#------------------------------------------------------------------------------ #$Date: 2021-11-03 23:17:23 +0200 (Wed, 03 Nov 2021) $ #$Revision: 270254 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/91/4519114.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519114 loop_ _publ_author_name 'Alanazi, Abdulaziz M.' 'McNaughter, Paul D.' 'Alam, Firoz' 'Vitorica-Yrezabal, Inigo J' 'Whitehead, George F. S.' 'Tuna, Floriana' 'O'Brien, Paul' 'Collison, David' 'Lewis, David J.' _publ_section_title ; Structural Investigations of \a-MnS Nanocrystals and Thin Films Synthesized from Manganese(II) Xanthates by Hot Injection, Solvent-Less Thermolysis, and Doctor Blade Routes. ; _journal_issue 42 _journal_name_full 'ACS omega' _journal_page_first 27716 _journal_page_last 27725 _journal_paper_doi 10.1021/acsomega.1c02907 _journal_volume 6 _journal_year 2021 _chemical_formula_moiety 'C20 H42 Mn N2 O2 S4' _chemical_formula_sum 'C20 H42 Mn N2 O2 S4' _chemical_formula_weight 525.73 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-I 2ya' _space_group_name_H-M_alt 'I 1 2/a 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2017-09-18 _audit_creation_method ; Olex2 1.2 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _cell_angle_alpha 90 _cell_angle_beta 108.507(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.6601(3) _cell_length_b 8.15454(13) _cell_length_c 23.5223(5) _cell_measurement_reflns_used 13369 _cell_measurement_temperature 240.00(10) _cell_measurement_theta_max 67.7170 _cell_measurement_theta_min 3.9580 _cell_volume 2848.48(10) _computing_cell_refinement 'CrysAlisPro 1.171.39.30c (Rigaku OD, 2017)' _computing_data_collection 'CrysAlisPro 1.171.39.30c (Rigaku OD, 2017)' _computing_data_reduction 'CrysAlisPro 1.171.39.30c (Rigaku OD, 2017)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 240.00(10) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -81.00 8.00 1.00 1.00 -- 5.00 -76.00-120.00 89 2 \w 16.00 92.00 1.00 1.00 -- 5.00 57.00-150.00 76 3 \w -69.00 38.00 1.00 1.00 -- 5.00 -57.00 90.00 107 4 \w 15.00 45.00 1.00 1.00 -- 5.00 -76.00-120.00 30 5 \w -116.00 -90.00 1.00 1.00 -- -30.00 -54.00 -44.14 26 6 \w -42.00 -6.00 1.00 1.00 -- -30.00 -54.00 -44.14 36 7 \w -77.00 26.00 1.00 1.00 -- -45.10 57.00 0.00 103 8 \w -144.00-119.00 1.00 1.00 -- -62.00 -73.00 -25.47 25 9 \w -53.00 -24.00 1.00 1.00 -- -62.00 -73.00 -25.47 29 10 \w -133.00-107.00 1.00 1.00 -- -66.00 -75.00 137.01 26 11 \w -54.00 -26.00 1.00 1.00 -- -66.00 -76.00 -86.86 28 12 \w -146.00-120.00 1.00 1.00 -- -66.00 -76.00 -86.86 26 13 \w -51.00 -26.00 1.00 1.00 -- -66.00 -76.00 160.52 25 14 \w -75.00 -26.00 1.00 1.00 -- -66.00 -76.00-139.20 49 15 \w -53.00 -28.00 1.00 1.00 -- -66.00 -75.00 137.01 25 16 \w -152.00-126.00 1.00 1.00 -- -66.00 -71.00 83.24 26 17 \w -59.00 -29.00 1.00 1.00 -- -66.00 -71.00 83.24 30 18 \w -128.00-103.00 1.00 1.00 -- -66.00 -76.00 160.52 25 19 \w -109.00 -31.00 1.00 1.00 -- -70.00 -74.00 62.05 78 20 \w -64.00 -32.00 1.00 1.00 -- -70.00 -74.00 -30.47 32 21 \w -80.00 -34.00 1.00 1.00 -- -74.00 -76.00 25.46 46 22 \w -162.00-113.00 1.00 1.00 -- -74.00 -76.00 25.46 49 23 \w -71.00 -43.00 1.00 1.00 -- -78.00 -73.00 145.04 28 24 \w -76.00 -45.00 1.00 1.00 -- -82.00 -71.00 -12.85 31 25 \w -74.00 -42.00 1.00 1.00 -- -82.00 -76.00-126.69 32 26 \w -73.00 -48.00 1.00 1.00 -- -86.00 -73.00 -36.01 25 27 \w -76.00 -50.00 1.00 1.00 -- -90.00 -76.00 -48.51 26 28 \w -108.00 -54.00 1.00 1.00 -- -90.00 -71.00 -77.56 54 29 \w -81.00 -51.00 1.00 1.00 -- -90.00 -75.00-175.57 30 30 \w -177.00-100.00 1.00 1.00 -- -90.00 -76.00 -48.51 77 31 \w -135.00-107.00 1.00 1.00 -- -90.00 -75.00-175.57 28 32 \w -159.00-124.00 1.00 1.00 -- -94.00 -73.00-123.94 35 33 \w -89.00 -56.00 1.00 1.00 -- -94.00 -75.00 169.18 33 34 \w -141.00-115.00 1.00 1.00 -- -94.00 -75.00 169.18 26 35 \w -82.00 -55.00 1.00 1.00 -- -94.00 -76.00 -6.53 27 36 \w -130.00-104.00 1.00 1.00 -- -94.00 -76.00 -6.53 26 37 \w -94.00 -54.00 