#------------------------------------------------------------------------------ #$Date: 2021-10-03 22:54:42 +0300 (Sun, 03 Oct 2021) $ #$Revision: 269491 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/90/4519069.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519069 loop_ _publ_author_name 'Ankade, Shidheshwar B.' 'Samal, Pragnya Paramita' 'Soni, Vineeta' 'Gonnade, Rajesh G.' 'Krishnamurty, Sailaja' 'Punji, Benudhar' _publ_section_title ; Ni(II)-Catalyzed Intramolecular C--H/C--H Oxidative Coupling: An Efficient Route to Functionalized Cycloindolones and Indenoindolones ; _journal_issue 19 _journal_name_full 'ACS Catalysis' _journal_page_first 12384 _journal_page_last 12393 _journal_paper_doi 10.1021/acscatal.1c03314 _journal_volume 11 _journal_year 2021 _chemical_formula_moiety 'C36 H30 N4 O2' _chemical_formula_sum 'C36 H30 N4 O2' _chemical_formula_weight 550.64 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 96.740(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.7476(11) _cell_length_b 9.0897(5) _cell_length_c 18.6802(12) _cell_measurement_reflns_used 9852 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 32.40 _cell_measurement_theta_min 2.20 _cell_volume 2824.0(3) _computing_cell_refinement 'SAINT (Bruker, 2016)' _computing_data_collection 'APEX3 (Bruker, 2016)' _computing_data_reduction 'SAINT (Bruker, 2016)' _computing_molecular_graphics 'Bruker SHELXTL, Mercury 2020.20' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector 'Photon II CPAD Area Detector' _diffrn_detector_area_resol_mean 7.39 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Kappa Duo PHOTON II CPAD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0757 _diffrn_reflns_av_unetI/netI 0.0369 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 87933 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.000 _diffrn_reflns_theta_min 2.385 _diffrn_source 'micro-focus sealed tube' _diffrn_source_type 'Incoatech I\mS HB' _exptl_absorpt_coefficient_mu 0.082 _exptl_absorpt_correction_T_max 0.980 _exptl_absorpt_correction_T_min 0.974 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (BRUKER, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.295 _exptl_crystal_description block _exptl_crystal_F_000 1160 _exptl_crystal_size_max 0.320 _exptl_crystal_size_mid 0.270 _exptl_crystal_size_min 0.250 _refine_diff_density_max 0.413 _refine_diff_density_min -0.264 _refine_diff_density_rms 0.051 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 381 _refine_ls_number_reflns 8236 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.031 _refine_ls_R_factor_all 0.0652 _refine_ls_R_factor_gt 0.0452 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0498P)^2^+1.3502P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1068 _refine_ls_wR_factor_ref 0.1212 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6352 _reflns_number_total 8236 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c03314_si_006.cif _cod_data_source_block Comp_18 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 4519069 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.974 _shelx_estimated_absorpt_t_max 0.980 _shelx_res_file ; TITL mo_SACYCLOPROPANON_0m_a.res in P2(1)/c mo_SACYCLOPROPANON_0m_a.res created by SHELXL-2018/3 at 23:41:24 on 12-Jul-2021 REM Old TITL mo_SACYCLOPROPANON_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.119, Rweak 0.004, Alpha 0.021, Orientation as input REM Formula found by SHELXT: C36 N4 O2 CELL 0.71073 16.7476 9.0897 18.6802 90.000 96.740 90.000 ZERR 4.000 0.0011 0.0005 0.0012 0.000 0.002 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 144 120 16 8 TEMP -173.150 OMIT 2 0 0 OMIT -1 1 1 OMIT 22 0 10 OMIT 0 1 1 OMIT -3.0 60.00 CONF SIZE 0.32 0.27 0.25 ACTA L.S. 10 BOND $H LIST 6 FMAP 2 PLAN 20 WGHT 0.049800 1.350200 FVAR 0.61344 O1 4 0.664543 0.722893 0.222855 11.00000 0.02659 0.01747 = 0.03034 -0.00217 -0.00285 0.00002 O2 4 0.816503 0.474997 0.119043 11.00000 0.02740 0.02266 = 0.01884 -0.00550 -0.00034 -0.00049 N1 3 0.699563 0.261456 0.259857 11.00000 0.01573 0.01410 = 0.01704 0.00144 -0.00386 -0.00180 N2 3 0.716095 0.071653 0.343802 11.00000 0.02149 0.02223 = 0.02234 0.00571 -0.00104 0.00016 N3 3 0.819378 0.478446 0.347523 11.00000 0.01401 0.01563 = 0.01399 0.00053 -0.00235 -0.00186 N4 3 0.816347 0.352790 0.456453 11.00000 0.02239 0.02034 = 0.01794 0.00406 -0.00192 -0.00048 C1 1 0.622565 0.227849 0.226610 11.00000 0.01541 0.01804 = 0.01710 -0.00027 -0.00286 -0.00200 C2 1 0.579377 0.096079 0.225366 11.00000 0.02124 0.01745 = 0.02428 0.00205 -0.00239 -0.00284 AFIX 43 H2 2 0.601513 0.010132 0.248881 11.00000 -1.20000 AFIX 0 C3 1 0.502840 0.096799 0.188247 11.00000 0.02189 0.02148 = 0.03032 0.00055 -0.00401 -0.00742 AFIX 43 H3 2 0.471885 0.008990 0.186046 11.00000 -1.20000 AFIX 0 C4 1 0.469659 0.223886 0.153719 11.00000 0.01824 0.02587 = 0.03050 0.00094 -0.00726 -0.00405 AFIX 43 H4 2 0.416501 0.220793 0.129578 11.00000 -1.20000 AFIX 0 C5 1 0.512929 0.352895 0.154290 11.00000 0.01912 0.02056 = 0.02416 0.00148 -0.00543 0.00001 AFIX 43 H5 2 0.490164 0.438534 0.130942 11.00000 -1.20000 AFIX 0 C6 1 0.591483 0.354893 0.190190 11.00000 0.01737 0.01692 = 0.01821 -0.00025 -0.00225 -0.00096 C7 1 0.651546 0.468217 0.202953 11.00000 0.01695 0.01554 = 0.01612 0.00019 -0.00226 -0.00133 C8 1 0.715965 0.407972 0.245710 11.00000 0.01712 0.01381 = 0.01440 0.00031 -0.00193 -0.00116 C9 1 0.751576 0.159510 0.300039 11.00000 0.01917 0.01496 = 0.01519 0.00008 -0.00299 0.00117 C10 1 0.832773 0.155632 0.291890 11.00000 0.02006 0.01716 = 0.02041 0.00083 0.00145 0.00098 AFIX 43 H10 2 0.854944 0.219617 0.259190 11.00000 -1.20000 AFIX 0 C11 1 0.880434 0.055227 0.333083 11.00000 0.01942 0.02239 = 0.02662 -0.00133 -0.00068 0.00420 AFIX 43 H11 2 0.936611 0.050792 0.330048 11.00000 -1.20000 AFIX 0 C12 1 0.845360 -0.038689 0.378764 11.00000 0.02657 0.02180 = 0.02606 0.00517 -0.00293 0.00618 AFIX 43 H12 2 0.876761 -0.108662 0.407473 11.00000 -1.20000 AFIX 0 C13 1 0.763325 -0.027795 0.381437 11.00000 0.02866 0.02441 = 0.02605 0.00998 0.00035 0.00024 AFIX 43 H13 2 0.739031 -0.094372 0.411577 11.00000 -1.20000 AFIX 0 C14 1 0.643558 0.624270 0.180314 11.00000 0.01595 0.01722 = 0.02226 0.00215 -0.00088 0.00074 C15 1 0.606393 0.654697 0.104783 11.00000 0.02809 0.01940 = 0.02391 0.00616 -0.00521 0.00194 C16 1 0.523603 0.726909 0.101255 11.00000 0.03368 0.02808 = 0.04191 0.00412 -0.01173 0.01223 AFIX 23 H16A 2 0.483022 0.700555 0.060395 11.00000 -1.20000 H16B 2 0.501662 0.746356 0.147295 11.00000 -1.20000 AFIX 0 C17 1 0.595037 0.814451 0.085167 11.00000 0.05320 0.02245 = 0.03638 0.01182 -0.00840 0.00329 AFIX 23 H17A 2 0.616811 0.888405 0.121191 11.00000 -1.20000 H17B 2 0.598191 0.842655 0.034387 11.00000 -1.20000 AFIX 0 C18 1 0.621601 0.547359 0.045896 11.00000 0.03197 0.03040 = 0.02111 0.00384 -0.00498 0.00141 AFIX 137 H18A 2 0.598206 0.585991 -0.000894 