#------------------------------------------------------------------------------ #$Date: 2021-10-03 22:08:13 +0300 (Sun, 03 Oct 2021) $ #$Revision: 269464 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519037.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519037 loop_ _publ_author_name 'Zhang, Zong-Hui' 'Fang, Han' 'Xue, Dong-Xu' 'Bai, Junfeng' _publ_section_title ; Tuning Open Metal Site-Free ncb Type of Metal-Organic Frameworks for Simultaneously High Gravimetric and Volumetric Methane Storage Working Capacities. ; _journal_issue 37 _journal_name_full 'ACS applied materials & interfaces' _journal_page_first 44956 _journal_page_last 44963 _journal_paper_doi 10.1021/acsami.1c13757 _journal_volume 13 _journal_year 2021 _chemical_formula_moiety 'C60 H39 Fe3 N9 O16' _chemical_formula_sum 'C60 H39 Fe3 N9 O16' _chemical_formula_weight 1309.55 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2021-06-03 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 33.5266(5) _cell_length_b 33.5266(5) _cell_length_c 33.5266(5) _cell_measurement_reflns_used 8089 _cell_measurement_temperature 243(2) _cell_measurement_theta_max 39.28 _cell_measurement_theta_min 3.23 _cell_volume 37685.0(10) _computing_cell_refinement 'SAINT V8.40A (Bruker, 2019)' _computing_data_reduction 'SAINT V8.40A (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 243.0 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0400 _diffrn_reflns_av_unetI/netI 0.0394 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -6 _diffrn_reflns_number 16844 _diffrn_reflns_point_group_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_theta_full 39.522 _diffrn_reflns_theta_max 39.522 _diffrn_reflns_theta_min 1.863 _diffrn_source_current 50.0 _diffrn_source_power 2.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.035 _exptl_absorpt_correction_T_max 0.7478 _exptl_absorpt_correction_T_min 0.6341 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1012 before and 0.0861 after correction. The Ratio of minimum to maximum transmission is 0.8480. The \l/2 correction factor is Not present. ; _exptl_crystal_colour black _exptl_crystal_colour_primary black _exptl_crystal_density_diffrn 0.462 _exptl_crystal_description Polyhedron _exptl_crystal_F_000 5344 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.15 _refine_diff_density_max 0.656 _refine_diff_density_min -0.651 _refine_diff_density_rms 0.063 _refine_ls_abs_structure_details ; Flack x determined using 798 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.430(15) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.292 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 241 _refine_ls_number_reflns 2035 _refine_ls_number_restraints 848 _refine_ls_restrained_S_all 1.113 _refine_ls_R_factor_all 0.0879 _refine_ls_R_factor_gt 0.0836 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1062P)^2^+314.0114P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2322 _refine_ls_wR_factor_ref 0.2361 _reflns_Friedel_coverage 0.827 _reflns_Friedel_fraction_full 0.971 _reflns_Friedel_fraction_max 0.968 _reflns_number_gt 1891 _reflns_number_total 2035 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file am1c13757_si_004.cif _cod_data_source_block a _cod_original_cell_volume 37685.0(17) _cod_database_code 4519037 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.750 _shelx_estimated_absorpt_t_min 0.750 _olex2_refinement_description ; 1. Restrained distances C00J-N00F 1.5 with sigma of 0.05 C13-C00J = C00J-N00F 1.43 with sigma of 0.02 C00I-C15 = C15-C5 1.43 with sigma of 0.02 N00F-N00F_$1 1.43 with sigma of 0.01 C15-C5 = C5-C13 1.43 with sigma of 0.02 C5-C13 = C13-C00J 1.43 with sigma of 0.02 C8-C7 1.43 with sigma of 0.02 C39-C96 = C96-C00B 1.43 with sigma of 0.02 N3-C39 = C39-C96 1.43 with sigma of 0.02 O5-C8 1.43 with sigma of 0.02 N00A-C8 1.43 with sigma of 0.02 N00A-C00B 1.43 with sigma of 0.02 N3-C39 1.43 with sigma of 0.001 N00F-N1 1.25 with sigma of 0.001 O05-C00I 1.239 with sigma of 0.01 C11-C00I_$3 1.482 with sigma of 0.001 C13-N00F 2.477 with sigma of 0.04 C00I-C5 2.477 with sigma of 0.04 C5-C00J 2.477 with sigma of 0.04 C15-C13 2.477 with sigma of 0.04 C39-C00B 2.477 with sigma of 0.04 N3-C96 2.477 with sigma of 0.04 C8-C1 \\sim C8-C21 with sigma of 0.02 C6-C00I \\sim C5-C00I with sigma of 0.02 N1-C4 \\sim N1-C14 with sigma of 0.02 N00F-C9 \\sim N00F-C13 with sigma of 0.02 2. Restrained planarity N00F, C00J, C13, C5, C15 with sigma of 0.1 N1, C12, C4, C3, C11, C10, C14 with sigma of 0.1 N00F, C15, C6, C9, C00J, C13, C5 with sigma of 0.1 C00I, C15, C6, C9, C00J, C13, C5, N00F with sigma of 0.1 3. Uiso/Uaniso restraints and constraints C39 \\sim C96 \\sim C00B \\sim N3 \\sim N00A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A C00I \\sim C15 \\sim C6 \\sim C9 \\sim C00J \\sim C13 \\sim C5 \\sim C009 \\sim C00B \\sim C39 \\sim C96 \\sim C8 \\sim C7 \\sim C21 \\sim C23 \\sim C00P \\sim C2 \\sim C1 \\sim C12 \\sim C4 \\sim C3 \\sim C11 \\sim C10 \\sim C14 \\sim N3 \\sim N00A \\sim N00F \\sim N1: within 3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 3.8A Uanis(C23) \\sim Ueq, Uanis(C009) \\sim Ueq, Uanis(C21) \\sim Ueq, Uanis(C00P) \\sim Ueq, Uanis(C39) \\sim Ueq, Uanis(C00J) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C1) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C96) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O03) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C00I) \\sim Ueq, Uanis(O03) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(N3) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C2) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 4. Rigid body (RIGU) restrains C00J, C00I, N00F, C13, C5, C15, O05 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C00P, C23, C21, C7, C2, C1, C8, O5, N00A, C00B, C96 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C009, O02, Fe00 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C23, C00P, C2, C1, C7, C21 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C5, N00F, C15, C00J, C13, C3, C4, C6, C9, C10, N1, C11, C12, C14, C00I with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Fixed Sof: N00A(0.5) H00A(0.5) N00F(0.25) C15(0.25) C6(0.25) H6(0.25) C9(0.25) H9(0.25) C00J(0.25) C13(0.25) H13(0.25) C5(0.25) H5(0.25) O5(0.5) C8(0.5) C7(0.5) C21(0.5) H21(0.5) C23(0.5) H23(0.5) C00P(0.5) C2(0.5) H2(0.5) C1(0.5) H1(0.5) N1(0.25) C12(0.25) C4(0.25) H4(0.25) C3(0.25) H3(0.25) C11(0.25) C10(0.25) H10(0.25) C14(0.25) H14(0.25) 6.a Aromatic/amide H refined with riding coordinates: N00A(H00A), C6(H6), C9(H9), C13(H13), C5(H5), C39(H39), C96(H96), C21(H21), C23(H23), C2(H2), C1(H1), C4(H4), C3(H3), C10(H10), C14(H14) 6.b Fitted hexagon refined as free rotating group: C15(C6,C9,C00J,C13,C5), C7(C21,C23,C00P,C2,C1), C12(C4,C3,C11,C10,C14) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; a.res created by SHELXL-2014/7 TITL a_a.res in I-43m REM REM {'C00U': 'AtomInfo()', 'C00T': 'AtomInfo()', 'C00W': 'AtomInfo()', REM 'C00V': 'AtomInfo()', 'C00P': 'AtomInfo()', 'N008': 'AtomInfo()', REM 'N009': 'AtomInfo()', 'N006': 'AtomInfo()', 'N007': 'AtomInfo()', REM 'C00M': 'AtomInfo()', 'C00L': 'AtomInfo()', 'C00O': 'AtomInfo()', REM 'C00N': 'AtomInfo()', 'C00S': 'AtomInfo()', 'I001': 'AtomInfo()', REM 'O00E': 'AtomInfo()', 'N00G': 'AtomInfo()', 'O00Q': 'AtomInfo()', REM 'O00R': 'AtomInfo()', 'FE03': 'AtomInfo()', 'FE02': 'AtomInfo()', REM 'FE05': 'AtomInfo()', 'FE04': 'AtomInfo()', 'O00A': 'AtomInfo()', REM 'O00C': 'AtomInfo()', 'N00J': 'AtomInfo()', 'N00K': 'AtomInfo()', REM 'O00F': 'AtomInfo()', 'O00I': 'AtomInfo()', 'O00H': 'AtomInfo()', REM 'N00D': 'AtomInfo()', 'N00B': 'AtomInfo()'} REM CELL 1.54178 33.5266 33.5266 33.5266 90 90 90 ZERR 8 0.0005 0.0005 0.0005 0 0 0 LATT -2 SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM -Z,-Y,+X SYMM +Z,-Y,-X SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +Z,+X,+Y SYMM +Y,+Z,+X SYMM -Y,-Z,+X SYMM +Z,-X,-Y SYMM -Y,+Z,-X SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,-Z,-X SYMM +X,-Y,-Z SYMM -X,+Y,-Z SYMM -X,-Y,+Z SYMM -Y,-X,+Z SYMM +Y,+X,+Z SYMM -Z,+Y,-X SYMM +Z,+Y,+X SYMM +X,-Z,-Y SYMM +X,+Z,+Y SFAC C H Fe N O UNIT 480 312 24 72 128 EQIV $1 +Y,+X,+Z EQIV $2 1-Y,1-X,+Z EQIV $3 1-X,1-Y,+Z DFIX 1.5 0.05 C00J N00F DANG 2.477 C13 N00F DANG 2.477 C00I C5 DFIX 1.43 C13 C00J C00J N00F DANG 2.477 C5 C00J DFIX 1.43 C00I C15 C15 C5 DFIX 1.43 0.01 N00F N00F_$1 FLAT N00F C00J C13 C5 C15 DANG 2.477 C15 C13 DFIX 1.43 C15 C5 C5 C13 RIGU C00J C00I N00F C13 C5 C15 O05 DFIX 1.43 C5 C13 C13 C00J DFIX 1.43 C8 C7 RIGU C00P C23 C21 C7 C2 C1 C8 O5 N00A C00B C96 DFIX 1.43 C39 C96 C96 C00B DANG 2.477 C39 C00B DANG 2.477 N3 C96 DFIX 1.43 N3 C39 C39 C96 DFIX 1.43 O5 C8 DFIX 1.43 N00A C8 DFIX 1.43 N00A C00B DFIX 1.43 0.001 N3 C39 RIGU C009 O02 Fe00 RIGU C23 C00P C2 C1 C7 C21 ISOR 0.01 0.02 C23 C009 C21 C00P C39 C00J ISOR 0.01 0.02 C1 ISOR 0.01 0.02 C96 ISOR 0.01 0.02 O03 ISOR 0.001 0.002 C00I O03 ISOR 0.01 0.02 N3 SIMU C39 C96 C00B N3 N00A SADI C8 C1 C8 C21 ISOR 0.01 0.02 C2 DFIX 1.25 0.001 N00F N1 RIGU C5 N00F C15 C00J C13 C3 C4 C6 C9 C10 N1 C11 C12 C14 C00I SADI C6 C00I C5 C00I FLAT N1 C12 C4 C3 C11 C10 C14 SADI N1 C4 N1 C14 FLAT N00F C15 C6 C9 C00J C13 C5 SADI N00F C9 N00F C13 FLAT C00I C15 C6 C9 C00J C13 C5 N00F SIMU 0.01 0.02 3.8 $C $N DFIX 1.239 0.01 O05 C00I DFIX 1.482 0.001 C11 C00I_$3 L.S. 99 PLAN 2 SIZE 0.15 0.15 0.15 TEMP -30.15 CONF FREE C5 C00I_$2 FREE C5 C00I FREE N1 C14 FREE N1 C4 FREE O05 C15 FREE N00F C13 FREE N00F C9 FREE C6 C00I_$2 FREE C6 C00I FREE C8 C21 FREE C8 C1 MORE -1 ABIN BOND $H fmap 2 acta REM REM REM WGHT 0.106200 314.011414 FVAR 0.11514 FE00 3 0.644660 0.286483 0.713517 10.50000 0.03757 0.03886 = 0.03886 0.00233 -0.00682 0.00682 O02 5 0.668418 0.283479 0.773194 11.00000 0.08656 0.08722 = 0.03961 0.01276 -0.00774 -0.03168 O03 5 0.692300 0.307700 0.692300 10.16667 0.04151 0.04151 = 0.04151 0.00010 -0.00010 0.00010 N3 4 0.586788 0.263326 0.736674 10.50000 0.10259 0.10768 = 0.10768 0.00479 0.00478 -0.00478 O05 5 0.615771 0.339041 0.722729 11.00000 0.01785 0.07486 = 0.14260 -0.02138 0.01882 0.00395 PART -1 N00A 4 0.480660 0.217751 0.776247 10.50000 0.10452 0.10851 = 0.10561 0.00527 0.00124 -0.00122 AFIX 43 H00A 2 0.468470 0.206656 0.756205 10.50000 -1.20000 AFIX 0 N00F 4 0.532623 0.502979 0.731728 10.25000 0.06472 0.06565 = 0.05998 -0.00034 -0.00038 -0.00179 PART 0 C00I 1 0.627490 0.372510 0.729184 10.50000 0.06045 0.06045 = 0.05988 -0.00002 0.00002 -0.00011 PART -1 AFIX 66 C15 1 0.604024 0.403942 0.729780 10.25000 0.06362 0.06395 = 0.05971 -0.00141 0.00125 -0.00001 C6 1 0.620752 0.441848 0.728317 10.25000 0.06409 0.06430 = 0.05993 -0.00089 0.00043 -0.00111 AFIX 43 H6 2 0.648591 0.444839 0.726857 10.25000 -1.20000 AFIX 65 C9 1 0.596314 0.475332 0.729012 10.25000 0.06404 0.06429 = 0.05979 -0.00034 0.00044 -0.00188 AFIX 43 H9 2 0.607627 0.500967 0.728023 10.25000 -1.20000 AFIX 65 C00J 1 0.555148 0.470911 0.731169 10.25000 0.06477 0.06452 = 0.06055 -0.00129 0.00032 -0.00151 C13 1 0.538419 0.433004 0.732632 10.25000 0.06419 0.06419 = 0.06054 -0.00042 0.00094 -0.00102 AFIX 43 H13 2 0.510579 0.430014 0.734092 10.25000 -1.20000 AFIX 65 C5 1 0.562856 0.399520 0.731938 10.25000 0.06390 0.06378 = 0.06010 -0.00126 0.00070 -0.00041 AFIX 43 H5 2 0.551542 0.373885 0.732927 10.25000 -1.20000 AFIX 0 PART 0 C009 1 0.687550 0.312450 0.787070 10.50000 0.05636 0.05636 = 0.04123 0.00689 -0.00689 -0.00624 C00B 1 0.519518 0.232507 0.767493 10.50000 0.10519 0.10679 = 0.10679 0.00746 0.00226 -0.00226 C39 1 0.578684 0.272831 0.777456 11.00000 0.10565 0.11113 = 0.10721 0.00435 0.00244 -0.00190 AFIX 43 H39 2 0.597589 0.285154 0.794094 11.00000 -1.20000 AFIX 0 C96 1 0.539158 0.262051 0.791224 11.00000 0.10328 0.10896 = 0.10479 0.00559 0.00353 -0.00239 AFIX 43 H96 2 0.527366 0.273542 0.813918 11.00000 -1.20000 AFIX 0 PART -1 O5 5 0.475792 0.246816 0.837972 10.50000 0.09294 0.07217 = 0.08199 0.03334 -0.00849 0.01788 C8 1 0.458596 0.218215 0.812388 10.50000 0.10637 0.10836 = 0.10646 0.00684 0.00162 -0.00080 AFIX 66 C7 1 0.417170 0.210486 0.815441 10.50000 0.10530 0.10771 = 0.10540 0.00735 0.00119 0.00005 C21 1 0.400775 0.179281 0.793616 10.50000 0.10664 0.10744 = 0.10617 0.00669 0.00092 -0.00009 AFIX 43 H21 2 0.417533 0.160861 0.780733 10.50000 -1.20000 AFIX 65 C23 1 0.359599 0.175314 0.790840 10.50000 0.10613 0.10667 = 0.10567 0.00617 0.00241 0.00026 AFIX 43 H23 2 0.348512 0.154212 0.776080 10.50000 -1.20000 AFIX 65 C00P 1 0.334818 0.202551 0.809891 10.50000 0.10519 0.10836 = 0.10569 0.00580 0.00110 -0.00003 C2 1 0.351213 0.233756 