#------------------------------------------------------------------------------ #$Date: 2021-10-03 22:53:30 +0300 (Sun, 03 Oct 2021) $ #$Revision: 269488 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519066.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519066 loop_ _publ_author_name 'Ankade, Shidheshwar B.' 'Samal, Pragnya Paramita' 'Soni, Vineeta' 'Gonnade, Rajesh G.' 'Krishnamurty, Sailaja' 'Punji, Benudhar' _publ_section_title ; Ni(II)-Catalyzed Intramolecular C--H/C--H Oxidative Coupling: An Efficient Route to Functionalized Cycloindolones and Indenoindolones ; _journal_issue 19 _journal_name_full 'ACS Catalysis' _journal_page_first 12384 _journal_page_last 12393 _journal_paper_doi 10.1021/acscatal.1c03314 _journal_volume 11 _journal_year 2021 _chemical_formula_moiety 'C21 H20 N2 O' _chemical_formula_sum 'C21 H20 N2 O' _chemical_formula_weight 316.39 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 94.915(4) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 10.5707(12) _cell_length_b 14.0848(15) _cell_length_c 22.353(2) _cell_measurement_reflns_used 9937 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 29.04 _cell_measurement_theta_min 2.33 _cell_volume 3315.8(6) _computing_cell_refinement 'SAINT (Bruker, 2016)' _computing_data_collection 'APEX3 (Bruker, 2016)' _computing_data_reduction 'SAINT (Bruker, 2016)' _computing_molecular_graphics 'Bruker SHELXTL, Mercury 2020.20' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 298(2) _diffrn_detector 'Photon II CPAD Area Detector' _diffrn_detector_area_resol_mean 7.39 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Kappa Duo PHOTON II CPAD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0726 _diffrn_reflns_av_unetI/netI 0.0441 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 54791 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.994 _diffrn_reflns_theta_min 1.934 _diffrn_source 'micro-focus sealed tube' _diffrn_source_type 'Incoatech I\mS HB' _exptl_absorpt_coefficient_mu 0.079 _exptl_absorpt_correction_T_max 0.991 _exptl_absorpt_correction_T_min 0.988 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS(Bruker, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.268 _exptl_crystal_description plate _exptl_crystal_F_000 1344 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.110 _refine_diff_density_max 0.221 _refine_diff_density_min -0.189 _refine_diff_density_rms 0.034 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.069 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 433 _refine_ls_number_reflns 7978 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.069 _refine_ls_R_factor_all 0.0938 _refine_ls_R_factor_gt 0.0558 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0442P)^2^+1.0307P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1221 _refine_ls_wR_factor_ref 0.1432 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5089 _reflns_number_total 7978 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c03314_si_005.cif _cod_data_source_block Comp_15 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 4519066 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.988 _shelx_estimated_absorpt_t_max 0.991 _shelx_res_file ; TITL mo_SA_InpyCOCy_1_Me_0m_a.res in P2(1)/c mo_SA_InpyCOCy_1_Me_0m_a.res created by SHELXL-2018/3 at 18:45:14 on 26-Jun-2021 REM Old TITL mo_SA_InpyCOCy_1_Me_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.185, Rweak 0.007, Alpha 0.043, Orientation as input REM Formula found by SHELXT: C42 N4 O2 CELL 0.71073 10.5707 14.0848 22.3529 90.000 94.915 90.000 ZERR 8.000 0.0012 0.0015 0.0024 0.000 0.004 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 168 160 16 8 OMIT 0 1 2 OMIT -3.00 56.00 TEMP 24.850 L.S. 30 ACTA SIZE 0.15 0.12 0.11 CONF BOND $H LIST 6 FMAP 2 PLAN 20 WGHT 0.044200 1.030700 FVAR 0.72974 O1A 4 1.145879 0.601677 0.662353 11.00000 0.03764 0.08787 = 0.06292 0.00733 0.02263 0.00759 N1A 3 0.816373 0.601071 0.785209 11.00000 0.03306 0.04862 = 0.04275 -0.00281 0.01330 0.00015 N2A 3 0.684732 0.656460 0.855527 11.00000 0.04503 0.06708 = 0.05471 -0.00819 0.02098 0.00102 C1A 1 0.919320 0.571442 0.825663 11.00000 0.03688 0.04403 = 0.04293 -0.00502 0.01042 0.00005 C2A 1 0.922701 0.546106 0.885636 11.00000 0.05084 0.06644 = 0.04601 0.00126 0.01640 0.00359 AFIX 43 H2A 2 0.850904 0.550507 0.906789 11.00000 -1.20000 AFIX 0 C3A 1 1.036978 0.514060 0.912726 11.00000 0.06461 0.09167 = 0.04430 0.00594 0.00692 0.01403 AFIX 43 H3A 2 1.041784 0.496843 0.953023 11.00000 -1.20000 AFIX 0 C4A 1 1.145023 0.506667 0.881815 11.00000 0.04943 0.08394 = 0.05231 -0.00095 -0.00077 0.01206 AFIX 43 H4A 2 1.220229 0.484395 0.901550 11.00000 -1.20000 AFIX 0 C5A 1 1.141855 0.531869 0.822539 11.00000 0.03579 0.06021 = 0.05058 -0.00588 0.00627 0.00192 AFIX 43 H5A 2 1.214375 0.526943 0.801944 11.00000 -1.20000 AFIX 0 C6A 1 1.028952 0.564863 0.793615 11.00000 0.03414 0.04178 = 0.04402 -0.00541 0.00913 -0.00253 C7A 1 0.988648 0.592221 0.733243 11.00000 0.03310 0.04282 = 0.04324 -0.00404 0.01095 -0.00144 C8A 1 0.862282 0.611842 0.729809 11.00000 0.03377 0.04434 = 0.04215 -0.00202 0.01184 -0.00141 C9A 1 0.806713 0.641525 0.669348 11.00000 0.03607 0.06433 = 0.04533 0.00325 0.00927 0.00277 AFIX 23 H9AA 2 0.773855 0.705785 0.669996 11.00000 -1.20000 H9AB 2 0.739216 0.598936 0.654300 11.00000 -1.20000 AFIX 0 C10A 1 0.923047 0.634987 0.630877 11.00000 0.03768 0.05215 = 0.04193 -0.00110 0.01200 -0.00211 C11A 1 1.036276 0.607831 0.675716 11.00000 0.03585 0.04666 = 0.04785 -0.00276 0.01352 0.00052 C12A 1 0.949949 0.728737 0.599702 11.00000 0.05169 0.05662 = 0.05412 0.00387 0.01137 -0.00715 AFIX 23 H12A 2 0.951178 0.779820 0.628849 11.00000 -1.20000 H12B 2 1.033312 0.725524 0.584741 11.00000 -1.20000 AFIX 0 C13A 1 0.851885 0.751307 0.547778 11.00000 0.06861 0.07013 = 0.06035 0.01894 0.00517 -0.00561 AFIX 23 H13A 2 0.770417 0.763179 0.563285 11.00000 -1.20000 H13B 2 0.876973 0.808487 0.527693 11.00000 -1.20000 AFIX 0 C14A 1 0.838540 0.670236 0.502785 11.00000 0.08879 0.10148 = 0.04758 0.01005 0.00089 -0.01088 AFIX 23 H14A 2 0.772130 0.685260 0.471555 11.00000 -1.20000 H14B 2 0.917419 0.662714 0.484085 11.00000 -1.20000 AFIX 0 C15A 1 0.806504 0.578235 0.533060 11.00000 0.08284 0.07869 = 0.05077 -0.00948 0.00198 -0.01483 AFIX 23 H15A 2 0.802489 0.527100 0.503891 11.00000 -1.20000 H15B 2 0.723838 0.583748 0.548526 11.00000 -1.20000 AFIX 0 C16A 1 0.905712 0.555016 0.584222 11.00000 0.05886 0.05758 = 0.05397 -0.00529 0.01430 -0.00427 AFIX 23 H16A 2 0.986303 0.543013 0.567889 11.00000 -1.20000 H16B 2 0.880901 0.497426 0.603944 11.00000 -1.20000 AFIX 0 C17A 1 0.691315 0.621554 0.800575 11.00000 0.03482 0.03954 = 0.05166 -0.00127 0.01700 -0.00156 C18A 1 0.587467 0.604820 0.760876 11.00000 0.03811 0.05049 = 0.05792 -0.00555 0.01534 -0.00432 AFIX 43 H18A 2 0.596707 0.580852 0.722728 11.00000 -1.20000 AFIX 0 C19A 1 0.468660 0.624615 0.779215 11.00000 0.03509 0.05400 = 0.07927 0.00195 0.01374 -0.00189 AFIX 43 H19A 2 0.396262 0.614792 0.753278 11.00000 -1.20000 AFIX 0 C20A 1 0.458658 0.658847 0.835981 11.00000 0.04281 0.05077 = 0.08373 0.00100 0.03095 0.00483 AFIX 43 H20A 2 0.379677 0.671345 0.849639 11.00000 -1.20000 AFIX 0 C21A 1 0.567803 0.674132 0.871987 11.00000 0.05521 0.06707 = 0.06489 -0.00741 0.03041 0.00522 AFIX 43 H21A 2 0.560681 0.698278 0.910276 11.00000 -1.20000 AFIX 0 O1B 4 0.641230 0.854086 0.660693 11.00000 0.03753 0.09017 = 0.06081 -0.01218 0.02143 -0.00928 N1B 3 0.309349 0.855642 0.782097 11.00000 0.02940 0.04657 = 0.03391 -0.00164 0.00816 -0.00042 N2B 3 0.175454 0.800150 0.851625 11.00000 0.04049 0.05545 = 0.04268 0.00206 0.01253 -0.00140 C1B 1 0.411320 0.886019 0.822622 11.00000 0.03269 0.03856 = 0.03712 0.00057 0.00462 0.00086 C2B 1 0.413305 0.910495 0.882819 11.00000 0.04582 0.05345 = 0.03878 -0.00342 0.00989 -0.00112 AFIX 43 H2B 2 0.341359 0.904718 0.903751 11.00000 -1.20000 AFIX 0 C3B 1 0.526733 0.943829 0.910369 11.00000 0.05679 0.06880 = 0.03792 -0.00917 0.00083 -0.00755 AFIX 43 H3B 2 0.530811 0.960598 0.950730 11.00000 -1.20000 AFIX 0 C4B 1 0.634789 0.953041 0.879612 11.00000 0.04486 0.06857 = 0.04782 -0.00329 -0.00310 -0.01099 AFIX 43 H4B 2 0.709170 0.976408 0.899538 11.00000 -1.20000 AFIX 0 C5B 1 0.633248 0.928139 0.820260 11.00000 0.03212 0.05468 = 0.04829 0.00268 0.00443 -0.00231 AFIX 43 H5B 2 0.705914 0.934238 0.799880 11.00000 -1.20000 AFIX 0 C6B 1 0.521026 0.893562 0.791018 11.00000 0.03300 0.03910 = 0.03870 0.00110 0.00566 0.00039 C7B 1 0.482183 0.865772 0.730567 11.00000 0.03187 0.04146 = 0.03884 -0.00059 0.00842 -0.00073 C8B 1 0.356062 0.845211 0.726787 11.00000 0.03398 0.04098 = 0.03510 -0.00066 0.00941 0.00015 C9B 1 0.301371 0.814814 0.666404 11.00000 0.03531 0.06619 = 0.03954 -0.00813 0.01037 -0.00463 AFIX 23 H9BA 2 0.234134 0.857284 0.650898 11.00000 -1.20000 H9BB 2 0.268418 0.750599 0.667267 11.00000 -1.20000 AFIX 0 C10B 1 0.418585 0.820744 0.628373 11.00000 0.03652 0.05484 = 0.03645 -0.00293 0.01176 -0.00147 C11B 1 0.531401 0.848607 0.673424 11.00000 0.03646 0.04728 = 0.04405 -0.00144 0.01346 -0.00113 C12B 1 0.401649 0.898607 0.580950 11.00000 0.06239 0.06962 = 0.05504 0.01260 0.01176 0.00329 AFIX 23 H12C 2 0.376025 0.956786 0.599747 11.00000 -1.20000 H12D 2 0.482446 0.910276 0.564734 11.00000 -1.20000 AFIX 0 C13B 1 0.303367 0.873083 0.529911 11.00000 0.08008 0.11454 = 0.05245 0.02181 -0.00140 0.01066 AFIX 23 H13C 2 0.300604 0.922490 0.499596 11.00000 -1.20000 H13D 2 0.220230 0.869286 0.545062 11.00000 -1.20000 AFIX 0 C14B 1 0.334758 0.778531 0.501684 11.00000 0.07742 0.15197 = 0.04024 -0.01704 0.00437 -0.00160 AFIX 23 H14C 2 0.268170 0.762225 0.470822 11.00000 -1.20000 H14D 2 0.413611 0.784464 0.482770 11.00000 -1.20000 AFIX 0 C15B 1 0.347640 0.699947 0.548106 11.00000 0.06135 0.09376 = 0.05417 -0.02653 0.01176 -0.00295 AFIX 23 H15C 2 0.372446 0.641599 0.529242 11.00000 -1.20000 H15D 2 0.266261 0.689322 0.563996 11.00000 -1.20000 AFIX 0 C16B 1 0.445863 0.725326 0.599057 11.00000 0.04822 0.06017 = 0.05059 -0.01114 0.01077 0.00231 AFIX 23 H16C 2 0.528939 0.727940 0.583760 11.00000 -1.20000 H16D 2 0.447909 0.675800 0.629278 11.00000 -1.20000 AFIX 0 C17B 1 0.183641 0.835774 0.797041 11.00000 0.03262 0.03681 = 0.04023 -0.00290 0.01248 0.00070 C18B 1 0.080637 0.855008 0.756949 11.00000 0.03636 0.04697 = 0.04607 0.00318 0.01002 0.00458 AFIX 43 H18B 2 0.090978 0.879264 0.718980 11.00000 -1.20000 AFIX 0 C19B 1 -0.038694 0.836966 0.775172 11.00000 0.03139 0.05395 = 0.06363 -0.00071 0.00748 0.00328 AFIX 43 H19B 2 -0.110607 0.848608 0.749255 11.00000 -1.20000 