11.00000 -1.50000 H18B 2 0.596790 0.452464 0.054780 11.00000 -1.50000 H18C 2 0.679648 0.534149 0.045690 11.00000 -1.50000 AFIX 0 C19 1 0.891686 0.555864 0.357765 11.00000 0.01309 0.01388 = 0.01659 -0.00060 -0.00041 0.00007 C20 1 0.942041 0.584441 0.421150 11.00000 0.01533 0.01700 = 0.01543 0.00001 -0.00167 0.00225 AFIX 43 H20 2 0.930731 0.545919 0.466150 11.00000 -1.20000 AFIX 0 C21 1 1.009200 0.671167 0.415984 11.00000 0.01524 0.01971 = 0.01898 -0.00265 -0.00354 0.00080 AFIX 43 H21 2 1.044183 0.693629 0.458353 11.00000 -1.20000 AFIX 0 C22 1 1.026514 0.726425 0.349383 11.00000 0.01442 0.02123 = 0.02423 -0.00221 -0.00008 -0.00360 AFIX 43 H22 2 1.073139 0.785125 0.347420 11.00000 -1.20000 AFIX 0 C23 1 0.976764 0.696822 0.286450 11.00000 0.01838 0.02027 = 0.01847 -0.00020 0.00229 -0.00200 AFIX 43 H23 2 0.989355 0.733476 0.241487 11.00000 -1.20000 AFIX 0 C24 1 0.907266 0.611549 0.290237 11.00000 0.01570 0.01521 = 0.01556 -0.00074 -0.00141 0.00021 C25 1 0.842981 0.560702 0.237961 11.00000 0.01706 0.01427 = 0.01423 0.00046 -0.00209 -0.00039 C26 1 0.791046 0.480771 0.274503 11.00000 0.01575 0.01402 = 0.01411 0.00007 -0.00301 0.00069 C27 1 0.775387 0.430523 0.403925 11.00000 0.01639 0.01428 = 0.01550 0.00009 -0.00113 -0.00236 C28 1 0.694440 0.467706 0.401519 11.00000 0.01611 0.02004 = 0.01856 -0.00222 -0.00145 0.00010 AFIX 43 H28 2 0.668304 0.524891 0.363124 11.00000 -1.20000 AFIX 0 C29 1 0.653489 0.418490 0.456945 11.00000 0.01851 0.02706 = 0.02584 -0.00728 0.00315 -0.00577 AFIX 43 H29 2 0.597957 0.439820 0.456939 11.00000 -1.20000 AFIX 0 C30 1 0.694366 0.337656 0.512540 11.00000 0.03124 0.02751 = 0.02176 -0.00121 0.00622 -0.01201 AFIX 43 H30 2 0.667601 0.303283 0.551421 11.00000 -1.20000 AFIX 0 C31 1 0.775198 0.308099 0.510124 11.00000 0.03070 0.02480 = 0.02023 0.00630 -0.00234 -0.00391 AFIX 43 H31 2 0.803064 0.253222 0.548521 11.00000 -1.20000 AFIX 0 C32 1 0.834074 0.580313 0.158720 11.00000 0.01578 0.02001 = 0.01498 -0.00039 -0.00054 -0.00035 C33 1 0.848606 0.729639 0.129005 11.00000 0.02616 0.02377 = 0.01465 0.00319 -0.00161 -0.00553 C34 1 0.833513 0.742684 0.048044 11.00000 0.03660 0.03895 = 0.01761 0.00857 -0.00334 -0.01050 AFIX 23 H34A 2 0.811192 0.655819 0.020652 11.00000 -1.20000 H34B 2 0.814490 0.838690 0.027619 11.00000 -1.20000 AFIX 0 C35 1 0.918469 0.733542 0.083236 11.00000 0.03052 0.04389 = 0.02275 0.00667 0.00394 -0.01118 AFIX 23 H35A 2 0.951571 0.823970 0.084741 11.00000 -1.20000 H35B 2 0.948271 0.640934 0.077768 11.00000 -1.20000 AFIX 0 C36 1 0.833047 0.865192 0.172081 11.00000 0.03857 0.01765 = 0.02766 0.00375 -0.00223 -0.00395 AFIX 137 H36A 2 0.847490 0.953121 0.146101 11.00000 -1.50000 H36B 2 0.865600 0.860919 0.219186 11.00000 -1.50000 H36C 2 0.775958 0.869457 0.178897 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_SACYCLOPROPANON_0m_a.res in P2(1)/c REM wR2 = 0.121234, GooF = S = 1.03111, Restrained GooF = 1.03111 for all data REM R1 = 0.045180 for 6352 Fo > 4sig(Fo) and 0.065197 for all 8236 data REM 381 parameters refined using 0 restraints END WGHT 0.0498 1.3502 REM Highest difference peak 0.413, deepest hole -0.264, 1-sigma level 0.051 Q1 1 0.9086 0.5816 0.3253 11.00000 0.05 0.41 Q2 1 1.0250 0.6704 0.3824 11.00000 0.05 0.36 Q3 1 0.6177 0.4144 0.1976 11.00000 0.05 0.35 Q4 1 0.8380 0.5729 0.1992 11.00000 0.05 0.33 Q5 1 0.6783 0.4472 0.4328 11.00000 0.05 0.33 Q6 1 0.6064 0.2869 0.2027 11.00000 0.05 0.32 Q7 1 0.7493 0.4531 0.2598 11.00000 0.05 0.32 Q8 1 0.7320 0.2962 0.5033 11.00000 0.05 0.32 Q9 1 0.6819 0.4509 0.2280 11.00000 0.05 0.32 Q10 1 0.7907 0.1478 0.2864 11.00000 0.05 0.31 Q11 1 1.0018 0.6907 0.3205 11.00000 0.05 0.30 Q12 1 0.9724 0.6320 0.4133 11.00000 0.05 0.29 Q13 1 0.8249 0.4930 0.2515 11.00000 0.05 0.29 Q14 1 0.8074 0.4563 0.3075 11.00000 0.05 0.28 Q15 1 0.8542 0.5113 0.3565 11.00000 0.05 0.28 Q16 1 0.7280 0.4224 0.4023 11.00000 0.05 0.27 Q17 1 0.6293 0.6318 0.1386 11.00000 0.05 0.27 Q18 1 0.8699 0.6016 0.2636 11.00000 0.05 0.27 Q19 1 0.7365 0.4572 0.4095 11.00000 0.05 0.26 Q20 1 0.6589 0.2342 0.2491 11.00000 0.05 0.26 ; _shelx_res_checksum 75935 _shelx_hkl_file ; -2 0 0 7.00 3.70 3 0 0 2360.36 131.49 3 0 0 2441.66 130.89 3 0 0 2575.04 133.49 -3 0 0 2421.26 130.89 3 0 0 2527.65 131.89 3 0 0 2433.96 132.29 -3 0 0 2557.24 130.79 -3 0 0 2291.17 133.09 -3 0 0 2434.46 131.69 -4 0 0 1823.72 95.29 -4 0 0 1769.22 97.09 -4 0 0 1658.93 96.39 -4 0 0 1634.14 95.29 -4 0 0 1678.13 96.09 4 0 0 1835.42 96.49 4 0 0 1991.20 95.69 -4 0 0 1717.43 95.29 4 0 0 1844.12 97.69 4 0 0 1786.92 98.69 4 0 0 1714.13 95.39 5 0 0 1373.86 78.49 -5 0 0 1355.86 74.59 5 0 0 1369.96 77.09 -5 0 0 1310.17 75.39 -5 0 0 1407.46 74.39 -5 0 0 1287.47 75.69 -5 0 0 1338.27 74.59 5 0 0 1312.57 75.89 5 0 0 1431.56 74.79 5 0 0 1456.05 74.79 5 0 0 1336.47 75.69 -6 0 0 7085.19 405.16 -6 0 0 7514.75 405.86 6 0 0 7234.38 408.76 6 0 0 7679.73 405.86 -6 0 0 7716.43 404.26 6 0 0 7822.22 407.66 6 0 0 8242.67 404.66 -6 0 0 7320.77 404.16 6 0 0 8089.79 404.66 6 0 0 7273.27 405.96 7 0 0 48.70 5.70 -7 0 0 49.40 7.70 7 0 0 50.69 8.50 7 0 0 37.60 8.70 7 0 0 60.69 6.80 -7 0 0 54.09 5.60 7 0 0 64.19 6.20 -7 0 0 52.09 5.70 -7 0 0 47.90 7.10 -7 0 0 55.49 5.80 7 0 0 58.59 8.50 -8 0 0 85.69 8.00 -8 0 0 84.89 8.00 -8 0 0 79.89 9.20 -8 0 0 78.49 7.50 -8 0 0 83.49 8.80 8 0 0 82.69 9.10 8 0 0 102.29 14.70 8 0 0 84.29 8.10 8 0 0 73.29 9.10 8 0 0 87.69 12.50 8 0 0 83.09 8.10 -9 0 0 2279.17 135.29 -9 0 0 2356.36 133.19 9 0 0 2527.55 133.79 9 0 0 2461.65 140.59 9 0 0 2372.96 135.69 9 0 0 2471.05 136.59 -9 0 0 2495.15 133.19 9 0 0 2508.05 133.89 -9 0 0 2478.55 135.29 9 0 0 2420.76 138.39 10 0 0 598.34 36.00 10 0 0 571.44 36.00 -10 0 0 565.34 35.30 -10 0 0 585.14 37.40 10 0 0 586.24 38.60 -10 0 0 568.84 35.40 10 0 0 576.04 40.70 10 0 0 605.84 43.00 10 0 0 576.14 38.00 -10 0 0 544.75 37.60 11 0 0 14.40 5.60 11 0 0 13.50 4.80 -11 0 0 19.50 6.70 11 0 0 15.50 4.60 -11 0 0 8.40 4.60 -11 0 0 16.60 5.10 11 0 0 8.70 6.40 11 0 0 12.80 4.00 -11 0 0 18.60 4.50 11 0 0 14.50 8.70 -12 0 0 820.22 50.19 -12 0 0 756.22 50.49 -12 0 0 799.82 47.80 -12 0 0 787.42 47.70 12 0 0 824.82 56.89 12 0 0 828.52 51.79 12 0 0 723.43 47.70 13 0 0 118.19 16.80 13 0 0 80.89 11.70 -13 0 0 109.19 14.90 -13 0 0 88.19 13.90 -13 0 0 107.89 11.20 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10.90 12 6 0 69.89 18.30 -13 -6 0 0.00 4.60 -13 -6 0 3.00 6.70 -13 -6 0 1.70 4.70 -13 -6 0 3.20 4.00 -13 -6 0 2.30 4.30 -13 6 0 -1.30 4.70 13 6 0 6.10 9.10 13 6 0 -5.90 7.70 -13 6 0 0.20 6.50 -14 -6 0 230.68 23.20 -14 -6 0 233.78 20.60 -14 -6 0 240.88 18.90 14 -6 0 222.58 16.80 -14 -6 0 231.88 17.40 -14 6 0 201.28 21.30 14 6 0 238.78 28.80 -14 6 0 262.77 20.70 -14 6 0 202.58 22.60 14 6 0 256.57 37.70 15 -6 0 70.29 10.20 -15 -6 0 76.99 14.70 -15 -6 0 102.99 13.40 -15 -6 0 83.39 13.70 15 6 0 58.99 18.70 -15 6 0 88.19 13.10 15 6 0 76.09 20.10 -15 6 0 75.69 13.60 -16 -6 0 242.98 20.00 -16 -6 0 241.68 22.00 -16 -6 0 