#------------------------------------------------------------------------------ #$Date: 2021-10-03 22:07:39 +0300 (Sun, 03 Oct 2021) $ #$Revision: 269463 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519036.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519036 loop_ _publ_author_name 'Zhang, Zong-Hui' 'Fang, Han' 'Xue, Dong-Xu' 'Bai, Junfeng' _publ_section_title ; Tuning Open Metal Site-Free ncb Type of Metal-Organic Frameworks for Simultaneously High Gravimetric and Volumetric Methane Storage Working Capacities. ; _journal_issue 37 _journal_name_full 'ACS applied materials & interfaces' _journal_page_first 44956 _journal_page_last 44963 _journal_paper_doi 10.1021/acsami.1c13757 _journal_volume 13 _journal_year 2021 _chemical_formula_moiety 'C51.631 H35.905 Fe3 N6 O16' _chemical_formula_sum 'C51 H30 Fe3 N6 O16' _chemical_formula_weight 1150.36 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-07-08 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 29.8619(7) _cell_length_b 29.8619(7) _cell_length_c 29.8619(7) _cell_measurement_reflns_used 9988 _cell_measurement_temperature 243(2) _cell_measurement_theta_max 50.37 _cell_measurement_theta_min 5.54 _cell_volume 26628.8(11) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 243.0 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0371 _diffrn_reflns_av_unetI/netI 0.0394 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 25 _diffrn_reflns_limit_h_min -29 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 17499 _diffrn_reflns_point_group_measured_fraction_full 0.933 _diffrn_reflns_point_group_measured_fraction_max 0.933 _diffrn_reflns_theta_full 50.367 _diffrn_reflns_theta_max 50.367 _diffrn_reflns_theta_min 4.187 _exptl_absorpt_coefficient_mu 2.839 _exptl_absorpt_correction_T_max 0.7500 _exptl_absorpt_correction_T_min 0.5291 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0960 before and 0.0766 after correction. The Ratio of minimum to maximum transmission is 0.7055. The \l/2 correction factor is Not present. ; _exptl_crystal_colour black _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 0.574 _exptl_crystal_description polyhedron _exptl_crystal_F_000 4672 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.615 _refine_diff_density_min -0.472 _refine_diff_density_rms 0.072 _refine_ls_abs_structure_details ; Flack x determined using 894 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.252(15) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 155 _refine_ls_number_reflns 2407 _refine_ls_number_restraints 219 _refine_ls_restrained_S_all 1.046 _refine_ls_R_factor_all 0.0757 _refine_ls_R_factor_gt 0.0718 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0990P)^2^+212.4569P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1986 _refine_ls_wR_factor_ref 0.2026 _reflns_Friedel_coverage 0.748 _reflns_Friedel_fraction_full 0.863 _reflns_Friedel_fraction_max 0.863 _reflns_number_gt 2269 _reflns_number_total 2407 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file am1c13757_si_002.cif _cod_data_source_block a _cod_original_cell_volume 26628.8(19) _cod_database_code 4519036 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.601 _shelx_estimated_absorpt_t_min 0.601 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups 2. Restrained distances C7-C7_$1 2.336 with sigma of 0.01 C6-C6_$1 2.34 with sigma of 0.01 N1-C7 = C7-C6 1.43 with sigma of 0.02 C7-C6 = C6-C5 1.43 with sigma of 0.02 O3-C4 1.43 with sigma of 0.02 N2-C4 1.43 with sigma of 0.02 C4-C13 1.43 with sigma of 0.02 C7-C5 2.477 with sigma of 0.04 N1-C6 2.477 with sigma of 0.04 C4-C12 \\sim C4-C14 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints N1 \\sim C7 \\sim C6 \\sim Fe1: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A C10 \\sim C11 \\sim C14 \\sim C13 \\sim C12 \\sim C9: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A Uanis(O1) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(C8) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(N2) \\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C9) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(C7) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C14) \\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C10) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 4. Rigid body (RIGU) restrains C1, C2, O2, Fe1 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C12, C9, C10, C11, C14, C13, C4, O3, N2, C5 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C6, C5, N2, C7, N1, Fe1 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Sof(C14)=Sof(C9)=0.5*FVAR(2) Sof(H14)=Sof(C11)=Sof(H11)=Sof(C10)=Sof(H9)=Sof(C12)=Sof(H12)=Sof(C13)=FVAR(1) Fixed Sof: O3(0.5) N2(0.5) H2(0.5) C4(0.5) 6.a Aromatic/amide H refined with riding coordinates: N2(H2), C3(H3), C6(H6), C7(H7), C14(H14), C11(H11), C9(H9), C12(H12) 6.b Fitted hexagon refined as free rotating group: C14(C11,C10,C9,C12,C13) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; a.res created by SHELXL-2014/7 TITL a_a.res in I-43m REM Old TITL a in I-43m REM SHELXT solution in I-43m REM R1 0.179, Rweak 0.050, Alpha 0.007, Orientation as input REM Flack x = 0.191 ( 0.008 ) from Parsons' quotients REM Formula found by SHELXT: C36 N24 O16 Fe3 CELL 1.54178 29.8619 29.8619 29.8619 90 90 90 ZERR 8 0.0007 0.0007 0.0007 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,+Z SYMM -Y,-X,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +X,+Z,+Y SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM +X,-Z,-Y SYMM +Z,+Y,+X SYMM +Z,-Y,-X SYMM -Z,+Y,-X SYMM -Z,-Y,+X SFAC C H Fe N O UNIT 408 240 24 48 128 EQIV $1 +Z,+Y,+X DFIX 2.336 0.01 C7 C7_$1 ISOR 0.001 0.002 O1 ISOR 0.001 0.002 C8 ISOR 0.001 0.002 N2 C1 C9 DFIX 2.34 0.01 C6 C6_$1 RIGU C1 C2 O2 Fe1 RIGU C12 C9 C10 C11 C14 C13 C4 O3 N2 C5 SADI C4 C12 C4 C14 DANG 2.477 C7 C5 DANG 2.477 N1 C6 DFIX 1.43 N1 C7 C7 C6 DFIX 1.43 C7 C6 C6 C5 DFIX 1.43 O3 C4 DFIX 1.43 N2 C4 DFIX 1.43 C4 C13 ISOR 0.01 0.02 C7 SIMU N1 C7 C6 Fe1 RIGU C6 C5 N2 C7 N1 Fe1 SIMU C10 C11 C14 C13 C12 C9 ISOR 0.01 0.02 C14 C11 C10 L.S. 20 PLAN 27 SIZE 0.2 0.2 0.2 TEMP -30.15 CONF FREE C4 C14 FREE C4 C12 FREE C5 C4_$1 FREE C5 C4 BOND $H list 4 MORE -1 ABIN fmap 2 acta REM REM REM WGHT 0.099000 212.456894 FVAR 0.20331 0.62104 FE1 3 0.333012 0.410785 0.333012 10.50000 0.02020 0.01722 = 0.02020 -0.00238 -0.00331 -0.00238 O1 5 0.358187 0.358187 0.358187 10.16667 0.01128 0.01128 = 0.01128 0.00024 0.00024 0.00024 O2 5 0.391820 0.443766 0.324405 11.00000 0.01680 0.04443 = 0.06286 0.01553 0.00024 -0.00038 PART -1 O3 5 0.173591 0.565548 0.257921 10.50000 0.09200 0.16358 = 0.32712 0.12058 0.08161 0.05446 PART 0 O4 5 0.334342 0.385365 0.266944 11.00000 0.08428 0.03321 = 0.03704 0.00692 -0.03145 -0.01464 N1 4 0.303648 0.468590 0.303648 10.50000 0.05531 0.02304 = 0.05531 0.00526 -0.02863 0.00526 PART -1 N2 4 0.237841 0.572694 0.232521 10.50000 0.05018 0.05039 = 0.05061 0.00024 -0.00007 0.00014 AFIX 43 H2 2 0.253137 0.581012 0.209162 10.50000 -1.20000 AFIX 0 PART 0 C1 1 0.431323 0.431323 0.322284 10.50000 0.01799 0.01799 = 0.01791 0.00058 0.00058 -0.00030 C2 1 0.466772 0.466772 0.322779 10.50000 0.01927 0.01927 = 0.05104 -0.00357 -0.00357 0.00071 C3 1 0.455903 0.510932 0.323455 11.00000 0.02835 0.10124 = 0.12171 0.02678 0.00683 -0.01996 AFIX 43 H3 2 0.425585 0.519386 0.323929 11.00000 -1.20000 AFIX 0 PART -1 C4 1 0.201875 0.600985 0.243820 10.50000 0.10292 0.12592 = 0.13271 0.05126 0.05339 0.05983 PART 0 C5 1 0.252591 0.533992 0.252591 10.50000 0.12026 0.08585 = 0.12026 0.03610 0.01020 0.03610 C6 1 0.242937 0.524005 0.298344 11.00000 0.14102 0.15485 = 0.13368 0.06543 0.03600 0.08943 AFIX 43 H6 2 0.218940 0.538817 0.312330 11.00000 -1.20000 AFIX 0 C7 1 0.267932 0.492880 0.323268 11.00000 0.11686 0.09938 = 0.12074 0.01728 0.00663 0.04483 AFIX 43 H7 2 0.260813 0.488085 0.353554 11.00000 -1.20000 AFIX 0 C8 1 0.354693 0.354693 0.251143 10.50000 0.01549 0.01549 = 0.01557 -0.00053 -0.00053 0.00020 PART -1 AFIX 66 C14 1 0.207240 0.646898 0.176522 20.50000 0.08104 0.07089 = 0.10466 0.00599 0.00406 0.00960 AFIX 43 H14 2 0.234789 0.633532 0.169222 21.00000 -1.20000 AFIX 65 C11 1 0.191250 0.682560 0.151239 21.00000 0.07909 0.07211 = 0.10817 0.00489 0.01662 0.02269 AFIX 43 H11 2 0.207985 0.693310 0.126842 21.00000 -1.20000 AFIX 65 C10 1 0.150513 0.702325 0.162034 21.00000 0.08781 0.08064 = 0.09396 0.02424 0.01822 0.03688 C9 1 0.125767 0.686429 0.198112 20.50000 0.06879 0.06877 = 0.06895 -0.00008 -0.00012 0.00028 AFIX 43 H9 2 0.098218 0.699796 0.205412 21.00000 -1.20000 AFIX 65 C12 1 0.141756 0.650767 0.223395 21.00000 0.08634 0.10858 = 0.12832 0.04752 0.02677 0.03093 AFIX 43 H12 2 0.125021 0.640017 0.247792 21.00000 -1.20000 AFIX 65 C13 1 0.182493 0.631002 0.212600 21.00000 0.08483 0.11041 = 0.15068 0.04599 0.02597 0.03570 AFIX 0 HKLF 4 REM a_a.res in I-43m REM R1 = 0.0718 for 2269 Fo > 4sig(Fo) and 0.0757 for all 2407 data REM 155 parameters refined using 219 restraints END WGHT 0.0988 212.6942 REM Highest difference peak 0.615, deepest hole -0.472, 1-sigma level 0.072 Q1 1 0.2704 0.4699 0.2704 10.50000 0.05 0.31 Q2 1 0.2624 0.7376 0.2624 10.16667 0.05 0.30 Q3 1 0.3172 0.3172 0.3172 10.16667 0.05 0.29 Q4 1 0.2925 0.2925 0.2925 10.16667 0.05 0.27 Q5 1 0.2404 0.6910 0.2404 10.50000 0.05 0.26 Q6 1 0.3131 0.4826 0.3131 10.50000 0.05 0.26 Q7 1 0.4616 0.4616 0.3838 10.50000 0.05 0.25 Q8 1 0.3154 0.3154 0.2731 10.50000 0.05 0.25 Q9 1 0.1252 0.6799 0.1776 11.00000 0.05 0.25 Q10 1 0.4211 0.4211 0.3089 10.50000 0.05 0.25 Q11 1 0.4445 0.4325 0.4325 10.50000 0.05 0.24 Q12 1 0.4036 0.5964 0.4036 10.16667 0.05 0.24 Q13 1 0.1812 0.7166 0.1812 10.50000 0.05 0.24 Q14 1 0.5000 0.5000 0.2067 10.25000 0.05 0.24 Q15 1 0.2206 0.5370 0.2683 11.00000 0.05 0.23 Q16 1 0.3376 0.4766 0.3110 11.00000 0.05 0.23 Q17 1 0.3559 0.4647 0.3079 11.00000 0.05 0.23 Q18 1 0.3886 0.5752 0.3163 11.00000 0.05 0.22 Q19 1 0.2966 0.5073 0.3632 11.00000 0.05 0.22 Q20 1 0.3782 0.4440 0.3782 10.50000 0.05 0.22 Q21 1 0.1986 0.7047 0.1906 11.00000 0.05 0.22 Q22 1 0.3727 0.4562 0.3065 11.00000 0.05 0.21 Q23 1 0.2969 0.3991 0.2486 11.00000 0.05 0.21 Q24 1 0.2384 0.4935 0.2384 10.50000 0.05 0.21 Q25 1 0.0608 0.5616 0.1605 11.00000 0.05 0.21 Q26 1 0.2458 0.6135 0.2458 10.50000 0.05 0.21 Q27 1 0.2887 0.5235 0.3740 11.00000 0.05 0.21 ; _shelx_res_checksum 45345 _shelx_hkl_file ; 0 2 -2 4.70 2.60 0 2 2 2.90 1.40 2 2 0 2.90 2.90 2 1 -3 4226.78 284.57 -1 3 2 4195.28 284.27 -2 3 1 4283.97 289.47 0 3 -3 3077.29 211.48 0 3 3 3037.50 210.88 3 3 0 3252.37 211.58 3 3 -2 2034.60 136.59 -2 3 3 2052.79 135.69 2 3 -3 2060.99 136.49 3 2 -3 2119.19 136.49 -2 3 -3 1763.72 136.39 0 0 -4 2821.12 195.38 0 4 0 2961.60 195.88 2 0 -4 557.54 36.50 0 4 2 509.15 36.60 0 4 -2 516.95 37.30 1 1 -4 2205.48 164.18 1 4 -1 2142.49 164.48 -1 4 1 2217.18 164.28 1 -1 -4 2621.34 163.68 1 4 1 2581.14 164.48 -1 4 -1 2626.84 164.68 -1 1 -4 2581.64 164.38 3 1 -4 751.62 50.59 4 3 -1 762.22 51.09 -1 4 3 752.12 49.99 1 4 -3 756.02 51.09 -1 4 -3 675.93 50.89 1 4 3 682.53 50.19 2 4 0 514.25 36.10 -2 4 0 497.75 36.00 0 2 -4 525.05 36.00 4 2 -2 2013.80 137.49 2 4 -2 2036.90 137.59 -2 4 2 2017.00 136.99 2 2 -4 2013.30 137.29 -3 4 1 773.22 50.79 1 3 -4 759.92 50.99 3 4 -1 768.12 51.19 -3 4 -1 680.63 50.99 3 4 1 702.23 50.99 -1 3 -4 700.53 50.99 4 3 -3 2450.65 162.88 4 -3 3 2393.86 161.88 -3 4 3 2274.27 161.98 3 -4 3 2403.16 161.98 3 -3 4 2291.27 161.88 3 3 -4 2394.46 162.68 3 4 -3 2375.56 162.88 -3 4 -3 2531.95 162.98 -3 3 -4 2409.76 162.88 0 4 4 7303.47 492.85 -2 4 4 9999.00 674.43 0 5 1 1417.26 96.29 1 0 -5 1423.76 95.79 0 5 -1 1467.55 96.69 -1 0 -5 1333.67 95.89 0 5 -3 874.31 60.09 0 -5 3 836.12 58.69 0 5 3 861.51 58.99 3 0 -5 860.81 58.89 1 5 0 1373.86 96.59 0 1 -5 1412.66 96.19 0 -1 -5 1398.86 95.69 -1 5 0 1465.35 96.69 1 -5 2 2252.07 160.58 2 1 -5 2258.17 160.88 -1 5 2 2247.08 160.88 1 5 -2 2293.27 161.48 2 -1 -5 2502.85 160.38 1 5 2 2466.35 161.08 -2 1 -5 2437.86 161.18 -1 5 -2 2522.05 161.58 1 -5 4 1564.44 117.39 5 4 -1 1564.94 118.49 1 5 -4 1624.54 118.59 -1 5 4 1542.65 117.29 4 1 -5 1625.74 117.99 5 -4 1 1602.64 117.39 5 -4 -1 1946.81 117.49 -1 5 -4 1991.60 118.89 -1 -5 4 1891.71 117.39 1 5 4 1945.91 117.69 2 5 -1 2196.68 159.38 2 -5 1 2222.48 158.58 1 2 -5 2154.48 158.98 -2 5 1 2192.68 158.98 -1 2 -5 2506.05 159.18 2 -5 -1 2530.85 158.68 -2 5 -1 2442.36 159.48 2 5 1 2491.45 159.28 -2 5 3 6171.78 369.16 3 2 -5 6029.10 369.56 2 5 3 4703.43 369.16 -2 5 -3 4944.31 369.76 0 3 -5 860.81 58.59 3 -5 0 801.42 57.59 3 5 0 846.72 58.69 0 -3 5 826.52 57.49 -3 5 0 866.31 58.59 -2 3 -5 4604.24 314.47 -3 5 -2 4598.34 314.67 3 5 2 4727.03 314.37 4 -3 5 762.32 53.49 5 4 -3 780.82 55.19 