1.00 1.00 -- -94.00 -76.00 40.30 40 38 \w -89.00 -58.00 1.00 1.00 -- -94.00 -73.00-123.94 31 39 \w -181.00 -99.00 1.00 1.00 -- -94.00 -76.00 40.30 82 40 \w -81.00 -54.00 1.00 1.00 -- -94.00 -76.00 128.89 27 41 \w -175.00-127.00 1.00 1.00 -- -94.00 -76.00 128.89 48 42 \w -92.00 -59.00 1.00 1.00 -- -98.00 -74.00 -82.40 33 43 \w -184.00-102.00 1.00 1.00 -- -98.00 -74.00 -82.40 82 44 \w -185.00 -58.00 1.00 1.00 -- -98.00 -76.00-130.65 127 45 \w -186.00 -60.00 1.00 1.00 -- -98.00 -73.00 89.50 126 46 \w -170.00 -62.00 1.00 1.00 -- -98.00 -68.00-160.37 108 47 \w -191.00 -64.00 1.00 1.00 -- -102.00 -72.00 149.92 127 48 \w -120.00 -67.00 1.00 1.00 -- -107.20 76.00-150.00 53 49 \w -163.00 -69.00 1.00 1.00 -- -107.20 -72.00 -48.19 94 50 \w -123.00 -18.00 1.00 1.00 -- -107.20 76.00 -30.00 105 51 \w -154.00 -67.00 1.00 1.00 -- -107.20 -76.00 74.36 87 52 \w -194.00 -69.00 1.00 1.00 -- -107.20 -73.00 -23.05 125 53 \w -196.00-157.00 1.00 1.00 -- -107.20 -76.00 74.36 39 54 \w -159.00 -69.00 1.00 1.00 -- -107.20 -76.00 -90.00 90 55 \w -196.00-170.00 1.00 1.00 -- -107.20 -76.00 -90.00 26 56 \w -128.00 -49.00 1.00 1.00 -- -107.20 76.00 120.00 79 57 \w -197.00 -73.00 1.00 1.00 -- -107.20 -76.00 30.00 124 58 \w -154.00 -69.00 1.00 1.00 -- -107.20 -73.00 127.98 85 59 \w -196.00-171.00 1.00 1.00 -- -107.20 -73.00 127.98 25 60 \w -133.00 -58.00 1.00 1.00 -- -107.20 76.00 60.00 75 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC11 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0765049000 _diffrn_orient_matrix_UB_12 0.0805939000 _diffrn_orient_matrix_UB_13 -0.0180842000 _diffrn_orient_matrix_UB_21 -0.0685411000 _diffrn_orient_matrix_UB_22 0.0561302000 _diffrn_orient_matrix_UB_23 -0.0596553000 _diffrn_orient_matrix_UB_31 -0.0143954000 _diffrn_orient_matrix_UB_32 0.1614032000 _diffrn_orient_matrix_UB_33 0.0297705000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0415 _diffrn_reflns_av_unetI/netI 0.0182 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 29808 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 68.212 _diffrn_reflns_theta_min 5.777 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 6.636 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.44512 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.30c (Rigaku Oxford Diffraction, 2017) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.226 _exptl_crystal_description plate _exptl_crystal_F_000 1124 _exptl_crystal_size_max 0.455 _exptl_crystal_size_mid 0.312 _exptl_crystal_size_min 0.021 _refine_diff_density_max 1.336 _refine_diff_density_min -0.452 _refine_diff_density_rms 0.064 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.099 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 191 _refine_ls_number_reflns 2598 _refine_ls_number_restraints 264 _refine_ls_restrained_S_all 1.068 _refine_ls_R_factor_all 0.0709 _refine_ls_R_factor_gt 0.0679 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0850P)^2^+7.2721P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1796 _refine_ls_wR_factor_ref 0.1825 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2422 _reflns_number_total 2598 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao1c02907_si_006.cif _cod_data_source_block s4957r _cod_database_code 4519114 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_usercomment MG _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.873 _shelx_estimated_absorpt_t_min 0.152 _reflns_odcompleteness_completeness 99.61 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 68.13 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C7A-C6A = C7-C6 = C5A-C6A = C6-C5 = C5A-C4A = C4-C5 = C4A-C3A = C4-C3 = C3-C2 = C3A-C2A 1.54 with sigma of 0.01 C7-C5 \\sim C6-C4 with sigma of 0.02 C7A-C5A \\sim C6A-C4A with sigma of 0.02 3. Uiso/Uaniso restraints and constraints O1 \\sim C2A \\sim C5 \\sim C6A \\sim C7A \\sim C3A \\sim C4A \\sim C2 \\sim C3 \\sim C4 \\sim C5A \\sim C6 \\sim C7: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 