241.78 22.40 -16 -6 0 220.18 24.40 -16 6 0 212.48 23.10 16 6 0 200.38 35.20 -16 6 0 250.77 21.20 16 6 0 234.78 28.50 -16 6 0 225.38 24.30 -17 -6 0 10.40 7.80 -17 -6 0 0.80 5.40 -17 -6 0 0.70 6.10 -17 6 0 8.60 8.30 17 6 0 -12.50 11.70 17 6 0 -0.10 10.80 -17 6 0 7.40 7.70 -18 -6 0 74.79 13.80 -18 -6 0 87.79 16.50 -18 -6 0 77.09 14.60 -18 -6 0 95.59 18.60 -18 6 0 107.69 20.00 18 6 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21.90 6.10 -5 -7 0 71.39 9.40 -5 -7 0 75.89 6.80 -5 -7 0 64.49 12.90 5 -7 0 86.19 14.10 -5 -7 0 89.09 14.90 5 -7 0 69.49 10.00 -5 -7 0 70.79 7.50 -5 7 0 59.49 11.90 -5 7 0 86.69 11.70 -5 7 0 72.69 8.60 5 7 0 64.29 13.30 5 7 0 76.49 6.90 -5 7 0 63.29 10.30 5 7 0 62.19 13.00 5 7 0 60.89 13.30 -6 -7 0 16.30 3.40 6 -7 0 19.20 5.50 -6 -7 0 10.60 7.20 -6 -7 0 7.70 6.10 -6 -7 0 27.90 8.80 -6 -7 0 20.40 4.60 6 -7 0 31.70 8.80 -6 7 0 10.60 4.00 -6 7 0 23.30 6.40 -6 7 0 17.20 6.30 6 7 0 14.60 8.60 6 7 0 2.30 7.70 -6 7 0 14.60 5.60 6 7 0 12.30 3.70 6 7 0 2.50 6.60 -7 -7 0 402.76 29.30 7 -7 0 404.56 31.50 -7 -7 0 404.16 24.90 -7 -7 0 445.36 25.10 -7 -7 0 383.56 26.90 7 -7 0 431.76 29.00 -7 -7 0 433.06 33.30 -7 -7 0 389.66 32.70 -7 7 0 456.45 31.00 7 7 0 387.46 35.30 7 7 0 420.16 25.80 -7 7 0 419.86 30.70 7 7 0 453.25 37.90 7 7 0 407.96 36.20 -7 7 0 402.86 25.20 -7 7 0 383.76 30.10 -8 -7 0 344.07 31.00 -8 -7 0 395.76 23.70 8 -7 0 422.86 28.30 -8 -7 0 370.36 29.10 -8 -7 0 386.86 26.50 -8 -7 0 373.46 31.80 -8 -7 0 402.26 24.00 -8 -7 0 390.66 27.50 -8 7 0 387.96 29.50 8 7 0 362.86 34.50 8 7 0 389.96 36.40 -8 7 0 449.36 30.30 8 7 0 349.27 34.30 -8 7 0 377.46 27.40 8 7 0 374.96 24.90 -9 -7 0 13.60 8.50 -9 -7 0 31.30 7.30 9 -7 0 20.00 6.60 -9 -7 0 29.20 7.00 -9 -7 0 25.50 4.10 -9 -7 0 19.20 4.70 -9 7 0 28.10 7.90 9 7 0 13.50 10.10 9 7 0 11.70 11.40 9 7 0 23.50 6.00 -9 7 0 36.50 8.10 9 7 0 15.00 9.50 -9 7 0 24.70 9.00 -10 -7 0 85.59 15.90 -10 -7 0 109.59 9.50 -10 -7 0 100.69 8.50 -10 -7 0 96.69 13.00 10 -7 0 103.79 14.10 -10 -7 0 103.99 12.20 -10 7 0 104.49 12.00 10 7 0 69.19 10.20 10 7 0 112.59 21.10 -10 7 0 119.29 17.00 -10 7 0 93.89 13.60 -10 7 0 75.69 14.00 10 7 0 77.39 18.00 -11 -7 0 59.29 13.60 -11 -7 0 76.79 11.60 -11 -7 0 69.89 8.40 -11 -7 0 98.69 11.30 -11 7 0 75.49 13.30 -11 7 0 70.59 13.50 11 7 0 52.39 11.10 11 7 0 81.49 19.30 11 7 0 61.49 17.40 -11 7 0 95.29 12.70 -11 7 0 63.79 11.00 -12 -7 0 39.80 9.20 -12 -7 0 50.29 12.50 -12 -7 0 30.70 7.40 -12 -7 0 37.80 6.70 -12 7 0 34.60 10.40 12 7 0 31.10 7.90 -12 7 0 51.19 11.70 -12 7 0 57.09 10.50 -12 7 0 46.70 9.20 12 7 0 13.10 8.40 12 7 0 33.30 12.90 -13 -7 0 42.00 9.60 -13 -7 0 46.50 11.30 -13 -7 0 51.79 8.70 -13 -7 0 60.29 13.20 -13 7 0 77.79 14.20 13 7 0 40.90 15.10 -13 7 0 52.79 10.00 -13 7 0 72.19 11.90 13 7 0 43.60 16.50 -13 7 0 51.59 11.70 -14 -7 0 12.50 6.40 -14 -7 0 6.30 4.90 -14 -7 0 5.00 5.00 -14 -7 0 12.60 9.80 -14 -7 0 5.20 6.20 14 7 0 -0.40 8.60 -14 7 0 0.20 5.70 14 7 0 27.70 10.90 -14 7 0 16.80 9.80 -14 7 0 14.90 10.40 -14 7 0 1.80 4.90 -15 -7 0 21.10 7.80 -15 -7 0 -0.70 10.30 -15 -7 0 14.20 9.00 -15 -7 0 7.10 7.30 -15 -7 0 0.40 5.10 -15 7 0 1.80 4.60 15 7 0 2.70 8.40 15 7 0 4.90 11.90 -15 7 0 19.90 9.90 -16 -7 0 28.20 8.80 -16 -7 0 12.50 8.50 -16 -7 0 33.10 8.20 -16 -7 0 14.50 8.70 16 7 0 69.59 20.40 -16 7 0 3.70 8.40 16 7 0 11.70 16.90 -17 -7 0 4.00 7.50 -17 -7 0 5.40 5.80 -17 -7 0 6.70 7.50 -17 -7 0 2.50 7.90 17 7 0 7.60 14.90 -17 7 0 7.30 9.10 17 7 0 12.10 14.40 -17 7 0 10.00 6.90 -17 7 0 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93.99 10.50 -1 8 0 93.89 9.50 -1 8 0 127.79 19.00 -1 8 0 91.39 13.90 2 -8 0 -1.90 4.20 2 -8 0 -1.40 3.40 -2 -8 0 4.40 5.50 -2 -8 0 2.80 2.50 -2 8 0 4.40 3.90 -2 8 0 2.30 2.90 2 8 0 1.20 2.00 2 8 0 -0.80 5.30 -2 8 0 -0.90 3.20 2 8 0 -9.40 4.40 -2 8 0 0.70 3.30 -2 8 0 5.40 5.40 -2 8 0 1.90 5.40 2 8 0 -2.10 5.90 -2 8 0 0.60 2.60 -2 8 0 4.10 2.80 3 -8 0 58.19 12.20 -3 -8 0 62.99 6.70 3 -8 0 50.59 9.40 -3 -8 0 67.69 14.00 3 8 0 57.09 13.70 -3 8 0 52.99 8.80 -3 8 0 56.59 11.30 3 8 0 66.09 13.00 -3 8 0 48.80 7.70 -3 8 0 56.39 7.50 3 8 0 69.69 13.60 4 -8 0 28.10 9.80 4 -8 0 11.60 4.50 -4 -8 0 26.70 10.30 -4 -8 0 14.30 3.80 -4 8 0 10.60 6.50 4 8 0 29.80 10.00 -4 8 0 17.10 6.30 -4 8 0 11.00 5.30 4 8 0 0.30 7.40 4 8 0 7.40 7.20 -4 8 0 15.80 6.50 5 -8 0 -3.70 3.60 5 -8 0 3.00 6.70 -5 -8 0 -1.40 2.30 -5 -8 0 1.30 2.40 -5 -8 0 6.40 3.20 -5 -8 0 -5.50 6.30 -5 8 0 -2.00 3.90 -5 8 0 0.70 1.30 -5 8 0 -4.70 4.50 -5 8 0 -5.30 3.60 -5 8 0 2.70 4.40 5 8 0 2.60 5.80 5 8 0 23.10 9.40 5 8 0 -1.00 5.20 -6 -8 0 103.59 9.20 6 -8 0 114.39 16.60 -6 -8 0 81.29 15.10 -6 -8 0 92.19 8.20 6 -8 0 95.79 11.20 -6 -8 0 82.69 10.70 6 8 0 65.29 16.50 6 8 0 83.09 7.90 6 8 0 109.39 18.80 -6 8 0 99.09 15.60 -6 8 0 92.59 10.50 -6 8 0 106.19 11.90 6 8 0 73.19 16.00 -6 8 0 105.89 14.20 -7 -8 0 67.29 8.90 -7 -8 0 51.79 10.00 -7 -8 0 74.19 7.20 -7 -8 0 74.39 14.80 7 -8 0 82.89 15.10 7 -8 0 103.09 13.00 -7 8 0 70.19 11.30 7 8 0 82.29 7.90 -7 8 0 72.99 8.60 -7 8 0 77.59 13.60 -7 8 0 113.99 15.20 7 8 0 73.19 16.30 7 8 0 78.79 15.00 7 8 0 74.29 16.90 -8 -8 0 139.19 20.80 8 -8 0 169.48 19.90 -8 -8 0 161.38 11.60 8 -8 0 170.98 15.80 -8 8 0 161.78 17.30 -8 8 0 172.38 17.50 -8 8 0 181.28 16.30 8 8 0 141.49 23.90 8 8 0 152.08 24.30 -8 8 0 157.18 10.70 8 8 0 137.49 12.40 -9 -8 0 45.00 11.70 -9 -8 0 52.99 6.00 9 -8 0 69.89 11.40 -9 -8 0 56.89 6.40 -9 -8 0 48.50 8.70 -9 -8 0 29.80 11.60 9 8 0 54.79 8.00 -9 8 0 56.89 10.40 -9 8 0 52.79 10.80 9 8 0 29.10 12.80 -9 8 0 54.49 11.20 9 8 0 40.10 12.40 9 8 0 45.80 14.60 -10 -8 0 4.70 3.50 -10 -8 0 4.90 2.80 -10 -8 0 2.10 4.70 10 -8 0 4.10 4.70 -10 -8 0 9.00 7.90 -10 8 0 -3.50 5.00 10 8 0 -7.00 4.60 -10 8 0 2.00 5.20 10 8 0 -3.00 9.40 -10 8 0 1.20 4.50 -11 -8 0 98.19 8.60 -11 -8 0 106.99 9.70 -11 -8 0 96.19 18.60 -11 -8 0 92.79 13.00 -11 -8 0 110.29 14.60 -11 8 0 92.99 14.10 -11 8 0 124.89 18.60 -11 8 0 91.99 14.30 11 8 0 85.19 12.00 11 8 0 105.79 21.20 11 8 0 93.99 22.90 -12 -8 0 13.00 7.30 -12 -8 0 19.50 4.30 -12 -8 0 38.40 12.40 -12 -8 0 29.40 5.90 -12 -8 0 40.30 9.10 -12 8 0 31.10 8.60 12 8 0 42.30 15.40 12 8 0 46.30 9.30 12 8 0 24.80 13.70 -12 8 0 40.30 8.80 -12 8 0 30.00 9.60 -13 -8 0 10.40 6.10 -13 -8 0 2.40 4.90 -13 -8 0 10.10 9.30 -13 -8 0 -3.20 2.70 -13 -8 0 4.20 6.40 13 8 0 -6.80 10.60 -13 8 0 6.00 5.00 13 8 0 14.60 8.60 13 8 0 9.00 11.50 -13 8 0 16.80 7.80 -13 8 0 20.70 9.70 -14 -8 0 23.10 11.80 -14 -8 0 7.40 4.70 -14 -8 0 9.80 6.80 -14 -8 0 18.60 9.00 14 8 0 17.40 11.20 -14 8 0 16.20 6.80 14 8 0 -0.80 12.50 -14 8 0 22.50 10.00 -14 8 0 18.30 7.90 -15 -8 0 9.20 5.90 -15 -8 0 3.30 6.90 -15 -8 0 -4.60 3.30 -15 -8 0 4.50 4.90 -15 -8 0 7.70 8.30 -15 8 0 2.70 6.40 15 8 0 -13.30 11.00 15 8 0 -1.00 15.60 -15 8 0 -3.40 7.90 -16 -8 0 17.30 8.60 -16 -8 0 10.30 5.70 -16 -8 0 21.60 11.90 -16 -8 0 10.50 8.40 -16 8 0 9.40 6.80 -16 8 0 24.10 10.90 16 8 0 -20.20 11.90 -16 8 0 13.10 7.70 16 8 0 13.90 14.60 -17 -8 0 -0.70 7.60 -17 -8 0 8.70 6.50 -17 -8 0 30.40 11.70 -17 -8 0 15.00 9.90 -17 8 0 5.80 8.30 -17 8 0 5.20 6.90 17 8 0 13.70 18.00 17 8 0 -15.90 12.50 -17 8 0 21.60 11.30 -18 -8 0 166.18 23.00 -18 -8 0 133.89 24.20 -18 8 0 142.29 19.30 18 8 0 139.29 28.70 -18 8 0 171.18 25.60 18 8 0 146.99 33.20 -19 -8 0 8.50 10.60 -19 -8 0 23.10 13.90 19 8 0 -9.60 14.50 -19 8 0 14.00 10.60 19 8 0 50.69 23.20 -19 8 0 12.10 8.40 -20 -8 0 6.30 9.90 -20 -8 0 0.20 10.90 -20 8 0 -7.50 11.40 -20 8 0 7.70 9.30 -21 -8 0 -5.40 15.00 -21 8 0 0.50 9.70 0 -9 0 6.00 6.00 0 -9 0 0.10 3.20 0 9 0 -0.30 6.90 0 9 0 5.40 5.10 0 9 0 3.40 2.50 0 9 0 -0.10 4.80 0 9 0 3.40 3.60 -1 -9 0 13.90 4.50 -1 -9 0 14.90 8.30 1 -9 0 20.50 9.60 1 9 0 14.40 3.40 -1 9 0 11.60 4.70 -1 9 0 9.40 4.20 1 9 0 9.80 6.50 -1 9 0 17.00 4.00 -1 9 0 18.50 5.40 -1 9 0 16.30 4.90 1 9 0 21.00 7.20 1 9 0 20.30 11.30 -1 9 0 17.80 7.80 2 -9 0 25.00 9.60 -2 -9 0 25.80 5.50 -2 -9 0 28.10 10.40 2 -9 0 27.50 6.70 -2 9 0 24.40 5.00 -2 9 0 27.20 4.00 2 9 0 29.00 5.60 -2 9 0 21.90 6.60 -2 9 0 31.10 4.10 2 9 0 32.60 9.90 2 9 0 29.90 10.00 -2 9 0 59.29 13.40 2 9 0 40.80 12.80 -3 -9 0 17.50 4.20 3 -9 0 16.20 5.60 -3 -9 0 11.20 9.00 3 -9 0 16.80 8.20 -3 9 0 14.90 4.40 3 9 0 13.90 8.80 -3 9 0 7.70 6.80 -3 9 0 16.50 6.00 3 9 0 28.10 10.30 -3 9 0 16.10 7.20 3 9 0 10.10 7.60 -4 -9 0 12.10 7.40 -4 -9 0 10.00 3.30 4 -9 0 11.70 7.70 4 -9 0 5.80 5.20 4 9 0 8.70 3.10 -4 9 0 12.20 4.70 4 9 0 7.70 9.40 4 9 0 1.00 7.50 -4 9 0 -4.20 5.70 -4 9 0 0.10 4.00 -4 9 0 17.80 5.60 4 9 0 16.60 9.20 -4 9 0 10.90 7.40 -5 -9 0 5.40 3.20 5 -9 0 13.00 5.60 -5 -9 0 20.90 9.60 5 -9 0 11.50 8.30 -5 9 0 9.20 4.90 5 9 0 5.00 8.60 5 9 0 10.10 9.00 -5 9 0 8.30 7.20 5 9 0 13.30 3.10 -5 9 0 2.20 6.30 5 9 0 16.40 10.00 6 -9 0 77.69 11.50 6 -9 0 58.39 14.20 -6 -9 0 60.79 6.80 -6 -9 0 64.79 13.70 6 9 0 49.40 14.80 -6 9 0 70.19 11.10 -6 9 0 81.39 12.60 6 9 0 66.99 15.90 -6 9 0 42.90 9.00 -6 9 0 82.99 14.90 6 9 0 51.99 13.20 -7 -9 0 300.57 22.00 7 -9 0 339.07 25.10 7 -9 0 333.27 29.50 -7 -9 0 320.77 20.20 -7 -9 0 319.97 20.80 7 9 0 281.17 32.50 -7 9 0 366.36 26.40 7 9 0 346.27 33.70 -7 9 0 276.77 21.60 -7 9 0 308.87 24.80 -7 9 0 308.87 27.40 7 9 0 356.46 39.20 -8 -9 0 43.90 9.90 -8 -9 0 62.39 14.80 8 -9 0 55.39 13.30 -8 -9 0 52.69 6.50 8 -9 0 48.20 9.80 -8 -9 0 47.60 7.70 8 9 0 45.40 14.60 -8 9 0 56.49 10.60 8 9 0 72.79 7.00 -8 9 0 64.19 11.50 -8 9 0 70.99 13.20 8 9 0 54.69 18.60 -9 -9 0 158.88 18.50 -9 -9 0 149.79 22.80 -9 -9 0 168.88 15.40 9 -9 0 205.38 18.10 9 9 0 158.68 25.50 9 9 0 151.78 12.90 -9 9 0 181.58 19.40 9 9 0 167.08 27.50 -9 9 0 187.08 19.00 -9 9 0 171.38 17.00 9 9 0 144.59 25.60 -10 -9 0 10.60 6.10 -10 -9 0 4.80 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79.19 10.90 3 -10 0 85.19 20.70 3 10 0 69.49 5.30 -3 10 0 93.59 17.00 3 10 0 74.69 16.70 3 10 0 80.49 15.60 3 10 0 68.89 14.00 -3 10 0 67.79 9.10 -3 10 0 68.09 10.60 -4 -10 0 174.38 14.10 4 -10 0 202.88 17.70 4 -10 0 198.88 22.70 -4 -10 0 193.38 27.00 4 10 0 159.48 34.30 4 10 0 211.68 24.50 -4 10 0 206.88 23.00 -4 10 0 207.08 17.60 -4 10 0 169.78 18.00 4 10 0 182.48 32.40 -4 10 0 204.38 15.50 -5 -10 0 -7.80 6.90 5 -10 0 5.10 8.00 5 -10 0 -1.60 4.80 -5 -10 0 -1.80 2.60 5 10 0 3.30 8.10 -5 10 0 -14.50 7.40 -5 10 0 8.00 5.70 -5 10 0 10.10 6.30 5 10 0 -6.30 9.00 5 10 0 -18.70 9.90 -5 10 0 2.50 7.30 6 -10 0 58.89 14.40 -6 -10 0 94.39 18.20 6 -10 0 69.59 11.10 6 10 0 56.69 16.20 6 10 0 58.19 16.50 6 10 0 74.79 17.60 -6 10 0 63.29 11.80 -6 10 0 63.99 14.60 -6 10 0 73.49 11.60 7 -10 0 71.59 15.70 7 -10 0 74.09 12.00 -7 -10 0 85.19 17.90 7 10 0 48.60 14.50 -7 10 0 43.60 10.40 7 10 0 45.70 15.50 -7 10 0 47.10 12.10 -7 10 0 66.39 11.50 -7 10 0 74.09 12.40 7 10 0 39.70 18.40 -8 -10 0 14.10 10.30 8 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131.49 31.40 14 10 0 140.79 30.50 -15 -10 0 -0.90 10.60 15 10 0 49.20 22.20 15 10 0 9.20 16.60 -15 10 0 14.80 8.90 -16 -10 0 11.80 12.10 -16 -10 0 8.60 13.30 -16 10 0 9.50 10.60 -16 10 0 4.20 7.60 -17 -10 0 76.69 21.10 -17 -10 0 27.40 14.50 -17 10 0 10.70 10.40 -17 10 0 38.80 15.30 -18 -10 0 7.60 14.90 -18 10 0 4.10 8.80 -18 10 0 -14.10 15.40 -19 -10 0 12.40 16.40 -19 10 0 3.40 10.90 0 -11 0 7.20 4.90 0 -11 0 -1.70 8.80 0 11 0 -7.20 2.90 0 11 0 -2.20 5.40 0 11 0 9.90 8.20 0 11 0 2.90 5.50 1 -11 0 8.70 5.60 -1 -11 0 9.60 9.80 1 -11 0 19.90 10.90 -1 -11 0 7.40 4.60 -1 11 0 20.10 12.80 -1 11 0 12.70 4.90 1 11 0 8.00 9.60 1 11 0 11.60 7.40 -2 -11 0 17.60 8.00 2 -11 0 39.00 8.20 2 -11 0 28.20 11.40 2 11 0 36.30 13.20 2 11 0 60.19 12.70 2 11 0 32.80 9.90 -2 11 0 45.60 6.90 3 -11 0 9.30 10.80 3 -11 0 8.00 6.20 -3 -11 0 -1.40 8.70 3 11 0 6.20 10.70 -3 11 0 11.90 6.10 3 11 0 9.10 10.60 -3 11 0 11.80 7.10 -3 11 0 18.70 10.40 -4 -11 0 126.79 23.30 4 -11 0 118.69 13.50 4 -11 0 90.69 18.80 -4 11 0 118.69 19.90 4 11 0 118.19 23.60 -4 11 0 92.29 15.20 4 11 0 112.79 20.20 5 -11 0 82.89 18.30 5 -11 0 76.89 11.90 -5 -11 0 76.29 17.60 5 11 0 70.59 16.90 5 11 0 95.69 21.80 -5 11 0 60.89 11.10 -5 11 0 70.19 15.80 -5 11 0 60.89 10.50 -6 -11 0 19.10 13.40 6 -11 0 34.30 8.90 6 -11 0 33.10 14.00 -6 11 0 49.90 10.60 6 11 0 38.60 13.70 6 11 0 29.10 14.30 -6 11 0 24.50 7.90 -6 11 0 51.19 13.30 7 -11 0 28.40 10.90 -7 -11 0 29.80 14.50 -7 11 0 21.80 8.50 -7 11 0 32.40 10.30 -7 11 0 32.40 9.00 7 11 0 -8.60 10.70 7 11 0 34.10 15.20 8 -11 0 -6.60 8.30 -8 -11 0 7.70 10.90 -8 11 0 -3.20 6.50 -8 11 0 15.40 7.80 8 11 0 -15.40 10.50 -8 11 0 13.20 9.10 8 11 0 -4.90 11.20 -9 -11 0 35.60 14.00 -9 11 0 79.49 17.10 -9 11 0 47.60 11.90 9 11 0 75.79 23.00 -9 11 0 55.69 10.70 9 11 0 46.70 17.90 -10 -11 0 64.29 16.40 10 11 0 39.60 18.80 -10 11 0 16.50 9.70 10 11 0 35.20 16.50 -10 11 0 52.59 13.10 -11 11 0 12.50 10.90 11 11 0 9.60 18.70 -11 11 0 6.00 8.80 11 11 0 30.10 17.20 -11 11 0 16.30 8.80 -12 -11 0 18.80 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8.60 -2 13 0 -10.60 14.20 2 13 0 -2.90 8.70 2 13 0 9.00 14.80 3 -13 0 2.90 13.50 -3 -13 0 19.60 13.60 -3 13 0 -11.50 8.30 3 13 0 -1.90 9.90 -3 13 0 10.80 15.20 -4 -13 0 10.20 13.30 4 -13 0 22.90 14.90 -4 13 0 -24.90 12.70 -4 13 0 3.40 9.10 4 13 0 -9.90 14.40 4 13 0 -8.40 11.60 -5 -13 0 24.90 18.20 5 -13 0 33.60 17.00 -5 13 0 2.50 9.70 5 13 0 23.10 15.00 -5 13 0 26.70 16.30 5 13 0 53.69 20.60 6 -13 0 -7.80 15.00 -6 13 0 -15.60 13.70 -6 13 0 2.60 9.40 6 13 0 -20.20 14.30 7 -13 0 84.19 21.20 7 13 0 90.19 23.50 -7 13 0 60.29 13.50 -7 13 0 46.30 17.40 -8 13 0 -26.20 13.40 8 13 0 4.30 17.40 -8 13 0 21.60 16.40 0 14 0 7.60 19.80 1 14 0 -22.00 18.90 -1 14 0 2.70 15.50 -2 14 0 11.20 17.10 -3 14 0 -1.20 19.70 4 14 0 8.70 15.40 -4 14 0 -21.50 17.40 -5 14 0 -32.60 18.80 5 14 0 -30.90 15.30 6 14 0 -17.80 18.40 25 0 -1 -17.20 27.50 24 0 -1 -3.80 16.50 -24 0 1 11.10 10.70 24 0 -1 -15.90 23.10 -24 0 1 -7.20 8.10 -23 0 1 11.70 7.90 23 0 -1 20.20 20.20 23 0 -1 -14.00 12.10 -23 0 1 4.90 7.80 -22 0 1 6.90 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4 13.40 