5 -4 3 808.82 53.59 -3 5 4 773.72 53.59 3 -5 4 780.52 53.59 3 5 -4 774.42 55.19 4 3 -5 762.52 54.79 1 -4 5 1565.54 119.59 -4 5 1 1574.04 120.29 1 4 -5 1548.45 120.49 4 -5 1 1574.54 119.69 4 5 -1 1603.14 120.79 4 5 1 1987.00 120.89 -1 -4 5 1973.20 119.69 -1 4 -5 1884.61 120.79 4 -5 -1 1943.21 119.79 -4 5 -1 1978.60 120.89 5 3 -4 835.62 56.39 4 -5 3 791.32 55.09 4 5 -3 766.62 56.59 5 -3 4 786.72 54.89 3 -4 5 796.02 54.99 3 4 -5 829.72 56.39 -3 4 5 790.52 54.49 -4 5 3 793.52 55.39 0 5 -5 6106.09 405.46 0 5 5 5860.91 404.26 5 5 0 5999.40 405.46 5 2 -5 2845.72 201.78 5 5 -2 3011.50 202.18 -2 5 5 2988.10 200.68 2 -5 5 2905.51 200.98 2 5 -5 2976.50 202.08 5 -2 5 3039.10 200.88 5 -5 2 3012.40 200.98 5 5 -4 6382.96 426.86 5 4 -5 6377.06 426.76 4 5 -5 6146.79 426.76 -4 5 5 6299.07 425.56 0 6 2 730.43 52.89 2 0 -6 775.42 52.29 0 -6 2 813.92 52.29 0 6 -2 714.53 53.69 0 6 4 1029.90 74.09 6 -4 0 1120.49 73.89 0 -6 4 1087.09 73.89 0 6 -4 1088.19 75.59 1 6 -1 4368.36 319.57 1 1 -6 4565.44 319.07 -1 -1 -6 4276.47 318.77 -1 6 1 4564.64 319.37 -1 6 -1 4841.62 319.77 -1 1 -6 5172.58 319.37 1 6 1 5061.29 319.57 1 -1 -6 4905.61 318.57 3 1 -6 4952.30 312.17 1 6 -3 4922.81 312.87 -1 6 3 5030.70 312.07 -1 6 -3 4443.56 312.67 6 -3 -1 4087.79 311.47 1 6 3 4240.68 311.97 1 6 -5 921.81 70.19 1 -6 5 921.31 68.69 6 5 -1 873.21 70.09 6 -5 1 941.61 68.69 -1 6 5 892.51 68.39 6 -5 -1 1132.29 68.79 -1 6 -5 1130.39 70.59 -1 -6 5 1069.19 68.59 1 6 5 1141.09 68.99 2 6 0 744.33 53.79 0 -2 -6 761.62 51.89 2 -6 0 785.32 52.69 0 2 -6 753.32 53.29 -2 6 0 774.72 53.69 2 6 -2 3198.38 235.48 2 2 -6 3203.18 234.98 -2 6 2 3237.98 234.98 -2 -6 2 3725.73 234.58 2 6 2 3650.43 235.28 -2 2 -6 3662.83 235.38 -2 6 -2 3593.94 235.68 6 -4 2 1799.92 126.69 6 4 -2 1987.30 128.19 -2 6 4 1952.50 126.89 2 6 -4 1941.11 128.19 4 -2 6 1969.50 126.69 2 -6 4 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995.00 65.79 9 -3 6 994.50 66.19 6 9 -3 948.01 69.19 6 -9 -3 938.41 66.59 -6 9 -3 1047.00 69.39 -6 -9 3 952.60 65.69 -3 6 -9 984.10 68.79 6 -9 5 1301.67 88.79 5 6 -9 1333.27 90.69 9 -5 6 1321.77 88.39 -6 9 5 1296.17 89.19 6 9 -5 1317.47 91.49 5 -6 9 1271.87 88.59 -5 6 -9 1226.08 90.89 -6 9 -5 1238.38 91.29 -7 6 9 220.58 16.90 6 -9 7 218.78 19.70 -6 9 7 218.78 18.40 9 -7 6 232.58 19.30 6 9 -7 238.18 25.20 7 -6 9 218.58 19.10 7 6 -9 242.68 23.60 9 7 -6 231.78 24.60 7 9 0 111.89 17.50 7 -9 0 97.09 12.50 -7 9 0 103.59 16.00 0 7 -9 110.49 16.50 -7 9 2 1037.00 80.29 2 -7 9 1041.60 78.79 7 9 -2 1012.10 81.09 2 7 -9 1046.00 80.99 7 -9 2 1031.40 78.99 -2 7 -9 1295.77 81.59 7 -9 -2 1270.37 79.19 -7 -9 2 1253.37 77.99 -7 9 -2 1333.07 81.69 4 7 -9 443.66 36.20 -7 -9 -4 422.26 31.50 7 -9 4 457.95 33.30 -7 9 4 432.76 34.20 9 -4 7 460.25 32.50 4 -7 9 437.56 33.00 7 9 -4 470.85 37.00 -4 7 -9 462.65 36.70 -7 9 -4 477.35 37.00 7 -9 -4 459.95 33.40 7 9 -6 226.48 24.90 9 -6 7 223.58 19.00 6 7 -9 254.97 24.40 -7 9 6 216.98 19.50 7 -9 6 216.28 19.70 6 -7 9 230.08 19.20 7 9 -8 1607.24 108.59 -9 8 7 1535.95 105.79 9 -8 7 1500.95 105.29 8 -7 9 1489.35 105.29 8 7 -9 1557.04 108.09 -7 9 8 1522.05 104.99 9 8 -7 1592.04 108.39 -8 7 9 1503.65 104.69 7 -9 8 1500.75 105.49 1 8 -9 512.55 38.80 1 -8 9 475.35 34.90 -8 9 1 489.05 37.90 8 9 -1 488.75 38.90 8 -9 1 453.55 35.20 -8 9 -1 498.05 38.60 8 -9 -1 486.75 35.30 -1 8 -9 487.55 38.50 3 8 -9 39.60 11.80 8 -9 3 46.80 8.30 8 9 -3 37.10 12.30 3 -8 9 48.10 8.30 -8 9 3 47.20 10.60 -3 8 -9 23.60 11.20 -8 9 -3 33.70 12.00 8 -9 -3 20.60 7.80 5 8 -9 1974.80 140.69 5 -8 9 1933.71 138.39 8 -9 5 1916.91 138.39 8 9 -5 1917.51 140.79 9 -5 8 1956.80 138.19 -8 9 5 1957.50 139.19 -8 -9 -5 1888.51 137.39 8 -9 -5 2072.19 138.59 -9 5 -8 2284.07 141.69 -5 8 -9 2139.99 141.19 -8 9 -5 2293.17 141.69 9 7 -8 1558.04 106.29 8 -9 7 1470.45 103.39 9 -7 8 1491.95 103.19 7 -8 9 1483.95 103.39 -9 7 8 1479.75 103.39 -7 8 9 1514.95 102.29 -8 9 7 1487.85 103.59 7 8 -9 1545.15 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1125.69 81.79 -3 5 -10 1460.15 84.69 5 -10 -3 1458.65 82.69 -5 -10 -5 1375.96 95.59 -5 10 5 1399.06 96.79 5 -10 5 1388.76 96.29 5 5 -10 1369.56 97.79 10 -5 5 1417.36 95.89 5 10 -5 1346.47 98.69 -5 5 -10 1459.95 98.49 -5 10 -5 1487.25 98.99 5 -10 -5 1407.96 96.39 -5 -10 5 1357.36 95.49 5 -10 7 141.29 15.30 10 -7 5 151.98 14.90 7 5 -10 143.19 19.00 5 10 -7 158.58 22.10 -5 10 7 150.38 14.10 10 -9 5 4578.54 310.37 5 -10 9 4655.83 310.47 -10 9 5 4579.04 311.57 5 10 -9 4606.94 312.97 -9 5 -10 4654.43 313.07 -10 9 -5 4758.42 313.47 10 -9 -5 4345.77 310.37 -5 10 -9 4452.55 312.97 0 6 -10 1248.78 90.19 -6 10 0 1310.77 90.39 6 10 0 1277.57 90.69 6 -10 0 1277.47 88.59 -6 -10 0 1315.27 87.59 6 10 -2 783.62 59.79 10 -2 6 784.82 56.29 2 6 -10 780.22 59.09 -6 -10 -2 787.32 56.09 -6 10 2 766.92 58.59 6 -10 2 767.72 57.19 -6 -10 2 835.32 56.09 -6 10 -2 893.91 59.89 6 10 2 907.61 59.69 -2 6 -10 855.71 59.49 6 -10 -2 836.82 57.29 10 -4 6 447.76 34.20 -6 10 4 449.76 36.00 4 6 -10 420.26 37.40 6 10 -4 441.86 38.80 -6 -10 -4 407.26 33.50 6 -10 4 430.16 34.90 -6 10 -4 562.94 39.20 -6 -10 4 535.35 33.70 6 -10 -4 556.94 35.50 -4 6 -10 554.14 38.40 6 6 -10 2248.38 153.88 6 -6 10 2231.58 151.88 -6 10 6 2274.47 152.38 6 10 -6 2229.78 154.58 10 -6 6 2184.38 151.68 6 -10 6 2198.08 151.98 8 6 -10 827.32 58.79 -10 8 6 780.32 56.79 6 -10 8 772.72 55.99 6 10 -8 834.42 60.19 -6 10 8 783.82 54.89 -8 6 10 791.12 54.19 8 -6 10 787.42 55.69 10 -8 6 778.02 55.69 10 -8 -6 718.83 55.89 -10 8 -6 811.02 60.09 -8 6 -10 799.52 60.19 -6 10 -8 798.22 59.69 7 -10 -1 177.98 16.90 -7 -10 1 166.98 13.30 -1 7 -10 197.38 21.00 7 10 1 174.88 21.10 -7 10 -1 178.38 20.90 -7 -10 -3 513.95 36.10 7 -10 3 514.45 37.90 7 10 -3 548.35 41.50 10 -3 7 515.85 36.90 3 7 -10 506.55 40.70 -7 10 3 522.45 39.50 7 10 -5 135.49 22.30 5 -7 10 146.79 15.20 -7 -10 -5 154.58 12.60 7 -10 5 143.19 15.30 10 -5 7 159.98 14.40 5 7 -10 140.99 20.00 -7 10 5 147.09 16.30 7 7 -10 217.88 24.30 7 10 -7 200.98 25.70 7 -10 7 215.08 19.10 7 -7 10 201.98 19.10 -7 10 7 213.68 18.40 10 -7 7 195.38 18.50 -10 -9 -7 1225.08 86.29 10 -9 7 1288.27 87.59 -7 10 9 1244.28 86.39 7 -10 9 1242.88 87.59 9 7 -10 1311.67 90.79 9 -7 10 1272.67 87.49 -10 9 7 1193.98 88.09 7 10 -9 1289.87 91.49 10 9 -7 1329.67 91.39 -9 7 10 1254.57 86.49 -8 10 0 1586.54 112.09 0 8 -10 1654.63 112.49 8 10 0 1607.84 112.49 8 -10 0 1570.14 110.09 8 10 -2 63.89 13.90 -8 10 2 60.29 12.20 2 -8 10 62.89 9.30 2 8 -10 61.69 13.10 8 -10 2 55.09 9.40 4 8 -10 248.78 24.90 8 -10 4 227.28 20.20 -8 -10 -4 213.68 16.70 4 -8 10 230.28 20.10 8 10 -4 234.18 25.90 -8 10 4 233.98 21.80 10 -4 8 219.58 18.80 8 -10 6 790.22 56.39 10 -6 8 804.42 55.99 6 8 -10 865.81 59.99 6 -8 10 790.92 56.29 -8 10 6 783.42 56.89 8 10 -6 812.22 60.79 -8 -10 -6 765.82 54.79 -8 10 -6 846.52 60.99 -6 8 -10 767.92 60.09 -10 6 -8 835.62 61.49 8 -10 -6 719.93 56.39 8 -10 8 148.59 16.90 -10 8 8 166.38 16.50 8 10 -8 190.08 24.60 8 -8 10 141.09 17.10 -8 10 8 152.58 15.20 10 -8 8 151.38 16.30 8 8 -10 146.49 23.20 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2079.09 138.49 9 10 -9 2106.29 142.19 -9 10 -9 1959.00 142.49 -9 9 -10 1973.80 142.49 -10 9 -9 1961.20 142.69 -10 10 0 190.08 22.90 0 -10 10 175.28 17.50 0 10 -10 192.98 24.40 10 -10 0 167.38 17.50 10 -10 2 5520.45 356.26 -10 10 2 5545.35 358.06 2 10 -10 5541.55 358.86 2 -10 10 5412.56 356.16 -2 10 -10 4881.31 358.36 10 -10 -2 4769.52 356.06 -10 10 -2 5132.19 358.46 4 -10 10 1297.37 85.09 10 -10 4 1298.17 85.09 -10 10 4 1236.38 86.59 4 10 -10 1278.67 88.69 -10 4 -10 1196.18 88.69 -4 10 -10 1173.78 88.69 10 -10 -4 1106.49 84.99 -10 10 -4 1209.38 88.89 10 -6 10 2332.97 155.38 10 10 -6 2321.87 158.98 -10 10 6 2361.16 156.68 10 -10 6 2251.87 155.58 6 -10 10 2358.06 155.68 6 10 -10 2416.96 159.08 10 -10 -6 2044.50 155.58 -6 10 -10 2135.99 158.78 -10 6 -10 2305.47 159.08 -10 10 -6 2234.58 159.18 -10 -10 -8 1853.31 135.79 10 -8 10 2003.20 137.09 -10 8 10 1941.01 136.39 8 10 -10 2018.30 140.79 -10 10 8 2002.80 137.39 10 -10 8 2044.40 137.29 8 -10 10 1957.50 137.29 10 10 -8 2098.19 141.09 -8 10 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1204.88 93.89 -12 12 0 4882.81 322.27 0 12 -12 4761.02 322.67 12 -12 0 4473.05 319.17 2 12 -12 364.76 39.50 -12 12 2 343.57 37.30 12 -12 2 365.36 33.10 -12 12 -2 502.05 40.60 12 -12 -2 476.35 33.50 -2 12 -12 479.55 40.50 4 -12 12 1306.97 85.69 12 -12 4 1326.87 85.69 -12 12 4 1317.27 88.09 4 12 -12 1300.37 90.49 -12 4 -12 1133.69 89.89 -4 12 -12 1136.79 89.99 12 -12 -4 1090.89 85.49 -12 12 -4 1145.09 90.39 12 -12 6 238.78 24.20 6 12 -12 235.28 32.50 -12 12 6 224.28 25.60 6 -12 12 227.08 24.10 -6 12 -12 324.37 34.70 -12 12 -6 334.37 34.70 -12 6 -12 340.77 34.80 8 -12 12 1499.75 100.79 12 -12 8 1250.97 100.29 -12 12 8 1418.46 100.89 8 12 -12 1524.65 105.99 -12 8 -12 1554.64 107.19 -8 12 -12 1457.65 106.39 12 -12 -8 1410.26 100.89 -12 12 -8 1454.95 106.59 10 -12 12 108.59 15.90 12 -12 10 94.29 14.30 10 12 -12 95.69 23.40 -12 10 -12 79.19 23.70 -10 12 -12 83.69 23.20 12 -12 -10 79.29 15.30 -12 12 -10 96.79 25.80 12 -12 12 2590.24 183.78 12 -12 -12 2762.02 184.68 -12 12 -12 2685.43 190.28 0 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25.70 20 -15 9 34.90 15.40 9 -20 -15 22.20 17.80 20 -15 -9 26.20 15.30 -9 20 -15 29.60 31.30 -20 15 -9 45.20 30.60 -15 9 -20 44.10 25.20 20 -17 9 194.18 29.10 9 -20 -17 228.18 34.40 17 -9 -20 201.08 31.80 -17 9 -20 202.88 33.00 -9 20 -17 277.77 42.40 20 -17 -9 200.98 30.80 -20 17 -9 283.27 49.90 20 -19 9 234.78 30.40 19 -9 -20 226.48 30.90 -19 9 -20 230.48 34.90 -9 20 -19 285.87 41.40 -20 19 -9 284.27 49.80 20 -19 -9 238.48 32.30 0 10 -20 108.59 22.10 10 -20 0 94.89 18.10 -10 20 0 114.69 24.40 10 -20 2 286.47 31.60 -10 20 2 277.27 36.60 2 10 -20 260.37 35.30 -2 10 -20 288.17 36.50 10 -20 -2 308.97 31.20 -10 20 -2 328.07 40.80 10 -20 4 201.48 28.50 4 10 -20 225.78 32.40 -10 20 4 211.48 30.70 10 -20 -4 237.38 29.30 -4 10 -20 221.48 34.40 -10 20 -4 196.38 32.30 10 -20 6 196.88 29.50 6 10 -20 225.98 33.30 20 -6 -10 255.17 24.30 -10 20 -6 237.08 41.60 -20 6 -10 221.98 35.30 10 -20 -6 255.07 30.80 -6 10 -20 294.57 36.80 10 20 -8 249.38 45.60 10 -20 8 301.57 33.20 -10 20 -8 306.37 47.60 20 -8 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130.19 33.10 19 -11 -20 267.07 32.70 -19 11 -20 281.77 44.40 20 -19 -11 269.17 33.20 -11 20 -19 318.67 49.99 -20 19 -11 325.17 43.70 11 -20 -19 283.17 37.20 -12 20 0 120.09 24.90 12 -20 0 159.08 27.20 0 12 -20 185.28 28.80 2 12 -20 2.30 19.30 -12 20 2 6.60 18.10 12 -20 2 11.60 16.50 -2 12 -20 7.50 19.10 12 -20 -2 5.80 18.10 -12 20 -2 9.50 21.90 4 12 -20 67.89 22.70 -12 20 4 74.89 20.40 12 -20 4 54.79 17.80 -20 4 -12 100.29 27.70 20 -4 -12 94.09 13.90 12 -20 -4 141.39 21.90 -4 12 -20 123.99 23.70 -12 20 -4 128.09 29.40 12 -20 6 81.79 18.20 6 12 -20 92.89 23.10 -12 20 -6 66.59 29.30 -6 12 -20 61.79 23.70 12 -20 -6 78.39 19.90 -20 6 -12 48.40 27.20 20 -6 -12 64.39 13.60 12 -20 8 102.29 19.60 20 -8 -12 104.29 16.50 -12 20 -8 71.79 31.50 -20 8 -12 85.69 33.70 -8 12 -20 92.89 26.50 12 -20 -8 69.59 19.90 12 -20 10 37.90 19.30 20 -10 -12 -0.90 13.50 -10 12 -20 1.30 24.70 -20 10 -12 11.10 29.90 12 -20 -10 -2.70 18.80 -12 20 -10 -10.20 24.20 -20 12 -12 302.57 43.40 20 -12 -12 242.28 30.20 -12 12 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444.66 36.50 -13 20 -7 415.36 54.29 13 -20 -7 437.56 41.10 -7 13 -20 434.96 49.40 13 -20 9 120.49 20.60 -9 13 -20 74.89 25.90 20 -9 -13 61.09 15.60 13 -20 -9 72.39 21.70 -20 9 -13 68.89 32.20 -13 20 -9 41.80 29.50 13 -20 11 111.69 22.10 13 -20 -11 91.19 21.00 20 -11 -13 150.38 19.80 -11 13 -20 99.69 27.00 -13 20 -11 87.89 29.90 -20 11 -13 122.39 33.10 13 -20 -13 3.10 16.90 20 -13 -13 5.70 14.40 -13 13 -20 11.90 25.70 -13 20 -13 -11.50 29.80 13 -13 -20 16.30 20.50 -20 13 -13 -17.10 28.30 20 -15 -13 76.39 18.10 13 -20 -15 61.49 19.20 -15 13 -20 119.09 31.50 -20 15 -13 136.99 34.80 -13 20 -15 110.69 34.10 15 -13 -20 98.79 23.30 -20 17 -13 12.20 25.60 13 -20 -17 18.50 20.00 20 -17 -13 14.60 16.10 -17 13 -20 22.60 24.50 17 -13 -20 22.30 18.60 -13 20 -17 32.60 31.60 14 -20 0 27.00 18.80 -14 20 0 20.40 21.20 0 14 -20 14.00 22.40 2 14 -20 181.68 28.90 -14 20 2 227.58 35.50 14 -20 2 204.68 29.90 -20 2 -14 172.88 30.30 -14 20 -2 179.28 30.40 14 -20 -2 190.48 29.30 -2 14 -20 242.98 39.20 4 14 -20 93.29 23.70 14 -20 4 57.79 16.60 -4 14 -20 66.19 25.00 14 -20 -4 62.69 18.70 -14 20 -4 47.30 26.20 -20 4 -14 68.49 27.60 6 14 -20 50.19 22.70 14 -20 6 65.19 19.20 -6 14 -20 51.49 27.10 -14 20 -6 32.70 25.80 14 -20 -6 35.10 19.80 -20 6 -14 29.40 27.40 20 -6 -14 32.10 13.50 14 -20 8 88.19 21.20 8 14 -20 86.39 24.70 -20 8 -14 56.89 26.10 -14 20 -8 89.99 30.00 14 -20 -8 105.29 22.30 -8 14 -20 72.99 