AFIX 0 C20B 1 -0.050653 0.801807 0.831650 11.00000 0.03697 0.04933 = 0.06549 -0.00537 0.02273 -0.00360 AFIX 43 H20B 2 -0.130136 0.790299 0.845042 11.00000 -1.20000 AFIX 0 C21B 1 0.058565 0.784149 0.867784 11.00000 0.04830 0.06011 = 0.04937 0.00281 0.02182 -0.00352 AFIX 43 H21B 2 0.050626 0.759513 0.905882 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_SA_InpyCOCy_1_Me_0m_a.res in P2(1)/c REM wR2 = 0.143183, GooF = S = 1.06883, Restrained GooF = 1.06883 for all data REM R1 = 0.055782 for 5089 Fo > 4sig(Fo) and 0.093768 for all 7978 data REM 433 parameters refined using 0 restraints END WGHT 0.0442 1.0307 REM Highest difference peak 0.221, deepest hole -0.189, 1-sigma level 0.034 Q1 1 0.3694 0.8172 0.6464 11.00000 0.05 0.22 Q2 1 0.9789 0.5863 0.8122 11.00000 0.05 0.21 Q3 1 0.4715 0.8326 0.6490 11.00000 0.05 0.20 Q4 1 0.8719 0.6440 0.6469 11.00000 0.05 0.19 Q5 1 0.4172 0.8733 0.7255 11.00000 0.05 0.18 Q6 1 0.9791 0.6317 0.6525 11.00000 0.05 0.18 Q7 1 0.4607 0.9174 0.8049 11.00000 0.05 0.18 Q8 1 0.9253 0.6814 0.6194 11.00000 0.05 0.17 Q9 1 0.1323 0.8787 0.7834 11.00000 0.05 0.17 Q10 1 0.9073 0.6022 0.6096 11.00000 0.05 0.17 Q11 1 0.5027 0.8816 0.7003 11.00000 0.05 0.16 Q12 1 0.4095 0.8578 0.6097 11.00000 0.05 0.16 Q13 1 0.4765 0.8829 0.8107 11.00000 0.05 0.16 Q14 1 0.3219 0.8665 0.7494 11.00000 0.05 0.16 Q15 1 0.5034 0.9000 0.7553 11.00000 0.05 0.15 Q16 1 0.2515 0.8535 0.7897 11.00000 0.05 0.15 Q17 1 0.8495 0.6565 0.7091 11.00000 0.05 0.14 Q18 1 0.9238 0.5810 0.7260 11.00000 0.05 0.14 Q19 1 0.0244 0.8773 0.7755 11.00000 0.05 0.14 Q20 1 0.3166 0.8573 0.6984 11.00000 0.05 0.14 ; _shelx_res_checksum 85782 _shelx_hkl_file ; -1 0 0 12.80 2.60 3 0 0 -0.10 1.60 3 0 0 1.40 1.80 3 0 0 -0.20 2.10 -3 0 0 1.80 2.00 -3 0 0 1.80 2.00 -3 0 0 0.40 2.20 -3 0 0 -0.60 0.90 -3 0 0 2.80 2.10 -4 0 0 4005.60 195.98 -4 0 0 3904.01 199.18 -4 0 0 3873.61 198.18 4 0 0 3715.93 198.58 4 0 0 3458.85 198.08 -4 0 0 3713.93 199.08 -5 0 0 5.90 4.50 -5 0 0 3.90 1.70 -5 0 0 9.30 4.00 5 0 0 6.30 3.40 -5 0 0 12.00 3.70 5 0 0 6.80 3.00 5 0 0 4.80 3.40 -5 0 0 7.50 3.70 -6 0 0 2007.40 102.39 6 0 0 1905.31 102.99 -6 0 0 1929.41 98.69 -6 0 0 1642.64 104.09 -6 0 0 1880.51 103.59 -6 0 0 1856.61 103.79 -7 0 0 12.70 5.80 -7 0 0 13.70 6.10 -7 0 0 12.50 5.90 -7 0 0 12.70 2.70 7 0 0 16.80 5.70 -8 0 0 1218.58 78.99 -8 0 0 1328.37 77.79 -8 0 0 1296.37 70.39 -8 0 0 1431.06 78.89 8 0 0 1344.07 76.89 -9 0 0 342.37 27.50 -9 0 0 319.47 19.50 9 0 0 343.87 27.30 -9 0 0 322.57 32.60 -9 0 0 337.17 28.00 -10 0 0 87.79 17.90 -10 0 0 57.79 5.50 10 0 0 75.59 14.00 -10 0 0 80.39 16.80 -10 0 0 59.99 12.80 -11 0 0 18.80 9.90 -11 0 0 15.90 10.50 11 0 0 11.40 8.20 -11 0 0 13.90 10.90 -12 0 0 -5.80 7.40 12 0 0 14.60 8.60 -12 0 0 20.80 9.80 -13 0 0 21.40 11.60 13 0 0 23.50 10.90 -13 0 0 27.20 11.40 -13 0 0 36.60 13.20 -14 0 0 8.60 7.90 -14 0 0 0.00 9.10 -14 0 0 6.80 10.20 14 0 0 14.10 9.80 1 -1 0 230.28 14.20 -1 -1 0 273.37 13.80 -1 -1 0 238.38 13.40 1 -1 0 275.87 14.30 -1 -1 0 257.37 14.20 1 -1 0 241.68 14.10 -1 1 0 273.27 14.00 -1 1 0 213.78 14.00 -1 1 0 221.88 14.10 3 -1 0 11.10 2.70 -3 -1 0 14.80 3.80 -3 -1 0 14.60 1.90 -3 -1 0 13.40 3.00 3 -1 0 10.40 3.10 -3 -1 0 16.80 3.20 3 -1 0 12.90 3.50 3 1 0 11.40 2.90 3 1 0 14.30 3.50 -3 1 0 13.40 3.60 3 1 0 10.50 2.80 -3 1 0 10.60 3.10 3 1 0 10.80 1.60 -3 1 0 5.00 2.70 -3 1 0 15.60 3.70 -4 -1 0 142.09 10.20 4 -1 0 127.59 12.60 -4 -1 0 122.49 12.50 4 -1 0 135.69 11.00 4 -1 0 117.99 10.20 -4 -1 0 147.69 10.90 -4 -1 0 129.89 8.00 -4 1 0 140.89 9.20 -4 1 0 141.49 11.50 4 1 0 149.39 13.10 -4 1 0 126.69 12.90 -4 1 0 137.79 10.30 4 1 0 110.79 10.10 4 1 0 142.99 10.40 4 1 0 126.19 8.00 5 -1 0 1.10 2.90 5 -1 0 -2.80 2.30 -5 -1 0 0.70 2.30 -5 -1 0 0.40 1.00 -5 -1 0 1.50 2.40 5 -1 0 8.20 3.50 -5 1 0 2.50 2.00 -5 1 0 -0.80 3.00 5 1 0 0.10 2.20 -5 1 0 3.00 2.80 5 1 0 1.90 3.30 5 1 0 -1.80 2.20 -5 1 0 -2.50 1.70 -5 1 0 1.40 3.50 -6 -1 0 260.37 22.30 -6 -1 0 282.47 21.00 -6 -1 0 293.67 16.80 -6 -1 0 295.47 20.10 6 -1 0 291.67 21.00 -6 -1 0 328.47 22.30 -6 1 0 299.27 22.20 -6 1 0 310.67 22.00 6 1 0 283.97 20.90 -6 1 0 271.57 22.30 -6 1 0 276.37 21.90 -6 1 0 307.07 18.20 6 1 0 317.27 21.00 -7 -1 0 7.60 6.00 7 -1 0 16.50 5.80 -7 -1 0 14.80 6.40 -7 -1 0 11.10 5.60 -7 -1 0 11.10 2.40 -7 1 0 9.20 5.70 -7 1 0 8.90 5.60 7 1 0 12.30 5.20 -7 1 0 10.40 2.90 -7 1 0 8.90 6.00 -8 -1 0 19.10 3.00 -8 -1 0 29.30 8.10 8 -1 0 20.10 7.60 -8 -1 0 13.10 6.00 -8 -1 0 25.00 8.70 8 1 0 33.10 8.40 -8 1 0 16.20 7.90 -8 1 0 24.50 4.60 -8 1 0 14.60 6.80 -8 1 0 15.50 7.50 -9 -1 0 53.79 4.60 -9 -1 0 45.00 11.00 -9 -1 0 57.69 12.80 9 -1 0 84.59 13.80 -9 -1 0 55.59 13.00 -9 1 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575.04 31.20 -2 -6 0 613.34 32.60 -2 6 0 568.74 35.10 -2 6 0 601.44 33.30 2 6 0 563.84 34.40 -2 6 0 570.74 34.30 -2 6 0 611.94 34.20 3 -6 0 26.50 6.00 -3 -6 0 38.80 4.90 3 -6 0 30.10 5.70 3 -6 0 20.50 4.60 -3 -6 0 34.00 3.10 -3 -6 0 33.10 6.90 -3 6 0 21.40 5.00 -3 6 0 27.70 6.50 -3 6 0 26.90 5.80 3 6 0 34.70 6.20 -4 -6 0 11.10 3.70 -4 -6 0 3.10 3.40 4 -6 0 5.70 3.40 -4 -6 0 2.10 2.20 -4 -6 0 4.00 2.10 4 -6 0 1.30 2.70 -4 6 0 5.70 4.10 -4 6 0 4.60 3.20 -4 6 0 1.90 3.60 4 6 0 8.30 3.50 4 6 0 7.60 3.70 -5 -6 0 338.77 21.10 -5 -6 0 324.97 25.00 5 -6 0 329.37 23.50 -5 -6 0 332.67 22.30 5 6 0 353.86 21.90 -5 6 0 356.46 24.70 -5 6 0 363.66 26.70 -5 6 0 327.47 24.80 5 6 0 380.76 20.30 5 6 0 379.36 24.80 -6 -6 0 152.08 16.00 6 -6 0 152.48 14.30 -6 -6 0 155.58 12.20 -6 6 0 167.78 15.90 6 6 0 155.88 11.60 -6 6 0 144.79 16.30 6 6 0 176.98 15.40 6 6 0 173.98 11.40 -6 6 0 168.88 15.60 -7 -6 0 23.20 5.70 -7 -6 0 30.50 8.90 7 -6 0 27.00 7.30 7 6 0 27.20 8.40 -7 6 0 25.50 8.60 -7 6 0 26.10 8.70 7 6 0 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428.16 31.60 5 7 0 515.55 30.70 -6 -7 0 5.80 2.90 -6 -7 0 7.40 5.70 6 -7 0 4.20 4.40 -6 7 0 -0.60 4.80 6 7 0 10.20 3.70 6 7 0 18.00 6.80 -6 7 0 13.40 7.00 -6 7 0 4.10 3.90 6 7 0 10.10 2.50 7 -7 0 71.79 12.30 -7 -7 0 48.20 11.60 -7 -7 0 76.99 8.00 7 7 0 72.79 7.00 -7 7 0 64.59 12.70 -7 7 0 64.99 13.10 -7 7 0 92.19 14.30 7 7 0 70.69 7.10 7 7 0 89.49 14.10 -8 -7 0 25.40 9.70 -8 -7 0 19.40 5.30 8 -7 0 12.40 7.40 -8 7 0 21.10 7.20 8 7 0 23.20 8.50 -8 7 0 11.70 7.00 8 7 0 16.50 3.50 -8 7 0 9.00 8.50 8 7 0 16.00 4.30 9 -7 0 5.50 5.60 -9 -7 0 21.00 6.00 -9 -7 0 3.40 7.80 -9 7 0 14.60 8.50 9 7 0 23.50 9.10 9 7 0 9.60 2.50 -9 7 0 6.00 6.40 -9 7 0 14.10 9.80 10 -7 0 -5.30 5.80 -10 -7 0 8.20 7.60 -10 -7 0 -0.20 4.50 10 7 0 0.10 7.10 -10 7 0 21.60 11.10 -10 7 0 9.00 6.30 -10 7 0 14.20 9.20 -11 -7 0 -0.30 7.30 -11 -7 0 5.90 6.70 11 -7 0 1.10 7.40 -11 -7 0 -5.20 6.40 -11 7 0 -12.20 6.80 -11 7 0 3.10 7.70 -11 7 0 -5.20 6.50 11 7 0 10.10 8.50 -12 -7 0 -3.20 7.60 -12 -7 0 -3.30 7.40 12 -7 0 8.60 8.70 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56.29 14.90 11 8 0 38.10 13.00 -11 8 0 81.99 17.90 -12 -8 0 -17.20 5.80 -12 -8 0 11.40 6.90 -12 -8 0 5.20 7.50 12 -8 0 5.10 8.70 -12 8 0 12.20 8.90 -12 8 0 -14.50 8.60 12 8 0 -6.10 7.70 -12 8 0 12.20 11.00 -13 -8 0 10.50 11.40 -13 -8 0 11.20 10.50 13 -8 0 16.10 10.50 -13 8 0 15.80 13.10 -13 8 0 8.60 10.90 -13 8 0 9.20 12.90 13 8 0 24.00 11.80 0 -9 0 0.50 2.40 0 -9 0 -0.80 2.70 0 -9 0 3.80 2.30 0 9 0 4.00 2.90 0 9 0 3.00 3.50 -1 -9 0 10.60 3.70 1 -9 0 5.00 3.10 1 -9 0 13.70 4.30 -1 -9 0 15.70 4.00 -1 -9 0 13.10 3.50 -1 9 0 9.90 4.60 1 9 0 12.90 3.70 -1 9 0 13.40 4.00 1 9 0 9.80 5.10 2 -9 0 27.20 5.40 2 -9 0 23.30 5.70 -2 -9 0 25.80 4.10 -2 -9 0 23.80 4.40 2 9 0 28.20 5.10 -2 9 0 31.80 6.80 -2 9 0 32.70 7.60 2 9 0 37.70 7.90 -3 -9 0 2.10 2.40 3 -9 0 4.50 3.40 -3 -9 0 5.10 1.70 3 -9 0 4.60 3.40 -3 -9 0 3.60 1.90 3 9 0 16.50 5.90 -3 9 0 7.20 5.10 -3 9 0 3.90 2.40 -3 9 0 6.60 4.20 4 -9 0 1.00 3.10 -4 -9 0 0.30 3.00 -4 -9 0 0.60 1.20 4 9 0 2.40 3.40 -4 9 0 1.30 3.10 4 9 0 2.30 3.80 -4 9 0 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6 10 0 4.70 5.30 6 10 0 5.20 3.50 -7 -10 0 333.07 28.70 -7 -10 0 339.67 19.70 7 -10 0 404.36 27.50 -7 10 0 360.86 27.60 -7 10 0 332.07 28.20 -7 10 0 396.56 32.50 7 10 0 365.36 28.90 7 10 0 359.96 24.70 -8 -10 0 5.60 8.70 8 -10 0 6.60 7.20 -8 -10 0 2.80 2.70 -8 10 0 1.90 6.60 8 10 0 4.30 7.60 8 10 0 12.30 5.10 -8 10 0 7.40 6.40 -8 10 0 -11.70 6.00 -9 -10 0 31.40 12.40 9 -10 0 45.50 11.50 -9 10 0 33.90 10.80 9 10 0 19.50 9.50 9 10 0 30.00 5.60 -9 10 0 34.50 12.50 -9 10 0 12.50 8.80 -10 -10 0 1.40 7.70 10 -10 0 2.20 7.40 -10 10 0 4.00 10.80 10 10 0 11.00 3.30 -10 10 0 5.30 7.20 10 10 0 12.70 9.70 -10 10 0 -0.80 8.30 -11 -10 0 113.89 21.10 11 -10 0 133.79 20.90 -11 10 0 153.18 25.10 -11 10 0 142.59 25.70 -11 10 0 119.49 21.40 11 10 0 126.69 22.50 -12 -10 0 15.80 11.20 -12 -10 0 16.30 9.60 12 -10 0 -0.60 9.60 -12 10 0 9.90 9.70 12 10 0 8.90 11.20 -12 10 0 15.80 10.60 -12 10 0 0.90 12.60 0 -11 0 19.60 4.50 0 11 0 29.30 6.00 0 11 0 38.90 8.50 -1 -11 0 117.09 10.00 -1 -11 0 116.19 9.70 1 -11 0 107.69 10.20 1 11 0 126.99 11.00 1 11 0 139.39 13.90 -1 11 0 127.39 11.20 -1 11 0 105.59 14.70 -2 -11 0 16.70 3.40 -2 11 0 12.20 6.50 2 11 0 21.60 7.70 -2 11 0 10.20 4.70 2 11 0 18.70 5.00 -3 -11 0 140.49 8.80 -3 -11 0 142.59 9.30 3 -11 0 157.88 13.30 -3 11 0 138.09 16.00 3 11 0 129.19 14.90 -3 11 0 162.78 14.30 -4 -11 0 18.50 7.10 4 -11 0 15.30 5.70 -4 11 0 16.30 6.10 4 11 0 16.20 6.50 -4 11 0 10.70 6.90 4 11 0 18.70 7.70 5 -11 0 11.10 5.50 -5 -11 0 5.70 6.10 -5 11 0 8.50 4.40 5 11 0 7.00 6.20 -5 11 0 3.10 6.90 5 11 0 0.80 5.20 -6 -11 0 -1.00 7.00 6 -11 0 5.80 6.50 -6 11 0 7.60 5.10 -6 11 0 4.70 6.20 -6 11 0 -0.50 6.10 6 11 0 5.70 5.90 6 11 0 8.80 7.00 7 -11 0 1.10 4.90 -7 -11 0 2.30 6.90 7 11 0 6.30 7.00 -7 11 0 -4.70 7.00 -7 11 0 -3.70 5.70 7 11 0 5.10 5.10 -7 11 0 3.60 7.10 -8 -11 0 0.70 6.70 8 -11 0 -6.60 5.40 -8 11 0 -4.70 4.40 8 11 0 1.30 4.80 -8 11 0 3.90 7.10 -8 11 0 0.20 6.40 8 11 0 -1.60 7.20 -9 -11 0 -10.80 6.60 9 -11 0 18.00 8.20 -9 11 0 3.00 10.00 9 11 0 13.80 5.50 -9 11 0 11.80 7.30 9 11 0 12.00 9.40 -9 11 0 -0.20 6.60 -10 -11 0 -1.50 8.40 10 -11 0 14.50 9.40 10 11 0 10.00 11.40 -10 11 0 10.10 8.40 -10 11 0 -5.60 8.00 -10 11 0 -6.90 9.30 11 -11 0 6.50 7.90 -11 -11 0 18.50 10.10 -11 11 0 18.70 10.20 11 11 0 21.10 11.60 -11 11 0 1.30 7.30 0 -12 0 24.80 5.80 0 12 0 31.70 6.50 0 12 0 45.80 9.90 -1 12 0 -0.80 3.80 1 12 0 3.60 3.70 1 12 0 0.70 5.80 -1 12 0 6.20 6.20 -2 -12 0 13.30 3.50 -2 12 0 15.70 5.60 2 12 0 7.70 4.30 2 12 0 14.50 7.30 -2 12 0 6.50 7.20 -3 -12 0 9.20 2.50 -3 -12 0 9.20 1.80 -3 12 0 19.10 5.60 3 12 0 9.00 6.70 -3 12 0 18.50 8.60 4 -12 0 6.30 5.40 -4 -12 0 -3.90 3.70 -4 12 0 2.20 3.30 4 12 0 4.90 5.20 4 12 0 1.40 4.10 -4 12 0 3.70 