11.80 -10 -10 4 -5.20 5.30 -10 -10 4 -1.40 4.00 -10 10 4 11.40 7.30 -10 10 4 2.10 10.20 -10 10 4 9.70 5.10 10 10 -4 13.10 14.50 10 10 -4 6.40 11.10 -9 -10 4 69.79 15.40 9 -10 -4 90.69 18.60 -9 -10 4 81.89 10.70 -9 10 4 81.19 11.10 9 10 -4 79.59 21.10 9 10 -4 64.29 20.80 -9 10 4 91.29 12.70 -9 10 4 83.09 18.00 -8 -10 4 65.29 15.40 -8 -10 4 75.49 10.30 8 -10 -4 83.49 16.00 -8 10 4 49.30 8.40 -8 10 4 71.49 17.10 8 10 -4 65.49 17.70 -8 10 4 39.10 8.80 -8 10 4 59.29 6.80 8 10 -4 80.99 19.70 -7 -10 4 20.30 6.40 -7 -10 4 20.70 10.20 7 -10 -4 18.30 11.20 7 10 -4 30.00 13.60 -7 10 4 32.20 10.50 7 10 -4 9.40 11.20 -7 10 4 20.20 4.80 -7 10 4 26.30 6.90 -6 -10 4 133.39 21.30 6 -10 -4 143.49 20.80 -6 -10 4 153.28 13.50 -6 10 4 143.39 13.40 -6 10 4 146.29 23.50 -6 10 4 111.49 11.70 -6 10 4 116.79 11.60 -6 10 4 88.69 15.40 6 10 -4 144.79 25.40 6 10 -4 118.99 20.20 -6 10 4 106.09 11.00 6 10 -4 137.99 23.20 6 10 -4 95.19 12.10 5 -10 -4 7.50 8.00 -5 -10 4 12.60 4.70 -5 -10 4 4.10 6.80 -5 10 4 7.70 3.60 -5 10 4 12.70 8.00 -5 10 4 4.50 5.00 5 10 -4 22.90 12.80 5 10 -4 2.50 10.50 5 10 -4 0.30 5.20 -5 10 4 1.70 5.10 -5 10 4 6.00 3.90 4 -10 -4 31.10 13.60 -4 -10 4 22.80 11.10 -4 -10 4 29.40 7.10 -4 10 4 52.49 14.50 4 10 -4 35.00 7.00 4 10 -4 47.10 14.50 4 10 -4 50.09 13.40 4 10 -4 41.00 13.40 -4 10 4 24.60 4.30 -4 10 4 25.80 4.70 -4 10 4 14.80 6.80 -4 10 4 30.40 6.30 3 -10 -4 -4.00 5.90 -3 -10 4 8.60 8.60 -3 -10 4 -2.70 4.10 3 10 -4 9.90 5.10 -3 10 4 2.50 1.90 3 10 -4 -6.10 7.00 3 10 -4 4.30 8.20 -3 10 4 10.60 4.70 3 10 -4 0.80 8.20 -3 10 4 1.90 4.20 -3 10 4 2.40 8.20 -3 10 4 4.60 4.80 -2 -10 4 34.70 7.60 -2 -10 4 30.90 11.20 2 -10 -4 19.30 9.30 2 10 -4 28.20 6.40 -2 10 4 7.70 9.60 2 10 -4 14.30 11.20 2 10 -4 26.80 9.90 -2 10 4 15.50 5.10 -2 10 4 16.30 4.50 2 10 -4 22.50 9.20 -2 10 4 28.90 5.50 -1 -10 4 16.40 6.30 1 -10 -4 17.00 8.20 -1 -10 4 6.40 7.60 1 -10 -4 11.10 8.40 1 10 -4 15.50 7.00 -1 10 4 13.90 10.30 -1 10 4 19.50 6.40 1 10 -4 11.30 7.10 1 10 -4 12.60 5.20 -1 10 4 4.70 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4 -11.20 8.40 -5 10 -4 10.00 5.90 -5 10 -4 1.90 6.50 5 10 4 -8.20 7.40 -5 10 -4 5.00 4.30 -5 10 -4 9.50 7.60 -5 10 -4 3.90 7.80 5 10 4 3.80 13.00 -6 -10 -4 5.80 9.10 6 -10 4 7.00 5.30 -6 -10 -4 8.20 8.90 -6 10 -4 13.40 7.00 -6 10 -4 3.70 6.50 -6 10 -4 16.20 8.50 6 10 4 -0.80 9.50 6 10 4 18.90 12.50 -7 -10 -4 21.00 12.20 7 -10 4 18.70 7.60 -7 -10 -4 10.10 11.10 -7 10 -4 24.50 8.30 -7 10 -4 33.80 11.10 -7 10 -4 22.20 9.40 7 10 4 16.00 11.50 7 10 4 24.80 14.90 -8 -10 -4 42.70 14.20 8 -10 4 36.90 10.00 -8 -10 -4 48.30 15.20 -8 10 -4 55.09 12.70 -8 10 -4 49.40 11.50 -8 10 -4 51.79 12.20 8 10 4 53.99 16.90 8 10 4 32.10 15.20 -9 -10 -4 20.10 12.40 9 -10 4 5.10 7.10 -9 -10 -4 -0.40 9.50 -9 10 -4 8.20 8.10 9 10 4 16.80 15.70 9 10 4 12.90 13.60 10 -10 4 36.20 10.50 -10 -10 -4 79.59 18.40 -10 -10 -4 40.60 16.00 10 10 4 56.09 18.80 10 10 4 41.10 17.10 -10 10 -4 43.00 13.90 -10 10 -4 54.49 10.40 -10 10 -4 40.50 9.60 -11 -10 -4 3.80 10.40 -11 -10 -4 1.80 6.60 11 -10 4 11.30 8.10 -11 -10 -4 -6.40 10.50 11 10 4 16.90 16.70 11 10 4 4.10 13.10 -11 10 -4 -1.30 7.10 -11 10 -4 8.30 9.60 -11 10 -4 1.40 10.60 -12 -10 -4 -8.40 6.50 -12 -10 -4 11.70 13.00 12 -10 4 -2.60 6.60 -12 10 -4 -5.70 10.10 12 10 4 -12.40 13.70 12 10 4 0.50 13.00 -12 10 -4 4.70 7.70 13 -10 4 -4.70 7.30 13 10 4 13.50 15.90 -13 10 -4 -3.50 9.30 13 10 4 11.50 14.40 -13 10 -4 -17.00 9.40 -14 -10 -4 -0.90 8.80 -14 -10 -4 49.70 15.70 14 10 4 3.20 16.90 -14 10 -4 -2.10 11.00 -14 10 -4 13.50 9.50 14 10 4 -3.70 15.30 -15 -10 -4 56.19 13.30 -15 -10 -4 67.29 20.80 15 10 4 60.79 24.70 -15 10 -4 52.19 14.10 15 10 4 37.50 21.70 -16 -10 -4 16.40 13.10 -16 10 -4 34.00 14.20 -17 -10 -4 -26.70 12.80 -17 10 -4 -12.30 9.20 -18 -10 -4 -15.70 15.10 -17 11 4 -11.40 12.60 -15 -11 4 141.49 25.70 -15 11 4 231.18 24.80 -14 -11 4 -3.60 13.10 -14 11 4 -4.20 9.00 -14 11 4 -1.40 11.50 -13 -11 4 91.69 20.80 13 11 -4 116.39 28.70 -13 11 4 87.29 15.50 13 11 -4 86.09 23.30 -13 11 4 115.69 21.00 12 11 -4 73.29 23.50 -12 11 4 81.59 13.20 12 11 -4 83.49 24.30 -12 11 4 78.09 18.30 -11 -11 4 0.90 6.20 -11 -11 4 15.50 12.60 -11 11 4 9.40 6.00 -11 11 4 14.30 8.00 -11 11 4 12.00 11.70 -10 -11 4 76.69 18.30 10 11 -4 63.39 23.30 -10 11 4 63.99 10.90 -10 11 4 57.79 16.30 -10 11 4 42.70 8.60 10 11 -4 67.19 18.40 -9 -11 4 150.58 25.70 9 -11 -4 96.69 19.00 -9 11 4 131.39 13.90 -9 11 4 107.69 12.90 9 11 -4 90.69 22.80 9 11 -4 150.38 29.10 -9 11 4 148.29 23.20 8 -11 -4 83.39 17.90 -8 -11 4 64.29 16.70 -8 11 4 61.19 16.60 8 11 -4 73.99 19.70 8 11 -4 66.29 16.90 -8 11 4 70.79 9.90 -8 11 4 65.69 9.80 -7 -11 4 180.28 27.60 -7 11 4 227.28 26.30 -7 11 4 199.68 17.20 7 11 -4 224.18 33.90 7 11 -4 204.28 30.20 6 -11 -4 13.10 10.40 -6 -11 4 13.60 12.00 6 11 -4 9.20 10.70 6 11 -4 16.10 12.90 -6 11 4 12.70 10.30 -6 11 4 14.80 6.00 -6 11 4 13.30 5.00 -5 -11 4 336.07 31.30 5 -11 -4 176.78 27.10 -5 -11 4 250.87 20.40 5 11 -4 265.67 28.80 -5 11 4 228.78 16.10 -5 11 4 259.07 28.10 -5 11 4 248.38 20.50 5 11 -4 267.07 36.80 4 -11 -4 97.29 18.20 -4 -11 4 89.19 18.40 -4 -11 4 95.79 12.40 -4 11 4 92.79 20.20 4 11 -4 96.69 19.40 -4 11 4 71.29 11.20 4 11 -4 96.29 21.80 3 -11 -4 107.19 20.30 -3 -11 4 123.29 13.10 -3 -11 4 80.69 19.50 3 11 -4 95.39 16.90 3 11 -4 91.09 21.60 -3 11 4 84.79 19.20 -3 11 4 97.89 13.30 -2 -11 4 1.20 9.60 -2 -11 4 17.30 7.10 2 -11 -4 27.00 11.90 2 11 -4 3.50 8.90 -2 11 4 10.00 8.60 2 11 -4 0.10 8.30 1 -11 -4 50.19 15.70 -1 -11 4 60.49 10.50 -1 -11 4 80.79 17.10 1 11 -4 69.99 13.30 -1 11 4 64.19 9.10 -1 11 4 58.19 16.10 1 11 -4 60.29 11.00 -1 11 4 52.59 8.50 0 -11 4 20.70 11.00 0 -11 4 17.00 7.20 0 -11 -4 2.10 9.50 0 11 4 56.39 16.10 0 11 4 15.80 7.20 0 11 4 1.50 6.60 0 11 -4 17.30 11.00 0 11 -4 7.30 6.60 1 -11 4 -5.60 7.30 1 -11 4 4.20 5.70 -1 -11 -4 4.60 8.80 1 11 4 -3.50 7.90 -1 11 -4 7.90 4.50 1 11 4 -0.60 7.80 1 11 4 -9.70 8.70 -1 11 -4 6.50 9.40 -1 11 -4 6.40 4.70 -2 -11 -4 12.50 10.10 -2 -11 -4 20.80 9.30 2 -11 4 3.20 5.90 2 -11 4 -8.20 9.30 -2 11 -4 12.10 9.70 2 11 4 4.60 10.00 2 11 4 -3.40 9.20 -3 -11 -4 16.90 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11.60 -9 -9 -12 12.30 11.40 -9 -9 -12 8.40 5.90 9 9 12 18.70 11.30 -9 9 -12 9.70 10.80 -9 9 -12 19.40 9.20 9 9 12 24.90 15.40 -10 -9 -12 -20.10 12.00 -10 -9 -12 9.40 7.00 10 -9 12 -3.20 7.40 -10 -9 -12 -10.00 11.50 -10 -9 -12 3.30 13.40 10 9 12 -1.80 25.80 -10 9 -12 0.10 8.70 -10 9 -12 -10.70 7.90 10 9 12 15.00 14.30 -11 -9 -12 18.70 12.90 -11 -9 -12 33.70 15.30 11 -9 12 1.30 8.60 -11 -9 -12 7.80 7.50 11 9 12 2.00 17.10 -11 9 -12 20.70 9.30 -12 -9 -12 229.98 20.70 12 -9 12 164.48 24.50 -12 -9 -12 186.78 29.60 -12 -9 -12 253.47 34.10 12 9 12 198.88 31.00 -12 9 -12 209.38 30.30 -12 9 -12 227.58 20.80 -12 9 -12 189.68 26.40 12 9 12 150.18 34.20 -13 -9 -12 7.60 9.70 -13 -9 -12 21.20 14.50 -13 -9 -12 15.80 17.20 13 -9 12 27.80 12.80 -13 9 -12 29.30 12.40 -13 