25.60 20 -8 -14 135.89 17.90 20 -10 -14 102.59 17.80 -10 14 -20 80.39 30.40 -20 10 -14 111.19 33.40 14 -20 -10 68.69 21.40 -14 20 -10 125.99 35.10 14 -20 12 9.80 18.70 -12 14 -20 19.10 23.70 -14 20 -12 16.40 27.50 -20 12 -14 31.50 28.90 20 -12 -14 25.40 15.20 12 -14 -20 22.70 23.30 14 -20 -12 35.10 21.40 -20 14 -14 64.89 31.00 14 -14 -20 68.69 21.30 -14 20 -14 62.19 33.00 14 -20 -14 40.70 17.80 20 -14 -14 48.00 16.30 -14 14 -20 87.59 29.60 -14 20 -16 65.79 34.00 -16 14 -20 48.30 27.80 14 -20 -16 52.99 21.80 16 -14 -20 22.80 17.00 -20 16 -14 50.29 31.60 20 -16 -14 48.30 17.90 -1 15 -20 95.39 25.50 -15 20 -1 127.29 28.10 15 -20 -1 89.69 18.80 -20 1 -15 78.19 25.00 15 -20 3 27.50 16.20 3 15 -20 46.90 22.50 -15 20 3 57.69 20.30 -20 3 -15 43.20 27.20 -3 15 -20 34.20 22.90 -15 20 -3 40.10 25.30 15 -20 -3 47.90 18.50 5 15 -20 471.05 51.89 15 -20 5 457.55 44.20 15 -20 -5 482.75 44.80 -15 20 -5 503.15 56.79 -20 5 -15 521.95 55.89 20 -5 -15 501.05 40.20 -5 15 -20 518.75 53.99 7 15 -20 523.55 48.80 15 -20 7 447.26 40.30 -20 7 -15 391.06 52.59 15 -20 -7 350.96 41.30 20 -7 -15 407.66 36.80 -15 20 -7 402.96 54.99 -7 15 -20 428.86 51.79 -9 -15 -20 49.00 12.20 15 -20 9 35.70 16.60 9 -15 -20 16.40 21.60 -20 9 -15 38.90 27.10 -15 20 -9 35.70 30.20 20 -9 -15 36.80 15.20 -9 15 -20 28.60 26.30 15 -20 -9 31.60 19.60 15 -20 11 20.70 15.80 -15 20 -11 9.40 28.00 11 -15 -20 14.40 21.50 -20 11 -15 8.10 28.00 20 -11 -15 18.50 15.40 -11 15 -20 2.40 27.00 15 -20 -11 16.40 21.00 13 -15 -20 99.49 24.80 -13 15 -20 92.69 31.20 -15 20 -13 98.79 32.10 20 -13 -15 99.29 19.70 -20 13 -15 108.09 32.00 15 -20 -13 100.79 24.30 -15 20 -15 100.69 34.50 15 -15 -20 33.00 17.30 -15 15 -20 68.09 27.90 -20 15 -15 62.09 28.80 20 -15 -15 76.99 18.60 15 -20 -15 67.29 22.10 -20 0 -16 24.90 24.50 16 -20 0 24.20 18.60 -16 20 0 25.90 22.70 0 16 -20 26.90 24.80 2 16 -20 125.09 26.30 -16 20 2 159.08 26.20 16 -20 2 96.19 18.80 -20 -2 -16 151.78 27.60 -16 20 -2 49.60 25.40 -2 16 -20 78.19 27.20 16 -20 -2 45.60 18.50 -20 2 -16 100.49 28.80 16 -20 4 673.13 54.19 4 16 -20 748.93 63.09 -20 4 -16 662.13 63.99 16 -20 -4 565.04 54.19 -4 16 -20 685.13 63.79 20 -4 -16 652.43 50.49 -16 20 -4 654.03 65.09 16 -20 6 47.40 17.40 6 16 -20 81.99 25.70 -6 -16 -20 75.59 14.60 -6 16 -20 33.10 23.40 16 -20 -6 48.50 18.70 -20 6 -16 66.09 29.80 6 -16 -20 36.50 18.80 20 -6 -16 72.79 15.50 -16 20 -6 54.59 28.00 -8 -16 -20 759.92 54.89 8 16 -20 802.82 65.39 16 -20 8 757.52 58.99 20 -8 -16 723.53 56.79 -8 16 -20 732.73 69.49 16 -20 -8 698.03 59.99 8 -16 -20 689.33 61.49 -16 20 -8 772.72 72.29 -20 8 -16 709.03 69.39 16 -20 10 58.89 19.90 -10 16 -20 51.89 27.00 10 -16 -20 41.50 22.10 -16 20 -10 40.10 27.10 20 -10 -16 54.79 17.20 16 -20 -10 57.69 21.80 -20 10 -16 42.30 29.80 12 -16 -20 71.49 23.90 -20 12 -16 57.69 30.10 20 -12 -16 44.50 15.90 16 -20 -12 57.39 21.80 -12 16 -20 66.09 29.80 -16 20 -12 49.00 32.90 -14 16 -20 50.39 26.90 -20 14 -16 52.19 30.60 14 -16 -20 57.29 21.70 20 -14 -16 46.10 15.90 -16 20 -14 34.20 26.60 16 -20 -14 26.90 17.80 1 17 -20 46.10 26.60 17 -20 1 15.20 16.40 -20 -1 -17 40.00 22.40 -1 -17 -20 12.00 14.50 -17 20 1 30.50 22.20 17 -20 -1 72.69 20.00 -17 20 -1 54.79 25.20 -1 17 -20 88.39 28.90 -20 1 -17 87.79 27.20 1 -17 -20 69.99 18.50 -3 -17 -20 77.99 16.60 -20 -3 -17 71.99 23.60 -17 20 3 83.59 22.60 17 -20 3 68.89 18.00 3 17 -20 71.09 25.90 -3 17 -20 65.19 26.30 -17 20 -3 97.49 28.30 -20 3 -17 87.19 26.20 17 -20 -3 75.39 20.70 3 -17 -20 104.19 21.40 -20 -5 -17 302.77 40.80 -5 -17 -20 290.97 29.70 17 -20 5 267.27 33.60 5 17 -20 316.67 43.50 5 -17 -20 287.77 36.20 -20 5 -17 334.07 45.70 -5 17 -20 274.17 46.50 17 -20 -5 277.27 34.80 -17 20 -5 290.77 48.10 20 -5 -17 296.07 30.00 -7 -17 -20 320.17 30.40 17 -20 7 311.57 36.60 7 17 -20 304.87 44.40 -7 17 -20 341.87 49.60 -20 7 -17 360.76 48.90 20 -7 -17 371.46 33.50 7 -17 -20 364.86 40.30 -17 20 -7 400.26 53.19 17 -20 -7 353.66 38.50 17 -20 9 200.58 30.90 -17 20 -9 284.77 43.00 -20 9 -17 265.17 38.40 17 -20 -9 225.08 33.30 9 -17 -20 208.98 35.60 20 -9 -17 201.08 27.80 -9 17 -20 264.17 38.90 -17 20 -11 174.78 36.10 20 -11 -17 159.58 26.50 17 -20 -11 155.98 25.20 -20 11 -17 147.19 34.00 -11 17 -20 129.89 30.20 -13 17 -20 15.80 27.50 17 -20 -13 22.90 18.60 13 -17 -20 35.10 21.90 -20 13 -17 30.60 26.40 -17 20 -13 23.70 29.50 20 -13 -17 20.60 15.50 0 18 -20 135.59 30.20 -18 20 0 116.19 26.90 18 -20 0 73.59 18.40 0 -18 -20 150.58 21.50 -20 0 -18 99.99 25.00 2 18 -20 151.78 27.60 -20 2 -18 82.29 24.70 18 -20 -2 44.60 18.70 -18 20 -2 69.29 26.30 2 -18 -20 93.49 21.50 -2 18 -20 70.79 27.00 4 18 -20 46.00 27.10 18 -20 4 23.50 17.00 -4 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22.40 13.00 -3 -21 0 42.20 11.60 3 21 0 34.10 22.20 -3 21 0 25.80 18.70 3 21 -2 122.39 23.30 -3 21 -2 50.99 22.70 3 -21 -2 64.39 15.50 -3 -21 2 59.09 12.80 -2 3 -21 46.50 11.80 3 21 2 69.59 21.30 -3 -21 -4 57.79 13.20 3 21 -4 55.79 23.20 3 -21 4 59.79 16.60 -3 21 4 71.59 18.70 3 21 4 99.99 20.40 3 -21 -4 90.79 15.80 -4 3 -21 98.79 15.20 -3 -21 4 112.89 17.60 -3 21 -4 72.79 23.00 -3 -21 -6 1689.33 106.49 3 -21 6 1704.63 107.39 3 21 -6 1406.36 114.69 -6 3 -21 1468.65 108.19 -3 21 -6 1340.27 114.19 -3 -21 6 1477.55 105.99 3 -21 -6 1499.85 107.29 -3 -21 -8 129.29 20.20 3 -21 8 137.19 23.40 3 21 -8 114.39 31.40 -3 21 -8 115.09 30.60 -3 -21 8 90.89 14.70 3 -21 -8 91.09 17.20 -8 3 -21 118.49 19.30 -21 8 -3 76.59 26.40 21 -10 3 395.86 34.50 -21 10 3 380.56 46.40 3 -21 10 412.56 38.10 3 21 -10 371.16 52.29 -3 -21 -10 410.86 35.80 21 -10 -3 471.25 35.30 -3 21 -10 400.46 52.09 -10 3 -21 468.15 42.30 -21 10 -3 415.16 50.19 3 -21 -10 467.75 38.40 -3 -21 -12 15.40 12.80 3 21 -12 26.10 27.80 -21 12 3 18.60 21.00 21 -12 3 18.50 12.40 21 -12 -3 43.70 13.70 -12 3 -21 44.60 19.70 -21 12 -3 27.70 24.00 -3 21 -12 50.59 28.40 3 -21 -12 58.19 18.20 -3 -21 -14 116.89 17.50 3 21 -14 98.09 32.60 -14 -3 -21 98.19 20.40 -21 14 3 83.49 24.00 21 -14 3 105.69 16.70 -3 21 -14 93.99 30.50 -14 3 -21 100.79 23.70 21 -14 -3 121.19 17.80 3 -21 -14 151.18 21.40 -21 14 -3 74.69 27.70 -21 16 3 100.79 24.20 -3 -21 -16 94.59 16.00 -16 -3 -21 106.69 20.60 21 -16 3 89.99 16.70 3 21 -16 117.39 31.80 -16 3 -21 78.69 22.40 -21 16 -3 86.39 30.10 3 -21 -16 77.89 19.80 -3 21 -16 97.39 34.00 21 -16 -3 91.79 18.10 21 -18 3 383.06 36.90 -21 18 3 425.46 43.90 3 21 -18 381.96 51.89 -18 -3 -21 381.36 41.40 -3 -21 -18 391.36 35.20 -3 21 -18 379.96 54.29 -21 18 -3 399.36 51.69 -18 3 -21 387.56 45.10 21 -18 -3 384.26 37.60 3 -21 -18 373.16 38.40 3 21 -20 120.49 30.10 -3 -21 -20 117.99 16.30 21 -20 3 101.09 17.60 -3 21 -20 61.89 29.10 21 -20 -3 80.79 18.50 3 -21 -20 90.89 20.30 -21 20 -3 41.20 25.70 20 -3 -21 75.39 16.20 -20 3 -21 72.99 22.30 -4 21 1 75.59 20.30 4 21 -1 62.89 22.70 -4 -21 -1 69.39 13.00 4 -21 1 83.09 16.50 1 4 -21 67.89 13.20 4 -21 -1 123.69 18.10 -4 -21 1 106.39 17.10 4 21 1 85.39 22.50 -1 4 -21 93.09 14.30 -4 21 -1 133.19 25.60 4 21 -3 65.09 27.00 -4 21 3 78.09 21.00 4 -21 3 79.39 17.70 -4 -21 3 91.09 14.20 4 -21 -3 108.79 17.40 -4 21 -3 122.29 26.80 4 21 3 112.69 22.60 -3 4 -21 113.49 16.50 4 -21 5 331.37 34.20 -4 -21 -5 314.47 30.90 4 21 -5 292.37 45.50 -4 21 5 307.67 36.80 -4 -21 5 446.66 31.70 -4 21 -5 388.26 45.20 4 -21 -5 449.06 35.30 -5 4 -21 415.36 35.20 4 21 -7 615.54 67.39 4 -21 7 729.93 57.09 -4 -21 -7 702.13 54.79 -4 -21 7 817.72 55.09 -4 21 -7 670.03 66.79 -7 4 -21 798.72 59.69 4 -21 -7 802.32 57.29 -21 9 4 13.70 22.30 -4 -21 -9 31.60 13.00 4 21 -9 22.30 26.50 4 -21 9 14.30 14.80 -21 9 -4 27.20 25.60 -9 4 -21 25.40 16.70 4 -21 -9 33.60 17.00 -4 21 -9 19.60 25.50 21 -9 -4 22.10 11.60 -4 -21 -11 10.30 11.80 21 -11 4 13.40 11.70 4 21 -11 7.10 25.00 -21 11 4 4.50 21.40 4 -21 11 6.30 16.00 21 -11 -4 28.80 13.00 -11 4 -21 7.90 18.20 4 -21 -11 26.20 17.20 -21 11 -4 26.50 28.20 -4 21 -11 6.10 24.60 4 21 -13 104.29 30.20 21 -13 4 146.29 17.90 -21 13 4 116.89 25.00 -4 -21 -13 150.88 21.90 -21 13 -4 116.29 30.50 4 -21 -13 91.19 18.40 -13 4 -21 149.29 25.70 21 -13 -4 142.09 23.40 -4 21 -13 71.09 27.70 4 21 -15 114.89 34.20 -4 -21 -15 108.99 17.50 21 -15 4 136.09 19.30 -21 15 4 129.89 25.40 -4 21 -15 80.39 29.40 4 -21 -15 154.48 21.90 21 -15 -4 148.99 25.40 -15 4 -21 121.69 24.80 -21 15 -4 110.39 29.70 -4 -21 -17 16.00 13.20 21 -17 4 9.70 15.70 4 21 -17 17.00 28.60 -21 17 -4 14.50 27.60 21 -17 -4 21.40 16.10 -17 4 -21 15.20 21.60 4 -21 -17 21.00 17.50 -4 21 -17 40.60 31.40 21 -19 4 28.90 16.80 4 21 -19 24.60 27.50 4 -21 -19 63.59 19.10 -19 4 -21 78.09 23.30 -21 19 -4 83.59 28.20 21 -19 -4 74.89 18.90 19 -4 -21 91.59 17.00 -4 21 -19 72.99 29.10 5 -21 0 412.86 36.30 -5 -21 0 410.76 33.00 -5 21 0 418.26 44.60 5 21 0 415.66 46.20 0 5 -21 401.06 35.70 -5 -21 -2 379.36 31.30 5 -21 2 388.36 34.90 2 5 -21 374.06 33.40 5 21 -2 331.17 45.90 -5 21 2 379.46 41.40 5 21 2 413.36 43.10 -5 21 -2 426.76 44.70 -2 5 -21 381.56 35.00 -5 -21 2 365.46 31.20 5 -21 -2 417.16 35.60 5 -21 4 318.97 34.50 5 21 -4 289.77 45.90 -5 -21 -4 313.67 30.90 -5 21 4 326.17 38.80 -5 -21 4 448.46 31.60 5 -21 -4 451.25 35.70 -5 21 -4 426.26 46.50 -4 5 -21 434.56 36.30 -5 -21 -6 1013.80 70.69 5 -21 6 1029.50 73.19 5 21 -6 917.21 81.99 -5 21 -6 938.01 81.69 -6 5 -21 1042.70 75.69 -5 -21 6 969.60 70.79 5 -21 -6 1006.30 73.29 5 21 -8 211.08 34.80 5 -21 8 304.87 29.00 -5 -21 -8 284.77 24.30 -8 5 -21 225.58 32.60 21 -8 -5 226.38 23.20 5 -21 -8 225.98 28.90 -21 8 -5 164.08 32.40 -5 21 -8 230.98 37.30 -5 -21 -10 339.67 30.60 21 -10 5 320.87 30.20 5 -21 10 355.06 35.20 -21 10 5 348.97 41.60 5 21 -10 292.07 49.60 -5 21 -10 470.75 52.09 -21 10 -5 439.96 50.49 -5 -21 -12 226.88 24.30 21 -12 5 210.08 24.90 -21 12 5 202.68 35.40 5 -21 12 211.48 30.10 5 21 -12 152.98 33.30 -21 12 -5 310.67 46.50 -5 21 -12 280.17 47.40 -21 14 5 130.89 23.90 5 21 -14 73.09 28.20 -5 -21 -14 129.39 20.80 21 -14 5 142.29 19.00 -5 21 -14 225.28 35.30 -5 -21 -16 -0.10 12.30 5 21 -16 -9.80 28.00 21 -16 5 12.20 14.90 -21 16 5 8.80 5.70 5 -21 -16 0.80 18.00 -16 5 -21 -8.70 20.70 21 -16 -5 11.90 15.90 -5 21 -16 9.00 26.30 -21 16 -5 0.50 25.00 5 21 -18 551.64 59.09 21 -18 5 543.05 44.50 -5 -21 -18 563.84 41.50 5 -21 -18 475.95 46.20 -21 18 -5 501.85 58.09 -5 21 -18 530.15 61.29 21 -18 -5 461.55 45.20 -18 5 -21 501.05 53.29 21 -20 5 126.19 20.00 -5 -21 -20 136.69 20.50 5 21 -20 118.99 28.90 5 -21 -20 151.38 22.50 -5 21 -20 180.78 34.20 21 -20 -5 151.98 21.30 -21 20 -5 197.38 34.00 -20 5 -21 135.69 26.90 20 -5 -21 173.18 24.60 6 21 -1 121.09 27.30 6 -21 1 143.79 20.10 -6 -21 -1 153.58 17.30 1 6 -21 138.49 22.70 -6 21 1 131.19 23.30 6 -21 -1 139.29 23.50 -6 21 -1 108.99 23.30 -1 6 -21 127.19 23.30 -6 -21 1 130.99 17.30 6 21 1 121.29 25.80 6 -21 3 1729.73 113.49 6 21 -3 1648.14 120.79 3 6 -21 1637.24 113.79 -6 21 3 1688.93 116.99 -6 -21 -3 1716.43 111.29 -6 -21 3 1493.85 110.99 -6 21 -3 1478.75 118.69 -3 6 -21 1525.95 114.79 6 -21 -3 1536.25 113.09 -6 -21 -5 1020.80 70.19 6 -21 5 1030.00 72.89 6 21 -5 942.91 81.89 -6 21 5 1041.50 74.79 -5 6 -21 1019.70 75.69 -6 21 -5 870.71 80.09 6 -21 -5 972.50 72.99 -6 -21 5 975.20 70.09 6 -21 7 1380.66 98.59 6 21 -7 1217.48 107.09 -6 -21 -7 1399.76 96.59 6 -21 -7 1478.95 99.09 -21 7 -6 1263.77 106.79 -6 21 -7 1332.67 106.89 -7 6 -21 1564.74 102.79 6 -21 9 978.40 70.99 6 21 -9 834.02 80.59 -21 9 6 842.62 74.79 -6 -21 -9 907.71 67.79 -6 21 -9 920.31 81.39 21 -9 -6 1026.40 68.49 -9 6 -21 999.70 75.39 -21 9 -6 959.40 81.49 6 -21 -9 1020.20 70.99 21 -11 6 97.29 15.00 -21 11 6 83.99 22.10 6 -21 11 100.99 19.10 -6 -21 -11 115.99 19.00 6 21 -11 79.69 32.50 21 -11 -6 109.59 16.10 -21 11 -6 96.99 30.80 -11 6 -21 117.69 25.40 -6 21 -11 108.09 32.90 6 -21 -11 104.29 19.60 21 -13 6 2.40 13.20 6 21 -13 15.90 28.20 -6 -21 -13 12.90 11.60 21 -13 -6 2.50 14.20 -21 13 -6 11.90 24.90 6 -21 -13 5.10 16.20 -13 6 -21 4.00 19.20 -6 21 -13 13.50 27.10 21 -15 6 225.18 26.90 -6 -21 -15 208.28 22.70 6 21 -15 192.98 35.10 -15 6 -21 192.38 29.60 -6 21 -15 142.39 32.40 21 -15 -6 195.98 27.70 -21 15 -6 239.58 38.70 6 -21 -15 191.68 31.20 21 -17 6 850.41 61.99 6 21 -17 826.62 74.79 -6 -21 -17 866.51 59.09 21 -17 -6 756.42 62.19 -6 21 -17 827.22 76.79 -17 6 -21 779.22 69.39 6 -21 -17 727.23 63.69 -21 17 -6 824.32 74.59 6 21 -19 282.27 46.10 -6 -21 -19 266.57 28.00 21 -19 6 273.77 32.70 -21 19 -6 363.76 49.99 6 -21 -19 324.97 36.90 -6 21 -19 355.86 52.29 21 -19 -6 367.96 35.00 19 -6 -21 344.47 32.70 -19 6 -21 364.16 44.10 7 -21 0 671.63 51.99 -7 -21 0 666.33 48.30 -7 21 0 644.04 58.79 7 21 0 643.24 60.79 0 7 -21 698.33 54.09 7 -21 2 556.54 44.60 -7 21 2 548.95 49.90 -7 -21 -2 577.24 40.10 2 7 -21 568.54 45.20 7 21 -2 458.85 54.19 -7 21 -2 530.45 52.39 7 -21 -2 559.54 44.60 -7 -21 2 450.65 39.60 -2 7 -21 546.45 