6.30 -5 -12 0 147.39 16.50 5 -12 0 161.58 15.60 5 12 0 180.78 17.70 -5 12 0 148.19 14.60 -5 12 0 179.58 17.30 5 12 0 176.98 18.30 -5 12 0 169.98 18.50 6 -12 0 17.90 6.90 -6 -12 0 7.50 7.70 -6 12 0 8.40 5.90 -6 12 0 11.60 5.60 -6 12 0 27.70 10.20 6 12 0 7.80 6.90 6 12 0 8.90 7.10 7 -12 0 38.40 9.00 -7 -12 0 29.30 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11 -2 3.80 2.60 2 11 -2 0.90 3.90 -2 11 2 -1.70 4.00 -1 -11 2 261.77 17.60 -1 11 2 292.97 22.80 -1 11 2 279.57 19.80 1 11 -2 271.77 18.30 1 11 -2 288.17 21.70 0 -11 2 -0.70 2.70 0 -11 -2 3.10 3.40 0 -11 2 1.00 3.30 0 11 2 2.30 3.60 0 11 2 -2.10 3.60 0 11 -2 8.40 5.80 0 11 -2 3.00 3.00 -1 -11 -2 148.59 11.90 -1 11 -2 167.18 15.60 1 11 2 128.99 12.10 1 11 2 133.19 15.10 -1 11 -2 141.79 12.20 2 -11 2 18.90 4.50 -2 -11 -2 17.30 4.50 2 11 2 18.60 7.40 -2 11 -2 26.50 6.40 -2 11 -2 17.20 7.50 2 11 2 22.80 6.00 2 11 2 23.80 7.60 -3 -11 -2 96.99 7.80 3 -11 2 88.39 9.60 3 -11 2 77.79 8.90 -3 -11 -2 64.99 6.50 -3 11 -2 79.89 14.00 -3 11 -2 107.89 12.90 -3 11 -2 110.99 15.20 3 11 2 87.19 13.80 3 11 2 77.09 13.50 4 -11 2 10.20 5.80 -4 -11 -2 -0.50 2.00 -4 11 -2 0.90 4.20 4 11 2 -3.10 5.40 4 11 2 6.80 5.80 -4 11 -2 -3.60 5.00 -4 11 -2 7.30 3.50 -5 -11 -2 49.00 10.70 -5 -11 -2 56.79 5.50 5 -11 2 59.29 10.50 5 11 2 71.49 13.90 -5 11 -2 50.09 12.20 -5 11 -2 72.29 9.80 5 11 2 68.29 12.10 -5 11 -2 82.69 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4.50 7.30 -8 13 2 -0.90 7.60 8 13 -2 1.00 6.30 -8 13 2 -0.70 5.70 8 13 -2 20.50 9.60 -8 13 2 0.00 8.60 7 -13 -2 -4.60 5.50 -7 13 2 5.30 6.00 -7 13 2 8.50 6.20 7 13 -2 3.40 6.40 -7 13 2 -2.00 6.30 7 13 -2 11.50 8.20 -6 -13 2 6.50 6.40 6 -13 -2 5.40 6.30 -6 13 2 8.60 5.50 -6 13 2 -2.00 5.50 6 13 -2 6.10 5.70 6 13 -2 6.50 7.10 -6 13 2 9.00 5.50 -5 -13 2 79.69 12.70 5 -13 -2 82.79 12.60 5 13 -2 69.79 13.80 -5 13 2 97.89 15.30 5 13 -2 74.69 14.00 -5 13 2 70.39 11.20 -5 13 2 85.49 15.30 -4 -13 2 2.50 4.60 -4 13 2 -5.80 4.20 4 13 -2 -4.30 5.90 -4 13 2 5.60 7.00 -3 -13 2 3.50 4.30 -3 13 2 0.10 5.40 3 13 -2 5.00 5.80 -3 13 2 4.20 4.80 -2 -13 2 4.20 2.40 -2 -13 2 5.20 3.50 -2 13 2 1.00 4.60 -2 13 2 6.60 4.90 2 13 -2 10.40 6.30 -1 -13 2 18.70 4.60 -1 -13 2 10.30 3.70 -1 13 2 13.40 7.30 1 13 -2 12.50 5.10 1 13 -2 19.90 7.50 -1 13 2 7.10 4.80 0 -13 2 4.40 4.10 0 -13 2 -0.60 3.20 0 13 -2 -6.00 3.10 0 13 -2 4.20 5.20 0 13 2 0.40 4.10 0 13 2 -5.40 6.10 1 -13 2 2.80 3.70 -1 -13 -2 12.40 5.60 -1 13 -2 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5.10 -4 14 2 2.00 8.20 -3 -14 2 95.79 12.90 -3 14 2 96.39 16.60 3 14 -2 96.59 16.90 -3 14 2 109.79 14.90 -2 -14 2 -0.80 1.30 -2 -14 2 2.40 2.40 -2 -14 2 9.40 5.20 -2 14 2 -0.60 4.50 2 14 -2 -7.70 5.10 -2 14 2 -4.30 6.90 -1 -14 2 50.29 7.30 -1 14 2 48.90 10.80 -1 14 2 25.60 10.30 1 14 -2 51.39 8.30 1 14 -2 70.49 13.90 0 -14 2 -1.10 3.60 0 14 -2 0.30 3.90 0 14 2 -3.30 3.70 0 14 -2 -6.90 5.40 0 14 2 -1.60 6.80 1 -14 2 25.90 6.40 1 14 2 35.50 7.80 1 14 2 46.60 11.30 -1 14 -2 36.60 9.60 -1 14 -2 28.50 7.30 -2 -14 -2 -5.10 2.50 -2 -14 -2 2.20 4.40 -2 14 -2 2.20 7.00 -2 14 -2 2.80 4.70 2 14 2 -4.80 7.00 2 14 2 -4.20 7.70 -3 -14 -2 4.80 4.20 -3 -14 -2 5.10 2.50 3 14 2 12.40 9.00 -3 14 -2 9.80 5.30 3 14 2 2.70 7.80 -3 14 -2 2.50 6.60 -4 -14 -2 -0.60 5.10 -4 -14 -2 2.00 1.80 -4 -14 -2 0.80 2.60 -4 14 -2 1.50 5.20 4 14 2 12.60 8.10 4 14 2 6.10 6.80 -4 14 -2 2.20 7.70 5 -14 2 68.29 11.60 -5 14 -2 70.69 14.60 5 14 2 117.09 17.50 5 14 2 58.69 13.50 -5 14 -2 91.59 14.40 -6 -14 -2 2.10 7.00 6 -14 2 14.80 7.60 -6 14 -2 10.00 8.40 -6 14 -2 10.70 5.40 6 14 2 13.40 8.40 -6 14 -2 20.20 10.10 6 14 2 13.70 8.30 -7 -14 -2 112.29 18.60 7 -14 2 120.19 17.20 7 14 2 103.89 17.00 -7 14 -2 124.79 21.60 -7 14 -2 129.39 19.70 -7 14 -2 130.79 14.40 7 14 2 155.48 23.20 -8 -14 -2 -16.10 8.60 8 14 2 11.40 10.60 -8 14 -2 0.00 5.90 8 14 2 8.40 8.40 -8 14 -2 3.80 9.40 -8 14 -2 2.30 8.10 -9 -14 -2 17.40 9.80 9 -14 2 6.00 7.10 -9 14 -2 2.30 8.10 -9 14 -2 2.60 9.20 9 14 2 -2.00 9.30 -9 14 -2 -4.60 6.50 9 -15 -2 7.40 7.40 -9 -15 2 2.40 9.60 -9 15 2 -10.80 8.50 -9 15 2 -2.50 6.20 -9 15 2 11.70 9.90 9 15 -2 7.20 9.60 9 15 -2 -0.20 7.60 -8 -15 2 3.40 9.10 8 -15 -2 2.90 7.00 -8 15 2 -4.90 5.70 8 15 -2 -13.10 8.40 -8 15 2 6.60 10.10 8 15 -2 6.00 7.20 -8 15 2 -10.00 6.20 -7 -15 2 8.80 8.50 -7 15 2 6.50 6.60 7 15 -2 7.40 8.30 7 15 -2 1.90 9.90 -7 15 2 -8.00 7.10 6 -15 -2 2.90 6.00 -6 -15 2 3.90 7.70 6 15 -2 16.70 8.20 -6 15 2 9.80 8.20 6 15 -2 -0.40 6.70 -6 15 2 -4.40 6.50 -5 -15 2 2.60 6.70 -5 15 2 8.70 9.00 5 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38.70 10.50 4 11 -3 32.80 8.50 -3 -11 3 4.30 3.40 -3 -11 3 3.10 2.80 3 -11 -3 -4.00 4.20 3 11 -3 3.80 4.90 -3 11 3 10.80 5.40 -2 -11 3 136.49 9.70 -2 -11 3 139.09 11.40 -2 -11 3 127.09 7.90 -2 -11 3 120.59 10.50 -2 11 3 163.78 13.60 -2 11 3 89.89 14.20 2 11 -3 132.89 13.20 -1 -11 3 5.40 2.80 -1 -11 3 -0.30 2.40 -1 -11 3 3.30 2.90 -1 11 3 -0.10 4.60 1 11 -3 0.20 3.80 -1 11 3 1.00 3.40 1 11 -3 5.40 3.20 0 -11 3 15.80 4.20 0 -11 3 9.50 3.40 0 11 3 7.50 6.40 0 11 -3 10.10 3.90 0 11 -3 13.90 6.00 0 11 3 11.10 4.40 -1 -11 -3 11.10 4.30 -1 11 -3 25.20 7.90 1 11 3 29.90 6.20 -1 11 -3 34.40 6.50 1 11 3 17.40 7.40 -2 -11 -3 696.23 45.00 -2 11 -3 785.82 49.99 2 11 3 784.42 50.29 -2 11 -3 932.61 47.90 2 11 3 804.32 51.79 2 11 3 735.33 46.40 -2 11 -3 882.01 49.70 3 -11 3 0.30 4.10 3 -11 3 11.70 4.80 -3 -11 -3 3.30 2.60 3 11 3 7.80 6.70 -3 11 -3 12.40 6.50 -3 11 -3 10.70 4.80 3 11 3 -0.80 5.30 -4 -11 -3 73.19 7.30 4 11 3 87.39 14.10 -4 11 -3 94.19 15.70 -4 11 -3 84.89 8.70 -4 11 -3 101.39 13.30 5 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6.50 5.30 -8 -10 -4 24.40 9.40 8 10 4 15.10 6.00 -8 10 -4 6.30 6.60 8 10 4 15.10 9.80 -8 10 -4 3.20 6.20 -8 10 -4 4.10 8.60 -9 -10 -4 46.50 13.60 9 -10 4 60.09 13.00 -9 -10 -4 75.99 10.90 -9 10 -4 55.19 13.90 -9 10 -4 61.69 12.20 9 10 4 60.29 14.80 9 10 4 62.39 10.00 -9 10 -4 57.49 15.40 -10 -10 -4 -7.90 6.00 10 -10 4 6.10 7.70 -10 -10 -4 0.10 7.60 -10 10 -4 -4.60 5.60 -10 10 -4 -3.80 7.30 10 10 4 4.80 8.40 -10 10 -4 8.40 8.90 10 10 4 -5.50 4.50 -11 -10 -4 38.60 9.30 11 -10 4 109.59 17.60 -11 -10 -4 66.69 16.60 11 10 4 80.09 10.20 -11 10 -4 98.49 22.30 -11 10 -4 87.09 16.80 -11 10 -4 73.49 18.30 -12 -10 -4 11.40 12.90 12 -10 4 11.30 8.80 -12 -10 -4 -12.30 7.90 -12 10 -4 4.70 11.40 12 10 4 13.10 12.80 -12 10 -4 19.20 9.00 -11 -11 4 -4.80 8.50 -11 -11 4 15.40 10.50 11 -11 -4 15.90 10.90 -11 11 4 10.30 10.60 11 11 -4 6.10 9.30 -11 11 4 7.90 9.90 10 -11 -4 9.30 8.00 -10 -11 4 2.40 9.90 -10 -11 4 5.50 6.80 -10 11 4 5.10 8.50 -10 11 4 14.10 8.60 10 11 -4 1.60 9.30 -10 11 4 5.50 8.10 9 -11 -4 7.30 8.50 -9 -11 4 10.10 7.00 -9 -11 4 -4.10 6.90 -9 11 4 15.80 8.60 -9 11 4 4.90 7.30 -9 11 4 1.80 7.40 9 11 -4 1.20 7.00 8 -11 -4 8.50 8.00 -8 11 4 14.20 8.90 8 11 -4 6.50 4.60 -8 11 4 15.30 9.00 8 11 -4 7.50 7.50 -8 11 4 13.90 7.70 -7 -11 4 1.00 6.00 7 -11 -4 4.40 5.60 -7 11 4 11.80 7.80 -7 11 4 8.50 5.70 -7 11 4 10.50 8.30 7 11 -4 25.40 6.30 6 -11 -4 -0.40 5.70 -6 -11 4 6.10 6.00 -6 11 4 -0.10 5.90 6 11 -4 -4.40 3.60 -6 11 4 -1.90 6.10 6 11 -4 -1.70 5.60 -5 -11 4 24.70 7.50 5 -11 -4 45.50 9.50 -5 -11 4 39.20 5.70 -5 11 4 29.40 7.50 -5 11 4 47.00 11.00 -5 11 4 42.40 9.90 5 11 -4 34.80 10.40 -4 -11 4 3.80 4.10 -4 -11 4 9.00 3.40 4 -11 -4 -3.60 4.20 -4 11 4 -2.80 3.60 4 11 -4 4.30 4.70 -4 11 4 1.70 5.60 -3 -11 4 22.20 4.50 -3 11 4 20.10 6.80 3 11 -4 15.80 6.10 -2 -11 4 2.10 3.10 -2 -11 4 0.20 2.90 -2 -11 4 -3.10 1.90 2 11 -4 10.20 4.30 -2 11 4 -2.90 3.70 -2 11 4 -2.40 3.60 -1 -11 4 25.90 4.10 -1 -11 4 24.30 3.80 -1 -11 4 25.70 5.40 -1 11 4 26.60 6.50 -1 11 4 7.90 7.00 1 11 -4 16.70 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17.40 10.40 -7 11 -4 18.90 7.80 -7 11 -4 27.00 12.00 -7 11 -4 24.70 8.90 8 -11 4 2.90 6.10 -8 -11 -4 10.00 8.00 -8 -11 -4 2.10 4.10 -8 11 -4 3.40 7.30 8 11 4 -4.10 8.00 8 11 4 -1.20 5.20 -8 11 -4 6.70 8.70 -8 11 -4 6.30 5.70 -9 -11 -4 -1.10 5.50 -9 -11 -4 15.00 9.10 9 -11 4 9.20 7.70 -9 11 -4 10.70 10.50 -9 11 -4 6.70 7.80 -9 11 -4 4.80 5.00 9 11 4 0.80 9.90 9 11 4 10.60 5.60 -10 -11 -4 -6.20 5.60 -10 -11 -4 5.10 9.30 -10 11 -4 -1.70 8.70 -10 11 -4 -7.40 5.80 10 11 4 -1.10 5.20 10 11 4 4.40 8.40 11 -11 4 -6.80 6.60 -11 -11 -4 -17.60 7.60 -11 -11 -4 -6.10 7.30 -11 11 -4 11.40 13.10 -11 11 -4 -6.40 9.80 11 11 4 17.50 12.00 -11 11 -4 0.90 10.00 -11 -12 4 37.70 11.80 11 -12 -4 41.50 13.80 -11 -12 4 28.90 13.70 11 12 -4 53.09 15.50 -11 12 4 49.40 14.10 -11 12 4 83.59 18.50 -11 12 4 48.20 14.20 -10 -12 4 -7.70 6.90 -10 -12 4 8.00 11.00 10 -12 -4 -10.00 6.70 -10 12 4 1.10 7.60 10 12 -4 1.50 8.30 -10 12 4 4.80 8.00 -10 12 4 13.60 9.90 9 -12 -4 18.10 8.50 -9 -12 4 35.40 11.40 -9 12 4 41.20 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13 -4 1.10 5.80 -8 13 -4 -0.50 8.10 8 13 4 -8.00 5.90 -8 13 -4 3.30 8.30 8 13 4 0.60 7.90 -9 -13 -4 -14.30 7.60 9 -13 4 17.90 8.90 -9 13 -4 0.60 8.60 -9 13 -4 5.40 7.90 9 13 4 5.30 7.20 10 -13 4 5.50 8.80 10 13 4 -18.00 8.70 -10 13 -4 5.80 10.40 -10 13 -4 7.50 8.10 -10 13 -4 6.30 11.80 10 13 4 -0.70 6.40 10 -14 -4 6.50 9.40 -10 -14 4 -2.50 10.10 -10 -14 4 -9.60 8.30 -10 14 4 2.50 9.30 -10 14 4 9.10 11.70 -9 -14 4 9.00 9.30 9 -14 -4 7.70 8.60 -9 14 4 4.20 9.10 9 14 -4 11.70 10.70 9 14 -4 -6.00 5.50 -9 14 4 3.50 6.70 -9 14 4 -1.50 8.70 8 -14 -4 -12.60 5.80 -8 -14 4 -8.90 6.50 8 14 -4 2.30 6.50 -8 14 4 6.60 11.40 8 14 -4 4.20 8.70 -8 14 4 -2.20 6.50 -8 14 4 -4.00 7.40 7 -14 -4 96.49 15.60 -7 -14 4 103.29 15.10 -7 14 4 91.19 16.00 -7 14 4 128.59 17.30 -7 14 4 82.59 17.20 7 14 -4 95.89 15.20 7 14 -4 69.29 14.40 -6 -14 4 30.70 8.70 6 -14 -4 24.60 9.50 -6 14 4 21.60 9.80 -6 14 4 50.19 11.70 6 14 -4 27.20 11.20 6 14 -4 11.30 8.50 -5 -14 4 16.00 6.70 5 -14 -4 4.90 6.40 -5 14 4 0.90 7.30 5 14 -4 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2.70 3.20 0 -11 6 4.50 3.00 0 11 -6 4.30 2.90 0 11 6 5.60 7.10 0 11 -6 4.00 4.50 0 11 6 5.80 3.50 0 11 6 10.00 6.70 0 11 -6 5.30 3.50 1 -11 6 893.81 51.39 1 11 6 943.91 62.89 1 11 6 1051.09 62.89 1 11 6 994.40 57.29 -1 11 -6 986.40 54.69 -1 11 -6 1043.00 57.39 -2 -11 -6 7.40 3.80 2 -11 6 2.10 2.60 2 11 6 2.00 5.60 -2 11 -6 2.10 5.30 -2 11 -6 6.30 4.10 -3 -11 -6 146.19 12.00 3 -11 6 147.79 12.20 3 -11 6 154.28 12.90 3 11 6 187.18 18.00 -3 11 -6 163.68 15.00 -3 11 -6 175.18 17.80 3 11 6 150.88 17.30 4 -11 6 -2.60 4.10 4 -11 6 10.90 5.70 -4 -11 -6 9.90 4.00 -4 11 -6 1.10 4.10 4 11 6 1.60 7.30 -4 11 -6 7.90 3.30 4 11 6 4.10 5.70 -4 11 -6 5.90 7.00 5 -11 6 58.09 10.20 -5 -11 -6 54.79 8.00 -5 11 -6 43.00 11.70 5 11 6 58.29 12.10 5 11 6 48.90 12.00 -5 