9 -12 16.60 16.20 13 9 12 2.50 22.10 13 9 12 0.70 15.80 -14 -9 -12 -2.20 9.50 14 9 12 -1.40 36.20 -16 -9 -12 6.20 11.10 -18 -10 12 59.29 21.10 -17 -10 12 -8.30 12.70 -17 -10 12 -0.70 14.50 -17 -10 12 7.20 19.10 -17 -10 12 13.60 19.10 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282.87 27.30 9 -4 -22 281.87 34.10 9 4 -22 233.38 37.60 -9 4 22 280.77 30.30 9 4 -22 359.46 52.79 8 -4 -22 -1.30 6.20 -8 -4 22 7.80 7.70 -8 -4 22 6.40 7.70 8 -4 -22 0.00 17.80 8 -4 -22 -12.70 10.10 -8 -4 22 0.50 11.60 -8 4 22 17.90 10.80 8 4 -22 -20.90 13.50 8 4 -22 19.60 15.20 -8 4 22 9.20 5.60 -7 -4 22 14.00 8.30 7 -4 -22 27.40 12.90 7 -4 -22 -9.40 6.50 -7 -4 22 12.50 9.90 7 -4 -22 21.20 19.40 7 4 -22 15.60 14.30 -7 4 22 14.50 9.70 -7 4 22 9.40 5.80 7 4 -22 -5.20 16.10 -6 -4 22 61.79 12.90 6 -4 -22 46.60 14.50 6 -4 -22 64.89 20.80 -6 -4 22 52.29 15.50 6 -4 -22 75.99 13.30 6 4 -22 56.39 23.50 -6 4 22 69.59 18.00 6 4 -22 101.99 24.40 5 -4 -22 61.39 14.20 -5 -4 22 112.49 16.00 -5 -4 22 61.79 15.60 5 -4 -22 85.59 27.40 5 -4 -22 94.49 19.80 5 4 -22 55.79 21.00 -5 4 22 54.79 15.20 5 4 -22 71.59 19.70 -4 -4 22 4.30 6.50 4 -4 -22 8.10 12.10 4 -4 -22 -11.20 13.20 -4 -4 22 18.00 11.70 4 -4 -22 4.00 8.80 -4 4 22 19.10 6.20 4 4 -22 7.80 13.70 -4 4 22 8.90 9.00 4 4 -22 -0.70 15.50 3 -4 -22 4.50 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-4 2 -28 5.50 15.60 9 3 -28 6.10 19.00 -8 3 28 1.60 9.40 8 3 -28 -17.70 16.50 7 3 -28 3.70 19.50 -7 3 28 -8.30 8.80 -6 3 28 -4.50 7.80 4 -3 -28 -13.90 16.10 4 -3 -28 5.70 31.60 -4 3 28 6.50 7.90 4 3 -28 -1.30 15.30 3 -3 -28 107.39 38.60 3 3 -28 69.39 21.10 -3 3 28 91.19 14.60 2 -3 -28 21.10 31.00 -2 3 28 -8.90 8.40 -2 3 28 5.10 17.60 2 3 -28 -20.10 14.20 1 -3 -28 -34.90 28.20 -1 3 28 17.40 10.00 -1 3 28 6.10 18.20 1 3 -28 -12.70 12.70 0 -3 -28 -33.00 25.90 0 3 28 -11.10 18.60 0 3 -28 2.20 14.40 -1 -3 -28 5.60 28.20 -1 3 -28 57.99 17.40 1 3 28 24.30 20.60 2 3 28 33.20 21.10 -2 3 -28 24.20 16.70 3 3 28 -45.60 18.90 4 3 28 -20.20 22.20 -8 4 28 15.70 10.10 -7 4 28 -8.20 9.20 7 4 -28 10.00 21.10 6 -4 -28 14.20 36.50 -6 4 28 -9.20 10.60 6 4 -28 9.30 17.70 5 4 -28 -1.10 16.90 -5 4 28 10.40 9.60 4 4 -28 28.70 18.10 3 -4 -28 -30.00 16.80 3 -4 -28 32.90 49.50 3 4 -28 3.10 16.70 2 -4 -28 19.30 37.40 2 4 -28 8.90 16.70 1 -4 -28 6.50 33.00 1 -4 -28 2.10 15.50 0 -4 -28 20.50 17.70 0 -4 -28 87.39 38.40 -1 -4 -28 61.39 36.50 2 -5 -28 -26.40 20.40 1 -5 -28 -16.30 42.70 1 -5 -28 37.80 21.90 0 -5 28 12.20 30.70 0 -5 -28 -52.99 35.90 1 -5 28 -20.60 26.70 -1 -5 -28 -20.20 36.60 -1 0 29 -0.60 10.50 0 0 29 -5.30 21.10 0 0 29 -7.70 11.20 -4 1 29 8.40 9.80 -3 1 29 -11.20 10.80 -2 1 29 -8.40 9.60 -1 1 29 2.40 10.70 0 1 29 6.80 10.20 0 1 -29 -13.30 16.40 0 1 29 4.70 24.60 1 1 29 5.40 8.90 -2 1 -29 -28.90 15.10 2 1 29 16.50 11.60 -3 1 -29 35.00 19.80 3 1 29 58.39 14.60 -4 1 -29 12.90 17.70 9 -2 -29 -37.30 46.00 8 -2 -29 -26.10 45.30 7 -2 -29 13.50 35.40 6 -2 -29 -7.70 29.90 5 -2 -29 -12.30 29.20 5 2 -29 -25.00 16.50 -5 2 29 26.50 10.80 4 -2 -29 -34.40 26.80 4 2 -29 -31.20 18.00 -4 2 29 -1.60 8.70 -3 2 29 40.20 12.50 -2 2 29 1.20 9.00 -1 2 29 6.80 10.30 -1 2 29 30.70 21.50 1 2 -29 1.20 17.50 0 2 29 22.70 24.20 0 2 29 -15.50 10.20 0 2 -29 10.50 16.30 1 2 29 20.40 22.50 -1 2 -29 86.19 21.90 -2 2 -29 98.79 22.30 2 2 29 67.69 26.80 8 -3 -29 -15.10 37.50 8 3 -29 -16.80 21.20 7 -3 -29 -2.20 36.70 7 3 -29 11.30 19.40 6 -3 -29 14.80 37.60 -6 3 29 -8.60 10.00 6 3 -29 -10.00 18.20 5 -3 -29 52.59 43.20 5 3 -29 1.90 18.70 -5 3 29 21.60 11.80 4 -3 -29 33.10 36.00 4 3 -29 6.10 20.70 -4 3 29 1.80 10.10 3 -3 -29 43.00 37.50 3 3 -29 11.60 19.90 -3 3 29 2.30 11.40 2 3 -29 -23.50 17.30 1 3 -29 -13.90 17.70 4 -4 -29 46.30 45.40 3 -4 -29 10.20 37.80 2 -4 -29 -22.70 20.90 -1 1 30 48.00 31.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 82791 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.66454(6) 0.72289(10) 0.22285(5) 0.0253(2) Uani 1 1 d . . . . . O2 O 0.81650(6) 0.47500(10) 0.11904(5) 0.0232(2) Uani 1 1 d . . . . . N1 N 0.69956(6) 0.26146(11) 0.25986(5) 0.0161(2) Uani 1 1 d . . . . . N2 N 0.71610(7) 0.07165(12) 0.34380(6) 0.0223(2) Uani 1 1 d . . . . . N3 N 0.81938(6) 0.47845(11) 0.34752(5) 0.01486(19) Uani 1 1 d . . . . . N4 N 0.81635(7) 0.35279(12) 0.45645(6) 0.0206(2) Uani 1 1 d . . . . . C1 C 0.62257(7) 0.22785(13) 0.22661(7) 0.0172(2) Uani 1 1 d . . . . . C2 C 0.57938(8) 0.09608(14) 0.22537(7) 0.0214(3) Uani 1 1 d . . . . . H2 H 0.601513 0.010132 0.248881 0.026 Uiso 1 1 calc R U . . . C3 C 0.50284(8) 0.09680(15) 0.18825(8) 0.0251(3) Uani 1 1 d . . . . . H3 H 0.471885 0.008990 0.186046 0.030 Uiso 1 1 calc R U . . . C4 C 0.46966(8) 0.22389(15) 0.15372(8) 0.0257(3) Uani 1 1 d . . . . . H4 H 0.416501 0.220793 0.129578 0.031 Uiso 1 1 calc R U . . . C5 C 0.51293(8) 0.35290(14) 0.15429(7) 0.0219(3) Uani 1 1 d . . . . . H5 H 0.490164 0.438534 0.130942 0.026 Uiso 1 1 calc R U . . . C6 C 0.59148(7) 0.35489(13) 0.19019(7) 0.0178(2) Uani 1 1 d . . . . . C7 C 0.65155(7) 0.46822(13) 0.20295(6) 0.0165(2) Uani 1 1 d . . . . . C8 C 0.71596(7) 0.40797(13) 0.24571(6) 0.0154(2) Uani 1 1 d . . . . . C9 C 0.75158(7) 0.15951(13) 0.30004(6) 0.0168(2) Uani 1 1 d . . . . . C10 C 0.83277(8) 0.15563(14) 0.29189(7) 0.0193(2) Uani 1 1 d . . . . . H10 H 0.854944 0.219617 0.259190 0.023 Uiso 1 1 calc R U . . . C11 C 0.88043(8) 0.05523(15) 0.33308(7) 0.0231(3) Uani 1 1 d . . . . . H11 H 0.936611 0.050792 0.330048 0.028 Uiso 1 1 calc R U . . . C12 C 0.84536(9) -0.03869(15) 0.37876(8) 0.0253(3) Uani 1 1 d . . . . . H12 H 0.876761 -0.108662 0.407473 0.030 Uiso 1 1 calc R U . . . C13 C 0.76332(9) -0.02779(16) 0.38144(8) 0.0266(3) Uani 1 1 d . . . . . H13 H 0.739031 -0.094372 0.411577 0.032 Uiso 1 1 calc R U . . . C14 C 0.64356(7) 0.62427(13) 0.18031(7) 0.0187(2) Uani 1 1 d . . . . . C15 C 0.60639(9) 0.65470(15) 0.10478(7) 0.0245(3) Uani 1 1 d . . . . . C16 C 0.52360(10) 0.72691(17) 0.10125(10) 0.0358(4) Uani 1 1 d . . . . . H16A H 0.483022 0.700555 0.060395 0.043 Uiso 1 1 calc R U . . . H16B H 0.501662 0.746356 0.147295 0.043 Uiso 1 1 calc R U . . . C17 C 0.59504(11) 0.81445(17) 0.08517(9) 0.0384(4) Uani 1 1 d . . . . . H17A H 0.616811 0.888405 0.121191 0.046 Uiso 1 1 calc R U . . . H17B H 0.598191 0.842655 0.034387 0.046 Uiso 1 1 calc R U . . . C18 C 0.62160(9) 0.54736(16) 0.04590(8) 0.0285(3) Uani 1 1 d . . . . . H18A H 0.598206 0.585991 -0.000894 0.043 Uiso 1 1 calc R U . . . H18B H 0.596790 0.452464 0.054780 0.043 Uiso 1 1 calc R U . . . H18C H 0.679648 0.534149 0.045690 0.043 Uiso 1 1 calc R U . . . C19 C 0.89169(7) 0.55586(13) 0.35776(6) 0.0147(2) Uani 1 1 d . . . . . C20 C 0.94204(7) 0.58444(13) 0.42115(6) 0.0162(2) Uani 1 1 d . . . . . H20 H 0.930731 0.545919 0.466150 0.019 Uiso 1 1 calc R U . . . C21 C 1.00920(7) 0.67117(14) 0.41598(7) 0.0184(2) Uani 1 1 d . . . . . H21 H 1.044183 0.693629 0.458353 0.022 Uiso 1 1 calc R U . . . C22 C 1.02651(7) 0.72642(14) 0.34938(7) 