46.90 -7 -21 -4 643.64 52.49 7 -21 4 733.13 56.79 7 21 -4 673.53 66.39 4 7 -21 699.83 56.79 -7 21 4 718.53 59.69 -7 21 -4 733.43 64.99 7 -21 -4 772.72 56.89 -7 -21 4 805.92 52.99 -4 7 -21 785.32 59.59 7 21 -6 1211.98 107.39 -7 -21 -6 1414.16 96.59 7 -21 6 1390.56 99.29 -6 7 -21 1487.35 103.19 -7 21 -6 1279.87 106.39 7 -21 -6 1514.25 99.89 -21 8 7 130.99 23.90 7 -21 8 94.99 18.90 7 21 -8 110.99 31.30 -7 -21 -8 114.89 17.10 -21 8 -7 102.99 28.40 -8 7 -21 146.79 24.10 7 -21 -8 156.28 26.10 21 -8 -7 165.48 19.00 -7 21 -8 115.69 29.80 7 -21 10 402.66 38.40 7 21 -10 333.57 51.79 -7 -21 -10 379.96 32.10 21 -10 7 391.46 33.50 -21 10 7 404.06 41.70 -21 10 -7 378.86 51.69 21 -10 -7 416.36 34.30 -10 7 -21 434.66 44.10 -7 21 -10 374.16 53.49 7 -21 -10 451.95 39.10 7 21 -12 364.36 52.29 -7 -21 -12 409.56 31.10 7 -21 12 405.26 38.20 21 -12 7 431.86 33.40 7 -21 -12 310.97 37.80 -12 7 -21 347.67 43.90 -7 21 -12 301.67 53.59 21 -12 -7 342.17 34.40 -21 12 -7 294.17 50.19 7 21 -14 383.76 52.69 -7 -21 -14 392.26 29.90 21 -14 7 399.86 33.00 -7 21 -14 287.37 53.49 21 -14 -7 296.87 33.90 -14 7 -21 275.77 42.80 7 -21 -14 322.27 37.90 -21 14 -7 297.47 50.89 7 21 -16 69.99 27.10 21 -16 7 87.89 16.60 -7 21 -16 76.79 34.60 21 -16 -7 45.70 16.90 -21 16 -7 53.89 30.00 -16 7 -21 36.60 24.90 7 -21 -16 55.89 19.20 7 21 -18 351.26 48.90 21 -18 7 319.27 34.60 -7 21 -18 385.26 53.69 21 -18 -7 378.36 37.40 7 -21 -18 351.86 39.40 -21 18 -7 381.96 52.89 -18 7 -21 365.76 44.10 18 -7 -21 380.36 36.90 20 -7 -21 38.10 15.00 7 -21 -20 33.40 18.30 -7 21 -20 34.80 26.80 -21 20 -7 44.90 28.10 -20 7 -21 40.60 23.10 21 -20 -7 48.90 17.70 8 21 -1 135.19 30.10 -8 21 1 153.98 25.90 8 -21 1 138.89 25.20 1 8 -21 160.18 28.30 -8 -21 -1 149.19 16.90 -1 8 -21 216.98 30.20 -8 -21 1 201.28 17.70 8 -21 -1 230.38 26.80 -8 21 -1 212.18 35.30 3 8 -21 141.29 21.30 -8 21 3 112.99 21.80 8 21 -3 101.69 27.10 -8 -21 -3 118.39 14.60 8 -21 3 146.99 20.50 -3 8 -21 125.09 22.00 -8 21 -3 78.59 24.10 8 -21 -3 83.59 18.30 -8 -21 -5 300.57 22.80 5 8 -21 303.37 31.90 8 21 -5 264.67 44.60 -8 21 -5 193.58 33.60 8 -21 -5 220.98 30.80 -5 8 -21 228.38 34.80 -8 -21 -7 115.09 17.00 8 21 -7 103.79 31.00 8 -21 7 146.49 21.60 -8 21 -7 129.29 31.40 -21 7 -8 135.39 30.20 8 -21 -7 188.88 27.60 -7 8 -21 157.58 24.20 -8 -21 -9 111.59 18.80 8 -21 9 91.29 19.60 8 21 -9 56.89 27.70 -21 9 -8 87.89 29.70 8 -21 -9 121.39 20.60 -9 8 -21 160.18 26.60 -8 21 -9 137.59 32.90 21 -9 -8 131.69 20.00 8 -21 11 49.00 17.80 8 21 -11 35.30 29.10 -8 21 -11 29.20 27.00 8 -21 -11 46.20 17.80 -11 8 -21 49.10 22.40 -21 11 -8 35.50 30.70 21 -11 -8 35.50 13.50 8 21 -13 398.66 54.69 21 -13 8 443.06 36.40 -8 21 -13 389.36 56.99 21 -13 -8 404.46 37.50 8 -21 -13 408.96 41.30 -21 13 -8 425.66 55.49 -13 8 -21 406.06 46.90 21 -15 8 7.40 14.30 8 21 -15 17.40 28.40 -8 21 -15 9.30 31.90 8 -21 -15 7.20 19.60 21 -15 -8 5.00 16.30 -15 8 -21 0.40 21.80 -21 15 -8 11.60 29.30 21 -17 8 155.98 25.60 8 21 -17 208.88 34.50 21 -17 -8 155.98 27.50 -17 8 -21 137.29 27.40 -8 21 -17 167.28 37.90 -21 17 -8 123.99 30.20 8 -21 -17 127.89 23.90 17 -8 -21 148.79 22.40 21 -19 8 96.39 17.50 -21 19 -8 107.89 32.80 21 -19 -8 88.89 18.60 8 -21 -19 61.49 19.60 -19 8 -21 86.19 25.70 -8 21 -19 70.99 30.60 19 -8 -21 78.99 18.20 9 -21 0 6.10 15.40 0 9 -21 16.50 17.10 -9 21 0 26.70 22.20 -9 21 2 158.58 25.10 2 9 -21 176.38 29.50 9 -21 2 208.58 26.50 -2 9 -21 189.38 31.70 -9 21 -2 184.08 31.00 9 -21 -2 132.69 20.90 -9 21 4 15.20 16.60 4 9 -21 32.00 17.60 9 -21 4 22.90 15.70 9 21 -4 11.70 26.30 -4 9 -21 20.80 17.80 9 -21 -4 42.70 18.30 -9 21 -4 6.90 22.00 6 9 -21 942.41 72.49 9 -21 6 883.81 70.09 9 21 -6 795.82 79.79 -21 6 -9 954.60 81.09 -6 9 -21 1021.30 75.49 -9 21 -6 921.21 79.89 9 -21 -6 1027.60 70.99 9 21 -8 72.69 29.70 9 -21 8 102.09 18.80 -21 8 -9 68.79 26.60 -8 9 -21 142.19 25.10 -9 21 -8 106.29 30.60 21 -8 -9 124.69 19.10 9 -21 -8 89.09 18.40 9 -21 10 282.17 31.10 9 21 -10 179.78 33.10 -9 21 -10 171.68 34.30 21 -10 -9 276.27 26.70 -10 9 -21 252.27 39.40 -21 10 -9 245.28 40.00 9 -21 -10 261.97 32.40 9 21 -12 15.20 27.40 9 -21 12 32.60 18.90 -9 21 -12 27.40 27.90 21 -12 -9 53.49 16.00 -21 12 -9 32.10 27.00 9 -21 -12 28.30 20.20 -12 9 -21 52.89 24.30 9 21 -14 182.68 33.90 -14 9 -21 138.49 28.00 -9 21 -14 127.09 32.20 -21 14 -9 117.89 29.60 21 -14 -9 116.89 18.60 9 -21 -14 105.89 21.70 9 -21 -16 66.29 19.40 -16 9 -21 68.19 24.80 -21 16 -9 70.19 26.90 21 -16 -9 79.39 18.40 -9 21 -16 140.79 36.80 16 -9 -21 102.19 22.30 21 -18 -9 740.73 58.89 -18 9 -21 740.93 66.99 -21 18 -9 786.12 72.49 9 -21 -18 726.23 61.09 18 -9 -21 731.73 59.19 10 -21 1 43.00 17.20 1 10 -21 74.59 21.10 -10 21 1 44.90 20.60 -1 10 -21 106.89 23.40 -10 21 -1 101.99 26.00 10 -21 -1 89.79 18.10 10 -21 3 390.76 39.30 -10 21 3 422.76 43.40 3 10 -21 410.36 42.60 -3 10 -21 434.26 43.70 10 -21 -3 467.05 40.20 -10 21 -3 418.16 48.60 5 10 -21 359.16 43.80 -5 10 -21 531.55 47.30 -21 5 -10 450.45 54.59 -10 21 -5 492.15 52.99 10 -21 -5 479.65 42.00 10 21 -7 336.47 50.69 10 -21 7 377.26 38.50 -21 7 -10 389.36 52.49 -7 10 -21 424.06 45.10 -10 21 -7 406.86 52.29 21 -7 -10 421.26 33.20 10 -21 -7 403.06 39.80 10 21 -9 251.07 45.60 10 -21 9 289.27 32.80 21 -9 -10 276.77 26.90 10 -21 -9 243.58 32.20 -21 9 -10 207.48 36.80 -9 10 -21 268.87 38.50 -10 21 -9 268.27 48.40 -11 10 -21 304.57 42.00 -10 21 -11 210.08 37.10 -21 11 -10 186.78 35.40 21 -11 -10 278.77 28.40 10 -21 -11 280.07 34.10 -10 21 -13 235.58 40.20 -13 10 -21 147.69 28.30 -21 13 -10 225.38 38.30 21 -13 -10 188.38 27.40 10 -21 -13 189.58 32.50 -21 15 -10 185.38 37.10 10 -21 -15 116.29 23.40 -15 10 -21 165.68 31.70 15 -10 -21 144.09 23.80 21 -15 -10 160.38 26.60 -10 21 -15 152.18 33.80 10 -21 -17 91.39 19.90 -17 10 -21 122.79 27.30 -10 21 -17 135.79 31.90 17 -10 -21 122.29 21.00 -21 17 -10 183.68 36.70 21 -17 -10 159.38 26.40 -11 21 0 729.93 63.99 0 11 -21 705.33 61.39 11 -21 0 751.82 57.99 11 -21 2 158.08 26.20 11 -21 -2 80.59 18.60 -11 21 -2 85.09 25.10 -2 11 -21 105.49 23.80 4 11 -21 0.70 19.00 11 -21 4 8.80 15.40 -21 4 -11 20.10 23.70 -4 11 -21 38.50 21.80 11 -21 -4 5.30 17.20 21 -4 -11 -0.20 2.10 -11 21 -4 23.90 23.90 11 -21 6 81.49 17.90 6 11 -21 110.79 22.60 -6 11 -21 112.99 25.30 -21 6 -11 73.99 28.80 11 -21 -6 112.29 21.80 -11 21 -6 105.89 31.30 11 -21 8 30.70 16.90 21 -8 -11 49.70 13.60 -11 21 -8 17.70 23.90 -21 8 -11 35.40 30.50 -8 11 -21 35.10 22.10 11 -21 -8 60.89 22.00 -11 21 -10 306.27 51.39 -21 10 -11 289.47 42.60 -10 11 -21 297.87 43.30 21 -10 -11 257.57 28.90 11 -21 -10 315.17 36.20 11 -21 12 399.26 36.90 -11 21 -12 334.37 54.99 11 -21 -12 299.67 37.80 -21 12 -11 323.57 51.79 -12 11 -21 282.17 46.10 21 -12 -11 328.67 33.30 -21 14 -11 85.99 30.80 11 -21 -14 50.29 20.30 14 -11 -21 93.09 22.80 -11 21 -14 81.99 34.90 21 -14 -11 59.69 16.50 -14 11 -21 56.99 24.20 21 -16 -11 119.29 19.70 11 -21 -16 53.99 20.00 16 -11 -21 87.19 21.00 -21 16 -11 95.49 28.90 -11 21 -16 108.29 34.80 -16 11 -21 107.49 26.30 21 -18 -11 63.99 18.30 -11 21 -18 63.79 29.50 -21 18 -11 45.10 28.90 18 -11 -21 47.70 17.40 -18 11 -21 45.90 23.80 11 -21 -18 39.20 21.30 12 -21 1 114.19 19.80 1 12 -21 165.08 26.40 -12 21 1 128.39 25.00 -12 21 3 4.50 18.70 12 -21 3 7.30 17.60 3 12 -21 24.50 19.90 -12 21 -3 42.30 25.80 -3 12 -21 41.90 21.90 -21 3 -12 39.60 23.90 12 -21 -3 42.80 16.90 5 12 -21 203.08 35.70 12 -21 5 183.18 29.40 -21 5 -12 292.07 45.80 -12 21 -5 262.87 43.50 7 12 -21 422.56 41.10 12 -21 7 375.46 36.80 -12 21 -7 275.47 49.10 -21 7 -12 334.77 50.99 -7 12 -21 309.17 44.30 12 -21 -7 320.67 37.40 21 -7 -12 320.57 30.60 12 -21 9 40.40 20.00 21 -9 -12 53.29 14.40 -12 21 -9 36.30 27.10 -9 12 -21 43.40 24.20 12 -21 -9 33.30 18.40 -21 9 -12 22.20 30.60 12 -21 11 395.86 37.50 -11 12 -21 347.87 45.90 -21 11 -12 339.27 52.59 12 -21 -11 299.87 38.50 -12 21 -11 323.77 52.89 21 -11 -12 319.77 32.70 12 -21 -13 134.09 24.10 21 -13 -12 105.89 18.90 -21 13 -12 157.08 36.10 -12 21 -13 160.28 37.70 13 -12 -21 136.79 24.50 -13 12 -21 122.59 28.10 -21 15 -12 34.60 27.10 15 -12 -21 31.20 20.60 -15 12 -21 40.60 25.70 21 -15 -12 37.90 17.30 12 -21 -15 33.00 20.90 -12 21 -15 20.90 28.70 -17 12 -21 170.78 31.00 17 -12 -21 170.78 30.20 21 -17 -12 193.38 28.10 -12 21 -17 198.08 36.90 -21 17 -12 253.67 40.10 12 -21 -17 186.88 27.70 13 -21 0 39.00 17.30 -13 21 0 77.49 24.90 0 13 -21 40.20 21.00 -13 21 2 104.39 23.00 2 13 -21 119.99 25.20 13 -21 2 65.59 17.50 13 -21 -2 64.59 19.50 -2 13 -21 70.99 23.60 -21 2 -13 57.89 27.20 -13 21 -2 61.79 23.90 13 -21 4 113.59 21.00 4 13 -21 128.89 25.80 13 -21 -4 108.39 21.00 -13 21 -4 125.79 30.50 -4 13 -21 150.58 29.00 -21 4 -13 106.79 27.30 6 13 -21 9.60 21.20 13 -21 6 11.10 16.70 -13 21 -6 8.40 28.90 13 -21 -6 1.80 20.00 -21 6 -13 6.00 27.50 -6 13 -21 17.00 21.20 13 -21 8 366.26 39.40 21 -8 -13 389.16 34.60 -8 13 -21 412.76 48.00 -13 21 -8 382.06 53.19 -21 8 -13 391.16 53.59 13 -21 -8 415.56 40.80 -21 10 -13 183.38 36.60 -10 13 -21 204.38 32.90 21 -10 -13 188.68 25.30 13 -21 -10 191.18 32.10 -13 21 -10 223.08 38.00 13 -21 12 90.09 22.30 13 -21 -12 106.19 22.10 -21 12 -13 121.19 32.20 -13 21 -12 80.79 28.80 -12 13 -21 106.59 26.40 12 -13 -21 134.59 24.50 21 -12 -13 136.39 18.80 -21 14 -13 153.98 34.30 14 -13 -21 129.89 24.40 -13 21 -14 120.29 32.70 13 -21 -14 141.59 25.20 -14 13 -21 150.68 30.70 21 -14 -13 135.69 20.20 16 -13 -21 90.69 20.50 -13 21 -16 120.39 32.30 21 -16 -13 125.99 20.20 -21 16 -13 142.39 34.70 -16 13 -21 125.09 30.00 13 -21 -16 85.69 20.00 1 14 -21 12.70 21.40 14 -21 1 8.10 15.90 -14 21 1 16.90 20.60 -14 21 -1 23.80 22.70 -1 14 -21 19.10 21.20 14 -21 -1 11.30 19.40 -21 1 -14 25.40 23.70 3 14 -21 98.59 24.90 14 -21 3 71.39 18.00 -14 21 3 98.89 22.60 -3 14 -21 140.29 28.00 -21 3 -14 116.49 31.30 -14 21 -3 103.49 26.40 14 -21 -3 93.89 21.20 5 14 -21 165.28 29.50 14 -21 5 111.99 21.90 7 14 -21 421.36 43.10 14 -21 7 355.56 34.90 -21 7 -14 285.87 42.10 14 -21 -7 259.67 36.10 -7 14 -21 312.27 45.30 21 -7 -14 304.57 29.90 -14 21 -7 272.77 49.80 14 -21 9 152.48 22.40 21 -9 -14 130.79 23.20 -21 9 -14 131.59 34.00 -14 21 -9 135.99 32.70 14 -21 -9 107.99 22.90 -9 14 -21 135.49 29.70 14 -21 11 14.30 19.00 -21 11 -14 47.50 29.90 -11 14 -21 82.79 28.00 21 -11 -14 69.49 15.70 11 -14 -21 56.09 22.70 -14 21 -11 77.89 31.90 14 -21 -11 64.19 22.20 -13 14 -21 133.39 29.50 21 -13 -14 118.89 18.80 14 -21 -13 139.59 25.00 13 -14 -21 121.29 24.20 -21 13 -14 108.49 28.80 -14 21 -13 171.98 38.60 14 -21 -15 24.80 20.10 15 -14 -21 8.50 16.90 21 -15 -14 13.90 15.40 -15 14 -21 19.40 23.20 -21 15 -14 21.40 27.80 -14 21 -15 18.30 26.70 -21 0 -15 88.69 29.10 15 -21 0 86.59 21.70 -15 21 0 60.19 23.40 0 15 -21 62.19 24.30 15 -21 2 89.99 19.30 2 15 -21 107.69 25.10 -15 21 2 135.29 24.60 -2 15 -21 175.98 29.30 15 -21 -2 100.99 21.40 4 15 -21 117.89 27.70 15 -21 4 104.19 21.50 -15 21 -4 157.08 33.10 15 -21 -4 140.99 23.90 -4 15 -21 107.99 26.50 -21 4 -15 116.19 28.40 6 15 -21 234.78 38.90 15 -21 6 222.18 31.30 -21 6 -15 229.68 37.00 -6 15 -21 163.18 30.10 15 -21 -6 183.78 32.70 21 -6 -15 186.78 24.10 -15 21 -6 225.88 36.80 15 -21 8 7.40 17.80 -8 -15 -21 11.70 11.60 -15 21 -8 -18.40 26.30 -8 15 -21 2.10 23.10 8 -15 -21 -6.40 17.80 -21 8 -15 23.70 29.70 21 -8 -15 17.00 13.30 15 -21 -8 7.70 18.50 -21 10 -15 166.78 33.90 -10 15 -21 176.48 32.50 -15 21 -10 157.98 33.60 21 -10 -15 153.78 24.20 15 -21 -10 93.49 21.80 10 -15 -21 129.49 24.90 -15 21 -12 48.70 29.20 12 -15 -21 33.70 21.70 -21 12 -15 30.10 28.00 21 -12 -15 36.80 14.70 -12 15 -21 32.10 26.70 15 -21 -12 12.30 19.30 -14 15 -21 17.40 24.80 21 -14 -15 15.20 16.30 -15 21 -14 25.40 30.40 -21 14 -15 35.60 26.00 15 -21 -14 21.50 18.60 14 -15 -21 23.30 20.90 -21 -1 -16 177.88 30.30 -16 21 1 158.98 26.70 -16 21 -1 100.69 26.40 -1 16 -21 95.79 26.00 16 -21 -1 87.79 21.00 -21 1 -16 77.09 25.40 -21 -3 -16 104.89 25.70 16 -21 3 99.19 21.60 3 16 -21 68.69 23.90 16 -21 -3 66.69 21.60 -3 16 -21 56.39 25.80 -16 21 -3 59.49 26.10 -21 3 -16 42.50 24.70 -5 -16 -21 0.80 12.60 16 -21 5 6.90 17.90 5 16 -21 -2.90 22.40 21 -5 -16 -3.00 9.10 -21 5 -16 3.20 23.90 -5 16 -21 12.50 23.10 16 -21 -5 3.60 16.60 -16 21 -5 -11.30 27.40 16 -21 7 42.80 17.50 7 16 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3.70 15.90 -4 -17 -21 7.80 13.60 -21 -4 -17 8.40 22.80 4 17 -21 12.70 22.60 17 -21 -4 -3.30 16.60 -21 4 -17 7.30 24.30 4 -17 -21 21.40 19.70 -4 17 -21 25.60 24.90 21 -4 -17 -0.10 2.90 -17 21 -4 21.80 25.90 -21 -6 -17 819.12 67.89 6 17 -21 828.02 68.89 17 -21 6 781.52 62.29 -6 -17 -21 831.02 59.29 6 -17 -21 743.23 64.39 21 -6 -17 778.32 59.59 -21 6 -17 807.52 72.09 -6 17 -21 769.72 71.69 -17 21 -6 819.82 74.79 -8 -17 -21 160.28 19.40 17 -21 8 157.18 22.00 21 -8 -17 156.78 24.00 -17 21 -8 