 Fe3 N6 O16' _chemical_formula_weight 1267.52 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-05-15 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 32.5991(9) _cell_length_b 32.5991(9) _cell_length_c 32.5991(9) _cell_measurement_reflns_used 5805 _cell_measurement_temperature 243.0 _cell_measurement_theta_max 39.97 _cell_measurement_theta_min 3.32 _cell_volume 34643.1(17) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 243.0 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0509 _diffrn_reflns_av_unetI/netI 0.0462 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 27 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 16106 _diffrn_reflns_point_group_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 39.972 _diffrn_reflns_theta_max 39.972 _diffrn_reflns_theta_min 1.916 _diffrn_source_current 50.0 _diffrn_source_power 2.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.201 _exptl_absorpt_correction_T_max 0.7479 _exptl_absorpt_correction_T_min 0.4198 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0904 before and 0.0687 after correction. The Ratio of minimum to maximum transmission is 0.5743. The \l/2 correction factor is Not present. ; _exptl_crystal_colour brown _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 0.486 _exptl_crystal_description Polyhedron _exptl_crystal_F_000 5176 _exptl_crystal_size_max 0.08 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.493 _refine_diff_density_min -0.436 _refine_diff_density_rms 0.057 _refine_ls_abs_structure_details ; Flack x determined using 724 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.217(17) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.116 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 169 _refine_ls_number_reflns 1945 _refine_ls_number_restraints 266 _refine_ls_restrained_S_all 1.091 _refine_ls_R_factor_all 0.0803 _refine_ls_R_factor_gt 0.0745 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1042P)^2^+249.1832P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2002 _refine_ls_wR_factor_ref 0.2052 _reflns_Friedel_coverage 0.828 _reflns_Friedel_fraction_full 0.973 _reflns_Friedel_fraction_max 0.973 _reflns_number_gt 1764 _reflns_number_total 1945 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file am1c13757_si_003.cif _cod_data_source_block a _cod_original_cell_volume 34643(3) _cod_database_code 4519035 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.844 _shelx_estimated_absorpt_t_min 0.844 _olex2_refinement_description ; 1. Restrained distances C16-C2 = C2-C10 1.43 with sigma of 0.02 N1-C16 = C16-C2 1.43 with sigma of 0.02 C9-C5 1.43 with sigma of 0.001 N2-C9 1.43 with sigma of 0.001 O3-C9 1.43 with sigma of 0.001 N2-C10 1.43 with sigma of 0.001 C1-C12 = C12-C14 1.43 with sigma of 0.02 C6-C14 = C14-C12 1.43 with sigma of 0.02 C16-C10 2.477 with sigma of 0.04 N1-C2 2.477 with sigma of 0.04 C6-C12 2.477 with sigma of 0.04 C1-C14 2.477 with sigma of 0.04 C9-C11 \\sim C15-C9 with sigma of 0.02 2. Uiso/Uaniso restraints and constraints Uanis(C4) \\sim Ueq, Uanis(N1) \\sim Ueq, Uanis(C10) \\sim Ueq, Uanis(C8) \\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C6) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O2) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O3) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C15) \\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C5) \\sim Ueq, Uanis(C9) \\sim Ueq, Uanis(C2) \\sim Ueq, Uanis(C16) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C13) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O1) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 3. Rigid body (RIGU) restrains O2, Fe1, O1, O4, N1, C4, C8, C16, C1, C2, C12, C10, C14, N2, C6 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C10, N2, C9, O3, C5, C15, C7, C13, C3, C11 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 4. Others Fixed Sof: N2(0.5) H2(0.5) O3(0.5) C9(0.5) C5(0.5) C11(0.5) H11(0.5) C3(0.5) H3(0.5) C13(0.5) C7(0.5) H7(0.5) C15(0.5) H15(0.5) 5.a Aromatic/amide H refined with riding coordinates: N2(H2), C12(H12), C14(H14), C16(H16), C2(H2A), C11(H11), C3(H3), C7(H7), C15(H15) 5.b Fitted hexagon refined as free rotating group: C5(C11,C3,C13,C7,C15) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; a.res created by SHELXL-2014/7 TITL a_a.res in I-43m REM Old TITL a_a.res in I-43m REM SHELXT solution in I-43m REM R1 0.176, Rweak 0.033, Alpha 0.004, Orientation as input REM Flack x = 0.122 ( 0.010 ) from Parsons' quotients REM Formula found by SHELXT: C42 Fe3 N3 O22 CELL 1.54178 32.5991 32.5991 32.5991 90 90 90 ZERR 8 0.0009 0.0009 0.0009 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,+Z SYMM -Y,-X,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +X,+Z,+Y SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM +X,-Z,-Y SYMM +Z,+Y,+X SYMM +Z,-Y,-X SYMM -Z,+Y,-X SYMM -Z,-Y,+X SFAC C H Fe N O UNIT 480 312 24 48 128 ISOR 0.001 0.002 C4 N1 C10 C8 C1 C6 RIGU O2 Fe1 O1 O4 N1 C4 C8 C16 C1 C2 C12 C10 C14 N2 C6 ISOR 0.001 0.002 O2 DFIX 1.43 C16 C2 C2 C10 DANG 2.477 C16 C10 DFIX 1.43 N1 C16 C16 C2 DANG 2.477 N1 C2 DFIX 1.43 0.001 C9 C5 DFIX 1.43 0.001 N2 C9 DFIX 1.43 0.001 O3 C9 DFIX 1.43 0.001 N2 C10 RIGU C10 N2 C9 O3 C5 C15 C7 C13 C3 C11 ISOR 0.01 0.02 O3 ISOR 0.01 0.02 C15 C11 C5 C9 C2 C16 ISOR 0.01 0.02 C13 ISOR 0.01 0.02 O1 SADI C9 C11 C15 C9 DFIX 1.43 C1 C12 C12 C14 DANG 2.477 C6 C12 DANG 2.477 C1 C14 DFIX 1.43 C6 C14 C14 C12 L.S. 99 0 0 PLAN 1 SIZE 0.08 0.08 0.08 TEMP -30.15 CONF BIND C9 C5 FREE C9 C11 FREE C15 C9 BOND $H list 4 MORE -1 ABIN fmap 2 53 acta REM REM REM WGHT 0.104200 249.183212 FVAR 0.16258 FE1 3 0.628069 0.699402 0.300598 10.50000 0.01832 0.02546 = 0.02546 -0.00003 0.00048 -0.00048 O1 5 0.650538 0.759298 0.301862 11.00000 0.06545 0.04184 = 0.07615 0.01698 -0.04378 -0.01064 O4 5 0.599496 0.643357 0.290464 11.00000 0.01333 0.03609 = 0.10529 0.00098 -0.01629 -0.00691 O2 5 0.677230 0.677230 0.322770 10.16667 0.02885 0.02885 = 0.02885 0.00024 0.00024 -0.00024 N1 4 0.573811 0.729146 0.270854 10.50000 0.04680 0.04727 = 0.04727 0.00017 -0.00047 0.00047 C1 1 0.579018 0.579018 0.291979 10.50000 0.03594 0.03594 = 0.03576 0.00013 0.00013 -0.00034 C4 1 0.675155 0.775934 0.324845 10.50000 0.01996 0.01973 = 0.01996 0.00028 0.00017 -0.00028 C6 1 0.516374 0.516374 0.290204 10.50000 0.06927 0.06927 = 0.06939 -0.00011 -0.00011 -0.00022 C8 1 0.611377 0.611377 0.286406 10.50000 0.03503 0.03503 = 0.03501 -0.00049 -0.00049 0.00002 PART -1 N2 4 0.462654 0.778259 0.227385 10.50000 0.07707 0.09147 = 0.06833 0.00933 0.00526 0.01244 AFIX 43 H2 2 0.455583 0.802028 0.237249 10.50000 -1.20000 AFIX 0 PART 0 C10 1 0.501340 0.761088 0.238912 10.50000 0.08975 0.09001 = 0.09001 -0.00005 -0.00020 0.00020 C12 1 0.587899 0.538177 0.289273 11.00000 0.05016 0.04219 = 0.05217 -0.00881 -0.01865 0.00808 AFIX 43 H12 2 0.615629 0.530813 0.286400 11.00000 -1.20000 AFIX 0 C14 1 0.557634 0.504807 0.290486 11.00000 0.06684 0.05280 = 0.16960 -0.00082 -0.00111 -0.00896 AFIX 43 H14 2 0.565618 0.477114 0.291404 11.00000 -1.20000 AFIX 0 C16 1 0.558907 0.712133 0.233787 11.00000 0.08711 0.11717 = 0.08581 -0.01637 -0.01833 0.01074 AFIX 43 H16 2 0.571231 0.689246 0.221305 11.00000 -1.20000 AFIX 0 C2 1 0.523890 0.732085 0.216640 11.00000 0.08193 0.10007 = 0.07436 -0.00526 -0.01049 0.00913 AFIX 43 H2A 2 0.515773 0.725596 0.189743 11.00000 -1.20000 AFIX 0 PART -1 O3 5 0.450897 0.744554 0.161253 10.50000 0.08766 0.14162 = 0.09701 -0.00849 -0.01455 0.03388 C9 1 0.435247 0.757523 0.200127 10.50000 0.09799 0.10911 = 0.10008 -0.00229 -0.00622 0.01153 AFIX 66 C5 1 0.403289 0.786537 0.192296 10.50000 0.08099 0.09261 = 0.09125 0.00063 -0.00389 0.00078 C11 1 0.382440 0.803091 0.225603 10.50000 0.08333 0.10224 = 0.09146 -0.00045 -0.00540 0.00152 AFIX 43 H11 2 0.395537 0.805211 0.251205 10.50000 -1.20000 AFIX 65 C3 1 0.342224 0.816509 0.221054 10.50000 0.09150 0.18511 = 0.09973 -0.01909 -0.01304 0.02765 AFIX 43 H3 2 0.328125 0.827704 0.243578 10.50000 -1.20000 AFIX 65 C13 1 0.322857 0.813375 0.183196 10.50000 0.07810 0.08500 = 0.08864 0.01246 -0.00118 -0.00070 C7 1 0.343705 0.796821 0.149888 10.50000 0.07256 0.07531 = 0.09046 0.00972 -0.00233 -0.00482 AFIX 43 H7 2 0.330608 0.794701 0.124287 10.50000 -1.20000 AFIX 65 C15 1 0.383921 0.783402 0.154438 10.50000 0.07590 0.08482 = 0.08580 0.00177 0.00028 -0.00171 AFIX 43 H15 2 0.398020 0.772208 0.131913 10.50000 -1.20000 AFIX 0 HKLF 4 REM a_a.res in I-43m REM R1 = 0.0745 for 1764 Fo > 4sig(Fo) and 0.0803 for all 1945 data REM 169 parameters refined using 266 restraints END WGHT 0.1050 232.7183 REM Highest difference peak 0.493, deepest hole -0.436, 1-sigma level 0.057 Q1 1 0.7237 0.7236 0.2764 10.16667 0.05 0.49 ; _shelx_res_checksum 37003 _shelx_hkl_file ; 0 -1 1 2153.28 166.18 0 1 1 2053.69 166.18 -2 1 1 9065.59 720.33 2 -1 1 9252.37 720.43 -1 1 2 9171.68 720.73 1 -1 2 9225.68 720.73 1 1 2 9191.78 720.73 -1 -1 2 9042.90 720.73 2 1 1 9059.29 720.43 -2 0 2 1183.28 95.69 0 -2 2 1222.38 96.19 0 2 2 1206.78 96.19 2 0 2 1204.18 95.89 -2 2 2 2312.57 173.78 2 -2 2 2322.47 173.98 2 2 2 1940.11 173.78 -1 0 3 2607.24 207.38 1 0 3 2628.34 207.48 0 1 3 2552.14 201.98 3 0 1 2559.54 201.08 -3 0 1 2512.05 200.88 0 -1 3 2568.14 202.08 2 -1 3 310.37 31.20 -2 1 3 308.07 30.80 2 1 3 415.36 31.50 -2 -1 3 400.96 31.10 -1 2 3 281.77 30.40 -3 1 2 289.97 28.90 3 -1 2 304.07 29.50 1 -2 3 308.47 30.80 3 1 2 400.16 29.80 1 2 3 405.06 30.90 -1 -2 3 421.96 31.00 -3 -1 2 391.36 29.30 -3 0 3 9990.30 787.02 0 3 3 9999.00 787.62 3 0 3 9960.90 787.22 -2 3 3 5025.90 413.06 -3 2 3 5039.50 412.86 -3 3 2 4922.31 412.76 3 -2 3 4947.10 412.96 2 3 3 5504.55 413.46 -3 -2 3 5485.15 412.96 3 2 3 5430.16 413.16 3 3 2 5460.65 413.16 0 0 4 358.26 32.10 2 0 4 606.74 50.19 -2 0 4 583.94 49.90 -1 1 4 6993.50 561.94 4 -1 1 7195.78 560.84 -4 1 1 6922.81 560.64 1 -1 4 7181.68 562.04 4 1 1 6941.51 560.94 -1 -1 4 7333.37 562.04 1 1 4 7256.97 562.04 -3 1 4 30.20 10.30 3 -1 4 23.40 10.90 -1 4 3 7.20 11.80 -3 -1 4 22.50 10.30 3 1 4 24.80 11.10 1 4 3 27.70 13.30 0 2 4 609.04 50.29 4 0 2 576.74 48.40 0 -2 4 606.34 50.29 -4 0 2 583.84 47.80 2 -2 4 4736.73 329.07 -2 2 4 4675.13 328.87 -4 2 2 4625.74 327.97 -2 -2 4 3660.53 328.57 2 2 4 3617.64 328.57 4 2 2 3598.14 327.97 4 -1 3 14.50 9.00 -1 3 4 8.10 11.30 1 -3 4 26.40 13.20 -4 1 3 23.90 8.20 -1 -3 4 29.10 12.70 4 1 3 26.30 9.60 -4 -1 3 37.10 8.60 1 3 4 34.90 13.10 -4 3 3 1290.97 104.39 -3 3 4 1308.27 105.09 -3 4 3 1294.77 105.09 3 -3 4 1256.67 105.19 4 -3 3 1291.67 103.39 3 4 3 1321.97 105.59 3 3 4 1325.87 105.59 4 3 3 1273.27 104.89 -4 0 4 2573.14 200.78 0 4 4 2526.75 201.88 4 -4 0 2395.26 199.98 4 0 4 2614.84 201.28 4 -4 -2 487.25 40.50 2 4 4 454.65 44.40 -4 -2 4 476.55 41.90 4 2 4 492.75 43.10 -4 4 4 6624.04 518.85 4 -4 4 6449.55 517.55 4 -4 -4 6417.56 517.35 4 4 4 6757.32 519.25 -1 0 5 1251.57 102.09 1 0 5 1263.57 102.29 3 0 5 744.53 62.19 5 -3 0 745.63 59.09 -3 0 5 691.73 61.09 0 -1 5 1223.58 99.59 5 0 1 1222.58 97.19 0 1 5 1227.18 99.79 -5 2 1 153.38 15.30 2 -1 5 150.08 22.80 -2 1 5 161.48 21.60 -1 5 4 2017.00 159.78 4 -1 5 2080.49 159.28 -4 1 5 2037.80 158.78 5 -4 1 2050.59 157.38 4 1 5 1939.21 159.18 1 -5 -4 1933.91 157.28 5 -4 -1 1874.11 157.18 -4 -1 5 1939.71 158.68 1 5 4 1964.00 159.78 5 -1 2 171.58 17.10 -5 1 2 155.08 15.50 1 -2 5 152.38 23.30 -1 2 5 164.08 22.20 -3 2 5 737.73 65.29 3 -2 5 692.83 65.69 2 -5 3 761.62 63.09 -5 3 2 706.73 63.29 5 -3 2 669.93 62.69 2 -5 -3 852.91 62.69 -3 -2 5 846.52 65.39 5 3 2 832.62 64.29 3 2 5 869.71 65.89 0 3 5 760.42 63.29 3 -5 0 739.73 59.79 -5 0 3 714.23 59.89 0 -3 5 769.12 63.29 5 0 3 710.73 60.69 5 -2 3 746.13 63.89 3 -5 2 689.63 62.79 -5 2 3 709.03 63.19 -2 3 5 706.33 65.49 2 -3 5 686.63 65.99 3 -5 -2 824.92 62.69 -2 -3 5 857.81 65.89 5 2 3 876.81 64.39 2 3 5 888.31 66.69 -5 4 3 5412.46 411.66 5 -4 3 5453.65 410.86 -4 3 5 5520.35 412.16 -3 5 4 5514.15 412.56 4 -3 5 5421.56 410.76 3 -5 4 5661.53 410.76 4 -3 5 5464.35 412.46 3 -5 -4 4900.11 410.46 5 -4 -3 4765.62 410.46 4 3 5 5033.80 412.26 5 4 3 5131.89 412.06 3 5 4 4473.85 412.26 -4 -3 5 4875.41 411.96 -1 4 5 2035.60 161.08 1 -4 5 2138.29 161.48 4 -5 1 2025.80 158.98 -5 1 4 1989.10 159.48 5 -1 4 2141.79 160.28 -5 -1 4 1904.11 159.48 1 4 5 2004.40 161.38 4 -5 -1 1912.71 158.78 -1 -4 5 1944.01 161.18 5 1 4 1917.71 159.98 3 -4 5 5782.12 422.26 4 -5 3 5589.54 420.26 -4 5 3 5526.95 421.66 5 -3 4 5507.85 420.36 5 -3 4 5665.53 421.56 -3 4 5 5452.55 421.86 3 -4 5 5548.25 420.16 -5 3 4 5350.66 421.06 4 5 3 5050.29 421.76 3 4 5 4464.75 421.66 4 -5 -3 4832.12 419.96 5 3 4 5103.09 421.46 -5 0 5 942.71 75.19 0 5 5 931.21 77.89 5 -5 0 859.61 73.79 5 0 5 910.21 75.89 5 -2 5 2319.97 217.58 -5 2 5 2352.46 217.08 -2 5 5 2313.87 218.08 5 -5 2 2411.16 216.18 2 -5 5 2445.16 215.88 2 5 5 3124.99 219.18 5 -5 -2 3047.99 216.18 2 -5 -5 3166.68 216.18 -5 -2 5 3048.69 217.58 5 2 5 3069.49 218.18 -5 4 5 86.99 17.20 -5 5 4 84.29 16.40 -4 5 5 75.89 19.00 5 -4 5 87.99 13.10 4 -5 5 79.59 12.70 5 -5 4 93.99 12.90 5 -4 5 93.79 18.30 0 -6 0 269.77 25.60 0 0 6 321.77 32.30 2 0 6 438.76 43.00 6 -2 0 469.45 37.60 0 -6 2 440.36 37.80 0 -6 -2 425.26 38.00 -2 0 6 441.66 42.10 6 -4 0 1575.74 128.29 4 0 6 1668.43 130.89 0 6 4 1582.44 131.59 -4 0 6 