4. Rigid body (RIGU) restrains O1, C2A, C5, C6A, C7A, C3A, C4A, C2, C3, C4, C5A, C6, C7 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 S1, C1, S2, O1 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 5. Others Sof(C2A)=Sof(H2AA)=Sof(H2AB)=Sof(C6A)=Sof(H6AA)=Sof(H6AB)=Sof(C7A)=Sof(H7AA)= Sof(H7AB)=Sof(H7AC)=Sof(C3A)=Sof(H3AA)=Sof(H3AB)=Sof(C4A)=Sof(H4AA)=Sof(H4AB)= Sof(C5A)=Sof(H5AA)=Sof(H5AB)=1-FVAR(1) Sof(C5)=Sof(H5A)=Sof(H5B)=Sof(C2)=Sof(H2A)=Sof(H2B)=Sof(C3)=Sof(H3A)=Sof(H3B)= Sof(C4)=Sof(H4A)=Sof(H4B)=Sof(C6)=Sof(H6A)=Sof(H6B)=Sof(C7)=Sof(H7A)=Sof(H7B)= Sof(H7C)=FVAR(1) 6.a Secondary CH2 refined with riding coordinates: C2A(H2AA,H2AB), C5(H5A,H5B), C6A(H6AA,H6AB), C10(H10A,H10B), C3A(H3AA,H3AB), C4A(H4AA,H4AB), C2(H2A,H2B), C3(H3A,H3B), C4(H4A,H4B), C5A(H5AA,H5AB), C6(H6A, H6B) 6.b Idealised Me refined as rotating group: C9(H9A,H9B,H9C), C8(H8A,H8B,H8C), C7A(H7AA,H7AB,H7AC), C7(H7A,H7B,H7C) ; _shelx_res_file ; TITL s4957r_a.res in I2/a s4957r.res created by SHELXL-2016/6 at 14:47:03 on 18-Sep-2017 REM Old TITL REM SHELXT solution in I2/a REM R1 0.393, Rweak 0.457, Alpha 0.073, Orientation as input REM Formula found by SHELXT: C18 N8 O2 Mn CELL 1.54184 15.660138 8.154542 23.522272 90 108.5072 90 ZERR 4 0.000299 0.000128 0.000484 0 0.0021 0 LATT 2 SYMM 0.5-X,+Y,-Z SFAC C H Mn N O S UNIT 80 168 4 8 8 16 DFIX 1.54 0.01 C7A C6A C7 C6 C5A C6A C6 C5 C5A C4A C4 C5 C4A C3A C4 C3 C3 = C2 C3A C2A SADI C7 C5 C6 C4 SADI C7A C5A C6A C4A SIMU O1 C2A C5 C6A C7A C3A C4A C2 C3 C4 C5A C6 C7 RIGU O1 C2A C5 C6A C7A C3A C4A C2 C3 C4 C5A C6 C7 RIGU 0.001 0.001 S1 C1 S2 O1 L.S. 10 PLAN 20 SIZE 0.021 0.312 0.455 BOND $H list 4 fmap 2 acta REM REM REM WGHT 0.085000 7.272100 FVAR 4.52396 0.32677 MN1 3 0.250000 0.136985 0.500000 10.50000 0.05013 0.03596 = 0.06319 0.00000 0.00791 0.00000 S2 6 0.422556 0.215470 0.527924 11.00000 0.06075 0.07688 = 0.09671 -0.01782 0.02605 -0.01013 S1 6 0.295080 0.341802 0.587485 11.00000 0.06876 0.07783 = 0.09141 -0.02468 0.02704 -0.01514 O1 5 0.454409 0.448298 0.611308 11.00000 0.06907 0.10326 = 0.13581 -0.05957 0.04420 -0.03235 C1 1 0.392855 0.342169 0.576341 11.00000 0.08127 0.05456 = 0.07930 -0.01386 0.02513 -0.02128 N006 4 0.248990 -0.080083 0.438473 11.00000 0.07227 0.07080 = 0.12162 -0.04198 0.02099 0.00005 PART 2 C2A 1 0.539871 0.468245 0.605129 -21.00000 0.06213 0.10806 = 0.16794 -0.05687 0.04328 -0.03577 AFIX 23 H2AA 2 0.535707 0.535851 0.570421 -21.00000 -1.20000 H2AB 2 0.564317 0.362408 0.599519 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C5 1 0.624107 0.816349 0.704968 21.00000 0.10989 0.09701 = 0.10317 -0.00992 0.03926 -0.01481 AFIX 23 H5A 2 0.687499 0.818973 0.728265 21.00000 -1.20000 H5B 2 0.619522 0.853272 0.664906 21.00000 -1.20000 AFIX 0 PART 0 C9 1 0.315066 -0.058898 0.406132 11.00000 0.12714 0.14401 = 0.15227 -0.07016 0.06465 0.00372 AFIX 137 H9A 2 0.299766 0.036465 0.381004 11.00000 -1.50000 H9B 2 0.314255 -0.153853 0.381842 11.00000 -1.50000 H9C 2 0.374148 -0.045527 0.434520 11.00000 -1.50000 AFIX 0 C8 1 0.158491 -0.096320 0.393557 11.00000 0.10288 0.15181 = 0.18369 -0.12074 0.00116 -0.01253 AFIX 137 H8A 2 0.115301 -0.121349 0.413531 11.00000 -1.50000 H8B 2 0.159192 -0.182977 0.366084 11.00000 -1.50000 H8C 2 0.142297 0.004836 0.371932 11.00000 -1.50000 AFIX 0 PART 2 C6A 1 0.575703 0.994803 0.710385 -21.00000 0.09463 0.11360 = 0.07293 -0.00306 0.02946 -0.01381 AFIX 23 H6AA 2 0.569750 1.033241 0.670283 -21.00000 -1.20000 H6AB 2 0.516420 0.991551 0.715134 -21.00000 -1.20000 AFIX 0 PART 0 C10 1 0.274267 -0.225332 0.477846 11.00000 0.15866 0.04332 = 0.25354 -0.02984 0.06759 0.01072 AFIX 23 H10A 2 0.259815 -0.324310 0.453818 11.00000 -1.20000 H10B 2 0.338644 -0.224338 0.498421 11.00000 -1.20000 AFIX 0 PART 2 C7A 1 0.638036 1.106646 0.757151 -21.00000 0.14116 0.08647 = 0.09512 -0.00539 0.01397 -0.00443 AFIX 137 H7AA 2 0.651466 1.057167 0.796038 -21.00000 -1.50000 H7AB 2 0.609115 1.210490 0.757062 -21.00000 -1.50000 H7AC 2 