144.19 30.80 8 -17 -21 98.89 22.60 17 -21 -8 136.39 23.40 -21 8 -17 135.09 29.10 -8 17 -21 112.19 28.10 17 -21 10 135.39 22.60 -10 17 -21 106.99 28.70 10 -17 -21 126.29 24.40 -17 21 -10 182.68 35.80 -21 10 -17 110.69 27.60 17 -21 -10 147.69 23.30 21 -10 -17 170.88 24.30 -12 17 -21 153.38 30.90 17 -21 -12 183.48 31.50 12 -17 -21 206.38 27.40 21 -12 -17 166.38 25.10 -17 21 -12 143.99 32.90 -21 12 -17 165.98 31.50 18 -21 1 8.50 17.50 -1 -18 -21 34.90 15.60 1 18 -21 14.00 23.70 -18 21 1 20.50 21.00 -21 -1 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11 -18 -21 27.30 17.20 -11 18 -21 49.30 27.20 18 -21 -11 64.39 21.30 21 -11 -18 72.99 16.00 -19 21 0 20.90 22.90 -21 0 -19 43.00 23.20 19 -21 0 12.10 16.90 0 -19 -21 34.50 16.50 0 19 -21 7.60 25.30 19 -21 2 87.69 19.40 -2 -19 -21 136.99 23.20 -21 -2 -19 139.59 25.50 2 19 -21 159.68 31.20 -19 21 2 142.59 25.40 -19 21 -2 116.39 27.80 19 -21 -2 87.79 20.20 -21 2 -19 127.69 27.20 2 -19 -21 110.19 21.10 -2 19 -21 113.69 29.80 -4 -19 -21 17.60 13.20 4 19 -21 34.00 24.40 -21 -4 -19 29.30 19.70 19 -21 4 17.00 16.30 -21 4 -19 85.49 25.90 19 -21 -4 75.59 20.70 4 -19 -21 48.40 17.60 -4 19 -21 67.59 28.10 -19 21 -4 72.29 26.60 -21 -6 -19 256.87 35.40 6 19 -21 271.07 41.60 19 -21 6 289.77 34.60 -6 -19 -21 272.37 28.40 -6 19 -21 363.56 48.50 -19 21 -6 362.86 50.09 19 -21 -6 368.66 36.70 -21 6 -19 345.27 44.30 6 -19 -21 335.57 37.40 21 -6 -19 338.37 30.70 19 -21 8 97.59 19.10 21 -8 -19 66.89 15.60 8 -19 -21 42.50 18.00 19 -21 -8 88.29 21.70 -21 8 -19 96.29 28.20 -8 19 -21 82.79 28.50 -19 21 -8 85.19 30.60 -20 21 1 23.60 20.90 -1 -20 -21 18.70 14.50 1 20 -21 40.10 23.30 -21 -1 -20 6.30 19.80 20 -21 1 16.60 16.20 -20 21 -1 40.50 23.40 -1 20 -21 52.49 27.80 -21 1 -20 63.99 22.50 20 -21 -1 34.20 17.40 1 -20 -21 42.60 15.80 -21 -3 -20 85.79 21.00 3 20 -21 128.19 28.70 -3 20 -21 77.79 27.80 20 -21 -3 52.89 17.40 -21 3 -20 54.59 23.40 -20 21 -3 90.59 28.40 3 -20 -21 65.79 18.20 20 -21 5 137.99 20.90 5 20 -21 111.79 26.70 -5 -20 -21 135.99 20.50 20 -21 -5 177.38 28.60 21 -5 -20 150.78 21.80 -21 5 -20 184.78 30.10 5 -20 -21 129.89 21.40 -5 20 -21 190.88 33.90 -20 21 -5 151.78 30.10 21 -7 -20 51.49 14.80 -7 20 -21 39.70 26.80 7 -20 -21 38.30 17.50 20 -21 -7 37.20 18.40 -20 21 -7 50.09 28.70 -21 7 -20 45.10 23.00 -21 0 -21 -4.00 16.00 -21 21 0 -1.50 19.90 0 -21 -21 -1.00 14.00 0 21 -21 3.60 22.60 21 -21 0 -6.10 14.70 -2 -21 -21 185.58 24.00 21 -21 2 159.18 22.00 2 21 -21 166.58 30.80 -21 2 -21 164.38 27.00 2 -21 -21 196.68 27.70 -2 21 -21 148.79 30.10 21 -21 -2 197.58 27.80 -21 21 -2 202.88 30.90 0 -22 0 12.60 12.10 0 22 0 12.00 21.40 0 22 -2 15.20 22.20 0 22 2 -2.80 17.80 0 -22 -2 2.10 11.70 0 -22 2 7.60 12.10 0 22 4 15.70 17.90 0 22 -4 14.90 25.20 0 -22 4 17.00 14.40 0 -22 -4 27.90 13.30 0 -22 6 419.06 36.10 0 22 6 465.45 39.10 0 22 -6 343.37 49.20 0 -22 -6 410.16 36.30 0 -22 -8 94.39 17.30 0 -22 8 126.99 21.80 0 22 -8 76.89 29.30 -22 10 0 7.00 24.80 0 -22 -10 45.80 15.70 0 22 -10 28.10 27.90 0 -22 10 40.50 15.20 -12 0 -22 11.30 15.10 -22 12 0 -3.90 23.50 0 22 -12 3.10 24.60 22 -12 0 -1.70 11.90 0 -22 -12 9.90 15.00 22 -14 0 -1.30 12.80 0 -22 -14 -3.70 15.70 0 22 -14 14.40 25.10 -14 0 -22 -2.80 16.00 -22 14 0 4.40 22.30 0 22 -16 14.00 28.90 0 -22 -16 43.00 16.30 -22 16 0 28.20 22.70 22 -16 0 24.50 15.50 -16 0 -22 25.80 18.20 -18 0 -22 170.78 30.10 0 22 -18 232.08 38.00 -22 18 0 223.78 37.70 22 -18 0 177.68 27.00 0 -22 -18 162.58 25.50 0 22 -20 23.10 25.30 0 -22 -20 34.50 15.50 -22 20 0 33.00 21.90 22 -20 0 10.70 14.40 -1 -22 -1 73.29 14.20 1 22 -1 60.39 22.30 1 -22 1 99.19 15.70 -1 22 1 75.09 22.60 -1 -22 -3 146.39 22.70 1 22 -3 153.38 30.70 -1 22 3 153.98 24.70 1 -22 3 157.08 23.90 -1 22 -3 159.78 29.00 1 22 3 214.58 28.30 1 -22 -3 179.18 23.90 -1 -22 3 201.88 23.00 1 -22 5 -8.20 13.50 -1 -22 -5 11.00 12.00 -1 22 5 17.20 16.80 1 22 -5 15.40 23.20 1 22 5 -10.40 16.30 -1 -22 5 -4.30 11.70 -1 22 -5 -0.20 22.50 1 -22 -5 1.50 13.30 1 22 -7 115.59 27.10 1 -22 7 167.68 23.90 -1 -22 -7 164.08 22.20 -1 -22 7 139.29 21.70 -1 22 -7 76.29 27.50 1 -22 -7 104.09 17.60 1 -22 9 438.56 36.20 -22 9 1 366.26 47.80 1 22 -9 393.26 51.49 -1 -22 -9 463.65 35.70 -1 22 -9 318.87 50.49 -1 -22 9 369.16 35.00 1 -22 -9 368.96 35.50 -22 9 -1 368.46 49.20 -9 1 -22 367.36 36.10 -22 11 1 7.50 25.00 22 -11 1 8.60 11.50 -1 -22 -11 -1.70 14.70 1 22 -11 -17.80 28.80 -11 1 -22 20.20 15.70 22 -11 -1 25.50 11.40 1 -22 -11 27.50 16.10 -1 22 -11 18.50 25.70 -22 11 -1 13.50 26.70 1 22 -13 78.09 27.90 22 -13 1 105.59 15.70 -22 13 1 117.69 29.30 -22 13 -1 68.19 25.90 1 -22 -13 64.69 15.90 -1 22 -13 59.69 30.50 -13 1 -22 95.69 20.70 22 -13 -1 57.09 14.20 -1 -22 -15 100.79 17.70 22 -15 1 116.69 17.70 -15 -1 -22 146.09 33.90 -22 15 1 102.99 25.60 1 22 -15 82.19 33.20 1 -22 -15 120.49 19.90 22 -15 -1 86.99 16.10 -15 1 -22 96.29 21.90 -1 22 -15 102.19 31.70 -22 15 -1 85.59 28.30 1 22 -17 182.58 36.20 22 -17 1 155.68 26.20 -1 -22 -17 161.58 25.50 -22 17 1 181.18 30.70 22 -17 -1 173.98 26.70 -1 22 -17 191.88 37.30 1 -22 -17 196.48 27.90 -22 17 -1 210.38 33.70 -17 1 -22 188.68 27.70 -22 19 1 27.90 21.60 -1 -22 -19 14.40 14.10 22 -19 1 18.30 15.50 1 22 -19 4.70 23.90 22 -19 -1 23.00 15.00 1 -22 -19 28.80 16.30 -22 19 -1 36.70 22.70 -1 22 -19 6.10 25.50 -19 1 -22 21.80 17.40 -2 -22 0 -3.20 11.70 2 -22 0 7.50 12.70 -2 22 0 3.20 19.20 2 22 0 8.80 19.20 2 -22 2 561.54 47.90 -2 22 2 622.24 54.89 -2 -22 -2 567.54 46.60 2 22 -2 531.75 57.79 -2 22 -2 828.72 59.59 2 -22 4 5.10 13.40 -2 -22 -4 18.50 12.50 -2 22 4 19.20 18.20 2 22 -4 15.10 22.30 2 22 4 -11.00 17.60 -2 22 -4 -16.30 23.80 2 -22 -4 11.00 15.30 -2 -22 4 1.10 12.10 2 22 -6 307.97 46.50 -2 -22 -6 302.87 30.80 2 -22 6 341.67 33.10 -2 22 -6 454.75 47.90 -2 -22 -8 32.90 14.50 2 -22 8 16.10 15.60 2 22 -8 10.00 26.80 -22 8 -2 42.70 28.00 2 -22 -8 49.90 17.00 -2 22 -8 20.30 25.70 -2 -22 8 39.20 14.20 -8 2 -22 58.89 15.10 -22 10 2 346.57 48.70 2 -22 10 381.36 39.20 2 22 -10 327.47 54.49 -2 -22 -10 420.96 37.80 -22 10 -2 450.15 52.69 -2 22 -10 444.46 55.49 -10 2 -22 476.65 41.60 2 -22 -10 503.45 39.90 22 -10 -2 534.35 35.50 2 22 -12 101.79 33.40 -22 12 2 69.29 24.10 22 -12 -2 61.19 13.80 -22 12 -2 70.19 30.00 -12 2 -22 68.19 19.50 2 -22 -12 64.69 16.40 -2 22 -12 66.49 31.40 22 -14 2 519.35 40.50 -2 -22 -14 504.45 40.80 2 22 -14 499.85 59.09 -22 14 2 504.85 51.09 -22 14 -2 451.85 55.29 -2 22 -14 442.16 58.29 -14 2 -22 467.15 46.90 22 -14 -2 459.35 40.70 2 -22 -14 490.95 42.80 22 -16 2 48.70 15.40 -2 -22 -16 60.09 15.40 -22 16 2 27.60 22.60 2 22 -16 31.90 27.80 -2 22 -16 74.29 27.50 -22 16 -2 82.09 26.00 -16 2 -22 116.09 22.70 2 22 -18 112.19 29.70 22 -18 2 130.69 19.30 -2 -22 -18 132.49 17.70 -22 18 2 143.69 26.10 2 -22 -18 100.39 19.90 -22 18 -2 82.89 26.70 22 -18 -2 90.09 18.20 -2 22 -18 114.69 32.20 -18 2 -22 88.39 22.90 -2 -22 -20 13.60 13.30 2 22 -20 12.50 25.60 22 -20 2 11.50 15.20 -20 2 -22 39.80 18.20 -2 22 -20 65.99 28.70 -22 20 -2 52.79 24.80 22 -20 -2 41.80 15.20 2 -22 -20 57.29 17.60 3 -22 1 173.98 24.70 -3 -22 -1 146.89 21.00 3 22 -1 173.48 30.80 -3 22 1 153.28 26.00 -3 -22 1 155.88 21.10 -3 22 -1 198.78 31.00 3 22 1 221.48 31.60 3 -22 -1 188.88 24.70 3 -22 3 631.54 48.10 3 22 -3 591.04 58.19 -3 -22 -3 595.74 45.90 -3 22 3 660.93 53.59 3 22 3 618.04 54.89 -3 -22 3 598.04 45.80 3 -22 -3 588.64 47.90 -3 22 -3 477.15 56.59 -3 -22 -5 271.27 26.60 3 -22 5 279.57 29.70 -3 22 5 279.87 32.80 3 22 -5 253.37 44.30 3 22 -7 666.13 58.79 -7 3 -22 499.85 44.90 -3 -22 7 537.05 42.10 -3 22 -7 436.76 56.19 3 -22 -7 541.35 44.50 -3 -22 -9 175.28 22.10 3 -22 9 180.88 25.60 3 22 -9 89.49 27.70 -22 9 3 136.89 26.20 -9 3 -22 143.89 21.80 -22 9 -3 112.29 30.20 3 -22 -9 129.99 19.90 -3 22 -9 78.09 27.80 -22 11 3 400.06 48.60 3 22 -11 328.87 55.39 22 -11 3 423.76 36.50 -3 -22 -11 413.86 38.10 3 -22 11 403.96 40.80 3 -22 -11 518.75 41.20 -22 11 -3 506.95 55.59 -11 3 -22 544.35 44.70 -3 22 -11 500.55 56.89 22 -11 -3 507.15 37.50 -22 13 3 103.19 26.10 22 -13 3 125.59 21.50 -3 -22 -13 114.39 17.70 3 22 -13 94.19 31.00 22 -13 -3 181.38 22.80 3 -22 -13 160.58 27.10 -13 3 -22 180.08 25.30 -22 13 -3 183.18 34.40 -3 22 -13 132.99 32.00 -3 -22 -15 32.90 14.40 -22 15 3 30.80 21.10 22 -15 3 31.30 14.80 3 22 -15 20.80 24.30 22 -15 -3 9.90 14.50 -15 3 -22 11.10 18.80 -3 22 -15 29.00 32.90 -22 15 -3 22.40 27.30 3 -22 -15 10.20 15.20 -3 -22 -17 206.78 25.30 3 22 -17 205.58 35.80 -22 17 3 215.38 35.90 22 -17 3 196.08 27.00 -17 3 -22 227.38 34.70 -22 17 -3 216.18 33.00 3 -22 -17 219.88 30.30 22 -17 -3 200.78 28.00 -3 22 -17 170.28 32.40 3 22 -19 195.48 34.80 22 -19 3 192.18 26.90 -3 -22 -19 192.98 23.10 22 -19 -3 168.68 26.70 19 -3 -22 172.58 25.10 -22 19 -3 211.58 33.60 -3 22 -19 179.08 36.10 -19 3 -22 147.29 26.30 3 -22 -19 183.38 29.00 -4 -22 0 19.90 11.30 4 -22 0 21.90 14.60 -4 22 0 18.50 21.30 4 22 0 20.40 23.20 4 -22 2 5.10 13.10 -4 -22 -2 9.10 10.80 4 22 -2 3.90 24.80 -4 22 2 14.00 18.60 4 -22 -2 -1.80 13.60 -4 22 -2 -0.70 23.60 -2 4 -22 0.50 10.50 -4 -22 2 11.30 11.20 4 22 2 -4.30 20.60 -4 4 -22 119.29 21.60 -4 22 -4 101.99 26.40 -4 -22 4 132.69 19.60 4 -22 -4 144.89 19.90 4 -22 6 253.17 28.00 -4 -22 -6 254.07 24.10 4 22 -6 258.27 44.20 4 -22 -6 195.58 28.50 -4 -22 6 192.68 23.70 -6 4 -22 203.58 27.90 4 22 -8 245.88 40.30 -4 -22 -8 314.67 29.50 4 -22 8 318.67 33.60 -4 22 -8 301.47 48.00 -8 4 -22 362.56 35.80 4 -22 -8 387.56 33.90 -22 8 -4 299.77 48.80 -4 -22 -10 58.39 14.00 -22 10 4 47.20 21.40 4 -22 10 76.19 19.20 4 22 -10 47.10 28.80 -4 22 -10 20.90 29.60 22 -10 -4 37.60 12.10 -10 4 -22 26.00 17.50 -22 10 -4 20.10 24.70 4 -22 -10 39.80 18.60 4 22 -12 49.70 30.70 -4 -22 -12 75.99 15.00 22 -12 4 66.39 13.80 -22 12 4 63.79 22.40 -22 12 -4 69.99 30.00 -4 22 -12 30.10 26.80 22 -12 -4 59.59 14.60 4 -22 -12 35.50 16.50 -12 4 -22 54.39 20.80 -4 -22 -14 37.10 13.60 22 -14 4 19.10 14.20 -22 14 4 30.40 21.50 4 22 -14 25.60 29.10 22 -14 -4 13.20 13.90 -22 14 -4 12.30 27.70 -14 4 -22 -0.80 19.00 -4 22 -14 10.40 31.70 4 -22 -14 14.80 16.40 -22 16 4 295.27 37.50 22 -16 4 242.28 29.30 -4 -22 -16 290.27 27.40 4 22 -16 274.07 48.10 -4 22 -16 294.07 52.29 -22 16 -4 254.47 45.60 4 -22 -16 236.58 32.80 -16 4 -22 278.37 38.00 22 -16 -4 255.87 30.10 4 22 -18 218.98 37.50 -4 -22 -18 169.58 22.80 22 -18 4 171.18 26.80 4 -22 -18 199.08 30.40 22 -18 -4 173.98 27.10 -22 18 -4 218.28 35.20 -4 22 -18 229.98 38.80 -18 4 -22 195.98 29.40 5 -22 1 20.90 16.20 -5 22 1 6.70 21.20 5 22 -1 15.20 23.70 -5 -22 -1 9.00 10.70 5 -22 -1 -1.90 14.20 5 22 1 9.00 21.70 -5 22 -1 -2.60 19.40 -5 -22 1 10.70 10.10 -1 5 -22 -0.30 11.30 -5 -22 -3 254.37 24.40 5 22 -3 242.88 36.30 -5 22 3 271.97 35.80 5 -22 3 253.47 29.60 -5 -22 -5 448.96 36.20 -5 22 5 366.86 38.50 5 22 -5 414.26 52.39 5 -22 5 461.25 40.20 -5 -22 5 487.15 36.30 5 -22 -5 502.55 40.40 -5 5 -22 496.45 41.50 -5 22 -5 420.06 51.39 5 22 -7 165.18 32.80 -5 -22 -7 188.48 21.60 5 -22 7 192.58 27.40 -5 22 -7 256.47 42.30 5 22 -9 170.58 34.80 -22 9 5 188.08 29.10 -5 -22 -9 224.18 23.40 5 -22 9 216.18 29.60 5 -22 11 72.19 18.50 -5 -22 -11 85.99 14.80 -22 11 5 52.99 22.20 5 22 -11 48.90 30.50 5 -22 -11 55.19 18.20 -5 22 -11 82.59 32.40 -22 11 -5 59.79 29.20 -11 5 -22 69.79 21.00 22 -11 -5 70.29 14.50 5 22 -13 53.09 27.40 22 -13 5 63.39 14.30 -22 13 5 56.49 21.10 -13 5 -22 21.50 19.90 22 -13 -5 33.20 14.80 5 -22 -13 27.80 17.90 -22 13 -5 37.10 28.70 -5 22 -13 17.40 30.80 22 -15 5 546.35 42.20 -5 -22 -15 541.55 40.90 5 22 -15 534.55 60.69 -5 22 -15 484.05 61.79 5 -22 -15 484.65 45.80 -22 15 -5 499.05 57.69 22 -15 -5 470.55 43.30 -15 5 -22 489.25 50.19 -5 -22 -17 155.78 21.10 5 22 -17 140.99 32.00 22 -17 5 143.89 25.60 -17 5 -22 202.88 28.80 5 -22 -17 171.88 30.30 -22 17 -5 189.78 33.90 22 -17 -5 155.18 26.90 -5 22 -17 147.79 33.00 -5 -22 -19 290.87 25.90 5 22 -19 319.37 44.60 22 -19 5 340.07 29.80 -5 22 -19 297.17 42.60 -19 5 -22 237.68 37.70 5 -22 -19 227.38 33.60 -22 19 -5 312.27 40.90 22 -19 -5 223.88 31.10 19 -5 -22 200.58 30.10 6 -22 0 399.96 37.10 0 6 -22 406.36 35.60 6 22 0 391.76 47.00 -6 22 0 371.26 44.60 -6 -22 0 381.76 31.40 2 6 -22 300.57 30.20 -6 -22 -2 317.97 27.00 6 22 -2 302.27 44.70 6 -22 2 302.17 32.30 -6 22 2 347.47 39.60 6 22 -4 245.68 43.50 -6 22 4 285.17 33.10 6 -22 4 274.97 29.40 -6 -22 -4 265.07 22.70 -6 -22 4 192.88 22.80 -4 6 -22 221.78 29.80 -6 22 -4 202.38 34.30 6 -22 -4 203.78 29.50 -6 -22 -6 1880.91 135.29 6 22 -6 1672.93 144.79 6 -22 6 1929.21 137.29 -6 22 -6 1920.21 144.79 -6 6 -22 2149.19 140.49 6 -22 -6 2202.88 137.89 6 22 -8 18.00 28.70 -22 8 6 15.90 21.10 6 -22 8 19.80 16.20 -6 -22 -8 26.10 11.10 -8 6 -22 78.79 20.10 -6 22 -8 73.59 31.20 -22 8 -6 78.59 31.50 6 22 -10 51.59 28.40 -6 22 -10 7.00 28.90 6 -22 -10 -1.90 15.70 -22 10 -6 25.20 28.70 22 -10 -6 8.30 11.90 -10 6 -22 1.40 18.90 6 -22 12 241.68 30.60 -22 12 6 244.58 34.40 6 22 -12 192.08 35.60 22 -12 6 238.78 24.70 -6 -22 -12 233.58 23.10 22 -12 -6 195.58 25.60 -22 12 -6 226.08 39.30 -6 22 -12 131.59 32.10 6 -22 -12 207.88 31.00 -12 6 -22 193.08 34.30 -6 -22 -14 301.87 28.40 6 22 -14 284.57 51.59 22 -14 6 297.57 30.60 -22 14 -6 308.17 50.69 6 -22 -14 297.37 35.30 22 -14 -6 322.27 32.00 -14 6 -22 327.07 41.20 -6 22 -14 334.57 53.39 22 -16 6 31.80 14.90 -6 -22 -16 42.60 11.90 6 22 -16 13.10 26.60 -16 6 -22 19.50 21.90 -6 22 -16 16.50 29.00 -22 16 -6 40.40 30.10 22 -16 -6 19.40 15.80 6 -22 -16 12.60 18.70 6 22 -18 616.64 62.09 -6 -22 -18 686.83 53.29 22 -18 6 603.94 48.90 22 -18 -6 601.74 49.80 -6 22 -18 662.53 67.49 6 -22 -18 604.54 52.69 18 -6 -22 609.44 50.59 -18 6 -22 610.54 57.39 -22 18 -6 546.25 62.99 1 7 -22 179.08 25.60 7 -22 1 164.68 26.50 -7 22 1 211.08 28.70 -7 -22 -1 165.48 17.60 7 22 -1 117.69 27.60 7 -22 -1 130.69 20.30 -7 -22 1 128.69 17.70 -7 22 -1 137.99 27.60 -1 7 -22 152.68 25.90 -7 -22 -3 738.93 51.09 3 7 -22 740.83 55.59 7 22 -3 714.63 66.19 7 -22 3 754.02 55.49 -7 22 3 746.43 59.89 -3 7 -22 513.55 56.29 7 -22 5 189.88 28.10 -7 -22 -5 198.78 19.40 7 22 -5 126.49 29.70 7 -22 -7 126.79 20.80 -7 22 -7 106.49 29.50 -7 7 -22 127.09 23.20 -22 7 -7 91.89 31.30 -22 9 7 440.16 47.00 -7 -22 -9 427.86 37.70 7 22 -9 422.06 57.09 7 -22 9 446.86 44.20 -7 22 -9 515.65 58.79 -9 7 -22 583.94 49.50 -22 9 -7 508.15 57.79 22 -9 -7 579.84 38.70 7 -22 -9 541.75 44.80 7 22 -11 61.09 30.80 7 -22 11 80.49 20.40 -7 -22 -11 96.09 14.00 7 -22 -11 101.89 19.50 -22 11 -7 122.09 31.70 -11 7 -22 151.08 26.40 22 -11 -7 138.69 21.50 -7 22 -11 126.39 33.30 -22 13 -7 185.68 34.00 22 -13 -7 155.38 23.70 7 -22 -13 100.69 20.10 -7 22 -13 113.19 30.90 -13 7 -22 145.99 26.30 22 -15 7 251.37 27.70 7 22 -15 311.47 41.40 7 -22 -15 235.48 33.50 22 -15 -7 238.38 28.60 -7 22 -15 207.38 35.40 -15 7 -22 233.28 38.30 -22 15 -7 181.98 32.80 7 22 -17 212.78 35.30 22 -17 7 175.38 25.30 -7 22 -17 175.58 36.70 -17 7 -22 148.89 27.90 -22 17 -7 230.38 37.40 17 -7 -22 139.29 21.70 7 -22 -17 153.08 25.40 22 -17 -7 124.89 20.60 8 -22 0 76.09 17.50 -8 22 0 97.69 25.90 0 8 -22 76.69 19.00 -8 -22 0 81.19 11.10 -8 22 2 17.50 20.00 -8 -22 -2 17.30 13.10 2 8 -22 28.60 15.60 8 -22 2 9.00 15.10 8 22 -2 12.20 22.90 -2 8 -22 44.90 18.00 8 -22 -2 49.40 16.80 -8 22 -2 30.30 23.00 4 8 -22 304.07 33.50 -8 22 4 328.87 36.60 8 22 -4 254.07 46.10 8 -22 4 284.47 34.00 -8 22 -4 343.67 45.20 8 -22 -4 366.46 34.60 -4 8 -22 342.87 37.80 8 -22 6 23.10 18.90 8 22 -6 27.40 25.30 8 -22 -6 79.49 19.50 -22 6 -8 63.39 29.50 -8 22 -6 59.79 29.00 -6 8 -22 71.29 20.40 8 -22 8 166.58 27.70 -22 8 8 176.08 25.30 8 22 -8 104.39 29.60 8 -22 10 32.10 18.60 8 22 -10 37.70 29.20 8 -22 -10 45.30 19.90 22 -10 -8 38.20 13.30 -8 22 -10 21.00 29.80 -22 10 -8 37.90 31.70 -10 8 -22 32.20 21.20 8 22 -12 78.49 33.90 8 -22 12 96.39 21.90 -8 22 -12 141.39 35.20 -12 8 -22 115.09 24.40 -22 12 -8 112.09 30.50 22 -12 -8 128.39 22.50 8 -22 -12 106.49 20.00 8 22 -14 64.49 25.70 8 -22 -14 65.39 20.80 22 -14 -8 52.39 16.00 -22 14 -8 47.70 27.90 -14 8 -22 57.59 22.30 -8 22 -14 53.69 32.70 8 22 -16 87.79 31.30 -8 22 -16 124.59 34.30 -16 8 -22 123.29 28.00 -22 16 -8 125.99 32.60 22 -16 -8 115.79 18.90 -18 8 -22 137.49 27.70 -8 22 -18 106.39 28.50 18 -8 -22 135.09 21.00 8 -22 -18 108.79 21.40 -22 18 -8 130.79 32.30 22 -18 -8 130.99 19.80 -9 22 1 421.46 45.10 9 -22 1 430.76 37.90 1 9 -22 455.45 41.30 -9 22 -1 332.87 45.30 9 -22 -1 376.56 37.90 -1 9 -22 370.26 40.90 3 9 -22 169.98 28.80 9 -22 3 177.58 27.50 -9 22 3 197.38 31.70 9 -22 -3 134.69 22.50 -9 22 -3 114.69 27.70 -3 9 -22 159.48 25.80 9 22 -5 123.59 29.30 9 -22 5 192.98 28.40 5 9 -22 189.48 28.20 9 22 -7 416.56 56.79 9 -22 7 448.16 44.40 9 -22 -7 522.55 45.00 -22 7 -9 475.65 57.39 -7 9 -22 588.64 50.29 -9 22 -7 524.35 56.99 9 22 -9 40.10 29.70 9 -22 9 35.60 20.20 -9 22 -9 35.50 27.40 -9 9 -22 47.70 21.60 22 -9 -9 61.79 13.00 9 -22 -9 47.10 20.30 -22 9 -9 70.89 32.40 9 -22 11 297.07 36.20 9 22 -11 294.27 49.10 22 -11 -9 325.87 30.80 -9 22 -11 348.27 53.69 9 -22 -11 324.87 37.00 -11 9 -22 354.46 43.70 -22 11 -9 307.27 50.49 9 22 -13 34.50 23.90 -13 9 -22 15.00 22.40 -22 13 -9 35.20 31.30 -9 22 -13 14.30 27.30 22 -13 -9 8.50 14.20 9 -22 -13 17.80 17.50 22 -15 -9 111.99 18.60 -22 15 -9 140.29 34.90 9 -22 -15 83.39 21.20 -9 22 -15 83.89 30.60 -15 9 -22 120.49 26.40 -17 9 -22 50.29 22.00 17 -9 -22 51.79 18.10 -22 17 -9 80.89 31.90 22 -17 -9 61.99 16.80 -9 22 -17 42.90 26.00 9 -22 -17 54.09 21.80 10 -22 0 21.00 16.60 0 10 -22 32.40 18.90 -10 22 0 8.00 20.90 10 -22 2 401.06 39.50 2 10 -22 392.16 42.50 -10 22 2 367.46 44.50 10 -22 -2 448.86 40.50 -10 22 -2 456.95 49.60 -2 10 -22 492.35 45.30 -10 22 4 -6.40 11.70 4 10 -22 68.99 19.40 10 -22 4 66.09 19.10 -10 22 -4 19.90 23.40 10 -22 -4 22.20 18.60 -4 10 -22 41.00 20.40 -10 22 6 4.10 5.80 -6 10 -22 8.90 20.00 -10 22 -6 8.90 27.90 -22 6 -10 18.00 26.30 10 -22 -6 7.30 18.80 22 -6 -10 0.10 2.30 10 -22 8 18.20 17.20 -22 8 -10 26.00 26.10 -10 22 -8 23.50 27.60 -8 10 -22 23.50 22.00 10 -22 -8 49.99 20.30 10 -22 10 372.26 39.20 -22 10 -10 394.76 53.99 -10 22 -10 430.26 56.09 22 -10 -10 395.26 34.50 10 -22 -10 376.86 40.60 -10 10 -22 402.36 45.00 10 -22 12 15.00 18.30 10 -22 -12 38.90 22.00 -12 10 -22 30.20 21.80 22 -12 -10 31.30 14.10 -10 22 -12 43.20 28.60 -22 12 -10 50.69 31.80 -14 10 -22 427.26 50.79 -10 22 -14 498.25 61.29 -22 14 -10 452.65 56.39 22 -14 -10 438.86 39.60 16 -10 -22 7.30 18.40 10 -22 -16 23.60 21.70 22 -16 -10 8.20 15.20 -10 22 -16 12.40 30.80 -22 16 -10 5.70 25.50 -16 10 -22 -0.60 20.80 -11 22 1 -1.80 19.70 1 11 -22 -17.90 18.10 11 -22 1 8.70 18.20 11 -22 -1 21.70 17.10 -11 22 -1 6.30 22.10 -1 11 -22 7.30 19.60 3 11 -22 370.06 44.00 -11 22 3 422.06 43.90 11 -22 3 379.36 40.50 11 -22 -3 474.35 41.60 -11 22 -3 523.85 51.79 11 -22 5 49.90 16.80 5 11 -22 63.29 20.20 11 -22 -5 48.90 18.50 -11 22 -5 50.59 25.60 -22 5 -11 50.29 30.30 -5 11 -22 63.89 22.00 11 -22 7 75.69 20.50 11 -22 -7 106.49 21.00 -22 7 -11 77.79 27.30 -7 11 -22 144.59 26.80 -11 22 -7 120.59 30.40 11 -22 9 262.17 35.50 -22 9 -11 340.57 51.59 -9 11 -22 320.77 43.60 -11 22 -9 355.66 52.49 22 -9 -11 319.87 29.70 11 -22 -9 320.57 37.20 11 -22 11 16.40 17.30 -11 22 -11 3.90 30.10 11 -22 -11 28.70 20.20 -11 11 -22 -3.90 21.30 22 -11 -11 -7.20 13.40 -22 11 -11 1.00 27.70 -22 13 -11 96.39 29.70 22 -13 -11 127.59 18.00 11 -22 -13 122.19 23.80 -11 22 -13 128.69 35.80 -13 11 -22 139.39 28.00 11 -22 -15 165.98 25.10 -15 11 -22 182.58 30.90 22 -15 -11 152.78 26.20 -11 22 -15 140.89 33.00 15 -11 -22 135.09 23.80 -22 15 -11 195.68 36.80 0 12 -22 -5.30 19.80 12 -22 0 -8.10 16.20 -12 22 0 -2.50 20.90 12 -22 2 60.99 17.00 2 12 -22 101.19 23.20 -2 12 -22 81.89 23.60 -12 22 -2 55.99 24.90 12 -22 -2 47.50 17.50 4 12 -22 54.89 21.20 12 -22 4 32.70 16.50 -22 4 -12 32.50 25.80 -12 22 -4 56.89 27.60 -4 12 -22 54.49 22.10 12 -22 -4 48.70 17.60 12 -22 6 221.28 31.20 6 12 -22 215.98 33.10 12 -22 -6 187.78 31.10 -22 6 -12 162.68 35.00 -6 12 -22 197.38 29.90 -12 22 -6 183.28 32.80 22 -8 -12 191.38 19.90 -22 8 -12 108.89 32.60 -12 22 -8 150.68 34.80 12 -22 -8 133.39 24.10 -8 12 -22 153.28 28.80 12 -22 10 17.80 16.30 12 -22 -10 44.90 21.40 -22 10 -12 18.90 31.00 -12 22 -10 30.30 26.50 -10 12 -22 38.60 24.30 22 -10 -12 33.30 13.70 12 -22 12 1.90 18.00 22 -12 -12 13.70 14.20 -22 12 -12 30.10 31.10 -12 22 -12 24.60 28.10 12 -22 -12 10.80 21.20 -12 12 -22 17.20 23.00 22 -14 -12 51.89 15.60 -14 12 -22 63.89 25.10 12 -22 -14 80.09 21.60 14 -12 -22 51.49 19.80 -22 14 -12 82.89 31.80 -12 22 -14 61.09 29.40 -22 16 -12 14.50 29.10 16 -12 -22 12.40 19.10 12 -22 -16 15.20 19.90 -12 22 -16 12.10 30.60 22 -16 -12 29.00 15.80 -16 12 -22 16.60 21.90 13 -22 1 81.09 19.90 1 13 -22 114.79 24.50 -13 22 1 98.99 24.90 13 -22 -1 67.89 21.20 -1 13 -22 67.09 23.60 -13 22 -1 52.39 23.60 13 -22 3 105.09 22.40 -13 22 3 117.59 23.70 3 13 -22 120.39 25.70 -22 3 -13 168.28 32.80 -3 13 -22 165.48 27.40 13 -22 -3 190.68 30.60 -13 22 -3 151.08 28.70 5 13 -22 60.19 22.20 13 -22 5 47.20 17.80 -13 22 -5 22.00 23.20 -22 5 -13 30.70 25.10 13 -22 -5 5.50 17.80 -5 13 -22 30.90 21.40 13 -22 7 199.48 29.50 13 -22 -7 126.49 24.30 -7 13 -22 137.09 26.90 -22 7 -13 149.19 33.10 -13 22 -7 113.99 28.40 13 -22 9 40.40 16.90 -13 22 -9 2.60 24.50 13 -22 -9 7.30 17.90 -9 13 -22 2.90 21.40 22 -9 -13 8.00 12.70 -22 9 -13 12.70 29.80 13 -22 11 119.19 22.00 13 -22 -11 110.49 23.50 -22 11 -13 132.99 33.30 -11 13 -22 121.49 28.40 -13 22 -11 122.39 35.60 22 -11 -13 138.49 22.60 -13 22 -13 389.36 56.39 13 -13 -22 359.36 40.70 -22 13 -13 333.37 51.69 22 -13 -13 337.67 33.20 13 -22 -13 317.87 39.20 -13 13 -22 330.57 45.90 13 -22 -15 193.48 26.90 -13 22 -15 195.38 39.20 -15 13 -22 185.18 32.10 -22 15 -13 229.68 38.70 22 -15 -13 152.28 26.00 15 -13 -22 176.38 26.30 -22 0 -14 0.50 24.30 14 -22 0 2.40 16.30 -14 22 0 -6.10 21.50 0 14 -22 12.00 22.30 -14 22 2 519.65 48.70 2 14 -22 530.25 50.69 14 -22 2 489.75 43.90 14 -22 -2 390.36 43.20 -22 2 -14 462.05 55.09 -2 14 -22 446.26 50.59 -14 22 -2 448.66 52.19 -14 22 4 1.40 4.80 14 -22 4 21.90 19.50 4 14 -22 23.40 21.50 22 -4 -14 2.20 2.50 -4 14 -22 12.50 22.20 -14 22 -4 -4.50 22.50 14 -22 -4 3.90 19.30 -22 4 -14 -1.10 26.50 14 -22 6 250.07 34.40 6 14 -22 299.87 39.50 -6 14 -22 295.17 43.30 14 -22 -6 263.07 36.50 -14 22 -6 322.27 48.80 -22 6 -14 307.67 48.40 14 -22 8 67.29 20.10 -22 8 -14 56.49 29.00 -8 14 -22 61.89 26.50 -14 22 -8 52.69 30.20 14 -22 -8 48.30 19.40 22 -8 -14 79.99 14.00 14 -22 10 390.16 41.60 14 -22 -10 413.06 43.80 -10 14 -22 461.05 51.39 -14 22 -10 494.25 58.99 -22 10 -14 456.55 56.89 10 -14 -22 460.45 45.80 22 -10 -14 447.96 37.60 -22 12 -14 73.99 29.80 12 -14 -22 70.09 22.20 -12 14 -22 81.59 27.90 14 -22 -12 61.29 22.60 22 -12 -14 73.19 16.20 -14 22 -12 40.60 28.40 -14 22 -14 814.82 75.49 -22 14 -14 721.73 71.89 14 -22 -14 733.83 62.29 14 -14 -22 786.22 62.49 22 -14 -14 772.52 58.19 -14 14 -22 745.73 69.29 -15 22 1 91.09 24.50 1 15 -22 108.89 26.90 -22 -1 -15 101.99 28.70 15 -22 1 58.49 18.30 -15 22 -1 90.19 25.60 15 -22 -1 95.29 21.70 -1 15 -22 61.69 24.00 -22 1 -15 68.59 25.20 -15 22 3 -10.80 9.80 3 15 -22 37.10 22.70 15 -22 3 31.40 19.30 -22 3 -15 -0.50 22.90 -3 15 -22 -0.80 22.00 -15 22 -3 4.10 24.40 15 -22 -3 4.50 17.50 5 15 -22 536.75 50.39 15 -22 5 472.65 44.50 -22 5 -15 491.45 57.19 15 -22 -5 439.06 45.70 -5 15 -22 478.75 52.79 -15 22 -5 503.55 57.19 15 -22 7 236.08 31.50 15 -22 -7 225.48 33.90 -7 15 -22 199.08 31.00 -15 22 -7 158.08 31.10 -22 7 -15 197.38 34.20 15 -22 9 65.99 20.50 -9 -15 -22 54.49 13.30 22 -9 -15 125.39 16.60 -15 22 -9 99.29 28.50 9 -15 -22 107.79 24.50 15 -22 -9 74.79 21.00 -22 9 -15 99.19 29.70 -9 15 -22 129.69 29.80 15 -22 11 100.89 21.20 22 -11 -15 159.98 23.50 15 -22 -11 132.39 22.40 11 -15 -22 168.28 27.10 -22 11 -15 174.18 35.50 -11 15 -22 175.78 30.90 -15 22 -11 128.79 30.30 -15 22 -13 221.68 39.80 -13 15 -22 171.48 31.70 22 -13 -15 193.88 25.80 15 -22 -13 186.08 32.70 13 -15 -22 156.88 25.20 -22 13 -15 154.38 32.90 0 16 -22 19.00 22.30 -22 0 -16 35.20 24.80 16 -22 0 23.90 18.90 -16 22 0 39.10 23.00 2 16 -22 38.80 24.20 -22 -2 -16 78.09 27.90 -16 22 2 60.29 22.30 -16 22 -2 105.29 26.70 -2 16 -22 97.99 25.10 -22 2 -16 121.79 28.70 16 -22 -2 107.69 21.70 16 -22 4 261.47 32.90 -22 -4 -16 249.78 40.40 4 16 -22 256.37 40.90 -22 4 -16 247.78 36.30 16 -22 -4 237.68 35.00 -4 16 -22 258.17 42.10 -16 22 -4 308.17 45.50 16 -22 6 11.20 16.60 6 16 -22 27.30 21.50 -6 -16 -22 18.40 13.40 -16 22 -6 9.50 25.70 -22 6 -16 42.30 28.10 16 -22 -6 10.40 20.90 6 -16 -22 34.00 20.90 -6 16 -22 15.40 23.00 -8 -16 -22 73.79 14.20 16 -22 8 73.39 20.40 8 -16 -22 153.58 26.00 22 -8 -16 118.19 20.00 -8 16 -22 85.09 25.50 -16 22 -8 120.59 31.10 -22 8 -16 115.69 31.20 16 -22 -8 107.29 22.90 16 -22 10 -1.00 15.90 -22 10 -16 10.30 26.90 -10 16 -22 7.60 22.90 10 -16 -22 5.40 18.30 16 -22 -10 11.30 19.90 22 -10 -16 3.80 12.70 -16 22 -10 11.60 28.30 -16 22 -12 14.50 29.50 22 -12 -16 -4.40 13.00 -12 16 -22 12.00 23.80 16 -22 -12 10.00 17.60 -22 12 -16 34.00 28.60 12 -16 -22 4.80 20.00 17 -22 1 97.29 20.00 -17 22 1 154.48 26.70 -22 -1 -17 135.39 27.10 1 17 -22 147.29 27.40 -1 -17 -22 173.18 26.50 1 -17 -22 192.48 28.00 -17 22 -1 207.78 31.40 -1 17 -22 153.28 28.50 -22 1 -17 140.19 27.10 17 -22 -1 138.59 22.30 -3 -17 -22 186.38 27.40 -22 -3 -17 205.48 36.90 17 -22 3 207.28 32.00 3 17 -22 244.98 34.30 -3 17 -22 225.48 40.30 3 -17 -22 212.18 32.50 -22 3 -17 237.08 41.40 -17 22 -3 284.87 37.50 17 -22 -3 219.48 32.70 -5 -17 -22 145.59 23.50 17 -22 5 141.99 22.90 5 17 -22 