0.831716 10.50000 0.10622 0.10727 = 0.10563 0.00563 0.00098 0.00014 AFIX 43 H2 2 0.334454 0.252176 0.844599 10.50000 -1.20000 AFIX 65 C1 1 0.392388 0.237724 0.834493 10.50000 0.10601 0.10807 = 0.10627 0.00500 0.00117 -0.00075 AFIX 43 H1 2 0.403475 0.258826 0.849253 10.50000 -1.20000 AFIX 0 N1 4 0.500241 0.512688 0.716002 10.25000 0.06477 0.06508 = 0.05934 -0.00107 -0.00049 -0.00286 AFIX 66 C12 1 0.466814 0.543116 0.718382 10.25000 0.06425 0.06575 = 0.05859 -0.00091 -0.00115 -0.00303 C4 1 0.475711 0.583085 0.724879 10.25000 0.06469 0.06541 = 0.05841 -0.00030 -0.00084 -0.00344 AFIX 43 H4 2 0.502388 0.591220 0.727761 10.25000 -1.20000 AFIX 65 C3 1 0.445162 0.611025 0.727116 10.25000 0.06471 0.06567 = 0.05814 0.00033 -0.00139 -0.00277 AFIX 43 H3 2 0.451180 0.638055 0.731509 10.25000 -1.20000 AFIX 65 C11 1 0.405716 0.598997 0.722856 10.25000 0.06431 0.06579 = 0.05747 0.00028 -0.00132 -0.00335 C10 1 0.396817 0.559028 0.716359 10.25000 0.06405 0.06597 = 0.05800 -0.00017 -0.00169 -0.00258 AFIX 43 H10 2 0.370141 0.550894 0.713478 10.25000 -1.20000 AFIX 65 C14 1 0.427366 0.531087 0.714121 10.25000 0.06443 0.06593 = 0.05826 -0.00067 -0.00155 -0.00331 AFIX 43 H14 2 0.421348 0.504058 0.709727 10.25000 -1.20000 AFIX 0 HKLF 4 REM a_a.res in I-43m REM R1 = 0.0836 for 1891 Fo > 4sig(Fo) and 0.0879 for all 2035 data REM 241 parameters refined using 848 restraints END WGHT 0.1407 362.8661 REM Highest difference peak 0.656, deepest hole -0.651, 1-sigma level 0.063 Q1 1 0.6832 0.3373 0.6927 11.00000 0.05 0.66 Q2 1 0.6814 0.3042 0.6732 11.00000 0.05 0.64 ; _shelx_res_checksum 83507 _shelx_hkl_file ; 0 1 1 625.54 47.30 -1 1 2 7109.79 547.25 -1 2 1 7471.35 547.35 1 -1 2 7023.60 547.35 2 -1 1 7117.39 547.25 1 2 1 7443.26 547.35 2 1 1 7470.45 547.35 -2 0 2 2656.13 200.98 0 2 2 2680.43 201.08 2 0 2 2669.93 201.08 -2 2 2 583.54 41.30 2 -2 2 565.04 41.40 2 2 2 484.75 41.50 1 0 3 759.12 57.39 -1 0 3 754.12 57.29 3 0 1 731.83 55.89 0 1 3 749.13 56.09 0 -1 3 737.63 56.09 -1 3 2 736.33 52.09 3 -2 1 684.33 51.89 2 -1 3 708.23 52.09 -2 1 3 709.43 51.99 3 2 1 673.03 52.09 1 3 2 677.63 52.19 -2 -1 3 646.94 51.99 2 1 3 648.44 52.09 3 -1 2 704.03 51.69 -3 1 2 701.83 51.49 1 -2 3 700.03 51.89 -1 2 3 690.33 51.79 1 2 3 661.83 51.89 3 1 2 635.44 51.79 -3 0 3 7071.89 536.15 0 3 3 7304.87 536.45 3 0 3 6995.20 536.35 -3 2 3 3551.84 290.07 -3 3 2 3624.34 290.07 -2 3 3 3587.14 290.17 2 -3 3 3630.54 290.27 3 -2 3 3679.13 290.17 2 3 3 4298.17 290.47 3 2 3 4168.48 290.37 3 3 2 4284.07 290.47 0 0 4 2895.91 218.38 2 0 4 40.70 5.20 0 4 2 32.00 4.40 -2 0 4 28.00 3.90 4 -1 1 7357.56 558.54 -1 1 4 7425.76 558.84 1 -1 4 7446.25 558.84 1 1 4 7376.26 558.84 -1 -1 4 7408.76 558.84 4 1 1 7521.65 558.74 -3 1 4 785.92 56.79 -1 4 3 805.22 57.09 3 -1 4 799.92 57.09 3 1 4 695.63 56.99 1 4 3 712.53 57.09 -3 -1 4 690.03 56.89 4 0 2 25.40 3.50 0 2 4 31.10 4.10 0 -2 4 27.80 4.00 -2 2 4 2257.87 157.28 2 -2 4 2278.37 157.48 4 -2 2 2192.78 157.18 2 4 2 2013.00 157.48 2 2 4 1813.92 157.38 4 2 2 1950.10 157.38 4 -1 3 768.22 56.19 -1 3 4 753.32 56.39 -4 1 3 783.92 55.99 1 -3 4 804.72 56.49 4 1 3 663.93 56.29 1 3 4 660.83 56.39 -4 3 3 482.25 33.80 -3 3 4 468.25 34.10 -3 4 3 464.85 34.00 3 -3 4 460.85 34.30 4 -3 3 457.95 34.10 3 4 3 433.46 34.50 3 3 4 382.36 33.60 4 3 3 390.86 33.60 4 3 3 435.46 34.50 -4 0 4 982.00 74.59 0 4 4 986.80 74.99 4 0 4 985.20 74.89 -4 4 4 649.43 53.29 4 -4 4 779.72 52.89 4 -4 4 659.83 53.49 -1 0 5 338.87 27.40 1 0 5 362.86 27.50 0 5 3 1857.61 134.69 3 0 5 1707.83 134.09 3 0 5 1770.02 134.59 -3 0 5 1780.02 134.39 5 0 1 337.67 26.30 0 1 5 355.86 26.90 0 -1 5 333.27 26.80 -2 1 5 351.06 27.60 5 -2 1 346.47 27.10 2 -1 5 366.26 27.90 4 -1 5 1731.83 133.39 -4 1 5 1725.63 133.19 -1 5 4 1736.13 133.49 4 -1 5 1678.93 132.79 1 5 4 1869.41 133.59 4 1 5 1722.43 132.79 -4 -1 5 1817.32 133.19 4 1 5 1817.32 133.39 5 -1 2 345.77 26.90 -1 2 5 353.36 27.40 3 -2 5 227.78 18.50 -3 2 5 218.18 18.10 -2 5 3 222.18 18.40 5 -3 2 226.98 17.70 3 -2 5 215.38 17.30 5 0 3 1758.52 132.39 0 -3 5 1747.03 132.59 -5 0 3 1762.12 132.09 0 3 5 1697.03 132.59 0 -3 5 1792.02 132.09 -2 3 5 207.38 17.80 2 -3 5 215.88 16.80 -5 2 3 221.48 16.80 2 -3 5 220.78 18.10 5 -2 3 209.68 17.40 -4 3 5 4049.29 306.97 -3 5 4 4078.29 307.07 5 -4 3 4058.49 306.97 4 -3 5 3977.20 306.67 3 -5 4 3936.91 306.67 4 -3 5 4090.29 307.17 5 -4 3 3870.51 306.57 4 3 5 4174.38 307.27 4 3 5 3926.41 306.67 3 5 4 4357.76 307.47 5 4 3 4288.47 307.37 5 -1 4 1652.13 130.09 5 -1 4 1723.43 130.49 -1 4 5 1688.43 130.69 1 -4 5 1694.03 130.09 1 -4 5 1660.53 130.69 -5 1 4 1770.62 130.29 -5 -1 4 1762.92 130.39 1 4 5 1844.22 130.79 5 1 4 1673.33 130.09 1 4 5 1761.02 130.09 5 1 4 1751.32 130.59 -3 4 5 4021.70 305.87 -5 3 4 4008.80 305.67 5 -3 4 3931.01 305.47 5 -3 4 4011.40 305.87 4 -5 3 3978.70 305.47 3 -4 5 4147.49 306.07 3 -4 5 3978.50 305.47 5 3 4 4193.18 306.17 3 4 5 4040.90 305.57 3 4 5 4252.87 306.27 5 3 4 4023.30 305.57 4 5 3 4107.09 306.27 -5 0 5 2097.79 159.38 0 5 5 2156.98 159.78 5 0 5 2024.00 159.08 5 0 5 2167.08 159.68 5 -2 5 1452.15 114.39 -5 2 5 1520.95 114.59 -2 5 5 1526.05 114.99 2 -5 5 1521.55 114.39 5 -2 5 1527.55 114.89 5 -5 2 1577.14 114.59 -5 -2 5 1484.45 114.79 2 5 5 1511.55 115.19 5 2 5 1519.45 115.09 -5 4 5 2600.64 185.08 -5 5 4 2637.04 185.08 -4 5 5 2635.94 185.28 4 -5 5 2526.15 184.78 4 -5 5 2582.94 185.48 5 -4 5 2542.85 185.38 5 -5 4 2553.14 184.78 5 -5 4 2590.24 185.38 5 -4 5 2476.65 184.78 4 5 5 2040.10 185.48 5 4 5 2079.99 185.38 5 5 4 2143.69 185.48 0 0 6 4624.04 348.97 -2 0 6 321.97 25.70 2 0 6 318.97 24.70 2 0 6 323.97 25.90 0 6 4 86.09 10.90 4 0 6 83.89 7.80 4 0 6 81.49 10.30 -4 0 6 84.69 9.40 1 -1 6 3065.39 246.68 1 -1 6 3108.69 247.18 6 -1 1 3189.18 246.78 -1 1 6 3316.97 247.18 -1 -1 6 3325.27 247.18 1 1 6 3321.27 246.68 6 1 1 3508.15 246.98 1 1 6 3375.06 247.28 3 -1 6 1168.68 87.39 6 -3 1 1139.09 86.69 -3 1 6 1178.18 87.19 3 -1 6 1119.99 86.59 -3 -1 6 1152.78 87.19 3 1 6 1122.59 87.39 -5 1 6 203.98 21.00 -1 6 5 227.48 21.90 -5 -1 6 303.67 21.30 5 1 6 310.87 22.00 0 -2 6 338.97 24.80 0 -2 6 322.97 25.90 0 2 6 306.27 25.90 6 0 2 317.27 25.30 2 -2 6 2880.21 209.38 6 -2 2 3072.19 209.48 -2 2 6 3052.39 209.88 2 -2 6 3035.60 209.98 -2 -2 6 2570.84 209.78 2 2 6 2512.05 209.88 6 2 2 2674.63 209.68 2 2 6 2435.26 209.28 4 -2 6 3634.84 261.77 6 -4 2 3428.86 261.27 -2 6 4 3679.03 261.77 4 -2 6 3525.45 261.07 -4 2 6 3541.75 261.47 4 2 6 3656.33 262.17 2 6 4 2803.02 261.67 6 -1 3 1137.39 84.99 1 -3 6 1155.58 85.39 -1 3 6 1135.69 85.29 1 -3 6 1145.19 84.69 6 1 3 1129.79 85.19 6 1 3 1065.49 84.59 1 3 6 1125.49 84.69 -1 -3 6 1113.89 84.59 1 3 6 1077.79 85.39 -3 3 6 4177.78 283.67 6 -3 3 4124.19 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8 3473.95 274.17 8 -1 1 3548.04 274.27 -1 1 8 3679.03 274.97 1 1 8 3891.91 275.07 -1 -1 8 3721.13 274.97 1 1 8 3747.53 274.27 -1 -1 8 3682.43 274.17 -3 1 8 2722.13 203.78 3 -1 8 2734.73 204.68 -3 1 8 2797.12 204.48 3 -1 8 2724.73 203.88 -3 -1 8 2595.44 203.78 -3 -1 8 2656.63 204.48 -5 1 8 2595.94 185.08 5 -1 8 2534.45 184.48 8 -5 1 2552.84 184.48 5 -1 8 2545.05 185.38 5 1 8 2376.06 184.48 5 1 8 2360.76 185.28 -5 -1 8 2318.27 184.98 -5 -1 8 2289.27 184.28 8 -7 1 367.96 27.80 -1 8 7 356.26 29.90 -7 1 8 352.16 29.00 7 -1 8 391.06 28.20 7 -1 8 376.46 29.80 1 8 7 348.27 30.10 7 1 8 340.27 29.80 7 1 8 371.06 28.20 -7 -1 8 349.27 29.00 0 -2 8 2233.98 162.08 0 -2 8 1985.60 161.18 8 0 2 2210.58 161.48 0 2 8 2090.19 161.18 0 2 8 2181.38 162.08 8 0 2 2135.29 161.28 2 -2 8 1121.89 71.09 -2 -2 8 805.42 70.79 8 2 2 850.51 70.39 -4 2 8 523.45 44.10 4 -2 8 526.55 43.20 8 -4 2 516.65 43.30 8 -4 2 513.45 43.00 4 -2 8 511.05 44.40 4 2 8 627.24 44.60 -4 -2 8 656.63 44.30 -4 -2 8 664.83 43.10 8 -6 2 170.48 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143.89 12.40 8 -2 14 152.08 19.40 -8 -2 14 126.89 12.60 8 2 14 134.59 16.70 -8 -2 14 150.28 17.80 8 2 14 135.79 14.20 -10 2 14 4.00 8.30 10 -2 14 16.20 6.40 2 -14 10 23.10 10.60 14 -10 2 22.80 4.30 10 -2 14 0.90 10.20 -10 2 14 14.20 3.60 2 -14 10 11.60 6.20 -10 -2 14 9.20 4.00 -10 -2 14 21.40 9.50 10 2 14 22.10 11.20 10 2 14 9.10 6.10 -12 2 14 234.08 23.90 2 -14 12 244.38 27.40 14 -12 2 231.68 21.00 12 -2 14 246.48 26.80 12 -2 14 236.18 22.30 2 -14 12 241.68 22.40 -2 -14 12 291.27 22.40 -12 -2 14 273.37 20.60 -12 -2 14 288.87 25.00 12 2 14 289.07 28.10 12 2 14 288.67 22.50 -2 -14 12 270.47 27.80 1 -3 14 345.47 26.50 1 -3 14 371.16 30.00 -1 3 14 339.27 26.40 -1 3 14 348.67 29.70 14 -1 3 370.46 26.10 -1 -3 14 262.57 29.20 1 3 14 253.67 29.40 -3 3 14 1153.78 88.29 -3 3 14 1167.08 90.19 3 -3 14 1183.38 88.49 14 -3 3 1203.48 88.19 3 -3 14 1179.38 90.39 -3 -3 14 1130.49 88.29 -3 -3 14 1175.78 90.29 3 3 14 1142.99 90.39 3 3 14 1147.09 88.49 5 -3 14 743.03 62.09 -5 3 14 761.82 63.79 14 -5 3 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366.66 29.40 14 -2 4 387.76 29.20 -2 4 14 381.56 32.60 14 -2 4 374.76 29.80 2 -4 14 362.06 29.60 2 -4 14 397.16 32.80 -2 -4 14 405.16 32.50 -2 -4 14 348.07 29.30 2 4 14 366.06 29.60 -4 4 14 364.36 29.30 -4 4 14 386.66 32.60 4 -4 14 366.16 29.70 4 -4 14 397.96 33.10 14 -4 4 376.56 29.60 14 -4 4 363.76 29.10 14 -6 4 438.36 36.70 -6 4 14 439.46 36.70 6 -4 14 432.86 40.20 6 -4 14 545.35 38.20 14 -6 4 405.96 37.10 -6 4 14 405.06 39.50 -6 -4 14 519.45 36.90 6 4 14 531.15 37.40 6 4 14 538.75 40.90 -6 -4 14 531.05 39.90 -8 4 14 189.78 15.10 14 -8 4 184.38 15.60 14 -8 4 201.48 16.40 8 -4 14 203.68 21.70 4 -14 8 192.98 16.70 -8 4 14 185.58 19.80 8 -4 14 204.48 16.60 8 4 14 154.28 16.70 -8 -4 14 170.58 20.00 8 4 14 168.78 22.10 -8 -4 14 157.88 15.40 14 -10 4 282.77 20.90 4 -14 10 277.47 21.90 10 -4 14 281.77 22.00 -10 4 14 291.17 24.50 10 -4 14 262.07 26.10 14 -10 4 256.57 21.80 4 -14 10 286.07 26.50 10 4 14 190.08 26.70 10 4 14 209.38 22.00 -10 -4 14 182.68 24.50 12 -4 14 86.09 13.60 12 -4 14 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14 415.46 39.90 14 -4 6 430.76 36.40 -4 6 14 466.85 39.60 4 6 14 534.25 37.10 -14 -4 6 536.55 37.50 -4 -6 14 517.05 36.60 -4 -6 14 541.45 39.70 6 -6 14 230.78 21.30 6 -6 14 225.58 25.50 14 -6 6 229.98 20.80 14 -6 6 239.78 22.10 -6 6 14 238.98 24.90 -6 -6 14 280.07 20.80 6 6 14 274.17 21.40 6 6 14 292.47 26.30 -6 -6 14 283.77 25.00 -8 6 14 28.00 9.70 6 -14 8 14.30 6.20 6 -14 8 14.50 9.70 14 -8 6 14.40 5.10 14 -8 6 12.70 6.90 8 -6 14 22.40 6.20 8 -6 14 16.60 10.50 -8 -6 14 10.50 9.40 8 6 14 20.80 11.10 8 6 14 24.80 6.20 -8 -6 14 33.00 5.30 14 -10 6 136.09 12.70 10 -6 14 144.89 16.70 -10 6 14 151.98 17.10 6 -14 10 138.69 13.80 14 -10 6 132.79 14.80 10 -6 14 130.69 13.50 6 -14 10 151.38 18.80 -10 -6 14 117.19 15.70 10 6 14 99.79 17.30 10 6 14 91.09 13.70 14 -12 6 136.19 12.30 12 -6 14 137.79 13.60 6 -14 12 134.19 13.70 12 -6 14 127.39 16.30 -12 6 14 125.99 15.20 6 -14 12 120.89 16.20 14 -12 6 117.49 14.60 -6 -14 12 92.49 16.00 -12 -6 14 101.79 14.80 12 6 14 85.19 16.00 12 6 14 93.39 13.80 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57.29 14.50 13 -13 14 38.50 14.50 14 -13 13 58.39 9.80 13 -14 13 42.50 14.60 13 -13 14 54.09 10.00 13 -14 13 50.89 9.70 -13 -13 14 104.39 16.60 -13 -14 13 100.29 18.10 -13 -13 14 84.99 9.70 -14 -13 13 88.29 16.80 -14 0 14 1377.66 104.89 0 -14 14 1385.66 104.19 0 -14 14 1389.06 106.99 14 -14 0 1334.57 103.39 14 0 14 1376.76 104.09 14 0 14 1335.17 106.69 14 -14 2 595.74 48.60 -14 2 14 607.84 49.60 14 -2 14 649.83 52.29 14 -2 14 634.94 48.90 2 -14 14 632.54 52.69 14 -14 2 634.04 48.10 14 -14 -2 648.44 47.70 -14 -2 14 621.44 50.39 -2 -14 14 628.04 49.00 14 2 14 608.44 49.10 14 2 14 623.94 52.79 14 -14 4 26.80 8.40 14 -4 14 48.30 8.70 -14 4 14 33.70 8.30 14 -14 4 46.90 7.00 14 -4 14 27.50 12.20 4 -14 14 49.00 8.80 4 -14 14 40.90 13.10 -4 -14 14 74.49 8.80 -14 -4 14 69.89 8.20 -14 -4 14 60.99 11.50 -4 -14 14 62.19 15.60 14 4 14 60.59 9.30 14 4 14 63.49 14.00 14 -6 14 37.80 7.90 14 -6 14 29.90 12.30 14 -14 6 24.10 6.80 14 -14 6 43.10 9.20 6 -14 14 37.20 7.80 6 -14 14 39.00 13.60 -6 -14 14 45.30 8.00 -6 -14 14 20.30 14.10 -14 -6 14 33.50 5.60 -14 -6 14 23.50 10.90 14 6 14 26.90 13.70 14 -8 14 25.70 7.70 14 -8 14 41.70 12.30 14 -14 8 24.30 6.90 14 -14 8 27.30 10.00 8 -14 14 29.80 7.90 8 -14 14 11.40 13.00 -8 -14 14 23.80 7.90 -8 -14 14 18.70 13.90 -14 -8 14 23.50 6.00 -14 -8 14 20.40 11.90 14 8 14 22.50 14.00 14 -10 14 75.19 10.60 14 -10 14 78.99 14.80 14 -14 10 77.89 9.90 14 -14 10 100.59 14.10 10 -14 14 79.09 10.70 10 -14 14 86.49 16.00 -10 -14 14 68.39 10.80 -10 -14 14 69.69 16.80 -14 -10 14 72.99 9.50 -14 -10 14 79.79 15.50 14 -14 12 453.85 42.80 14 -12 14 505.75 39.60 14 -12 14 485.25 43.50 14 -14 12 528.55 