11 -6 42.40 9.80 -5 11 -6 49.10 7.80 6 -11 6 10.00 6.80 -6 -11 -6 5.80 5.90 -6 -11 -6 -4.60 3.40 -6 11 -6 7.90 6.70 -6 11 -6 -3.10 5.60 6 11 6 -13.00 6.40 6 11 6 2.30 6.00 -6 11 -6 6.70 4.60 7 -11 6 5.60 6.40 -7 -11 -6 1.70 4.70 -7 -11 -6 9.60 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9 -4 -9 62.29 11.70 -9 4 9 63.39 12.70 -9 4 9 63.09 9.50 -9 4 9 79.99 10.60 9 4 -9 51.09 10.70 -9 4 9 74.79 13.50 -8 -4 9 87.89 9.80 -8 -4 9 84.59 14.00 8 -4 -9 84.29 12.70 -8 4 9 67.49 13.60 -8 4 9 92.09 9.80 -8 4 9 96.29 11.60 8 4 -9 89.59 12.00 -8 4 9 90.79 14.00 -8 4 9 86.19 9.90 -7 -4 9 25.00 7.40 7 -4 -9 11.50 6.20 -7 -4 9 20.30 5.00 -7 4 9 21.40 5.90 -7 4 9 24.40 5.90 7 4 -9 20.90 5.10 7 4 -9 22.50 5.00 -7 4 9 18.70 7.20 -7 4 9 19.00 6.80 -7 4 9 23.40 5.60 -6 -4 9 249.88 17.10 -6 -4 9 268.17 20.50 6 -4 -9 260.97 18.90 -6 4 9 268.67 17.90 6 4 -9 271.77 16.00 6 4 -9 252.17 17.30 6 4 -9 275.37 18.20 -6 4 9 236.78 19.00 -6 4 9 263.07 21.30 -6 4 9 283.17 20.70 -5 -4 9 1066.59 64.49 -5 -4 9 1093.09 61.09 5 -4 -9 1235.88 64.19 5 4 -9 1121.69 61.59 5 4 -9 1214.08 62.19 -5 4 9 1085.39 65.89 -5 4 9 1032.80 62.49 -5 4 9 1285.07 65.79 5 4 -9 1150.98 62.99 -5 4 9 1148.69 63.09 -5 4 9 1209.08 65.59 5 4 -9 1106.09 65.39 4 -4 -9 117.79 9.40 -4 -4 9 106.79 6.80 -4 -4 9 102.29 9.60 4 4 -9 106.99 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225.88 15.90 0 4 9 212.08 17.60 0 4 -9 253.87 13.50 0 4 9 250.97 14.90 1 -4 9 25.20 6.50 1 -4 9 23.90 2.50 1 -4 9 29.90 4.90 -1 -4 -9 23.70 4.70 1 4 9 23.80 5.80 -1 4 -9 23.50 5.40 1 4 9 21.60 6.10 -1 4 -9 38.40 4.90 -2 -4 -9 22.00 4.60 2 -4 9 33.50 6.40 2 -4 9 24.30 6.60 2 4 9 19.30 5.80 -2 4 -9 37.70 5.50 -2 4 -9 39.30 6.20 -2 4 -9 27.80 6.30 2 4 9 31.60 7.00 -3 -4 -9 100.49 9.40 3 -4 9 78.39 12.10 3 -4 9 81.59 7.90 3 4 9 85.99 9.50 -3 4 -9 105.69 11.10 3 4 9 84.49 11.60 -3 4 -9 102.09 9.40 -4 -4 -9 33.60 6.90 4 -4 9 47.10 7.60 4 4 9 35.30 7.30 4 4 9 38.40 8.70 -4 4 -9 47.90 9.00 -4 4 -9 26.90 7.30 -4 4 -9 45.50 7.80 -5 -4 -9 112.29 13.80 5 -4 9 99.79 10.60 -5 4 -9 98.99 13.50 -5 4 -9 95.69 14.00 5 4 9 118.69 11.40 5 4 9 112.39 15.30 -5 4 -9 81.79 13.40 6 -4 9 61.19 10.60 -6 -4 -9 62.29 10.40 -6 -4 -9 51.49 10.60 -6 4 -9 50.29 10.80 -6 4 -9 41.90 10.80 -6 4 -9 62.89 12.10 6 4 9 70.49 13.10 6 4 9 77.19 11.30 7 -4 9 20.50 7.20 -7 -4 -9 8.50 5.80 -7 -4 -9 8.90 5.80 7 4 9 11.10 7.80 -7 4 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8.70 13 -5 -9 2.50 6.60 -13 5 9 12.00 12.30 -13 5 9 1.00 7.90 -13 5 9 15.60 10.50 13 5 -9 10.30 7.10 -12 -5 9 55.49 16.00 12 -5 -9 27.00 9.80 -12 -5 9 55.49 11.30 -12 5 9 30.50 11.50 -12 5 9 56.09 10.20 12 5 -9 63.29 12.70 -12 5 9 70.59 16.90 11 -5 -9 44.90 11.40 -11 -5 9 12.00 10.00 -11 -5 9 37.70 9.30 -11 5 9 23.20 7.40 -11 5 9 28.60 7.60 -11 5 9 38.20 12.80 11 5 -9 17.70 7.60 10 -5 -9 4.30 6.20 -10 -5 9 0.30 4.90 -10 -5 9 16.00 8.80 -10 5 9 -0.70 7.00 -10 5 9 4.70 4.80 -10 5 9 -7.60 5.00 -10 5 9 9.20 7.70 10 5 -9 -5.10 4.20 9 -5 -9 24.80 8.20 -9 -5 9 19.20 10.80 -9 -5 9 21.00 7.00 -9 5 9 7.70 6.00 -9 5 9 9.70 6.20 -9 5 9 28.40 9.70 9 5 -9 19.20 6.70 -9 5 9 23.00 8.90 -8 -5 9 176.48 18.10 8 -5 -9 168.28 16.30 -8 -5 9 171.88 14.40 -8 5 9 162.58 15.20 -8 5 9 186.88 16.40 8 5 -9 175.38 14.80 -8 5 9 177.68 17.40 8 5 -9 199.38 15.80 -8 5 9 209.28 19.40 7 -5 -9 24.80 7.50 -7 -5 9 22.60 6.80 -7 -5 9 22.10 5.10 -7 5 9 12.90 6.90 -7 5 9 32.60 6.90 7 5 -9 23.30 5.80 -7 5 9 34.50 8.70 7 5 -9 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5 -9 16.90 8.90 12 -5 9 37.30 10.80 -12 -5 -9 19.30 9.50 -12 -5 -9 22.20 11.40 -12 5 -9 20.40 12.10 -12 5 -9 37.70 14.60 12 5 9 34.00 12.70 -12 5 -9 29.60 13.10 13 -6 -9 17.70 12.20 -13 -6 9 25.20 10.30 -13 6 9 -13.10 7.00 -13 6 9 8.00 7.90 -13 6 9 10.20 9.10 13 6 -9 17.60 10.50 -13 6 9 25.70 10.40 -12 -6 9 40.60 13.10 -12 -6 9 14.80 8.10 12 -6 -9 40.60 12.50 12 6 -9 40.50 10.40 -12 6 9 32.60 8.80 -12 6 9 38.50 11.70 -12 6 9 44.10 10.20 11 -6 -9 18.70 8.30 -11 -6 9 11.20 8.60 -11 -6 9 20.50 6.70 -11 6 9 5.80 6.40 -11 6 9 -2.20 5.60 -11 6 9 2.40 6.60 11 6 -9 -1.20 6.00 -11 6 9 11.90 8.50 -10 -6 9 25.80 10.30 10 -6 -9 31.10 9.70 -10 -6 9 25.20 7.80 -10 6 9 20.70 7.90 -10 6 9 28.80 9.70 -10 6 9 13.30 8.20 -10 6 9 28.10 10.70 10 6 -9 38.90 9.30 9 -6 -9 194.78 18.80 -9 -6 9 163.78 25.20 -9 -6 9 192.08 16.40 -9 6 9 220.58 18.10 -9 6 9 210.48 19.20 -9 6 9 196.68 21.70 -9 6 9 201.58 20.70 9 6 -9 189.78 17.90 -8 -6 9 14.20 7.50 8 -6 -9 9.80 6.50 -8 -6 9 12.30 4.70 -8 6 9 17.60 7.70 -8 6 9 16.60 7.30 8 6 -9 20.50 5.50 -8 6 9 26.20 8.00 -8 6 9 10.70 7.10 8 6 -9 16.00 5.50 7 -6 -9 28.60 7.40 -7 -6 9 43.70 5.80 -7 -6 9 36.20 9.30 -7 6 9 23.40 8.60 7 6 -9 38.90 5.60 7 6 -9 36.70 7.30 -7 6 9 41.40 9.20 7 6 -9 38.70 4.70 -7 6 9 45.40 9.00 -6 -6 9 409.26 29.30 -6 -6 9 426.36 25.20 6 -6 -9 445.86 28.90 6 6 -9 453.45 26.00 6 6 -9 425.76 25.80 -6 6 9 440.06 31.20 -6 6 9 493.85 31.30 6 6 -9 436.66 27.30 -6 6 9 427.86 28.50 -6 6 9 450.45 30.80 -5 -6 9 458.05 27.30 5 -6 -9 574.64 32.40 -5 -6 9 504.05 31.80 -5 6 9 502.05 31.90 5 6 -9 501.65 28.10 5 6 -9 493.75 29.80 -5 6 9 535.05 34.60 -5 6 9 565.64 33.90 5 6 -9 537.55 32.70 -5 6 9 492.75 33.50 5 6 -9 514.15 29.10 -4 -6 9 85.79 8.20 4 -6 -9 85.09 8.80 4 6 -9 82.19 8.40 4 6 -9 82.89 6.20 -4 6 9 78.09 8.30 -4 6 9 98.39 10.60 4 6 -9 83.69 8.10 -4 6 9 89.59 9.50 4 6 -9 80.39 6.80 -4 6 9 102.49 13.70 -4 6 9 110.89 10.70 -3 -6 9 477.45 27.60 3 -6 -9 471.45 29.10 -3 6 9 481.35 30.80 -3 6 9 499.25 30.60 -3 6 9 537.65 30.80 3 6 -9 471.85 30.00 3 6 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11.00 6.00 -8 -7 9 29.30 9.50 8 -7 -9 52.49 10.80 -8 -7 9 43.10 6.90 -8 7 9 22.90 9.50 8 7 -9 37.00 5.70 8 7 -9 45.40 9.10 -8 7 9 42.80 9.60 -8 7 9 33.30 10.30 -8 7 9 41.80 11.10 7 -7 -9 36.90 8.50 -7 -7 9 37.10 5.70 -7 -7 9 28.90 8.10 -7 7 9 39.80 10.20 -7 7 9 28.90 8.40 7 7 -9 35.30 4.90 7 7 -9 30.50 7.20 7 7 -9 39.40 5.40 -7 7 9 27.00 8.00 -7 7 9 21.70 8.10 -6 -7 9 235.08 14.40 6 -7 -9 250.67 18.90 -6 -7 9 229.28 13.90 -6 -7 9 244.48 19.10 -6 7 9 221.68 20.30 6 7 -9 222.98 16.90 6 7 -9 233.68 14.40 -6 7 9 269.97 19.50 -6 7 9 295.27 21.50 6 7 -9 241.08 13.70 -6 7 9 238.88 21.10 -5 -7 9 77.79 8.70 5 -7 -9 84.29 11.20 5 7 -9 69.29 7.50 -5 7 9 98.69 13.30 5 7 -9 79.49 5.70 -5 7 9 99.79 12.50 -5 7 9 101.39 15.00 5 7 -9 77.99 5.30 5 7 -9 84.69 8.30 -5 7 9 59.29 10.10 5 7 -9 75.49 9.80 -4 -7 9 551.74 34.70 4 -7 -9 594.94 36.20 4 7 -9 591.54 34.40 -4 7 9 626.04 38.10 -4 7 9 600.44 37.40 4 7 -9 582.74 36.20 4 7 -9 637.24 35.70 -4 7 9 645.34 37.70 4 7 -9 606.04 32.50 -4 7 9 671.13 40.80 4 7 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135.19 13.50 -4 7 -9 123.59 11.40 5 -7 9 8.50 4.50 -5 -7 -9 -4.70 3.20 -5 7 -9 -4.20 5.00 5 7 9 6.60 3.80 5 7 9 6.90 5.00 -5 7 -9 0.40 3.60 -5 7 -9 -1.30 3.20 -6 -7 -9 -3.80 4.90 6 -7 9 -4.90 3.90 -6 -7 -9 -6.60 2.40 -6 7 -9 2.20 6.20 6 7 9 -14.60 5.20 -6 7 -9 -1.40 5.10 6 7 9 2.30 4.70 -6 7 -9 -3.60 4.50 -7 -7 -9 74.19 15.50 7 -7 9 73.99 12.50 -7 -7 -9 66.89 12.00 7 7 9 53.79 13.90 -7 7 -9 72.19 14.50 -7 7 -9 38.40 12.40 -7 7 -9 76.69 14.10 7 7 9 64.59 11.40 8 -7 9 94.49 14.70 -8 -7 -9 71.99 16.00 -8 -7 -9 93.39 14.30 -8 7 -9 66.69 16.40 8 7 9 84.39 16.60 8 7 9 96.39 13.80 -8 7 -9 87.59 16.10 -8 7 -9 78.69 15.40 9 -7 9 17.70 8.40 -9 -7 -9 9.80 8.50 -9 -7 -9 2.80 7.80 -9 7 -9 -9.30 7.00 9 7 9 19.70 6.30 -9 7 -9 4.70 8.10 -9 7 -9 12.40 8.00 9 7 9 23.30 10.30 -10 -7 -9 7.90 6.50 -10 -7 -9 21.20 9.00 10 -7 9 14.10 8.50 -10 7 -9 8.00 9.30 10 7 9 3.20 7.60 10 7 9 16.80 7.60 -10 7 -9 12.60 9.10 -10 7 -9 36.20 10.90 -11 -7 -9 9.50 7.80 11 -7 9 8.60 8.90 11 7 9 10.90 6.20 -11 7 -9 11.10 8.40 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10 53.49 13.40 -9 3 10 48.70 7.60 9 3 -10 46.70 9.10 -9 3 10 36.70 6.70 -9 3 10 48.40 11.00 -9 3 10 37.50 7.40 -8 -3 10 58.89 12.30 8 -3 -10 45.80 9.30 -8 -3 10 42.80 8.10 8 3 -10 53.29 8.70 -8 3 10 37.50 9.80 -8 3 10 40.60 6.70 -8 3 10 39.40 11.50 -8 3 10 41.00 7.50 -8 3 10 51.99 7.20 -7 -3 10 4.20 4.80 7 -3 -10 -3.90 3.30 -7 -3 10 6.40 3.30 -7 3 10 5.20 4.30 -7 3 10 1.60 3.00 -7 3 10 7.30 6.80 -7 3 10 6.30 3.60 -7 3 10 -1.80 2.30 7 3 -10 2.80 3.60 6 -3 -10 681.53 40.20 -6 -3 10 664.03 42.10 -6 3 10 777.62 44.40 6 3 -10 668.23 40.50 -6 3 10 738.83 42.00 -6 3 10 645.24 40.30 -6 3 10 672.23 38.20 6 3 -10 627.54 38.30 6 3 -10 666.73 37.70 5 -3 -10 366.86 22.40 -5 -3 10 338.37 21.50 -5 -3 10 321.97 20.30 -5 -3 10 348.87 23.70 -5 3 10 403.26 24.00 -5 3 10 308.27 20.40 -5 3 10 355.16 24.60 5 3 -10 320.87 20.00 5 3 -10 352.56 21.20 5 3 -10 358.46 22.70 -5 3 10 359.46 20.60 -5 3 10 347.67 23.30 -4 -3 10 1.70 1.20 -4 -3 10 3.00 2.30 -4 -3 10 0.20 2.50 4 3 -10 3.10 2.80 -4 3 10 4.60 2.70 -4 3 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12 10 8.80 10.70 -9 12 10 -7.50 4.40 -9 12 10 1.90 7.50 9 12 -10 -5.00 4.20 -9 12 10 0.60 7.10 9 12 -10 -7.10 6.80 -8 -12 10 5.40 6.70 8 -12 -10 0.40 7.40 8 12 -10 11.20 8.10 8 12 -10 0.20 4.90 -8 12 10 3.70 9.20 -8 12 10 -3.00 5.30 -8 12 10 14.60 9.20 -8 12 10 3.20 7.70 -7 -12 10 13.00 6.20 7 -12 -10 13.50 7.90 -7 12 10 22.10 11.50 -7 12 10 2.10 6.70 -7 12 10 24.10 9.70 -7 12 10 8.30 6.80 7 12 -10 12.60 6.80 -6 -12 10 2.70 4.10 6 -12 -10 -2.40 5.60 -6 12 10 -14.40 6.70 -6 12 10 7.20 6.80 -6 12 10 5.70 6.50 6 12 -10 -3.30 3.70 -6 12 10 13.00 7.50 -5 -12 10 205.18 14.20 5 -12 -10 201.88 18.80 -5 12 10 212.88 24.30 5 12 -10 235.88 18.30 -5 12 10 213.78 20.90 -5 12 10 191.58 19.10 -4 12 10 -4.00 5.70 -4 12 10 -0.10 5.50 -4 12 10 0.00 5.70 4 12 -10 -4.20 4.10 -3 12 10 21.60 11.20 3 12 -10 2.70 4.70 -3 12 10 9.40 7.70 -3 12 10 1.70 4.90 -2 12 10 12.50 5.20 -2 12 10 17.60 10.30 2 12 -10 4.20 4.60 -2 12 10 13.20 7.60 -1 -12 10 -3.10 2.10 1 12 -10 -8.30 3.80 -1 12 10 -4.80 6.00 1 12 -10 0.70 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14 77.89 17.60 10 -7 -14 58.49 12.40 -10 -7 14 51.69 12.80 10 7 -14 86.09 12.70 -10 7 14 79.79 10.40 -10 7 14 56.79 13.30 -10 7 14 84.49 14.10 -10 7 14 77.09 15.50 -9 -7 14 4.10 2.70 9 -7 -14 10.50 6.50 -9 -7 14 3.20 6.40 9 7 -14 5.90 5.00 -9 7 14 -2.30 7.40 -9 7 14 5.20 6.80 -9 7 14 -0.50 5.30 -9 7 14 4.70 8.40 -8 -7 14 13.50 6.00 -8 -7 14 5.60 1.40 8 -7 -14 16.60 6.30 -8 7 14 7.10 8.40 -8 7 14 9.40 7.60 8 7 -14 18.00 7.10 8 7 -14 12.10 5.80 -8 7 14 12.20 7.50 8 7 -14 10.70 5.30 -8 7 14 26.70 7.10 8 7 -14 12.00 3.80 -7 -7 14 171.78 15.30 7 7 -14 135.29 12.40 -7 7 14 166.18 15.60 -7 7 14 165.38 16.90 -7 7 14 188.78 15.10 -7 7 14 160.48 18.20 7 7 -14 162.58 14.20 7 7 -14 142.89 12.90 -7 7 14 167.68 18.30 7 7 -14 148.39 11.30 -6 -7 14 181.08 14.80 6 -7 -14 199.18 