157.48 28.70 -22 -5 -17 162.98 28.80 -22 5 -17 197.78 33.40 17 -22 -5 131.59 23.00 -17 22 -5 187.58 33.10 -5 17 -22 176.68 31.80 5 -17 -22 163.48 25.30 17 -22 7 175.98 23.80 -22 -7 -17 158.28 26.30 -7 -17 -22 153.78 19.80 17 -22 -7 135.29 23.40 -7 17 -22 177.38 31.30 -22 7 -17 130.39 28.70 7 -17 -22 86.79 21.70 -17 22 -7 115.69 29.00 -22 -9 -17 67.59 19.70 17 -22 9 56.69 17.00 -9 17 -22 87.79 28.60 9 -17 -22 36.10 18.90 22 -9 -17 68.39 14.60 -22 9 -17 83.39 29.40 17 -22 -9 54.99 19.40 -17 22 -9 41.00 25.60 0 -18 -22 175.98 27.80 -22 0 -18 228.68 32.40 -18 22 0 193.88 29.80 0 18 -22 158.08 29.30 18 -22 0 167.38 29.90 -2 -18 -22 135.79 19.10 18 -22 2 118.79 21.90 2 18 -22 86.49 25.70 -22 -2 -18 107.59 25.10 -22 2 -18 103.19 27.60 2 -18 -22 79.39 19.90 -2 18 -22 120.49 29.40 18 -22 -2 85.69 21.30 -18 22 -2 88.79 26.30 -22 -4 -18 166.78 27.40 4 18 -22 188.08 31.10 -4 -18 -22 179.08 24.30 4 -18 -22 199.98 31.40 -18 22 -4 198.08 32.40 -22 4 -18 146.89 28.60 18 -22 -4 130.79 22.90 -4 18 -22 223.48 32.70 -22 -6 -18 576.94 53.99 6 18 -22 626.84 56.89 -6 -18 -22 596.84 45.60 18 -22 6 582.54 50.29 18 -22 -6 591.84 51.49 6 -18 -22 584.54 52.29 -18 22 -6 623.04 61.99 -6 18 -22 617.54 60.49 -22 6 -18 583.54 59.49 18 -22 8 106.29 20.70 -22 -8 -18 118.49 23.10 -22 8 -18 143.39 29.90 18 -22 -8 170.88 24.60 22 -8 -18 140.19 21.90 8 -18 -22 159.78 25.40 -18 22 -8 122.79 31.00 -8 18 -22 100.19 27.40 -19 22 1 22.70 19.90 1 19 -22 26.40 22.60 -22 -1 -19 19.30 20.50 19 -22 1 15.00 16.30 -1 -19 -22 6.30 14.30 -1 19 -22 26.10 24.30 -19 22 -1 9.10 22.00 1 -19 -22 17.00 15.40 19 -22 -1 2.20 14.70 -22 1 -19 20.70 21.60 -3 -19 -22 188.38 25.00 19 -22 3 181.18 29.10 3 19 -22 221.08 38.20 -22 -3 -19 177.18 27.50 -22 3 -19 130.19 27.60 -3 19 -22 156.08 30.80 3 -19 -22 167.98 29.70 19 -22 -3 175.08 29.40 -19 22 -3 221.78 32.90 -5 -19 -22 290.77 26.70 -22 -5 -19 263.27 33.60 5 19 -22 337.87 41.70 19 -22 5 288.57 32.90 19 -22 -5 254.27 33.80 -22 5 -19 224.68 41.10 -19 22 -5 285.07 39.30 5 -19 -22 243.68 33.80 -5 19 -22 234.98 42.60 0 -20 -22 23.50 14.80 -20 22 0 15.20 20.20 -22 0 -20 28.60 19.70 20 -22 0 26.80 16.40 0 20 -22 13.20 22.00 20 -22 2 18.00 15.60 -22 -2 -20 6.60 17.00 2 20 -22 22.40 24.00 -2 -20 -22 3.60 12.90 2 -20 -22 45.50 16.80 -22 2 -20 22.70 19.90 -20 22 -2 65.99 24.80 20 -22 -2 31.50 15.70 -2 20 -22 27.90 24.00 0 23 -1 231.18 38.20 0 23 1 162.28 27.90 0 -23 -1 214.08 25.20 0 -23 1 231.98 25.70 0 23 -3 253.87 43.00 0 23 3 276.37 38.90 0 -23 3 318.77 29.60 0 -23 -3 275.27 29.50 0 23 5 1.40 16.70 0 -23 -5 3.00 14.20 0 -23 5 17.50 13.40 0 23 -5 9.90 26.30 0 -23 7 31.40 13.80 0 23 -7 25.00 28.30 0 -23 -7 24.90 15.50 0 -23 9 151.08 23.20 -23 9 0 71.99 27.40 0 -23 -9 109.79 18.30 0 23 -9 81.59 30.10 -23 11 0 474.35 53.89 0 -23 -11 489.85 41.00 0 23 -11 420.86 56.09 -23 13 0 334.17 47.60 23 -13 0 319.67 30.60 0 -23 -13 340.27 32.90 0 23 -13 312.87 53.19 0 23 -15 373.86 54.39 0 -23 -15 391.56 35.60 -23 15 0 404.76 48.20 23 -15 0 365.66 34.20 0 -23 -17 2.50 13.50 23 -17 0 5.40 13.30 0 23 -17 17.60 26.20 -23 17 0 3.80 22.10 0 -23 -19 42.20 15.10 23 -19 0 16.10 14.20 0 23 -19 54.89 27.90 -23 19 0 49.10 22.50 -1 -23 0 205.48 25.70 1 23 0 221.18 39.30 -1 23 0 226.48 39.00 1 -23 0 224.18 26.40 1 -23 2 78.89 15.50 -1 -23 -2 90.09 16.50 1 23 -2 37.20 23.80 -1 23 2 77.19 22.90 1 -23 -2 143.49 22.40 -1 23 -2 127.49 24.90 -1 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197.58 33.90 -1 23 -16 203.98 39.40 1 -23 -16 163.58 26.30 1 23 -18 126.39 28.40 23 -18 1 150.38 19.10 -1 -23 -18 135.59 18.40 -23 18 1 129.99 26.50 23 -18 -1 124.89 18.30 -23 18 -1 141.79 29.00 1 -23 -18 125.69 19.00 -1 23 -18 120.99 31.60 2 23 -1 79.89 27.40 -2 23 1 47.40 21.40 2 -23 1 75.99 17.00 -2 -23 -1 82.69 15.30 -2 -23 -3 61.79 14.00 2 -23 3 69.69 17.50 2 23 -3 40.50 24.10 -2 23 3 57.39 20.20 -2 23 -3 112.89 25.80 -2 -23 -5 96.19 15.50 2 -23 5 99.49 18.20 2 23 -5 70.39 30.00 2 -23 -5 71.09 16.30 -2 -23 5 92.39 15.70 -2 23 -5 65.39 25.60 -2 -23 -7 45.10 13.80 2 23 -7 44.10 27.10 2 -23 7 61.09 17.60 2 -23 -7 47.50 16.50 -2 -23 7 29.30 13.30 -2 23 -7 19.00 24.80 2 -23 9 163.28 26.40 -23 9 2 138.79 29.30 -2 -23 -9 179.58 23.40 2 23 -9 108.29 30.00 -23 9 -2 250.37 43.60 2 -23 -9 200.98 27.10 -2 23 -9 165.78 31.80 2 23 -11 164.28 36.40 -23 11 2 137.29 28.30 -2 -23 -11 182.28 25.00 -23 11 -2 171.38 30.20 -2 23 -11 155.28 31.50 -2 -23 -13 192.88 23.10 2 23 -13 195.38 33.30 2 -23 -13 142.39 20.40 23 -13 -2 120.39 21.00 -13 2 -23 135.79 23.50 -23 13 -2 93.89 27.60 -2 23 -13 134.69 35.70 -23 15 2 169.38 27.20 23 -15 2 180.58 23.30 2 23 -15 157.78 31.60 -2 -23 -15 178.18 23.90 -15 2 -23 140.09 23.90 2 -23 -15 113.59 19.40 23 -15 -2 136.09 23.60 -23 15 -2 179.48 32.60 -2 23 -15 120.59 32.80 23 -17 2 41.10 15.10 -2 -23 -17 44.00 14.80 2 23 -17 31.70 28.50 -23 17 2 33.10 21.60 -23 17 -2 39.30 24.20 -2 23 -17 66.59 32.90 23 -17 -2 76.09 15.50 3 -23 0 287.57 30.40 -3 23 0 297.37 39.80 -3 -23 0 273.87 27.30 3 23 0 275.47 42.40 -3 -23 -2 71.89 14.30 3 23 -2 59.69 25.40 3 -23 2 80.69 17.80 -3 23 2 43.60 20.90 3 23 2 127.19 24.20 3 -23 4 278.47 29.40 -3 23 4 252.47 34.00 -3 -23 -4 257.37 25.70 3 23 -4 181.28 32.50 -3 23 -4 233.18 42.20 -3 -23 4 214.18 25.40 3 -23 -4 245.18 29.20 3 23 -6 257.57 46.00 -3 -23 -6 274.27 26.60 3 -23 6 296.87 30.40 -3 -23 6 240.58 26.80 3 -23 -6 239.98 30.60 -3 23 -6 251.07 38.70 -23 8 3 232.68 40.80 3 -23 8 257.77 29.50 -3 -23 -8 234.28 25.30 3 23 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2.90 30.60 23 -13 -4 81.39 15.10 -23 13 -4 57.89 26.70 -13 4 -23 61.39 19.60 4 -23 -13 67.69 17.90 -4 23 -13 82.09 33.90 -4 -23 -15 193.68 25.30 -23 15 4 203.18 30.60 4 23 -15 204.48 38.10 23 -15 4 192.98 26.50 -15 4 -23 280.37 34.90 -23 15 -4 300.57 45.80 -4 23 -15 319.37 52.19 4 -23 -15 302.17 31.50 4 23 -17 81.29 30.40 23 -17 -4 28.30 15.00 -17 4 -23 37.10 18.90 -23 17 -4 18.50 24.70 -4 23 -17 39.30 30.90 4 -23 -17 34.80 18.00 5 23 0 9.60 22.60 -5 23 0 11.50 20.40 -5 -23 0 1.20 10.50 5 -23 0 15.60 16.40 -5 -23 -2 103.99 14.40 5 23 -2 102.69 29.10 5 -23 2 77.49 16.80 -5 23 2 102.09 24.10 5 23 2 99.99 26.40 5 -23 -2 75.19 17.30 -5 23 -2 93.49 27.50 -5 -23 2 98.99 14.20 5 23 -4 796.22 76.79 5 -23 4 958.10 66.59 -5 23 4 870.91 69.59 -5 -23 -4 862.61 62.99 -5 23 -4 787.32 74.69 -5 -23 4 911.01 63.19 -4 5 -23 846.62 66.19 5 -23 -4 900.71 66.39 -5 -23 -6 102.89 17.90 5 -23 6 94.89 19.10 5 23 -6 103.89 32.10 -6 5 -23 94.39 18.50 5 -23 -6 89.49 18.30 -5 23 -6 84.49 27.10 -23 8 5 89.39 23.90 5 23 -8 91.19 33.20 -5 -23 -8 107.79 19.40 5 -23 8 93.89 19.70 5 -23 -8 177.28 27.30 -5 23 -8 186.68 34.40 -23 8 -5 129.49 31.30 5 23 -10 83.69 33.70 -23 10 5 70.29 23.50 -5 -23 -10 76.59 14.40 5 -23 10 70.09 18.00 -10 5 -23 79.79 20.40 -23 10 -5 83.09 30.20 5 -23 -10 74.09 18.50 -5 23 -10 60.99 30.20 -23 12 5 77.49 21.90 5 23 -12 68.99 32.20 -5 -23 -12 73.49 14.00 -23 12 -5 47.30 31.10 -5 23 -12 59.59 30.00 -12 5 -23 32.80 19.90 23 -12 -5 38.30 13.80 5 -23 -12 35.30 19.00 5 23 -14 58.39 28.80 23 -14 5 57.69 14.50 -23 14 5 90.99 19.90 -5 -23 -14 59.39 13.70 23 -14 -5 60.09 15.40 5 -23 -14 52.09 18.20 -23 14 -5 50.39 27.20 -14 5 -23 64.99 20.60 -5 23 -14 42.50 29.20 5 23 -16 261.07 39.60 23 -16 5 193.48 26.10 -5 -23 -16 199.08 23.50 5 -23 -16 189.68 30.90 -5 23 -16 257.77 40.30 -23 16 -5 282.07 38.80 23 -16 -5 213.78 27.50 -16 5 -23 210.38 34.20 5 23 -18 87.29 27.00 23 -18 5 92.99 16.60 -5 -23 -18 95.09 14.50 23 -18 -5 90.59 17.00 5 -23 -18 105.09 20.40 -5 23 -18 106.09 31.50 -18 5 -23 72.49 20.10 18 -5 -23 107.39 18.10 -23 18 -5 121.29 29.90 6 -23 -1 68.19 16.80 -6 23 -1 51.69 24.10 -1 6 -23 65.79 20.40 -6 -23 1 80.59 12.60 6 23 -3 246.58 36.80 6 -23 3 262.87 31.10 -6 -23 -3 276.37 24.00 -6 23 3 281.57 35.90 -3 6 -23 247.18 29.90 6 -23 -3 224.68 31.10 -6 -23 3 242.68 24.10 -6 23 -3 232.28 41.70 6 -23 5 77.19 18.00 6 23 -5 87.09 29.00 -6 -23 -5 94.69 16.70 6 -23 -5 83.49 18.90 -5 6 -23 99.59 19.30 -6 23 -5 89.89 28.30 -6 -23 -7 118.69 18.50 6 -23 7 136.19 21.60 6 23 -7 93.59 32.30 -23 7 -6 92.49 29.00 -6 23 -7 80.09 26.90 6 -23 -7 164.28 22.80 -7 6 -23 159.98 22.80 -6 -23 -9 111.69 18.10 -23 9 6 115.69 23.80 6 23 -9 91.69 30.60 6 -23 9 149.49 21.90 6 -23 -9 76.39 18.90 -9 6 -23 97.19 22.10 -6 23 -9 92.09 32.40 -23 9 -6 108.09 33.30 6 -23 11 348.27 37.40 6 23 -11 347.47 54.39 -23 11 6 351.46 41.60 -6 -23 -11 339.37 30.50 23 -11 -6 367.66 30.40 6 -23 -11 351.56 37.60 -11 6 -23 363.06 40.50 -6 23 -11 361.36 53.99 -23 11 -6 376.96 52.89 6 23 -13 37.50 31.20 -6 -23 -13 44.50 12.00 -23 13 -6 12.80 29.60 23 -13 -6 10.70 13.80 -6 23 -13 13.30 31.80 -13 6 -23 7.70 18.50 6 -23 -13 -8.80 18.30 6 23 -15 303.77 40.90 -6 -23 -15 269.87 26.60 23 -15 6 270.67 27.30 6 -23 -15 191.58 32.40 -15 6 -23 199.08 35.00 23 -15 -6 206.38 28.20 -6 23 -15 270.77 42.00 23 -17 6 91.09 16.10 6 23 -17 99.49 30.20 6 -23 -17 44.60 17.80 -23 17 -6 143.39 31.70 23 -17 -6 78.29 16.60 -17 6 -23 76.59 21.20 -6 23 -17 89.49 30.90 0 7 -23 21.90 14.40 7 -23 0 14.70 18.30 -7 23 0 26.70 23.10 -7 -23 0 23.00 9.70 -7 23 2 27.90 20.10 -7 -23 -2 45.60 10.20 7 -23 2 61.89 19.10 7 23 -2 34.90 25.60 7 -23 -2 24.90 15.80 -7 23 -2 23.90 21.30 -2 7 -23 31.50 15.60 -7 -23 2 41.40 10.50 7 23 -4 135.29 30.00 -7 -23 -4 185.08 18.70 7 -23 4 189.78 27.70 -4 7 -23 190.88 28.60 7 -23 -4 136.39 21.60 -7 23 -4 125.09 28.70 -7 -23 -6 105.89 16.50 7 23 -6 65.19 27.90 7 -23 6 127.49 21.60 7 -23 -6 165.08 23.00 -6 7 -23 150.48 22.90 -23 6 -7 82.89 27.70 -7 23 -6 103.39 29.30 7 23 -8 36.70 27.60 -7 23 -8 198.08 33.50 7 23 -10 68.29 29.30 7 -23 10 63.79 17.80 -23 10 -7 96.39 29.50 -7 23 -10 168.38 34.80 7 23 -12 148.89 35.90 23 -12 -7 139.49 18.00 -23 12 -7 128.89 34.60 7 -23 -12 113.59 22.90 -7 23 -12 120.09 34.10 -12 7 -23 129.39 25.60 7 23 -14 22.30 28.30 -23 14 -7 41.90 29.80 23 -14 -7 9.30 14.00 -14 7 -23 16.10 19.20 -7 23 -14 26.00 30.20 7 -23 -14 14.00 16.60 7 23 -16 355.56 50.19 -7 23 -16 403.96 55.29 23 -16 -7 339.67 34.30 -23 16 -7 377.06 51.69 -16 7 -23 326.27 41.20 7 -23 -16 353.86 37.90 8 -23 1 80.79 17.50 -8 23 1 105.79 25.00 1 8 -23 105.19 18.70 -1 8 -23 69.69 18.70 -8 23 -1 31.20 22.20 8 -23 -1 69.39 19.50 3 8 -23 245.48 31.70 8 23 -3 226.28 35.40 -8 23 3 251.97 34.60 8 -23 3 256.47 30.10 8 -23 -3 169.58 30.10 -3 8 -23 185.68 31.50 -8 23 -3 162.88 33.50 8 23 -5 92.89 30.20 8 -23 5 133.29 22.90 -8 23 -5 134.29 28.90 -5 8 -23 182.18 30.90 8 -23 -5 195.58 29.40 -7 8 -23 208.98 33.90 -23 7 -8 234.28 39.90 -8 23 -7 230.28 38.60 8 -23 9 92.89 19.70 8 23 -9 136.79 34.50 -8 23 -9 172.58 30.90 -23 9 -8 182.78 35.00 8 23 -11 160.48 32.70 8 -23 11 116.49 19.90 23 -11 -8 149.09 20.50 8 -23 -11 96.79 22.60 -8 23 -11 101.59 33.80 -11 8 -23 101.29 24.80 -23 11 -8 79.59 31.10 8 23 -13 42.30 24.40 -23 13 -8 41.20 25.90 -13 8 -23 52.29 22.40 23 -13 -8 39.20 14.70 -8 23 -13 61.69 33.10 8 -23 -13 43.50 19.20 8 -23 -15 102.59 21.20 -23 15 -8 95.69 27.10 23 -15 -8 142.99 24.30 -8 23 -15 165.48 36.00 -15 8 -23 147.99 26.00 23 -17 -8 202.18 25.90 8 -23 -17 184.78 31.10 17 -8 -23 200.68 30.10 -8 23 -17 158.78 32.70 -23 17 -8 206.98 36.00 -17 8 -23 189.98 34.10 0 9 -23 96.99 20.60 -9 23 0 90.19 24.20 9 -23 0 80.49 18.40 -9 23 2 166.08 27.90 2 9 -23 178.58 25.30 9 -23 2 152.88 28.40 -2 9 -23 244.88 32.20 9 -23 -2 245.48 30.60 -9 23 -2 243.18 40.00 4 9 -23 370.36 37.10 9 -23 4 329.97 36.80 -9 23 -4 358.96 48.70 -4 9 -23 392.96 41.20 9 -23 -4 383.66 37.30 9 23 -6 106.49 31.00 9 -23 6 137.19 22.80 -9 23 -6 106.29 32.60 9 -23 -6 88.89 20.90 -23 6 -9 58.39 27.70 -6 9 -23 93.69 22.40 9 23 -8 119.59 32.90 9 -23 8 93.29 20.50 -23 8 -9 125.29 29.40 9 -23 10 43.60 16.60 9 23 -10 87.29 31.50 -23 10 -9 23.30 28.00 9 -23 -10 23.50 19.90 -9 23 -10 16.50 30.70 -10 9 -23 22.80 21.30 9 23 -12 379.46 50.89 9 -23 12 365.46 38.80 9 -23 -12 334.77 39.00 23 -12 -9 377.66 33.70 -9 23 -12 410.26 56.79 -12 9 -23 358.36 44.10 -23 12 -9 391.86 55.29 -9 23 -14 15.80 24.90 9 -23 -14 18.80 19.10 -23 14 -9 39.10 29.50 -14 9 -23 38.00 22.30 23 -14 -9 16.80 14.40 16 -9 -23 449.26 41.90 -9 23 -16 460.15 57.59 9 -23 -16 416.16 42.30 -16 9 -23 398.46 47.00 -23 16 -9 446.56 55.29 23 -16 -9 401.86 37.60 1 10 -23 106.49 21.60 -10 23 1 98.39 23.80 10 -23 1 70.69 18.50 -1 10 -23 111.59 22.50 10 -23 -1 107.39 22.00 -10 23 -1 100.19 25.50 -10 23 3 110.29 23.40 3 10 -23 112.69 21.70 10 -23 3 77.29 18.60 -3 10 -23 168.48 25.10 -10 23 -3 128.09 28.20 10 -23 5 61.19 19.30 -5 10 -23 71.89 21.90 10 -23 -5 53.79 18.90 -23 5 -10 40.30 26.10 -10 23 -5 57.89 26.60 10 -23 7 91.89 21.40 -7 10 -23 147.89 26.10 -23 7 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353.66 52.79 -9 12 -23 391.76 45.30 12 -23 -9 356.46 40.30 -12 23 -9 400.96 54.79 