39.60 12 -14 14 530.45 44.50 12 -14 14 514.65 39.70 -12 -14 14 527.85 45.20 -12 -14 14 476.95 39.40 -14 -14 12 429.56 44.40 -14 -12 14 459.15 39.00 -14 -12 14 461.05 44.50 14 -14 14 958.80 82.79 14 -14 14 1012.30 79.89 -14 -14 14 1102.29 84.29 -14 -14 14 1072.69 79.79 -1 0 15 20.20 9.30 1 0 15 11.50 5.10 1 0 15 23.20 9.90 -1 0 15 12.90 5.00 3 0 15 814.52 62.39 3 0 15 751.92 59.79 -3 0 15 835.32 62.09 -3 0 15 741.93 59.59 -5 0 15 1112.19 88.79 5 0 15 1208.48 91.29 5 0 15 1157.78 89.09 -5 0 15 1216.58 90.89 -7 0 15 8.10 4.10 7 0 15 7.70 5.60 7 0 15 16.70 10.40 -7 0 15 12.40 9.10 -9 0 15 9.90 4.00 9 0 15 11.70 6.00 9 0 15 19.20 10.90 -9 0 15 8.00 8.80 -11 0 15 16.90 3.90 0 -15 11 12.10 6.70 -11 0 15 29.50 9.50 15 -11 0 15.20 3.80 11 0 15 20.60 12.00 11 0 15 19.60 6.70 0 -15 11 17.00 10.90 15 -13 0 1.90 3.80 -13 0 15 5.10 8.80 0 -15 13 -13.10 11.70 13 0 15 6.20 6.70 13 0 15 2.50 12.20 0 -15 13 1.50 7.00 0 1 15 15.30 5.00 0 -1 15 14.60 5.20 0 1 15 22.40 9.60 0 -1 15 5.90 9.40 -2 1 15 1911.51 148.89 -2 1 15 1802.82 147.19 2 -1 15 1911.81 149.09 2 -1 15 1837.62 147.29 -2 -1 15 2129.59 149.09 2 1 15 1961.90 147.29 2 1 15 2094.89 149.19 -2 -1 15 1954.10 147.19 15 -4 1 1038.40 83.99 -4 1 15 1123.19 86.39 4 -1 15 1085.89 84.59 4 -1 15 1097.89 86.79 -4 1 15 1090.69 84.29 4 1 15 1149.78 84.59 -4 -1 15 1173.28 86.49 -4 -1 15 1140.29 84.39 6 -1 15 307.87 28.60 15 -6 1 298.37 23.00 -6 1 15 305.67 23.50 -6 1 15 323.07 27.60 6 -1 15 324.27 24.50 -6 -1 15 268.87 23.60 6 1 15 285.37 24.40 6 1 15 272.57 28.30 -6 -1 15 284.47 27.40 15 -8 1 187.08 14.10 -8 1 15 178.68 14.50 -8 1 15 211.78 19.60 8 -1 15 179.58 16.20 8 -1 15 193.08 21.60 8 1 15 144.79 21.40 -8 -1 15 158.38 19.60 8 1 15 144.59 16.10 -8 -1 15 150.38 14.60 10 -1 15 362.96 34.40 -10 1 15 370.56 29.20 15 -10 1 385.46 29.20 10 -1 15 368.96 30.50 -10 1 15 377.06 32.80 10 1 15 385.06 34.60 -10 -1 15 362.46 29.30 -10 -1 15 392.06 33.10 10 1 15 388.46 30.60 1 -15 12 606.94 45.80 12 -1 15 561.44 49.10 -12 1 15 571.14 47.30 12 -1 15 577.54 45.70 1 -15 12 572.14 49.60 15 -12 1 594.04 44.70 -12 -1 15 570.84 47.50 12 1 15 573.84 45.70 -1 -15 12 615.44 45.80 12 1 15 575.64 49.50 -1 -15 12 570.64 49.50 1 -15 14 41.60 14.40 15 -14 1 44.10 5.80 -14 1 15 37.90 9.40 14 -1 15 54.69 8.20 14 -1 15 46.20 13.60 1 -15 14 41.90 8.20 -1 -15 14 38.00 8.30 14 1 15 26.80 13.10 -1 -15 14 31.30 13.30 14 1 15 37.00 8.80 -14 -1 15 36.00 10.10 1 -2 15 1917.51 147.19 -1 2 15 1974.20 147.19 1 -2 15 1821.22 145.29 -1 2 15 1806.92 145.29 -1 -2 15 1921.11 145.29 -1 -2 15 1906.51 146.99 1 2 15 2125.49 147.39 1 2 15 1925.41 145.39 -3 2 15 684.33 58.19 3 -2 15 643.14 55.99 15 -3 2 670.53 55.49 3 -2 15 657.73 58.59 -3 2 15 644.84 55.79 -3 -2 15 807.22 55.89 3 2 15 813.22 56.09 -3 -2 15 856.31 58.59 3 2 15 833.32 58.89 5 -2 15 1067.49 83.79 5 -2 15 1133.99 86.09 15 -5 2 1096.59 83.29 -5 2 15 1119.69 85.59 -5 2 15 1058.89 83.49 5 2 15 1092.09 85.99 5 2 15 1103.49 83.89 -5 -2 15 1062.59 83.49 -5 -2 15 1190.98 85.79 15 -7 2 30.10 4.40 -7 2 15 33.80 4.90 7 -2 15 39.10 11.00 7 -2 15 30.70 6.30 -7 2 15 25.50 9.50 7 2 15 8.90 9.90 7 2 15 11.40 6.20 -7 -2 15 6.50 9.30 -9 2 15 67.39 7.80 9 -2 15 66.49 13.00 15 -9 2 72.59 7.70 9 -2 15 71.79 8.70 -9 2 15 60.69 11.60 -9 -2 15 59.79 7.00 9 2 15 96.09 13.30 9 2 15 44.10 13.10 -9 -2 15 56.89 11.60 11 -2 15 331.27 32.30 11 -2 15 334.07 28.10 15 -11 2 329.07 26.80 -11 2 15 340.07 30.10 2 -15 11 329.87 28.20 2 -15 11 341.87 32.60 -11 -2 15 369.66 30.90 -11 -2 15 351.36 26.80 11 2 15 343.17 28.10 11 2 15 359.26 33.10 15 -13 2 652.13 46.70 2 -15 13 626.94 51.49 -13 2 15 619.44 48.80 13 -2 15 593.44 51.09 13 -2 15 624.34 47.70 2 -15 13 663.83 47.70 13 2 15 554.94 47.70 -2 -15 13 587.64 51.79 -2 -15 13 592.84 47.70 -13 -2 15 573.74 49.50 13 2 15 559.34 51.29 0 3 15 838.92 62.69 0 3 15 750.92 60.19 0 -3 15 741.13 60.19 0 -3 15 841.52 62.89 2 -3 15 666.33 57.09 -2 3 15 676.43 56.89 -2 3 15 643.44 54.49 2 -3 15 648.84 54.59 15 -2 3 666.33 54.29 -2 -3 15 848.12 57.39 -2 -3 15 768.72 54.59 2 3 15 798.32 54.79 4 -3 15 335.17 32.20 15 -4 3 319.37 27.80 4 -3 15 324.37 28.50 -4 3 15 313.67 28.10 -4 3 15 319.47 31.50 4 3 15 406.56 28.80 -4 -3 15 402.96 28.30 -4 -3 15 411.16 32.00 4 3 15 420.96 32.60 -6 3 15 9.20 9.10 6 -3 15 3.60 9.70 6 -3 15 1.70 5.50 15 -6 3 3.10 3.90 -6 3 15 8.20 4.40 6 3 15 10.00 9.60 -6 -3 15 11.90 4.70 6 3 15 11.40 5.50 -6 -3 15 8.00 9.00 -8 3 15 41.10 5.70 15 -8 3 41.20 5.70 8 -3 15 37.70 7.30 -8 3 15 35.70 10.10 8 -3 15 36.70 11.30 -8 -3 15 67.09 7.50 8 3 15 65.39 12.90 8 3 15 51.09 7.00 -8 -3 15 61.79 11.10 -10 3 15 110.89 12.90 10 -3 15 114.19 12.40 10 -3 15 102.99 14.80 3 -15 10 102.79 12.20 3 -15 10 91.69 14.60 15 -10 3 109.49 10.00 -10 -3 15 82.69 13.20 10 3 15 83.29 15.60 10 3 15 81.59 12.20 -10 -3 15 79.69 9.90 -12 3 15 495.95 40.60 12 -3 15 471.75 38.80 15 -12 3 490.65 37.90 3 -15 12 433.86 42.70 12 -3 15 478.75 42.50 3 -15 12 490.35 39.00 -12 -3 15 505.85 41.30 12 3 15 504.55 39.10 -12 -3 15 479.55 37.70 -3 -15 12 492.15 39.10 -3 -15 12 509.85 43.30 12 3 15 528.15 43.50 14 -3 15 203.78 25.00 14 -3 15 196.08 19.30 15 -14 3 198.88 17.50 3 -15 14 201.48 19.40 3 -15 14 213.98 25.90 -14 3 15 204.58 20.10 14 3 15 232.98 26.30 14 3 15 206.88 19.70 -14 -3 15 198.38 22.20 -3 -15 14 199.88 19.50 -3 -15 14 216.28 26.80 1 -4 15 1090.29 88.49 -1 4 15 1146.59 88.59 15 -1 4 1119.39 86.29 1 -4 15 1091.79 86.49 -1 4 15 1096.19 86.39 1 4 15 1204.68 88.79 -1 -4 15 1170.18 86.49 1 4 15 1144.59 86.49 -1 -4 15 1182.98 88.59 3 -4 15 307.57 31.80 15 -3 4 330.77 27.40 -3 4 15 308.67 27.60 -3 4 15 314.87 31.20 3 -4 15 325.97 28.00 -3 -4 15 395.46 27.70 3 4 15 418.46 32.10 -3 -4 15 425.66 31.80 -5 4 15 280.17 25.30 5 -4 15 280.67 21.40 5 -4 15 280.77 26.00 15 -5 4 265.87 20.50 -5 4 15 271.17 20.70 -5 -4 15 225.68 20.70 -5 -4 15 237.08 25.10 5 4 15 234.88 26.30 5 4 15 215.58 21.30 7 -4 15 102.19 12.00 15 -7 4 96.19 10.30 -7 4 15 96.59 10.30 -7 4 15 117.39 13.90 7 -4 15 103.29 14.50 -7 -4 15 115.79 13.80 7 4 15 106.29 12.20 7 4 15 112.89 15.30 -7 -4 15 104.49 10.60 4 -15 9 -0.10 6.00 9 -4 15 -0.30 6.10 -9 4 15 -0.50 8.90 4 -15 9 1.80 10.00 15 -9 4 7.20 4.50 9 -4 15 13.50 10.80 -9 -4 15 5.30 4.40 9 4 15 3.00 10.70 -9 -4 15 1.30 9.40 9 4 15 3.70 6.30 11 -4 15 199.58 23.10 11 -4 15 185.58 17.60 15 -11 4 192.68 16.10 -11 4 15 177.98 20.30 4 -15 11 186.18 17.60 4 -15 11 182.08 23.10 11 4 15 186.98 24.30 -11 -4 15 184.48 21.40 -11 -4 15 171.28 15.70 11 4 15 191.98 17.80 15 -13 4 517.85 39.70 -13 4 15 510.35 41.70 4 -15 13 516.75 44.80 13 -4 15 514.55 44.20 4 -15 13 578.14 40.80 13 -4 15 532.65 40.60 -4 -15 13 524.45 40.70 13 4 15 465.95 45.10 -13 -4 15 466.15 39.30 -4 -15 13 489.45 45.10 -13 -4 15 484.15 43.00 15 0 5 1208.78 90.89 0 5 15 1183.78 90.29 15 0 5 1219.38 90.09 0 -5 15 1187.98 92.49 0 5 15 1192.68 92.59 0 -5 15 1134.49 90.19 2 -5 15 1096.69 85.69 -2 5 15 1167.38 85.69 -2 5 15 1094.79 83.29 15 -2 5 1061.69 83.79 15 -2 5 1122.69 83.19 2 -5 15 1030.20 83.39 2 5 15 1133.09 85.99 2 5 15 1094.59 83.49 -2 -5 15 1129.39 85.49 -2 -5 15 1046.90 83.29 4 -5 15 271.77 21.60 -4 5 15 265.87 21.10 15 -4 5 275.77 20.90 15 -4 5 272.87 21.60 4 -5 15 316.27 26.60 -4 5 15 289.47 25.80 -4 -5 15 217.68 25.20 4 5 15 210.98 26.10 4 5 15 226.58 21.70 -4 -5 15 227.28 21.00 6 -5 15 47.10 7.00 6 -5 15 44.50 11.80 15 -6 5 50.89 7.10 -6 5 15 49.80 11.00 -6 5 15 55.59 6.20 15 -6 5 54.29 6.10 6 5 15 18.70 11.00 -6 -5 15 17.40 10.40 6 5 15 27.30 7.10 8 -5 15 74.79 9.30 5 -15 8 75.69 8.90 15 -8 5 72.79 8.80 15 -8 5 70.09 9.20 8 -5 15 71.99 13.50 -8 5 15 78.09 12.30 8 5 15 83.19 14.80 8 5 15 75.09 9.30 -8 -5 15 80.39 12.50 -8 -5 15 85.69 9.20 -10 5 15 9.40 9.50 10 -5 15 14.50 6.90 15 -10 5 20.90 6.30 5 -15 10 7.40 6.50 10 -5 15 8.90 11.10 15 -10 5 11.70 5.00 5 -15 10 13.10 11.40 -10 -5 15 6.90 9.90 10 5 15 21.40 12.40 10 5 15 11.10 12.00 -10 -5 15 7.40 4.60 5 -15 12 155.38 17.40 5 -15 12 173.48 23.30 12 -5 15 176.58 17.60 -12 5 15 165.18 19.60 15 -12 5 174.78 17.30 12 -5 15 156.58 23.00 15 -12 5 169.48 16.00 -12 -5 15 189.68 22.10 12 5 15 214.98 24.60 -5 -15 12 225.08 24.60 -12 -5 15 197.28 15.60 12 5 15 189.88 17.50 14 -5 15 156.18 23.20 5 -15 14 146.79 20.50 15 -14 5 168.68 16.00 5 -15 14 166.08 17.70 -14 5 15 140.19 17.40 14 -5 15 182.78 17.50 14 5 15 182.38 18.00 -14 -5 15 183.08 15.10 14 5 15 204.18 25.70 -5 -15 14 183.08 17.90 -5 -15 14 205.58 26.20 -14 -5 15 202.98 22.00 15 -1 6 323.47 23.60 -1 6 15 298.67 28.30 -1 6 15 293.87 23.80 1 -6 15 301.27 23.80 1 -6 15 302.37 28.00 15 -1 6 289.07 25.00 1 6 15 305.37 28.40 -1 -6 15 258.47 27.70 -1 -6 15 270.37 23.50 1 6 15 272.77 23.90 15 1 6 287.37 23.60 15 1 6 278.77 25.30 3 -6 15 8.90 10.40 15 -3 6 12.00 6.70 -3 6 15 6.90 4.90 -3 6 15 5.40 10.10 15 -3 6 8.20 4.70 3 -6 15 10.30 5.60 -15 -3 6 8.10 5.20 3 6 15 15.40 6.00 3 6 15 14.70 10.00 -3 -6 15 7.80 5.10 -3 -6 15 15.90 9.30 5 -6 15 50.89 11.70 15 -5 6 48.00 6.20 15 -5 6 48.50 8.00 5 -6 15 52.49 7.30 -5 6 15 53.79 11.30 -5 -6 15 21.30 10.90 5 6 15 23.00 12.50 15 -7 6 276.77 22.70 -7 6 15 293.77 27.30 7 -6 15 282.17 28.00 7 -6 15 274.87 23.50 6 -15 7 271.27 23.20 15 -7 6 269.37 23.80 -7 -6 15 263.57 22.60 7 6 15 296.07 28.80 7 6 15 299.47 23.60 -7 -6 15 288.57 27.40 9 -6 15 162.48 20.90 6 -15 9 143.79 19.90 15 -9 6 121.29 14.60 6 -15 9 151.38 14.50 9 -6 15 131.19 14.20 15 -9 6 149.59 13.20 -9 6 15 169.28 18.50 9 6 15 125.89 18.00 -9 -6 15 123.09 12.90 9 6 15 116.89 14.40 -9 -6 15 128.79 16.30 6 -15 11 1.80 6.60 11 -6 15 4.50 11.70 11 -6 15 4.00 6.70 -11 6 15 2.80 8.90 15 -11 6 3.50 6.90 6 -15 11 0.90 11.00 15 -11 6 6.70 5.40 -11 -6 15 14.60 10.80 11 6 15 26.70 12.10 -11 -6 15 14.60 5.00 11 6 15 27.00 7.90 15 -13 6 123.19 13.00 13 -6 15 110.89 13.00 6 -15 13 97.89 15.60 6 -15 13 98.99 13.20 -13 6 15 97.69 11.60 13 -6 15 103.09 15.60 15 -13 6 87.49 11.00 -6 -15 13 67.59 17.00 -13 -6 15 68.09 8.60 -13 -6 15 76.49 14.00 13 6 15 57.99 16.40 -6 -15 13 67.29 10.40 0 7 15 9.60 5.40 0 7 15 7.10 11.10 15 0 7 10.70 8.00 0 -7 15 7.20 5.30 0 -7 15 8.10 10.10 15 0 7 10.80 5.40 15 -2 7 12.40 7.60 2 -7 15 32.10 11.10 2 -7 15 25.00 5.90 -2 7 15 25.80 11.00 -2 -7 15 8.50 16.00 -2 -7 15 12.10 5.50 15 2 7 21.40 8.90 15 2 7 10.90 5.90 2 7 15 12.20 10.00 2 7 15 11.20 5.50 -4 7 15 104.29 14.60 15 -4 7 103.89 11.40 15 -4 7 124.39 14.10 4 -7 15 109.29 15.30 4 -7 15 97.59 12.20 -15 -4 7 118.29 13.10 4 7 15 114.19 15.70 -4 -7 15 105.99 14.20 4 7 15 115.59 12.20 -4 -7 15 102.69 11.60 7 -15 6 281.47 23.80 15 -6 7 285.47 23.40 6 -7 15 320.57 28.70 15 -6 7 290.17 24.80 6 -7 15 281.77 24.00 -6 7 15 261.57 27.80 6 7 15 278.87 24.10 -6 -7 15 297.67 27.90 -6 -7 15 300.27 23.50 6 7 15 284.77 29.00 15 -8 7 69.19 9.80 7 -15 8 59.99 12.60 15 -8 7 65.29 8.00 8 -7 15 111.59 13.40 7 -15 8 53.99 8.60 8 -7 15 67.89 13.60 -8 7 15 60.09 12.50 8 7 15 74.19 9.60 -8 -7 15 73.49 9.50 8 7 15 73.69 13.30 -8 -7 15 79.69 13.00 7 -15 10 14.00 6.60 10 -7 15 10.00 6.80 15 -10 7 9.20 5.50 7 -15 10 8.00 10.70 15 -10 7 12.00 7.60 10 -7 15 3.70 11.30 -10 7 15 13.20 9.80 -10 -7 15 21.90 11.00 10 7 15 8.90 12.80 -10 -7 15 16.40 5.40 7 -15 12 42.90 8.60 15 -12 7 65.49 8.10 7 -15 12 60.59 13.60 15 -12 7 62.69 10.20 12 -7 15 75.79 9.30 12 -7 15 57.99 13.90 -12 7 15 55.29 10.50 12 7 15 67.89 15.50 -12 -7 15 67.69 9.20 -12 -7 15 75.89 13.50 7 -15 14 53.19 15.20 14 -7 15 83.69 14.90 7 -15 14 74.09 10.50 15 -14 7 84.69 9.70 14 -7 15 67.39 10.40 -14 -7 15 111.29 15.00 -7 -15 14 88.69 10.60 -14 -7 15 91.29 10.10 -7 -15 14 90.59 17.90 14 7 15 72.99 16.40 1 -8 15 185.28 21.20 1 -8 15 178.08 15.60 15 -1 8 190.58 15.60 -1 8 15 178.48 21.60 15 -1 8 180.78 18.40 -1 -8 15 145.39 20.60 1 8 15 171.88 21.60 -1 -8 15 138.19 15.40 15 1 8 153.98 19.10 15 1 8 163.88 15.60 15 -3 8 34.00 6.90 3 -8 15 40.40 7.20 3 -8 15 30.20 11.40 15 -3 8 46.50 9.50 -3 8 15 34.20 11.30 3 8 15 46.00 11.90 -3 -8 15 60.99 7.10 -15 -3 8 61.59 7.90 -3 -8 15 77.79 12.70 15 3 8 66.99 11.00 5 -8 15 76.09 13.90 5 -8 15 78.39 9.30 15 -5 8 68.09 10.00 8 -15 5 81.99 8.90 15 -5 8 62.89 10.60 -5 8 15 96.19 13.80 5 8 15 85.09 13.30 -5 -8 15 75.19 10.20 -5 -8 15 76.19 13.30 -15 -5 8 91.19 10.90 7 -8 15 54.39 13.10 8 -15 7 66.29 12.30 7 -8 15 58.09 8.50 8 -15 7 56.59 8.20 15 -7 8 58.49 9.90 15 -7 8 61.69 7.80 -7 8 15 72.99 13.10 7 8 15 76.19 13.90 -15 -7 8 76.29 11.10 -7 -8 15 65.29 7.90 -7 -8 15 61.99 12.60 8 -15 9 91.09 14.20 15 -9 8 99.19 11.20 -9 8 15 99.99 13.70 15 -9 8 86.49 11.70 9 -8 15 94.89 14.90 8 -15 9 91.89 12.00 9 -8 15 105.09 12.50 9 8 15 76.69 15.30 -9 -8 15 83.59 10.80 -9 -8 15 90.09 14.60 11 -8 15 18.20 12.10 -11 8 15 17.50 9.00 8 -15 11 8.70 6.90 15 -11 8 12.00 8.40 8 -15 11 