0.0201(2) Uani 1 1 d . . . . . H22 H 1.073139 0.785125 0.347420 0.024 Uiso 1 1 calc R U . . . C23 C 0.97676(7) 0.69682(14) 0.28645(7) 0.0190(2) Uani 1 1 d . . . . . H23 H 0.989355 0.733476 0.241487 0.023 Uiso 1 1 calc R U . . . C24 C 0.90727(7) 0.61155(13) 0.29024(6) 0.0157(2) Uani 1 1 d . . . . . C25 C 0.84298(7) 0.56070(13) 0.23796(6) 0.0155(2) Uani 1 1 d . . . . . C26 C 0.79105(7) 0.48077(13) 0.27450(6) 0.0150(2) Uani 1 1 d . . . . . C27 C 0.77539(7) 0.43052(13) 0.40392(6) 0.0156(2) Uani 1 1 d . . . . . C28 C 0.69444(7) 0.46771(14) 0.40152(7) 0.0185(2) Uani 1 1 d . . . . . H28 H 0.668304 0.524891 0.363124 0.022 Uiso 1 1 calc R U . . . C29 C 0.65349(8) 0.41849(15) 0.45695(7) 0.0238(3) Uani 1 1 d . . . . . H29 H 0.597957 0.439820 0.456939 0.029 Uiso 1 1 calc R U . . . C30 C 0.69437(9) 0.33766(16) 0.51254(8) 0.0266(3) Uani 1 1 d . . . . . H30 H 0.667601 0.303283 0.551421 0.032 Uiso 1 1 calc R U . . . C31 C 0.77520(9) 0.30810(15) 0.51012(7) 0.0257(3) Uani 1 1 d . . . . . H31 H 0.803064 0.253222 0.548521 0.031 Uiso 1 1 calc R U . . . C32 C 0.83407(7) 0.58031(14) 0.15872(6) 0.0171(2) Uani 1 1 d . . . . . C33 C 0.84861(8) 0.72964(15) 0.12900(7) 0.0218(3) Uani 1 1 d . . . . . C34 C 0.83351(9) 0.74268(18) 0.04804(7) 0.0316(3) Uani 1 1 d . . . . . H34A H 0.811192 0.655819 0.020652 0.038 Uiso 1 1 calc R U . . . H34B H 0.814490 0.838690 0.027619 0.038 Uiso 1 1 calc R U . . . C35 C 0.91847(9) 0.73354(19) 0.08324(8) 0.0323(3) Uani 1 1 d . . . . . H35A H 0.951571 0.823970 0.084741 0.039 Uiso 1 1 calc R U . . . H35B H 0.948271 0.640934 0.077768 0.039 Uiso 1 1 calc R U . . . C36 C 0.83305(10) 0.86519(15) 0.17208(8) 0.0284(3) Uani 1 1 d . . . . . H36A H 0.847490 0.953121 0.146101 0.043 Uiso 1 1 calc R U . . . H36B H 0.865600 0.860919 0.219186 0.043 Uiso 1 1 calc R U . . . H36C H 0.775958 0.869457 0.178897 0.043 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0266(5) 0.0175(4) 0.0303(5) -0.0022(4) -0.0029(4) 0.0000(4) O2 0.0274(5) 0.0227(5) 0.0188(4) -0.0055(4) -0.0003(4) -0.0005(4) N1 0.0157(5) 0.0141(4) 0.0170(5) 0.0014(4) -0.0039(4) -0.0018(4) N2 0.0215(5) 0.0222(5) 0.0223(5) 0.0057(4) -0.0010(4) 0.0002(4) N3 0.0140(4) 0.0156(4) 0.0140(4) 0.0005(4) -0.0023(4) -0.0019(4) N4 0.0224(5) 0.0203(5) 0.0179(5) 0.0041(4) -0.0019(4) -0.0005(4) C1 0.0154(5) 0.0180(5) 0.0171(5) -0.0003(4) -0.0029(4) -0.0020(4) C2 0.0212(6) 0.0175(6) 0.0243(6) 0.0021(5) -0.0024(5) -0.0028(5) C3 0.0219(6) 0.0215(6) 0.0303(7) 0.0006(5) -0.0040(5) -0.0074(5) C4 0.0182(6) 0.0259(7) 0.0305(7) 0.0009(5) -0.0073(5) -0.0040(5) C5 0.0191(6) 0.0206(6) 0.0242(6) 0.0015(5) -0.0054(5) 0.0000(5) C6 0.0174(6) 0.0169(5) 0.0182(6) -0.0003(4) -0.0023(4) -0.0010(4) C7 0.0169(5) 0.0155(5) 0.0161(5) 0.0002(4) -0.0023(4) -0.0013(4) C8 0.0171(5) 0.0138(5) 0.0144(5) 0.0003(4) -0.0019(4) -0.0012(4) C9 0.0192(6) 0.0150(5) 0.0152(5) 0.0001(4) -0.0030(4) 0.0012(4) C10 0.0201(6) 0.0172(6) 0.0204(6) 0.0008(5) 0.0014(5) 0.0010(4) C11 0.0194(6) 0.0224(6) 0.0266(7) -0.0013(5) -0.0007(5) 0.0042(5) C12 0.0266(7) 0.0218(6) 0.0261(7) 0.0052(5) -0.0029(5) 0.0062(5) C13 0.0287(7) 0.0244(6) 0.0260(7) 0.0100(5) 0.0003(5) 0.0002(5) C14 0.0159(5) 0.0172(5) 0.0223(6) 0.0021(5) -0.0009(4) 0.0007(4) C15 0.0281(7) 0.0194(6) 0.0239(6) 0.0062(5) -0.0052(5) 0.0019(5) C16 0.0337(8) 0.0281(7) 0.0419(9) 0.0041(6) -0.0117(7) 0.0122(6) C17 0.0532(10) 0.0225(7) 0.0364(8) 0.0118(6) -0.0084(7) 0.0033(7) C18 0.0320(7) 0.0304(7) 0.0211(6) 0.0038(5) -0.0050(5) 0.0014(6) C19 0.0131(5) 0.0139(5) 0.0166(5) -0.0006(4) -0.0004(4) 0.0001(4) C20 0.0153(5) 0.0170(5) 0.0154(5) 0.0000(4) -0.0017(4) 0.0023(4) C21 0.0152(5) 0.0197(6) 0.0190(6) -0.0027(5) -0.0035(4) 0.0008(4) C22 0.0144(6) 0.0212(6) 0.0242(6) -0.0022(5) -0.0001(5) -0.0036(4) C23 0.0184(6) 0.0203(6) 0.0185(6) -0.0002(5) 0.0023(4) -0.0020(5) C24 0.0157(5) 0.0152(5) 0.0156(5) -0.0007(4) -0.0014(4) 0.0002(4) C25 0.0171(5) 0.0143(5) 0.0142(5) 0.0005(4) -0.0021(4) -0.0004(4) C26 0.0157(5) 0.0140(5) 0.0141(5) 0.0001(4) -0.0030(4) 0.0007(4) C27 0.0164(5) 0.0143(5) 0.0155(5) 0.0001(4) -0.0011(4) -0.0024(4) C28 0.0161(6) 0.0200(6) 0.0186(6) -0.0022(5) -0.0015(4) 0.0001(4) C29 0.0185(6) 0.0271(7) 0.0258(6) -0.0073(5) 0.0031(5) -0.0058(5) C30 0.0312(7) 0.0275(7) 0.0218(6) -0.0012(5) 0.0062(5) -0.0120(6) C31 0.0307(7) 0.0248(6) 0.0202(6) 0.0063(5) -0.0023(5) -0.0039(5) C32 0.0158(5) 0.0200(6) 0.0150(5) -0.0004(4) -0.0005(4) -0.0003(4) C33 0.0262(6) 0.0238(6) 0.0146(6) 0.0032(5) -0.0016(5) -0.0055(5) C34 0.0366(8) 0.0389(8) 0.0176(6) 0.0086(6) -0.0033(6) -0.0105(6) C35 0.0305(8) 0.0439(9) 0.0227(7) 0.0067(6) 0.0039(6) -0.0112(6) C36 0.0386(8) 0.0176(6) 0.0277(7) 0.0038(5) -0.0022(6) -0.0039(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 N1 C1 108.49(10) . . ? C8 N1 C9 126.93(10) . . ? C1 N1 C9 124.57(10) . . ? C9 N2 C13 116.54(12) . . ? C26 N3 C19 108.53(10) . . ? C26 N3 C27 125.74(10) . . ? C19 N3 C27 124.73(10) . . ? C27 N4 C31 116.41(11) . . ? N1 C1 C2 130.03(11) . . ? N1 C1 C6 107.74(10) . . ? C2 C1 C6 122.22(11) . . ? C3 C2 C1 116.82(12) . . ? C3 C2 H2 121.6 . . ? C1 C2 H2 121.6 . . ? C2 C3 C4 121.80(12) . . ? C2 C3 H3 119.1 . . ? C4 C3 H3 119.1 . . ? C5 C4 C3 121.11(12) . . ? C5 C4 H4 119.4 . . ? C3 C4 H4 119.4 . . ? C4 C5 C6 118.48(12) . . ? C4 C5 H5 120.8 . . ? C6 C5 H5 120.8 . . ? C5 C6 C1 119.49(11) . . ? C5 C6 C7 133.24(11) . . ? C1 C6 C7 107.16(10) . . ? C8 C7 C6 107.21(10) . . ? C8 C7 C14 125.74(11) . . ? C6 C7 C14 126.84(11) . . ? C7 C8 N1 109.38(10) . . ? C7 C8 C26 127.78(11) . . ? N1 C8 C26 122.84(10) . . ? N2 C9 C10 124.49(11) . . ? N2 C9 N1 115.12(11) . . ? C10 C9 N1 120.39(11) . . ? C11 C10 C9 117.68(12) . . ? C11 C10 H10 121.2 . . ? C9 C10 H10 121.2 . . ? C10 C11 C12 119.33(12) . . ? C10 C11 H11 120.3 . . ? C12 C11 H11 120.3 . . ? C13 C12 C11 118.20(12) . . ? C13 C12 H12 120.9 . . ? C11 C12 H12 120.9 . . ? N2 C13 C12 123.71(13) . . ? N2 C13 H13 118.1 . . ? C12 C13 H13 118.1 . . ? O1 C14 C7 120.48(11) . . ? O1 C14 C15 122.18(11) . . ? C7 C14 C15 117.30(11) . . ? C14 C15 C17 115.72(12) . . ? C14 C15 C18 118.56(11) . . ? C17 C15 C18 118.18(13) . . ? C14 C15 C16 113.21(12) . . ? C17 C15 C16 59.12(11) . . ? C18 C15 C16 118.33(12) . . ? C17 C16 C15 59.63(10) . . ? C17 C16 H16A 117.8 . . ? C15 C16 H16A 117.8 . . ? C17 C16 H16B 117.8 . . ? C15 C16 H16B 117.8 . . ? H16A C16 H16B 114.9 . . ? C16 C17 C15 61.25(10) . . ? C16 C17 H17A 117.6 . . ? C15 C17 H17A 117.6 . . ? C16 C17 H17B 117.6 . . ? C15 C17 H17B 117.6 . . ? H17A C17 H17B 114.7 . . ? C15 C18 H18A 109.5 . . ? C15 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C15 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? N3 C19 C20 129.73(11) . . ? N3 C19 C24 107.88(10) . . ? C20 C19 C24 122.34(11) . . ? C21 C20 C19 117.48(11) . . ? C21 C20 H20 121.3 . . ? C19 C20 H20 121.3 . . ? C20 C21 C22 121.27(11) . . ? C20 C21 H21 119.4 . . ? C22 C21 H21 119.4 . . ? C23 C22 C21 121.11(11) . . ? C23 C22 H22 119.4 . . ? C21 C22 H22 119.4 . . ? C22 C23 C24 118.89(12) . . ? C22 C23 H23 120.6 . . ? C24 C23 H23 120.6 . . ? C23 C24 C19 118.89(11) . . ? C23 C24 C25 134.33(11) . . ? C19 C24 C25 106.77(10) . . ? C26 C25 C24 107.38(10) . . ? C26 C25 C32 124.37(11) . . ? C24 C25 C32 128.16(11) . . ? C25 C26 N3 109.40(10) . . ? C25 C26 C8 128.45(11) . . ? N3 C26 C8 122.15(10) . . ? N4 C27 C28 124.58(11) . . ? N4 C27 N3 116.18(11) . . ? C28 C27 N3 119.24(11) . . ? C29 C28 C27 117.65(12) . . ? C29 C28 H28 121.2 . . ? C27 C28 H28 121.2 . . ? C28 C29 C30 119.23(13) . . ? C28 C29 H29 120.4 . . ? C30 C29 H29 120.4 . . ? C29 C30 C31 118.48(13) . . ? C29 C30 H30 120.8 . . ? C31 C30 H30 120.8 . . ? N4 C31 C30 123.63(13) . . ? N4 C31 H31 118.2 . . ? C30 C31 H31 118.2 . . ? O2 C32 C25 119.96(11) . . ? O2 C32 C33 121.47(11) . . ? C25 C32 C33 118.56(10) . . ? C32 C33 C34 115.31(11) . . ? C32 C33 C36 119.75(11) . . ? C34 C33 C36 116.79(12) . . ? C32 C33 C35 113.38(12) . . ? C34 C33 C35 59.11(9) . . ? C36 C33 C35 118.05(12) . . ? C35 C34 C33 61.11(9) . . ? C35 C34 H34A 117.7 . . ? C33 C34 H34A 117.7 . . ? C35 C34 H34B 117.7 . . ? C33 C34 H34B 117.7 . . ? H34A C34 H34B 114.8 . . ? C34 C35 C33 59.78(9) . . ? C34 C35 H35A 117.8 . . ? C33 C35 H35A 117.8 . . ? C34 C35 H35B 117.8 . . ? C33 C35 H35B 117.8 . . ? H35A C35 H35B 114.9 . . ? C33 C36 H36A 109.5 . . ? C33 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C33 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C14 1.2219(16) . ? O2 C32 1.2252(15) . ? N1 C8 1.3914(15) . ? N1 C1 1.3978(15) . ? N1 C9 1.4239(15) . ? N2 C9 1.3316(16) . ? N2 C13 1.3441(17) . ? N3 C26 1.3908(14) . ? N3 C19 1.3942(15) . ? N3 C27 1.4230(15) . ? N4 C27 1.3322(15) . ? N4 C31 1.3444(17) . ? C1 C2 1.3980(17) . ? C1 C6 1.4086(17) . ? C2 C3 1.3839(18) . ? C2 H2 0.9500 . ? C3 C4 1.4054(19) . ? C3 H3 0.9500 . ? C4 C5 1.3779(18) . ? C4 H4 0.9500 . ? C5 C6 1.4049(17) . ? C5 H5 0.9500 . ? C6 C7 1.4400(16) . ? C7 C8 1.3782(16) . ? C7 C14 1.4817(17) . ? C8 C26 1.4661(16) . ? C9 C10 1.3864(18) . ? C10 C11 1.3849(18) . ? C10 H10 0.9500 . ? C11 C12 1.386(2) . ? C11 H11 0.9500 . ? C12 C13 1.384(2) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C14 C15 1.4995(18) . ? C15 C17 1.5042(19) . ? C15 C18 1.514(2) . ? C15 C16 1.528(2) . ? C16 C17 1.496(3) . ? C16 H16A 0.9900 . ? C16 H16B 0.9900 . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 C20 1.3951(16) . ? C19 C24 1.4116(16) . ? C20 C21 1.3861(17) . ? C20 H20 0.9500 . ? C21 C22 1.4031(18) . ? C21 H21 0.9500 . ? C22 C23 1.3852(17) . ? C22 H22 0.9500 . ? C23 C24 1.4071(17) . ? C23 H23 0.9500 . ? C24 C25 1.4421(16) . ? C25 C26 1.3747(17) . ? C25 C32 1.4810(16) . ? C27 C28 1.3928(17) . ? C28 C29 1.3817(19) . ? C28 H28 0.9500 . ? C29 C30 1.386(2) . ? C29 H29 0.9500 . ? C30 C31 1.386(2) . ? C30 H30 0.9500 . ? C31 H31 0.9500 . ? C32 C33 1.4971(18) . ? C33 C34 1.5085(18) . ? C33 C36 1.511(2) . ? C33 C35 1.528(2) . ? C34 C35 1.498(2) . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C35 H35A 0.9900 . ? C35 H35B 0.9900 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C8 N1 C1 C2 -179.82(13) . . . . ? C9 N1 C1 C2 1.2(2) . . . . ? C8 N1 C1 C6 1.11(14) . . . . ? C9 N1 C1 C6 -177.88(11) . . . . ? N1 C1 C2 C3 179.10(13) . . . . ? C6 C1 C2 C3 -2.0(2) . . . . ? C1 C2 C3 C4 -0.4(2) . . . . ? C2 C3 C4 C5 1.3(2) . . . . ? C3 C4 C5 C6 0.1(2) . . . . ? C4 C5 C6 C1 -2.4(2) . . . . ? C4 C5 C6 C7 -178.09(14) . . . . ? N1 C1 C6 C5 -177.48(11) . . . . ? C2 C1 C6 C5 3.4(2) . . . . ? N1 C1 C6 C7 -0.73(14) . . . . ? C2 C1 C6 C7 -179.89(12) . . . . ? C5 C6 C7 C8 176.20(14) . . . . ? C1 C6 C7 C8 0.09(14) . . . . ? C5 C6 C7 C14 1.3(2) . . . . ? C1 C6 C7 C14 -174.86(12) . . . . ? C6 C7 C8 N1 0.60(14) . . . . ? C14 C7 C8 N1 175.62(11) . . . . ? C6 C7 C8 C26 -178.53(12) . . . . ? C14 C7 C8 C26 -3.5(2) . . . . ? C1 N1 C8 C7 -1.07(14) . . . . ? C9 N1 C8 C7 177.88(11) . . . . ? C1 N1 C8 C26 178.11(11) . . . . ? C9 N1 C8 C26 -2.94(19) . . . . ? C13 N2 C9 C10 -0.81(19) . . . . ? C13 N2 C9 N1 178.74(11) . . . . ? C8 N1 C9 N2 139.20(12) . . . . ? C1 N1 C9 N2 -42.01(17) . . . . ? C8 N1 C9 C10 -41.23(18) . . . . ? C1 N1 C9 C10 137.56(13) . . . . ? N2 C9 C10 C11 -1.21(19) . . . . ? N1 C9 C10 C11 179.26(11) . . . . ? C9 C10 C11 C12 1.65(19) . . . . ? C10 C11 C12 C13 -0.2(2) . . . . ? C9 N2 C13 C12 2.5(2) . . . . ? C11 C12 C13 N2 -2.0(2) . . . . ? C8 C7 C14 O1 -41.05(19) . . . . ? C6 C7 C14 O1 133.00(14) . . . . ? C8 C7 C14 C15 141.05(13) . . . . ? C6 C7 C14 C15 -44.90(18) . . . . ? O1 C14 C15 C17 -1.2(2) . . . . ? C7 C14 C15 C17 176.67(13) . . . . ? O1 C14 C15 C18 148.02(13) . . . . ? C7 C14 C15 C18 -34.12(18) . . . . ? O1 C14 C15 C16 -66.78(17) . . . . ? C7 C14 C15 C16 111.08(14) . . . . ? C14 C15 C16 C17 107.08(14) . . . . ? C18 C15 C16 C17 -107.63(15) . . . . ? C14 C15 C17 C16 -102.80(15) . . . . ? C18 C15 C17 C16 107.87(15) . . . . ? C26 N3 C19 C20 179.47(12) . . . . ? C27 N3 C19 C20 10.36(19) . . . . ? C26 N3 C19 C24 1.96(13) . . . . ? C27 N3 C19 C24 -167.15(10) . . . . ? N3 C19 C20 C21 -177.06(12) . . . . ? C24 C19 C20 C21 0.14(18) . . . . ? C19 C20 C21 C22 -0.88(18) . . . . ? C20 C21 C22 C23 0.36(19) . . . . ? C21 C22 C23 C24 0.93(19) . . . . ? C22 C23 C24 C19 -1.62(18) . . . . ? C22 C23 C24 C25 179.45(13) . . . . ? N3 C19 C24 C23 178.86(11) . . . . ? C20 C19 C24 C23 1.12(18) . . . . ? N3 C19 C24 C25 -1.95(13) . . . . ? C20 C19 C24 C25 -179.68(11) . . . . ? C23 C24 C25 C26 -179.76(13) . . . . ? C19 C24 C25 C26 1.22(13) . . . . ? C23 C24 C25 C32 3.5(2) . . . . ? C19 C24 C25 C32 -175.48(11) . . . . ? C24 C25 C26 N3 -0.03(13) . . . . ? C32 C25 C26 N3 176.83(11) . . . . ? C24 C25 C26 C8 179.06(11) . . . . ? C32 C25 C26 C8 -4.1(2) . . . . ? C19 N3 C26 C25 -1.20(13) . . . . ? C27 N3 C26 C25 167.77(11) . . . . ? C19 N3 C26 C8 179.64(10) . . . . ? C27 N3 C26 C8 -11.38(18) . . . . ? C7 C8 C26 C25 -52.0(2) . . . . ? N1 C8 C26 C25 128.94(14) . . . . ? C7 C8 C26 N3 126.94(14) . . . . ? N1 C8 C26 N3 -52.08(17) . . . . ? C31 N4 C27 C28 0.21(18) . . . . ? C31 N4 C27 N3 179.56(11) . . . . ? C26 N3 C27 N4 140.21(12) . . . . ? C19 N3 C27 N4 -52.54(16) . . . . ? C26 N3 C27 C28 -40.40(17) . . . . ? C19 N3 C27 C28 126.86(12) . . . . ? N4 C27 C28 C29 -1.07(19) . . . . ? N3 C27 C28 C29 179.59(11) . . . . ? C27 C28 C29 C30 1.17(19) . . . . ? C28 C29 C30 C31 -0.5(2) . . . . ? C27 N4 C31 C30 0.6(2) . . . . ? C29 C30 C31 N4 -0.4(2) . . . . ? C26 C25 C32 O2 -43.86(18) . . . . ? C24 C25 C32 O2 132.33(13) . . . . ? C26 C25 C32 C33 137.36(13) . . . . ? C24 C25 C32 C33 -46.46(18) . . . . ? O2 C32 C33 C34 4.74(19) . . . . ? C25 C32 C33 C34 -176.49(12) . . . . ? O2 C32 C33 C36 152.38(13) . . . . ? C25 C32 C33 C36 -28.86(18) . . . . ? O2 C32 C33 C35 -60.78(16) . . . . ? C25 C32 C33 C35 117.98(12) . . . . ? C32 C33 C34 C35 -103.21(14) . . . . ? C36 C33 C34 C35 108.16(14) . . . . ? C32 C33 C35 C34 106.51(13) . . . . ? C36 C33 C35 C34 -106.05(14) . . . . ?