12 -23 11 641.64 52.49 23 -11 -12 576.84 47.80 12 -23 -11 593.44 54.09 -11 12 -23 643.24 60.19 -12 23 -11 680.73 67.49 -23 11 -12 625.64 65.29 -13 12 -23 230.18 39.20 23 -13 -12 196.58 25.00 12 -23 -13 199.58 33.70 13 -12 -23 136.99 23.90 -12 23 -13 242.58 39.00 -23 13 -12 180.68 32.40 13 -23 0 286.77 35.40 -13 23 0 332.57 42.90 0 13 -23 305.97 40.90 13 -23 2 204.08 29.90 -13 23 2 225.38 34.10 -13 23 -2 151.08 30.30 -2 13 -23 135.39 25.80 -23 2 -13 121.09 32.10 13 -23 -2 79.89 20.90 -13 23 -4 60.89 26.10 13 -23 -4 78.39 22.70 -4 13 -23 90.59 25.30 -23 4 -13 103.39 30.60 13 -23 6 25.60 19.60 13 -23 -6 16.90 20.50 -23 6 -13 0.70 26.70 -13 23 -6 17.30 27.20 -6 13 -23 -0.70 21.60 13 -23 8 44.70 19.40 13 -23 -8 32.00 21.50 -8 13 -23 37.50 22.60 -13 23 -8 53.39 31.20 -23 8 -13 80.39 31.40 13 -23 10 68.19 19.90 -13 23 -10 75.79 31.20 -10 13 -23 74.09 24.10 13 -23 -10 60.79 21.00 -23 10 -13 93.99 30.50 12 -13 -23 248.78 31.50 23 -12 -13 202.08 26.10 -23 12 -13 291.97 40.90 -12 13 -23 239.68 34.60 -13 23 -12 225.58 38.90 1 14 -23 168.98 28.20 14 -23 1 154.78 25.40 -14 23 1 168.18 28.20 -14 23 -1 253.27 39.70 -23 1 -14 254.97 44.40 14 -23 3 109.19 20.20 -23 3 -14 77.29 29.20 -3 14 -23 110.39 26.80 14 -23 -3 93.99 21.60 -14 23 -3 133.99 31.00 14 -23 5 32.00 16.90 5 14 -23 60.19 21.50 14 -23 -5 53.09 21.00 -5 14 -23 51.49 24.20 -23 5 -14 38.80 28.20 -14 23 -5 53.59 28.90 14 -23 7 12.90 18.70 -23 7 -14 19.70 24.80 14 -23 -7 8.80 19.80 -7 14 -23 29.10 22.80 -14 23 -7 -0.30 27.60 -9 -14 -23 23.40 11.60 14 -23 9 17.60 18.20 14 -23 -9 23.90 20.90 -9 14 -23 9.20 23.40 -23 9 -14 37.00 27.10 -14 23 -9 17.80 28.00 14 -23 11 255.37 33.00 -23 11 -14 305.77 40.70 11 -14 -23 271.47 37.50 -11 14 -23 229.08 40.50 23 -11 -14 254.27 27.30 -14 23 -11 275.87 41.20 14 -23 -11 237.88 35.60 -23 0 -15 313.97 48.50 -15 23 0 368.86 43.90 0 15 -23 413.86 45.80 15 -23 0 339.67 38.50 2 15 -23 217.88 30.50 -23 -2 -15 215.48 32.70 15 -23 2 178.68 25.30 -15 23 2 216.78 34.00 -15 23 -2 174.78 31.90 15 -23 -2 133.89 24.70 -23 2 -15 153.88 33.20 -2 15 -23 179.08 31.30 15 -23 4 181.78 30.30 4 15 -23 168.48 28.20 -23 4 -15 265.67 45.10 15 -23 6 214.98 31.50 -15 23 -6 287.97 39.00 15 -23 -6 192.28 33.80 -23 6 -15 178.68 34.60 -6 15 -23 184.38 31.40 -8 -15 -23 192.98 20.50 15 -23 8 182.58 29.40 -23 8 -15 103.99 28.80 15 -23 -8 124.79 23.90 8 -15 -23 131.39 26.00 -8 15 -23 142.59 28.70 -15 23 -8 149.09 32.60 15 -23 10 119.89 21.70 -23 10 -15 151.18 31.50 10 -15 -23 96.39 21.20 23 -10 -15 156.98 21.80 15 -23 -10 148.99 24.10 -15 23 -10 125.79 32.20 -10 15 -23 170.38 29.30 16 -23 1 174.68 30.20 -23 -1 -16 160.08 28.90 1 16 -23 215.68 36.60 -16 23 1 203.78 35.10 -16 23 -1 170.08 30.00 -23 1 -16 145.19 29.80 -1 16 -23 169.98 30.00 16 -23 3 283.67 34.30 -23 -3 -16 280.87 42.60 3 16 -23 280.37 39.10 -16 23 -3 275.17 44.80 -3 16 -23 277.87 41.00 16 -23 -3 229.08 34.70 -23 3 -16 230.38 35.60 16 -23 5 185.48 30.40 -23 -5 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13.3088 -4.1154 11 18 13 -8.1200 -15.1592 11 18 15 -5.1541 9.1749 11 18 17 -2.0610 -1.5264 11 19 12 4.2410 -5.7296 11 19 14 -14.6170 7.6673 11 19 16 -24.7783 5.5262 11 19 18 -3.0942 -6.7807 11 20 11 -26.6616 -4.2339 11 20 13 2.4830 -9.6741 11 20 15 -3.8321 -1.8105 11 20 17 3.6607 -11.4752 11 20 19 12.3397 11.0287 11 21 12 -5.0090 -0.8360 11 21 14 5.2907 -8.6495 11 21 16 8.4654 -14.5594 11 21 18 0.9409 0.0019 11 22 11 7.2998 -1.9283 11 22 13 10.8164 -8.7400 11 22 15 -10.2977 -14.4618 11 23 12 7.1119 10.0854 11 23 14 -3.8590 12.7676 11 24 11 -5.8973 7.3915 11 24 13 2.6344 8.4204 11 25 12 -10.8750 6.6260 12 12 12 19.7970 -10.5049 12 13 13 19.9437 -40.8668 12 14 12 -10.1546 10.4156 12 14 14 20.0404 -0.0046 12 15 13 20.1373 9.4974 12 15 15 8.1275 -23.8004 12 16 12 -1.7349 -32.7271 12 16 14 -8.5171 -26.4195 12 16 16 5.7664 -28.2268 12 17 13 7.8412 -2.4835 12 17 15 4.5365 -25.0490 12 17 17 -16.3277 2.6230 12 18 12 -6.9707 23.4075 12 18 14 -9.8035 -4.1353 12 18 16 3.7247 -9.5367 12 18 18 5.4604 7.4690 12 19 13 -5.2104 -20.1396 12 19 15 -11.4955 -11.5324 12 19 17 16.0272 5.4852 12 19 19 9.2650 7.0874 12 20 12 5.4471 14.7330 12 20 14 18.7338 -4.9472 12 20 16 3.6240 7.3444 12 20 18 -3.5420 0.5062 12 21 13 -11.6816 27.2345 12 21 15 -8.8310 14.9325 12 21 17 -1.3456 -2.9743 12 22 12 -7.5080 -5.3866 12 22 14 -8.3756 -4.8296 12 22 16 -4.8899 7.7947 12 23 13 4.8291 -3.4062 12 24 12 17.8144 11.3291 13 14 13 -29.6399 1.0738 13 15 14 -44.5953 6.4420 13 16 13 26.9605 1.6512 13 16 15 14.8774 -0.1408 13 17 14 -25.3246 -7.4783 13 17 16 3.7248 -1.1647 13 18 13 -9.1563 2.2294 13 18 15 -7.6996 2.0983 13 18 17 -7.2535 -7.4375 13 19 14 -4.2714 -7.7440 13 19 16 -1.2382 -7.5202 13 19 18 6.1251 -0.0636 13 20 13 12.1702 -13.7123 13 20 15 8.6588 -12.3824 13 20 17 -4.0765 2.7424 13 21 14 -6.2419 0.7106 13 21 16 1.8103 -8.2071 13 22 13 4.7989 5.8531 13 22 15 4.8520 2.7037 14 14 14 -6.4608 9.7538 14 15 15 -27.8240 -19.4288 14 16 14 -14.2073 -9.8229 14 16 16 -5.1906 -11.0871 14 17 15 -8.7321 3.4610 14 17 17 6.0335 16.7597 14 18 14 -6.0109 7.3813 14 18 16 0.0196 -3.4873 14 18 18 15.3554 11.5015 14 19 15 1.3796 -6.9070 14 19 17 -2.4933 1.0942 14 20 14 -0.4074 -14.7484 14 20 16 5.0678 5.4141 14 21 15 1.2030 6.8184 14 22 14 -4.0706 -10.5652 15 16 15 -1.0347 4.0391 15 17 16 3.5171 2.7212 15 18 15 -3.1896 -3.4082 15 18 17 5.6458 3.2671 15 19 16 3.3718 9.0075 15 20 15 8.3470 9.1639 16 16 16 33.0530 -8.4317 16 17 17 -18.6364 8.2747 16 18 16 0.0464 30.9219 0 0 0 0.0 0.0 ; _shelx_fab_checksum 28157 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1/2, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.33301(4) 0.41079(6) 0.33301(4) 0.0192(6) Uani 1 2 d S TU P . . O1 O 0.3582(2) 0.3582(2) 0.3582(2) 0.0113(13) Uani 1 6 d S TU P . . O2 O 0.3918(2) 0.4438(2) 0.3244(2) 0.0414(19) Uani 1 1 d . U . . . O3 O 0.1736(9) 0.5655(10) 0.2579(15) 0.194(16) Uani 0.5 1 d D U P A -1 O4 O 0.3343(3) 0.3854(2) 0.2669(2) 0.052(2) Uani 1 1 d . . . . . N1 N 0.3036(3) 0.4686(4) 0.3036(3) 0.045(3) Uani 1 2 d DS TU P . . N2 N 0.2378(9) 0.5727(4) 0.2325(9) 0.050(4) Uani 0.5 1 d D U P A -1 H2 H 0.2531 0.5810 0.2092 0.060 Uiso 0.5 1 calc R U P A -1 C1 C 0.4313(3) 0.4313(3) 0.3223(4) 0.0180(18) Uani 1 2 d S TU P . . C2 C 0.4668(3) 0.4668(3) 0.3228(5) 0.030(3) Uani 1 2 d S TU P . . C3 C 0.4559(4) 0.5109(5) 0.3235(5) 0.084(5) Uani 1 1 d . . . . . H3 H 0.4256 0.5194 0.3239 0.101 Uiso 1 1 calc R U . . . C4 C 0.2019(9) 0.6010(10) 0.2438(10) 0.121(9) Uani 0.5 1 d D U P A -1 C5 C 0.2526(6) 0.5340(8) 0.2526(6) 0.109(8) Uani 1 2 d DS TU P . . C6 C 0.2429(5) 0.5240(7) 0.2983(5) 0.143(8) Uani 1 1 d D U . . . H6 H 0.2189 0.5388 0.3123 0.172 Uiso 1 1 calc R U . . . C7 C 0.2679(5) 0.4929(6) 0.3233(5) 0.112(5) Uani 1 1 d D U . . . H7 H 0.2608 0.4881 0.3536 0.135 Uiso 1 1 calc R U . . . C8 C 0.3547(3) 0.3547(3) 0.2511(4) 0.0155(18) Uani 1 2 d S TU P . . C14 C 0.2072(5) 0.6469(6) 0.1765(6) 0.086(9) Uani 0.311(8) 1 d DG U P A -1 H14 H 0.2348 0.6335 0.1692 0.103 Uiso 0.621(15) 1 calc R U P A -1 C11 C 0.1912(6) 0.6826(6) 0.1512(5) 0.086(7) Uani 0.621(15) 1 d G U P A -1 H11 H 0.2080 0.6933 0.1268 0.104 Uiso 0.621(15) 1 calc R U P A -1 C10 C 0.1505(6) 0.7023(5) 0.1620(6) 0.087(6) Uani 0.621(15) 1 d G U P A -1 C9 C 0.1258(5) 0.6864(6) 0.1981(7) 0.069(8) Uani 0.311(8) 1 d G U P A -1 H9 H 0.0982 0.6998 0.2054 0.083 Uiso 0.621(15) 1 calc R U P A -1 C12 C 0.1418(5) 0.6508(7) 0.2234(6) 0.108(9) Uani 0.621(15) 1 d DG U P A -1 H12 H 0.1250 0.6400 0.2478 0.129 Uiso 0.621(15) 1 calc R U P A -1 C13 C 0.1825(5) 0.6310(6) 0.2126(6) 0.115(9) Uani 0.621(15) 1 d DG U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0202(7) 0.0172(10) 0.0202(7) -0.0024(6) -0.0033(9) -0.0024(6) O1 0.0113(13) 0.0113(13) 0.0113(13) 0.0002(8) 0.0002(8) 0.0002(8) O2 0.017(3) 0.044(4) 0.063(5) 0.016(4) 0.000(3) 0.000(3) O3 0.092(13) 0.164(18) 0.33(4) 0.12(2) 0.082(17) 0.054(13) O4 0.084(6) 0.033(4) 0.037(4) 0.007(3) -0.031(4) -0.015(4) N1 0.055(5) 0.023(6) 0.055(5) 0.005(4) -0.029(6) 0.005(4) N2 0.050(4) 0.050(4) 0.051(4) 0.0002(14) -0.0001(14) 0.0001(14) C1 0.0180(18) 0.0180(18) 0.018(2) 0.0006(9) 0.0006(9) -0.0003(13) C2 0.019(4) 0.019(4) 0.051(9) -0.004(4) -0.004(4) 0.001(5) C3 0.028(7) 0.101(12) 0.122(13) 0.027(10) 0.007(8) -0.020(7) C4 0.103(12) 0.126(14) 0.133(16) 0.051(12) 0.053(12) 0.060(11) C5 0.120(9) 0.086(11) 0.120(9) 0.036(8) 0.010(11) 0.036(8) C6 0.141(14) 0.155(15) 0.134(11) 0.065(11) 0.036(10) 0.089(13) C7 0.117(9) 0.099(9) 0.121(9) 0.017(7) 0.007(7) 0.045(7) C8 0.0155(18) 0.0155(18) 0.016(2) -0.0005(10) -0.0005(10) 0.0002(14) C14 0.081(12) 0.071(12) 0.105(12) 0.006(9) 0.004(8) 0.010(9) C11 0.079(9) 0.072(10) 0.108(11) 0.005(8) 0.017(8) 0.023(7) C10 0.088(9) 0.081(9) 0.094(10) 0.024(8) 0.018(7) 0.037(7) C9 0.069(8) 0.069(8) 0.069(8) -0.0001(14) -0.0001(14) 0.0003(14) C12 0.086(11) 0.109(14) 0.128(15) 0.048(13) 0.027(11) 0.031(10) C13 0.085(11) 0.110(14) 0.151(15) 0.046(12) 0.026(10) 0.036(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Fe1 O2 96.3(3) . . ? O1 Fe1 O2 96.3(3) . 21 ? O1 Fe1 O4 93.7(3) . 21 ? O1 Fe1 O4 93.7(3) . . ? O1 Fe1 N1 178.4(5) . . ? O2 Fe1 O2 89.1(4) . 21 ? O2 Fe1 O4 169.7(3) . 21 ? O2 Fe1 O4 92.3(3) 21 21 ? O2 Fe1 O4 92.3(3) . . ? O2 Fe1 O4 169.7(3) 21 . ? O2 Fe1 N1 84.9(3) 21 . ? O2 Fe1 N1 84.9(3) . . ? O4 Fe1 O4 84.6(5) 21 . ? O4 Fe1 N1 85.1(3) 21 . ? O4 Fe1 N1 85.1(3) . . ? Fe1 O1 Fe1 119.96(3) . 9 ? Fe1 O1 Fe1 119.96(3) . 5 ? Fe1 O1 Fe1 119.96(3) 9 5 ? C1 O2 Fe1 133.2(7) . . ? C8 O4 Fe1 130.7(7) . . ? C7 N1 Fe1 123.8(6) 21 . ? C7 N1 Fe1 123.8(6) . . ? C7 N1 C7 111.1(12) 21 . ? C4 N2 H2 114.9 . . ? C5 N2 H2 114.9 . . ? C5 N2 C4 130(3) . . ? O2 C1 O2 124.7(11) 13 . ? O2 C1 C2 117.4(6) 13 . ? O2 C1 C2 117.4(6) . . ? C3 C2 C1 121.2(7) . . ? C3 C2 C1 121.2(7) 13 . ? C3 C2 C3 117.6(13) . 13 ? C2 C3 C3 121.2(7) . 14_665 ? C2 C3 H3 119.4 . . ? C3 C3 H3 119.4 14_665 . ? N2 C4 O3 94(2) . . ? N2 C4 C13 122.3(19) . . ? C13 C4 O3 115(3) . . ? N2 C5 C6 122(2) . . ? N2 C5 C6 113.2(18) . 21 ? C6 C5 C6 110.0(17) . 21 ? C5 C6 H6 118.7 . . ? C7 C6 C5 122.5(11) . . ? C7 C6 H6 118.7 . . ? N1 C7 H7 119.4 . . ? C6 C7 N1 121.3(9) . . ? C6 C7 H7 119.4 . . ? O4 C8 O4 128.5(12) . 13 ? C11 C14 H14 120.0 . . ? C11 C14 C13 120.0 . . ? C13 C14 H14 120.0 . . ? C14 C11 H11 120.0 . . ? C14 C11 C10 120.0 . . ? C10 C11 H11 120.0 . . ? C9 C10 C11 120.0 . . ? C10 C9 H9 120.0 . . ? C10 C9 C12 120.0 . . ? C12 C9 H9 120.0 . . ? C9 C12 H12 120.0 . . ? C13 C12 C9 120.0 . . ? C13 C12 H12 120.0 . . ? C14 C13 C4 120.6(10) . . ? C12 C13 C4 118.3(10) . . ? C12 C13 C14 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 O1 1.8967(19) . ? Fe1 O2 2.030(6) 21 ? Fe1 O2 2.030(6) . ? Fe1 O4 2.114(7) 21 ? Fe1 O4 2.114(7) . ? Fe1 N1 2.125(11) . ? O1 Fe1 1.8967(19) 5 ? O1 Fe1 1.8967(19) 9 ? O2 C1 1.238(8) . ? O3 C4 1.42(2) . ? O4 C8 1.196(9) . ? N1 C7 1.417(10) . ? N1 C7 1.417(10) 21 ? N2 H2 0.8700 . ? N2 C4 1.41(2) . ? N2 C5 1.37(2) . ? C1 O2 1.238(8) 13 ? C1 C2 1.497(18) . ? C2 C3 1.358(17) . ? C2 C3 1.358(17) 13 ? C3 C3 1.40(3) 14_665 ? C3 H3 0.9400 . ? C4 C13 1.42(2) . ? C5 C6 1.428(15) . ? C5 C6 1.428(15) 21 ? C6 H6 0.9400 . ? C6 C7 1.405(15) . ? C7 H7 0.9400 . ? C8 O4 1.196(9) 13 ? C14 H14 0.9400 . ? C14 C11 1.3900 . ? C14 C13 1.3900 . ? C11 H11 0.9400 . ? C11 C10 1.3900 . ? C10 C9 1.3900 . ? C9 H9 0.9400 . ? C9 C12 1.3900 . ? C12 H12 0.9400 . ? C12 C13 1.3900 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Fe1 O2 C1 O2 2(2) . . . 13 ? Fe1 O2 C1 C2 -170.6(8) . . . . ? Fe1 O4 C8 O4 -13(2) . . . 13 ? Fe1 N1 C7 C6 -165.0(16) . . . . ? O2 Fe1 O1 Fe1 -132.8(6) 21 . . 9 ? O2 Fe1 O1 Fe1 43.1(7) 21 . . 5 ? O2 Fe1 O1 Fe1 132.8(6) . . . 5 ? O2 Fe1 O1 Fe1 -43.1(7) . . . 9 ? O2 C1 C2 C3 175.7(13) . . . 13 ? O2 C1 C2 C3 2.9(19) 13 . . 13 ? O2 C1 C2 C3 -175.7(13) 13 . . . ? O2 C1 C2 C3 -2.9(19) . . . . ? O3 C4 C13 C14 -139(2) . . . . ? O3 C4 C13 C12 54(4) . . . . ? O4 Fe1 O1 Fe1 134.4(6) 21 . . 9 ? O4 Fe1 O1 Fe1 49.6(7) . . . 9 ? O4 Fe1 O1 Fe1 -134.4(6) . . . 5 ? O4 Fe1 O1 Fe1 -49.6(7) 21 . . 5 ? N2 C4 C13 C14 -25(4) . . . . ? N2 C4 C13 C12 167(2) . . . . ? N2 C5 C6 C7 -160(2) . . . . ? C1 C2 C3 C3 -179.3(8) . . . 14_665 ? C3 C2 C3 C3 2(2) 13 . . 14_665 ? C4 N2 C5 C6 -158(3) . . . 21 ? C4 N2 C5 C6 -23(4) . . . . ? C5 N2 C4 O3 -36(4) . . . . ? C5 N2 C4 C13 -160(3) . . . . ? C5 C6 C7 N1 -2(4) . . . . ? C6 C5 C6 C7 -24(4) 21 . . . ? C7 N1 C7 C6 28(3) 21 . . . ? C14 C11 C10 C9 0.0 . . . . ? C11 C14 C13 C4 -168(3) . . . . ? C11 C14 C13 C12 0.0 . . . . ? C11 C10 C9 C12 0.0 . . . . ? C10 C9 C12 C13 0.0 . . . . ? C9 C12 C13 C4 168(2) . . . . ? C9 C12 C13 C14 0.0 . . . . ? C13 C14 C11 C10 0.0 . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.623 -0.817 -0.760 18258.8 2305.5 ?