0.692873 1.122878 0.747873 -21.00000 -1.50000 AFIX 0 C3A 1 0.601837 0.551068 0.662463 -21.00000 0.05742 0.08457 = 0.12992 -0.00383 0.01394 -0.00591 AFIX 23 H3AA 2 0.602823 0.487856 0.697599 -21.00000 -1.20000 H3AB 2 0.662829 0.558728 0.660833 -21.00000 -1.20000 AFIX 0 C4A 1 0.563260 0.723990 0.665439 -21.00000 0.06859 0.08436 = 0.11656 -0.01518 0.02096 -0.01183 AFIX 23 H4AA 2 0.502079 0.713475 0.666486 -21.00000 -1.20000 H4AB 2 0.560983 0.783630 0.629307 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C2 1 0.551485 0.458347 0.608150 21.00000 0.06236 0.10331 = 0.13554 -0.04936 0.05052 -0.00943 AFIX 23 H2A 2 0.589980 0.375844 0.633369 21.00000 -1.20000 H2B 2 0.552281 0.445332 0.567331 21.00000 -1.20000 AFIX 0 C3 1 0.580640 0.632729 0.631846 21.00000 0.05906 0.10391 = 0.11054 -0.02846 0.04231 -0.03026 AFIX 23 H3A 2 0.534682 0.711431 0.611444 21.00000 -1.20000 H3B 2 0.636262 0.662119 0.624531 21.00000 -1.20000 AFIX 0 C4 1 0.594398 0.634701 0.699836 21.00000 0.07923 0.08889 = 0.09713 -0.01158 0.02622 -0.00427 AFIX 23 H4A 2 0.641367 0.560729 0.722553 21.00000 -1.20000 H4B 2 0.539256 0.616556 0.709374 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C5A 1 0.619386 0.824860 0.720989 -21.00000 0.09079 0.10258 = 0.12097 -0.03604 0.03994 -0.02850 AFIX 23 H5AA 2 0.615529 0.776998 0.757847 -21.00000 -1.20000 H5AB 2 0.682139 0.830492 0.722973 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C6 1 0.576926 0.944318 0.731856 21.00000 0.14188 0.12117 = 0.11022 -0.01053 0.04336 0.00184 AFIX 23 H6A 2 0.580479 0.905326 0.771501 21.00000 -1.20000 H6B 2 0.513754 0.942005 0.708052 21.00000 -1.20000 AFIX 0 C7 1 0.605026 1.124556 0.738751 21.00000 0.19606 0.11162 = 0.10876 0.00613 0.04166 0.01528 AFIX 137 H7A 2 0.632792 1.149414 0.780453 21.00000 -1.50000 H7B 2 0.552862 1.192547 0.722675 21.00000 -1.50000 H7C 2 0.647078 1.144943 0.717457 21.00000 -1.50000 AFIX 0 HKLF 4 REM s4957r_a.res in I2/a REM R1 = 0.0679 for 2422 Fo > 4sig(Fo) and 0.0709 for all 2598 data REM 191 parameters refined using 264 restraints END WGHT 0.0851 7.2695 REM Highest difference peak 1.336, deepest hole -0.452, 1-sigma level 0.064 Q1 1 0.4318 0.1329 0.5039 11.00000 0.05 1.34 Q2 1 0.3414 0.3546 0.5709 11.00000 0.05 0.96 Q3 1 0.5127 0.3716 0.5698 11.00000 0.05 0.38 Q4 1 0.3778 0.2744 0.5037 11.00000 0.05 0.36 Q5 1 0.4232 0.3121 0.5708 11.00000 0.05 0.30 Q6 1 0.2838 0.1467 0.4914 11.00000 0.05 0.27 Q7 1 0.3271 -0.0467 0.3951 11.00000 0.05 0.18 Q8 1 0.3044 0.2377 0.6009 11.00000 0.05 0.18 Q9 1 0.2193 -0.0143 0.4216 11.00000 0.05 0.18 Q10 1 0.2500 -0.2480 0.5000 10.50000 0.05 0.17 Q11 1 0.1620 -0.1203 0.3765 11.00000 0.05 0.17 Q12 1 0.6865 0.8524 0.6930 11.00000 0.05 0.17 Q13 1 0.6219 0.6512 0.5954 11.00000 0.05 0.16 Q14 1 0.2530 -0.2270 0.4492 11.00000 0.05 0.16 Q15 1 0.1194 -0.0350 0.3907 11.00000 0.05 0.16 Q16 1 0.2441 -0.1540 0.4581 11.00000 0.05 0.15 Q17 1 0.6434 0.7520 0.7426 11.00000 0.05 0.15 Q18 1 0.1422 -0.1980 0.3850 11.00000 0.05 0.15 Q19 1 0.2705 -0.0826 0.4249 11.00000 0.05 0.15 Q20 1 0.2004 -0.0923 0.4162 11.00000 0.05 0.14 ; _shelx_res_checksum 31767 _shelx_hkl_file ; 0 0 -4 21489.8 845.808 5 0 0 4 21146.6 872.902 7 0 0 4 19965.6 849.216 2 0 0 -4 21188.0 868.429 1 0 0 4 19986.8 870.021 1 0 0 -4 21167.5 850.344 2 0 0 6 280068. 10866.6 1 0 0 -6 272577. 10860.6 11 0 0 6 278530. 10866.8 7 0 0 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311.892 297.045 41 2 -2 -22 471.320 384.014 54 2 2 -22 307.482 304.874 38 -2 -2 22 317.461 356.490 51 2 2 -22 225.869 314.976 44 2 -2 -22 265.852 268.400 42 -2 2 22 454.046 387.561 41 -2 2 22 28.3230 465.075 50 2 -2 -22 82.6938 325.693 25 2 2 -20 713.169 397.173 54 -2 2 20 887.997 407.637 41 2 -2 -20 2009.91 426.109 54 2 2 -20 1262.39 352.590 38 -2 2 20 914.752 480.087 50 2 -2 -20 1053.47 348.205 14 2 -2 -20 1449.87 318.612 42 -2 -2 20 1407.10 384.491 51 2 2 -20 840.642 350.348 44 2 2 -20 1402.31 363.552 43 -2 2 20 933.898 455.424 47 -2 -2 20 62.2071 408.530 58 -2 -2 20 