6.50 11.40 11 -8 15 14.80 7.30 15 -11 8 12.20 6.20 -11 -8 15 10.60 5.70 11 8 15 19.30 13.50 -11 -8 15 7.30 11.20 8 -15 13 62.39 9.60 15 -13 8 66.09 11.40 13 -8 15 72.69 15.00 8 -15 13 65.59 14.80 13 -8 15 68.19 9.70 15 -13 8 79.79 9.20 -13 -8 15 69.79 14.30 -8 -15 13 67.99 15.90 -13 -8 15 70.69 8.40 13 8 15 76.79 17.20 -8 -15 13 77.79 10.20 15 0 9 4.10 5.70 0 -9 15 -5.20 10.00 0 9 15 2.70 11.40 0 -9 15 9.70 5.80 15 0 9 16.10 9.20 15 -2 9 73.29 8.10 2 -9 15 71.89 8.30 -2 9 15 72.89 12.80 15 -2 9 65.59 11.10 2 -9 15 61.89 12.20 -2 -9 15 55.19 7.70 15 2 9 49.40 7.50 15 2 9 57.59 11.30 -2 -9 15 42.40 12.10 2 9 15 49.00 12.70 -15 -2 9 52.19 8.00 15 -4 9 4.70 5.40 9 -15 4 2.80 5.50 4 -9 15 6.90 10.10 15 -4 9 6.00 8.60 4 -9 15 0.30 5.90 -4 9 15 0.40 10.90 -4 -9 15 4.50 10.40 15 4 9 -7.20 9.30 -15 -4 9 7.60 6.90 -4 -9 15 4.50 5.90 4 9 15 -7.50 11.00 9 -15 6 134.29 18.90 15 -6 9 146.09 17.30 15 -6 9 147.49 14.20 -6 9 15 164.18 19.90 6 -9 15 170.78 15.50 6 -9 15 156.78 21.60 9 -15 6 159.58 14.50 6 9 15 119.09 18.10 -15 -6 9 127.49 17.20 -6 -9 15 125.79 17.20 -6 -9 15 125.59 14.10 -8 9 15 112.09 14.20 15 -8 9 77.49 11.80 8 -9 15 78.79 14.50 9 -15 8 78.39 13.80 8 -9 15 90.59 12.00 9 -15 8 87.89 11.60 15 -8 9 88.19 11.20 -8 -9 15 81.89 14.50 -8 -9 15 80.69 9.70 -15 -8 9 99.29 13.90 8 9 15 78.69 15.30 15 -10 9 11.00 6.10 9 -15 10 6.70 10.70 15 -10 9 7.70 8.90 10 -9 15 10.10 11.90 9 -15 10 16.30 6.80 10 -9 15 10.80 7.20 -10 9 15 11.50 9.40 -10 -9 15 23.20 6.60 -10 -9 15 15.10 11.60 10 9 15 24.40 14.50 9 -15 12 36.70 12.90 15 -12 9 39.20 7.60 12 -9 15 49.70 14.10 9 -15 12 36.20 8.50 12 -9 15 46.70 8.80 15 -12 9 34.10 10.30 12 9 15 30.70 15.20 -12 -9 15 36.30 13.20 -9 -15 12 38.80 13.40 -12 -9 15 34.60 7.00 14 -9 15 57.09 9.30 9 -15 14 64.99 9.60 15 -14 9 61.49 8.80 9 -15 14 56.59 15.20 15 -14 9 61.29 11.70 14 -9 15 77.79 14.70 -14 -9 15 42.20 7.70 14 9 15 40.20 17.60 -9 -15 14 34.80 15.90 -14 -9 15 48.40 14.20 -9 -15 14 48.50 9.40 -1 10 15 381.76 34.80 1 -10 15 382.96 34.60 10 -15 1 375.56 29.90 15 -1 10 386.66 30.30 1 -10 15 355.96 30.30 15 -1 10 394.66 33.30 1 10 15 355.56 34.70 15 1 10 391.66 30.50 -1 -10 15 385.26 30.40 -15 -1 10 358.16 30.40 15 1 10 385.56 33.60 -1 -10 15 370.86 34.40 3 -10 15 105.49 14.80 -3 10 15 102.29 14.90 15 -3 10 102.99 11.50 10 -15 3 101.39 11.20 3 -10 15 98.09 11.70 15 -3 10 123.49 13.70 -15 -3 10 90.29 11.10 -3 -10 15 84.79 11.70 3 10 15 75.09 14.30 15 3 10 85.09 13.90 15 3 10 79.39 11.90 -3 -10 15 95.69 17.20 10 -15 5 23.30 6.00 15 -5 10 8.50 8.90 5 -10 15 -0.50 10.80 15 -5 10 12.10 5.90 10 -15 5 21.70 9.60 5 -10 15 8.40 6.60 -5 10 15 5.20 11.70 -15 -5 10 9.20 8.10 -5 -10 15 10.90 6.30 15 5 10 8.20 10.70 -5 -10 15 5.80 10.90 -15 -5 10 11.00 3.80 5 10 15 10.90 11.90 10 -15 7 5.40 9.80 10 -15 7 12.30 6.50 15 -7 10 4.50 9.10 7 -10 15 4.00 6.60 15 -7 10 9.70 6.00 -7 10 15 7.10 10.70 7 -10 15 0.30 11.30 -7 -10 15 12.50 11.40 7 10 15 2.50 13.60 -7 -10 15 13.30 6.10 -15 -7 10 17.90 9.70 -15 -7 10 9.20 4.60 -9 10 15 11.90 10.00 9 -10 15 19.00 7.20 9 -10 15 17.30 11.90 15 -9 10 11.10 9.20 15 -9 10 15.10 6.70 10 -15 9 14.60 6.90 10 -15 9 17.80 11.20 -15 -9 10 7.20 10.40 -9 -10 15 14.70 6.40 -9 -10 15 12.20 12.30 9 10 15 1.00 12.60 10 -15 11 40.00 8.20 10 -15 11 49.70 13.20 15 -11 10 51.49 7.90 11 -10 15 40.60 14.10 11 -10 15 41.50 8.40 15 -11 10 47.20 11.00 -11 -10 15 68.59 14.40 11 10 15 35.00 14.00 -11 -10 15 38.00 7.60 -15 -11 10 44.10 13.30 13 -10 15 338.37 26.70 10 -15 13 311.07 26.70 15 -13 10 343.47 26.20 13 -10 15 293.07 31.60 15 -13 10 274.47 29.00 10 -15 13 298.87 32.30 13 10 15 256.17 34.20 -10 -15 13 285.97 33.30 -13 -10 15 298.07 25.80 -13 -10 15 306.47 32.20 -10 -15 13 321.17 26.80 0 -11 15 4.70 14.90 0 -11 15 12.00 6.40 15 0 11 13.30 6.20 11 -15 0 14.10 5.30 0 11 15 31.50 12.40 15 0 11 26.10 10.90 15 -2 11 342.27 28.20 -2 11 15 346.87 33.30 2 -11 15 335.97 33.00 11 -15 2 319.57 27.70 11 -15 2 323.57 29.70 2 -11 15 345.17 28.40 15 -2 11 340.27 31.40 -2 -11 15 360.96 32.80 15 2 11 334.87 28.40 -2 -11 15 363.86 28.40 -15 -2 11 352.86 29.10 15 2 11 404.16 32.50 2 11 15 359.06 33.70 15 -4 11 203.78 21.30 15 -4 11 195.18 17.30 11 -15 4 178.48 16.80 4 -11 15 204.68 24.10 -4 11 15 187.08 23.70 4 -11 15 210.08 17.70 11 -15 4 185.08 20.20 -4 -11 15 181.08 23.80 -15 -4 11 156.18 19.10 4 11 15 169.68 24.30 15 4 11 215.18 23.40 -4 -11 15 177.48 17.50 -6 11 15 12.40 11.40 6 -11 15 6.00 6.70 11 -15 6 15.00 9.90 11 -15 6 7.30 6.20 15 -6 11 0.50 9.60 15 -6 11 5.40 6.20 6 -11 15 1.90 12.30 -6 -11 15 10.50 6.50 -15 -6 11 15.60 9.30 15 6 11 15.40 11.90 -6 -11 15 4.20 11.50 6 11 15 15.40 11.90 -15 -6 11 17.50 4.30 -8 11 15 1.40 10.80 8 -11 15 7.40 7.00 11 -15 8 13.40 6.60 11 -15 8 9.20 10.40 8 -11 15 11.70 12.00 15 -8 11 19.00 9.60 15 -8 11 9.40 6.50 -8 -11 15 -2.50 11.60 -8 -11 15 6.30 6.50 -15 -8 11 11.20 10.70 -15 -8 11 13.00 5.30 8 11 15 3.40 13.20 11 -15 10 51.19 13.00 15 -10 11 43.40 11.60 10 -11 15 62.19 9.00 10 -11 15 55.09 14.90 11 -15 10 41.00 8.40 15 -10 11 59.09 8.30 -10 -11 15 42.60 8.10 10 11 15 38.10 14.00 -15 -10 11 53.09 13.90 -10 -11 15 57.49 14.40 15 -12 11 388.36 34.70 12 -11 15 384.96 36.80 15 -12 11 396.56 31.70 11 -15 12 402.56 32.00 11 -15 12 383.46 36.40 12 -11 15 398.16 32.00 -12 -11 15 367.66 31.40 -12 -11 15 374.66 37.10 12 11 15 352.16 39.20 -15 -12 11 373.46 36.80 -11 -15 12 395.96 38.00 15 -14 11 187.88 22.80 15 -14 11 193.58 18.70 14 -11 15 196.08 25.10 11 -15 14 227.38 26.80 11 -15 14 193.78 19.30 14 -11 15 189.08 19.10 -11 -15 14 192.48 24.50 -15 -14 11 184.48 26.20 -14 -11 15 161.48 17.80 -11 -15 14 175.68 19.00 -14 -11 15 162.98 22.40 15 -1 12 580.34 45.20 12 -15 1 559.54 46.00 15 -1 12 615.04 48.40 1 -12 15 595.34 45.40 12 -15 1 566.74 44.60 -1 12 15 597.04 49.30 1 -12 15 558.04 48.90 -1 -12 15 597.24 45.40 -1 -12 15 540.35 48.90 12 -15 -1 569.54 44.40 15 1 12 573.24 48.50 -15 -1 12 551.14 45.70 15 1 12 606.34 45.40 1 12 15 564.84 49.30 15 -3 12 482.85 38.20 3 -12 15 464.75 38.30 3 -12 15 473.95 42.40 -3 12 15 496.15 42.60 12 -15 3 459.15 37.70 12 -15 3 456.35 39.50 15 -3 12 479.25 41.30 15 3 12 488.35 38.40 15 3 12 506.65 42.20 -15 -3 12 511.55 39.60 3 12 15 483.35 43.30 -3 -12 15 510.75 38.40 12 -15 -3 465.05 37.20 -3 -12 15 496.85 42.60 -5 12 15 194.28 23.90 5 -12 15 187.28 24.50 15 -5 12 170.58 21.60 5 -12 15 169.18 17.60 12 -15 5 165.68 20.00 12 -15 5 168.88 16.70 15 -5 12 147.09 17.10 15 5 12 212.38 24.10 12 -15 -5 198.58 15.30 -5 -12 15 202.78 24.20 -15 -5 12 184.28 15.20 5 12 15 191.08 24.80 -5 -12 15 193.68 17.60 -15 -5 12 222.48 20.50 7 -12 15 72.39 15.50 12 -15 7 74.29 12.20 15 -7 12 65.69 9.10 7 -12 15 60.49 9.30 12 -15 7 60.39 8.70 15 -7 12 40.30 11.90 -15 -7 12 72.59 8.70 -7 -12 15 64.89 8.90 15 7 12 75.39 16.30 -7 -12 15 71.69 14.80 -15 -7 12 75.09 12.60 7 12 15 54.99 15.20 9 -12 15 56.09 15.40 12 -15 9 36.80 8.10 12 -15 9 47.40 11.90 9 -12 15 42.10 8.80 15 -9 12 40.70 8.10 15 -9 12 29.60 11.50 -9 -12 15 54.79 8.70 9 12 15 54.59 16.60 -15 -9 12 52.29 13.00 -15 -9 12 53.79 7.10 -9 -12 15 48.30 14.60 11 -12 15 391.66 37.80 15 -11 12 398.36 32.20 11 -12 15 421.56 32.70 12 -15 11 406.06 36.40 15 -11 12 384.66 35.50 12 -15 11 419.46 32.40 -15 -11 12 367.66 31.70 -11 -12 15 370.96 32.00 -11 -12 15 391.86 38.10 -15 -11 12 378.96 36.90 13 -12 15 395.56 34.40 13 -12 15 366.16 39.00 12 -15 13 402.56 39.00 15 -13 12 376.66 37.40 12 -15 13 362.56 34.30 15 -13 12 384.06 34.10 -15 -13 12 472.55 40.20 -12 -15 13 477.85 41.20 -13 -12 15 430.26 33.90 -12 -15 13 488.95 34.50 -13 -12 15 465.35 40.30 0 13 15 8.20 12.60 -15 0 13 -0.30 6.70 0 -13 15 -6.20 6.70 13 -15 0 -4.40 6.10 13 -15 0 -1.50 4.60 15 0 13 8.30 6.70 15 0 13 8.20 11.60 0 -13 15 4.40 11.70 15 -2 13 621.84 46.70 2 -13 15 675.03 46.90 2 -13 15 609.44 50.69 13 -15 2 594.24 47.30 15 -2 13 623.94 49.80 -2 13 15 642.94 51.39 13 -15 2 595.44 45.90 15 2 13 595.94 50.29 -2 -13 15 571.34 46.70 -2 -13 15 549.65 50.69 2 13 15 569.34 51.29 -15 -2 13 571.04 47.70 15 2 13 572.54 46.80 13 -15 -2 550.04 45.60 15 -4 13 544.75 43.00 13 -15 4 493.95 41.00 4 -13 15 528.45 39.90 13 -15 4 537.75 39.30 15 -4 13 538.85 39.80 4 -13 15 533.25 44.30 4 13 15 481.35 45.40 15 4 13 475.35 44.20 15 4 13 452.35 39.90 -4 -13 15 506.55 44.50 -15 -4 13 443.66 41.40 -4 -13 15 473.05 39.90 6 -13 15 88.29 10.30 6 -13 15 84.79 15.30 13 -15 6 104.39 12.60 15 -6 13 103.59 12.50 15 -6 13 115.99 14.70 13 -15 6 100.49 11.30 15 6 13 65.29 15.60 6 13 15 60.59 17.40 -15 -6 13 66.09 12.90 -6 -13 15 66.89 10.20 -15 -6 13 60.29 9.00 -6 -13 15 56.29 15.10 8 -13 15 67.69 9.70 8 -13 15 72.09 15.40 13 -15 8 65.59 12.70 15 -8 13 62.19 9.40 13 -15 8 78.59 9.50 15 -8 13 88.29 13.60 -8 -13 15 71.59 9.70 -15 -8 13 73.19 9.90 -8 -13 15 74.59 15.70 -15 -8 13 89.89 14.70 15 8 13 76.89 16.30 10 -13 15 317.77 32.80 13 -15 10 307.57 30.70 15 -10 13 296.67 30.60 15 -10 13 328.47 26.90 10 -13 15 332.67 27.20 13 -15 10 342.17 26.90 -15 -10 13 304.27 26.00 -10 -13 15 304.07 33.40 -10 -13 15 306.87 26.80 -15 -10 13 279.87 31.80 15 -12 13 443.06 35.40 12 -13 15 354.16 40.20 12 -13 15 377.66 35.60 13 -15 12 368.76 39.20 13 -15 12 404.66 35.40 15 -12 13 360.96 38.60 -13 -15 12 493.65 41.70 -12 -13 15 499.65 35.30 -15 -12 13 451.85 41.00 -15 -12 13 482.75 34.90 -12 -13 15 503.35 41.80 13 -15 14 92.89 11.80 14 -13 15 90.39 17.10 15 -14 13 84.19 16.00 14 -13 15 77.39 11.70 13 -15 14 92.89 17.40 15 -14 13 93.49 11.70 -13 -15 14 104.49 19.20 -14 -13 15 97.99 11.50 -13 -15 14 97.29 12.00 -15 -14 13 79.09 18.20 -14 -13 15 94.39 18.70 -15 -14 13 88.29 11.20 15 -1 14 66.19 13.90 1 -14 15 42.40 8.50 15 -1 14 43.10 8.90 14 -15 1 51.89 6.40 1 -14 15 40.90 13.90 -15 1 14 47.70 8.70 -1 -14 15 39.30 8.50 -1 -14 15 26.20 13.80 -15 -1 14 39.70 9.60 15 1 14 34.90 13.20 15 1 14 35.40 8.50 14 -15 -1 54.79 7.20 15 -3 14 186.08 24.60 3 -14 15 209.18 26.00 15 -3 14 202.88 19.10 14 -15 3 209.28 18.40 14 -15 3 188.48 17.70 3 -14 15 199.48 19.30 15 3 14 213.88 26.00 -3 -14 15 211.98 26.30 -3 -14 15 208.08 19.50 15 3 14 211.78 19.60 -15 -3 14 212.08 21.50 14 -15 5 156.18 15.70 5 -14 15 153.38 17.20 14 -15 5 145.89 18.00 15 -5 14 137.29 16.80 15 -5 14 179.78 22.70 5 -14 15 126.59 19.70 -5 -14 15 214.68 25.00 15 5 14 207.18 25.10 -5 -14 15 205.78 17.40 -15 -5 14 200.88 21.00 14 -15 7 74.49 9.50 7 -14 15 79.39 10.70 14 -15 7 75.29 12.30 15 -7 14 90.99 14.90 15 -7 14 66.69 10.40 7 -14 15 42.00 16.20 -7 -14 15 98.89 10.50 -7 -14 15 74.39 15.60 15 7 14 92.39 16.90 -15 -7 14 86.49 9.80 -15 -7 14 103.89 14.60 14 -15 9 55.09 12.20 15 -9 14 52.19 9.10 15 -9 14 61.79 13.60 9 -14 15 77.79 17.00 14 -15 9 65.49 8.90 9 -14 15 56.99 9.30 -15 -9 14 31.20 13.70 -9 -14 15 48.30 9.40 -9 -14 15 44.10 17.10 -15 -9 14 43.70 7.60 11 -14 15 209.48 26.90 14 -15 11 196.48 19.10 14 -15 11 208.28 24.70 15 -11 14 206.88 19.50 15 -11 14 199.18 24.70 11 -14 15 205.58 19.90 -11 -14 15 179.68 19.30 -11 -14 15 147.39 23.30 -15 -11 14 191.98 18.30 -15 -11 14 188.28 26.40 15 -13 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28.30 10.80 13 -4 21 -2.60 9.20 4 -21 13 0.90 15.90 4 -21 13 -4.70 9.00 13 -4 21 -8.80 16.80 -13 4 21 2.80 12.20 -13 -4 21 4.10 14.70 13 4 21 5.70 18.60 13 4 21 -8.90 9.00 -4 -21 13 5.00 18.40 -4 -21 13 -3.60 9.70 4 -21 15 12.70 17.30 4 -21 15 13.10 10.50 15 -4 21 19.10 10.10 15 -4 21 20.40 17.30 -4 -21 15 12.50 10.60 -4 -21 15 -14.10 19.90 15 4 21 3.40 10.80 15 4 21 11.60 18.50 -15 -4 21 3.60 14.90 17 -4 21 13.80 10.20 4 -21 17 15.70 10.50 4 -21 17 8.20 18.20 17 -4 21 11.80 17.40 17 4 21 16.30 19.20 -4 -21 17 0.00 19.10 -4 -21 17 2.30 11.00 -17 -4 21 16.40 16.60 0 -5 21 42.00 7.80 0 -5 21 44.80 15.70 0 5 21 25.00 15.20 0 5 21 21.60 7.80 2 -5 21 163.28 16.00 2 -5 21 147.09 20.20 -2 5 21 147.89 15.40 -2 5 21 146.79 20.20 -2 -5 21 141.69 20.50 2 5 21 128.39 20.10 -2 -5 21 140.69 15.50 2 5 21 121.89 16.00 -4 5 21 363.76 28.30 -4 5 21 373.36 35.50 4 -5 21 352.76 36.40 4 -5 21 382.46 29.20 4 5 21 308.17 36.70 4 5 21 302.47 29.10 -4 -5 21 339.27 35.50 -4 -5 21 317.87 28.40 -6 5 21 27.00 14.40 6 -5 21 32.10 16.10 6 -5 21 25.50 9.40 6 5 21 59.59 17.60 -6 -5 21 57.39 8.50 -6 -5 21 59.99 15.90 6 5 21 57.39 9.50 -8 5 21 287.07 31.40 8 -5 21 278.77 25.40 5 -21 8 295.37 25.40 8 -5 21 276.67 33.80 -8 -5 21 268.07 24.10 -8 -5 21 303.77 32.80 8 5 21 291.17 25.70 8 5 21 236.98 34.30 -21 -8 5 285.97 26.30 -10 5 21 648.34 53.39 10 -5 21 603.64 55.59 5 -21 10 647.74 49.80 10 -5 21 638.34 49.80 5 -21 10 594.04 54.39 -10 -5 21 619.14 48.70 10 5 21 598.04 56.59 -10 -5 21 685.83 55.09 10 5 21 579.24 49.70 5 -21 12 143.59 17.60 12 -5 21 155.78 17.80 12 -5 21 128.59 23.00 -12 5 21 165.48 19.90 5 -21 