1608.94 130.39 -1 -6 -1 5106.09 407.26 1 -6 1 4939.51 407.06 1 -1 6 5223.38 409.16 -1 1 6 5117.79 408.96 1 -6 -1 5175.68 407.16 -1 -6 1 5360.66 407.46 -1 -1 6 5172.98 408.96 1 1 6 5271.77 409.06 6 1 1 5073.49 406.96 3 -1 6 4566.34 332.47 6 -3 1 4592.54 330.37 1 -6 3 4280.17 330.07 -3 1 6 4339.67 331.97 1 -6 -3 3876.91 330.07 6 -3 -1 4009.70 330.07 -3 -1 6 3879.81 331.77 3 1 6 3897.31 331.97 1 -6 5 298.77 27.00 -1 6 5 302.77 36.60 -5 1 6 311.57 31.80 5 -1 6 307.47 33.90 6 -5 1 298.97 28.80 6 0 2 415.36 36.30 0 2 6 430.56 41.90 2 -6 0 440.46 36.50 0 -2 6 429.66 41.60 2 -6 2 5468.35 401.46 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8 710.33 73.79 -1 -5 8 740.43 74.39 8 -1 -5 745.43 68.19 3 -5 8 2016.90 154.28 8 -3 5 1979.10 156.18 -8 3 5 1981.40 155.38 3 -5 8 1932.81 158.58 5 -8 3 2017.20 154.78 -3 5 8 1958.60 158.18 -3 -5 8 1850.01 157.98 8 3 5 1772.62 156.18 8 -3 -5 1934.51 153.98 5 -8 -3 1972.70 154.58 3 5 8 1878.61 158.28 -5 5 8 1977.80 159.28 5 -5 8 1944.11 155.78 5 -5 8 1971.60 159.68 -5 8 5 1945.11 159.28 -8 5 5 1924.41 157.28 5 -8 5 1988.40 156.08 8 -5 5 1921.01 156.18 8 -7 5 1019.80 83.59 -5 8 7 1040.90 88.49 7 -5 8 988.30 87.79 5 -8 7 1036.50 83.39 -7 5 8 1104.39 87.29 -8 7 5 1040.40 86.19 7 -5 8 1051.69 83.59 5 8 7 1038.90 89.49 5 -8 -7 980.50 82.89 8 -7 -5 986.00 82.89 7 5 8 1016.20 88.19 8 7 5 986.40 87.29 7 -5 -8 977.60 82.19 6 -8 0 386.76 34.60 0 -6 8 413.76 31.90 8 0 6 337.17 37.80 -8 0 6 337.27 35.40 0 6 8 342.27 41.70 6 -8 2 231.18 26.10 -8 2 6 221.18 26.80 8 -2 6 216.18 29.40 -2 6 8 232.98 30.80 2 -6 8 234.38 23.40 6 -8 -2 262.67 25.60 8 -2 -6 256.27 22.30 8 2 6 269.17 30.50 2 6 8 233.98 35.90 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826.02 67.89 7 -9 -6 824.52 59.89 9 -6 -7 777.42 58.89 9 6 7 796.42 65.39 6 7 9 754.02 67.59 6 -7 -9 802.82 58.99 9 -8 7 88.19 19.20 8 -7 9 107.09 19.00 -7 9 8 73.79 23.90 -8 7 9 89.49 24.50 -9 8 7 119.79 23.30 7 -9 8 104.79 18.80 9 8 7 178.08 26.20 8 7 9 145.19 26.20 7 -9 -8 175.38 20.80 9 -8 -7 157.48 19.80 -1 8 9 771.92 76.59 1 -8 9 789.92 68.69 9 -1 8 770.72 73.59 -9 1 8 817.22 72.19 8 -9 1 785.82 70.39 9 1 8 875.71 74.29 1 8 9 916.81 78.19 -9 -1 8 899.21 72.39 8 -9 -1 921.81 70.49 -1 -8 9 888.61 68.19 -9 3 8 831.62 78.09 8 -9 3 856.11 76.49 9 -3 8 828.22 79.59 -3 8 9 836.82 82.89 3 -8 9 830.82 75.29 3 8 9 1067.79 84.39 8 -9 -3 1034.10 76.29 9 3 8 1038.70 80.59 8 9 3 973.20 81.79 9 -3 -8 961.70 74.39 -9 5 8 597.54 53.69 -8 9 5 597.74 54.99 -5 8 9 599.44 57.59 5 -8 9 631.34 49.40 8 -9 5 610.34 50.49 9 -5 8 603.24 50.79 5 8 9 530.95 58.79 8 9 5 521.05 56.79 9 -5 -8 519.15 47.70 8 -9 -5 516.35 49.20 9 5 8 509.55 55.39 -8 9 7 89.69 22.30 9 -7 8 90.59 16.90 8 -9 7 102.89 18.40 -9 7 8 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4 294.37 30.20 6 -4 10 273.87 39.80 -4 10 6 294.07 40.80 4 -10 8 879.91 72.79 -10 8 4 868.41 75.59 -8 4 10 892.51 78.19 8 -4 10 897.21 73.49 8 -4 10 845.22 78.89 -4 10 8 882.01 80.89 10 -8 4 879.21 73.69 10 -1 5 32.20 13.30 10 1 -5 32.60 9.00 -1 5 10 40.90 23.20 5 -10 1 18.60 12.60 -10 1 5 36.60 10.10 1 -5 10 40.50 9.10 1 -5 10 17.20 20.80 1 5 10 84.69 22.80 -1 -5 10 91.89 22.80 10 1 5 88.99 14.80 3 -5 10 89.19 23.70 5 -10 3 89.49 15.90 10 -3 5 71.79 15.80 -10 3 5 90.99 13.60 -3 5 10 95.89 25.00 3 -5 10 77.79 12.20 10 -3 -5 73.49 12.40 3 5 10 92.89 25.80 10 3 5 82.09 17.20 -3 -5 10 73.69 22.80 5 -10 -3 115.39 16.20 5 -5 10 779.52 71.99 -10 5 5 752.62 65.99 -5 5 10 781.52 71.59 5 -5 10 781.62 64.79 5 -10 5 768.92 65.39 10 -5 5 809.22 66.29 -5 10 5 803.12 71.99 10 -7 5 753.12 68.89 -7 5 10 761.62 74.19 7 -5 10 793.82 68.39 -5 10 7 702.73 74.69 7 -5 10 757.42 74.99 5 -10 7 749.73 68.19 -10 7 5 764.02 70.39 5 10 7 960.50 77.79 5 -10 -7 881.81 68.39 7 5 10 906.71 75.69 10 -7 -5 935.91 68.19 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180.88 24.80 9 7 10 220.88 34.00 7 -10 -9 170.78 25.40 7 10 9 213.58 35.50 10 9 7 220.28 33.20 9 -7 -10 175.58 22.80 0 -8 10 66.49 10.40 8 -10 0 68.89 15.70 0 8 10 39.50 22.00 -10 0 8 60.99 16.60 10 0 8 72.49 19.90 2 -8 10 1205.28 105.39 -2 8 10 1169.18 112.09 -10 2 8 1196.48 107.79 10 -2 8 1145.59 109.09 8 -10 2 1177.78 106.59 8 -10 -2 1508.15 106.79 10 2 8 1416.66 110.09 2 8 10 1489.05 113.09 -2 -8 10 1345.67 104.69 10 -2 -8 1456.45 104.89 10 -4 8 893.41 75.79 -4 8 10 858.91 78.99 10 -4 8 858.01 72.59 8 -10 4 834.92 72.19 -8 10 4 883.51 76.59 4 -8 10 838.62 70.99 -10 4 8 856.31 73.99 -6 8 10 191.38 30.80 -10 6 8 176.08 24.10 10 -6 8 135.99 19.70 -8 10 6 155.08 26.50 6 -8 10 143.69 19.10 8 -10 6 114.89 19.10 6 8 10 62.39 27.80 -8 8 10 435.26 49.70 -10 8 8 450.15 46.80 -8 10 8 467.05 50.09 10 -8 8 467.15 41.80 8 -10 8 485.15 41.30 8 -8 10 456.05 41.00 8 8 10 389.96 51.99 8 -10 -8 372.46 39.70 8 10 8 380.16 51.99 8 -8 -10 395.26 39.20 10 8 8 365.86 49.20 10 -8 -8 422.96 39.40 -10 1 9 1072.69 91.79 9 -10 1 1042.10 89.69 10 -1 9 1088.29 93.49 1 -9 10 1050.99 88.09 -1 9 10 1022.10 96.29 10 1 9 1120.29 93.89 -10 -1 9 1108.29 91.69 9 -10 -1 1102.59 89.59 -1 -9 10 1095.29 87.59 1 9 10 1229.18 98.29 3 -9 10 877.31 67.59 -10 3 9 892.21 71.69 9 -10 3 857.81 69.29 10 -3 9 857.71 73.29 -3 9 10 829.52 77.59 -9 10 3 850.61 72.89 9 10 3 787.12 75.19 9 -10 -3 741.33 68.39 3 9 10 790.82 77.89 10 3 9 748.13 73.39 10 -3 -9 743.43 66.09 10 -5 9 110.99 18.70 -5 9 10 111.79 26.60 -9 10 5 153.58 25.60 9 -10 5 143.09 19.80 5 -9 10 156.68 18.30 -10 5 9 130.59 22.70 9 -10 -5 86.89 17.90 10 -5 -9 101.29 14.90 10 5 9 54.29 24.50 5 9 10 58.99 25.60 9 10 5 112.29 28.00 -9 10 7 74.09 23.80 10 -7 9 60.09 17.40 9 -10 7 71.49 17.70 -7 9 10 62.59 25.60 7 -9 10 93.29 17.10 -10 7 9 100.99 22.40 7 9 10 175.48 28.80 9 10 7 160.18 27.60 -10 9 9 243.18 36.40 -9 9 10 243.68 36.90 -9 10 9 276.07 38.40 9 -9 10 208.38 32.50 9 -10 9 213.18 32.70 10 -9 9 222.58 33.00 9 -10 -9 329.37 31.10 9 -9 -10 315.97 30.30 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4318.87 312.97 2 1 11 4182.28 316.97 -2 -1 11 4300.67 317.17 1 -11 4 262.77 30.80 -4 1 11 250.57 40.40 4 -1 11 261.17 37.70 11 -4 1 271.27 32.00 11 -4 -1 360.26 31.60 -1 -11 4 353.96 30.40 4 1 11 331.57 41.50 -4 -1 11 381.36 41.60 11 4 1 351.66 30.30 1 -11 -4 358.86 32.50 1 -11 6 123.99 15.20 6 -1 11 136.29 26.90 -1 11 6 93.59 25.90 11 -6 1 135.49 17.80 -6 1 11 78.69 22.30 -11 6 1 107.99 14.60 -1 -11 6 81.59 13.80 1 11 6 49.40 25.50 6 1 11 73.39 23.70 11 -6 -1 75.99 15.50 -6 -1 11 72.79 23.10 11 6 1 79.49 16.60 -1 11 8 36.90 25.10 8 -1 11 39.40 21.70 11 -8 1 47.50 14.90 -8 1 11 54.39 20.60 1 -11 8 46.60 12.10 -8 -1 11 12.90 20.80 11 8 1 25.70 17.80 -1 -11 8 13.50 10.30 8 1 11 11.30 22.80 1 11 8 15.80 24.60 11 -8 -1 25.10 14.00 10 -1 11 1637.24 136.99 -10 1 11 1605.24 135.39 11 -10 1 1598.74 132.29 1 -11 10 1632.04 130.99 -1 11 10 1659.43 139.99 -1 -11 10 1599.44 130.59 1 11 10 1629.14 139.39 11 -10 -1 1601.34 132.29 -10 -1 11 1689.33 135.59 10 1 11 1692.63 137.49 -1 2 11 3600.14 320.27 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9 222.48 34.90 0 -3 11 499.45 52.99 3 -11 0 506.85 44.20 11 0 -3 521.85 42.80 11 0 3 477.95 41.50 0 3 11 473.45 53.39 2 -3 11 72.69 23.80 -2 3 11 83.99 23.90 2 -3 11 101.89 12.00 3 -11 2 115.79 15.20 -2 -3 11 77.69 24.70 11 2 3 69.09 13.00 2 3 11 63.39 24.50 11 -2 -3 68.49 12.70 3 -11 -2 76.69 15.70 -11 4 3 78.79 10.00 11 -4 3 100.69 16.20 4 -3 11 117.69 25.80 3 -11 4 70.19 14.60 -4 3 11 73.59 22.90 3 -11 -4 73.99 14.50 4 3 11 93.19 25.10 11 4 3 65.29 14.90 -4 -3 11 71.19 23.70 11 -4 -3 61.09 13.40 6 -3 11 696.03 75.99 11 -6 3 743.33 69.59 -6 3 11 757.72 74.89 -3 11 6 691.53 75.99 -11 6 3 689.93 68.49 3 -11 6 747.43 68.69 -6 -3 11 908.01 75.19 11 6 3 887.41 71.69 6 3 11 897.01 77.09 3 -11 -6 978.40 69.59 11 -6 -3 949.80 68.99 3 11 6 1003.90 78.09 11 -8 3 564.64 54.99 8 -3 11 557.44 62.29 3 -11 8 545.95 53.69 -8 3 11 585.74 60.29 -11 8 3 583.74 55.89 -3 11 8 539.75 64.09 -8 -3 11 760.72 61.09 8 3 11 806.42 63.69 11 8 3 785.12 59.79 11 -10 3 936.01 77.39 -11 10 3 947.91 79.89 10 -3 11 929.71 82.89 -10 3 11 897.11 81.09 3 -11 10 900.31 75.69 -3 11 10 947.81 86.69 10 -3 -11 918.91 73.79 11 -10 -3 853.41 76.59 11 10 3 888.61 81.99 3 11 10 927.01 86.89 10 3 11 898.11 83.29 11 1 -4 289.57 27.80 -1 4 11 242.48 35.50 11 -1 4 233.08 28.10 1 -4 11 271.37 37.60 1 -4 11 271.07 26.60 4 -11 1 253.47 30.20 1 4 11 350.06 40.50 11 -1 -4 366.56 28.40 4 -11 -1 354.56 30.90 -1 -4 11 331.47 40.70 11 1 4 346.37 29.40 4 -11 3 77.49 14.80 3 -4 11 80.79 12.20 -11 3 4 75.49 10.00 -3 4 11 84.19 23.70 11 -3 4 101.59 17.50 3 -4 11 64.59 25.80 4 -11 -3 72.09 16.00 -3 -4 11 65.89 24.40 11 3 4 76.09 15.30 3 4 11 79.29 25.70 11 -3 -4 82.19 13.30 4 -11 5 636.44 49.50 -11 5 4 614.94 48.20 -5 4 11 661.33 57.89 5 -4 11 607.14 58.69 -4 11 5 615.64 58.59 5 -4 11 622.14 48.60 11 -5 4 623.74 50.09 11 -5 -4 515.05 48.40 11 5 4 465.15 50.89 4 11 5 494.95 59.09 4 -11 -5 478.35 49.10 5 4 11 494.05 57.29 -5 -4 11 484.85 55.79 -7 4 11 484.95 50.09 7 -4 11 490.95 41.20 11 -7 4 490.25 41.70 -11 7 4 472.75 42.40 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338.07 36.60 6 -5 11 329.57 35.10 5 -11 6 345.37 35.70 6 -5 11 351.36 45.90 -11 6 5 318.87 35.90 -6 5 11 274.47 45.00 -6 -5 11 446.66 46.00 6 5 11 399.16 47.50 11 6 5 413.16 40.80 5 11 6 439.16 48.60 11 -6 -5 417.46 34.90 5 -11 -6 426.46 36.10 8 -5 11 2095.19 177.98 -11 8 5 2021.00 179.48 -5 11 8 2067.09 183.08 -8 5 11 2092.69 182.08 5 -11 8 2068.99 177.68 8 -5 11 2020.40 182.58 11 -8 5 2090.79 178.48 5 11 8 2444.66 184.68 11 -8 -5 2328.27 177.88 8 5 11 2603.34 184.28 11 8 5 2535.65 182.08 5 -11 -8 2368.36 178.08 10 -5 11 1778.42 149.99 -11 10 5 1806.62 147.79 -5 11 10 1886.21 152.18 5 -11 10 1799.12 144.29 10 -5 11 1827.02 145.19 -10 5 11 1765.12 148.69 11 -10 5 1791.42 145.09 10 5 11 1742.93 150.38 11 10 5 1773.32 149.39 11 -10 -5 1674.83 144.39 5 11 10 1833.92 152.98 10 -5 -11 1826.22 143.19 11 1 -6 103.89 12.70 6 -11 1 123.79 18.10 1 -6 11 92.89 25.90 1 -6 11 109.19 14.70 -11 1 6 103.79 14.40 11 -1 6 112.49 17.80 -1 6 11 127.49 27.70 11 -1 -6 96.59 13.10 11 1 6 91.29 17.70 -1 -6 11 51.19 24.90 6 -11 -1 103.19 17.40 1 6 11 95.69 25.90 11 3 -6 748.33 62.79 -3 6 11 658.13 72.29 11 -3 6 705.83 65.59 6 -11 3 723.73 65.39 3 -6 11 705.63 73.09 -11 3 6 696.23 64.39 3 -6 11 718.43 63.59 6 -11 -3 934.21 65.69 11 3 6 865.51 67.59 -3 -6 11 939.81 73.89 3 6 11 902.21 74.19 -6 11 5 334.37 44.80 6 -11 5 316.37 35.70 5 -6 11 332.27 34.00 -5 6 11 349.27 45.20 5 -6 11 340.57 46.30 11 -5 6 351.26 37.10 -11 5 6 304.67 35.30 11 -5 -6 392.26 33.90 6 -11 -5 419.26 35.80 11 5 6 404.66 40.50 5 6 11 463.85 47.90 6 11 5 435.66 47.50 6 -11 7 75.39 15.60 7 -6 11 32.40 23.50 11 -7 6 29.20 15.00 -6 11 7 41.50 22.90 -7 6 11 42.40 23.00 -11 7 6 43.60 16.30 7 -6 11 49.80 14.20 6 11 7 -0.70 24.00 7 6 11 5.50 25.00 11 -7 -6 10.60 13.40 11 7 6 0.00 19.70 6 -11 -7 14.60 13.20 11 -9 6 261.37 32.30 -6 11 9 319.87 39.80 -11 9 6 288.47 36.10 9 -6 11 279.87 31.50 -9 6 11 293.87 41.00 6 -11 9 253.47 30.60 11 9 6 283.47 40.00 6 11 9 239.78 37.50 9 -6 -11 278.57 27.30 6 -11 -9 252.57 31.00 9 6 11 274.07 37.90 11 -9 -6 243.38 30.00 11 0 -7 1176.08 93.79 0 -7 11 1129.49 93.59 7 -11 0 1148.19 95.79 0 7 11 1211.38 102.09 -11 0 7 1202.08 95.89 11 0 7 1163.58 97.49 11 2 -7 1080.19 93.29 11 -2 7 1050.99 96.99 2 -7 11 1089.39 93.99 -2 7 11 1121.89 101.89 -11 2 7 1054.59 95.49 7 -11 2 1040.10 95.39 11 2 7 1322.07 98.19 11 -2 -7 1375.26 94.09 7 -11 -2 1376.56 95.89 4 -7 11 463.95 39.90 11 4 -7 463.65 37.20 7 -11 4 452.45 41.80 -7 11 4 491.75 49.80 -11 4 7 460.05 41.70 11 -4 7 515.15 42.50 -4 7 11 448.16 51.89 7 11 4 404.46 51.89 7 -11 -4 389.56 40.70 11 4 7 378.86 45.20 11 -4 -7 411.96 38.80 4 7 11 420.66 51.19 11 -6 7 41.60 16.10 -6 7 11 36.10 22.90 7 -11 6 45.90 15.00 -7 11 6 34.50 21.70 -11 6 7 46.00 16.40 6 -7 11 38.20 13.30 7 11 6 3.40 25.90 6 7 11 16.70 24.10 7 -11 -6 0.60 13.30 11 6 7 18.20 19.80 11 -6 -7 5.60 11.50 -11 8 7 1182.18 106.19 7 -11 8 1091.89 103.39 -7 11 8 1094.09 109.39 -8 7 11 1182.48 109.49 8 -7 11 1159.68 103.39 11 -8 7 1088.19 103.79 7 -11 -8 1431.06 103.69 11 -8 -7 1473.15 103.29 8 7 11 1552.74 112.09 7 11 8 1466.55 112.49 11 -10 7 1600.74 127.49 -10 7 11 1617.34 131.89 7 -11 10 1620.24 126.79 -11 10 7 1630.14 130.79 10 -7 11 1583.84 127.29 -7 11 10 1677.03 134.29 10 -7 -11 1508.85 125.59 11 10 7 1442.26 132.69 10 7 11 1541.65 133.39 11 -10 -7 1459.45 126.29 7 11 10 1458.55 134.89 8 -11 1 46.20 14.90 1 -8 11 58.89 10.30 11 -1 8 69.29 18.60 -1 8 11 18.40 23.20 -11 1 8 61.09 15.30 1 8 11 13.00 24.90 11 -1 -8 18.00 8.70 -1 -8 11 22.20 8.00 8 -11 -1 22.50 15.20 11 1 8 18.20 17.30 -3 8 11 562.64 63.19 -11 3 8 548.65 54.69 11 -3 8 570.94 56.89 3 -8 11 564.34 51.99 8 -11 3 557.14 53.59 3 8 11 807.02 64.09 8 -11 -3 762.92 54.29 8 -11 5 2054.99 178.78 -11 5 8 2019.20 180.08 5 -8 11 2005.30 178.18 -5 8 11 2092.09 183.88 -8 11 5 2023.70 182.38 11 -5 8 2055.89 179.18 8 -11 -5 2323.27 178.78 5 8 11 2537.45 185.68 11 5 8 2466.35 182.68 11 -5 -8 2496.25 177.88 8 11 5 2559.04 184.88 7 -8 11 1155.18 101.59 -11 7 8 1167.58 104.39 11 -7 8 1099.79 102.19 -7 8 11 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189.88 28.30 -1 12 11 132.79 34.80 -11 -1 12 188.28 28.80 -1 -12 11 167.78 20.30 1 12 11 131.99 34.00 11 1 12 176.18 