1903.46 449.077 45 -2 2 20 953.416 312.720 45 2 -2 -20 1529.68 260.658 28 -2 -2 20 1545.92 349.500 41 2 -2 -18 652.651 320.279 14 -2 2 18 450.976 394.377 47 2 2 -18 253.696 316.959 38 2 2 -18 322.778 245.553 14 -2 -2 18 784.702 351.273 51 2 -2 -18 187.029 224.854 28 2 2 -18 583.816 389.889 54 -2 2 18 649.988 387.387 41 -2 2 18 446.182 311.640 45 -2 2 18 300.480 227.362 16 2 2 -18 390.527 326.312 44 -2 -2 18 500.165 308.468 41 -2 2 18 921.460 439.453 50 2 2 -18 616.867 312.433 43 2 -2 -18 871.879 281.724 42 -2 -2 18 178.172 373.126 58 -2 -2 18 634.622 271.918 19 -2 -2 16 5795.38 487.495 58 -2 -2 16 6566.16 433.118 19 2 -2 -16 6787.61 449.729 42 -2 2 16 7383.80 448.346 16 -2 2 16 5800.92 530.182 50 2 2 -16 6853.21 573.463 54 -2 -2 16 6641.83 459.078 41 2 -2 -16 6811.56 419.631 28 2 -2 -16 6975.46 483.764 14 2 2 -16 6635.93 520.323 44 -2 -2 16 6784.03 485.885 51 2 2 -16 7066.58 505.092 38 -2 2 16 7435.51 529.064 41 2 2 -16 7151.47 464.610 14 -2 2 16 7068.20 492.192 45 2 -2 -14 32489.7 1397.99 11 -2 -2 14 31080.0 1409.81 45 -2 2 14 33819.1 1482.64 41 -2 -2 14 33134.4 1404.14 41 -2 2 14 31375.2 1432.14 45 2 2 -14 32249.3 1423.51 14 2 2 -14 31789.1 1446.38 25 2 -2 -14 31078.4 1378.59 28 2 2 -14 33021.4 1471.67 38 2 2 -14 30927.8 1419.78 28 2 2 -14 32730.3 1474.42 44 -2 -2 14 33131.2 1386.87 19 -2 2 14 31231.2 1419.82 7 -2 2 14 31765.3 1400.51 16 -2 -2 12 35389.5 1429.36 19 -2 2 12 35471.5 1462.91 7 2 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1 -2 2 6 11923.6 523.671 4 -2 -2 6 10808.1 538.006 19 2 -2 -6 11658.1 490.060 2 -2 2 6 11568.6 539.530 7 -2 -2 6 10673.5 529.488 21 -2 -2 6 12855.6 533.955 2 2 -2 -6 11502.9 476.073 6 -2 2 4 39861.9 1736.30 7 2 -2 -4 45099.4 1726.80 3 2 2 -4 43335.9 1731.65 3 -2 -2 4 42378.1 1744.82 19 -2 -2 4 43044.5 1735.50 1 2 -2 -4 43613.7 1729.59 1 -2 -2 4 42581.6 1738.71 2 2 2 -4 42523.6 1740.71 2 -2 2 4 42727.4 1725.27 4 2 -2 -2 56910.0 2264.13 3 2 2 -2 56218.0 2247.12 3 2 2 -2 55170.1 2269.99 12 -2 -2 2 58097.0 2260.83 2 -2 2 2 57269.0 2253.94 7 -2 2 2 56776.5 2262.71 3 2 2 -2 56402.6 2261.87 2 2 -2 -2 56586.0 2256.51 4 -2 2 0 45035.7 1752.82 3 -2 -2 0 42409.5 1724.53 2 2 2 0 45004.1 1758.42 7 -2 2 0 45091.1 1755.06 8 -2 -2 0 44997.2 1752.32 6 -2 2 0 42403.7 1717.52 7 2 -2 0 45305.3 1736.56 4 2 -2 0 45384.5 1753.13 3 -2 2 -2 73998.0 2901.10 8 2 -2 2 73415.9 2893.46 3 2 2 2 71062.8 2895.59 7 2 -2 2 75948.1 2871.70 1 2 -2 2 70138.3 2890.55 17 -2 -2 -2 73098.3 2887.02 6 -2 -2 -2 70323.7 2886.52 9 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28855.4 1146.62 3 -2 2 -10 30018.0 1167.82 8 -2 2 -10 28514.0 1216.60 30 2 -2 10 28787.3 1205.16 10 -2 -2 -10 26337.3 1182.10 26 2 -2 10 27717.0 1184.28 1 2 2 10 27237.3 1197.61 10 2 2 10 29230.1 1223.51 41 -2 -2 -10 26250.3 1199.99 27 -2 2 -12 1740.93 248.779 30 -2 -2 -12 1794.30 183.103 5 -2 2 -12 1847.33 232.523 38 -2 -2 -12 1777.01 265.065 27 -2 2 -12 1087.06 283.857 42 2 2 12 1384.02 274.578 47 2 -2 12 1594.87 245.603 19 -2 2 -12 1354.21 211.880 25 -2 2 -12 1762.73 177.045 8 2 -2 12 1263.28 275.767 45 2 -2 12 1918.75 270.549 10 2 2 12 1907.86 260.835 41 -2 -2 -14 8140.42 493.625 27 2 2 14 8810.71 600.824 50 2 2 14 7792.63 531.144 41 2 -2 14 7792.18 503.751 10 2 -2 14 7599.68 456.545 19 -2 -2 -14 7715.13 528.290 28 2 2 14 7985.78 570.146 58 -2 2 -14 7933.62 506.897 49 -2 2 -14 8451.13 502.144 38 2 2 14 8306.33 564.495 7 -2 2 -14 8577.44 490.860 30 2 2 14 8550.15 616.727 60 2 2 14 7771.26 559.449 47 2 -2 14 9048.37 565.097 45 -2 2 -14 7063.57 464.824 25 -2 -2 -14 7843.01 536.516 11 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5350.89 595.060 54 2 2 20 6274.34 556.615 41 2 2 20 6103.81 554.335 50 -2 -2 -20 6350.28 598.874 54 2 -2 20 5339.56 572.248 58 -2 2 -20 7223.44 569.203 43 -2 -2 -20 5480.61 451.076 25 2 -2 20 6047.65 503.120 41 -2 -2 -20 5886.73 439.356 14 2 -2 20 5771.61 422.864 51 -2 2 -20 5064.28 407.206 38 2 2 20 4452.28 630.360 58 2 2 20 6497.27 655.882 47 -2 -2 -20 5880.28 463.969 