12 121.19 21.70 -12 -5 21 136.19 14.50 12 5 21 111.79 23.30 -12 -5 21 153.68 21.10 -5 -21 12 93.59 23.20 12 5 21 128.99 18.00 -14 5 21 13.80 11.50 14 -5 21 21.70 10.00 14 -5 21 25.00 17.70 5 -21 14 31.10 10.30 5 -21 14 32.30 17.60 -5 -21 14 20.60 20.60 -14 -5 21 -0.10 16.10 14 5 21 16.90 19.00 -5 -21 14 15.90 10.90 16 -5 21 20.80 17.40 16 -5 21 33.10 11.10 5 -21 16 25.90 10.40 5 -21 16 27.90 18.10 -5 -21 16 25.90 20.50 -16 -5 21 29.10 15.60 -5 -21 16 18.30 11.30 16 5 21 26.30 19.70 1 -6 21 6.50 7.80 1 -6 21 -5.10 14.50 -1 6 21 10.90 7.30 -1 6 21 10.00 15.30 -1 -6 21 -11.40 14.50 -1 -6 21 7.40 7.20 1 6 21 -4.20 15.10 1 6 21 4.20 7.10 3 -6 21 0.90 8.10 -3 6 21 1.40 7.10 -3 6 21 4.40 13.20 3 -6 21 -2.30 14.90 3 6 21 14.40 8.10 -3 -6 21 14.60 7.00 3 6 21 2.60 14.80 -3 -6 21 10.00 14.60 5 -6 21 34.10 9.30 -5 6 21 31.80 14.80 5 -6 21 17.70 15.70 5 6 21 46.70 8.70 5 6 21 60.49 16.90 -5 -6 21 50.99 8.30 -5 -6 21 79.59 17.70 7 -6 21 223.48 31.20 -7 6 21 221.48 28.80 6 -21 7 261.07 22.60 7 -6 21 272.07 22.90 -7 -6 21 234.78 21.30 7 6 21 231.18 32.20 7 6 21 214.98 22.40 -7 -6 21 205.18 30.20 -9 6 21 233.68 30.30 6 -21 9 237.58 31.10 9 -6 21 265.77 24.80 6 -21 9 271.87 24.80 9 -6 21 287.47 33.80 9 6 21 245.18 34.70 9 6 21 270.07 24.90 -9 -6 21 272.47 23.30 -9 -6 21 264.57 32.60 -21 -9 6 283.37 26.30 6 -21 11 75.49 17.20 11 -6 21 78.09 19.60 6 -21 11 90.99 11.70 11 -6 21 90.09 12.10 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23.50 17.10 1 -8 21 40.20 8.60 -1 -8 21 34.70 8.40 1 8 21 11.10 15.60 -1 -8 21 9.00 16.90 3 -8 21 96.39 12.20 -3 8 21 115.29 19.40 3 -8 21 108.49 20.40 -3 -8 21 141.29 21.60 3 8 21 93.89 20.20 -3 -8 21 99.69 14.20 5 -8 21 280.77 25.60 8 -21 5 303.97 25.50 5 -8 21 296.17 34.00 -5 8 21 273.97 32.90 21 -5 8 287.47 24.30 -5 -8 21 276.97 24.90 5 8 21 259.77 34.60 -5 -8 21 303.17 34.70 7 -8 21 152.08 24.10 7 -8 21 168.48 19.50 21 -7 8 192.58 17.40 -7 8 21 182.98 23.10 8 -21 7 175.88 22.70 8 -21 7 182.88 19.50 7 8 21 155.68 23.40 -7 -8 21 210.98 18.50 -7 -8 21 207.48 24.60 -9 8 21 47.50 15.10 8 -21 9 49.30 15.90 9 -8 21 35.10 17.90 8 -21 9 65.29 10.30 9 -8 21 60.89 10.70 9 8 21 33.40 19.00 -21 -9 8 48.60 11.40 -9 -8 21 51.59 9.30 -9 -8 21 51.99 17.90 -11 8 21 -3.20 13.10 11 -8 21 15.90 16.70 11 -8 21 11.90 8.90 8 -21 11 1.00 15.00 8 -21 11 8.20 9.40 -11 -8 21 10.40 7.50 -21 -11 8 5.20 12.20 -11 -8 21 8.50 16.50 11 8 21 -2.10 18.20 8 -21 13 52.99 17.30 -13 8 21 34.40 13.00 13 -8 21 35.70 17.90 13 -8 21 36.70 10.30 8 -21 13 41.70 9.90 -13 -8 21 38.40 18.30 -8 -21 13 26.00 19.20 -8 -21 13 27.80 11.50 -13 -8 21 32.70 8.10 -21 -13 8 29.70 14.60 13 8 21 21.90 19.50 8 -21 15 37.20 10.70 8 -21 15 31.80 18.20 15 -8 21 36.20 17.80 15 -8 21 33.10 10.90 -8 -21 15 25.70 11.70 -21 -15 8 26.90 15.20 -8 -21 15 17.90 20.70 -15 -8 21 32.80 18.30 15 8 21 18.00 19.50 0 -9 21 78.89 11.10 0 -9 21 101.39 21.10 0 9 21 78.89 18.00 2 -9 21 166.08 23.10 2 -9 21 227.38 20.40 -2 9 21 225.88 26.30 -2 -9 21 195.98 19.50 -2 -9 21 169.08 23.30 2 9 21 206.58 26.80 21 -4 9 625.34 48.20 9 -21 4 648.44 48.70 4 -9 21 585.34 55.39 4 -9 21 636.44 48.90 -4 9 21 600.54 54.29 -4 -9 21 624.54 55.09 -4 -9 21 589.14 48.40 4 9 21 567.04 55.29 21 -6 9 259.57 23.20 9 -21 6 272.87 24.30 6 -9 21 230.98 33.60 6 -9 21 259.27 24.30 9 -21 6 253.57 29.70 -6 9 21 259.67 32.00 -6 -9 21 283.77 33.30 6 9 21 247.78 34.40 -6 -9 21 277.77 23.60 8 -9 21 57.79 10.60 9 -21 8 56.99 15.40 21 -8 9 70.49 8.90 8 -9 21 70.29 18.70 9 -21 8 68.59 10.40 -8 9 21 51.19 15.90 -8 -9 21 44.40 9.50 -8 -9 21 46.10 18.30 8 9 21 45.60 19.50 -10 9 21 464.25 41.00 10 -9 21 448.96 43.60 9 -21 10 413.16 41.30 9 -21 10 467.65 35.90 21 -10 9 417.56 33.90 10 -9 21 452.85 36.20 -10 -9 21 404.36 34.90 10 9 21 337.37 44.60 -21 -10 9 402.06 37.70 -10 -9 21 439.46 43.60 12 -9 21 141.39 17.90 -12 9 21 115.49 18.00 12 -9 21 115.29 21.80 9 -21 12 134.59 17.10 9 -21 12 115.39 19.90 12 9 21 61.59 21.40 -12 -9 21 114.29 21.80 -9 -21 12 89.79 20.30 -21 -12 9 96.59 17.90 -12 -9 21 111.99 14.50 9 -21 14 29.00 17.70 14 -9 21 35.00 10.80 14 -9 21 28.90 18.00 9 -21 14 30.60 10.40 -14 -9 21 49.60 8.50 -9 -21 14 25.70 18.70 -9 -21 14 37.30 11.40 -21 -14 9 33.60 15.70 -14 -9 21 58.59 18.90 14 9 21 39.60 20.20 1 -10 21 3.50 8.40 10 -21 1 -0.50 7.60 1 -10 21 7.50 14.60 -1 10 21 6.30 16.20 -1 -10 21 2.00 8.00 1 10 21 5.60 16.10 -1 -10 21 -9.50 14.00 3 -10 21 62.29 17.90 3 -10 21 53.69 10.70 21 -3 10 66.09 10.20 10 -21 3 75.99 10.30 -3 10 21 99.49 18.40 -3 -10 21 63.19 16.30 3 10 21 56.29 18.00 -3 -10 21 65.59 9.90 -5 10 21 680.93 56.19 21 -5 10 649.04 49.70 5 -10 21 571.24 56.39 10 -21 5 654.03 50.19 5 -10 21 660.93 50.29 10 -21 5 629.24 53.69 -5 -10 21 641.04 49.99 5 10 21 539.65 56.59 -5 -10 21 610.74 56.49 7 -10 21 791.22 71.89 10 -21 7 871.41 69.69 10 -21 7 849.41 66.19 -7 10 21 898.11 70.99 7 -10 21 854.11 66.39 21 -7 10 865.21 65.69 -7 -10 21 820.22 71.79 7 10 21 772.82 72.49 -7 -10 21 889.51 66.09 -9 10 21 459.85 41.90 21 -9 10 443.26 35.20 9 -10 21 436.76 44.10 9 -10 21 458.95 36.60 10 -21 9 438.96 41.20 10 -21 9 440.26 36.40 -9 -10 21 430.56 35.70 -9 -10 21 398.56 44.10 9 10 21 347.67 45.20 11 -10 21 14.80 17.80 10 -21 11 11.10 9.10 10 -21 11 15.30 15.30 11 -10 21 24.50 9.90 -11 -10 21 11.00 17.80 11 10 21 -0.50 18.70 -21 -11 10 -4.90 12.00 -11 -10 21 12.60 8.00 10 -21 13 25.20 10.50 13 -10 21 19.40 11.00 13 -10 21 21.80 18.20 10 -21 13 26.30 16.80 13 10 21 25.50 21.20 -10 -21 13 29.30 11.40 -13 -10 21 45.10 19.00 -10 -21 13 19.90 17.10 -21 -13 10 26.50 14.60 -13 -10 21 28.10 8.70 -10 -21 15 12.70 18.60 -21 -15 10 21.80 15.50 11 -21 0 107.29 14.40 0 -11 21 115.69 15.30 0 11 21 130.39 21.30 0 -11 21 95.69 20.70 -2 11 21 42.30 17.90 2 -11 21 23.20 17.30 11 -21 2 38.30 12.80 11 -21 2 31.50 8.50 2 -11 21 36.10 9.90 21 -2 11 36.60 8.70 -2 -11 21 38.50 9.40 11 -21 -2 48.60 8.00 2 11 21 31.60 18.90 -2 -11 21 35.10 15.10 4 -11 21 50.79 10.20 -4 11 21 55.29 17.60 11 -21 4 48.00 14.60 21 -4 11 41.80 9.10 4 -11 21 35.20 17.80 11 -21 4 44.70 9.20 4 11 21 35.60 18.90 -4 -11 21 43.10 20.50 -4 -11 21 38.20 9.40 -6 11 21 92.09 18.80 11 -21 6 95.79 11.70 11 -21 6 80.79 16.10 6 -11 21 91.59 12.30 21 -6 11 102.99 14.00 6 -11 21 68.19 20.40 6 11 21 70.89 20.10 -6 -11 21 88.59 11.30 -6 -11 21 68.69 17.90 -8 11 21 18.30 16.40 8 -11 21 4.20 9.30 21 -8 11 12.40 8.00 11 -21 8 12.80 9.10 8 -11 21 18.90 18.00 11 -21 8 11.20 14.20 -8 -11 21 7.30 20.00 8 11 21 -12.70 17.20 -8 -11 21 3.20 8.10 21 -10 11 13.60 8.30 10 -11 21 21.70 10.30 11 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5 -7 22 99.19 22.10 -5 -7 22 180.38 17.50 -5 -7 22 207.08 23.90 5 7 22 200.38 18.70 5 7 22 163.98 24.10 7 -22 7 299.07 29.20 7 -7 22 295.57 29.50 7 -22 7 296.37 34.60 7 -7 22 294.47 37.30 -7 7 22 336.27 35.80 -7 -7 22 393.36 38.20 7 7 22 373.56 39.30 -7 -7 22 389.96 28.40 -9 7 22 115.79 19.20 9 -7 22 115.29 21.60 7 -22 9 111.19 14.10 9 -7 22 97.89 13.80 7 -22 9 105.89 19.60 -9 -7 22 147.89 21.60 -9 -7 22 145.89 15.10 9 7 22 110.49 20.60 11 -7 22 5.50 9.90 -11 7 22 15.10 14.10 7 -22 11 16.10 9.60 7 -22 11 22.70 16.80 11 -7 22 33.00 18.80 -11 -7 22 40.80 18.60 11 7 22 21.50 18.70 -22 -11 7 40.90 12.30 -11 -7 22 27.70 8.20 13 -7 22 13.80 17.50 7 -22 13 10.90 16.70 7 -22 13 2.10 9.80 -13 7 22 7.00 12.10 13 -7 22 22.40 10.80 -7 -22 13 14.20 17.30 -22 -13 7 19.50 13.30 13 7 22 23.80 19.90 -13 -7 22 13.20 7.00 -7 -22 13 12.80 10.90 -13 -7 22 26.40 17.50 15 -7 22 5.70 10.50 7 -22 15 5.00 17.00 7 -22 15 17.30 10.60 15 -7 22 14.50 18.30 -22 -15 7 -4.50 13.90 -7 -22 15 8.20 11.80 15 7 22 -16.60 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4.60 16.10 -12 -8 22 19.60 18.20 -8 -22 12 16.90 21.30 12 8 22 1.00 19.80 -22 -12 8 20.70 13.00 -12 -8 22 30.40 8.30 14 -8 22 15.10 18.70 14 -8 22 14.90 10.60 8 -22 14 22.70 10.90 8 -22 14 5.30 16.40 -8 -22 14 18.60 11.40 -14 -8 22 26.60 19.00 14 8 22 20.50 19.90 -8 -22 14 22.00 22.00 -22 -14 8 29.50 14.70 1 -9 22 479.35 38.30 1 -9 22 415.36 45.50 -1 9 22 475.05 45.80 1 9 22 495.75 46.20 -1 -9 22 415.26 45.50 -1 -9 22 491.85 38.30 -3 9 22 445.86 43.80 9 -22 3 468.35 36.50 3 -9 22 451.05 36.50 3 -9 22 385.46 43.70 3 9 22 429.16 44.70 -3 -9 22 393.26 43.90 -3 -9 22 456.85 36.30 22 -5 9 179.48 17.40 9 -22 5 176.48 25.40 5 -9 22 148.79 24.60 9 -22 5 167.48 19.20 -5 9 22 178.98 23.50 5 -9 22 168.18 19.20 -5 -9 22 199.48 25.00 -5 -9 22 204.98 18.80 5 9 22 149.39 25.50 7 -9 22 122.79 22.20 9 -22 7 111.29 13.90 9 -22 7 102.19 18.90 7 -9 22 126.89 17.20 -7 9 22 133.99 20.80 -7 -9 22 166.28 23.80 -7 -9 22 143.39 15.90 7 9 22 100.89 22.60 -9 9 22 267.27 32.20 9 -9 22 251.17 25.20 9 -22 9 205.08 31.20 9 -9 22 242.88 34.20 9 -22 9 275.77 24.90 -9 -9 22 277.27 23.80 -9 -9 22 268.67 34.80 9 9 22 254.87 36.80 -11 9 22 251.37 31.00 11 -9 22 282.57 26.20 9 -22 11 262.87 32.80 9 -22 11 291.07 25.60 11 -9 22 241.48 35.70 11 9 22 201.58 31.30 -11 -9 22 285.77 24.30 -11 -9 22 252.67 36.00 13 -9 22 116.79 22.60 9 -22 13 142.39 18.40 13 -9 22 135.89 18.10 9 -22 13 137.59 21.00 -13 -9 22 127.89 22.90 -9 -22 13 88.39 23.60 -9 -22 13 93.59 15.00 -22 -13 9 98.79 17.60 -13 -9 22 105.39 14.90 13 9 22 85.69 24.60 0 10 22 78.09 18.30 10 -22 0 69.49 10.40 0 -10 22 70.39 19.90 0 -10 22 69.99 10.90 10 -22 2 98.79 12.30 2 -10 22 119.59 15.70 2 -10 22 92.09 22.10 -2 10 22 106.39 20.50 -2 -10 22 119.09 15.50 -2 -10 22 87.49 20.10 2 10 22 111.49 21.70 10 -22 4 39.40 15.00 4 -10 22 16.60 18.50 -4 10 22 29.20 17.00 10 -22 4 17.30 8.80 4 -10 22 36.40 9.80 4 10 22 25.90 18.60 -4 -10 22 58.19 20.40 -4 -10 22 41.50 8.90 -6 10 22 127.39 22.00 10 -22 6 120.59 18.60 10 -22 6 122.29 16.20 22 -6 10 124.89 14.70 6 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5 -11 22 178.58 18.40 22 -5 11 125.09 16.20 11 -22 5 137.29 17.10 11 -22 5 129.39 19.20 -5 11 22 133.89 22.10 -5 -11 22 137.89 17.10 -5 -11 22 167.18 24.40 5 11 22 115.99 24.00 11 -22 7 28.60 14.80 22 -7 11 15.80 8.40 7 -11 22 28.80 10.50 -7 11 22 17.70 15.70 7 -11 22 21.20 18.90 11 -22 7 19.60 9.60 -7 -11 22 13.20 20.00 7 11 22 -3.20 18.90 -7 -11 22 37.10 9.50 11 -22 9 299.97 26.70 -9 11 22 289.27 34.60 9 -11 22 297.17 27.10 9 -11 22 258.37 36.00 11 -22 9 296.67 33.10 22 -9 11 289.47 25.20 -9 -11 22 249.18 32.50 -9 -11 22 295.87 25.80 9 11 22 265.97 38.70 11 -11 22 253.57 35.80 11 -22 11 249.97 32.40 11 -11 22 265.47 26.60 11 -22 11 266.27 26.00 11 11 22 233.78 34.20 -11 -11 22 291.77 25.20 -11 -11 22 324.97 37.00 12 -22 0 -1.30 2.90 12 -22 0 5.70 7.90 0 -12 22 5.40 17.10 0 12 22 1.50 17.40 0 -12 22 2.50 9.20 -2 12 22 48.60 19.10 2 -12 22 48.30 22.60 12 -22 2 71.59 10.20 2 -12 22 49.60 11.10 -2 -12 22 87.79 11.90 2 12 22 65.59 19.90 -2 -12 22 55.29 20.50 22 -4 12 73.19 11.50 -4 12 22 78.39 19.60 4 -12 22 76.69 12.20 4 -12 22 59.19 17.60 12 -22 4 56.89 15.40 12 -22 4 84.89 11.40 -4 -12 22 97.19 11.70 -4 -12 22 84.29 20.40 4 12 22 75.29 20.40 22 -6 12 8.50 8.20 12 -22 6 -1.30 13.20 12 -22 6 4.50 8.80 -6 12 22 16.70 16.20 6 -12 22 -5.30 9.70 6 -12 22 0.90 18.40 12 -22 -6 2.50 1.80 -6 -12 22 28.90 9.10 -6 -12 22 20.80 19.40 6 12 22 1.00 18.60 22 -8 12 10.60 8.30 12 -22 8 5.40 9.10 12 -22 8 2.90 14.40 8 -12 22 29.60 19.10 8 -12 22 19.30 9.90 -8 -12 22 19.20 8.90 -8 -12 22 20.90 19.90 8 12 22 25.00 20.70 22 -10 12 11.10 8.20 10 -12 22 10.20 10.80 12 -22 10 19.50 10.40 12 -22 10 13.20 15.00 10 -12 22 6.90 18.70 10 12 22 11.40 22.00 -10 -12 22 25.00 9.60 -10 -12 22 14.50 18.20 1 -13 22 54.59 21.40 13 -22 1 62.49 9.70 1 -13 22 58.99 10.90 -1 13 22 84.79 21.70 -1 -13 22 73.79 11.30 1 13 22 82.59 21.40 -1 -13 22 43.80 21.10 13 -22 3 3.40 8.20 3 -13 22 9.40 21.70 13 -22 3 0.80 3.10 22 -3 13 -1.20 8.60 -3 13 22 7.10 18.00 3 -13 22 8.20 9.90 -3 -13 22 8.20 9.50 13 -22 -3 -1.40 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8 -14 22 18.50 19.40 14 -22 8 -0.20 4.00 8 -14 22 7.40 10.30 22 -8 14 25.30 9.30 14 -22 8 11.10 9.50 -8 -14 22 34.30 9.80 -8 -14 22 15.90 18.10 1 -15 22 88.59 22.40 1 -15 22 126.19 15.20 -1 -15 22 105.69 23.40 -1 -15 22 140.29 18.00 22 -3 15 -4.00 9.20 3 -15 22 -4.70 17.00 3 -15 22 2.40 9.90 15 -22 3 -0.70 1.60 -3 -15 22 -1.90 10.60 -3 -15 22 -4.00 18.20 5 -15 22 23.90 16.80 5 -15 22 58.69 12.10 22 -5 15 55.79 11.00 15 -22 5 62.69 9.70 -5 -15 22 32.50 12.00 -5 -15 22 29.90 18.70 22 -7 15 -0.60 9.60 7 -15 22 6.70 18.10 15 -22 7 5.10 9.20 7 -15 22 13.30 10.60 15 -22 7 2.30 6.40 -7 -15 22 7.60 10.50 -7 -15 22 -1.20 16.90 0 -16 22 4.10 20.20 0 -16 22 -0.60 10.40 2 -16 22 46.00 11.40 2 -16 22 43.80 21.80 -2 -16 22 5.10 20.90 -2 -16 22 19.00 10.10 22 -4 16 3.40 3.90 22 -4 16 7.60 9.60 16 -22 4 -1.10 1.60 4 -16 22 3.50 16.90 4 -16 22 -3.50 10.20 -4 -16 22 4.40 10.70 -4 -16 22 13.40 19.80 -1 0 23 33.20 8.20 -1 0 23 24.90 15.90 1 0 23 44.80 8.70 1 0 23 38.30 16.70 -3 0 23 80.99 18.00 3 0 23 91.19 11.40 3 0 23 95.79 19.70 -3 0 23 87.39 10.60 -5 0 23 4.10 7.20 -5 0 23 5.20 15.20 5 0 23 3.80 8.30 5 0 23 14.50 14.60 -7 0 23 150.98 16.00 7 0 23 164.88 17.70 7 0 23 116.99 23.20 -7 0 23 152.58 21.30 9 0 23 14.90 17.20 -9 0 23 -5.00 14.50 9 0 23 10.10 8.80 -9 0 23 9.80 6.90 0 -23 11 169.98 26.00 -11 0 23 203.88 27.70 11 0 23 171.68 20.80 11 0 23 146.59 25.40 0 -23 11 199.98 21.00 13 0 23 94.19 13.80 -13 0 23 80.09 18.60 0 -23 13 87.09 21.90 13 0 23 112.39 23.90 0 -23 13 109.39 14.30 0 -23 15 11.70 10.80 15 0 23 4.80 19.90 0 -23 15 5.50 19.10 -15 0 23 -7.70 12.60 15 0 23 5.70 10.90 0 1 23 34.30 8.80 0 1 23 24.70 16.20 0 -1 23 47.20 8.40 0 -1 23 37.90 17.10 -2 1 23 8.90 15.50 -2 1 23 14.90 8.00 2 -1 23 10.50 7.70 2 -1 23 3.70 15.00 2 1 23 5.50 15.40 -2 -1 23 10.80 7.60 -2 -1 23 -3.40 15.00 2 1 23 7.80 7.70 4 -1 23 4.60 8.40 4 -1 23 8.90 16.50 -4 1 23 0.00 14.70 -4 1 23 7.20 7.40 -4 -1 23 19.80 7.30 4 1 23 7.60 15.30 4 1 23 5.20 8.00 -4 -1 23 6.90 14.20 6 -1 23 157.48 18.10 6 -1 23 139.09 23.90 -6 1 23 146.59 21.40 -6 1 23 156.98 16.50 -6 -1 23 161.88 22.00 6 1 23 175.28 18.40 -6 -1 23 169.18 16.50 6 1 23 139.79 22.80 8 -1 23 184.88 28.80 -8 1 23 256.97 22.50 8 -1 23 252.17 24.40 -8 1 23 210.28 31.00 8 1 23 250.37 35.50 -8 -1 23 291.17 31.70 -8 -1 23 278.37 22.60 8 1 23 275.77 24.30 -10 1 23 -14.10 14.10 1 -23 10 7.30 17.40 10 -1 23 3.90 18.20 10 -1 23 1.90 9.30 1 -23 10 -5.10 9.50 -10 -1 23 10.30 15.00 -10 -1 23 -2.40 6.60 10 1 23 -15.90 18.10 10 1 23 -8.00 9.50 12 -1 23 18.30 19.60 1 -23 12 -1.50 10.40 -12 1 23 22.30 15.70 1 -23 12 15.00 18.80 12 -1 23 23.70 9.90 -12 -1 23 15.50 15.70 -1 -23 12 13.50 10.60 12 1 23 11.40 10.30 12 1 23 2.20 17.90 -1 -23 12 10.20 18.20 14 -1 23 27.00 20.50 1 -23 14 18.00 18.40 1 -23 14 16.80 10.80 14 -1 23 16.80 10.80 -14 1 23 24.00 14.20 14 1 23 34.50 11.40 -1 -23 14 27.40 19.20 -14 -1 23 27.80 16.00 -1 -23 14 20.60 11.60 14 1 23 20.20 20.30 -1 2 23 15.70 16.40 1 -2 23 18.10 15.10 1 -2 23 13.70 7.70 -1 2 23 6.60 7.40 -1 -2 23 18.00 14.80 1 2 23 15.30 8.20 1 2 23 -2.10 15.00 -1 -2 23 8.20 7.90 3 -2 23 9.60 8.20 -3 2 23 12.40 14.60 3 -2 23 11.30 15.10 -3 2 23 21.00 8.10 -3 -2 23 13.90 7.40 3 2 23 21.10 7.90 3 2 23 24.40 16.20 -3 -2 23 26.10 14.90 -5 2 23 50.59 15.90 -5 2 23 39.40 8.40 5 -2 23 42.90 9.60 5 -2 23 37.60 16.50 -5 -2 23 21.70 8.00 5 2 23 21.70 9.70 5 2 23 33.30 19.40 -5 -2 23 20.60 14.80 7 -2 23 159.18 24.30 -7 2 23 181.68 17.70 7 -2 23 191.58 19.80 -7 2 23 197.58 23.10 -7 -2 23 191.08 24.40 -7 -2 23 183.68 18.00 7 2 23 182.98 19.70 7 2 23 153.18 25.10 -9 2 23 30.30 7.00 2 -23 9 16.80 9.40 9 -2 23 46.30 19.90 -9 2 23 29.10 16.40 9 -2 23 13.10 9.30 -9 -2 23 0.50 7.00 9 2 23 -5.20 16.90 9 2 23 7.10 9.60 -9 -2 23 3.20 15.00 -11 2 23 158.58 21.90 11 -2 23 148.09 18.00 11 -2 23 104.29 22.80 2 -23 11 141.79 18.80 2 -23 11 113.49 21.70 11 2 23 136.49 23.40 11 2 23 150.28 19.00 -2 -23 11 83.99 21.20 -11 -2 23 140.09 21.10 -11 -2 23 137.39 18.20 -2 -23 11 155.88 19.50 13 -2 23 121.59 23.60 2 -23 13 102.29 14.50 -13 2 23 131.59 19.10 2 -23 13 80.49 19.60 13 -2 23 112.69 14.60 13 2 23 109.79 14.80 -13 -2 23 149.19 20.60 13 2 23 95.29 23.40 -2 -23 13 115.89 24.80 -2 -23 13 110.09 14.90 2 -23 15 15.20 19.00 15 -2 23 -3.80 18.90 15 -2 23 -1.40 10.90 2 -23 15 -4.30 10.40 15 2 23 2.00 10.40 -2 -23 15 13.80 11.50 -15 -2 23 -0.40 13.60 15 2 23 20.50 20.00 -2 -23 15 -16.20 17.90 0 3 23 107.39 19.70 0 -3 23 86.69 11.10 0 -3 23 74.99 18.80 0 3 23 88.19 11.00 2 -3 23 11.10 8.20 2 -3 23 19.40 15.60 -2 3 23 30.10 16.30 -2 3 23 14.10 8.00 -2 -3 23 17.10 7.90 2 3 23 14.20 16.10 -2 -3 23 9.90 15.90 2 3 23 23.80 8.40 -4 3 23 34.60 16.30 4 -3 23 35.20 9.10 4 -3 23 43.10 19.40 -4 3 23 42.90 8.70 4 3 23 40.10 17.30 -4 -3 23 28.20 15.70 -4 -3 23 34.30 8.10 4 3 23 17.40 9.10 6 -3 23 214.18 22.60 6 -3 23 176.18 26.40 -6 3 23 219.28 30.60 -6 3 23 226.48 21.10 -6 -3 23 270.97 31.30 6 3 23 240.38 33.80 -6 -3 23 246.28 21.30 6 3 23 264.77 22.80 8 -3 23 372.16 33.30 8 -3 23 338.57 41.70 -8 3 23 316.67 39.00 8 3 23 378.86 42.60 -8 -3 23 412.66 32.10 8 3 23 423.06 33.70 -8 -3 23 455.05 40.70 -10 3 23 17.80 14.70 10 -3 23 23.40 10.40 3 -23 10 27.70 10.50 10 -3 23 16.20 18.30 3 -23 10 22.10 18.50 10 3 23 34.20 10.40 -10 -3 23 50.99 8.00 -10 -3 23 33.90 16.90 10 3 23 57.09 19.90 3 -23 12 14.70 18.80 -12 3 23 32.90 15.40 3 -23 12 17.80 10.20 12 -3 23 20.50 18.80 12 -3 23 29.90 10.10 -12 -3 23 19.10 16.60 -3 -23 12 34.40 18.70 12 3 23 39.90 20.90 12 3 23 23.10 11.10 -3 -23 12 38.10 11.60 3 -23 14 62.19 20.60 3 -23 14 76.09 12.70 -14 3 23 78.19 16.20 14 -3 23 53.09 20.50 14 -3 23 68.79 11.90 -3 -23 14 81.99 24.10 14 3 23 77.59 22.30 -3 -23 14 87.29 13.70 14 3 23 61.49 12.70 -14 -3 23 83.19 18.50 1 -4 23 4.30 7.80 1 -4 23 14.60 16.20 -1 4 23 9.70 7.80 -1 4 23 14.80 16.50 1 4 23 12.30 17.00 -1 -4 23 10.30 8.20 1 4 23 7.00 8.10 -1 -4 23 4.50 15.20 3 -4 23 49.10 9.20 -3 4 23 43.60 8.60 -3 4 23 46.10 16.90 3 -4 23 30.10 18.30 -3 -4 23 46.70 17.10 3 4 23 31.90 9.50 -3 -4 23 31.50 8.70 3 4 23 26.70 18.10 -5 4 23 110.59 11.10 5 -4 23 103.29 11.80 -5 4 23 74.99 18.40 5 -4 23 71.09 20.50 5 4 23 78.49 11.80 -5 -4 23 63.59 10.60 -5 -4 23 90.69 19.20 5 4 23 61.69 20.70 7 -4 23 267.87 36.00 7 -4 23 311.67 26.10 -7 4 23 308.37 33.30 -7 -4 23 280.67 24.60 7 4 23 264.67 26.30 -7 -4 23 268.47 34.30 7 4 23 262.57 36.50 -9 4 23 206.48 27.30 9 -4 23 213.48 19.60 9 -4 23 153.38 24.70 4 -23 9 224.88 29.10 -9 -4 23 154.98 23.00 9 4 23 129.49 24.70 -9 -4 23 151.48 17.10 9 4 23 149.19 19.50 11 -4 23 33.20 20.40 4 -23 11 47.20 11.00 -11 4 23 48.10 16.50 4 -23 11 29.10 18.60 11 -4 23 41.00 10.60 11 4 23 8.20 19.60 11 4 23 15.70 9.70 -11 -4 23 31.90 7.70 -11 -4 23 28.50 17.10 13 -4 23 32.30 10.70 -13 4 23 20.70 14.70 4 -23 13 15.10 10.70 4 -23 13 32.70 18.90 13 -4 23 24.50 20.20 13 4 23 12.00 10.80 -4 -23 13 25.60 11.60 13 4 23 29.80 20.60 -4 -23 13 24.90 21.00 -13 -4 23 27.00 16.80 0 5 23 27.20 17.80 0 5 23 17.00 8.50 0 -5 23 13.20 8.50 0 -5 23 17.60 16.10 2 -5 23 44.70 9.20 -2 5 23 41.80 8.70 -2 5 23 35.20 17.00 2 -5 23 20.90 16.70 -2 -5 23 21.60 16.30 2 5 23 15.20 15.30 2 5 23 21.20 9.50 -2 -5 23 23.80 8.70 4 -5 23 82.09 18.80 -4 5 23 97.19 10.50 -4 5 23 82.09 18.10 4 -5 23 86.19 11.10 -4 -5 23 73.79 18.40 4 5 23 46.50 19.20 -4 -5 23 72.29 10.80 4 5 23 77.79 11.90 -6 5 23 102.69 20.00 6 -5 23 82.29 21.20 6 -5 23 96.79 13.30 6 5 23 109.99 22.40 -6 -5 23 137.79 15.10 6 5 23 137.59 16.50 -6 -5 23 153.98 21.40 8 -5 23 284.57 38.00 5 -23 8 276.17 35.00 5 -23 8 323.57 28.70 8 -5 23 291.97 28.50 -8 5 23 270.57 34.80 -8 -5 23 356.86 27.20 8 5 23 325.27 28.30 -8 -5 23 370.16 36.80 8 5 23 319.27 39.00 10 -5 23 187.08 21.40 -10 5 23 203.38 29.10 5 -23 10 195.78 21.60 10 -5 23 163.88 26.80 5 -23 10 141.59 24.60 -10 -5 23 226.68 19.20 -10 -5 23 243.68 26.80 10 5 23 218.28 21.50 10 5 23 174.08 26.50 5 -23 12 19.80 10.30 5 -23 12 9.80 17.50 -12 5 23 25.30 15.30 12 -5 23 14.10 10.30 12 -5 23 4.20 17.70 -12 -5 23 13.40 16.70 -5 -23 12 21.30 11.40 12 5 23 17.50 10.80 -5 -23 12 27.40 20.60 12 5 23 15.60 19.40 -12 -5 23 16.70 7.60 14 -5 23 3.20 20.00 5 -23 14 7.60 10.50 5 -23 14 2.40 18.50 14 -5 23 0.90 10.30 -5 -23 14 -6.10 19.30 -5 -23 14 -4.80 11.60 14 5 23 -4.90 19.80 -14 -5 23 -8.30 16.50 1 -6 23 183.28 18.30 -1 6 23 148.09 22.70 -1 6 23 153.58 17.60 1 -6 23 131.09 23.20 1 6 23 152.68 23.20 -1 -6 23 167.58 23.50 -1 -6 23 176.18 17.90 1 6 23 163.78 17.90 3 -6 23 179.18 27.20 3 -6 23 236.68 22.90 -3 6 23 246.28 31.40 3 6 23 247.88 33.50 -3 -6 23 256.07 22.30 -3 -6 23 216.18 32.10 3 6 23 250.97 22.70 5 -6 23 91.29 12.60 -5 6 23 96.39 19.70 5 -6 23 75.99 20.60 -5 -6 23 136.19 15.20 -5 -6 23 123.99 20.80 5 6 23 130.39 16.00 5 6 23 115.19 21.60 7 -6 23 108.29 13.10 6 -23 7 113.69 13.10 -7 6 23 89.49 19.20 7 -6 23 100.99 21.70 6 -23 7 87.89 19.20 7 6 23 89.99 12.60 -7 -6 23 93.29 20.50 7 6 23 96.89 22.60 -7 -6 23 104.49 12.00 -9 6 23 263.37 31.80 6 -23 9 240.98 32.70 6 -23 9 266.37 25.20 9 -6 23 265.97 35.90 9 -6 23 267.07 25.10 9 6 23 239.38 25.20 9 6 23 215.78 31.10 -9 -6 23 273.47 23.40 -9 -6 23 289.77 34.50 11 -6 23 132.29 18.50 11 -6 23 137.39 24.10 6 -23 11 117.69 22.20 -11 6 23 134.79 20.70 6 -23 11 113.69 15.10 -11 -6 23 147.69 22.80 -11 -6 23 146.59 15.70 11 6 23 170.68 27.00 13 -6 23 41.70 20.10 6 -23 13 38.90 18.40 13 -6 23 59.39 11.80 6 -23 13 51.19 11.80 -13 6 23 54.69 15.30 -6 -23 13 68.79 12.90 13 6 23 56.19 22.80 -13 -6 23 91.59 19.60 -6 -23 13 48.10 20.80 0 -7 23 143.49 17.40 0 7 23 166.48 24.10 0 -7 23 135.19 23.00 2 -7 23 220.48 30.80 2 -7 23 210.08 19.90 -2 7 23 191.68 25.20 -2 -7 23 188.28 19.50 -2 -7 23 165.38 25.00 2 7 23 159.88 25.30 -4 7 23 322.67 35.10 4 -7 23 305.47 35.90 4 -7 23 314.47 27.00 4 7 23 262.07 37.10 -4 -7 23 291.67 26.20 -4 -7 23 256.57 35.70 7 -23 6 115.89 13.20 -6 7 23 103.39 19.30 6 -7 23 80.49 21.20 6 -7 23 114.09 13.30 -6 -7 23 91.19 11.70 -6 -7 23 87.89 20.40 6 7 23 50.89 21.10 8 -7 23 94.19 12.50 8 -7 23 68.59 20.00 -8 7 23 111.89 20.60 7 -23 8 80.89 18.60 7 -23 8 98.59 13.20 -8 -7 23 103.19 20.80 8 7 23 66.49 21.60 -8 -7 23 90.79 11.30 7 -23 10 235.48 22.30 10 -7 23 173.08 27.40 7 -23 10 176.68 26.40 10 -7 23 197.78 22.20 -10 7 23 213.68 29.50 -10 -7 23 227.38 20.50 -10 -7 23 224.88 27.30 10 7 23 191.98 29.60 12 -7 23 40.70 20.90 12 -7 23 46.30 11.40 -12 7 23 33.00 15.40 7 -23 12 40.90 11.40 7 -23 12 34.20 17.90 -12 -7 23 52.89 8.90 12 7 23 45.60 21.50 -7 -23 12 44.20 22.40 -12 -7 23 72.69 19.70 -1 8 23 267.87 34.40 1 -8 23 244.18 24.20 1 -8 23 234.28 34.30 -1 -8 23 258.57 34.20 1 8 23 261.17 34.80 -1 -8 23 290.27 24.20 -3 8 23 348.07 40.40 3 -8 23 360.76 32.40 3 -8 23 359.66 41.30 8 -23 3 384.16 32.60 -3 -8 23 413.66 32.20 3 8 23 370.86 41.40 -3 -8 23 404.76 41.50 5 -8 23 291.07 38.10 8 -23 5 302.27 29.50 5 -8 23 319.17 29.60 -5 8 23 316.67 37.30 -5 -8 23 336.27 39.70 -5 -8 23 395.96 29.00 5 8 23 334.27 39.20 -7 8 23 89.89 19.80 8 -23 7 80.49 18.60 8 -23 7 95.99 12.40 7 -8 23 106.79 13.40 7 -8 23 71.69 21.00 -7 -8 23 91.39 11.70 7 8 23 63.69 20.70 -7 -8 23 85.69 21.20 -9 8 23 181.08 23.90 9 -8 23 153.98 19.50 9 -8 23 158.08 25.00 8 -23 9 161.18 19.10 8 -23 9 143.79 22.10 -9 -8 23 162.48 24.60 -9 -8 23 172.78 17.80 9 8 23 109.29 24.40 11 -8 23 49.70 21.60 -11 8 23 22.40 15.50 11 -8 23 34.10 11.30 8 -23 11 50.19 17.50 8 -23 11 46.20 11.10 -11 -8 23 47.00 9.20 11 8 23 23.90 21.30 -11 -8 23 51.09 20.30 8 -23 13 22.60 17.80 13 -8 23 18.00 11.10 8 -23 13 16.80 10.30 13 -8 23 28.60 18.50 13 8 23 18.50 21.40 -8 -23 13 24.80 18.40 -13 -8 23 13.80 18.20 -8 -23 13 26.70 12.30 0 -9 23 8.70 17.50 0 9 23 1.80 17.40 0 -9 23 8.50 9.10 -2 9 23 21.60 17.40 2 -9 23 8.70 18.10 9 -23 2 11.40 9.00 2 -9 23 24.80 8.90 -2 -9 23 10.50 8.80 2 9 23 17.10 18.70 -2 -9 23 26.10 19.40 4 -9 23 218.58 20.20 9 -23 4 203.88 20.10 -4 9 23 189.78 25.20 9 -23 4 203.58 26.40 4 -9 23 187.08 26.50 4 9 23 115.19 25.00 -4 -9 23 146.19 26.30 -4 -9 23 153.78 19.20 9 -23 6 276.17 25.80 -6 9 23 292.67 34.60 6 -9 23 262.27 36.10 9 -23 6 275.87 31.80 6 -9 23 270.27 26.00 -6 -9 23 281.37 25.00 -6 -9 23 245.08 35.80 6 9 23 247.48 36.50 9 -23 8 159.48 22.50 9 -23 8 168.98 19.40 8 -9 23 146.79 25.40 -8 9 23 162.58 23.10 8 -9 23 177.58 20.00 -8 -9 23 162.08 18.40 8 9 23 126.59 25.30 -8 -9 23 165.98 24.60 10 -9 23 94.29 22.40 9 -23 10 104.29 20.50 10 -9 23 88.49 14.40 9 -23 10 119.59 14.90 -10 9 23 127.39 20.20 -10 -9 23 158.68 16.20 -10 -9 23 173.38 24.70 10 9 23 113.19 25.00 9 -23 12 12.20 9.90 12 -9 23 8.90 10.30 12 -9 23 -7.00 18.70 9 -23 12 -2.00 16.90 -12 -9 23 27.30 19.70 12 9 23 27.00 21.10 -12 -9 23 41.70 9.30 -9 -23 12 26.90 19.10 1 -10 23 2.30 9.30 -1 10 23 4.90 17.90 10 -23 1 -8.50 8.60 1 -10 23 20.20 20.70 1 10 23 5.10 17.70 -1 -10 23 10.90 18.80 -1 -10 23 10.90 9.00 3 -10 23 33.30 10.30 3 -10 23 28.20 19.70 10 -23 3 35.00 9.60 -3 10 23 42.60 18.40 10 -23 3 19.90 14.40 3 10 23 45.20 19.20 -3 -10 23 25.50 16.50 -3 -10 23 48.70 9.60 5 -10 23 215.48 21.80 -5 10 23 198.28 26.90 10 -23 5 177.68 21.20 10 -23 5 190.28 27.70 5 -10 23 132.59 26.00 5 10 23 183.58 28.00 -5 -10 23 260.17 20.90 -5 -10 23 218.28 27.70 7 -10 23 225.88 22.80 -7 10 23 200.98 26.40 10 -23 7 208.38 29.20 7 -10 23 172.48 27.90 10 -23 7 218.98 22.40 7 10 23 217.38 30.80 -7 -10 23 233.78 29.70 -7 -10 23 228.08 21.50 9 -10 23 91.59 22.60 9 -10 23 105.39 14.50 10 -23 9 142.09 17.80 -9 10 23 111.09 20.70 10 -23 9 99.59 19.90 -9 -10 23 143.49 16.70 -9 -10 23 156.98 23.40 9 10 23 113.09 23.20 10 -23 11 -3.10 