30.70 12 -11 -1 169.48 22.40 0 2 12 126.19 27.80 2 -12 0 127.99 17.90 0 -2 12 96.19 26.20 12 0 -2 119.09 15.80 -2 2 12 1821.02 144.59 2 -12 2 1821.32 138.99 2 -2 12 1837.12 144.99 12 -2 2 1827.92 139.29 -2 -2 12 1641.94 144.19 12 -2 -2 1659.23 138.49 12 2 2 1588.04 137.09 2 2 12 1719.03 144.49 2 -12 -2 1666.73 138.89 -4 2 12 704.23 69.69 2 -12 4 744.53 61.49 12 -4 2 721.53 62.09 4 -2 12 719.03 70.29 -2 -12 4 705.53 60.99 2 -12 -4 739.43 61.89 4 2 12 745.63 70.79 12 4 2 709.63 61.09 -4 -2 12 738.03 69.59 12 -4 -2 758.22 61.39 2 -12 6 15.60 12.20 12 -6 2 17.90 15.00 6 -2 12 14.50 25.00 -6 2 12 40.90 22.20 -12 6 2 15.60 9.30 -2 12 6 -0.20 24.00 12 -6 -2 10.20 13.00 6 2 12 33.90 25.30 12 6 2 19.80 14.70 2 12 6 14.70 25.90 -2 -12 6 5.80 11.30 -6 -2 12 21.80 21.60 2 -12 8 180.78 24.90 8 -2 12 241.58 35.40 12 -8 2 216.28 25.60 -8 2 12 212.28 31.80 -2 12 8 166.08 33.70 -12 8 2 182.58 25.80 2 12 8 173.18 33.50 -2 -12 8 200.58 22.90 8 2 12 248.68 35.00 12 -8 -2 188.68 26.40 -8 -2 12 250.57 33.30 12 8 2 209.68 27.70 -12 10 2 857.71 74.09 -2 12 10 929.11 82.69 10 -2 12 892.41 79.39 12 -10 2 885.41 72.59 -10 2 12 906.51 77.19 2 -12 10 840.52 70.39 -10 -2 12 818.42 77.19 -2 -12 10 829.82 69.39 2 12 10 811.32 83.59 12 10 2 771.02 76.59 10 2 12 819.72 79.79 12 -10 -2 787.72 71.79 1 -3 12 143.59 33.10 -1 3 12 137.59 32.70 -1 -3 12 277.07 35.30 12 -1 -3 226.28 24.50 12 1 3 221.38 21.10 3 -12 -1 232.38 26.00 1 3 12 287.57 36.00 3 -3 12 2037.00 170.48 -3 3 12 2053.59 176.58 12 -3 3 2083.09 171.68 3 -12 3 1947.61 171.28 3 -3 12 2060.09 176.78 3 3 12 2289.47 177.08 12 -3 -3 2349.17 171.18 -3 -3 12 2201.38 176.38 12 3 3 2162.78 171.18 3 -12 -3 2246.28 171.48 3 -12 5 817.92 75.39 5 -3 12 862.11 83.39 -5 3 12 854.71 82.49 -3 12 5 817.82 83.29 12 -5 3 906.11 76.29 12 5 3 1148.19 77.29 3 -12 7 364.16 38.80 12 -7 3 361.86 40.70 7 -3 12 347.97 49.50 -7 3 12 380.66 48.20 -3 12 7 399.56 52.99 -12 7 3 370.46 38.40 12 7 3 509.95 43.70 3 12 7 576.54 55.29 7 3 12 515.05 51.89 -7 -3 12 499.15 48.80 -12 9 3 2765.32 228.08 -9 3 12 2829.52 230.88 -3 12 9 2854.41 232.98 12 -9 3 2704.83 227.08 3 -12 9 2936.91 226.58 9 -3 12 2867.61 231.78 -9 -3 12 2863.41 231.08 12 9 3 2904.81 230.18 9 3 12 2922.51 232.18 12 -9 -3 2677.33 226.68 3 12 9 2986.70 233.98 -3 12 11 153.98 37.20 -11 3 12 126.19 26.00 -12 11 3 123.59 24.30 12 -11 3 117.89 21.30 11 -3 12 104.49 26.80 3 -12 11 160.38 18.90 11 -3 12 124.09 21.60 12 11 3 115.69 28.80 3 12 11 104.79 36.80 12 -11 -3 119.69 20.40 11 3 12 104.49 28.40 0 4 12 866.61 79.39 4 -12 0 863.91 71.59 12 0 -4 859.61 70.39 0 -4 12 893.81 79.09 12 0 4 815.72 69.89 2 -4 12 693.13 58.69 4 -12 2 729.03 61.19 -2 4 12 706.53 69.39 2 -4 12 700.03 69.59 2 4 12 721.03 69.99 4 -12 -2 754.02 61.09 12 2 4 714.13 60.09 -2 -4 12 708.13 69.19 12 -2 -4 701.03 59.49 12 -4 4 71.09 16.30 -4 4 12 86.09 25.50 4 -12 4 63.09 14.80 4 -4 12 57.79 12.70 -12 4 4 68.99 10.10 4 -4 12 69.49 26.50 12 -4 -4 78.59 14.00 4 -12 -4 82.99 16.80 4 4 12 98.79 29.00 -4 -4 12 100.89 27.30 12 4 4 69.19 16.00 12 -6 4 525.65 52.59 6 -4 12 549.05 61.69 -12 6 4 536.15 50.19 6 -4 12 514.25 50.79 -4 12 6 552.04 61.59 4 -12 6 564.84 51.59 -6 4 12 581.04 60.59 4 12 6 652.53 62.89 12 6 4 622.24 54.59 12 -6 -4 634.54 51.29 -6 -4 12 652.63 59.99 4 -12 -6 661.43 52.09 6 4 12 672.53 62.59 4 -12 8 760.42 68.99 8 -4 12 747.73 76.59 -8 4 12 766.22 76.19 12 -8 4 716.63 70.39 -4 12 8 837.22 79.19 -12 8 4 787.92 70.29 8 -4 12 795.42 69.39 8 4 12 1038.10 79.69 12 -8 -4 974.50 69.49 4 -12 10 597.54 49.50 12 -10 4 567.14 51.39 -12 10 4 571.64 53.19 -10 4 12 595.14 58.09 10 -4 12 592.84 59.39 10 -4 12 573.84 51.19 -4 12 10 616.64 63.69 10 4 12 378.76 59.19 4 12 10 379.66 62.79 12 -1 5 1192.18 103.89 12 1 -5 1218.38 102.99 -1 5 12 1197.08 110.79 5 -12 1 1158.58 104.09 1 -5 12 1202.18 110.59 1 -5 12 1212.28 102.49 -1 -5 12 1628.44 111.99 1 5 12 1604.64 112.09 3 -5 12 855.91 81.79 12 -3 5 895.91 74.99 3 -5 12 836.02 72.49 -3 5 12 907.11 82.39 -12 3 5 804.42 71.49 5 -12 3 865.61 74.19 12 3 5 1086.09 75.49 12 -5 5 520.15 48.50 -5 12 5 515.25 57.39 -5 5 12 533.65 57.39 5 -5 12 567.84 46.50 -12 5 5 532.45 45.80 5 -12 5 549.74 47.90 5 -5 12 536.35 57.69 12 5 5 503.25 50.19 5 -12 -5 502.15 47.70 5 5 12 498.85 57.49 5 12 5 551.54 59.69 12 -5 -5 527.45 46.50 -5 -5 12 550.14 57.09 12 -7 5 140.89 21.80 7 -5 12 159.38 20.80 -12 7 5 150.58 21.40 -5 12 7 168.38 32.00 7 -5 12 145.19 31.80 5 -12 7 149.69 21.50 -7 5 12 120.19 29.10 7 5 12 228.68 34.10 12 -7 -5 214.58 23.70 5 12 7 163.68 33.20 5 -12 -7 216.08 25.50 -5 12 9 1793.92 149.88 -12 9 5 1770.62 144.49 12 -9 5 1805.72 143.49 9 -5 12 1782.72 142.99 9 -5 12 1793.82 148.79 -9 5 12 1828.42 148.19 5 -12 9 1795.72 142.49 9 5 12 1759.92 149.19 5 12 9 1703.83 150.28 12 9 5 1709.83 146.79 12 -9 -5 1667.63 142.39 11 -5 12 341.57 36.60 12 -11 5 351.46 36.40 5 -12 11 319.27 33.00 -11 5 12 318.57 42.60 -5 12 11 369.96 46.20 -12 11 5 328.17 40.20 11 5 12 215.98 41.00 12 11 5 222.88 38.50 6 -12 0 9.20 13.70 12 0 -6 20.30 9.70 0 -6 12 20.50 25.30 12 0 6 2.40 13.40 0 -6 12 12.00 7.50 0 6 12 12.10 23.00 2 -6 12 22.10 9.80 2 -6 12 1.90 23.90 12 2 -6 9.50 9.20 -2 6 12 -0.50 23.70 -12 2 6 16.30 8.90 6 -12 2 13.40 13.80 6 -12 -2 14.40 14.30 12 2 6 28.40 14.90 -2 -6 12 19.80 23.80 12 -2 -6 15.50 10.50 2 6 12 22.40 23.80 4 -6 12 509.35 49.50 -4 6 12 512.05 61.19 -12 4 6 531.95 49.70 12 -4 6 551.14 52.79 6 -12 4 528.85 51.39 4 -6 12 554.14 61.99 -4 -6 12 650.23 61.19 12 -4 -6 663.53 49.90 12 4 6 594.74 54.19 4 6 12 706.23 61.89 6 -12 -4 660.03 51.69 6 -12 6 1442.86 129.19 12 -6 6 1452.65 129.79 6 -6 12 1445.96 128.69 -12 6 6 1393.06 129.29 6 -6 12 1445.86 135.59 -6 12 6 1513.15 135.29 -6 6 12 1498.45 135.29 6 -12 -6 1807.82 129.69 6 6 12 1801.52 136.59 12 6 6 1885.91 133.09 6 12 6 1897.61 137.89 12 -6 -6 1695.03 128.79 -8 6 12 1153.48 104.89 8 -6 12 1174.78 98.19 -12 8 6 1110.39 99.59 12 -8 6 1147.49 98.89 6 -12 8 1180.88 97.99 8 -6 12 1229.68 106.09 -6 12 8 1115.19 105.59 8 6 12 1195.08 105.99 6 12 8 1311.37 107.89 12 8 6 1295.37 103.19 12 -8 -6 1229.38 97.79 6 -12 -8 1187.28 98.09 -12 10 6 1335.87 108.79 10 -6 12 1377.36 106.19 12 -10 6 1171.58 105.89 -10 6 12 1388.66 111.99 -6 12 10 1399.36 115.19 6 -12 10 1322.67 105.29 6 12 10 1178.28 114.89 12 -10 -6 1222.38 105.19 10 6 12 1238.18 113.29 12 10 6 1193.48 111.29 12 1 -7 196.28 21.50 7 -12 1 224.88 27.60 1 -7 12 212.88 21.60 12 -1 7 175.58 28.20 -1 7 12 231.48 35.10 1 7 12 338.37 42.10 -3 7 12 405.06 51.69 12 3 -7 358.76 34.80 -12 3 7 351.86 37.40 12 -3 7 354.96 40.60 3 -7 12 368.26 36.30 7 -12 3 348.77 38.70 12 3 7 482.25 43.00 3 7 12 506.35 53.09 12 -3 -7 480.25 36.30 7 -12 -3 503.25 39.90 -5 7 12 120.09 30.00 -7 12 5 159.98 30.40 -12 5 7 165.88 21.60 12 -5 7 144.49 22.40 7 -12 5 153.08 22.20 5 -7 12 148.29 19.60 12 -5 -7 207.58 22.20 12 5 7 245.58 27.70 7 12 5 198.38 32.20 5 7 12 154.68 31.20 7 -12 -5 212.88 26.00 12 -7 7 72.19 18.50 7 -7 12 105.19 17.60 -7 12 7 79.09 26.80 -7 7 12 65.69 27.50 -12 7 7 85.79 19.00 7 -12 7 69.29 17.80 12 7 7 170.38 26.20 7 12 7 190.18 32.40 -9 7 12 359.86 47.00 12 -9 7 341.27 38.10 9 -7 12 337.47 36.00 -7 12 9 323.27 49.20 -12 9 7 369.46 39.80 7 -12 9 356.86 35.80 7 12 9 211.88 43.40 -11 7 12 3.70 23.40 -12 11 7 -0.70 20.20 7 -12 11 5.00 16.50 12 -11 7 18.00 19.50 11 -7 12 9.70 18.20 -7 12 11 -8.40 25.40 7 12 11 10.60 30.50 12 -11 -7 14.40 16.90 12 11 7 3.70 25.20 11 7 12 11.60 28.30 11 -7 -12 12.30 13.00 12 0 8 128.39 21.70 12 0 -8 97.69 14.80 0 8 12 100.19 28.30 0 -8 12 107.39 13.00 8 -12 0 122.19 19.80 2 -8 12 176.88 21.40 8 -12 2 213.78 27.10 -2 8 12 157.78 31.90 12 -2 8 194.18 29.00 12 2 -8 175.38 18.70 -12 2 8 189.28 24.90 12 -2 -8 192.78 20.50 8 -12 -2 190.88 23.50 12 2 8 223.58 31.20 2 8 12 177.78 32.60 12 -4 8 745.33 69.99 4 -8 12 761.82 67.99 8 -12 4 709.53 69.49 -12 4 8 766.62 69.69 -4 8 12 791.52 78.69 -8 12 4 765.52 76.49 8 -12 -4 1018.70 69.89 8 12 4 1058.19 79.79 12 -6 8 1185.98 97.79 -8 12 6 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113.49 28.10 13 -9 -6 149.69 22.00 -6 13 11 257.67 41.70 -11 6 13 247.08 34.30 13 -11 6 173.68 25.00 11 -6 13 186.38 24.60 -13 11 6 208.78 28.30 6 -13 11 205.08 28.10 13 11 6 139.19 31.70 13 -11 -6 133.19 23.10 6 13 11 191.08 42.40 11 6 13 133.99 34.70 0 -7 13 1423.26 116.69 7 -13 0 1466.65 119.29 13 0 -7 1537.55 117.39 13 0 7 1434.76 119.99 0 7 13 1429.36 126.69 0 -7 13 1482.15 126.39 2 -7 13 1150.18 109.09 2 -7 13 1102.89 98.59 13 2 -7 1108.59 98.29 -2 7 13 1175.58 108.79 7 -13 2 1078.19 100.39 13 -2 -7 1364.66 99.09 13 2 7 1339.67 102.39 7 -13 -2 1374.26 101.19 2 7 13 1365.76 109.59 7 -13 4 2083.09 182.58 13 4 -7 2218.48 180.88 4 -7 13 2198.28 181.68 13 -4 7 2174.78 183.28 -4 7 13 2139.29 188.88 4 -7 13 2181.38 189.08 -13 4 7 2081.19 181.78 7 -13 -4 2496.05 182.98 4 7 13 2524.65 189.48 7 13 4 2250.67 189.18 13 4 7 2455.45 184.98 13 -4 -7 2528.95 181.68 -6 7 13 702.63 73.49 -7 13 6 773.82 73.49 7 -13 6 766.02 63.79 13 -6 7 785.92 64.99 6 -7 13 794.12 62.39 -13 6 7 743.93 62.79 7 -13 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57.59 13 3 -8 464.15 40.10 13 -3 8 452.85 46.40 8 -13 3 465.55 45.60 3 -8 13 464.45 42.20 13 -3 -8 485.05 41.80 8 -13 -3 504.95 45.20 3 8 13 547.95 59.89 13 3 8 477.35 48.40 5 -8 13 509.75 42.20 13 5 -8 476.75 38.60 8 -13 5 483.25 44.40 -8 13 5 467.55 54.59 -13 5 8 481.75 43.00 13 -5 8 489.55 45.50 -5 8 13 514.65 57.29 13 5 8 428.56 48.50 8 -13 -5 410.86 44.00 13 -5 -8 379.36 40.90 8 13 5 368.06 56.09 5 8 13 419.56 57.99 13 -7 8 634.74 55.49 -8 13 7 543.75 64.19 7 -8 13 620.84 53.69 -13 7 8 574.14 54.89 -7 8 13 591.14 65.39 8 -13 7 579.54 54.09 8 -13 -7 599.64 54.19 7 8 13 635.44 66.19 8 13 7 628.34 66.69 13 -7 -8 574.04 52.29 13 7 8 585.84 60.29 -9 8 13 397.46 50.09 -8 13 9 410.46 51.99 9 -8 13 373.16 37.50 8 -13 9 398.86 37.90 -13 9 8 365.06 39.90 13 -9 8 386.36 40.10 8 -13 -9 298.37 37.40 13 9 8 327.57 47.60 13 -9 -8 329.27 36.10 9 8 13 251.57 43.60 8 13 9 239.48 43.70 13 -11 8 661.33 55.89 11 -8 13 639.44 54.49 -11 8 13 660.23 64.89 8 -13 11 578.54 53.79 -8 13 11 652.33 67.79 -13 11 8 571.64 58.39 8 13 11 546.45 68.99 11 8 13 512.35 66.89 13 -11 -8 492.05 53.19 13 11 8 465.45 63.99 13 0 -9 17.30 9.20 0 9 13 27.90 28.30 9 -13 0 16.00 15.40 13 0 9 18.60 18.60 0 -9 13 19.90 8.70 2 -9 13 178.88 20.40 13 -2 9 193.08 25.70 9 -13 2 211.18 24.20 -13 2 9 192.48 23.80 -2 9 13 158.88 34.10 9 -13 -2 131.69 22.40 13 2 9 106.39 24.50 2 9 13 108.09 33.00 13 -2 -9 122.79 16.90 13 -4 9 222.38 33.90 9 -13 4 224.18 32.10 -4 9 13 235.18 39.40 4 -9 13 240.28 28.70 -13 4 9 219.98 30.30 -9 13 4 244.88 35.90 9 13 4 357.16 43.40 4 9 13 252.37 39.60 9 -13 -4 324.87 32.50 13 4 9 311.47 38.30 13 -4 -9 301.37 27.30 6 -9 13 190.48 25.70 -9 13 6 159.38 31.50 13 -6 9 175.38 24.40 -13 6 9 194.88 24.60 9 -13 6 169.28 23.00 -6 9 13 209.68 34.60 9 13 6 145.99 34.10 13 -6 -9 155.98 23.00 6 9 13 144.59 34.30 9 -13 -6 145.49 23.70 13 6 9 171.48 30.20 9 -13 8 356.86 38.60 13 -8 9 387.76 40.40 -13 8 9 376.36 41.10 8 -9 13 401.16 38.00 -8 9 13 379.16 52.49 -9 13 8 386.96 50.79 13 -8 -9 316.07 35.90 9 13 8 353.36 48.60 13 8 9 329.17 47.50 9 -13 -8 296.27 37.70 8 9 13 403.46 51.49 -9 13 10 525.65 67.99 9 -13 10 608.14 57.59 -13 10 9 592.54 61.29 13 -10 9 641.04 59.29 -10 9 13 603.34 68.39 10 -9 13 609.54 57.99 13 10 9 707.73 68.59 9 -13 -10 680.43 57.49 9 13 10 693.13 72.99 10 9 13 681.13 72.39 13 -10 -9 626.04 56.59 13 -12 9 354.06 44.20 -13 12 9 387.76 49.10 9 -13 12 430.56 43.30 -12 9 13 429.56 54.29 -9 13 12 441.36 59.09 12 -9 13 416.06 44.80 13 -12 -9 421.86 42.70 13 12 9 397.36 57.49 12 9 13 424.66 58.99 9 13 12 341.17 51.69 10 -13 1 259.67 32.90 -1 10 13 233.28 39.90 -13 1 10 256.47 31.60 1 -10 13 233.88 26.40 13 -1 10 291.07 35.00 -1 -10 13 263.07 25.00 13 1 10 300.57 38.50 13 -1 -10 267.87 25.10 10 -13 -1 304.27 33.10 1 10 13 326.87 45.20 -13 3 10 1028.60 88.69 13 -3 10 1065.89 88.89 3 -10 13 1043.80 86.09 -10 13 3 1049.00 94.19 10 -13 3 1044.00 88.19 13 -3 10 1040.60 91.49 -3 10 13 1090.49 98.99 10 -13 -3 1104.09 88.29 13 -3 -10 1033.60 85.19 13 3 10 1036.80 92.69 3 10 13 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51.49 37.40 13 13 10 23.00 34.90 -13 12 13 1043.60 98.39 -13 13 12 1046.00 97.89 -12 13 13 1132.79 100.89 12 -13 13 1084.49 90.29 13 -12 13 1011.40 90.29 13 -13 12 1058.89 90.79 12 13 13 935.11 104.69 13 12 13 989.90 104.09 13 13 12 973.00 103.79 0 -14 0 1062.79 88.59 0 0 14 1089.69 97.49 0 -14 2 213.88 27.30 2 0 14 229.78 35.60 14 -2 0 211.98 27.90 -2 0 14 233.88 35.00 0 -14 4 142.39 20.20 4 0 14 177.88 35.40 -4 0 14 170.58 33.50 14 -4 0 194.18 22.70 0 14 6 836.62 80.89 -6 0 14 830.72 77.09 0 -14 6 780.32 67.09 14 6 0 771.52 66.99 14 -6 0 769.42 68.39 6 0 14 834.82 78.79 0 -14 8 102.59 17.40 14 -8 0 105.79 20.10 14 8 0 96.09 19.90 8 0 14 100.69 31.40 -8 0 14 93.19 27.90 -14 8 0 107.39 15.20 0 14 8 81.89 33.50 -14 10 0 67.29 17.20 14 -10 0 62.19 18.70 14 10 0 89.69 22.80 -10 0 14 101.89 29.00 0 -14 10 76.59 15.70 10 0 14 76.59 29.80 0 14 10 69.59 32.40 12 0 14 80.49 29.50 -12 0 14 130.59 28.90 0 14 12 140.19 41.10 14 12 0 112.99 29.30 0 -14 12 128.49 17.70 14 -12 0 150.18 23.80 1 -1 14 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405.26 54.19 9 1 14 382.46 54.99 -9 -1 14 331.87 51.19 14 -9 -1 359.46 42.80 14 9 1 359.36 45.30 -1 -14 9 336.67 39.20 -14 11 1 1092.19 92.39 -11 1 14 1074.09 97.79 1 -14 11 1090.89 89.89 -1 14 11 1163.78 105.39 14 -11 1 1112.09 92.39 11 -1 14 1056.89 99.79 -1 -14 11 1104.89 89.49 14 11 1 1090.29 96.59 11 1 14 1056.59 99.99 -11 -1 14 1025.90 97.19 14 -11 -1 1103.09 92.09 1 14 11 1139.29 105.09 -13 1 14 626.74 60.39 -14 13 1 631.44 57.79 1 -14 13 643.04 51.49 13 -1 14 627.44 65.69 14 -13 1 658.53 55.29 -1 14 13 681.23 72.29 14 -13 -1 494.35 55.19 -1 -14 13 488.25 50.19 14 13 1 529.25 62.89 1 14 13 517.65 72.09 13 1 14 568.44 65.39 0 -2 14 245.48 36.90 0 -2 14 198.48 20.10 0 2 14 243.08 37.60 14 0 -2 194.48 25.60 2 -14 0 213.58 27.70 -2 2 14 2647.24 195.38 14 -2 2 2563.64 189.18 2 -2 14 2666.63 195.88 2 -14 2 2586.64 188.88 2 2 14 2157.18 194.18 2 -14 -2 2113.49 188.58 14 -2 -2 2072.39 188.28 -2 -2 14 2095.29 194.18 2 -14 4 1402.96 124.99 -4 2 14 1457.55 132.29 14 -4 2 1429.76 125.59 14 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14 10.70 28.60 -1 -3 14 19.20 27.40 3 -14 -1 -3.10 14.80 14 -1 -3 15.60 13.00 -3 3 14 202.28 36.70 14 -3 3 202.58 31.40 3 -14 3 208.38 30.40 3 -3 14 194.08 25.70 3 -3 14 258.27 40.80 14 3 3 287.77 24.30 14 -3 -3 281.87 28.70 3 -14 -3 293.67 31.20 3 3 14 294.27 39.80 -3 -3 14 320.37 39.90 -5 3 14 847.42 85.69 5 -3 14 817.82 87.19 14 -5 3 807.32 77.89 3 -14 5 815.02 77.09 -3 14 5 872.71 88.59 5 -3 14 810.52 76.09 3 -14 -5 1007.70 78.29 3 14 5 1025.10 88.89 5 3 14 1029.40 87.59 14 5 3 968.40 76.99 14 -5 -3 1029.60 77.39 -5 -3 14 1091.39 86.99 -3 14 7 102.99 31.10 3 -14 7 123.59 17.90 -7 3 14 135.89 32.20 7 -3 14 91.79 17.50 -14 7 3 93.29 13.20 14 -7 3 135.39 22.10 7 -3 14 128.29 33.70 14 7 3 104.09 20.40 3 14 7 91.59 31.90 7 3 14 84.19 29.60 -7 -3 14 74.79 27.00 14 -7 -3 74.69 17.70 -9 3 14 62.79 26.10 3 -14 9 103.89 18.00 -3 14 9 60.89 34.30 9 -3 14 87.19 18.70 9 -3 14 79.19 31.90 -14 9 3 85.99 15.80 14 -9 3 114.49 21.40 14 9 3 104.29 23.80 3 14 9 89.19 32.40 -9 -3 14 96.49 29.00 14 -9 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197.08 42.30 12 4 14 232.18 39.70 14 12 4 210.78 33.20 14 -12 -4 201.28 24.50 14 1 -5 1440.06 119.69 5 -14 1 1388.46 120.89 -1 5 14 1499.45 129.09 1 -5 14 1416.16 118.79 1 -5 14 1421.76 128.09 5 -14 -1 1590.24 121.49 1 5 14 1600.94 129.09 -1 -5 14 1498.55 128.09 14 1 5 1461.75 119.59 14 -1 -5 1577.44 119.99 3 -5 14 798.42 74.69 14 -3 5 795.82 77.69 -3 5 14 843.72 86.89 5 -14 3 833.22 76.99 3 -5 14 813.72 85.49 14 3 -5 803.12 74.99 5 -14 -3 1055.49 77.69 14 -3 -5 1011.30 75.89 -3 -5 14 1034.90 86.19 14 3 5 1068.39 76.89 3 5 14 1058.89 88.29 5 -5 14 383.76 35.00 5 -5 14 384.86 51.29 5 -14 5 393.56 37.60 -5 14 5 407.26 53.79 -5 5 14 392.86 51.89 14 -5 5 397.16 38.90 5 14 5 381.66 53.49 14 -5 -5 308.27 35.30 14 5 5 318.97 37.70 -5 -5 14 326.17 44.00 5 -14 -5 329.17 37.90 5 5 14 364.16 52.69 5 -14 7 144.19 21.90 7 -5 14 103.29 19.00 7 -5 14 113.59 32.00 -14 7 5 125.29 17.00 -7 5 14 156.28 34.10 14 -7 5 134.09 23.60 -5 14 7 116.19 32.80 -7 -5 14 176.08 32.90 7 5 14 171.58 35.30 5 14 7 224.78 40.10 14 -7 -5 188.18 21.00 5 -14 -7 151.78 22.10 14 7 5 193.98 26.10 -14 9 5 461.15 44.20 9 -5 14 453.55 58.39 5 -14 9 474.65 45.20 -5 14 9 513.35 61.89 9 -5 14 486.35 45.70 -9 5 14 506.45 56.79 14 -9 5 491.75 47.70 9 5 14 473.05 58.89 14 -9 -5 430.66 45.10 5 14 9 476.25 62.69 14 9 5 442.06 51.49 11 -5 14 433.56 55.39 14 -11 5 476.95 44.70 -5 14 11 443.46 60.79 5 -14 11 481.85 41.50 -14 11 5 433.36 43.70 11 -5 14 434.36 43.50 -11 5 14 506.25 53.49 5 14 11 390.66 55.29 14 -11 -5 322.47 42.20 11 5 14 277.27 48.00 14 11 5 331.67 50.79 5 -14 13 64.09 18.10 -13 5 14 45.30 25.10 -5 14 13 96.09 35.20 13 -5 14 43.80 20.30 -14 13 5 73.59 22.70 14 -13 5 63.89 21.60 13 5 14 56.59 31.00 14 13 5 45.30 30.50 14 -13 -5 57.89 19.10 5 14 13 39.20 38.50 0 -6 14 724.13 62.29 14 0 6 749.62 64.99 0 -6 14 817.12 78.09 0 6 14 818.92 78.19 6 -14 0 754.22 66.29 14 0 -6 816.72 64.19 -2 6 14 439.96 57.79 6 -14 2 468.45 44.80 2 -6 14 468.55 56.59 2 -6 14 427.96 40.10 14 2 -6 500.45 40.90 -4 6 14 180.28 35.40 4 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14 78.79 28.50 12 -6 14 79.49 20.40 6 -14 12 102.09 20.10 14 12 6 75.89 30.50 6 14 12 97.89 38.90 14 -12 -6 62.19 20.90 12 6 14 54.69 33.90 1 -7 14 107.19 32.30 -1 7 14 147.89 35.50 14 1 -7 149.29 18.60 7 -14 1 130.69 20.10 14 -1 7 152.18 20.00 1 -7 14 146.59 16.20 14 -1 -7 105.29 16.00 1 7 14 72.59 31.60 7 -14 -1 86.59 19.70 14 1 7 105.19 19.70 7 -14 3 93.19 18.80 14 3 -7 130.09 14.80 3 -7 14 68.39 30.20 -3 7 14 113.99 31.70 3 -7 14 105.89 15.40 14 -3 7 115.59 20.50 14 3 7 114.49 21.00 14 -3 -7 99.99 15.90 7 -14 -3 89.39 20.10 3 7 14 90.09 31.70 -14 5 7 114.49 18.10 7 -14 5 97.09 20.50 14 5 -7 119.89 18.30 -5 7 14 102.09 33.00 -7 14 5 201.08 36.00 14 -5 7 112.39 22.30 5 -7 14 118.59 32.60 5 -7 14 128.69 19.00 7 14 5 179.88 33.60 14 5 7 195.08 25.30 5 7 14 212.38 38.30 14 -5 -7 169.88 22.00 7 -14 -5 198.48 23.60 -7 7 14 141.99 35.10 7 -14 7 192.28 23.20 -7 14 7 125.39 30.80 7 -7 14 127.59 18.80 -14 7 7 149.69 18.90 14 -7 7 154.98 23.40 14 7 7 99.59 24.90 7 -14 -7 97.89 22.10 7 7 14 94.39 34.50 14 -7 -7 93.59 18.40 7 14 7 112.39 34.80 -7 14 9 11.70 30.10 -14 9 7 9.10 15.50 14 -9 7 -14.70 18.70 -9 7 14 8.60 29.30 9 -7 14 7.20 16.60 7 -14 9 4.30 16.10 14 9 7 0.00 24.30 14 -9 -7 3.50 14.80 9 7 14 -3.80 30.50 7 14 9 12.20 29.80 -14 11 7 75.09 20.60 -11 7 14 45.20 28.10 -7 14 11 81.79 33.20 7 -14 11 83.79 19.30 11 -7 14 74.19 19.90 14 -11 7 67.99 22.20 7 14 11 37.20 37.80 11 7 14 15.20 31.50 14 -11 -7 41.70 18.80 14 11 7 27.00 26.90 -14 13 7 -6.70 20.80 14 -13 7 4.90 21.10 7 -14 13 23.50 17.40 -7 14 13 25.80 32.70 13 -7 14 2.30 19.60 -13 7 14 14.10 25.30 7 14 13 12.90 38.20 14 13 7 33.60 30.00 14 -13 -7 18.60 18.50 13 7 14 15.40 31.00 0 8 14 53.49 29.70 0 -8 14 101.09 12.10 14 0 -8 99.59 13.90 14 0 8 83.19 19.70 8 -14 0 98.49 19.60 2 -8 14 154.08 21.30 8 -14 2 208.98 25.60 14 2 -8 167.78 20.50 -2 8 14 139.69 34.40 2 8 14 211.08 36.10 8 -14 -2 243.48 28.40 14 2 8 242.38 30.90 14 4 -8 306.77 25.70 8 -14 4 302.87 32.90 4 -8 14 303.27 29.10 -14 4 8 289.47 27.80 -8 14 4 344.37 47.40 -4 8 14 265.37 40.30 14 -4 8 331.57 34.70 14 4 8 242.38 32.60 8 -14 -4 209.88 32.90 4 8 14 200.98 40.80 8 14 4 169.98 38.00 14 -4 -8 219.38 28.40 6 -8 14 188.48 26.80 -8 14 6 165.68 34.50 8 -14 6 179.58 24.90 -6 8 14 193.38 35.90 14 -6 8 166.68 25.90 14 6 -8 174.88 20.30 -14 6 8 180.08 23.20 14 6 8 255.47 31.30 14 -6 -8 232.18 25.60 8 14 6 252.77 41.70 8 -14 -6 229.88 26.30 6 8 14 201.78 39.30 8 -8 14 229.18 30.70 -14 8 8 233.88 30.10 -8 8 14 292.47 40.70 -8 14 8 215.68 36.90 14 -8 8 229.58 32.60 8 -14 8 278.37 32.00 14 8 8 203.38 33.30 8 14 8 227.68 42.30 8 8 14 158.88 37.00 8 -14 -8 205.38 27.90 14 -8 -8 197.18 28.70 10 -8 14 119.09 22.00 -14 10 8 138.29 24.80 -8 14 10 162.68 36.80 14 -10 8 193.48 26.50 -10 8 14 148.49 34.60 8 -14 10 168.08 25.00 8 14 10 132.09 36.20 10 8 14 140.09 38.50 14 -10 -8 181.28 23.70 14 10 8 161.78 32.80 -14 12 8 15.70 20.80 -12 8 14 11.60 27.60 8 -14 12 30.30 19.30 12 -8 14 13.30 18.80 14 -12 8 20.40 19.90 -8 14 12 -2.10 29.50 14 -12 -8 51.99 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40.20 28.50 9 -9 14 38.40 17.70 9 -14 9 32.00 17.90 14 -9 9 14.30 19.90 14 9 9 90.99 28.10 14 -9 -9 76.29 17.30 9 14 9 112.19 37.90 9 9 14 96.59 35.00 9 -14 -9 100.99 19.70 -11 9 14 311.67 43.00 14 -11 9 275.27 38.70 9 -14 11 292.27 35.20 -9 14 11 265.37 42.50 -14 11 9 257.67 38.50 11 -9 14 303.17 36.90 11 9 14 297.07 48.00 9 14 11 290.57 48.80 14 -11 -9 233.58 33.70 14 11 9 233.68 40.90 14 -13 9 441.96 49.40 -9 14 13 451.05 64.19 -13 9 14 447.26 56.79 13 -9 14 419.46 48.80 -14 13 9 442.66 52.49 9 -14 13 413.36 46.10 13 9 14 498.65 64.49 14 13 9 484.25 62.89 14 -13 -9 428.56 46.80 9 14 13 529.65 70.19 14 0 -10 85.59 11.60 14 0 10 47.00 21.90 10 -14 0 74.29 19.80 0 -10 14 82.79 12.10 0 10 14 63.49 32.80 10 -14 2 52.89 19.60 -2 10 14 28.60 32.20 14 -2 10 35.70 20.80 -14 2 10 35.80 15.30 2 -10 14 25.30 11.80 14 2 10 95.39 23.10 2 10 14 71.79 33.40 -4 10 14 568.24 65.39 14 -4 10 593.64 51.39 10 -14 4 564.74 49.60 -14 4 10 563.14 48.50 4 -10 14 558.64 46.50 -10 14 4 565.94 59.39 14 4 10 412.86 54.19 10 14 4 460.35 61.29 10 -14 -4 462.95 49.40 14 -4 -10 446.46 45.00 4 10 14 483.15 65.19 -14 6 10 558.44 49.99 -6 10 14 514.85 63.49 14 -6 10 542.95 51.89 10 -14 6 513.25 50.29 -10 14 6 517.55 60.19 6 -10 14 541.15 47.90 10 -14 -6 494.45 49.40 14 -6 -10 501.25 46.30 10 14 6 522.65 62.99 14 6 10 508.55 56.79 6 10 14 418.56 64.19 10 -14 8 158.58 24.60 -8 10 14 165.28 37.10 14 -8 10 181.78 26.60 8 -10 14 196.78 24.90 -14 8 10 156.58 26.00 -10 14 8 133.29 32.70 10 14 8 162.08 38.80 8 10 14 179.38 40.50 14 -8 -10 186.38 22.40 10 -14 -8 147.69 24.30 14 8 10 178.48 34.40 -10 10 14 104.09 34.10 -10 14 10 45.10 29.60 10 -10 14 62.89 20.40 10 -14 10 40.50 19.00 -14 10 10 55.49 22.40 14 -10 10 56.69 21.60 10 14 10 45.60 37.50 14 10 10 52.69 31.10 10 -14 -10 44.60 19.00 14 -10 -10 40.30 18.20 10 10 14 21.20 32.40 -12 10 14 471.75 61.39 14 -12 10 470.45 49.70 10 -14 12 431.76 48.10 -14 12 10 470.05 53.09 12 -10 14 437.96 49.30 -10 14 12 444.16 62.79 14 -12 -10 482.85 47.40 14 12 10 479.85 63.89 12 10 14 524.85 67.89 10 14 12 495.95 69.19 -1 11 14 1116.39 103.49 14 -1 11 1102.19 95.19 1 -11 14 1099.29 88.69 11 -14 1 1128.79 91.79 -1 -11 14 1040.70 87.79 11 -14 -1 1055.89 91.79 14 1 11 1023.50 95.79 1 11 14 1094.59 104.19 14 -1 -11 1140.99 88.79 11 -14 3 61.29 20.10 3 -11 14 82.69 15.50 14 -3 11 88.09 22.90 -3 11 14 68.89 33.00 -11 14 3 47.90 26.60 -14 3 11 75.59 19.30 11 14 3 116.69 33.70 14 3 11 103.09 25.90 14 -3 -11 105.89 13.90 11 -14 -3 97.89 20.40 3 11 14 95.19 33.80 -14 5 11 449.16 42.40 11 -14 5 477.35 42.90 -11 14 5 470.25 51.79 14 -5 11 485.45 44.50 5 -11 14 483.55 39.20 -5 11 14 478.85 60.59 14 -5 -11 326.27 36.70 14 5 11 312.57 49.20 5 11 14 281.57 49.40 11 14 5 293.87 48.30 11 -14 -5 330.17 41.60 -14 7 11 59.89 20.70 -11 14 7 66.69 27.70 14 -7 11 38.30 19.70 11 -14 7 60.29 19.60 7 -11 14 79.39 18.00 -7 11 14 66.89 33.60 11 -14 -7 26.40 18.90 14 7 11 47.90 28.50 7 11 14 28.10 32.70 11 14 7 25.70 32.70 14 -7 -11 32.90 14.90 9 -11 14 241.98 33.70 11 -14 9 282.87 35.60 -11 14 9 355.06 43.40 14 -9 11 271.47 38.20 -14 9 11 262.67 38.50 -9 11 14 267.87 42.20 14 -9 -11 258.27 31.90 9 11 14 222.78 42.90 14 9 11 240.98 39.90 11 -14 -9 235.38 34.20 11 14 9 208.48 43.70 -11 14 11 1650.53 133.59 -14 11 11 1572.54 128.69 -11 11 14 1653.43 134.19 14 -11 11 1573.04 125.49 11 -11 14 1395.06 123.99 11 -14 11 1622.04 124.69 11 14 11 1343.47 136.09 11 11 14 1414.96 136.19 14 11 11 1359.76 133.29 14 -11 -11 1399.06 123.09 -14 13 11 757.82 81.49 -13 11 14 811.22 85.59 14 -13 11 834.52 77.09 11 -14 13 792.72 75.49 -11 14 13 718.63 86.09 13 -11 14 764.92 76.49 11 14 13 990.40 95.09 14 13 11 1019.50 92.39 14 -13 -11 956.50 75.59 13 11 14 933.91 92.39 14 0 12 145.79 30.10 0 12 14 147.09 38.50 0 -12 14 132.29 16.50 12 -14 0 131.89 23.20 14 -2 12 529.85 55.79 -2 12 14 506.75 67.69 -14 2 12 503.55 50.29 -12 14 2 532.35 56.99 12 -14 2 562.04 50.79 2 -12 14 555.44 45.60 14 2 12 491.25 56.79 12 -14 -2 460.55 49.99 12 14 2 408.76 60.59 2 12 14 481.75 67.49 -12 14 4 126.89 29.70 -14 4 12 116.19 24.20 -4 12 14 120.89 37.10 12 -14 4 149.29 25.70 4 -12 14 146.99 20.70 14 -4 12 113.89 25.00 12 -14 -4 182.98 24.30 14 -4 -12 179.18 20.40 4 12 14 242.38 45.10 14 4 12 176.68 32.40 12 14 4 184.48 34.30 12 -14 6 64.79 20.30 6 -12 14 119.79 19.10 -14 6 12 106.79 23.20 14 -6 12 89.39 21.70 -12 14 6 81.39 28.70 -6 12 14 100.69 33.70 14 6 12 57.59 29.90 14 -6 -12 68.09 15.30 6 12 14 42.20 34.40 12 14 6 23.70 29.30 12 -14 -6 52.39 21.30 14 -8 12 10.20 21.10 -14 8 12 -10.70 20.00 -12 14 8 19.90 27.60 12 -14 8 13.50 20.70 8 -12 14 5.00 17.30 -8 12 14 -1.20 33.30 12 14 8 20.00 31.30 12 -14 -8 19.30 18.50 8 12 14 40.50 39.30 14 8 12 34.60 30.80 14 -8 -12 20.80 15.00 -10 12 14 509.35 63.19 14 -10 12 482.15 50.69 10 -12 14 465.35 48.00 12 -14 10 477.55 49.00 -12 14 10 454.25 59.49 -14 10 12 448.86 53.49 14 10 12 463.25 63.99 10 12 14 451.05 67.59 12 14 10 356.66 55.59 12 -14 -10 460.35 47.90 14 -10 -12 483.65 45.50 -12 14 12 216.38 41.00 -12 12 14 255.47 43.20 12 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11.50 38.80 14 7 13 15.40 29.30 -14 9 13 431.46 52.99 14 -9 13 438.16 49.80 -9 13 14 436.36 63.49 -13 14 9 438.16 56.59 13 -14 9 428.66 48.30 9 -13 14 433.76 46.70 13 14 9 447.36 65.19 13 -14 -9 459.95 47.10 14 9 13 537.85 64.29 9 13 14 533.55 70.79 14 -11 13 848.42 79.29 11 -13 14 829.92 78.09 13 -14 11 814.82 78.69 -13 14 11 812.12 86.49 -11 13 14 852.61 91.29 -14 11 13 831.12 84.79 13 -14 -11 977.90 78.19 13 14 11 998.80 94.79 11 13 14 923.81 95.79 14 11 13 979.50 93.99 -14 13 13 422.56 59.69 -13 13 14 440.46 65.29 -13 14 13 487.65 65.49 13 -14 13 452.15 53.19 13 -13 14 476.95 52.99 14 -13 13 488.45 53.89 13 14 13 626.64 74.39 13 13 14 609.74 75.19 14 13 13 618.44 74.29 0 -14 14 8.40 12.00 0 14 14 1.60 33.90 14 -14 0 11.50 19.60 14 0 14 7.60 26.30 14 14 0 13.90 26.90 -14 2 14 1719.53 136.89 -14 14 2 1684.83 137.09 -2 14 14 1706.63 147.59 2 -14 14 1756.12 131.99 14 -2 14 1652.63 139.89 14 -2 14 