28 -2 -2 -20 6331.85 507.193 42 2 -2 20 6417.57 502.297 45 2 2 22 2781.91 408.749 50 2 -2 22 3255.53 374.662 41 2 -2 22 3500.39 383.407 45 -2 2 -22 2236.68 456.451 54 -2 -2 -22 3292.88 382.397 42 -2 -2 -22 3766.79 384.878 38 -2 -2 -22 3647.35 349.051 28 -2 2 -22 3747.46 423.240 43 -2 -2 -22 3632.87 341.310 25 2 -2 22 2741.96 459.862 58 -2 -2 -22 3872.67 487.340 54 2 2 22 3464.25 489.896 47 2 2 22 3625.09 437.223 41 2 -2 24 567.318 216.073 45 -2 2 -24 503.880 234.685 43 2 2 24 523.122 208.838 50 2 2 24 686.674 295.968 47 -2 2 -24 536.737 297.797 54 2 -2 24 499.983 205.948 41 2 2 24 433.689 239.377 41 -2 -2 -24 586.571 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523.442 43 2 6 -14 3505.95 409.885 32 -2 -6 14 4912.07 529.512 51 2 -6 -14 4637.29 426.540 11 2 6 -14 4607.46 373.998 30 -2 6 14 4232.36 522.851 50 -2 -6 14 4332.87 460.502 19 -2 -6 14 3989.22 473.182 37 2 6 -14 4212.26 487.871 12 -2 -6 14 4447.52 413.103 45 -2 6 12 2994.18 389.066 60 -2 -6 12 2746.44 426.252 19 2 -6 -12 2709.20 371.341 11 -2 6 12 2712.81 448.629 50 -2 -6 12 3051.46 461.283 37 2 6 -12 2893.98 359.546 30 -2 -6 12 2375.76 454.943 51 2 6 -12 2281.96 366.648 32 -2 -6 12 2908.19 408.289 21 2 6 -12 2425.84 447.660 43 -2 -6 12 2993.97 358.796 45 2 6 -10 1273.47 321.495 32 2 6 -10 1304.79 305.603 56 -2 -6 10 1792.14 419.157 51 -2 6 10 1167.29 318.160 60 2 6 -10 1479.21 382.559 43 -2 -6 10 1935.59 317.900 45 2 -6 -10 1297.16 240.600 20 -2 -6 10 1637.29 402.647 21 2 6 -10 1163.80 296.125 30 -2 -6 10 1509.06 381.175 19 -2 6 10 1715.29 402.521 50 -2 -6 10 1050.21 414.543 37 -2 6 8 1168.15 270.837 56 2 6 -8 932.616 395.068 54 -2 -6 8 2220.67 434.673 21 2 6 -8 1364.89 341.103 56 2 6 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2 -6 8 16590.2 906.060 21 -2 6 -8 19049.0 991.076 49 -2 6 -8 16408.2 919.539 30 2 6 8 16708.9 848.266 56 -2 6 -8 16623.7 929.652 52 -2 6 -8 15482.7 918.023 43 -2 6 -8 17850.3 898.090 12 -2 6 -8 16637.7 863.100 56 2 -6 8 15545.2 930.429 45 -2 -6 -8 17479.5 822.425 24 2 6 8 17712.8 902.947 7 -2 -6 -8 18898.1 846.810 9 -2 -6 -8 17552.0 851.094 20 2 6 8 18465.1 983.691 44 -2 6 -8 15479.3 950.631 54 2 -6 10 44127.8 1985.45 45 2 -6 10 44796.1 1969.17 19 -2 6 -10 42404.9 2051.00 54 2 -6 10 43514.5 1931.95 21 -2 6 -10 46230.7 1994.53 12 -2 -6 -10 44349.0 1899.09 20 -2 6 -10 43564.2 2037.23 49 -2 6 -10 40719.6 1977.78 30 -2 6 -10 43328.2 2026.56 43 -2 6 -10 46844.8 1952.72 52 2 6 10 45801.1 1980.52 7 -2 6 -10 41093.6 1882.68 56 2 6 10 44952.0 2062.26 50 2 6 10 44585.9 1981.73 60 -2 -6 -10 48623.8 1928.49 26 2 -6 10 42039.3 2017.57 51 -2 6 -12 11709.1 756.635 12 -2 6 -12 11474.5 819.823 43 2 6 12 12772.8 867.557 50 -2 6 -12 13452.6 755.630 30 -2 6 -12 11512.7 861.793 54 -2 -6 -12 13070.2 711.591 26 -2 -6 -12 13761.4 813.668 11 2 6 12 12328.4 816.370 60 2 -6 12 12346.9 741.623 19 2 -6 12 12907.2 787.412 45 2 -6 12 12660.1 682.445 21 -2 6 -12 12732.7 821.077 49 -2 6 -12 13482.8 702.542 52 2 -6 12 11495.5 727.417 37 2 6 14 831.439 479.794 60 2 -6 14 564.444 306.116 19 -2 6 -14 389.735 274.171 30 -2 6 -14 353.514 384.152 43 -2 6 -14 237.898 296.942 12 -2 -6 -14 362.170 341.546 11 -2 6 -14 381.094 377.373 49 2 6 14 850.442 491.486 50 -2 -6 -14 60.4096 324.884 27 2 -6 14 698.870 371.476 45 2 -6 14 762.445 293.255 37 -2 6 -14-468.384 475.138 54 -2 6 -16 577.059 228.155 30 -2 6 -16 1319.88 349.416 43 2 6 16 398.536 411.396 60 -2 -6 -16 566.907 324.768 28 2 -6 16 522.286 257.791 19 2 -6 16 580.177 392.177 51 -2 -6 -16 1078.46 263.382 27 2 6 16 503.269 436.582 50 2 -6 16 763.399 333.270 45 -2 6 -16 805.803 375.400 54 -2 6 -18 155.975 240.853 43 2 6 18 676.646 302.771 60 -2 -6 -18 428.858 271.789 42 2 -6 18 48.7825 283.616 51 -2 6 -18 686.672 283.700 54 -2 6 -18 191.125 146.521 30 2 6 18 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1167.84 392.080 51 -2 7 11 1422.48 347.812 60 2 7 -11 1157.47 459.523 54 2 -7 -11 450.905 270.664 11 2 7 -9 7462.77 623.005 54 -2 -7 9 6707.32 551.988 51 -2 -7 