16.30 -6 7 14 156.38 16.80 6 7 -14 179.78 12.60 -6 7 14 242.68 20.90 -6 7 14 204.38 18.70 6 7 -14 159.08 14.30 -6 7 14 176.18 15.30 -6 7 14 194.48 15.80 6 7 -14 167.68 12.80 -5 -7 14 20.30 4.50 5 -7 -14 23.60 6.80 5 7 -14 15.80 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14 349.87 27.00 -7 8 14 385.66 25.40 7 8 -14 317.97 20.70 -7 8 14 334.97 28.40 7 8 -14 320.87 19.70 -7 8 14 376.36 29.10 -6 -8 14 -1.80 3.90 6 -8 -14 -0.10 5.20 -6 8 14 5.40 5.60 6 8 -14 -7.30 2.90 -6 8 14 1.20 5.30 6 8 -14 0.70 3.20 6 8 -14 1.80 2.40 -6 8 14 2.90 5.40 -6 8 14 5.50 7.50 5 -8 -14 237.58 18.50 -5 -8 14 252.37 16.30 -5 8 14 263.07 19.90 5 8 -14 224.88 15.40 -5 8 14 217.28 20.30 -5 8 14 274.97 23.90 5 8 -14 239.88 17.80 5 8 -14 212.78 15.50 -5 8 14 233.48 20.40 5 8 -14 251.77 16.00 4 -8 -14 111.29 11.80 -4 -8 14 110.19 8.30 4 8 -14 113.59 8.90 -4 8 14 126.09 15.60 -4 8 14 109.09 14.40 4 8 -14 107.19 9.80 4 8 -14 112.89 9.60 -4 8 14 125.09 18.50 3 8 -14 122.79 8.90 -3 8 14 127.09 15.50 3 8 -14 117.89 10.20 -3 8 14 124.79 13.70 2 8 -14 11.90 4.20 -2 8 14 1.70 5.30 -2 8 14 10.40 7.10 -1 8 14 32.60 9.70 1 8 -14 32.90 6.80 0 8 14 9.30 6.40 0 8 -14 -3.40 1.80 0 8 -14 4.00 3.50 -1 -8 -14 50.59 9.40 1 8 14 47.50 12.90 1 8 14 48.80 11.20 -1 8 -14 50.29 7.30 -1 8 -14 37.40 9.90 -2 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7.50 -5 9 15 2.70 6.30 5 9 -15 16.10 3.90 5 9 -15 15.70 4.00 -5 9 15 20.50 7.40 5 9 -15 15.30 4.60 -4 9 15 93.19 14.40 4 9 -15 73.29 9.40 -4 9 15 57.69 10.90 4 9 -15 77.79 7.60 -4 9 15 82.19 16.30 -3 9 15 -0.10 4.10 -3 9 15 6.00 5.90 3 9 -15 -3.50 2.80 -3 9 15 5.40 7.00 -2 9 15 25.30 11.50 2 9 -15 29.50 6.10 -2 9 15 13.40 7.20 -2 9 15 21.50 7.10 1 9 -15 1.30 3.70 -1 9 15 6.80 8.10 -1 9 15 8.80 5.80 -1 9 15 11.30 7.00 0 9 -15 173.18 16.10 0 9 15 198.48 17.60 0 9 15 196.78 21.60 0 9 -15 163.78 11.30 -1 -9 -15 26.10 7.30 -1 9 -15 25.60 8.30 1 9 15 29.70 9.30 1 9 15 21.60 9.90 -1 9 -15 22.70 5.00 -2 -9 -15 330.67 24.20 -2 9 -15 308.17 22.30 -2 9 -15 326.87 26.50 2 9 15 337.37 27.20 2 9 15 326.67 28.30 -3 -9 -15 -6.40 3.40 -3 9 -15 -4.80 4.20 -3 9 -15 0.70 2.10 3 9 15 10.70 7.50 3 9 15 5.70 9.20 -4 -9 -15 35.20 8.70 4 -9 15 46.30 6.80 -4 9 -15 54.59 13.10 -4 9 -15 61.89 11.50 4 9 15 46.00 11.10 4 9 15 48.20 12.20 -5 -9 -15 0.70 6.20 5 -9 15 6.90 4.80 5 9 15 7.10 7.80 -5 9 -15 7.70 9.10 5 9 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13.30 5.50 -6 12 -15 11.40 7.90 6 12 15 5.40 8.90 -6 12 -15 8.80 10.80 -6 12 -15 6.90 3.90 -7 -12 -15 3.10 6.50 -7 -12 -15 4.70 8.00 7 -12 15 0.30 5.60 -7 12 -15 8.10 9.30 7 12 15 -1.60 7.90 -7 12 -15 -0.80 5.00 7 12 15 -11.20 7.50 -7 12 -15 -15.50 6.80 -8 -12 -15 32.00 10.40 -8 -12 -15 -2.10 9.50 8 -12 15 16.50 8.30 -8 12 -15 4.60 7.70 -8 12 -15 9.30 6.60 8 12 15 10.30 10.80 -8 12 -15 3.50 12.50 8 12 15 9.00 10.30 8 -13 -15 2.20 7.50 -8 13 15 16.40 10.80 -8 13 15 -0.20 8.10 -7 13 15 -3.50 7.80 -7 13 15 8.20 11.30 7 13 -15 -2.10 5.60 -7 13 15 -2.30 6.50 6 13 -15 19.70 7.70 -6 13 15 18.70 11.40 -6 13 15 17.10 8.50 -5 13 15 -1.10 8.00 -5 13 15 -5.80 9.70 -5 13 15 -16.10 5.60 5 13 -15 4.30 5.30 4 13 -15 5.80 6.40 -4 13 15 3.90 8.10 -4 13 15 4.00 6.90 -4 13 15 16.40 10.60 -3 13 15 3.40 6.80 -3 13 15 -8.70 6.50 3 13 -15 3.20 4.90 -3 13 15 -5.80 5.50 -2 13 15 71.59 18.50 -2 13 15 70.89 14.60 -2 13 15 90.79 15.20 2 13 -15 65.69 11.90 -1 13 15 -0.80 4.40 -1 13 15 12.70 8.30 -1 13 15 13.90 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5.80 6 -1 -21 3.20 3.10 -6 1 21 -1.10 5.70 6 1 -21 3.70 2.30 -6 1 21 -0.10 4.90 -6 1 21 -3.50 5.10 5 -1 -21 10.10 3.50 -5 -1 21 9.40 7.90 -5 -1 21 7.60 4.20 5 1 -21 13.80 6.40 -5 1 21 9.40 8.50 5 1 -21 9.80 2.90 5 1 -21 12.20 3.70 -5 1 21 7.50 5.30 -4 1 21 -7.70 5.00 4 1 -21 8.80 4.90 4 1 -21 -0.30 2.70 -4 1 21 2.90 4.60 3 -1 -21 5.80 5.30 -3 -1 21 0.70 6.90 3 1 -21 9.50 4.90 -3 1 21 4.80 5.30 -2 -1 21 4.10 6.40 2 -1 -21 -1.40 3.60 2 1 -21 -1.00 4.90 -2 1 21 -4.10 5.50 -1 -1 21 134.09 19.30 1 -1 -21 124.89 17.00 1 1 -21 184.48 16.90 -1 1 21 158.38 21.20 0 -1 -21 -2.60 5.30 0 -1 21 27.20 8.90 0 1 21 24.40 9.70 0 1 -21 15.50 5.80 1 -1 21 3.40 8.00 -1 -1 -21 -9.00 5.60 1 1 21 12.10 9.20 -1 1 -21 8.80 5.60 -2 -1 -21 7.60 6.10 2 -1 21 21.30 8.70 2 1 21 26.20 3.80 2 1 21 7.40 7.70 2 1 21 21.00 4.10 -2 1 -21 8.10 6.20 3 -1 21 82.69 6.90 -3 -1 -21 67.59 13.30 3 -1 21 54.29 13.40 3 1 21 59.89 14.70 3 1 21 78.59 9.70 -3 1 -21 55.59 13.10 4 -1 21 -5.70 6.70 4 -1 21 -3.20 3.70 -4 -1 -21 1.40 5.90 4 1 21 -6.40 5.90 4 1 21 3.70 5.10 -4 1 -21 2.40 7.50 -5 -1 -21 17.90 9.70 5 -1 21 5.10 8.00 5 -1 21 9.40 5.40 -5 1 -21 5.00 7.60 -5 1 -21 8.00 8.30 5 1 21 2.90 7.10 -6 -1 -21 9.60 8.40 6 -1 21 9.00 8.20 -6 -1 -21 3.80 6.10 6 -1 21 6.80 6.00 6 1 21 1.80 7.60 -6 1 -21 6.30 7.90 6 1 21 -10.20 4.70 -6 1 -21 -15.40 4.40 -7 -1 -21 32.20 11.40 7 -1 21 22.50 8.20 7 -1 21 2.60 8.50 -7 -1 -21 14.70 8.80 -7 1 -21 16.80 10.10 -7 1 -21 18.30 10.40 7 1 21 30.40 10.00 7 1 21 33.40 12.50 -8 -1 -21 9.60 10.70 8 -1 21 -3.10 9.00 8 -1 21 8.50 7.40 -8 1 -21 3.40 8.50 8 1 21 7.50 7.90 -8 1 -21 -9.30 8.90 8 1 21 -5.10 7.40 -9 -1 -21 4.80 10.10 9 -1 21 5.40 8.70 -9 -1 -21 18.10 12.40 -9 1 -21 -8.80 9.50 9 1 21 24.20 11.10 -9 1 -21 7.20 11.20 9 1 21 5.20 9.60 11 -2 -21 131.19 14.20 -11 2 21 105.89 16.20 11 2 -21 125.69 13.60 -11 2 21 155.88 22.40 -10 -2 21 3.60 5.90 10 -2 -21 -4.70 5.20 -10 -2 21 15.80 8.10 10 2 -21 3.00 5.20 -10 2 21 -10.20 4.90 -10 2 21 -9.10 6.10 -9 -2 21 16.40 7.50 -9 -2 21 19.60 7.90 9 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311.17 23.20 -1 2 21 271.57 24.90 0 -2 21 7.80 7.30 0 -2 -21 11.60 7.20 0 2 -21 6.30 6.00 0 2 21 22.50 8.50 1 -2 21 309.67 26.60 -1 -2 -21 264.37 23.70 -1 2 -21 265.97 23.30 1 2 21 331.07 27.60 1 2 21 280.57 16.10 -2 -2 -21 12.00 7.80 2 -2 21 10.60 8.60 2 2 21 9.90 3.60 2 2 21 6.50 8.60 -2 2 -21 18.70 8.00 2 2 21 5.80 4.10 -3 -2 -21 43.90 11.10 3 -2 21 63.59 14.30 -3 2 -21 23.60 9.90 3 2 21 48.20 8.30 3 2 21 30.80 11.60 4 -2 21 6.90 7.60 -4 -2 -21 6.30 6.00 4 -2 21 9.50 4.20 4 2 21 0.20 7.90 4 2 21 8.10 5.90 -4 2 -21 12.00 6.50 -4 2 -21 3.40 5.70 5 -2 21 20.60 10.40 -5 -2 -21 3.20 6.70 5 -2 21 -1.40 4.60 -5 2 -21 9.10 8.00 -5 2 -21 11.00 7.40 5 2 21 1.50 5.60 5 2 21 10.20 7.30 -6 -2 -21 -12.50 5.40 -6 -2 -21 2.40 7.90 6 -2 21 -2.40 5.00 6 -2 21 -5.00 8.90 6 2 21 7.10 6.60 -6 2 -21 3.80 6.50 6 2 21 2.00 6.20 -6 2 -21 -6.80 6.60 -7 -2 -21 7.40 9.00 -7 -2 -21 2.50 9.20 7 -2 21 1.10 6.00 7 -2 21 6.80 9.40 7 2 21 28.10 8.70 -7 2 -21 20.40 10.50 7 2 21 -8.10 7.30 -7 2 -21 4.80 7.50 8 -2 21 17.70 11.10 -8 -2 -21 -8.00 8.00 8 -2 21 1.90 6.20 -8 2 -21 -2.60 7.70 -8 2 -21 2.20 8.40 8 2 21 13.50 9.50 8 2 21 -4.50 8.20 9 -2 21 13.80 8.40 -9 -2 -21 16.30 11.80 -9 -2 -21 18.00 12.20 -9 2 -21 5.40 11.00 -9 2 -21 1.40 8.90 9 2 21 7.90 9.50 9 2 21 23.30 11.50 -11 -3 21 2.10 7.50 11 -3 -21 20.50 7.60 -11 -3 21 -8.90 5.00 -11 3 21 -8.10 7.70 -11 3 21 5.50 8.20 -11 3 21 13.80 8.70 -10 -3 21 -2.00 7.30 -10 -3 21 -3.40 3.80 10 -3 -21 8.80 5.90 -10 3 21 -1.80 7.60 -10 3 21 8.20 7.40 -10 3 21 3.70 6.40 10 3 -21 4.50 4.70 9 -3 -21 28.90 6.70 -9 -3 21 13.60 7.90 -9 -3 21 22.30 6.30 -9 3 21 9.80 8.10 -9 3 21 32.00 9.20 -9 3 21 20.90 10.20 9 3 -21 31.30 6.00 8 -3 -21 4.40 4.40 -8 -3 21 -4.90 3.80 -8 -3 21 6.40 5.90 -8 -3 21 -0.30 6.80 -8 3 21 -0.30 6.10 8 3 -21 -0.20 2.70 -8 3 21 -5.00 4.60 -8 3 21 -3.10 5.00 7 -3 -21 35.80 7.00 -7 -3 21 27.50 8.50 -7 -3 21 23.10 5.40 -7 -3 21 35.80 9.20 7 3 -21 32.10 4.70 -7 3 21 19.70 7.50 -7 3 21 40.20 10.00 -7 3 21 20.80 9.10 -6 -3 21 3.50 5.30 6 -3 -21 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11.50 -9 -4 21 69.99 13.40 9 4 -21 62.19 8.30 -9 4 21 71.49 15.90 -9 4 21 71.89 13.00 -9 4 21 48.20 10.70 -8 -4 21 4.90 3.50 -8 -4 21 7.00 6.90 8 -4 -21 5.50 4.60 -8 4 21 4.50 6.40 8 4 -21 5.60 4.70 -8 4 21 2.60 7.50 8 4 -21 7.50 3.20 -8 4 21 -1.60 6.40 -7 -4 21 18.20 7.60 -7 -4 21 21.40 7.00 7 -4 -21 27.60 6.50 7 4 -21 22.60 6.70 -7 4 21 39.80 10.40 -7 4 21 22.60 8.40 -7 4 21 18.60 7.20 7 4 -21 25.20 3.80 6 -4 -21 8.00 4.70 -6 -4 21 -0.60 5.60 -6 4 21 1.00 5.60 -6 4 21 6.60 6.00 -5 -4 21 81.89 15.00 5 4 -21 81.19 11.50 5 4 -21 90.69 5.70 5 4 -21 104.39 13.60 -5 4 21 90.19 14.90 -5 4 21 111.79 14.60 -4 -4 21 8.20 7.00 -4 4 21 -3.00 3.70 4 4 -21 1.30 2.00 4 4 -21 -2.70 4.00 -4 4 21 5.80 5.70 -3 -4 21 4.50 6.90 3 4 -21 3.90 4.70 3 4 -21 11.50 3.80 -3 4 21 11.00 6.00 -3 4 21 5.60 7.10 2 -4 -21 1.40 5.20 -2 -4 21 3.10 7.10 -2 4 21 0.30 7.40 2 4 -21 4.40 3.20 2 4 -21 7.40 4.20 -1 -4 21 30.10 10.20 1 -4 -21 12.70 6.00 -1 4 21 9.20 8.00 1 4 -21 18.00 7.20 0 -4 -21 40.00 9.30 0 -4 21 21.00 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21 81.49 15.90 3 5 -21 65.49 6.50 3 5 -21 64.29 6.20 -3 5 21 75.99 12.70 3 5 -21 46.10 9.50 -2 -5 21 144.39 20.00 2 -5 -21 128.69 16.60 2 5 -21 114.79 15.20 -2 5 21 86.39 17.20 -1 -5 21 222.98 22.80 1 -5 -21 258.47 21.40 -1 5 21 223.68 14.00 1 5 -21 212.88 22.10 1 5 -21 205.98 14.60 -1 5 21 211.28 22.40 0 -5 -21 107.39 16.10 0 -5 21 49.99 12.40 0 5 21 76.09 9.50 0 5 21 75.49 8.00 0 5 21 76.29 15.30 0 5 -21 96.59 14.50 -1 -5 -21 -2.90 6.10 1 -5 21 -4.80 4.50 1 5 21 2.40 6.00 1 5 21 -1.90 4.80 -1 5 -21 6.00 6.60 1 5 21 6.90 4.60 -2 -5 -21 74.89 13.20 2 -5 21 58.69 13.90 2 5 21 56.19 10.40 2 5 21 54.49 13.40 -2 5 -21 42.30 8.90 -2 5 -21 66.09 14.10 3 -5 21 13.10 7.30 -3 -5 -21 9.00 6.00 -3 5 -21 23.70 7.30 3 5 21 5.10 7.00 -3 5 -21 21.70 8.90 4 -5 21 10.90 11.20 -4 -5 -21 25.70 9.70 -4 5 -21 1.30 7.50 -4 5 -21 22.50 8.00 4 5 21 16.50 8.90 4 5 21 16.50 8.30 5 -5 21 7.90 9.50 5 -5 21 -1.60 3.30 -5 -5 -21 -2.90 7.40 -5 5 -21 8.00 7.30 -5 5 -21 29.70 10.10 5 5 21 8.40 8.30 5 5 21 6.80 8.00 6 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33.80 12.30 2 6 21 34.40 9.20 -3 -6 -21 -2.80 5.60 3 -6 21 9.90 8.60 -3 6 -21 -0.70 4.50 -3 6 -21 1.60 5.10 3 6 21 7.10 7.70 3 6 21 10.00 6.80 -4 -6 -21 -0.40 4.50 4 6 21 -0.30 8.00 -4 6 -21 -5.10 5.20 -4 6 -21 1.20 6.00 -4 6 -21 -3.30 5.00 4 6 21 -3.30 6.60 -5 -6 -21 14.30 9.30 5 -6 21 10.10 4.40 -5 6 -21 10.30 8.50 -5 6 -21 7.20 7.10 -5 6 -21 19.20 7.30 5 6 21 13.80 7.90 5 6 21 17.50 9.50 -6 -6 -21 5.20 8.50 6 -6 21 8.80 5.40 -6 6 -21 9.90 7.70 -6 6 -21 2.40 5.80 -6 6 -21 -8.70 9.80 6 6 21 -3.80 7.00 6 6 21 5.90 10.00 -7 -6 -21 -2.20 8.90 7 -6 21 4.30 5.90 -7 -6 -21 7.00 11.50 -7 6 -21 2.80 7.00 7 6 21 13.50 9.80 7 6 21 10.00 8.30 -7 6 -21 14.50 12.00 -7 6 -21 -2.00 7.60 -8 -6 -21 38.90 11.80 8 -6 21 23.20 8.50 -8 -6 -21 -9.40 9.40 -8 6 -21 18.50 10.10 8 6 21 28.20 11.80 -8 6 -21 15.60 9.90 8 6 21 4.00 9.00 -8 6 -21 10.10 13.30 -10 -7 21 89.49 13.30 10 -7 -21 65.09 12.80 -10 7 21 103.89 17.10 -10 7 21 61.19 14.10 10 7 -21 70.19 10.40 -10 7 21 47.10 14.30 -9 -7 21 4.90 7.50 9 -7 -21 1.50 5.80 -9 7 21 4.80 9.20 -9 7 21 11.00 9.10 -9 7 21 -4.20 6.50 9 7 -21 1.70 5.10 -8 -7 21 0.70 5.70 8 -7 -21 13.30 6.80 -8 7 21 -1.70 7.30 -8 7 21 0.10 7.10 -8 7 21 1.00 8.30 8 7 -21 3.70 4.80 7 -7 -21 19.30 6.80 -7 -7 21 10.30 5.70 -7 7 21 19.10 8.40 7 7 -21 7.30 5.40 -7 7 21 14.30 9.90 -6 7 21 46.00 10.80 6 7 -21 21.00 3.40 6 7 -21 12.40 5.10 -6 7 21 22.30 10.00 -5 7 21 48.00 13.20 5 7 -21 58.59 4.80 -5 7 21 70.49 13.20 5 7 -21 61.29 9.90 -4 7 21 48.20 11.00 4 7 -21 61.79 5.50 -4 7 21 44.70 13.00 4 7 -21 54.49 9.90 3 7 -21 28.90 6.90 -3 7 21 55.69 11.60 3 7 -21 31.20 8.60 -3 7 21 35.60 6.00 -3 7 21 50.89 14.00 -3 7 21 45.50 6.60 -2 7 21 75.59 9.60 -2 7 21 61.49 11.50 2 7 -21 63.79 11.40 -2 7 21 63.59 14.20 -2 7 21 54.19 11.80 1 -7 -21 10.10 7.40 -1 7 21 8.10 5.70 1 7 -21 4.00 5.10 -1 7 21 1.00 8.60 1 7 -21 9.50 3.30 -1 7 21 9.50 6.10 1 7 -21 -1.30 2.20 0 -7 -21 22.90 9.00 0 7 -21 29.10 6.30 0 7 -21 22.50 4.60 0 7 21 30.00 10.40 0 7 -21 38.40 9.60 0 7 21 25.40 7.90 -1 -7 -21 1.70 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11.30 -7 -5 22 34.20 8.20 -7 5 22 42.20 10.40 7 5 -22 47.50 8.90 -7 5 22 33.20 10.30 -6 -5 22 1.30 6.90 6 -5 -22 2.90 4.20 -6 5 22 4.20 6.10 6 5 -22 0.80 5.00 -6 5 22 1.50 6.90 -5 -5 22 -6.50 6.10 5 5 -22 5.50 5.30 -5 5 22 23.10 8.20 -5 5 22 4.80 7.50 -4 -5 22 22.70 9.10 -4 5 22 7.90 6.70 4 5 -22 13.90 6.50 4 5 -22 19.00 3.00 -4 5 22 19.70 10.20 4 5 -22 16.20 3.30 -3 -5 22 21.60 9.00 -3 5 22 24.60 9.70 -3 5 22 13.30 7.40 3 5 -22 9.50 6.10 3 5 -22 10.20 3.70 3 5 -22 13.70 3.70 2 -5 -22 28.30 8.20 -2 -5 22 44.30 13.00 -2 5 22 67.59 14.10 2 5 -22 60.49 11.00 2 5 -22 33.50 5.50 1 -5 -22 2.20 5.50 -1 -5 22 9.70 7.90 -1 5 22 5.20 1.90 -1 5 22 0.70 6.10 1 5 -22 7.80 6.10 0 -5 -22 148.09 18.30 0 -5 22 102.19 18.60 0 5 22 121.99 19.70 0 5 22 126.19 10.20 0 5 22 125.19 10.40 0 5 -22 126.89 17.20 -1 -5 -22 13.30 6.90 1 -5 22 20.80 9.90 -1 5 -22 7.10 7.60 1 5 22 13.70 5.50 1 5 22 30.70 11.30 1 5 22 24.60 6.30 -2 -5 -22 107.69 16.20 2 -5 22 90.29 17.50 -2 5 -22 120.09 15.40 2 5 22 116.49 12.50 2 5 22 112.99 19.80 -2 5 -22 136.49 19.40 3 -5 22 -2.60 5.80 -3 -5 -22 -4.70 5.60 -3 5 -22 7.10 7.20 3 5 22 -9.30 6.10 -3 5 -22 -5.00 5.00 4 -5 22 8.70 9.10 -4 -5 -22 -3.60 6.70 4 5 22 5.50 6.90 4 5 22 0.50 7.90 -4 5 -22 -1.20 6.60 -4 5 -22 2.80 5.80 5 -5 22 -16.10 6.30 -5 -5 -22 -4.40 6.30 5 -5 22 0.60 3.30 -5 5 -22 2.30 6.60 -5 5 -22 7.50 9.10 5 5 22 5.30 8.80 5 5 22 5.60 7.60 -6 -5 -22 -4.80 6.60 6 -5 22 1.40 5.20 -6 5 -22 1.70 6.40 -6 5 -22 -13.40 6.40 -6 5 -22 7.00 10.50 6 5 22 6.80 8.00 6 5 22 -9.20 8.10 -7 -5 -22 4.80 10.70 7 -5 22 7.50 5.70 7 5 22 2.20 11.20 7 5 22 12.20 10.40 -7 5 -22 2.80 8.90 -7 5 -22 17.60 10.20 -7 5 -22 12.30 8.80 -8 -5 -22 2.70 10.10 8 -5 22 6.40 6.90 -8 -5 -22 0.40 9.90 -8 5 -22 14.40 11.20 -8 5 -22 0.30 9.70 8 5 22 -3.80 8.60 -8 5 -22 -4.00 8.30 9 -6 -22 16.50 7.40 -9 -6 22 24.90 8.50 -9 6 22 38.00 10.60 -9 6 22 35.90 10.50 -9 6 22 31.90 11.30 9 6 -22 33.50 7.80 8 -6 -22 21.40 6.90 -8 -6 22 11.80 7.60 -8 6 22 31.60 8.70 8 6 -22 12.80 6.00 -8 6 22 26.30 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4 23 26.00 9.50 -9 4 23 58.79 13.00 -8 -4 23 0.00 5.80 8 -4 -23 -0.60 5.30 -8 4 23 -6.60 5.50 8 4 -23 8.80 5.70 -8 4 23 13.00 6.50 -8 4 23 -1.50 7.70 -7 -4 23 3.20 6.50 7 -4 -23 6.80 5.00 -7 4 23 -8.40 5.90 -7 4 23 -1.50 5.30 7 4 -23 10.50 6.70 -6 -4 23 29.70 9.40 6 4 -23 34.30 8.40 -6 4 23 43.10 10.00 -6 4 23 59.99 13.60 -5 -4 23 38.80 11.70 5 4 -23 32.80 7.90 -5 4 23 24.90 8.80 -5 4 23 29.70 11.80 -4 -4 23 8.50 7.70 -4 4 23 0.70 7.30 -4 4 23 -3.80 4.30 4 4 -23 -0.80 3.80 4 4 -23 6.90 5.10 4 4 -23 -6.70 2.70 3 -4 -23 -0.10 5.30 -3 -4 23 1.70 7.10 -3 4 23 0.20 6.80 3 4 -23 7.00 6.30 3 4 -23 -1.60 5.00 2 -4 -23 2.80 5.60 -2 -4 23 -0.30 7.10 2 4 -23 15.30 6.20 -2 4 23 3.30 5.20 -1 -4 23 52.69 12.40 1 -4 -23 36.00 10.20 1 4 -23 55.79 12.20 -1 4 23 52.39 13.30 0 -4 23 39.20 12.50 0 -4 -23 41.90 10.40 0 4 23 44.60 13.40 0 4 -23 36.10 10.10 1 -4 23 -0.10 5.00 -1 -4 -23 4.90 6.60 -1 4 -23 3.60 6.20 1 4 23 3.70 3.10 1 4 23 -2.10 3.30 1 4 23 6.20 8.00 -2 -4 -23 58.49 13.10 2 -4 23 67.19 15.00 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-28 2.10 9.10 0 -6 -28 3.30 10.40 0 -6 28 37.60 13.70 0 6 28 24.90 11.40 0 6 -28 21.40 10.00 -1 -6 -28 3.10 7.10 1 -6 28 5.30 12.10 1 6 28 1.50 9.80 -1 6 -28 2.50 6.60 2 -6 28 -14.80 9.30 -2 -6 -28 13.60 9.00 2 6 28 7.60 12.40 -2 6 -28 -17.50 6.10 4 -7 -28 19.20 11.00 4 7 -28 19.80 9.10 -4 7 28 11.40 10.90 3 -7 -28 7.60 9.60 -3 7 28 11.10 12.90 3 7 -28 -4.40 6.00 2 -7 -28 9.30 9.00 -2 7 28 15.10 11.50 2 7 -28 8.70 8.80 1 -7 -28 36.40 12.40 1 7 -28 28.30 11.30 -1 7 28 25.40 13.10 0 -7 -28 17.70 9.10 0 7 -28 -2.40 7.40 0 7 28 -4.40 8.70 -1 -7 -28 14.80 9.40 -1 7 -28 -7.90 6.10 1 7 28 -12.60 9.30 1 -8 -28 28.10 11.20 -1 8 28 21.80 11.10 1 8 -28 25.20 9.90 5 0 -29 -1.70 7.10 -5 0 29 1.00 7.80 -4 0 29 18.10 9.70 4 0 -29 -1.20 7.20 3 0 -29 -3.70 7.00 -3 0 29 21.10 10.10 2 0 -29 8.20 7.20 1 0 -29 -9.50 6.60 -1 0 29 -0.80 8.60 0 0 -29 -0.50 8.40 0 0 29 -2.00 5.60 1 0 29 -2.30 6.60 -1 0 -29 8.60 8.00 -2 0 -29 3.70 9.10 2 0 29 -11.10 8.60 3 0 29 20.30 12.50 -3 0 -29 -14.20 8.80 5 -1 -29 -2.60 8.00 -5 -1 29 15.40 10.00 -5 1 29 16.20 11.00 5 1 -29 8.90 8.90 4 -1 -29 10.30 9.20 -4 -1 29 9.50 8.40 -4 1 29 -4.80 10.90 -3 -1 29 -1.90 10.20 3 -1 -29 24.50 8.90 2 -1 -29 -2.20 7.40 -2 1 29 11.60 9.60 1 -1 -29 -0.90 8.30 -1 -1 29 5.80 9.80 1 1 -29 3.80 9.70 -1 1 29 -5.60 7.80 0 -1 29 0.40 8.60 0 -1 -29 -4.50 7.00 0 1 -29 -9.40 6.70 0 1 29 3.50 7.20 1 -1 29 6.70 10.10 -1 -1 -29 -0.60 6.90 -1 1 -29 -12.10 7.50 1 1 29 -6.50 6.40 2 -1 29 8.20 10.00 -2 -1 -29 -12.10 5.40 2 1 29 4.50 9.90 -2 1 -29 -1.50 7.30 3 -1 29 20.80 11.50 -3 -1 -29 2.40 9.00 -3 1 -29 6.10 8.90 3 1 29 0.50 8.00 5 -2 -29 15.30 9.40 -5 -2 29 20.60 11.60 4 -2 -29 5.50 7.30 -4 -2 29 5.90 10.90 4 2 -29 -10.70 6.40 3 -2 -29 30.10 11.80 3 2 -29 23.60 8.90 -3 2 29 11.80 10.60 2 -2 -29 0.00 7.60 -2 2 29 1.10 9.20 2 2 -29 -5.60 7.10 -1 -2 29 1.00 8.80 1 -2 -29 -1.20 7.20 -1 2 29 -15.50 7.60 0 -2 -29 -1.70 6.70 0 -2 29 19.50 11.40 0 2 29 -0.90 6.80 0 2 -29 9.70 8.70 1 -2 29 -8.10 9.00 -1 -2 -29 -11.00 7.20 1 2 29 6.30 10.40 -1 2 -29 -2.70 7.10 -2 -2 -29 10.60 11.40 2 -2 29 -1.10 10.20 -2 2 -29 -0.30 8.90 2 2 29 -11.60 9.20 -3 -2 -29 34.70 14.20 3 -2 29 3.00 11.50 -3 2 -29 7.00 10.30 3 2 29 19.50 13.30 5 -3 -29 59.29 14.60 -5 -3 29 81.09 18.50 -5 3 29 53.29 15.00 5 3 -29 65.39 14.40 4 -3 -29 -0.60 5.30 -4 -3 29 6.60 10.10 -4 3 29 3.40 9.10 4 3 -29 5.40 8.80 3 -3 -29 -2.50 8.00 3 3 -29 -2.90 7.20 -3 3 29 8.30 9.40 -2 -3 29 6.00 9.30 2 -3 -29 -3.40 7.10 2 3 -29 -7.20 7.70 -2 3 29 0.10 9.70 1 -3 -29 -2.80 8.60 -1 -3 29 13.40 10.00 -1 3 29 -1.70 9.00 0 -3 -29 13.10 11.00 0 -3 29 30.40 13.50 0 3 -29 28.20 11.10 0 3 29 6.80 9.60 -1 -3 -29 8.10 8.70 1 -3 29 -3.60 9.80 1 3 29 8.60 9.90 -1 3 -29 -6.10 7.70 2 -3 29 -4.90 11.10 -2 3 -29 23.30 11.20 2 3 29 30.70 13.90 3 -3 29 5.10 11.40 -3 -3 -29 23.70 11.50 3 3 29 15.60 14.00 -3 3 -29 1.70 10.00 -3 3 -29 13.60 9.00 4 -4 -29 -0.10 8.70 -4 -4 29 13.60 10.90 -4 4 29 5.00 9.10 4 4 -29 0.00 6.40 3 -4 -29 22.00 11.10 -3 4 29 35.10 12.40 3 4 -29 12.70 9.10 2 -4 -29 9.10 6.50 -2 -4 29 -6.70 8.90 2 4 -29 -9.30 6.00 -2 4 29 18.20 10.40 -1 -4 29 -1.10 9.40 1 -4 -29 -5.10 7.40 1 4 -29 0.80 7.70 -1 4 29 -8.00 9.30 0 -4 29 25.30 11.70 0 -4 -29 14.60 9.40 0 4 29 28.30 13.80 0 4 -29 21.00 10.30 -1 -4 -29 11.40 10.40 1 -4 29 15.90 10.50 -1 4 -29 -0.20 9.10 1 4 29 12.40 10.10 2 -4 29 -6.40 9.50 -2 -4 -29 4.70 7.70 -2 4 -29 -9.40 8.60 2 4 29 14.40 10.50 -2 4 -29 -11.80 6.50 4 -5 -29 10.90 10.00 4 5 -29 24.60 9.50 -4 5 29 48.90 12.50 -3 -5 29 1.80 10.20 3 -5 -29 9.30 9.10 3 5 -29 -2.60 6.10 -3 5 29 15.00 10.20 2 -5 -29 -2.10 10.00 -2 -5 29 -3.10 7.70 -2 5 29 -2.50 10.10 2 5 -29 3.80 7.90 -1 -5 29 43.60 14.70 1 -5 -29 46.90 13.30 -1 5 29 27.10 12.90 1 5 -29 27.80 10.00 0 -5 -29 -2.30 5.10 0 -5 29 5.40 11.10 0 5 -29 11.80 9.50 0 5 29 10.80 9.80 1 -5 29 9.80 12.10 -1 -5 -29 4.30 9.30 1 5 29 4.00 9.80 -1 5 -29 7.50 8.40 2 -6 -29 -6.60 6.10 -2 -6 29 -5.80 9.50 2 6 -29 11.70 8.30 -2 6 29 6.00 9.50 1 -6 -29 20.70 10.70 -1 -6 29 14.50 12.50 -1 6 29 42.20 15.60 1 6 -29 1.10 7.70 0 -6 -29 44.10 13.00 0 -6 29 22.80 14.40 0 6 -29 29.50 12.10 0 6 29 36.80 14.60 4 0 -30 148.19 21.50 -4 0 30 152.28 24.70 -3 0 30 3.40 9.00 3 0 -30 -8.00 7.80 2 0 -30 19.30 8.60 -2 0 30 18.20 11.10 1 0 -30 -15.10 6.50 -1 0 30 10.20 11.00 0 0 30 0.40 10.10 0 0 -30 -4.60 7.60 1 0 30 13.40 9.50 -1 0 -30 10.20 10.90 -4 -1 30 11.50 9.80 4 -1 -30 7.70 10.00 -4 1 30 -5.00 10.20 4 1 -30 8.00 7.80 -3 -1 30 -7.50 9.00 3 -1 -30 -1.30 7.40 3 1 -30 3.10 7.60 -3 1 30 -2.20 9.60 2 -1 -30 1.00 5.80 -2 -1 30 23.80 11.70 2 1 -30 6.20 8.40 -2 1 30 4.10 10.00 -1 -1 30 -3.10 8.00 1 -1 -30 -7.90 7.80 1 1 -30 -9.20 7.30 -1 1 30 -21.90 7.10 0 -1 30 33.20 14.00 0 -1 -30 21.90 11.60 0 1 30 41.70 15.00 0 1 -30 20.50 11.00 1 -1 30 10.60 8.20 -1 -1 -30 4.40 9.00 -1 1 -30 -2.00 8.70 1 1 30 4.90 12.00 4 -2 -30 -6.50 7.20 -4 -2 30 -6.90 8.90 4 2 -30 5.80 7.50 -4 2 30 19.60 11.90 3 -2 -30 -4.70 8.00 -3 -2 30 3.70 8.10 3 2 -30 -0.30 7.00 -3 2 30 -2.40 9.50 -2 -2 30 7.40 9.60 2 -2 -30 -3.60 8.60 -2 2 30 8.60 11.30 2 2 -30 18.90 9.90 -1 -2 30 14.10 11.90 1 -2 -30 4.10 9.00 -1 2 30 3.30 11.50 1 2 -30 21.90 11.20 0 -2 30 66.59 17.70 0 -2 -30 60.39 16.30 0 2 30 55.59 18.00 0 2 -30 73.19 17.30 -1 -2 -30 3.00 10.20 1 -2 30 -1.80 10.30 1 2 30 4.80 10.40 -1 2 -30 8.70 9.80 3 -3 -30 0.60 9.50 -3 -3 30 9.70 11.40 3 3 -30 -3.10 8.00 -3 3 30 -0.70 9.40 -2 -3 30 37.40 14.30 2 -3 -30 -2.30 7.80 2 3 -30 24.30 9.70 -2 3 30 13.20 11.40 1 -3 -30 -2.50 7.90 -1 -3 30 2.60 10.40 -1 3 30 12.40 10.30 1 3 -30 1.30 8.50 0 -3 -30 41.50 13.70 0 -3 30 41.50 15.20 0 3 30 81.09 18.40 0 3 -30 38.90 13.80 -1 -3 -30 8.60 10.90 1 -3 30 -4.70 10.90 1 3 30 2.70 11.10 -1 3 -30 6.10 10.10 -2 -4 30 8.40 10.00 2 -4 -30 -1.90 8.50 -2 4 30 1.30 9.30 2 4 -30 1.90 9.10 -1 -4 30 11.90 11.60 1 -4 -30 6.00 10.30 -1 4 30 26.90 11.80 1 4 -30 9.60 9.