1885.11 135.49 14 -14 2 1752.12 134.49 2 14 14 1355.16 145.49 14 2 14 1319.27 139.59 14 14 2 1301.17 139.49 -14 4 14 943.21 91.89 -14 14 4 984.30 91.79 -4 14 14 1010.10 103.29 4 -14 14 986.80 86.79 14 -4 14 1011.30 90.19 14 -14 4 998.00 89.49 14 -14 -4 1133.19 89.49 4 14 14 1124.49 106.09 14 4 14 1094.99 98.19 14 14 4 1163.58 98.29 -14 6 14 112.79 27.60 -14 14 6 104.19 26.90 -6 14 14 131.19 42.50 6 -14 14 81.89 20.40 14 -6 14 96.79 23.40 14 -14 6 160.48 26.80 14 -14 -6 99.89 22.90 6 14 14 83.49 38.80 14 6 14 157.88 36.70 14 14 6 138.89 35.20 -14 8 14 352.36 46.40 -14 14 8 330.57 45.70 -8 14 14 269.67 46.00 8 -14 14 352.86 37.30 14 -8 14 303.67 40.90 14 -14 8 327.07 40.40 14 -14 -8 277.97 38.60 8 14 14 295.67 55.29 14 8 14 309.17 49.40 14 14 8 244.48 45.60 -14 10 14 217.28 37.60 -14 14 10 220.28 36.40 -10 14 14 289.87 47.90 10 -14 14 244.28 30.60 14 -10 14 301.87 34.30 14 -14 10 186.58 29.90 14 -14 -10 167.68 29.50 10 14 14 239.68 52.09 14 10 14 187.28 45.70 14 14 10 211.08 45.50 -14 12 14 81.19 32.10 -14 14 12 96.19 32.20 -12 14 14 131.69 40.80 12 -14 14 96.99 24.20 14 -12 14 114.99 26.10 14 -14 12 65.99 24.00 12 14 14 56.99 43.90 14 12 14 42.60 38.10 14 14 12 62.59 41.10 -14 14 14 1282.07 126.39 14 -14 14 1399.56 119.09 14 14 14 1552.94 135.29 1 0 15 3497.55 273.97 15 -1 0 3212.08 267.17 0 -15 1 3226.88 267.17 -1 0 15 3534.15 274.07 3 0 15 3826.02 309.27 0 -15 3 3698.63 302.87 15 -3 0 3769.22 303.17 -3 0 15 3970.60 309.27 -5 0 15 1702.03 145.29 0 -15 5 1693.53 137.29 15 -5 0 1701.93 137.89 5 0 15 1691.93 145.99 0 -15 7 187.98 23.50 0 15 7 222.98 43.30 -7 0 15 229.38 37.00 7 0 15 192.38 36.20 15 7 0 193.98 26.30 15 -7 0 219.38 26.70 15 9 0 453.55 45.30 0 15 9 463.85 62.69 -15 9 0 422.56 38.80 -9 0 15 410.06 55.09 15 -9 0 432.56 44.30 9 0 15 449.95 56.99 0 -15 9 409.26 40.80 -11 0 15 74.49 27.70 15 -11 0 70.89 21.10 15 11 0 56.09 23.10 -15 11 0 64.39 17.10 0 15 11 112.39 39.40 0 -15 11 52.89 15.30 11 0 15 78.89 32.30 -13 0 15 1478.15 127.79 0 15 13 1489.95 135.69 13 0 15 1456.65 130.09 -15 13 0 1396.36 123.29 15 13 0 1471.45 127.39 15 -13 0 1568.44 122.79 0 -15 13 1466.15 119.69 15 0 -1 3166.58 267.97 0 1 15 3538.25 274.97 1 -15 0 3362.16 268.37 0 -1 15 3442.86 274.37 -2 1 15 968.60 85.29 15 -2 1 958.30 74.99 2 -1 15 1006.60 86.19 1 -15 2 914.91 74.69 15 -2 -1 771.42 74.09 -2 -1 15 886.51 85.09 1 -15 -2 789.32 74.69 2 1 15 797.62 84.29 15 -4 1 1114.49 95.09 4 -1 15 1197.18 104.19 1 -15 4 1205.38 94.59 -4 1 15 1222.58 103.99 4 1 15 1148.49 104.79 -1 -15 4 1110.59 94.19 15 -4 -1 1039.90 94.39 -4 -1 15 1139.79 103.49 6 -1 15 0.50 30.10 15 -6 1 8.90 18.00 -6 1 15 8.90 26.80 1 -15 6 3.00 15.70 15 6 -1 13.50 10.30 -1 15 6 10.80 30.00 -1 -15 6 21.00 14.50 15 -6 -1 16.70 16.10 15 6 1 12.40 12.10 1 15 6 17.10 29.70 6 1 15 14.30 27.90 -6 -1 15 0.80 28.20 15 -8 1 5.80 17.40 1 -15 8 19.60 14.90 -8 1 15 22.20 28.70 15 8 -1 7.30 15.90 8 -1 15 2.00 27.30 -1 15 8 37.30 32.40 1 15 8 57.59 32.30 15 -8 -1 78.69 19.00 15 8 1 74.59 18.40 -15 8 -1 57.19 10.30 -1 -15 8 64.39 15.20 -8 -1 15 59.79 28.30 8 1 15 56.69 32.20 -10 1 15 338.57 44.30 15 10 -1 250.77 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25.20 -3 15 6 175.18 38.00 6 -3 15 160.08 21.00 6 -3 15 126.89 34.10 6 3 15 164.68 36.70 15 -6 -3 164.08 22.50 3 15 6 140.49 36.00 15 6 3 162.18 21.40 -6 -3 15 119.99 32.00 3 -15 8 172.18 22.00 -8 3 15 171.08 33.30 8 -3 15 251.47 40.20 8 -3 15 201.28 26.60 15 -8 3 193.98 25.20 -3 15 8 167.28 37.90 15 8 3 144.79 25.30 8 3 15 127.29 34.20 15 -8 -3 170.58 24.10 3 15 8 128.39 36.20 -8 -3 15 117.89 32.00 -3 15 10 708.93 77.69 -10 3 15 752.82 71.49 10 -3 15 726.43 61.49 15 -10 3 708.63 62.59 10 -3 15 748.53 72.89 -15 10 3 658.53 58.69 3 -15 10 716.73 59.99 15 -10 -3 605.04 60.79 10 3 15 667.13 73.59 3 15 10 612.34 77.09 15 10 3 638.74 65.39 -10 -3 15 602.64 70.79 12 -3 15 1093.49 85.09 3 -15 12 1027.10 82.99 -15 12 3 1019.10 84.49 -3 15 12 1057.59 99.49 12 -3 15 963.20 93.09 15 -12 3 1042.80 85.39 -12 3 15 1060.89 91.69 15 12 3 884.61 90.19 12 3 15 853.41 93.89 15 -12 -3 868.41 83.99 3 15 12 846.72 98.99 3 -15 14 16.00 16.10 14 -3 15 36.10 22.60 -15 14 3 44.90 20.50 14 -3 15 28.90 28.70 -3 15 14 26.90 35.60 -14 3 15 23.10 23.50 15 -14 3 14.40 21.50 15 -14 -3 32.30 21.30 3 15 14 34.00 36.20 15 14 3 19.70 28.70 14 3 15 14.10 31.10 1 -4 15 1207.38 105.89 4 -15 1 1203.78 95.79 -1 4 15 1298.67 105.49 15 1 -4 1100.49 94.19 1 -4 15 1127.59 92.49 1 4 15 1188.18 105.39 15 -1 -4 1090.29 94.29 4 -15 -1 1104.09 95.49 -1 -4 15 1139.09 105.29 15 3 -4 1011.50 78.19 15 -3 4 987.40 80.59 3 -4 15 1050.19 91.39 4 -15 3 1056.69 80.09 3 -4 15 982.40 77.19 -3 4 15 1032.10 90.89 -3 -4 15 917.81 89.29 3 4 15 860.41 90.49 15 -3 -4 868.81 78.59 15 3 4 837.32 76.39 4 -15 -3 818.02 79.29 15 5 -4 26.60 9.60 4 -15 5 25.50 15.70 5 -4 15 3.40 28.60 15 -5 4 30.20 18.90 -4 15 5 35.30 33.50 5 -4 15 35.10 13.70 -5 4 15 29.40 30.50 -5 -4 15 16.50 26.70 15 5 4 4.20 13.50 5 4 15 9.10 31.50 4 15 5 4.30 29.80 15 -5 -4 7.40 15.80 4 -15 -5 10.50 17.30 -7 4 15 265.77 41.00 4 -15 7 249.38 31.90 7 -4 15 199.48 38.70 7 -4 15 245.88 30.10 15 -7 4 232.68 33.80 -4 15 7 289.67 44.20 4 15 7 251.07 42.90 15 7 4 277.07 33.90 7 4 15 375.96 46.10 -7 -4 15 255.57 39.30 15 -7 -4 254.97 31.40 15 -9 4 225.08 28.40 -15 9 4 190.98 23.40 -9 4 15 235.98 40.00 -4 15 9 234.28 41.50 4 -15 9 213.48 29.60 9 -4 15 201.48 30.00 9 -4 15 208.58 37.20 15 -9 -4 233.58 30.50 15 9 4 200.68 30.80 9 4 15 299.07 43.30 -9 -4 15 206.38 38.40 4 15 9 203.28 40.30 15 -11 4 794.62 74.09 -11 4 15 875.51 82.09 11 -4 15 857.21 73.29 4 -15 11 830.72 71.79 -4 15 11 834.52 88.29 11 -4 15 847.42 83.19 -15 11 4 799.02 71.89 15 11 4 851.91 79.09 11 4 15 873.01 85.49 4 15 11 881.71 90.29 15 -11 -4 807.12 72.99 -13 4 15 493.25 56.19 13 -4 15 426.66 60.09 -4 15 13 477.85 67.09 -15 13 4 497.55 48.80 4 -15 13 478.25 45.50 15 -13 4 484.25 49.70 13 -4 15 514.55 49.50 15 -13 -4 357.56 47.50 4 15 13 480.65 62.99 13 4 15 449.36 61.69 15 13 4 471.45 57.69 15 0 -5 1675.53 131.19 0 -5 15 1605.84 140.79 5 -15 0 1646.24 132.69 0 -5 15 1557.54 129.39 0 5 15 1662.73 141.29 15 2 -5 531.05 43.70 2 -5 15 513.35 41.80 15 -2 5 508.85 47.90 -2 5 15 456.55 60.19 5 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8.80 16.40 15 10 5 -1.90 22.90 5 15 10 33.80 34.00 10 5 15 43.60 33.80 12 -5 15 457.15 46.90 -12 5 15 441.66 56.19 -15 12 5 500.85 45.90 -5 15 12 455.45 65.39 15 -12 5 492.45 48.90 5 -15 12 462.95 44.70 12 5 15 385.86 54.79 5 15 12 466.25 68.89 15 -12 -5 383.36 45.90 15 12 5 424.26 56.79 15 -14 5 63.59 21.70 14 -5 15 44.50 23.70 -5 15 14 26.80 35.60 5 -15 14 58.19 19.20 -15 14 5 85.39 21.50 -14 5 15 62.59 26.20 14 5 15 46.10 34.40 5 15 14 41.40 39.00 15 14 5 46.60 30.80 15 -14 -5 33.30 20.80 6 -15 1 8.10 16.50 1 -6 15 12.40 28.90 1 -6 15 11.00 8.90 15 1 -6 18.40 11.80 -1 6 15 -4.20 30.60 15 -1 -6 29.80 13.40 -1 -6 15 9.40 28.30 1 6 15 37.00 29.90 6 -15 -1 17.40 17.80 15 1 6 19.20 11.70 -3 6 15 105.09 33.30 3 -6 15 138.49 33.80 15 3 -6 156.58 21.40 3 -6 15 156.98 18.40 6 -15 3 174.78 24.10 15 -3 6 131.89 23.20 -3 -6 15 127.19 34.00 3 6 15 131.49 34.40 15 -3 -6 158.58 19.80 6 -15 -3 156.78 22.60 15 3 6 175.48 21.60 6 -15 5 376.96 40.60 5 -6 15 391.16 37.30 15 -5 6 384.16 41.80 -5 6 15 416.96 55.79 5 -6 15 374.56 55.79 -6 15 5 357.26 55.39 15 5 -6 355.96 36.10 -5 -6 15 454.15 55.49 6 15 5 400.46 58.19 6 -15 -5 389.86 41.10 15 5 6 402.86 41.10 15 -5 -6 397.26 38.30 5 6 15 445.36 55.99 -6 15 7 101.29 33.50 15 -7 6 139.89 23.20 7 -6 15 125.49 19.10 7 -6 15 137.19 36.90 6 -15 7 150.38 21.40 -7 6 15 149.39 35.40 -15 7 6 112.29 15.00 15 -7 -6 96.39 19.00 15 7 6 119.49 23.70 7 6 15 67.49 32.30 6 15 7 123.49 37.50 6 -15 -7 73.39 20.10 6 -15 9 152.28 22.80 9 -6 15 185.38 38.90 -9 6 15 202.28 36.50 -15 9 6 149.59 22.50 15 -9 6 191.48 26.80 -6 15 9 178.78 36.70 9 -6 15 192.68 24.00 9 6 15 151.68 36.20 15 -9 -6 147.09 23.20 6 15 9 123.89 37.30 15 9 6 157.88 29.60 15 -11 6 139.79 27.30 6 -15 11 153.28 24.10 11 -6 15 132.19 24.70 -15 11 6 208.08 27.80 -6 15 11 104.49 37.40 -11 6 15 203.28 36.90 15 -11 -6 234.28 25.80 6 15 11 289.07 48.10 15 11 6 244.88 35.80 11 6 15 199.48 37.60 -13 6 15 280.27 40.30 6 -15 13 253.87 33.70 15 -13 6 271.47 39.20 -6 15 13 300.27 49.40 -15 13 6 308.97 36.80 13 -6 15 255.27 37.10 15 13 6 278.67 43.80 6 15 13 245.88 48.60 15 -13 -6 302.07 34.20 13 6 15 233.68 44.20 15 0 -7 184.28 22.50 7 -15 0 235.98 26.40 0 -7 15 155.28 18.10 0 -7 15 187.78 36.80 15 0 7 180.18 25.00 0 7 15 232.58 39.20 2 -7 15 133.19 16.00 15 2 -7 131.19 16.70 2 -7 15 120.39 36.30 -2 7 15 110.09 33.50 15 -2 7 112.29 22.20 7 -15 2 122.29 23.00 15 -2 -7 138.79 18.00 15 2 7 154.38 21.20 7 -15 -2 118.29 22.70 2 7 15 134.59 37.90 4 -7 15 197.88 39.30 4 -7 15 219.58 27.50 15 -4 7 251.97 34.30 15 4 -7 234.38 25.60 -7 15 4 246.58 40.90 7 -15 4 237.98 31.60 -4 7 15 268.27 40.50 15 -4 -7 245.78 28.10 7 -15 -4 271.17 31.80 15 4 7 269.97 33.00 7 15 4 257.67 41.40 4 7 15 278.47 42.00 6 -7 15 126.29 18.30 -7 15 6 146.39 36.10 -15 6 7 113.59 14.60 15 -6 7 131.49 24.30 -6 7 15 105.39 32.80 7 -15 6 140.09 22.30 15 6 -7 137.59 15.90 7 15 6 77.69 35.40 15 -6 -7 87.69 18.10 7 -15 -6 80.69 20.10 15 6 7 104.49 23.40 6 7 15 98.09 33.70 7 -15 8 61.49 18.50 15 -8 7 64.49 20.80 -8 7 15 66.59 30.70 8 -7 15 51.29 18.20 -7 15 8 26.30 29.20 -15 8 7 62.09 14.40 15 8 7 133.79 25.70 7 -15 -8 106.49 19.80 7 15 8 74.89 33.30 15 -8 -7 118.69 18.70 8 7 15 133.59 35.10 10 -7 15 18.40 16.80 7 -15 10 -7.10 16.50 -10 7 15 19.80 30.70 -7 15 10 -0.70 30.50 15 -10 7 14.80 21.20 15 -10 -7 14.20 16.40 15 10 7 40.10 26.60 10 7 15 6.70 33.20 7 15 10 38.40 37.70 7 -15 12 342.07 37.70 15 -12 7 280.17 41.20 -15 12 7 393.86 38.50 -12 7 15 400.96 48.20 -7 15 12 343.77 49.40 12 -7 15 318.17 39.70 15 12 7 316.67 45.70 15 -12 -7 254.67 37.90 7 15 12 312.67 54.99 12 7 15 263.07 46.50 -14 7 15 219.08 36.30 14 -7 15 197.38 30.00 -15 14 7 256.57 34.50 15 -14 7 187.38 30.50 7 -15 14 232.98 33.10 -7 15 14 189.38 43.80 15 -14 -7 243.78 30.60 15 14 7 227.38 41.30 14 7 15 266.47 44.90 7 15 14 231.58 47.30 8 -15 1 14.60 17.00 15 1 -8 29.20 11.30 -1 8 15 12.40 29.60 1 -8 15 17.30 9.60 1 8 15 63.89 34.90 15 -1 -8 71.49 12.80 8 -15 -1 51.39 19.20 15 1 8 45.90 16.90 15 -3 8 218.18 30.30 8 -15 3 208.38 25.50 -3 8 15 246.88 41.40 3 -8 15 195.78 22.90 15 3 -8 193.18 21.50 3 8 15 131.49 36.50 15 -3 -8 157.18 23.30 15 3 8 160.48 26.10 8 -15 -3 157.28 25.60 15 5 -8 188.78 20.00 5 -8 15 192.08 24.30 -15 5 8 158.28 18.90 -8 15 5 197.48 36.80 15 -5 8 201.48 27.20 8 -15 5 208.88 25.40 -5 8 15 185.68 36.60 5 8 15 91.69 34.80 8 15 5 157.38 39.40 15 -5 -8 147.69 20.90 8 -15 -5 143.79 25.20 15 5 8 114.99 25.80 -7 8 15 50.19 34.50 -8 15 7 56.09 31.30 -15 7 8 77.29 14.60 8 -15 7 61.29 19.80 15 7 -8 66.49 11.80 15 -7 8 50.99 20.50 7 -8 15 61.19 17.80 7 8 15 95.29 33.00 15 7 8 136.79 26.60 8 15 7 132.19 37.80 8 -15 -7 85.99 19.50 -8 15 9 141.59 36.90 8 -15 9 102.19 20.70 9 -8 15 119.39 21.20 -9 8 15 141.39 34.90 -15 9 8 118.89 19.00 15 -9 8 128.09 25.50 15 9 8 97.19 28.10 15 -9 -8 108.49 20.20 8 -15 -9 117.39 21.60 8 15 9 97.79 35.10 9 8 15 84.39 35.30 8 -15 11 201.58 27.10 11 -8 15 155.78 26.20 -15 11 8 224.98 30.00 -11 8 15 138.19 36.40 15 -11 8 173.68 28.40 -8 15 11 194.08 42.70 15 -11 -8 188.98 25.20 8 15 11 164.28 41.60 11 8 15 242.28 45.10 15 11 8 245.88 37.60 -13 8 15 16.90 29.80 -15 13 8 57.19 18.80 -8 15 13 -7.80 34.90 8 -15 13 8.80 18.60 15 -13 8 19.10 22.70 13 -8 15 18.90 20.30 8 15 13 18.80 40.70 15 13 8 -1.90 31.70 13 8 15 42.50 37.50 15 -13 -8 37.30 19.60 15 0 9 420.36 42.90 0 -9 15 394.26 35.10 9 -15 0 415.66 42.40 0 9 15 381.96 56.99 15 0 -9 417.86 36.30 15 2 -9 215.18 22.60 15 -2 9 257.87 30.70 2 -9 15 241.38 24.20 9 -15 2 216.68 30.70 -2 9 15 174.68 38.40 15 2 9 247.38 30.30 15 -2 -9 230.48 25.10 9 -15 -2 200.18 27.00 2 9 15 184.38 39.10 -9 15 4 235.18 38.80 -15 4 9 223.48 23.20 15 -4 9 195.78 27.40 15 4 -9 197.28 21.80 -4 9 15 201.28 38.80 4 -9 15 194.08 26.20 9 -15 4 229.38 27.40 9 15 4 181.68 37.20 4 9 15 241.28 43.00 15 -4 -9 194.28 25.40 15 4 9 249.28 35.20 9 -15 -4 201.68 27.00 6 -9 15 185.48 22.80 -9 15 6 200.08 37.20 -15 6 9 159.08 22.50 9 -15 6 159.88 24.50 -6 9 15 148.79 37.50 15 -6 9 189.18 27.90 9 15 6 127.39 35.00 9 -15 -6 171.58 25.90 15 -6 -9 174.28 21.50 15 6 9 177.68 30.10 6 9 15 133.79 37.60 15 -8 9 80.09 22.60 -9 15 8 84.99 33.00 8 -9 15 109.39 20.60 -8 9 15 93.29 35.70 9 -15 8 115.19 23.60 -15 8 9 142.79 20.40 9 15 8 141.99 40.50 8 9 15 140.39 40.60 15 8 9 133.79 29.40 9 -15 -8 130.09 23.10 15 -8 -9 152.68 21.10 -10 9 15 216.28 39.70 -9 15 10 165.08 39.20 15 -10 9 113.49 27.40 9 -15 10 163.88 26.30 10 -9 15 155.78 26.50 -15 10 9 238.68 30.00 15 -10 -9 225.58 25.70 10 9 15 152.88 40.20 9 15 10 241.48 46.20 15 10 9 218.38 36.10 -9 15 12 312.47 47.20 -15 12 9 295.77 35.90 15 -12 9 301.77 40.30 9 -15 12 270.67 37.00 -12 9 15 373.86 47.10 12 -9 15 277.77 38.80 9 15 12 255.77 50.99 12 9 15 203.48 44.20 15 -12 -9 262.07 36.30 15 12 9 263.87 43.80 -14 9 15 61.69 29.70 -9 15 14 86.09 38.50 15 -14 9 49.60 23.10 9 -15 14 94.39 22.70 14 -9 15 65.59 23.70 14 9 15 67.99 38.00 9 15 14 50.19 42.40 15 -14 -9 68.19 22.80 15 14 9 44.60 35.50 -1 10 15 243.88 43.80 15 -1 10 237.88 37.90 1 -10 