9 6177.50 530.084 21 2 -7 -9 6496.51 425.140 20 -2 -7 9 6260.46 509.746 19 2 7 -9 6994.55 509.378 56 -2 7 9 6552.29 456.355 56 -2 7 9 6533.72 500.794 60 2 7 -9 6129.63 493.271 32 -2 -7 7 11316.0 691.405 19 -2 7 7 11053.2 676.524 55 -2 -7 7 11100.1 735.323 21 -2 -7 7 10609.3 772.708 37 2 7 -7 10815.9 741.260 54 2 -7 -7 11055.2 604.563 9 2 7 -7 12082.4 732.754 56 2 -7 -7 10505.7 618.023 21 -2 7 7 11161.0 657.873 60 -2 7 7 10669.8 636.006 56 -2 -7 7 12064.6 715.422 51 2 7 -7 10828.9 655.964 32 -2 7 5 13516.3 764.928 55 2 7 -5 14301.6 850.585 54 -2 7 5 13949.2 766.811 60 2 -7 -5 13436.2 760.765 21 -2 -7 5 15259.1 890.839 21 -2 -7 5 15241.8 893.876 37 -2 7 5 12617.6 744.381 56 -2 -7 5 14674.1 803.612 19 2 7 -5 13220.3 748.710 44 2 7 -5 13768.0 798.298 43 2 7 -5 13914.9 756.262 32 2 7 -5 13821.3 831.663 56 -2 -7 3 4468.43 583.594 21 2 7 -3 4777.36 421.151 44 -2 7 3 4488.46 439.089 55 -2 -7 3 5134.52 594.892 37 2 -7 -3 5048.83 432.239 19 -2 -7 3 4584.04 447.754 19 2 7 -3 4882.28 487.799 43 -2 7 3 5458.44 455.734 56 2 7 -3 4339.83 412.491 32 2 7 -3 5253.74 536.127 56 -2 7 3 5074.46 430.868 43 -2 7 1 829.596 302.423 43 2 7 -1 989.054 298.390 44 2 -7 -1 580.006 339.200 19 -2 7 1 976.699 357.031 56 2 7 -1 607.165 368.741 43 -2 7 1 614.414 315.254 55 -2 -7 1 718.400 418.132 37 -2 -7 1 1315.83 439.477 21 -2 7 1 1595.95 383.381 52 2 7 1 11476.1 699.366 43 -2 -7 -1 10883.6 615.731 9 2 7 1 10260.8 705.993 55 -2 7 -1 12368.6 717.733 52 -2 7 -1 10887.8 644.800 30 -2 7 -1 11117.7 664.324 43 2 7 1 10678.4 665.765 56 -2 7 -1 10931.3 635.872 48 -2 -7 -1 10244.6 671.139 21 2 7 1 10407.0 711.855 60 -2 -7 -1 9496.31 662.239 37 2 -7 1 10901.1 673.805 19 2 7 1 10152.8 655.763 44 -2 7 -3 51023.3 2340.73 56 2 7 3 53667.2 2336.85 55 2 7 3 52750.0 2293.95 56 -2 7 -3 54868.1 2301.64 30 -2 -7 -3 55179.8 2272.65 9 2 7 3 55639.2 2325.52 60 -2 7 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7 9 11072.3 748.769 50 2 -7 9 10528.7 706.767 19 -2 7 -9 12048.5 724.251 43 2 7 9 10261.7 616.686 56 -2 7 -9 11208.4 639.036 56 -2 7 -9 11399.6 754.772 54 -2 7 -9 11193.0 707.686 30 2 7 9 11490.4 727.604 60 2 -7 9 10631.8 680.065 21 2 -7 9 11001.0 690.007 45 -2 7 -9 12581.2 716.602 52 -2 -7 -9 10673.3 622.114 20 2 -7 9 9843.02 761.247 51 -2 7 -11 2100.27 292.955 56 2 -7 11 2008.59 315.578 21 2 -7 11 2537.76 494.873 51 -2 7 -11 2955.50 376.064 52 -2 -7 -11 2152.23 388.515 11 2 -7 11 2060.80 396.160 37 2 7 11 2255.71 461.601 60 -2 7 -11 1798.45 422.541 54 2 7 11 2027.60 454.887 50 2 -7 11 2641.21 384.231 45 -2 -7 -11 2251.71 332.504 26 -2 7 -11 2305.15 418.016 43 -2 7 -11 2436.00 371.167 30 2 -7 13 2501.43 325.956 19 2 -7 13 2478.85 344.159 37 -2 7 -13 2523.70 324.876 30 -2 7 -13 1065.72 375.583 54 2 7 13 2398.15 425.849 50 -2 7 -13 1416.34 371.105 43 -2 -7 -13 2141.71 332.139 27 2 -7 13 2468.33 447.018 51 2 7 13 1570.06 428.342 60 2 -7 13 2326.49 342.253 45 2 7 15 2913.58 407.364 60 -2 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4 -12 60451.7 2473.47 44 -4 4 12 57062.2 2453.43 59 -4 -4 12 59123.0 2423.82 51 -4 4 12 54308.9 2462.47 50 4 -4 -12 55110.1 2365.77 11 -4 -4 12 58235.2 2403.00 37 -4 4 12 55609.1 2437.49 47 4 4 -12 58015.3 2473.04 54 -4 -4 12 57875.9 2390.38 45 -4 -4 12 58570.7 2391.27 19 -4 -4 12 51160.5 2371.49 6 -4 4 10 34260.9 1519.29 45 4 4 -10 35591.0 1538.33 12 -4 -4 10 35530.8 1537.25 21 -4 -4 10 34646.8 1553.74 37 -4 -4 10 35864.0 1546.24 19 -4 -4 10 35794.5 1530.52 6 -4 4 10 33806.7 1514.27 39 -4 4 10 34274.5 1538.95 47 4 4 -10 37157.9 1503.17 30 -4 -4 10 37188.9 1529.66 45 4 4 -10 34185.2 1570.15 44 4 4 -10 34173.0 1546.35 43 4 4 -8 19261.0 880.416 43 4 4 -8 18638.4 871.019 12 -4 -4 8 16875.4 845.957 6 -4 4 8 17049.4 868.203 39 4 -4 -8 18202.5 802.573 2 4 4 -8 19684.2 839.518 30 -4 -4 8 19894.4 892.062 19 4 4 -8 19414.6 903.272 44 -4 -4 8 18654.6 893.485 21 4 4 -6 97685.1 3834.63 30 4 4 -6 95695.8 3856.99 12 -4 4 6 91778.4 3873.33 39 -4 -4 6 96998.7 3864.95 19 -4 4 6 93891.0 3813.20 30 -4 -4 