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 11274 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1A O 1.14588(12) 0.60168(11) 0.66235(6) 0.0618(4) Uani 1 1 d . . . . . N1A N 0.81637(12) 0.60107(10) 0.78521(6) 0.0409(3) Uani 1 1 d . . . . . N2A N 0.68473(14) 0.65646(13) 0.85553(7) 0.0546(4) Uani 1 1 d . . . . . C1A C 0.91932(15) 0.57144(13) 0.82566(8) 0.0409(4) Uani 1 1 d . . . . . C2A C 0.92270(18) 0.54611(15) 0.88564(8) 0.0537(5) Uani 1 1 d . . . . . H2A H 0.850904 0.550507 0.906789 0.064 Uiso 1 1 calc R U . . . C3A C 1.0370(2) 0.51406(18) 0.91273(9) 0.0667(6) Uani 1 1 d . . . . . H3A H 1.041784 0.496843 0.953023 0.080 Uiso 1 1 calc R U . . . C4A C 1.14502(19) 0.50667(17) 0.88182(9) 0.0622(6) Uani 1 1 d . . . . . H4A H 1.220229 0.484395 0.901550 0.075 Uiso 1 1 calc R U . . . C5A C 1.14185(16) 0.53187(14) 0.82254(8) 0.0487(5) Uani 1 1 d . . . . . H5A H 1.214375 0.526943 0.801944 0.058 Uiso 1 1 calc R U . . . C6A C 1.02895(15) 0.56486(12) 0.79362(8) 0.0396(4) Uani 1 1 d . . . . . C7A C 0.98865(15) 0.59222(12) 0.73324(8) 0.0393(4) Uani 1 1 d . . . . . C8A C 0.86228(15) 0.61184(12) 0.72981(7) 0.0396(4) Uani 1 1 d . . . . . C9A C 0.80671(16) 0.64152(15) 0.66935(8) 0.0482(5) Uani 1 1 d . . . . . H9AA H 0.773855 0.705785 0.669996 0.058 Uiso 1 1 calc R U . . . H9AB H 0.739216 0.598936 0.654300 0.058 Uiso 1 1 calc R U . . . C10A C 0.92305(16) 0.63499(13) 0.63088(8) 0.0434(4) Uani 1 1 d . . . . . C11A C 1.03628(16) 0.60783(13) 0.67572(8) 0.0429(4) Uani 1 1 d . . . . . C12A C 0.94995(18) 0.72874(15) 0.59970(9) 0.0537(5) Uani 1 1 d . . . . . H12A H 0.951178 0.779820 0.628849 0.064 Uiso 1 1 calc R U . . . H12B H 1.033312 0.725524 0.584741 0.064 Uiso 1 1 calc R U . . . C13A C 0.8519(2) 0.75131(17) 0.54778(10) 0.0664(6) Uani 1 1 d . . . . . H13A H 0.770417 0.763179 0.563285 0.080 Uiso 1 1 calc R U . . . H13B H 0.876973 0.808487 0.527693 0.080 Uiso 1 1 calc R U . . . C14A C 0.8385(3) 0.6702(2) 0.50278(10) 0.0796(7) Uani 1 1 d . . . . . H14A H 0.772130 0.685260 0.471555 0.095 Uiso 1 1 calc R U . . . H14B H 0.917419 0.662714 0.484085 0.095 Uiso 1 1 calc R U . . . C15A C 0.8065(2) 0.57824(18) 0.53306(10) 0.0710(6) Uani 1 1 d . . . . . H15A H 0.802489 0.527100 0.503891 0.085 Uiso 1 1 calc R U . . . H15B H 0.723838 0.583748 0.548526 0.085 Uiso 1 1 calc R U . . . C16A C 0.90571(19) 0.55502(15) 0.58422(9) 0.0563(5) Uani 1 1 d . . . . . H16A H 0.986303 0.543013 0.567889 0.068 Uiso 1 1 calc R U . . . H16B H 0.880901 0.497426 0.603944 0.068 Uiso 1 1 calc R U . . . C17A C 0.69131(15) 0.62155(12) 0.80058(8) 0.0412(4) Uani 1 1 d . . . . . C18A C 0.58747(16) 0.60482(13) 0.76088(9) 0.0482(5) Uani 1 1 d . . . . . H18A H 0.596707 0.580852 0.722728 0.058 Uiso 1 1 calc R U . . . C19A C 0.46866(17) 0.62461(14) 0.77921(10) 0.0556(5) Uani 1 1 d . . . . . H19A H 0.396262 0.614792 0.753278 0.067 Uiso 1 1 calc R U . . . C20A C 0.45866(18) 0.65885(14) 0.83598(10) 0.0576(6) Uani 1 1 d . . . . . H20A H 0.379677 0.671345 0.849639 0.069 Uiso 1 1 calc R U . . . C21A C 0.56780(19) 0.67413(16) 0.87199(10) 0.0609(6) Uani 1 1 d . . . . . H21A H 0.560681 0.698278 0.910276 0.073 Uiso 1 1 calc R U . . . O1B O 0.64123(11) 0.85409(11) 0.66069(6) 0.0618(4) Uani 1 1 d . . . . . N1B N 0.30935(12) 0.85564(10) 0.78210(6) 0.0363(3) Uani 1 1 d . . . . . N2B N 0.17545(13) 0.80015(11) 0.85163(6) 0.0457(4) Uani 1 1 d . . . . . C1B C 0.41132(15) 0.88602(12) 0.82262(7) 0.0360(4) Uani 1 1 d . . . . . C2B C 0.41331(17) 0.91050(13) 0.88282(8) 0.0457(4) Uani 1 1 d . . . . . H2B H 0.341359 0.904718 0.903751 0.055 Uiso 1 1 calc R U . . . C3B C 0.52673(18) 0.94383(15) 0.91037(8) 0.0547(5) Uani 1 1 d . . . . . H3B H 0.530811 0.960598 0.950730 0.066 Uiso 1 1 calc R U . . . C4B C 0.63479(18) 0.95304(15) 0.87961(9) 0.0542(5) Uani 1 1 d . . . . . H4B H 0.709170 0.976408 0.899538 0.065 Uiso 1 1 calc R U . . . C5B C 0.63325(16) 0.92814(13) 0.82026(8) 0.0450(4) Uani 1 1 d . . . . . H5B H 0.705914 0.934238 0.799880 0.054 Uiso 1 1 calc R U . . . C6B C 0.52103(15) 0.89356(12) 0.79102(7) 0.0368(4) Uani 1 1 d . . . . . C7B C 0.48218(14) 0.86577(12) 0.73057(7) 0.0371(4) Uani 1 1 d . . . . . C8B C 0.35606(14) 0.84521(12) 0.72679(7) 0.0363(4) Uani 1 1 d . . . . . C9B C 0.30137(16) 0.81481(15) 0.66640(7) 0.0466(4) Uani 1 1 d . . . . . H9BA H 0.234134 0.857284 0.650898 0.056 Uiso 1 1 calc R U . . . H9BB H 0.268418 0.750599 0.667267 0.056 Uiso 1 1 calc R U . . . C10B C 0.41858(15) 0.82074(13) 0.62837(7) 0.0421(4) Uani 1 1 d . . . . . C11B C 0.53140(15) 0.84861(13) 0.67342(8) 0.0420(4) Uani 1 1 d . . . . . C12B C 0.4016(2) 0.89861(16) 0.58095(9) 0.0620(6) Uani 1 1 d . . . . . H12C H 0.376025 0.956786 0.599747 0.074 Uiso 1 1 calc R U . . . H12D H 0.482446 0.910276 0.564734 0.074 Uiso 1 1 calc R U . . . C13B C 0.3034(2) 0.8731(2) 0.52991(10) 0.0828(8) Uani 1 1 d . . . . . H13C H 0.300604 0.922490 0.499596 0.099 Uiso 1 1 calc R U . . . H13D H 0.220230 0.869286 0.545062 0.099 Uiso 1 1 calc R U . . . C14B C 0.3348(2) 0.7785(2) 0.50168(10) 0.0899(9) Uani 1 1 d . . . . . H14C H 0.268170 0.762225 0.470822 0.108 Uiso 1 1 calc R U . . . H14D H 0.413611 0.784464 0.482770 0.108 Uiso 1 1 calc R U . . . C15B C 0.3476(2) 0.69995(18) 0.54811(10) 0.0694(7) Uani 1 1 d . . . . . H15C H 0.372446 0.641599 0.529242 0.083 Uiso 1 1 calc R U . . . H15D H 0.266261 0.689322 0.563996 0.083 Uiso 1 1 calc R U . . . C16B C 0.44586(18) 0.72533(15) 0.59906(9) 0.0526(5) Uani 1 1 d . . . . . H16C H 0.528939 0.727940 0.583760 0.063 Uiso 1 1 calc R U . . . H16D H 0.447909 0.675800 0.629278 0.063 Uiso 1 1 calc R U . . . C17B C 0.18364(14) 0.83577(12) 0.79704(7) 0.0360(4) Uani 1 1 d . . . . . C18B C 0.08064(15) 0.85501(13) 0.75695(8) 0.0428(4) Uani 1 1 d . . . . . H18B H 0.090978 0.879264 0.718980 0.051 Uiso 1 1 calc R U . . . C19B C -0.03869(16) 0.83697(14) 0.77517(9) 0.0495(5) Uani 1 1 d . . . . . H19B H -0.110607 0.848608 0.749255 0.059 Uiso 1 1 calc R U . . . C20B C -0.05065(16) 0.80181(13) 0.83165(9) 0.0495(5) Uani 1 1 d . . . . . H20B H -0.130136 0.790299 0.845042 0.059 Uiso 1 1 calc R U . . . C21B C 0.05857(17) 0.78415(14) 0.86778(9) 0.0516(5) Uani 1 1 d . . . . . H21B H 0.050626 0.759513 0.905882 0.062 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1A 0.0376(7) 0.0879(11) 0.0629(9) 0.0073(8) 0.0226(6) 0.0076(7) N1A 0.0331(7) 0.0486(9) 0.0428(8) -0.0028(7) 0.0133(6) 0.0002(6) N2A 0.0450(9) 0.0671(12) 0.0547(10) -0.0082(8) 0.0210(7) 0.0010(7) C1A 0.0369(9) 0.0440(10) 0.0429(10) -0.0050(8) 0.0104(7) 0.0000(7) C2A 0.0508(11) 0.0664(14) 0.0460(11) 0.0013(9) 0.0164(9) 0.0036(9) C3A 0.0646(14) 0.0917(18) 0.0443(12) 0.0059(11) 0.0069(10) 0.0140(12) C4A 0.0494(11) 0.0839(17) 0.0523(12) -0.0009(11) -0.0008(9) 0.0121(10) C5A 0.0358(9) 0.0602(13) 0.0506(11) -0.0059(9) 0.0063(8) 0.0019(8) C6A 0.0341(8) 0.0418(10) 0.0440(10) -0.0054(8) 0.0091(7) -0.0025(7) C7A 0.0331(8) 0.0428(10) 0.0432(10) -0.0040(8) 0.0109(7) -0.0014(7) C8A 0.0338(9) 0.0443(10) 0.0422(10) -0.0020(8) 0.0118(7) -0.0014(7) C9A 0.0361(9) 0.0643(13) 0.0453(10) 0.0032(9) 0.0093(8) 0.0028(8) C10A 0.0377(9) 0.0522(11) 0.0419(10) -0.0011(8) 0.0120(7) -0.0021(8) C11A 0.0358(9) 0.0467(11) 0.0478(10) -0.0028(8) 0.0135(8) 0.0005(7) C12A 0.0517(11) 0.0566(13) 0.0541(12) 0.0039(9) 0.0114(9) -0.0072(9) C13A 0.0686(14) 0.0701(16) 0.0604(14) 0.0189(11) 0.0052(11) -0.0056(11) C14A 0.0888(18) 0.101(2) 0.0476(13) 0.0100(13) 0.0009(12) -0.0109(15) C15A 0.0828(16) 0.0787(17) 0.0508(13) -0.0095(12) 0.0020(11) -0.0148(13) C16A 0.0589(12) 0.0576(13) 0.0540(12) -0.0053(10) 0.0143(9) -0.0043(10) C17A 0.0348(9) 0.0395(10) 0.0517(10) -0.0013(8) 0.0170(8) -0.0016(7) C18A 0.0381(9) 0.0505(12) 0.0579(12) -0.0055(9) 0.0153(8) -0.0043(8) C19A 0.0351(10) 0.0540(12) 0.0793(15) 0.0019(11) 0.0137(9) -0.0019(8) C20A 0.0428(11) 0.0508(12) 0.0837(15) 0.0010(11) 0.0309(10) 0.0048(9) C21A 0.0552(12) 0.0671(14) 0.0649(13) -0.0074(11) 0.0304(10) 0.0052(10) O1B 0.0375(7) 0.0902(11) 0.0608(9) -0.0122(8) 0.0214(6) -0.0093(7) N1B 0.0294(7) 0.0466(9) 0.0339(7) -0.0016(6) 0.0082(5) -0.0004(6) N2B 0.0405(8) 0.0554(10) 0.0427(8) 0.0021(7) 0.0125(6) -0.0014(7) C1B 0.0327(8) 0.0386(10) 0.0371(9) 0.0006(7) 0.0046(7) 0.0009(7) C2B 0.0458(10) 0.0535(12) 0.0388(10) -0.0034(8) 0.0099(8) -0.0011(8) C3B 0.0568(12) 0.0688(14) 0.0379(10) -0.0092(9) 0.0008(8) -0.0075(10) C4B 0.0449(10) 0.0686(14) 0.0478(11) -0.0033(10) -0.0031(8) -0.0110(9) C5B 0.0321(9) 0.0547(12) 0.0483(10) 0.0027(9) 0.0044(7) -0.0023(8) C6B 0.0330(8) 0.0391(10) 0.0387(9) 0.0011(7) 0.0057(7) 0.0004(7) C7B 0.0319(8) 0.0415(10) 0.0388(9) -0.0006(7) 0.0084(7) -0.0007(7) C8B 0.0340(8) 0.0410(10) 0.0351(9) -0.0007(7) 0.0094(7) 0.0002(7) C9B 0.0353(9) 0.0662(13) 0.0395(10) -0.0081(9) 0.0104(7) -0.0046(8) C10B 0.0365(9) 0.0548(12) 0.0364(9) -0.0029(8) 0.0118(7) -0.0015(8) C11B 0.0365(9) 0.0473(11) 0.0440(10) -0.0014(8) 0.0135(7) -0.0011(7) C12B 0.0624(13) 0.0696(15) 0.0550(13) 0.0126(11) 0.0118(10) 0.0033(11) C13B 0.0801(17) 0.115(2) 0.0525(14) 0.0218(14) -0.0014(12) 0.0107(15) C14B 0.0774(17) 0.152(3) 0.0402(13) -0.0170(15) 0.0044(11) -0.0016(17) C15B 0.0614(13) 0.0938(19) 0.0542(13) -0.0265(12) 0.0118(10) -0.0029(12) C16B 0.0482(11) 0.0602(13) 0.0506(11) -0.0111(9) 0.0108(9) 0.0023(9) C17B 0.0326(8) 0.0368(9) 0.0402(9) -0.0029(7) 0.0125(7) 0.0007(7) C18B 0.0364(9) 0.0470(11) 0.0461(10) 0.0032(8) 0.0100(7) 0.0046(7) C19B 0.0314(9) 0.0539(12) 0.0636(12) -0.0007(9) 0.0075(8) 0.0033(8) C20B 0.0370(9) 0.0493(12) 0.0655(13) -0.0054(9) 0.0227(9) -0.0036(8) C21B 0.0483(11) 0.0601(13) 0.0494(11) 0.0028(9) 0.0218(9) -0.0035(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8A N1A C1A 107.21(13) . . ? C8A N1A C17A 126.94(15) . . ? C1A N1A C17A 125.73(14) . . ? C17A N2A C21A 116.34(17) . . ? C2A C1A C6A 121.22(17) . . ? C2A C1A N1A 130.43(15) . . ? C6A C1A N1A 108.26(14) . . ? C3A C2A C1A 117.27(17) . . ? C3A C2A H2A 121.4 . . ? C1A C2A H2A 121.4 . . ? C2A C3A C4A 122.18(19) . . ? C2A C3A H3A 118.9 . . ? C4A C3A H3A 118.9 . . ? C5A C4A C3A 120.60(19) . . ? C5A C4A H4A 119.7 . . ? C3A C4A H4A 119.7 . . ? C4A C5A C6A 119.10(17) . . ? C4A C5A H5A 120.5 . . ? C6A C5A H5A 120.5 . . ? C5A C6A C1A 119.63(16) . . ? C5A C6A C7A 134.69(15) . . ? C1A C6A C7A 105.58(14) . . ? C8A C7A C6A 108.62(14) . . ? C8A C7A C11A 109.64(16) . . ? C6A C7A C11A 141.73(15) . . ? C7A C8A N1A 110.31(15) . . ? C7A C8A C9A 114.72(14) . . ? N1A C8A C9A 134.95(15) . . ? C8A C9A C10A 102.44(13) . . ? C8A C9A H9AA 111.3 . . ? C10A C9A H9AA 111.3 . . ? C8A C9A H9AB 111.3 . . ? C10A C9A H9AB 111.3 . . ? H9AA C9A H9AB 109.2 . . ? C12A C10A C16A 109.85(15) . . ? C12A C10A C11A 110.22(15) . . ? C16A C10A C11A 107.48(15) . . ? C12A C10A C9A 112.66(15) . . ? C16A C10A C9A 111.30(15) . . ? C11A C10A C9A 105.10(13) . . ? O1A C11A C7A 128.23(17) . . ? O1A C11A C10A 123.86(16) . . ? C7A C11A C10A 107.91(13) . . ? C13A C12A C10A 112.72(16) . . ? C13A C12A H12A 109.0 . . ? C10A C12A H12A 109.0 . . ? C13A C12A H12B 109.0 . . ? C10A C12A H12B 109.0 . . ? H12A