15 255.57 28.30 10 -15 1 292.37 35.60 15 1 -10 299.27 30.40 10 -15 -1 352.96 37.10 1 10 15 388.76 50.49 -1 -10 15 311.47 26.90 15 -1 -10 335.17 28.90 15 1 10 334.57 39.20 15 -3 10 726.63 61.59 -10 15 3 744.83 70.49 10 -15 3 690.93 60.09 -3 10 15 706.23 74.49 3 -10 15 704.33 55.99 3 10 15 585.74 74.29 10 -15 -3 585.64 59.79 15 -3 -10 611.54 55.39 10 15 3 609.34 72.39 15 3 10 577.94 63.19 10 -15 5 13.90 19.80 -10 15 5 16.50 27.20 -15 5 10 29.10 13.30 -5 10 15 17.20 34.40 5 -10 15 15.20 14.10 15 -5 10 20.00 19.20 15 5 10 9.70 22.40 15 -5 -10 10.50 13.30 10 15 5 31.00 30.70 5 10 15 13.00 30.60 10 -15 -5 15.90 18.60 10 -15 7 22.30 20.20 -10 15 7 3.10 26.40 7 -10 15 16.20 16.70 -7 10 15 25.00 30.60 15 -7 10 6.20 21.50 15 7 10 26.70 25.10 15 -7 -10 36.60 15.50 10 15 7 11.40 32.00 10 -15 -7 36.50 18.40 7 10 15 33.40 32.70 -10 15 9 195.38 40.00 9 -10 15 212.08 26.60 10 -15 9 189.78 28.20 -9 10 15 118.49 38.00 15 -9 10 157.68 28.60 -15 9 10 212.98 29.10 15 -9 -10 202.28 28.90 10 -15 -9 180.08 26.10 10 15 9 228.98 45.50 15 9 10 239.38 38.90 9 10 15 226.68 44.90 15 -11 10 216.58 31.10 -11 10 15 248.58 42.20 11 -10 15 239.58 31.50 10 -15 11 188.98 28.90 -10 15 11 192.48 40.40 -15 11 10 288.97 32.90 15 -11 -10 243.48 33.40 15 11 10 290.37 42.40 11 10 15 313.57 49.70 10 15 11 235.08 47.40 15 -13 10 226.08 32.30 13 -10 15 291.57 38.00 10 -15 13 270.87 36.30 -13 10 15 288.87 43.40 -10 15 13 314.97 46.50 13 10 15 197.68 45.70 15 13 10 196.18 44.40 10 15 13 181.28 48.10 15 -13 -10 203.18 30.70 0 11 15 66.99 37.90 0 -11 15 77.69 11.90 15 0 11 66.39 23.10 11 -15 0 63.19 21.40 -2 11 15 449.06 64.79 15 -2 11 422.86 48.10 11 -15 2 419.76 47.10 15 -2 11 399.36 49.99 2 -11 15 408.16 41.40 11 -15 -2 509.15 47.60 15 -2 -11 525.35 40.60 11 15 2 473.85 60.99 15 2 11 519.25 52.19 2 11 15 552.94 66.99 4 -11 15 828.92 70.59 11 -15 4 774.32 73.79 -11 15 4 790.62 81.19 15 -4 11 837.82 74.69 -4 11 15 780.82 86.19 -15 4 11 797.12 71.79 11 -15 -4 898.91 73.89 11 15 4 875.61 84.99 15 -4 -11 871.41 69.49 15 4 11 886.41 78.69 4 11 15 841.32 88.09 -15 6 11 208.58 27.70 11 -15 6 132.29 25.50 -11 15 6 124.29 32.80 15 -6 11 184.58 28.50 -6 11 15 126.89 38.60 6 -11 15 142.79 23.20 11 15 6 281.87 43.90 15 6 11 237.38 34.80 11 -15 -6 219.88 26.70 6 11 15 266.27 45.50 15 -6 -11 229.98 25.40 11 -15 8 173.68 29.10 -15 8 11 242.48 30.50 -11 15 8 127.09 36.10 8 -11 15 182.08 26.40 15 -8 11 180.98 29.90 -8 11 15 241.28 46.00 15 -8 -11 227.48 28.60 11 15 8 244.48 43.20 15 8 11 234.98 37.80 11 -15 -8 228.18 28.90 8 11 15 174.78 41.50 15 -10 11 223.88 32.50 10 -11 15 210.38 29.50 11 -15 10 245.98 31.90 -15 10 11 230.48 32.80 -10 11 15 299.87 46.70 -11 15 10 289.47 44.60 10 11 15 223.18 45.60 15 10 11 336.47 45.90 11 -15 -10 242.48 35.80 15 -10 -11 255.17 33.10 11 15 10 309.47 51.49 -12 11 15 20.00 32.90 11 -15 12 14.80 21.60 -15 12 11 0.20 13.90 -11 15 12 34.20 31.30 15 -12 11 17.30 22.40 12 -11 15 14.30 21.10 11 15 12 29.40 36.40 15 -12 -11 3.20 18.70 12 11 15 28.80 37.20 15 12 11 49.50 34.00 -14 11 15 212.38 37.90 11 -15 14 232.88 30.30 -11 15 14 165.78 41.10 14 -11 15 178.18 30.50 15 -14 11 174.38 31.10 14 11 15 102.29 43.20 15 -14 -11 141.29 27.70 15 14 11 127.29 42.60 11 15 14 106.59 45.60 15 -1 12 266.37 37.20 1 -12 15 278.57 28.30 12 -15 1 264.47 36.10 -1 12 15 197.08 43.50 15 1 12 221.78 36.70 -1 -12 15 319.37 26.40 1 12 15 304.17 50.69 12 -15 -1 283.37 33.40 -3 12 15 1084.49 98.29 12 -15 3 1061.19 84.29 -12 15 3 1008.40 90.49 15 -3 12 1074.89 85.19 3 -12 15 1067.69 80.59 -15 3 12 989.50 83.19 15 3 12 875.51 88.59 12 15 3 828.22 92.39 12 -15 -3 864.21 83.69 3 12 15 925.61 98.29 15 -3 -12 876.61 79.39 5 -12 15 441.86 41.30 -5 12 15 560.14 65.19 -15 5 12 488.35 44.00 12 -15 5 445.86 45.30 15 -5 12 446.66 47.10 -12 15 5 428.86 54.69 15 5 12 395.56 53.89 12 -15 -5 392.96 45.20 12 15 5 311.07 49.70 5 12 15 283.47 52.79 15 -5 -12 411.56 38.80 12 -15 7 311.17 38.70 -12 15 7 399.16 50.29 -7 12 15 386.96 51.69 7 -12 15 299.27 34.80 -15 7 12 365.36 37.30 15 -7 12 348.17 40.80 15 -7 -12 285.87 32.90 15 7 12 290.57 43.40 7 12 15 220.38 47.00 12 15 7 237.88 44.40 12 -15 -7 248.58 38.00 12 -15 9 233.28 31.80 9 -12 15 300.07 35.80 -15 9 12 302.47 35.60 -9 12 15 342.97 50.49 15 -9 12 297.37 40.40 -12 15 9 345.47 45.60 15 9 12 291.87 44.80 9 12 15 342.27 53.99 15 -9 -12 246.38 32.90 12 -15 -9 207.28 31.20 12 15 9 171.38 43.10 -12 15 11 50.79 32.20 -11 12 15 2.70 32.00 11 -12 15 5.30 21.60 12 -15 11 31.70 23.00 15 -11 12 -6.30 21.60 -15 11 12 -16.00 13.30 12 15 11 -9.90 38.30 11 12 15 5.20 35.70 15 11 12 12.20 32.10 15 -11 -12 21.40 18.70 -12 15 13 827.02 88.29 13 -12 15 864.81 76.59 12 -15 13 807.52 75.99 -13 12 15 867.31 88.49 15 -13 12 859.91 77.69 15 -13 -12 820.72 74.99 12 15 13 832.92 95.59 13 12 15 810.82 94.69 15 13 12 835.22 90.99 0 -13 15 1438.66 116.89 0 13 15 1451.45 132.89 13 -15 0 1456.65 120.29 15 0 13 1458.35 125.49 13 -15 2 195.98 27.50 15 -2 13 232.08 34.00 -13 15 2 178.08 32.00 2 -13 15 172.08 24.30 15 -2 13 148.19 26.60 -15 2 13 217.18 28.00 -2 13 15 132.29 41.20 2 13 15 127.29 40.10 15 2 13 176.08 34.30 13 -15 -2 215.68 28.40 13 15 2 207.18 37.30 -4 13 15 504.95 69.49 13 -15 4 508.05 50.09 15 -4 13 495.25 50.69 -13 15 4 453.95 56.09 -15 4 13 503.45 48.80 4 -13 15 479.15 44.90 13 -15 -4 423.06 48.60 13 15 4 476.75 61.79 4 13 15 471.25 70.59 15 4 13 454.75 58.49 15 -6 13 212.48 31.10 -15 6 13 318.17 35.20 -13 15 6 297.87 40.00 13 -15 6 291.27 36.90 6 -13 15 276.77 32.70 -6 13 15 192.18 43.10 6 13 15 247.48 48.00 13 15 6 182.38 39.80 13 -15 -6 223.28 30.30 15 6 13 300.97 43.80 -13 15 8 21.90 26.80 -8 13 15 39.50 37.80 15 -8 13 18.00 20.90 8 -13 15 22.70 18.20 13 -15 8 33.40 22.90 15 8 13 15.30 31.90 13 -15 -8 -3.10 19.70 8 13 15 36.10 42.70 13 15 8 26.90 33.20 15 -8 -13 12.30 15.40 -10 13 15 219.58 44.50 13 -15 10 297.07 38.90 10 -13 15 280.17 36.80 -13 15 10 282.27 42.60 15 -10 13 248.58 33.30 13 -15 -10 233.48 33.10 13 15 10 227.68 48.90 15 10 13 222.38 44.60 10 13 15 242.68 53.09 -13 15 12 763.92 84.39 15 -12 13 813.12 76.39 12 -13 15 802.92 74.69 -12 13 15 858.41 89.19 13 -15 12 795.72 75.39 13 15 12 874.51 94.59 12 13 15 809.42 94.79 15 12 13 905.41 91.79 -13 15 14 262.07 47.90 14 -13 15 252.87 35.70 -14 13 15 241.58 44.10 13 -15 14 266.87 35.30 15 -14 13 178.68 33.30 15 14 13 224.78 49.10 14 13 15 322.27 53.29 13 15 14 350.56 59.09 -14 15 1 166.68 31.40 1 -14 15 163.18 23.80 14 -15 1 168.38 27.60 -1 14 15 133.59 41.60 15 -1 14 161.38 33.40 1 14 15 189.18 48.40 14 15 1 227.08 39.30 15 1 14 200.18 35.20 14 -15 -1 223.58 28.50 14 -15 3 50.69 20.60 3 -14 15 22.50 15.10 -15 3 14 32.40 20.20 15 -3 14 15.90 22.30 -14 15 3 21.50 23.60 -3 14 15 55.99 36.40 15 3 14 14.80 29.30 3 14 15 28.80 36.60 14 -15 -3 4.00 19.80 14 15 3 37.50 29.70 15 -5 14 43.10 24.70 -14 15 5 48.20 25.90 -5 14 15 -2.50 34.90 5 -14 15 44.10 17.10 14 -15 5 47.00 22.60 -15 5 14 108.49 22.10 5 14 15 41.30 37.80 14 -15 -5 39.20 20.90 14 15 5 35.10 32.10 15 5 14 46.60 30.90 15 -7 14 216.78 33.80 -14 15 7 245.98 36.30 -7 14 15 201.08 43.90 7 -14 15 250.77 29.40 -15 7 14 237.58 34.70 14 -15 7 235.88 32.90 15 7 14 253.07 42.90 14 15 7 205.48 41.90 14 -15 -7 247.38 35.70 7 14 15 221.08 47.50 -14 15 9 73.59 28.30 -9 14 15 67.59 35.70 9 -14 15 52.69 21.00 15 -9 14 82.19 26.70 14 -15 9 102.39 24.90 9 14 15 79.69 46.60 15 9 14 52.69 38.20 14 15 9 71.79 40.00 14 -15 -9 56.79 23.80 -11 14 15 169.88 42.30 14 -15 11 120.29 26.60 11 -14 15 149.79 25.70 -14 15 11 147.09 34.00 15 -11 14 199.68 31.20 11 14 15 106.19 44.20 14 -15 -11 126.49 27.60 15 11 14 105.89 41.00 14 15 11 138.19 44.20 14 -15 13 206.98 34.00 -13 14 15 297.37 48.50 15 -13 14 305.87 38.00 13 -14 15 206.58 32.50 -14 15 13 281.97 44.90 14 15 13 316.27 53.59 15 13 14 218.58 49.70 13 14 15 245.88 52.09 -15 15 0 2363.96 202.48 0 15 15 2540.55 213.08 15 -15 0 2426.46 200.18 15 0 15 2485.35 206.18 15 15 0 2561.84 206.18 -15 2 15 517.25 53.39 -15 15 2 519.85 53.59 -2 15 15 544.55 74.89 2 -15 15 529.65 45.50 15 -2 15 538.95 61.39 15 -2 15 566.64 52.29 15 -15 2 511.05 51.29 2 15 15 358.46 66.09 15 2 15 336.57 54.29 15 15 2 386.86 55.69 -15 4 15 204.78 28.90 -15 15 4 180.88 28.40 -4 15 15 126.09 42.70 4 -15 15 175.78 22.40 15 -4 15 159.38 28.80 15 -15 4 130.49 25.40 15 -15 -4 96.49 25.00 4 15 15 127.89 45.50 15 4 15 121.99 36.70 15 15 4 94.39 34.70 -15 6 15 281.27 37.80 -15 15 6 269.77 36.40 -6 15 15 170.08 46.10 6 -15 15 230.68 33.10 15 -6 15 216.28 32.70 15 -15 6 205.58 31.80 15 -15 -6 229.68 31.20 6 15 15 308.57 53.79 15 6 15 285.37 45.40 15 15 6 291.87 45.70 -8 15 15 279.07 52.89 8 -15 15 264.17 31.00 15 -8 15 226.08 33.20 15 -15 8 248.08 33.30 15 -15 -8 195.18 30.70 8 15 15 203.28 48.70 15 8 15 238.38 45.00 15 15 8 215.58 44.20 -10 15 15 568.24 77.59 10 -15 15 557.24 57.69 15 -10 15 603.44 60.19 15 -15 10 577.34 60.39 15 -15 -10 565.04 58.09 10 15 15 600.94 83.69 15 10 15 674.13 77.79 15 15 10 567.54 76.79 -12 15 15 834.22 91.19 12 -15 15 784.72 76.09 15 -12 15 803.82 77.19 15 -15 12 757.02 77.19 12 15 15 880.41 98.59 15 12 15 911.61 95.99 15 15 12 922.91 94.89 -15 14 15 8.50 12.50 -14 15 15 75.49 37.50 14 -15 15 60.69 26.60 15 -14 15 50.29 25.70 15 -15 14 35.10 26.30 14 15 15 140.39 49.20 15 14 15 136.19 49.20 15 15 14 124.99 45.60 0 0 16 200.78 35.20 16 0 0 145.49 21.50 2 0 16 1131.69 102.79 16 -2 0 1025.40 91.09 0 -16 2 1096.29 91.29 -2 0 16 1140.09 101.79 4 0 16 83.89 31.70 0 -16 4 88.19 18.50 16 -4 0 90.79 18.60 -4 0 16 118.59 34.50 0 16 6 126.79 37.60 16 -6 0 226.88 27.20 -6 0 16 157.28 35.30 0 -16 6 196.18 28.10 6 0 16 222.18 40.60 0 -16 8 170.18 22.40 16 -8 0 166.18 24.90 16 8 0 156.98 22.50 0 16 8 120.79 36.70 8 0 16 161.38 36.80 -8 0 16 166.08 37.00 16 -10 0 175.48 27.70 0 16 10 204.58 44.90 16 10 0 209.58 28.90 0 -16 10 184.68 23.40 10 0 16 157.98 36.50 -10 0 16 194.88 36.80 -12 0 16 231.78 37.80 16 12 0 227.68 33.20 16 -12 0 197.68 28.10 0 16 12 153.38 42.80 0 -16 12 189.98 27.70 12 0 16 230.18 40.70 14 0 16 30.90 31.20 0 -16 14 9.20 13.80 0 16 14 -22.50 37.10 -16 14 0 -2.90 6.20 16 14 0 6.60 25.80 16 -14 0 2.20 20.90 16 -1 1 5448.65 455.45 16 1 -1 5551.84 455.25 1 -16 1 5458.05 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1 16 567.14 66.09 16 -11 1 571.24 55.29 1 -16 11 587.34 51.99 16 11 -1 562.44 56.79 16 11 1 557.64 57.99 1 16 11 513.85 73.39 16 -11 -1 580.44 55.09 -11 -1 16 531.65 64.99 11 1 16 576.54 68.49 -13 1 16 710.13 72.19 13 -1 16 693.63 76.69 1 -16 13 737.93 60.89 -1 16 13 696.03 83.09 16 13 -1 762.02 70.39 16 -13 1 677.53 64.79 16 -13 -1 692.93 65.09 1 16 13 578.54 83.59 13 1 16 649.83 75.99 16 13 1 678.73 70.49 16 -15 1 116.19 25.90 -1 16 15 87.39 42.20 1 -16 15 130.59 19.00 15 -1 16 91.59 35.80 16 15 -1 115.79 33.20 15 -1 16 113.19 27.30 16 -15 -1 159.48 26.50 15 1 16 170.18 37.80 1 16 15 227.58 53.29 16 15 1 155.08 35.10 0 -2 16 959.70 82.69 2 -16 0 1038.30 86.89 0 -2 16 1098.79 96.99 0 2 16 1163.18 98.49 16 0 -2 990.80 85.99 16 2 -2 3015.50 253.27 -2 2 16 3287.37 261.27 2 -16 2 3074.99 253.67 16 -2 2 3140.19 254.07 2 -2 16 3046.70 252.17 2 -2 16 3325.37 261.37 16 -2 -2 3212.18 253.57 2 2 16 3336.77 261.07 -2 -2 16 3280.07 260.87 2 -16 -2 3158.58 253.97 4 -2 16 1046.10 97.09 -4 2 16 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11 4.20 26.30 12 -11 19 39.10 23.70 -12 11 19 16.40 43.40 -11 19 12 42.50 42.00 12 11 19 65.69 49.99 19 -12 -11 43.80 23.60 19 12 11 49.70 34.80 11 19 12 78.29 53.49 11 -19 14 55.69 27.80 19 -14 11 10.40 27.00 14 -11 19 36.30 25.10 -11 19 14 31.10 41.60 -14 11 19 25.00 39.80 19 14 11 11.10 36.00 14 11 19 5.60 45.00 19 -14 -11 49.80 25.90 11 19 14 72.09 54.19 -1 12 19 -39.60 42.10 -12 19 1 -5.70 32.30 12 -19 1 22.50 24.70 19 -1 12 10.00 24.20 12 -19 -1 11.60 21.40 1 12 19 -11.60 41.00 12 19 1 6.90 40.40 12 -19 3 284.67 41.60 -3 12 19 319.67 59.39 -12 19 3 256.17 47.50 19 -3 12 268.17 37.60 12 19 3 365.96 55.69 12 -19 -3 299.37 41.00 19 3 12 274.87 38.80 3 12 19 250.57 52.89 19 -5 12 198.08 34.00 12 -19 5 294.07 36.40 -12 19 5 218.88 44.20 -5 12 19 285.47 56.19 12 -19 -5 221.78 32.30 5 12 19 222.28 51.79 19 5 12 259.87 35.70 12 19 5 245.58 48.10 19 -5 -12 264.47 32.70 12 -19 7 294.67 43.30 -7 12 19 329.77 60.29 19 -7 12 250.97 37.70 -12 19 7 328.77 53.29 7 -12 19 250.87 35.20 19 -7 -12 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25.70 7 -20 -1 37.00 22.80 20 3 -7 153.08 21.10 -3 7 20 164.88 49.20 20 -3 7 149.99 28.60 7 -20 3 151.18 27.60 20 -3 -7 124.39 21.90 7 20 3 125.69 42.80 7 -20 -3 105.29 26.50 3 7 20 180.88 50.09 5 -7 20 1611.74 130.49 -5 7 20 1674.93 149.29 -7 20 5 1684.93 148.79 20 5 -7 1633.64 130.99 20 -5 7 1689.93 135.69 7 -20 5 1616.14 134.19 5 7 20 1531.55 149.19 7 -20 -5 1584.14 134.89 7 20 5 1603.84 149.69 20 -5 -7 1525.85 132.19 20 7 -7 2034.90 158.88 -7 7 20 2113.09 176.38 20 -7 7 2046.40 163.38 7 -7 20 1933.41 159.38 7 -20 7 1988.50 161.78 -7 20 7 1951.50 175.38 20 -7 -7 1768.22 160.18 7 20 7 2038.50 178.18 7 7 20 1909.51 175.18 9 -7 20 59.89 21.70 20 9 -7 54.29 16.30 -9 7 20 76.49 40.70 -7 20 9 63.49 42.10 7 -20 9 91.39 24.80 20 -9 7 47.10 28.00 9 7 20 24.80 45.10 20 -9 -7 49.90 22.80 7 20 9 38.40 44.80 -11 7 20 420.36 58.19 20 11 -7 342.37 48.10 7 -20 11 387.06 45.60 11 -7 20 358.06 45.20 -7 20 11 369.16 64.09 20 -11 7 366.36 50.39 20 -11 -7 363.46 45.90 7 20 11 273.77 59.19 11 7 20 462.65 67.19 -7 20 13 60.19 47.30 13 -7 20 126.29 28.20 -13 7 20 108.79 42.80 20 -13 7 109.49 32.60 7 -20 13 97.69 26.50 13 7 20 133.69 51.99 20 -13 -7 86.49 26.20 7 20 13 41.50 47.30 20 -15 7 189.58 36.50 15 -7 20 247.58 35.30 7 -20 15 298.27 34.90 -7 20 15 274.57 63.39 20 15 7 231.88 48.60 15 7 20 258.47 58.89 7 20 15 156.18 56.39 20 -15 -7 262.67 35.20 20 0 8 1087.69 92.19 20 0 -8 1046.00 86.39 0 8 20 953.20 108.79 8 -20 0 1003.70 90.79 -2 8 20 1387.76 130.79 20 2 -8 1346.27 110.09 20 -2 8 1402.36 115.49 8 -20 2 1308.57 114.29 2 8 20 1262.87 129.39 8 -20 -2 1349.07 114.19 20 -2 -8 1363.96 110.89 -4 8 20 757.62 89.09 20 4 -8 768.62 62.59 -8 20 4 791.62 88.49 8 -20 4 765.62 68.09 20 -4 8 797.32 70.99 8 -20 -4 673.73 69.19 4 8 20 656.13 90.39 8 20 4 633.64 87.89 20 -4 -8 669.13 64.39 -6 8 20 323.27 57.59 -8 20 6 285.07 54.69 20 -6 8 312.47 40.10 6 -8 20 295.07 32.90 8 -20 6 285.07 36.90 20 -6 -8 280.77 37.10 8 20 6 295.97 54.39 6 8 20 315.37 56.29 -8 20 8 1818.52 182.18 8 -8 20 1968.10 167.48 20 -8 8 2015.90 171.28 -8 8 20 1903.41 183.58 8 -20 8 1929.41 169.48 8 20 8 2321.27 186.68 20 -8 -8 2364.86 168.88 8 8 20 2239.18 185.48 -10 8 20 1460.95 133.59 10 -8 20 1332.87 115.39 8 -20 10 1361.76 117.29 20 -10 8 1482.55 119.59 -8 20 10 1299.67 133.69 10 8 20 1373.06 135.39 8 20 10 1370.26 137.79 20 -10 -8 1353.66 116.19 8 -20 12 100.29 27.70 20 -12 8 96.29 30.30 12 -8 20 100.59 26.10 -8 20 12 64.89 43.20 -12 8 20 153.88 46.90 12 8 20 18.10 43.20 8 20 12 62.79 51.99 20 -12 -8 71.39 25.60 20 -14 8 -3.40 27.60 14 -8 20 -2.80 25.50 -14 8 20 28.60 39.50 8 -20 14 2.90 23.00 -8 20 14 15.50 50.59 20 -14 -8 13.60 24.40 20 14 8 -16.50 31.50 14 8 20 20.70 46.40 8 20 14 15.50 52.79 8 -20 16 44.00 25.60 16 -8 20 18.60 26.60 20 -16 8 -1.00 26.70 -8 20 16 31.50 45.20 20 16 8 24.60 37.30 16 8 20 5.50 44.40 20 -16 -8 44.40 27.10 8 20 16 14.80 61.19 -1 9 20 207.08 52.99 20 -1 9 225.38 33.50 20 1 -9 195.28 26.20 9 -20 1 159.18 29.20 20 -1 -9 238.68 28.00 1 9 20 227.28 50.59 9 -20 -1 271.07 33.90 -9 20 3 417.06 58.29 9 -20 3 321.07 42.20 20 -3 9 304.47 44.50 -3 9 20 266.47 56.49 9 -20 -3 342.97 43.30 9 20 3 227.88 50.59 3 9 20 233.88 52.69 20 -3 -9 332.17 35.10 20 -5 9 40.90 25.50 -5 9 20 36.70 41.30 9 -20 5 36.00 24.10 -9 20 5 72.59 41.70 20 -5 -9 46.20 18.80 9 20 5 54.29 41.80 5 9 20 48.90 44.00 9 -20 -5 42.80 24.40 9 -20 7 60.79 24.00 -7 9 20 62.09 42.50 7 -9 20 58.49 18.30 20 -7 9 81.29 29.10 -9 20 7 83.89 45.60 7 9 20 36.60 47.30 20 -7 -9 64.59 20.90 9 20 7 -8.90 44.60 9 -9 20 194.38 27.60 -9 9 20 170.68 48.30 -9 20 9 210.18 51.09 9 -20 9 167.98 30.00 20 -9 9 209.28 36.00 9 20 9 200.98 56.29 20 -9 -9 184.38 28.40 9 9 20 182.88 53.79 11 -9 20 144.59 26.20 20 -11 9 108.79 31.70 9 -20 11 122.69 27.40 -11 9 20 107.19 43.80 -9 20 11 57.29 43.70 11 9 20 67.79 47.80 20 -11 -9 91.89 25.90 9 20 11 83.19 53.79 13 -9 20 101.49 26.70 -9 20 13 187.68 52.39 20 -13 9 114.49 33.30 -13 9 20 147.09 47.80 9 -20 13 109.19 27.50 13 9 20 125.29 52.39 20 -13 -9 102.99 27.60 20 13 9 143.49 40.40 9 20 13 110.89 58.29 -15 9 20 12.30 14.00 15 -9 20 37.10 27.20 20 -15 9 23.30 29.70 9 -20 15 7.90 24.50 -9 20 15 10.90 42.90 20 -15 -9 1.50 26.30 9 20 15 2.00 56.99 15 9 20 -2.70 47.40 20 15 9 -27.40 32.90 20 0 10 -3.10 23.80 10 -20 0 20.40 22.20 0 10 20 -1.30 41.30 -10 20 2 406.46 58.39 20 -2 10 323.77 46.80 10 -20 2 321.67 43.10 -2 10 20 261.47 55.49 20 -2 -10 323.67 34.40 10 -20 -2 300.67 39.30 10 20 2 362.46 59.49 2 10 20 297.77 58.29 20 -4 10 698.43 70.49 -10 20 4 722.73 85.69 10 -20 4 728.83 70.29 -4 10 20 713.23 92.59 4 10 20 797.42 93.89 20 -4 -10 738.03 64.39 10 20 4 795.12 91.69 10 -20 -4 714.93 69.49 10 -20 6 48.20 24.10 -10 20 6 46.90 42.30 20 -6 10 22.50 25.20 -6 10 20 45.40 41.30 10 20 6 44.50 45.20 6 10 20 41.30 49.30 10 -20 -6 26.90 25.40 20 -6 -10 21.60 18.70 10 -20 8 1416.76 115.99 -8 10 20 1305.97 132.39 8 -10 20 1325.57 112.79 -10 20 8 1392.16 131.39 10 20 8 1404.06 134.89 20 -8 -10 1372.26 113.49 8 10 20 1263.87 134.99 -10 20 10 654.63 89.59 10 -20 10 775.52 69.89 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11 -20 7 345.67 47.50 7 -11 20 444.56 39.30 -7 11 20 335.87 63.69 -11 20 7 332.57 54.99 20 -7 11 373.66 50.79 20 -7 -11 376.66 41.20 11 20 7 328.97 58.59 11 -20 -7 418.06 48.50 7 11 20 388.86 68.99 11 -20 9 76.69 24.90 20 -9 11 80.99 29.30 -9 11 20 86.89 49.80 9 -11 20 119.69 23.80 -11 20 9 90.89 42.40 20 -9 -11 92.49 22.70 11 20 9 57.39 43.40 9 11 20 89.59 51.59 -11 11 20 336.67 58.29 11 -20 11 186.08 30.80 11 -11 20 232.38 30.20 20 -11 11 175.18 33.10 -11 20 11 285.67 52.49 11 11 20 165.98 54.39 20 -11 -11 154.98 29.20 20 11 11 182.48 40.70 11 20 11 84.59 47.60 -11 20 13 231.58 53.19 20 -13 11 196.28 36.80 13 -11 20 307.67 37.30 -13 11 20 309.77 55.69 11 -20 13 331.17 44.50 13 11 20 272.37 63.49 20 -13 -11 287.77 36.80 11 20 13 217.18 59.99 20 13 11 294.47 47.60 20 0 12 377.76 50.49 12 -20 0 341.37 47.20 0 12 20 400.16 65.59 20 -2 12 6.60 26.40 12 -20 2 43.50 26.40 -2 12 20 15.00 45.20 -12 20 2 42.60 39.00 12 -20 -2 42.70 23.70 12 20 2 63.89 39.70 2 12 20 48.10 45.10 -12 20 4 288.37 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201.08 49.10 21 -5 -2 202.08 27.90 5 2 21 221.48 50.89 2 21 5 187.08 48.00 7 -2 21 265.87 52.79 21 -7 2 224.58 33.80 7 -2 21 243.58 32.80 -7 2 21 202.38 52.09 2 -21 7 298.17 35.30 -2 21 7 226.18 56.59 21 -7 -2 298.57 39.50 2 21 7 272.07 56.79 -7 -2 21 263.67 49.99 7 2 21 227.18 51.59 9 -2 21 38.90 20.40 21 -9 2 45.40 26.30 9 -2 21 52.69 46.30 2 -21 9 41.90 23.80 -9 2 21 114.49 46.80 -2 21 9 65.09 46.50 -9 -2 21 19.10 39.20 2 21 9 27.20 50.69 21 -9 -2 -6.70 22.20 9 2 21 21.00 41.00 11 -2 21 185.98 30.20 -11 2 21 230.88 51.09 21 -11 2 204.28 33.70 11 -2 21 207.68 53.49 -2 21 11 154.48 55.39 21 -11 -2 290.57 35.00 2 21 11 183.38 53.29 11 2 21 168.58 49.20 13 -2 21 147.19 28.30 21 -13 2 131.09 30.70 -2 21 13 182.78 63.59 13 -2 21 165.18 49.90 -13 2 21 137.59 44.90 2 21 13 124.69 53.79 21 -13 -2 194.68 32.00 13 2 21 159.58 47.40 15 -2 21 14.30 25.70 21 -15 2 31.80 27.80 -2 21 15 12.60 55.09 15 -2 21 42.50 43.00 15 2 21 4.80 41.80 15 2 21 27.20 26.90 21 -15 -2 20.20 28.00 2 21 15 33.40 51.29 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483.05 51.19 11 -6 21 477.75 49.90 11 6 21 387.96 68.19 21 -11 -6 375.46 50.79 6 21 11 326.67 68.99 -6 21 13 78.29 47.90 13 -6 21 145.59 27.90 -13 6 21 102.59 44.90 6 -21 13 76.59 25.10 21 -13 6 80.99 28.40 21 -13 -6 55.79 25.90 13 6 21 142.49 55.09 6 21 13 37.00 53.29 21 -15 6 105.49 32.40 6 -21 15 74.89 25.70 15 -6 21 69.79 26.00 -6 21 15 83.99 51.89 21 -15 -6 80.39 30.10 6 21 15 65.69 53.39 15 6 21 110.69 53.39 7 -21 0 25.60 24.40 21 0 -7 26.00 16.70 21 0 7 10.10 23.30 0 7 21 38.40 45.40 21 -2 7 259.07 36.80 21 2 -7 240.88 32.50 7 -21 2 330.17 37.50 -2 7 21 223.48 54.39 2 7 21 272.77 56.89 21 -2 -7 274.87 34.50 7 -21 -2 281.87 35.70 21 4 -7 914.81 76.59 7 -21 4 888.11 81.79 -4 7 21 903.11 103.59 -7 21 4 955.50 101.79 21 -4 7 951.60 83.19 7 21 4 887.41 104.09 7 -21 -4 881.51 82.29 4 7 21 859.11 102.49 21 -4 -7 862.61 77.99 21 6 -7 824.62 72.29 21 -6 7 878.01 79.79 -6 7 21 897.91 100.29 7 -21 6 849.72 77.59 -7 21 6 888.41 98.49 6 7 21 792.72 98.59 7 21 6 798.52 101.89 21 -6 -7 852.51 75.09 21 8 -7 185.18 24.10 8 -7 21 164.18 25.70 -8 7 21 221.08 55.69 -7 21 8 243.18 57.59 7 -21 8 145.49 28.50 21 -8 7 175.78 33.40 21 -8 -7 268.97 35.80 7 21 8 251.17 55.19 8 7 21 233.28 50.69 21 -10 7 204.08 36.00 -7 21 10 220.08 53.89 7 -21 10 253.87 34.20 10 -7 21 276.87 38.70 -10 7 21 211.68 51.39 10 7 21 360.46 63.49 7 21 10 271.17 59.79 21 -10 -7 351.56 40.30 -7 21 12 277.37 62.19 -12 7 21 213.98 52.49 7 -21 12 312.67 36.40 12 -7 21 249.97 34.10 21 -12 7 212.48 37.20 12 7 21 206.98 51.69 7 21 12 208.68 61.19 21 -12 -7 256.27 34.60 -14 7 21 193.78 47.90 -7 21 14 173.98 52.19 7 -21 14 163.08 30.40 14 -7 21 220.68 33.00 21 -14 7 211.28 37.50 14 7 21 158.38 54.49 7 21 14 156.28 63.99 21 -14 -7 136.79 31.20 8 -21 1 18.00 22.00 21 1 -8 23.20 15.80 -1 8 21 -5.10 43.80 21 -1 8 32.20 26.50 8 -21 -1 18.00 22.10 21 -1 -8 25.00 16.30 21 1 8 19.00 27.00 1 8 21 19.40 42.40 8 -21 3 349.67 45.20 -8 21 3 310.57 54.69 21 -3 8 377.56 46.90 -3 8 21 272.27 55.09 21 3 -8 343.77 35.20 8 21 3 446.56 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160.68 32.10 21 -9 10 244.38 38.10 9 10 21 320.27 62.39 10 21 9 313.37 63.89 21 -9 -10 247.88 31.50 21 -11 10 190.68 35.90 10 -21 11 281.47 36.00 -10 21 11 313.67 58.49 11 -10 21 310.67 40.60 -11 10 21 384.86 62.29 21 -11 -10 228.98 33.50 11 10 21 244.68 62.49 10 21 11 262.07 64.29 -13 10 21 -57.89 41.00 10 -21 13 0.30 25.40 21 -13 10 16.60 28.70 13 -10 21 26.70 24.60 -10 21 13 4.60 43.20 10 21 13 44.30 52.09 21 -13 -10 10.60 26.00 13 10 21 33.60 53.89 0 11 21 92.59 51.29 21 0 11 89.99 30.90 11 -21 0 106.19 28.90 -11 21 2 142.79 43.50 11 -21 2 167.88 30.90 21 -2 11 232.98 36.80 -2 11 21 155.18 53.39 2 11 21 170.38 51.89 11 -21 -2 165.58 29.10 11 21 2 203.98 52.39 11 -21 4 22.20 26.60 -4 11 21 -12.70 45.30 -11 21 4 -17.40 35.90 21 -4 11 10.30 25.60 11 -21 -4 -13.50 22.40 4 11 21 5.00 52.69 11 21 4 -35.70 45.30 -11 21 6 494.85 71.89 11 -21 6 446.86 51.89 21 -6 11 460.15 54.19 -6 11 21 455.95 68.49 11 -21 -6 397.96 51.49 21 -6 -11 400.56 42.40 11 21 6 307.77 60.49 6 11 21 322.47 65.99 -8 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55.39 -6 7 23 -0.20 52.79 -7 23 6 1.80 41.00 7 -23 6 27.80 26.50 23 -6 7 24.60 29.20 23 6 -7 21.80 19.30 7 23 6 40.50 54.59 6 7 23 59.99 54.39 23 -6 -7 39.20 21.70 7 -23 8 765.92 76.69 23 -8 7 781.82 79.59 -8 7 23 728.23 104.29 -7 23 8 666.33 104.39 23 -8 -7 918.81 75.29 8 7 23 812.72 105.19 7 23 8 879.41 108.09 23 -10 7 130.09 33.90 -7 23 10 52.89 55.09 -10 7 23 80.99 53.79 7 -23 10 109.39 29.00 7 23 10 177.08 55.59 23 -10 -7 206.28 29.90 10 7 23 89.09 50.89 -12 7 23 25.80 47.20 7 -23 12 44.40 26.20 23 -12 7 51.09 30.60 12 -7 23 10.60 23.50 -7 23 12 62.09 57.19 7 23 12 9.90 61.29 23 -12 -7 44.60 26.70 12 7 23 25.50 51.79 -1 8 23 156.68 57.19 23 -1 8 113.49 29.90 23 1 -8 147.89 22.00 8 -23 1 94.49 30.60 8 -23 -1 157.78 34.10 1 8 23 115.39 50.39 23 -1 -8 146.89 23.00 23 1 8 163.68 34.70 23 -3 8 573.44 59.89 -3 8 23 411.36 69.99 -8 23 3 645.04 86.49 8 -23 3 615.94 58.89 23 3 8 556.64 61.79 8 23 3 414.56 69.79 23 -3 -8 495.85 50.19 3 8 23 341.67 69.29 -5 8 23 1397.86 143.99 8 -23 5 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17.3781 -8.2525 5 23 6 29.8760 -1.4196 5 23 8 2.9140 -37.6500 5 23 10 1.3599 -6.3996 5 23 12 -17.6243 -19.4418 5 24 5 -10.8221 7.6178 5 24 7 17.4751 28.4560 5 24 9 -10.8105 16.2406 5 24 11 -6.7129 15.4572 5 25 6 23.2359 -2.2381 5 25 8 -16.1043 -21.8001 5 26 5 5.9994 2.9681 6 6 6 -58.0867 137.8353 6 7 7 -41.7285 -64.6409 6 8 6 38.0075 -72.0552 6 8 8 16.7998 -34.8880 6 9 7 -8.8814 3.3308 6 9 9 -19.2770 24.5822 6 10 6 -37.4675 -42.0051 6 10 8 -58.7992 22.6250 6 10 10 -106.9829 -43.1997 6 11 7 30.6514 13.5732 6 11 9 -1.7764 -1.0164 6 11 11 15.5428 12.2415 6 12 6 86.6083 -20.2082 6 12 8 41.6121 24.7438 6 12 10 56.9046 7.4926 6 12 12 -22.7280 -32.4432 6 13 7 21.0712 30.5494 6 13 9 -18.0561 -51.4368 6 13 11 4.5195 -42.5127 6 13 13 -42.7722 -34.0309 6 14 6 43.6357 25.2075 6 14 8 -7.6280 4.9802 6 14 10 55.3192 22.9046 6 14 12 3.9957 12.6455 6 14 14 6.2381 -2.5369 6 15 7 -13.9944 35.9804 6 15 9 25.2062 15.2133 6 15 11 48.3498 68.6729 6 15 13 -19.7187 -31.0208 6 15 15 -20.7721 20.5197 6 16 6 -17.9267 61.5602 6 16 8 -6.3238 -30.2316 6 16 10 -22.3296 13.3491 6 16 12 -33.3933 33.7507 6 16 14 5.8663 -7.6356 6 16 16 -6.5232 -17.2355 6 17 7 2.5328 11.6169 6 17 9 -6.9205 16.4053 6 17 11 29.5918 -6.8413 6 17 13 45.2108 11.5720 6 17 15 16.4294 5.1358 6 17 17 -11.1237 -6.6723 6 18 6 25.0187 42.8308 6 18 8 -34.7033 -16.5634 6 18 10 -24.5279 -9.9891 6 18 12 -3.3186 6.9145 6 18 14 -49.2063 -9.1254 6 18 16 -7.7145 24.8182 6 18 18 -8.3649 -8.3086 6 19 7 40.5585 -8.2028 6 19 9 9.6483 -16.0689 6 19 11 -28.8290 -9.0642 6 19 13 -0.8882 -11.5010 6 19 15 -7.5006 0.7218 6 19 17 -3.5461 -21.1881 6 20 6 14.1520 79.5917 6 20 8 10.3300 -28.6961 6 20 10 11.7093 -7.7009 6 20 12 -8.5794 20.4759 6 20 14 14.4002 -5.2382 6 20 16 5.2158 11.5219 6 21 7 53.7139 27.5224 6 21 9 -4.8584 17.9780 6 21 11 0.8864 -11.3705 6 21 13 12.9544 5.1634 6 21 15 -12.5246 4.1880 6 22 6 -22.2513 -24.7370 6 22 8 -11.7988 6.8796 6 22 10 6.7418 -24.2542 6 22 12 -13.2994 22.8296 6 22 14 0.0627 1.5933 6 23 7 29.4421 0.2939 6 23 9 -0.1588 -11.0270 6 23 11 5.7048 8.1920 6 23 13 28.2187 12.0711 6 24 6 -18.4927 -1.0302 6 24 8 2.4986 3.7942 6 24 10 3.7578 -1.3110 6 25 7 17.7219 0.6583 7 8 7 -39.9826 -24.8449 7 9 8 -21.6687 -27.9314 7 10 7 -11.4740 40.9268 7 10 9 -22.6216 -20.1920 7 11 8 44.6838 -58.0795 7 11 10 -10.4334 48.3973 7 12 7 -65.3986 -49.8138 7 12 9 -48.6059 77.2745 7 12 11 -32.4153 34.9325 7 13 8 15.5882 7.4818 7 13 10 51.3766 28.4925 7 13 12 3.2478 29.7046 7 14 7 -37.8304 -42.5036 7 14 9 -5.8089 6.0966 7 14 11 -8.3844 14.8334 7 14 13 -4.8674 6.0497 7 15 8 6.0519 22.2049 7 15 10 10.6822 -8.3247 7 15 12 -17.8080 -35.0242 7 15 14 -13.8534 -16.2186 7 16 7 -34.3265 -18.5615 7 16 9 33.9655 19.4830 7 16 11 1.4352 -12.3204 7 16 13 -7.8237 49.5698 7 16 15 