9.50 11 -10 23 3.60 10.30 11 -10 23 7.20 19.10 23 -11 10 1.40 1.60 10 -23 11 9.30 16.40 -11 -10 23 4.30 19.90 -11 -10 23 4.00 9.00 11 10 23 18.40 21.70 0 -11 23 208.78 21.20 11 -23 0 195.28 20.30 0 -11 23 195.28 28.70 0 11 23 176.28 26.30 11 -23 2 131.79 19.00 2 -11 23 140.29 18.00 -2 11 23 147.99 23.40 11 -23 2 137.79 17.70 2 -11 23 109.49 25.10 11 -23 -2 142.79 16.80 -2 -11 23 158.58 18.00 -2 -11 23 113.89 22.20 2 11 23 132.39 23.60 -4 11 23 40.60 18.90 11 -23 4 59.89 15.30 11 -23 4 45.70 10.20 4 -11 23 43.70 20.10 4 -11 23 43.20 10.50 -4 -11 23 18.70 19.70 -4 -11 23 38.50 10.50 4 11 23 28.10 20.00 6 -11 23 138.99 24.90 -6 11 23 150.88 22.90 23 -6 11 178.08 16.50 11 -23 6 129.49 18.20 6 -11 23 142.09 19.00 11 -23 6 118.69 20.30 -6 -11 23 158.58 18.00 6 11 23 122.59 24.90 -6 -11 23 156.38 27.20 8 -11 23 47.10 11.90 -8 11 23 53.49 18.00 8 -11 23 45.50 20.70 11 -23 8 40.90 16.90 11 -23 8 45.00 10.60 8 11 23 20.60 20.70 -8 -11 23 54.69 11.10 -8 -11 23 65.49 21.60 10 -11 23 0.70 10.70 11 -23 10 -4.80 10.50 10 -11 23 -3.60 19.30 23 -10 11 3.40 1.80 11 -23 10 5.80 15.30 -10 -11 23 4.10 9.30 10 11 23 -3.20 19.30 -10 -11 23 3.30 19.00 12 -23 1 4.80 3.60 1 -12 23 5.90 22.10 1 -12 23 25.20 10.10 12 -23 1 19.40 8.50 -1 12 23 1.20 18.30 -1 -12 23 18.30 19.80 1 12 23 17.30 19.20 -1 -12 23 15.70 9.70 -3 12 23 28.40 18.60 3 -12 23 26.80 19.80 12 -23 3 27.70 9.40 3 -12 23 44.20 10.50 3 12 23 32.80 19.60 -3 -12 23 11.40 17.30 -3 -12 23 25.30 10.00 12 -23 5 26.40 13.60 5 -12 23 9.40 10.50 5 -12 23 7.50 19.90 23 -5 12 13.90 8.40 12 -23 5 12.80 9.30 -5 12 23 23.10 19.20 5 12 23 16.00 20.40 -5 -12 23 29.60 18.10 -5 -12 23 21.00 9.40 23 -7 12 35.20 9.40 7 -12 23 33.90 20.20 7 -12 23 38.00 11.80 -7 12 23 30.30 19.20 12 -23 7 34.00 10.40 12 -23 7 40.40 15.90 7 12 23 34.30 21.20 -7 -12 23 78.59 21.50 -7 -12 23 64.29 11.80 12 -23 9 15.50 10.00 9 -12 23 21.50 19.60 12 -23 9 12.60 15.50 9 -12 23 -0.80 10.50 9 12 23 19.70 19.80 -9 -12 23 33.10 10.10 -9 -12 23 24.40 22.50 0 -13 23 110.69 13.60 0 13 23 79.79 22.70 0 -13 23 75.29 18.80 2 -13 23 144.99 18.40 13 -23 2 111.19 15.90 -2 13 23 115.29 23.10 2 -13 23 103.69 23.70 -2 -13 23 129.19 17.80 -2 -13 23 120.69 25.70 2 13 23 150.68 26.30 13 -23 4 38.50 9.50 4 -13 23 11.30 22.50 -4 13 23 16.60 18.50 4 -13 23 33.80 10.70 4 13 23 22.10 19.80 -4 -13 23 24.50 11.10 -4 -13 23 30.80 20.50 6 -13 23 52.99 11.70 6 -13 23 44.00 20.80 23 -6 13 67.39 10.80 13 -23 6 53.89 10.90 6 13 23 60.69 22.40 -6 -13 23 76.59 12.40 -6 -13 23 73.19 21.40 8 -13 23 17.80 10.60 13 -23 8 -12.20 8.90 13 -23 8 29.90 9.90 23 -8 13 16.10 8.80 8 -13 23 22.90 20.50 -8 -13 23 56.59 23.50 -8 -13 23 25.10 10.20 8 13 23 24.50 23.60 1 -14 23 23.10 22.50 1 -14 23 34.80 10.70 1 14 23 31.80 20.40 -1 -14 23 32.00 11.60 -1 -14 23 34.10 19.30 3 -14 23 82.89 25.70 3 -14 23 86.19 13.70 -3 -14 23 57.89 18.70 3 14 23 92.49 23.80 -3 -14 23 99.59 12.70 14 -23 5 -5.00 4.50 14 -23 5 4.50 8.90 23 -5 14 -4.80 9.10 5 -14 23 -2.70 10.30 5 -14 23 3.90 17.50 5 14 23 -7.20 21.00 -5 -14 23 -8.40 16.60 -5 -14 23 -5.80 9.50 0 -15 23 -3.30 23.00 15 -23 0 8.80 3.00 0 -15 23 2.80 9.70 2 -15 23 13.70 17.60 2 -15 23 0.50 10.10 -2 -15 23 10.00 10.10 -2 -15 23 8.60 19.90 0 0 24 13.40 8.10 0 0 24 9.20 15.60 2 0 24 1.00 15.20 -2 0 24 -5.40 15.80 2 0 24 3.00 8.20 -2 0 24 -3.90 7.60 4 0 24 51.79 9.90 -4 0 24 71.29 10.10 -4 0 24 57.19 17.50 4 0 24 35.10 16.90 6 0 24 6.00 9.60 6 0 24 -2.00 17.30 -6 0 24 2.60 15.00 -6 0 24 9.40 7.40 -8 0 24 150.38 22.70 8 0 24 172.18 19.10 8 0 24 153.98 26.10 -8 0 24 164.08 16.80 -10 0 24 116.09 19.90 10 0 24 138.39 17.80 10 0 24 111.39 23.70 -10 0 24 112.09 16.40 0 -24 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1.8794 -2.8807 5 22 15 26.8889 10.0169 5 23 6 -6.7227 -11.3367 5 23 8 -20.0939 -30.5764 5 23 10 5.2931 63.0569 5 23 12 -47.1233 -33.3999 5 23 14 -19.4955 -16.8729 5 24 5 -51.8885 -7.2705 5 24 7 33.9164 -77.7431 5 24 9 -5.2853 -1.7483 5 24 11 -59.7786 56.5795 5 25 6 -55.2143 -20.7331 5 25 8 -5.0689 -31.4895 5 25 10 8.2096 -3.0511 5 26 5 -4.0604 -12.7265 5 26 7 16.3651 -3.1654 6 6 6 75.4916 -3.1312 6 7 7 66.0890 -109.0038 6 8 6 -79.2056 -7.2570 6 8 8 66.9899 -23.9880 6 9 7 33.2029 156.8392 6 9 9 12.2237 24.7768 6 10 6 119.4065 6.7833 6 10 8 -59.2722 11.9332 6 10 10 68.5660 -97.8201 6 11 7 7.9228 -28.9797 6 11 9 -45.5473 -51.9835 6 11 11 -119.0282 -15.0973 6 12 6 7.9927 -130.0872 6 12 8 -77.7811 -77.8779 6 12 10 -131.1188 112.8832 6 13 7 -5.8428 -102.7544 6 13 9 61.2470 -43.9873 6 13 11 37.9930 -89.9532 6 13 13 0.9302 42.5196 6 14 6 -61.1245 77.3945 6 14 8 47.2357 31.0641 6 14 10 -153.8332 43.2238 6 14 12 22.4879 -102.2108 6 14 14 -68.8295 -59.0239 6 15 7 -1.4307 69.9350 6 15 9 21.5677 -4.9694 6 15 11 -18.1873 -14.4678 6 15 13 38.2090 98.8505 6 15 15 -64.7119 -5.8393 6 16 6 5.7018 17.2624 6 16 8 -29.9166 -44.0648 6 16 10 -95.4426 -33.0760 6 16 12 40.1207 159.7846 6 16 14 -4.3297 1.4398 6 16 16 -34.9630 -3.7462 6 17 7 -5.1421 24.7136 6 17 9 78.1046 -1.5177 6 17 11 102.8201 23.8395 6 17 13 -90.4006 -26.5491 6 17 15 40.9443 -9.6242 6 17 17 -7.0654 -11.0069 6 18 6 11.7192 48.9509 6 18 8 -71.4095 80.8725 6 18 10 24.6076 -0.9210 6 18 12 -43.9375 -61.8974 6 18 14 -12.4120 8.0352 6 18 16 41.6339 -6.3294 6 18 18 12.9886 6.6267 6 19 7 1.6393 -18.4717 6 19 9 -1.5412 8.7989 6 19 11 -25.5460 -47.4050 6 19 13 71.9343 19.7613 6 19 15 32.6379 21.2743 6 19 17 -17.0660 -10.3125 6 19 19 -53.5967 -42.2623 6 20 6 117.4831 13.4771 6 20 8 93.2200 45.2354 6 20 10 -30.4339 -28.2869 6 20 12 -39.3304 -37.1535 6 20 14 28.8839 9.5587 6 20 16 -2.3918 2.0045 6 20 18 12.1598 -6.6854 6 21 7 -13.5014 -107.7871 6 21 9 8.8259 110.3310 6 21 11 -25.7050 68.6502 6 21 13 -12.9130 -2.7955 6 21 15 -24.7917 -15.2234 6 21 17 -17.4891 0.1740 6 22 6 23.6996 58.1056 6 22 8 -73.6026 -65.8768 6 22 10 -61.5201 -53.8438 6 22 12 2.1360 -21.5767 6 22 14 10.1325 1.9500 6 23 7 -3.2525 -47.1489 6 23 9 42.0609 -0.4903 6 23 11 63.1454 19.0469 6 23 13 -0.5155 -21.8804 6 24 6 63.4237 79.5611 6 24 8 14.1196 -18.4890 6 24 10 -0.9974 -17.4173 6 24 12 -35.7953 -9.9860 6 25 7 31.5599 -11.5138 6 25 9 -38.0107 -17.6249 6 26 6 10.9469 -39.7205 7 9 8 9.6729 39.4781 7 10 9 25.6209 16.2976 7 11 8 -132.6529 -40.7644 7 11 10 76.3883 -43.0664 7 12 9 -56.8356 56.1547 7 12 11 -36.0832 -32.9266 7 13 8 -42.9226 1.1698 7 13 10 44.7704 -59.5474 7 13 12 14.1810 -8.0352 7 14 7 132.8437 128.6907 7 14 9 -73.5720 -65.6283 7 14 11 -20.6032 -3.0603 7 14 13 -9.5674 -48.7210 7 15 8 13.2029 31.9476 7 15 10 11.9084 -49.8978 7 15 12 6.4053 17.7393 7 15 14 71.0210 -17.7450 7 16 7 10.0727 13.7405 7 16 9 41.0031 -39.8500 7 16 11 -23.4359 3.0035 7 16 13 -26.9092 -70.3697 7 16 15 10.8648 -15.6542 7 17 8 -22.1600 -0.9171 7 17 10 -11.9370 27.6328 7 17 12 59.8378 -41.3330 7 17 14 30.8173 3.5072 7 17 16 31.6121 8.1334 7 18 7 -75.3576 -84.4194 7 18 9 74.7880 52.8946 7 18 11 5.0615 54.7141 7 18 13 -1.8497 -4.5440 7 18 15 -17.0799 -14.3107 7 18 17 2.5519 -13.6854 7 19 8 67.4857 114.6690 7 19 10 -29.3514 58.8868 7 19 12 -17.3771 -30.7322 7 19 14 -34.6731 21.2208 7 19 16 3.9275 -1.9725 7 19 18 -10.6288 1.8128 7 20 7 -81.7508 -144.5800 7 20 9 48.2519 -164.0312 7 20 11 4.4961 -37.8720 7 20 13 -12.3216 26.8423 7 20 15 -17.9527 -25.3296 7 20 17 19.7294 13.7017 7 21 8 -2.4053 25.6056 7 21 10 -38.4750 26.2091 7 21 12 -0.2201 83.9202 7 21 14 45.6551 83.5574 7 21 16 7.6802 30.3097 7 22 7 68.9261 -108.2730 7 22 9 -12.9931 -32.7884 7 22 11 -9.6866 16.1252 7 22 13 2.7331 31.0029 7 22 15 7.6737 20.6942 7 23 8 5.1337 -24.3349 7 23 10 11.3499 -29.9779 7 23 12 0.0217 62.8380 7 24 7 -8.8678 -19.5461 7 24 9 -49.8653 38.7250 7 24 11 6.1320 34.8528 7 25 8 21.0022 -22.3659 8 8 8 -66.0069 -53.8100 8 10 8 25.5069 3.9209 8 10 10 -27.2509 -43.8851 8 11 9 -77.7183 23.2032 8 11 11 163.9087 5.3859 8 12 8 -100.9869 -125.1864 8 12 10 -39.1109 26.9959 8 12 12 62.2931 15.7495 8 13 9 -59.7479 54.7637 8 13 11 63.8955 46.9952 8 13 13 5.0453 1.3744 8 14 8 -72.8199 49.0258 8 14 10 -1.0553 -3.9390 8 14 12 -7.5655 -18.7758 8 14 14 -13.9857 54.1675 8 15 9 1.8243 -15.7938 8 15 11 32.0928 11.2297 8 15 13 73.3262 -3.2553 8 15 15 -41.8673 -21.6423 8 16 8 74.1966 -99.7267 8 16 10 -82.7676 70.0650 8 16 12 -41.6860 25.9308 8 16 14 33.4774 -1.4027 8 16 16 33.6340 4.6090 8 17 9 -94.7329 -23.3735 8 17 11 -82.0545 1.1196 8 17 13 -16.6856 12.5977 8 17 15 -16.3646 29.0306 8 17 17 55.9750 2.6577 8 18 8 -12.6684 -70.2834 8 18 10 16.4021 -115.5958 8 18 12 -31.9239 -21.4938 8 18 14 5.3402 0.7476 8 18 16 8.4498 7.7425 8 18 18 -33.5807 31.2704 8 19 9 -9.2127 -44.6462 8 19 11 68.8751 63.1364 8 19 13 37.4460 -22.6449 8 19 15 38.9521 11.1072 8 19 17 0.9223 1.7855 8 20 8 203.8519 149.5104 8 20 10 65.3011 13.7561 8 20 12 -2.8111 17.2491 8 20 14 10.9057 41.1686 8 20 16 -20.9935 -23.1034 8 21 9 69.6140 65.9661 8 21 11 1.9201 -12.6971 8 21 13 39.3657 -39.6974 8 21 15 -24.2031 -3.7008 8 22 8 -103.8507 52.7646 8 22 10 -25.0349 -24.8873 8 22 12 -36.5260 -24.5591 8 22 14 -15.0219 3.9270 8 23 9 -38.0965 21.2476 8 23 11 -36.0105 46.2707 8 23 13 -30.4795 -21.0511 8 24 8 -15.1925 -20.6351 8 24 10 -42.1916 -52.3329 9 10 9 118.4682 -1.7648 9 11 10 -35.7162 -17.2732 9 12 9 -99.7924 57.3628 9 12 11 -21.3570 143.5613 9 13 10 -118.7710 -68.2217 9 13 12 13.7911 -43.3095 9 14 9 -83.0805 -51.4809 9 14 11 -28.7979 -12.2259 9 14 13 30.6744 10.0902 9 15 10 -24.4988 -13.2412 9 15 12 -3.0939 13.7678 9 15 14 25.8114 13.5324 9 16 9 6.0034 14.7952 9 16 11 -92.7190 0.2043 9 16 13 -29.8797 -9.4930 9 16 15 -9.8297 -2.5158 9 17 10 -70.4249 -1.1466 9 17 12 -38.1272 76.3954 9 17 14 -12.3508 44.2270 9 17 16 11.9250 8.5281 9 18 9 -48.3781 -34.6142 9 18 11 36.3565 57.0226 9 18 13 -22.7455 18.2962 9 18 15 7.4126 -17.4326 9 18 17 -24.0417 17.1751 9 19 10 -53.0575 40.5007 9 19 12 -32.7723 -17.4202 9 19 14 -41.4545 1.2862 9 19 16 12.6099 -39.4936 9 19 18 -11.2128 -3.9896 9 20 9 -2.9190 -70.5463 9 20 11 -52.7048 -22.2453 9 20 13 33.6592 -25.9081 9 20 15 1.3190 -16.4019 9 21 10 -5.3060 -125.6324 9 21 12 1.7388 42.1283 9 21 14 -10.6786 26.9296 9 22 9 -28.9650 37.0338 9 22 11 27.4066 -15.7479 9 22 13 -36.5654 11.0329 9 23 10 64.7968 -38.2050 9 23 12 23.0603 -8.7994 9 24 9 9.8269 48.3617 10 11 11 -0.9489 3.0255 10 12 10 85.5464 95.3161 10 12 12 11.4577 24.5513 10 13 11 -67.2954 63.4830 10 13 13 -61.9151 82.3015 10 14 10 42.6885 80.9610 10 14 12 -78.7564 -65.8522 10 14 14 -74.3718 96.6475 10 15 11 3.8701 16.4090 10 15 13 60.7284 -21.7062 10 15 15 -32.6580 17.6674 10 16 10 -14.2055 50.2295 10 16 12 16.4378 -46.7901 10 16 14 9.6092 -42.4845 10 16 16 -53.1306 1.8229 10 17 11 -93.5201 28.4231 10 17 13 56.0380 -38.3893 10 17 15 -6.4907 22.3321 10 17 17 29.5187 22.4469 10 18 10 -56.5117 -0.0035 10 18 12 -56.9573 94.4908 10 18 14 14.6488 60.9024 10 18 16 17.0022 17.0235 10 18 18 22.0233 20.5807 10 19 11 -81.4153 21.1480 10 19 13 19.4824 -69.2120 10 19 15 -9.3595 -10.8176 10 19 17 2.2389 -4.1375 10 20 10 -119.4107 29.8220 10 20 12 -32.3004 5.7594 10 20 14 -1.4121 47.1771 10 20 16 -8.5458 -9.9382 10 21 11 61.7800 -23.4366 10 21 13 59.8728 -7.0747 10 21 15 18.4980 -11.2785 10 22 10 15.4134 -40.7822 10 22 12 -4.7483 -14.5443 10 23 11 13.1130 -5.0665 11 12 11 -71.5587 13.7367 11 13 12 49.0089 19.1385 11 14 11 -56.8916 -175.5072 11 14 13 -17.1071 -9.2279 11 15 12 -99.8812 -30.1797 11 15 14 8.2358 83.1927 11 16 11 8.9710 -99.3967 11 16 13 -26.1188 -25.4676 11 16 15 15.6575 -1.3980 11 17 12 -47.5875 -41.1975 11 17 14 41.8053 -2.6850 11 17 16 9.9239 -8.2000 11 18 11 41.3085 -43.2527 11 18 13 11.6509 -43.9414 11 18 15 8.5600 -12.9734 11 18 17 -11.3734 -7.7441 11 19 12 -0.9457 -35.8448 11 19 14 -28.0561 -17.4048 11 19 16 -7.9875 5.4251 11 20 11 41.4495 -13.8811 11 20 13 -11.2634 16.0286 11 20 15 -16.1769 3.9201 11 21 12 -0.7768 29.9835 11 21 14 -38.5590 14.4590 11 22 11 -43.2610 8.6317 12 12 12 -95.5306 42.3139 12 13 13 27.6250 -17.5467 12 14 12 -154.9384 39.8639 12 14 14 71.7917 149.3173 12 15 13 -74.1080 -10.1472 12 15 15 -39.0880 -17.6956 12 16 12 -27.4172 -101.1167 12 16 14 22.0445 34.4778 12 16 16 -42.8824 -3.4094 12 17 13 -1.5320 -50.2518 12 17 15 24.8248 -20.5037 12 17 17 15.4127 -3.5958 12 18 12 -17.5561 112.2764 12 18 14 -14.5799 -16.4162 12 18 16 -2.3044 -38.6907 12 19 13 -20.5127 -12.9968 12 19 15 5.4659 0.2027 12 20 12 19.8182 0.8020 12 20 14 -23.0318 -15.0395 12 21 13 -14.0263 -57.1224 13 14 13 58.0459 -149.1973 13 15 14 -14.9896 -47.3848 13 16 13 -20.1363 58.3753 13 16 15 76.6335 -6.6935 13 17 14 11.6433 -29.2262 13 17 16 30.6751 12.5330 13 18 13 -88.4309 64.1426 13 18 15 36.1777 15.4607 13 19 14 10.4945 0.4366 13 20 13 -14.5589 0.0597 14 14 14 37.1842 -72.4444 14 15 15 -6.0846 -21.9528 