C12A H12B 107.8 . . ? C14A C13A C12A 111.5(2) . . ? C14A C13A H13A 109.3 . . ? C12A C13A H13A 109.3 . . ? C14A C13A H13B 109.3 . . ? C12A C13A H13B 109.3 . . ? H13A C13A H13B 108.0 . . ? C15A C14A C13A 111.03(18) . . ? C15A C14A H14A 109.4 . . ? C13A C14A H14A 109.4 . . ? C15A C14A H14B 109.4 . . ? C13A C14A H14B 109.4 . . ? H14A C14A H14B 108.0 . . ? C14A C15A C16A 110.75(19) . . ? C14A C15A H15A 109.5 . . ? C16A C15A H15A 109.5 . . ? C14A C15A H15B 109.5 . . ? C16A C15A H15B 109.5 . . ? H15A C15A H15B 108.1 . . ? C15A C16A C10A 112.82(18) . . ? C15A C16A H16A 109.0 . . ? C10A C16A H16A 109.0 . . ? C15A C16A H16B 109.0 . . ? C10A C16A H16B 109.0 . . ? H16A C16A H16B 107.8 . . ? N2A C17A C18A 123.96(15) . . ? N2A C17A N1A 114.88(16) . . ? C18A C17A N1A 121.16(16) . . ? C17A C18A C19A 118.07(18) . . ? C17A C18A H18A 121.0 . . ? C19A C18A H18A 121.0 . . ? C20A C19A C18A 119.33(19) . . ? C20A C19A H19A 120.3 . . ? C18A C19A H19A 120.3 . . ? C21A C20A C19A 118.22(17) . . ? C21A C20A H20A 120.9 . . ? C19A C20A H20A 120.9 . . ? N2A C21A C20A 124.07(19) . . ? N2A C21A H21A 118.0 . . ? C20A C21A H21A 118.0 . . ? C8B N1B C1B 107.16(12) . . ? C8B N1B C17B 127.04(14) . . ? C1B N1B C17B 125.75(13) . . ? C17B N2B C21B 116.52(16) . . ? C2B C1B C6B 121.43(15) . . ? C2B C1B N1B 130.09(14) . . ? C6B C1B N1B 108.41(14) . . ? C3B C2B C1B 117.19(16) . . ? C3B C2B H2B 121.4 . . ? C1B C2B H2B 121.4 . . ? C2B C3B C4B 122.00(17) . . ? C2B C3B H3B 119.0 . . ? C4B C3B H3B 119.0 . . ? C5B C4B C3B 120.87(17) . . ? C5B C4B H4B 119.6 . . ? C3B C4B H4B 119.6 . . ? C4B C5B C6B 118.86(16) . . ? C4B C5B H5B 120.6 . . ? C6B C5B H5B 120.6 . . ? C5B C6B C1B 119.63(15) . . ? C5B C6B C7B 134.60(15) . . ? C1B C6B C7B 105.66(14) . . ? C8B C7B C6B 108.48(14) . . ? C8B C7B C11B 109.63(15) . . ? C6B C7B C11B 141.83(15) . . ? C7B C8B N1B 110.26(14) . . ? C7B C8B C9B 114.90(14) . . ? N1B C8B C9B 134.80(14) . . ? C8B C9B C10B 102.34(13) . . ? C8B C9B H9BA 111.3 . . ? C10B C9B H9BA 111.3 . . ? C8B C9B H9BB 111.3 . . ? C10B C9B H9BB 111.3 . . ? H9BA C9B H9BB 109.2 . . ? C12B C10B C16B 110.39(15) . . ? C12B C10B C11B 107.98(15) . . ? C16B C10B C11B 109.78(14) . . ? C12B C10B C9B 111.41(15) . . ? C16B C10B C9B 111.86(15) . . ? C11B C10B C9B 105.23(13) . . ? O1B C11B C7B 128.23(17) . . ? O1B C11B C10B 124.10(15) . . ? C7B C11B C10B 107.67(13) . . ? C13B C12B C10B 112.57(19) . . ? C13B C12B H12C 109.1 . . ? C10B C12B H12C 109.1 . . ? C13B C12B H12D 109.1 . . ? C10B C12B H12D 109.1 . . ? H12C C12B H12D 107.8 . . ? C12B C13B C14B 111.0(2) . . ? C12B C13B H13C 109.4 . . ? C14B C13B H13C 109.4 . . ? C12B C13B H13D 109.4 . . ? C14B C13B H13D 109.4 . . ? H13C C13B H13D 108.0 . . ? C15B C14B C13B 111.42(19) . . ? C15B C14B H14C 109.3 . . ? C13B C14B H14C 109.3 . . ? C15B C14B H14D 109.3 . . ? C13B C14B H14D 109.3 . . ? H14C C14B H14D 108.0 . . ? C14B C15B C16B 111.0(2) . . ? C14B C15B H15C 109.4 . . ? C16B C15B H15C 109.4 . . ? C14B C15B H15D 109.4 . . ? C16B C15B H15D 109.4 . . ? H15C C15B H15D 108.0 . . ? C15B C16B C10B 112.69(17) . . ? C15B C16B H16C 109.1 . . ? C10B C16B H16C 109.1 . . ? C15B C16B H16D 109.1 . . ? C10B C16B H16D 109.1 . . ? H16C C16B H16D 107.8 . . ? N2B C17B C18B 124.19(15) . . ? N2B C17B N1B 115.13(14) . . ? C18B C17B N1B 120.67(15) . . ? C17B C18B C19B 117.58(17) . . ? C17B C18B H18B 121.2 . . ? C19B C18B H18B 121.2 . . ? C20B C19B C18B 119.74(17) . . ? C20B C19B H19B 120.1 . . ? C18B C19B H19B 120.1 . . ? C19B C20B C21B 117.86(16) . . ? C19B C20B H20B 121.1 . . ? C21B C20B H20B 121.1 . . ? N2B C21B C20B 124.10(17) . . ? N2B C21B H21B 117.9 . . ? C20B C21B H21B 117.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1A C11A 1.2241(19) . ? N1A C8A 1.377(2) . ? N1A C1A 1.417(2) . ? N1A C17A 1.4236(19) . ? N2A C17A 1.330(2) . ? N2A C21A 1.343(2) . ? C1A C2A 1.385(2) . ? C1A C6A 1.417(2) . ? C2A C3A 1.380(3) . ? C2A H2A 0.9300 . ? C3A C4A 1.388(3) . ? C3A H3A 0.9300 . ? C4A C5A 1.369(3) . ? C4A H4A 0.9300 . ? C5A C6A 1.388(2) . ? C5A H5A 0.9300 . ? C6A C7A 1.433(2) . ? C7A C8A 1.360(2) . ? C7A C11A 1.437(2) . ? C8A C9A 1.487(2) . ? C9A C10A 1.563(2) . ? C9A H9AA 0.9700 . ? C9A H9AB 0.9700 . ? C10A C12A 1.531(3) . ? C10A C16A 1.535(3) . ? C10A C11A 1.542(2) . ? C12A C13A 1.522(3) . ? C12A H12A 0.9700 . ? C12A H12B 0.9700 . ? C13A C14A 1.520(3) . ? C13A H13A 0.9700 . ? C13A H13B 0.9700 . ? C14A C15A 1.514(3) . ? C14A H14A 0.9700 . ? C14A H14B 0.9700 . ? C15A C16A 1.520(3) . ? C15A H15A 0.9700 . ? C15A H15B 0.9700 . ? C16A H16A 0.9700 . ? C16A H16B 0.9700 . ? C17A C18A 1.372(2) . ? C18A C19A 1.382(2) . ? C18A H18A 0.9300 . ? C19A C20A 1.370(3) . ? C19A H19A 0.9300 . ? C20A C21A 1.366(3) . ? C20A H20A 0.9300 . ? C21A H21A 0.9300 . ? O1B C11B 1.2212(19) . ? N1B C8B 1.3779(19) . ? N1B C1B 1.414(2) . ? N1B C17B 1.4254(19) . ? N2B C17B 1.329(2) . ? N2B C21B 1.336(2) . ? C1B C2B 1.387(2) . ? C1B C6B 1.413(2) . ? C2B C3B 1.382(3) . ? C2B H2B 0.9300 . ? C3B C4B 1.389(3) . ? C3B H3B 0.9300 . ? C4B C5B 1.371(3) . ? C4B H4B 0.9300 . ? C5B C6B 1.392(2) . ? C5B H5B 0.9300 . ? C6B C7B 1.433(2) . ? C7B C8B 1.360(2) . ? C7B C11B 1.440(2) . ? C8B C9B 1.485(2) . ? C9B C10B 1.564(2) . ? C9B H9BA 0.9700 . ? C9B H9BB 0.9700 . ? C10B C12B 1.525(3) . ? C10B C16B 1.533(3) . ? C10B C11B 1.544(2) . ? C12B C13B 1.519(3) . ? C12B H12C 0.9700 . ? C12B H12D 0.9700 . ? C13B C14B 1.522(4) . ? C13B H13C 0.9700 . ? C13B H13D 0.9700 . ? C14B C15B 1.515(4) . ? C14B H14C 0.9700 . ? C14B H14D 0.9700 . ? C15B C16B 1.517(3) . ? C15B H15C 0.9700 . ? C15B H15D 0.9700 . ? C16B H16C 0.9700 . ? C16B H16D 0.9700 . ? C17B C18B 1.377(2) . ? C18B C19B 1.382(2) . ? C18B H18B 0.9300 . ? C19B C20B 1.372(3) . ? C19B H19B 0.9300 . ? C20B C21B 1.374(3) . ? C20B H20B 0.9300 . ? C21B H21B 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C8A N1A C1A C2A -176.2(2) . . . . ? C17A N1A C1A C2A 7.5(3) . . . . ? C8A N1A C1A C6A 0.25(19) . . . . ? C17A N1A C1A C6A -176.04(15) . . . . ? C6A C1A C2A C3A -0.2(3) . . . . ? N1A C1A C2A C3A 175.9(2) . . . . ? C1A C2A C3A C4A -0.3(3) . . . . ? C2A C3A C4A C5A 0.4(4) . . . . ? C3A C4A C5A C6A -0.1(3) . . . . ? C4A C5A C6A C1A -0.3(3) . . . . ? C4A C5A C6A C7A -176.1(2) . . . . ? C2A C1A C6A C5A 0.4(3) . . . . ? N1A C1A C6A C5A -176.40(16) . . . . ? C2A C1A C6A C7A 177.36(17) . . . . ? N1A C1A C6A C7A 0.53(19) . . . . ? C5A C6A C7A C8A 175.1(2) . . . . ? C1A C6A C7A C8A -1.1(2) . . . . ? C5A C6A C7A C11A -6.7(4) . . . . ? C1A C6A C7A C11A 177.1(2) . . . . ? C6A C7A C8A N1A 1.4(2) . . . . ? C11A C7A C8A N1A -177.47(15) . . . . ? C6A C7A C8A C9A 179.96(16) . . . . ? C11A C7A C8A C9A 1.1(2) . . . . ? C1A N1A C8A C7A -1.0(2) . . . . ? C17A N1A C8A C7A 175.23(16) . . . . ? C1A N1A C8A C9A -179.2(2) . . . . ? C17A N1A C8A C9A -3.0(3) . . . . ? C7A C8A C9A C10A 1.7(2) . . . . ? N1A C8A C9A C10A 179.84(19) . . . . ? C8A C9A C10A C12A -123.62(17) . . . . ? C8A C9A C10A C16A 112.47(17) . . . . ? C8A C9A C10A C11A -3.58(19) . . . . ? C8A C7A C11A O1A 176.43(19) . . . . ? C6A C7A C11A O1A -1.8(4) . . . . ? C8A C7A C11A C10A -3.5(2) . . . . ? C6A C7A C11A C10A 178.3(2) . . . . ? C12A C10A C11A O1A -53.9(2) . . . . ? C16A C10A C11A O1A 65.8(2) . . . . ? C9A C10A C11A O1A -175.54(18) . . . . ? C12A C10A C11A C7A 126.07(16) . . . . ? C16A C10A C11A C7A -114.23(16) . . . . ? C9A C10A C11A C7A 4.42(19) . . . . ? C16A C10A C12A C13A 52.4(2) . . . . ? C11A C10A C12A C13A 170.61(16) . . . . ? C9A C10A C12A C13A -72.3(2) . . . . ? C10A C12A C13A C14A -54.5(2) . . . . ? C12A C13A C14A C15A 55.9(3) . . . . ? C13A C14A C15A C16A -56.5(3) . . . . ? C14A C15A C16A C10A 56.2(2) . . . . ? C12A C10A C16A C15A -53.4(2) . . . . ? C11A C10A C16A C15A -173.35(16) . . . . ? C9A C10A C16A C15A 72.1(2) . . . . ? C21A N2A C17A C18A 1.1(3) . . . . ? C21A N2A C17A N1A -178.27(17) . . . . ? C8A N1A C17A N2A -144.10(18) . . . . ? C1A N1A C17A N2A 31.5(2) . . . . ? C8A N1A C17A C18A 36.5(3) . . . . ? C1A N1A C17A C18A -147.91(18) . . . . ? N2A C17A C18A C19A -0.6(3) . . . . ? N1A C17A C18A C19A 178.73(17) . . . . ? C17A C18A C19A C20A -0.7(3) . . . . ? C18A C19A C20A C21A 1.4(3) . . . . ? C17A N2A C21A C20A -0.3(3) . . . . ? C19A C20A C21A N2A -1.0(3) . . . . ? C8B N1B C1B C2B 176.88(18) . . . . ? C17B N1B C1B C2B -5.7(3) . . . . ? C8B N1B C1B C6B -0.20(18) . . . . ? C17B N1B C1B C6B 177.26(15) . . . . ? C6B C1B C2B C3B 0.9(3) . . . . ? N1B C1B C2B C3B -175.88(18) . . . . ? C1B C2B C3B C4B 0.2(3) . . . . ? C2B C3B C4B C5B -0.7(3) . . . . ? C3B C4B C5B C6B 0.2(3) . . . . ? C4B C5B C6B C1B 0.8(3) . . . . ? C4B C5B C6B C7B 176.29(19) . . . . ? C2B C1B C6B C5B -1.4(3) . . . . ? N1B C1B C6B C5B 176.01(15) . . . . ? C2B C1B C6B C7B -178.04(16) . . . . ? N1B C1B C6B C7B -0.65(18) . . . . ? C5B C6B C7B C8B -174.63(19) . . . . ? C1B C6B C7B C8B 1.29(19) . . . . ? C5B C6B C7B C11B 8.8(4) . . . . ? C1B C6B C7B C11B -175.3(2) . . . . ? C6B C7B C8B N1B -1.5(2) . . . . ? C11B C7B C8B N1B 176.27(14) . . . . ? C6B C7B C8B C9B -179.87(15) . . . . ? C11B C7B C8B C9B -2.1(2) . . . . ? C1B N1B C8B C7B 1.05(19) . . . . ? C17B N1B C8B C7B -176.38(15) . . . . ? C1B N1B C8B C9B 179.0(2) . . . . ? C17B N1B C8B C9B 1.6(3) . . . . ? C7B C8B C9B C10B -1.0(2) . . . . ? N1B C8B C9B C10B -178.90(18) . . . . ? C8B C9B C10B C12B -113.30(17) . . . . ? C8B C9B C10B C16B 122.61(17) . . . . ? C8B C9B C10B C11B 3.46(19) . . . . ? C8B C7B C11B O1B -175.60(19) . . . . ? C6B C7B C11B O1B 0.9(4) . . . . ? C8B C7B C11B C10B 4.4(2) . . . . ? C6B C7B C11B C10B -179.1(2) . . . . ? C12B C10B C11B O1B -65.8(2) . . . . ? C16B C10B C11B O1B 54.6(2) . . . . ? C9B C10B C11B O1B 175.14(18) . . . . ? C12B C10B C11B C7B 114.25(16) . . . . ? C16B C10B C11B C7B -125.36(16) . . . . ? C9B C10B C11B C7B -4.83(19) . . . . ? C16B C10B C12B C13B 53.0(2) . . . . ? C11B C10B C12B C13B 173.04(17) . . . . ? C9B C10B C12B C13B -71.9(2) . . . . ? C10B C12B C13B C14B -54.9(3) . . . . ? C12B C13B C14B C15B 55.8(3) . . . . ? C13B C14B C15B C16B -55.8(3) . . . . ? C14B C15B C16B C10B 55.0(2) . . . . ? C12B C10B C16B C15B -53.1(2) . . . . ? C11B C10B C16B C15B -172.05(16) . . . . ? C9B C10B C16B C15B 71.5(2) . . . . ? C21B N2B C17B C18B -1.1(3) . . . . ? C21B N2B C17B N1B 177.55(15) . . . . ? C8B N1B C17B N2B 143.95(17) . . . . ? C1B N1B C17B N2B -33.0(2) . . . . ? C8B N1B C17B C18B -37.3(2) . . . . ? C1B N1B C17B C18B 145.72(17) . . . . ? N2B C17B C18B C19B 0.8(3) . . . . ? N1B C17B C18B C19B -177.85(16) . . . . ? C17B C18B C19B C20B 0.5(3) . . . . ? C18B C19B C20B C21B -1.2(3) . . . . ? C17B N2B C21B C20B 0.3(3) . . . . ? C19B C20B C21B N2B 0.8(3) . . . . ?