7.8399 -34.8432 7 17 8 19.9640 39.5615 7 17 10 -32.2048 -4.9617 7 17 12 -22.9748 -11.0002 7 17 14 17.1570 21.5203 7 17 16 28.8962 -18.2107 7 18 7 24.7504 -2.7632 7 18 9 26.1625 -1.7398 7 18 11 12.0382 21.1234 7 18 13 -2.9226 20.8429 7 18 15 15.4022 19.2183 7 18 17 5.8221 9.4131 7 19 8 -9.2121 -22.0995 7 19 10 2.3614 -2.1539 7 19 12 -9.1129 -5.6140 7 19 14 -1.0067 11.2205 7 19 16 18.6812 -3.7423 7 19 18 -1.2296 -4.0988 7 20 7 -4.6253 3.4010 7 20 9 -1.9198 -6.4754 7 20 11 11.3664 -6.6407 7 20 13 9.4542 16.6325 7 20 15 -4.9109 -7.9123 7 20 17 11.8169 39.0378 7 21 8 1.2783 -25.9451 7 21 10 10.6163 -1.8803 7 21 12 22.2103 -3.0418 7 21 14 17.1643 12.9810 7 22 7 5.8297 22.0278 7 22 9 -7.1259 -13.4996 7 22 11 11.3160 -1.0233 7 22 13 -6.8195 1.1823 7 23 8 -6.1914 2.8402 7 23 10 6.1846 9.7762 7 23 12 -10.4850 -17.1168 7 24 7 -32.1997 30.5497 7 24 9 1.3714 14.2263 7 25 8 -3.8871 49.7561 8 8 8 -52.0959 9.1932 8 9 9 37.6201 -58.2153 8 10 8 -1.1373 -16.3772 8 10 10 3.2733 56.2531 8 11 9 -0.1370 -28.0327 8 11 11 9.3048 23.4888 8 12 8 47.7592 61.7042 8 12 10 32.5583 21.6987 8 12 12 -5.9241 -16.9865 8 13 9 -41.0495 -32.7914 8 13 11 -10.7403 -9.6718 8 13 13 -0.0151 -15.4626 8 14 8 -1.7397 5.9223 8 14 10 -4.3514 0.7083 8 14 12 13.0288 2.8550 8 14 14 9.5204 -10.0753 8 15 9 4.2972 9.0851 8 15 11 30.0561 -25.5656 8 15 13 -12.4601 -26.4119 8 15 15 -24.3688 32.4945 8 16 8 16.1811 -13.8481 8 16 10 -22.8598 -18.5318 8 16 12 15.4033 5.5025 8 16 14 -7.2938 1.0546 8 16 16 5.1095 -9.5206 8 17 9 4.1908 -33.8714 8 17 11 5.8270 -19.2537 8 17 13 28.2484 0.0188 8 17 15 13.9604 16.9198 8 17 17 -4.6181 -19.3007 8 18 8 -41.5923 -14.6300 8 18 10 -10.6471 -1.4056 8 18 12 -3.5392 6.1337 8 18 14 14.3349 3.5425 8 18 16 2.5884 -4.4906 8 18 18 -7.6012 -1.5988 8 19 9 25.9673 -19.4144 8 19 11 2.6967 3.8823 8 19 13 -5.7442 22.6752 8 19 15 2.4477 6.8997 8 19 17 11.1725 -7.6082 8 20 8 0.0973 8.2859 8 20 10 20.3016 -17.4451 8 20 12 18.2235 2.7705 8 20 14 -13.6671 3.7572 8 20 16 17.0518 -16.3949 8 21 9 -11.3566 -2.7655 8 21 11 -15.0554 -6.1890 8 21 13 4.8876 2.2350 8 21 15 -12.2412 3.3652 8 22 8 -2.2127 -11.6743 8 22 10 2.3430 14.3163 8 22 12 -7.8961 9.6421 8 23 9 -20.7812 5.2891 8 23 11 3.6344 -28.6344 8 24 8 28.5405 10.3995 9 10 9 72.2489 -2.1893 9 11 10 -31.1897 4.8399 9 12 9 -68.1091 68.0760 9 12 11 5.4685 22.5293 9 13 10 -30.4788 42.6387 9 13 12 10.9540 11.7822 9 14 9 32.8273 7.0751 9 14 11 -26.8265 -21.1498 9 14 13 31.9285 27.3640 9 15 10 4.9933 -1.4567 9 15 12 -6.0969 -4.1367 9 15 14 22.7559 -25.9355 9 16 9 32.7097 -28.1766 9 16 11 -20.2921 5.7813 9 16 13 -9.0894 2.0266 9 16 15 26.8992 -10.9956 9 17 10 24.3910 15.4857 9 17 12 -0.0151 -3.8086 9 17 14 34.5261 15.3238 9 17 16 -7.6568 -4.9590 9 18 9 5.3279 29.4115 9 18 11 -35.0529 6.5706 9 18 13 7.8846 -1.9986 9 18 15 12.4563 -15.2173 9 18 17 -7.5434 -5.8372 9 19 10 -3.5889 -26.0924 9 19 12 -3.9653 2.6872 9 19 14 19.3796 -2.1207 9 19 16 -9.5661 8.3495 9 20 9 -41.2221 23.2995 9 20 11 3.1742 3.7538 9 20 13 -4.2816 -32.0166 9 20 15 8.7318 2.9020 9 21 10 4.3271 -5.6733 9 21 12 24.0911 -13.1438 9 21 14 1.2230 -6.1764 9 22 9 17.6797 25.4100 9 22 11 18.5944 -16.3757 9 22 13 -22.1467 -14.1838 9 23 10 4.7611 33.0971 9 24 9 -6.7664 -22.6657 10 10 10 29.5486 -13.2402 10 11 11 17.2474 -4.9614 10 12 10 -7.6053 31.3831 10 12 12 15.1906 1.6360 10 13 11 9.4589 15.8915 10 13 13 -34.1782 -10.5783 10 14 10 -41.3706 -12.5963 10 14 12 7.0304 -6.8558 10 14 14 -46.8971 6.0783 10 15 11 -5.0504 17.3819 10 15 13 4.8634 -21.5842 10 15 15 -12.2830 12.6661 10 16 10 -18.4951 -20.6610 10 16 12 -26.3367 8.1966 10 16 14 -4.7468 9.2932 10 16 16 17.2654 8.1002 10 17 11 6.9079 -55.0243 10 17 13 -7.0088 -21.3590 10 17 15 -3.2229 -4.9390 10 17 17 13.5151 -2.4803 10 18 10 11.0273 -3.1271 10 18 12 26.8826 26.7569 10 18 14 -5.9457 7.6164 10 18 16 8.9956 -15.2757 10 19 11 -11.6999 6.6841 10 19 13 12.8191 4.9941 10 19 15 -19.8133 -29.6166 10 20 10 -26.2288 -22.4038 10 20 12 1.6379 3.2525 10 20 14 -4.5098 -14.4792 10 21 11 -16.3966 11.7346 10 21 13 -17.3789 -0.6881 10 22 10 -10.9784 21.8668 10 22 12 4.6890 13.2298 11 12 11 -0.6528 -38.9967 11 13 12 -47.7415 14.1345 11 14 11 -73.4227 22.1643 11 14 13 -45.7835 -13.7930 11 15 12 0.1924 0.1519 11 15 14 9.2048 0.8450 11 16 11 -35.9776 5.0459 11 16 13 -4.9224 -3.1879 11 16 15 11.1509 31.9803 11 17 12 17.3829 -21.0194 11 17 14 47.5293 4.3777 11 17 16 7.7458 -6.2540 11 18 11 13.2097 -34.8787 11 18 13 24.4816 -20.1195 11 18 15 9.1598 -8.2828 11 18 17 -26.1176 -15.6110 11 19 12 8.5450 -25.0161 11 19 14 20.4668 -15.3695 11 20 11 9.0495 -16.8356 11 20 13 6.2272 3.9631 11 21 12 -4.1597 16.0592 11 22 11 0.1426 6.0196 12 13 13 8.1653 41.1185 12 14 12 15.1259 -31.5600 12 14 14 30.5583 24.3805 12 15 13 0.5203 47.6386 12 15 15 12.3729 4.2426 12 16 12 29.0232 -34.7981 12 16 14 -14.8978 -13.2453 12 16 16 10.9892 -6.1377 12 17 13 -9.0659 -17.6675 12 17 15 -13.4662 -11.7014 12 17 17 12.4478 -8.5215 12 18 12 -19.5987 21.3162 12 18 14 -19.2370 -16.1441 12 18 16 -10.1452 -21.4776 12 19 13 3.8306 1.1334 12 19 15 3.7691 -19.9942 12 20 12 3.1330 36.5163 13 14 13 -33.6065 -3.0059 13 15 14 -7.2966 21.4688 13 16 13 -19.0836 -33.8977 13 16 15 -12.5547 -20.5593 13 17 14 -18.6552 19.6545 13 17 16 22.6489 14.8174 13 18 13 6.1079 -6.5264 13 18 15 -1.5894 -4.6294 13 19 14 18.6303 -2.6982 13 20 13 9.3509 7.5598 14 14 14 52.6907 3.1076 14 15 15 -37.9681 -35.6726 14 16 14 14.4258 -10.2669 14 16 16 -23.0261 -8.1088 14 17 15 9.8139 -16.5606 14 18 14 -5.3890 -11.0210 15 16 15 25.0109 -3.8615 0 0 0 0.0 0.0 ; _shelx_fab_checksum 53067 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1/2, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.62807(8) 0.69940(6) 0.30060(6) 0.0231(10) Uani 1 2 d S TU P . . O1 O 0.6505(3) 0.7593(3) 0.3019(3) 0.061(3) Uani 1 1 d . U . . . O4 O 0.5995(3) 0.6434(3) 0.2905(3) 0.052(3) Uani 1 1 d . U . . . O2 O 0.6772(3) 0.6772(3) 0.3228(3) 0.0288(14) Uani 1 6 d S TU P . . N1 N 0.5738(5) 0.7291(4) 0.2709(4) 0.047(2) Uani 1 2 d DS TU P . . C1 C 0.5790(4) 0.5790(4) 0.2920(6) 0.036(2) Uani 1 2 d DS TU P . . C4 C 0.6752(4) 0.7759(5) 0.3248(4) 0.020(2) Uani 1 2 d S TU P . . C6 C 0.5164(4) 0.5164(4) 0.2902(7) 0.069(2) Uani 1 2 d DS TU P . . C8 C 0.6114(5) 0.6114(5) 0.2864(6) 0.035(2) Uani 1 2 d S TU P . . N2 N 0.4627(5) 0.7783(8) 0.2274(8) 0.079(6) Uani 0.5 1 d D U P A -1 H2 H 0.4556 0.8020 0.2372 0.095 Uiso 0.5 1 calc R U P A -1 C10 C 0.5013(6) 0.7611(5) 0.2389(5) 0.090(2) Uani 1 2 d DS TU P . . C12 C 0.5879(4) 0.5382(4) 0.2893(4) 0.048(4) Uani 1 1 d D U . . . H12 H 0.6156 0.5308 0.2864 0.058 Uiso 1 1 calc R U . . . C14 C 0.5576(4) 0.5048(5) 0.2905(7) 0.096(7) Uani 1 1 d D U . . . H14 H 0.5656 0.4771 0.2914 0.116 Uiso 1 1 calc R U . . . C16 C 0.5589(5) 0.7121(6) 0.2338(5) 0.097(6) Uani 1 1 d D U . . . H16 H 0.5712 0.6892 0.2213 0.116 Uiso 1 1 calc R U . . . C2 C 0.5239(5) 0.7321(5) 0.2166(5) 0.085(5) Uani 1 1 d D U . . . H2A H 0.5158 0.7256 0.1897 0.103 Uiso 1 1 calc R U . . . O3 O 0.4509(7) 0.7446(9) 0.1613(6) 0.109(8) Uani 0.5 1 d D U P A -1 C9 C 0.4352(7) 0.7575(8) 0.2001(6) 0.102(8) Uani 0.5 1 d D U P A -1 C5 C 0.4033(5) 0.7865(7) 0.1923(6) 0.088(9) Uani 0.5 1 d DG U P A -1 C11 C 0.3824(7) 0.8031(7) 0.2256(6) 0.092(10) Uani 0.5 1 d DG U P A -1 H11 H 0.3955 0.8052 0.2512 0.111 Uiso 0.5 1 calc R U P A -1 C3 C 0.3422(7) 0.8165(7) 0.2211(7) 0.125(17) Uani 0.5 1 d G U P A -1 H3 H 0.3281 0.8277 0.2436 0.151 Uiso 0.5 1 calc R U P A -1 C13 C 0.3229(5) 0.8134(8) 0.1832(8) 0.084(8) Uani 0.5 1 d G U P A -1 C7 C 0.3437(6) 0.7968(8) 0.1499(6) 0.079(9) Uani 0.5 1 d G U P A -1 H7 H 0.3306 0.7947 0.1243 0.095 Uiso 0.5 1 calc R U P A -1 C15 C 0.3839(6) 0.7834(7) 0.1544(5) 0.082(9) Uani 0.5 1 d DG U P A -1 H15 H 0.3980 0.7722 0.1319 0.099 Uiso 0.5 1 calc R U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0183(18) 0.0255(13) 0.0255(13) 0.0000(16) 0.0005(10) -0.0005(10) O1 0.065(6) 0.042(5) 0.076(6) 0.017(5) -0.044(6) -0.011(4) O4 0.013(5) 0.036(5) 0.105(8) 0.001(4) -0.016(5) -0.007(4) O2 0.0288(14) 0.0288(14) 0.0288(14) 0.0002(8) 0.0002(8) -0.0002(8) N1 0.047(3) 0.047(2) 0.047(2) 0.0002(14) -0.0005(10) 0.0005(10) C1 0.036(2) 0.036(2) 0.036(3) 0.0001(10) 0.0001(10) -0.0003(14) C4 0.020(2) 0.020(3) 0.020(2) 0.0003(10) 0.0002(14) -0.0003(10) C6 0.069(2) 0.069(2) 0.069(3) -0.0001(10) -0.0001(10) -0.0002(15) C8 0.035(2) 0.035(2) 0.035(3) -0.0005(10) -0.0005(10) 0.0000(14) N2 0.077(9) 0.091(16) 0.068(14) 0.009(10) 0.005(9) 0.012(9) C10 0.090(3) 0.090(2) 0.090(2) -0.0001(15) -0.0002(10) 0.0002(10) C12 0.050(9) 0.042(7) 0.052(11) -0.009(6) -0.019(7) 0.008(5) C14 0.067(8) 0.053(9) 0.17(2) -0.001(10) -0.001(8) -0.009(7) C16 0.087(9) 0.117(11) 0.086(9) -0.016(8) -0.018(7) 0.011(8) C2 0.082(8) 0.100(9) 0.074(9) -0.005(7) -0.010(7) 0.009(7) O3 0.088(14) 0.142(18) 0.097(12) -0.008(12) -0.015(10) 0.034(13) C9 0.098(10) 0.109(13) 0.100(12) -0.002(9) -0.006(8) 0.012(9) C5 0.081(11) 0.093(14) 0.091(11) 0.001(9) -0.004(8) 0.001(9) C11 0.083(12) 0.102(15) 0.091(12) 0.000(9) -0.005(9) 0.002(10) C3 0.091(14) 0.19(4) 0.100(15) -0.019(17) -0.013(11) 0.028(18) C13 0.078(11) 0.085(14) 0.089(12) 0.012(10) -0.001(9) -0.001(10) C7 0.073(13) 0.08(2) 0.090(14) 0.010(13) -0.002(10) -0.005(13) C15 0.076(11) 0.085(15) 0.086(11) 0.002(9) 0.000(8) -0.002(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Fe1 O1 85.0(6) . 20_566 ? O1 Fe1 N1 83.1(4) . . ? O1 Fe1 N1 83.1(4) 20_566 . ? O4 Fe1 O1 169.7(4) 20_566 20_566 ? O4 Fe1 O1 89.5(4) . 20_566 ? O4 Fe1 O1 89.5(4) 20_566 . ? O4 Fe1 O1 169.7(4) . . ? O4 Fe1 O4 94.5(6) 20_566 . ? O4 Fe1 N1 87.6(4) . . ? O4 Fe1 N1 87.6(4) 20_566 . ? O2 Fe1 O1 93.0(5) . 20_566 ? O2 Fe1 O1 93.0(5) . . ? O2 Fe1 O4 96.0(5) . . ? O2 Fe1 O4 96.0(5) . 20_566 ? O2 Fe1 N1 174.7(8) . . ? C4 O1 Fe1 131.1(10) . . ? C8 O4 Fe1 133.0(13) . . ? Fe1 O2 Fe1 119.77(10) 11_566 8_656 ? Fe1 O2 Fe1 119.77(10) 8_656 . ? Fe1 O2 Fe1 119.77(10) 11_566 . ? C16 N1 Fe1 118.1(9) . . ? C16 N1 Fe1 118.1(9) 20_566 . ? C16 N1 C16 123.4(18) 20_566 . ? C12 C1 C8 121.9(9) . . ? C12 C1 C8 121.9(9) 13 . ? C12 C1 C12 114.2(17) . 13 ? O1 C4 O1 127.3(18) 23_656 . ? C14 C6 C6 119.3(10) . 2_665 ? C14 C6 C6 119.3(10) 13 2_665 ? C14 C6 C14 121(2) . 13 ? O4 C8 O4 129(2) . 13 ? O4 C8 C1 113.4(12) 13 . ? O4 C8 C1 113.4(12) . . ? C10 N2 H2 119.0 . . ? C10 N2 C9 122(2) . . ? C9 N2 H2 119.0 . . ? C2 C10 N2 126.2(17) . . ? C2 C10 N2 115.9(14) 20_566 . ? C2 C10 C2 115.1(19) . 20_566 ? C1 C12 H12 117.3 . . ? C1 C12 C14 125.3(14) . . ? C14 C12 H12 117.3 . . ? C6 C14 C12 116.5(15) . . ? C6 C14 H14 121.7 . . ? C12 C14 H14 121.7 . . ? N1 C16 H16 122.3 . . ? N1 C16 C2 115.5(16) . . ? C2 C16 H16 122.3 . . ? C10 C2 C16 121.6(16) . . ? C10 C2 H2A 119.2 . . ? C16 C2 H2A 119.2 . . ? O3 C9 N2 118(3) . . ? C5 C9 N2 104.7(14) . . ? C5 C9 O3 107.3(16) . . ? C11 C5 C9 118.3(11) . . ? C11 C5 C15 120.0 . . ? C15 C5 C9 116.2(11) . . ? C5 C11 H11 120.0 . . ? C3 C11 C5 120.0 . . ? C3 C11 H11 120.0 . . ? C11 C3 H3 120.0 . . ? C13 C3 C11 120.0 . . ? C13 C3 H3 120.0 . . ? C7 C13 C3 120.0 . . ? C13 C7 H7 120.0 . . ? C13 C7 C15 120.0 . . ? C15 C7 H7 120.0 . . ? C5 C15 H15 120.0 . . ? C7 C15 C5 120.0 . . ? C7 C15 H15 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 O1 2.086(9) . ? Fe1 O1 2.086(9) 20_566 ? Fe1 O4 2.077(9) . ? Fe1 O4 2.077(9) 20_566 ? Fe1 O2 1.901(3) . ? Fe1 N1 2.238(16) . ? O1 C4 1.225(11) . ? O4 C8 1.120(11) . ? O2 Fe1 1.901(3) 11_566 ? O2 Fe1 1.901(3) 8_656 ? N1 C16 1.415(16) 20_566 ? N1 C16 1.416(16) . ? C1 C8 1.50(3) . ? C1 C12 1.365(14) . ? C1 C12 1.365(14) 13 ? C4 O1 1.224(11) 23_656 ? C6 C6 1.51(4) 2_665 ? C6 C14 1.397(16) 13 ? C6 C14 1.397(16) . ? C8 O4 1.120(11) 13 ? N2 H2 0.8700 . ? N2 C10 1.4300(15) . ? N2 C9 1.4300(15) . ? C10 C2 1.401(16) 20_566 ? C10 C2 1.401(16) . ? C12 H12 0.9400 . ? C12 C14 1.469(15) . ? C14 H14 0.9400 . ? C16 H16 0.9400 . ? C16 C2 1.428(15) . ? C2 H2A 0.9400 . ? O3 C9 1.4300(15) . ? C9 C5 1.4301(15) . ? C5 C11 1.3900 . ? C5 C15 1.3900 . ? C11 H11 0.9400 . ? C11 C3 1.3900 . ? C3 H3 0.9400 . ? C3 C13 1.3900 . ? C13 C7 1.3900 . ? C7 H7 0.9400 . ? C7 C15 1.3900 . ? C15 H15 0.9400 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Fe1 O1 C4 O1 13(3) . . . 23_656 ? Fe1 O4 C8 O4 8(4) . . . 13 ? Fe1 O4 C8 C1 163.2(11) . . . . ? Fe1 N1 C16 C2 179.1(13) . . . . ? N1 C16 C2 C10 -12(3) . . . . ? C1 C12 C14 C6 7(3) . . . . ? C6 C6 C14 C12 178.3(11) 2_665 . . . ? C8 C1 C12 C14 -174.0(17) . . . . ? N2 C10 C2 C16 -170(2) . . . . ? N2 C9 C5 C11 -55(3) . . . . ? N2 C9 C5 C15 150.9(16) . . . . ? C10 N2 C9 O3 -54(3) . . . . ? C10 N2 C9 C5 -173(2) . . . . ? C12 C1 C8 O4 178.3(17) 13 . . 13 ? C12 C1 C8 O4 19(3) 13 . . . ? C12 C1 C8 O4 -178.3(17) . . . . ? C12 C1 C8 O4 -19(3) . . . 13 ? C12 C1 C12 C14 -10(3) 13 . . . ? C14 C6 C14 C12 -3(4) 13 . . . ? C16 N1 C16 C2 -7(3) 20_566 . . . ? C2 C10 C2 C16 30(4) 20_566 . . . ? O3 C9 C5 C11 179(2) . . . . ? O3 C9 C5 C15 25(3) . . . . ? C9 N2 C10 C2 -176(2) . . . 20_566 ? C9 N2 C10 C2 24(4) . . . . ? C9 C5 C11 C3 -153(2) . . . . ? C9 C5 C15 C7 153(2) . . . . ? C5 C11 C3 C13 0.0 . . . . ? C11 C5 C15 C7 0.0 . . . . ? C11 C3 C13 C7 0.0 . . . . ? C3 C13 C7 C15 0.0 . . . . ? C13 C7 C15 C5 0.0 . . . . ? C15 C5 C11 C3 0.0 . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.375 -0.476 -0.579 25410.6 5182.6 ?