14 16 14 100.8536 -137.1889 14 16 16 24.6767 -9.3420 14 17 15 -15.1563 0.0089 14 18 14 -0.6476 -68.4326 15 16 15 51.8812 30.5466 0 0 0 0.0 0.0 ; _shelx_fab_checksum 97669 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, z, -y' '-x, -z, y' '-z, -y, x' 'z, -y, -x' 'y, -x, -z' '-y, x, -z' 'z, x, y' 'y, z, x' '-y, -z, x' 'z, -x, -y' '-y, z, -x' '-z, -x, y' '-z, x, -y' 'y, -z, -x' 'x, -y, -z' '-x, y, -z' '-x, -y, z' '-y, -x, z' 'y, x, z' '-z, y, -x' 'z, y, x' 'x, -z, -y' 'x, z, y' 'x+1/2, y+1/2, z+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' '-z+1/2, -y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, -z+1/2, x+1/2' 'z+1/2, -x+1/2, -y+1/2' '-y+1/2, z+1/2, -x+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, -z+1/2, -x+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' '-z+1/2, y+1/2, -x+1/2' 'z+1/2, y+1/2, x+1/2' 'x+1/2, -z+1/2, -y+1/2' 'x+1/2, z+1/2, y+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe00 Fe 0.64466(11) 0.28648(8) 0.71352(8) 0.0384(14) Uani 1 2 d S TU P . . O02 O 0.6684(4) 0.2835(4) 0.7732(4) 0.071(4) Uani 1 1 d . U . . . O03 O 0.6923(5) 0.3077(5) 0.6923(5) 0.0415(15) Uani 1 6 d S TU P . . N3 N 0.5868(8) 0.2633(5) 0.7367(5) 0.106(6) Uani 1 2 d DS TU P . . O05 O 0.6158(3) 0.3390(3) 0.7227(5) 0.078(4) Uani 1 1 d D U . . . N00A N 0.4807(9) 0.2178(14) 0.7762(13) 0.106(5) Uani 0.5 1 d D U P A -1 H00A H 0.4685 0.2067 0.7562 0.127 Uiso 0.5 1 calc R U P A -1 N00F N 0.5326(9) 0.5030(9) 0.7317(12) 0.063(5) Uani 0.25 1 d D U P B -1 C00I C 0.6275(3) 0.3725(3) 0.7292(7) 0.060(2) Uani 1 2 d DS TU P . . C15 C 0.6040(6) 0.4039(6) 0.7298(7) 0.062(4) Uani 0.25 1 d DG U P B -1 C6 C 0.6208(7) 0.4418(6) 0.7283(17) 0.063(5) Uani 0.25 1 d DG U P B -1 H6 H 0.6486 0.4448 0.7269 0.075 Uiso 0.25 1 calc R U P B -1 C9 C 0.5963(9) 0.4753(6) 0.7290(18) 0.063(4) Uani 0.25 1 d DG U P B -1 H9 H 0.6076 0.5010 0.7280 0.075 Uiso 0.25 1 calc R U P B -1 C00J C 0.5551(8) 0.4709(8) 0.7312(9) 0.063(5) Uani 0.25 1 d DG U P B -1 C13 C 0.5384(6) 0.4330(9) 0.7326(15) 0.063(4) Uani 0.25 1 d DG U P B -1 H13 H 0.5106 0.4300 0.7341 0.076 Uiso 0.25 1 calc R U P B -1 C5 C 0.5629(6) 0.3995(7) 0.7319(15) 0.063(5) Uani 0.25 1 d DG U P B -1 H5 H 0.5515 0.3739 0.7329 0.075 Uiso 0.25 1 calc R U P B -1 C009 C 0.6875(6) 0.3125(6) 0.7871(8) 0.051(6) Uani 1 2 d S TU P . . C00B C 0.5195(10) 0.2325(7) 0.7675(7) 0.106(5) Uani 1 2 d DS TU P . . C39 C 0.5787(7) 0.2728(7) 0.7775(4) 0.108(5) Uani 1 1 d D U . . . H39 H 0.5976 0.2852 0.7941 0.130 Uiso 1 1 calc R U . . . C96 C 0.5392(7) 0.2621(7) 0.7912(7) 0.106(5) Uani 1 1 d D U . . . H96 H 0.5274 0.2735 0.8139 0.127 Uiso 1 1 calc R U . . . O5 O 0.4758(8) 0.2468(8) 0.8380(8) 0.082(7) Uani 0.5 1 d D U P A -1 C8 C 0.4586(10) 0.2182(13) 0.8124(13) 0.107(5) Uani 0.5 1 d D U P A -1 C7 C 0.4172(7) 0.2105(7) 0.8154(9) 0.106(6) Uani 0.5 1 d DG U P A -1 C21 C 0.4008(8) 0.1793(7) 0.7936(8) 0.107(6) Uani 0.5 1 d DG U P A -1 H21 H 0.4175 0.1609 0.7807 0.128 Uiso 0.5 1 calc R U P A -1 C23 C 0.3596(9) 0.1753(9) 0.7908(9) 0.106(6) Uani 0.5 1 d G U P A -1 H23 H 0.3485 0.1542 0.7761 0.127 Uiso 0.5 1 calc R U P A -1 C00P C 0.3348(7) 0.2026(10) 0.8099(9) 0.106(6) Uani 0.5 1 d G U P A -1 C2 C 0.3512(8) 0.2338(9) 0.8317(10) 0.106(6) Uani 0.5 1 d G U P A -1 H2 H 0.3345 0.2522 0.8446 0.128 Uiso 0.5 1 calc R U P A -1 C1 C 0.3924(9) 0.2377(8) 0.8345(10) 0.107(6) Uani 0.5 1 d DG U P A -1 H1 H 0.4035 0.2588 0.8493 0.128 Uiso 0.5 1 calc R U P A -1 N1 N 0.5002(8) 0.5127(11) 0.7160(10) 0.063(5) Uani 0.25 1 d D U P B -1 C12 C 0.4668(8) 0.5431(9) 0.7184(8) 0.063(5) Uani 0.25 1 d G U P B -1 C4 C 0.4757(14) 0.5831(9) 0.7249(19) 0.063(6) Uani 0.25 1 d DG U P B -1 H4 H 0.5024 0.5912 0.7278 0.075 Uiso 0.25 1 calc R U P B -1 C3 C 0.445(2) 0.6110(12) 0.727(2) 0.063(6) Uani 0.25 1 d G U P B -1 H3 H 0.4512 0.6381 0.7315 0.075 Uiso 0.25 1 calc R U P B -1 C11 C 0.4057(17) 0.5990(19) 0.7229(12) 0.063(6) Uani 0.25 1 d DG U P B -1 C10 C 0.3968(9) 0.559(2) 0.7164(17) 0.063(6) Uani 0.25 1 d G U P B -1 H10 H 0.3701 0.5509 0.7135 0.075 Uiso 0.25 1 calc R U P B -1 C14 C 0.4274(8) 0.5311(14) 0.7141(17) 0.063(6) Uani 0.25 1 d DG U P B -1 H14 H 0.4213 0.5041 0.7097 0.075 Uiso 0.25 1 calc R U P B -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe00 0.038(3) 0.0389(18) 0.0389(18) 0.002(2) -0.0068(14) 0.0068(14) O02 0.087(10) 0.087(9) 0.040(7) 0.013(6) -0.008(7) -0.032(8) O03 0.0415(15) 0.0415(15) 0.0415(15) 0.0001(9) -0.0001(9) 0.0001(9) N3 0.103(9) 0.108(7) 0.108(7) 0.005(8) 0.005(6) -0.005(6) O05 0.018(7) 0.075(7) 0.143(13) -0.021(7) 0.019(8) 0.004(6) N00A 0.105(8) 0.109(8) 0.106(7) 0.005(7) 0.001(6) -0.001(6) N00F 0.065(8) 0.066(8) 0.060(8) 0.000(7) 0.000(7) -0.002(7) C00I 0.060(2) 0.060(2) 0.060(3) 0.0000(11) 0.0000(11) -0.0001(15) C15 0.064(7) 0.064(6) 0.060(8) -0.001(6) 0.001(7) 0.000(6) C6 0.064(7) 0.064(7) 0.060(8) -0.001(6) 0.000(7) -0.001(6) C9 0.064(7) 0.064(7) 0.060(8) 0.000(7) 0.000(7) -0.002(6) C00J 0.065(7) 0.065(7) 0.061(8) -0.001(7) 0.000(7) -0.002(6) C13 0.064(7) 0.064(7) 0.061(8) 0.000(7) 0.001(7) -0.001(6) C5 0.064(7) 0.064(7) 0.060(8) -0.001(7) 0.001(7) 0.000(6) C009 0.056(7) 0.056(7) 0.041(9) 0.007(6) -0.007(6) -0.006(8) C00B 0.105(8) 0.107(6) 0.107(6) 0.007(8) 0.002(5) -0.002(5) C39 0.106(8) 0.111(8) 0.107(8) 0.004(8) 0.002(7) -0.002(7) C96 0.103(8) 0.109(7) 0.105(7) 0.006(7) 0.004(6) -0.002(6) O5 0.093(16) 0.072(14) 0.082(14) 0.033(11) -0.008(12) 0.018(12) C8 0.106(8) 0.108(8) 0.106(7) 0.007(7) 0.002(6) -0.001(6) C7 0.105(8) 0.108(8) 0.105(8) 0.007(7) 0.001(7) 0.000(6) C21 0.107(8) 0.107(8) 0.106(8) 0.007(7) 0.001(6) 0.000(6) C23 0.106(8) 0.107(8) 0.106(8) 0.006(7) 0.002(7) 0.000(7) C00P 0.105(8) 0.108(8) 0.106(9) 0.006(7) 0.001(7) 0.000(7) C2 0.106(8) 0.107(8) 0.106(8) 0.006(7) 0.001(7) 0.000(7) C1 0.106(8) 0.108(8) 0.106(8) 0.005(7) 0.001(6) -0.001(6) N1 0.065(8) 0.065(8) 0.059(9) -0.001(8) 0.000(8) -0.003(7) C12 0.064(9) 0.066(9) 0.059(10) -0.001(9) -0.001(9) -0.003(8) C4 0.065(10) 0.065(9) 0.058(10) 0.000(9) -0.001(9) -0.003(8) C3 0.065(10) 0.066(10) 0.058(11) 0.000(10) -0.001(10) -0.003(9) C11 0.064(10) 0.066(10) 0.057(11) 0.000(10) -0.001(10) -0.003(9) C10 0.064(10) 0.066(10) 0.058(11) 0.000(10) -0.002(10) -0.003(9) C14 0.064(9) 0.066(10) 0.058(10) -0.001(9) -0.002(9) -0.003(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O02 Fe00 O02 77.1(8) . 23_566 ? O02 Fe00 N3 89.0(7) 23_566 . ? O02 Fe00 N3 89.0(7) . . ? O03 Fe00 O02 93.1(7) . . ? O03 Fe00 O02 93.1(7) . 23_566 ? O03 Fe00 N3 177.3(11) . . ? O03 Fe00 O05 97.7(7) . 23_566 ? O03 Fe00 O05 97.7(7) . . ? O05 Fe00 O02 94.3(6) 23_566 23_566 ? O05 Fe00 O02 166.6(6) 23_566 . ? O05 Fe00 O02 94.3(6) . . ? O05 Fe00 O02 166.6(6) . 23_566 ? O05 Fe00 N3 80.5(6) 23_566 . ? O05 Fe00 N3 80.5(6) . . ? O05 Fe00 O05 92.1(8) . 23_566 ? C009 O02 Fe00 119.8(15) . . ? Fe00 O03 Fe00 119.72(15) 11_566 10_665 ? Fe00 O03 Fe00 119.72(15) . 11_566 ? Fe00 O03 Fe00 119.72(15) . 10_665 ? C39 N3 Fe00 114.9(14) . . ? C39 N3 Fe00 114.9(14) 23_566 . ? C39 N3 C39 113(3) 23_566 . ? C00I O05 Fe00 132.6(11) 19_665 . ? C00I O05 Fe00 132.6(11) . . ? C00I O05 C00I 0(2) 19_665 . ? C00B N00A H00A 114.8 . . ? C8 N00A H00A 114.8 . . ? C8 N00A C00B 130(4) . . ? N1 N00F C00J 135(3) . . ? O05 C00I O05 124.9(19) 19_665 . ? O05 C00I C15 107.3(14) 19_665 . ? O05 C00I C15 123.5(13) . . ? C00I C00I O05 0(10) 19_665 19_665 ? C00I C00I O05 0(10) 19_665 . ? C00I C00I C15 0(10) 19_665 . ? C00I C15 C6 119.4(12) . . ? C00I C15 C5 120.6(12) . . ? C6 C15 C5 120.0 . . ? C15 C6 H6 120.0 . . ? C15 C6 C9 120.0 . . ? C9 C6 H6 120.0 . . ? C6 C9 H9 120.0 . . ? C00J C9 C6 120.0 . . ? C00J C9 H9 120.0 . . ? N00F C00J C9 119.0(12) . . ? N00F C00J C13 121.0(12) . . ? C13 C00J C9 120.0 . . ? C00J C13 H13 120.0 . . ? C00J C13 C5 120.0 . . ? C5 C13 H13 120.0 . . ? C15 C5 H5 120.0 . . ? C13 C5 C15 120.0 . . ? C13 C5 H5 120.0 . . ? O02 C009 O02 131(3) 19_665 . ? C96 C00B N00A 112(3) 23_566 . ? C96 C00B N00A 123(3) . . ? C96 C00B C96 124(3) 23_566 . ? N3 C39 H39 122.5 . . ? N3 C39 C96 115(2) . . ? C96 C39 H39 122.5 . . ? C00B C96 C39 115(2) . . ? C00B C96 H96 122.7 . . ? C39 C96 H96 122.7 . . ? N00A C8 O5 108(3) . . ? N00A C8 C7 125(3) . . ? O5 C8 C7 119(2) . . ? C21 C7 C8 119.2(12) . . ? C21 C7 C1 120.0 . . ? C1 C7 C8 119.9(12) . . ? C7 C21 H21 120.0 . . ? C7 C21 C23 120.0 . . ? C23 C21 H21 120.0 . . ? C21 C23 H23 120.0 . . ? C00P C23 C21 120.0 . . ? C00P C23 H23 120.0 . . ? C23 C00P C2 120.0 . . ? C00P C2 H2 120.0 . . ? C1 C2 C00P 120.0 . . ? C1 C2 H2 120.0 . . ? C7 C1 H1 120.0 . . ? C2 C1 C7 120.0 . . ? C2 C1 H1 120.0 . . ? N00F N1 C12 143(3) . . ? C4 C12 N1 119.9(12) . . ? C4 C12 C14 120.0 . . ? C14 C12 N1 120.1(12) . . ? C12 C4 H4 120.0 . . ? C12 C4 C3 120.0 . . ? C3 C4 H4 120.0 . . ? C4 C3 H3 120.0 . . ? C11 C3 C4 120.0 . . ? C11 C3 H3 120.0 . . ? C3 C11 C10 120.0 . . ? C11 C10 H10 120.0 . . ? C11 C10 C14 120.0 . . ? C14 C10 H10 120.0 . . ? C12 C14 H14 120.0 . . ? C10 C14 C12 120.0 . . ? C10 C14 H14 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe00 O02 2.156(12) 23_566 ? Fe00 O02 2.156(12) . ? Fe00 O03 1.888(4) . ? Fe00 N3 2.23(3) . ? Fe00 O05 2.034(12) . ? Fe00 O05 2.034(12) 23_566 ? O02 C009 1.254(15) . ? O03 Fe00 1.888(4) 10_665 ? O03 Fe00 1.888(4) 11_566 ? N3 C39 1.4298(15) 23_566 ? N3 C39 1.4300(15) . ? O05 C00I 1.208(11) . ? O05 C00I 1.208(11) 19_665 ? N00A H00A 0.8700 . ? N00A C00B 1.42(2) . ? N00A C8 1.42(3) . ? N00F C00J 1.314(18) . ? N00F N1 1.2500(15) . ? C00I O05 1.208(11) 19_665 ? C00I C00I 0.00(6) 19_665 ? C00I C15 1.32(2) . ? C15 C6 1.3900 . ? C15 C5 1.3900 . ? C6 H6 0.9400 . ? C6 C9 1.3900 . ? C9 H9 0.9400 . ? C9 C00J 1.3900 . ? C00J C13 1.3900 . ? C13 H13 0.9400 . ? C13 C5 1.3900 . ? C5 H5 0.9400 . ? C009 O02 1.253(15) 19_665 ? C00B C96 1.43(2) . ? C00B C96 1.43(2) 23_566 ? C39 H39 0.9400 . ? C39 C96 1.449(18) . ? C96 H96 0.9400 . ? O5 C8 1.41(3) . ? C8 C7 1.42(3) . ? C7 C21 1.3900 . ? C7 C1 1.3900 . ? C21 H21 0.9400 . ? C21 C23 1.3900 . ? C23 H23 0.9400 . ? C23 C00P 1.3900 . ? C00P C2 1.3900 . ? C2 H2 0.9400 . ? C2 C1 1.3900 . ? C1 H1 0.9400 . ? N1 C12 1.52(3) . ? C12 C4 1.3900 . ? C12 C14 1.3900 . ? C4 H4 0.9400 . ? C4 C3 1.3900 . ? C3 H3 0.9400 . ? C3 C11 1.3900 . ? C11 C10 1.3900 . ? C10 H10 0.9400 . ? C10 C14 1.3900 . ? C14 H14 0.9400 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Fe00 O02 C009 O02 -52(4) . . . 19_665 ? Fe00 N3 C39 C96 172.9(17) . . . . ? Fe00 O05 C00I O05 18(4) . . . 19_665 ? Fe00 O05 C00I C00I 0.0(15) . . . 19_665 ? Fe00 O05 C00I C15 171.7(13) . . . . ? O02 Fe00 O03 Fe00 133.9(14) . . . 10_665 ? O02 Fe00 O03 Fe00 -56.7(15) . . . 11_566 ? O02 Fe00 O03 Fe00 -133.9(14) 23_566 . . 11_566 ? O02 Fe00 O03 Fe00 56.7(15) 23_566 . . 10_665 ? N3 C39 C96 C00B 20(4) . . . . ? O05 Fe00 O03 Fe00 131.3(14) 23_566 . . 11_566 ? O05 Fe00 O03 Fe00 -38.1(16) 23_566 . . 10_665 ? O05 Fe00 O03 Fe00 -131.3(14) . . . 10_665 ? O05 Fe00 O03 Fe00 38.1(16) . . . 11_566 ? O05 C00I C15 C6 -8(3) 19_665 . . . ? O05 C00I C15 C6 -165(3) . . . . ? O05 C00I C15 C5 172(3) 19_665 . . . ? O05 C00I C15 C5 15(3) . . . . ? N00A C00B C96 C39 180(3) . . . . ? N00A C8 C7 C21 42(6) . . . . ? N00A C8 C7 C1 -127(3) . . . . ? N00F C00J C13 C5 179.9(11) . . . . ? N00F N1 C12 C4 41(7) . . . . ? N00F N1 C12 C14 -139(7) . . . . ? C00I O05 C00I O05 0(100) 19_665 . . 19_665 ? C00I O05 C00I C15 0(59) 19_665 . . . ? C00I C00I C15 C6 0.0(13) 19_665 . . . ? C00I C00I C15 C5 0.00(7) 19_665 . . . ? C00I C15 C6 C9 -179.9(10) . . . . ? C00I C15 C5 C13 179.9(11) . . . . ? C15 C6 C9 C00J 0.0 . . . . ? C6 C15 C5 C13 0.0 . . . . ? C6 C9 C00J N00F -179.9(11) . . . . ? C6 C9 C00J C13 0.0 . . . . ? C9 C00J C13 C5 0.0 . . . . ? C00J N00F N1 C12 164(3) . . . . ? C00J C13 C5 C15 0.0 . . . . ? C5 C15 C6 C9 0.0 . . . . ? C00B N00A C8 O5 18(6) . . . . ? C00B N00A C8 C7 166(3) . . . . ? C39 N3 C39 C96 -53(4) 23_566 . . . ? C96 C00B C96 C39 13(5) 23_566 . . . ? O5 C8 C7 C21 -173(3) . . . . ? O5 C8 C7 C1 18(5) . . . . ? C8 N00A C00B C96 148(4) . . . 23_566 ? C8 N00A C00B C96 -20(7) . . . . ? C8 C7 C21 C23 -169(3) . . . . ? C8 C7 C1 C2 169(3) . . . . ? C7 C21 C23 C00P 0.0 . . . . ? C21 C7 C1 C2 0.0 . . . . ? C21 C23 C00P C2 0.0 . . . . ? C23 C00P C2 C1 0.0 . . . . ? C00P C2 C1 C7 0.0 . . . . ? C1 C7 C21 C23 0.0 . . . . ? N1 N00F C00J C9 139(5) . . . . ? N1 N00F C00J C13 -40(5) . . . . ? N1 C12 C4 C3 -179.9(12) . . . . ? N1 C12 C14 C10 179.9(12) . . . . ? C12 C4 C3 C11 0.0 . . . . ? C4 C12 C14 C10 0.0 . . . . ? C4 C3 C11 C10 0.0 . . . . ? C3 C11 C10 C14 0.0 . . . . ? C11 C10 C14 C12 0.0 . . . . ? C14 C12 C4 C3 0.0 . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.634 -0.862 -0.006 27693.1 6240.9 ?