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251.325 39 -8 -7 17 1072.81 296.698 57 8 7 -17 1354.73 262.043 32 8 7 -17 1271.00 229.310 44 8 7 -15 2267.17 268.963 43 8 7 -15 2260.45 350.132 32 -8 -7 15 2089.83 395.082 57 8 7 -15 1835.60 340.886 44 8 7 -13 211.273 259.191 43 -8 -7 13 94.5387 421.950 57 8 7 -13 221.653 328.420 32 -8 7 13 407.555 243.016 48 8 7 -13 61.3664 326.761 44 -8 -7 11 4245.70 384.196 24 8 7 -11 4479.18 394.849 43 8 7 -11 3535.87 379.065 56 8 -7 -11 3787.68 327.159 19 -8 -7 11 3823.51 402.803 35 8 7 -11 3984.93 451.110 32 -8 7 11 3820.11 384.704 48 8 7 -11 3481.40 449.189 44 -8 -7 9 11142.9 670.513 24 8 7 -9 12058.2 634.721 43 8 7 -9 9534.82 593.725 60 -8 -7 9 10955.3 833.271 57 -8 7 9 9374.89 552.300 56 8 7 -9 11319.5 682.068 56 -8 -7 9 10115.2 669.350 37 8 -7 -9 8947.22 574.101 19 -8 -7 9 10438.8 695.950 35 8 7 -9 10454.9 659.896 32 -8 7 9 11167.1 620.963 48 8 -7 -9 8973.87 544.887 17 8 7 -9 10000.6 672.161 44 -8 -7 7 6783.17 580.243 24 8 7 -7 7626.85 516.494 43 8 7 -7 7447.91 510.882 60 -8 -7 7 7530.88 691.573 57 -8 7 7 6639.84 479.556 56 8 7 -7 7911.25 654.329 56 8 7 -7 6617.34 537.456 55 -8 -7 7 7487.78 551.077 37 -8 -7 7 6822.71 517.981 20 -8 7 7 7639.70 476.070 52 8 -7 -7 6403.79 480.037 19 -8 -7 7 8330.83 648.883 35 8 7 -7 6716.96 550.644 32 -8 7 7 7668.49 505.991 48 8 -7 -7 6816.84 444.054 17 8 7 -7 6703.94 570.190 44 -8 -7 5 2362.25 446.424 24 8 7 -5 2154.49 365.505 60 -8 -7 5 2040.69 509.724 57 8 7 -5 2033.25 512.602 56 8 7 -5 1735.44 387.511 55 -8 -7 5 2016.24 355.235 20 -8 7 5 2069.16 345.355 52 -8 -7 5 1718.18 487.274 35 8 7 -5 2624.64 439.829 50 8 -7 -5 1669.66 322.120 19 8 7 -5 2026.13 396.518 32 -8 7 5 1500.90 327.435 48 8 -7 -5 1501.52 257.432 17 -8 7 5 1863.62 364.560 56 8 7 -5 1624.91 402.710 44 -8 -7 3 1415.98 393.549 24 8 7 -3 2014.57 373.649 60 -8 7 3 1612.21 403.661 56 8 7 -3 2121.78 499.196 56 -8 -7 3 1979.17 425.915 57 -8 -7 3 1905.21 373.373 20 -8 7 3 2470.85 376.632 52 -8 -7 3 1800.54 507.473 35 8 7 -3 2341.79 458.747 50 8 -7 -3 1421.11 323.160 19 -8 7 3 1667.64 356.452 48 8 -7 -3 1703.94 280.751 17 8 7 -3 2429.29 395.119 55 8 7 -3 1978.05 392.723 46 -8 -7 3 1741.24 399.620 26 8 7 -3 1892.66 393.600 44 -8 -7 1 5061.60 474.844 24 8 7 -1 4579.62 474.262 60 -8 7 1 3512.33 509.425 56 8 7 -1 4255.27 535.587 56 8 7 -1 3703.12 458.861 55 -8 -7 1 4873.45 436.088 20 -8 7 1 5107.15 494.560 52 8 -7 -1 4716.49 425.173 19 -8 -7 1 4813.44 554.633 35 -8 -7 1 3897.51 415.309 57 8 7 -1 4662.80 532.640 50 -8 7 1 5723.03 466.334 48 -8 7 1 5257.26 380.086 30 8 -7 -1 4901.31 394.524 17 8 7 -1 4573.49 491.576 46 -8 -7 1 5005.67 460.685 26 8 7 -1 4140.62 496.770 44 -8 -7 -1 26075.7 1234.01 24 8 7 1 27032.8 1271.36 60 8 7 1 24415.9 1265.13 56 8 7 1 26829.5 1279.86 55 -8 -7 -1 24730.7 1228.33 20 -8 7 -1 25135.8 1304.87 52 -8 -7 -1 26281.5 1269.19 35 8 7 1 25471.5 1327.54 50 -8 7 -1 29723.2 1277.30 48 -8 7 -1 26518.1 1210.25 30 8 7 1 25130.6 1299.91 46 8 -7 1 25721.9 1237.57 45 -8 -7 -1 28166.6 1265.82 26 -8 -7 -3 34579.5 1584.25 24 -8 7 -3 34539.2 1616.78 56 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273.187 30 8 -7 9 2086.71 329.961 45 -8 -7 -9 2911.29 302.488 27 8 7 11 2491.32 332.072 60 -8 7 -11 2481.43 219.846 52 8 -7 11 1931.20 252.339 51 8 7 11 2654.54 334.833 50 -8 -7 -11 2315.64 295.066 49 8 -7 11 2379.26 258.802 45 -8 -8 14 250.226 199.409 39 8 8 -14 206.349 187.898 55 8 8 -14-118.160 183.820 32 -8 -8 14 299.975 257.784 57 -8 -8 12 803.445 257.842 39 8 8 -12 290.529 240.186 55 8 8 -12 25.0866 231.410 32 8 8 -12 156.363 217.177 44 -8 -8 10 1612.46 433.131 57 8 8 -10 1706.31 306.823 55 -8 -8 10 1296.32 274.996 35 8 8 -10 1527.88 292.974 32 -8 8 10 973.079 217.030 48 8 8 -10 1267.62 289.299 44 -8 -8 8 3628.52 377.978 24 8 8 -8 3761.18 342.284 60 -8 -8 8 3527.71 498.483 57 -8 8 8 3345.04 288.879 56 8 8 -8 3703.56 420.941 56 8 8 -8 3678.33 365.014 55 -8 -8 8 3576.65 414.455 35 -8 8 8 3574.79 332.463 48 -8 -8 8 3748.26 335.146 26 8 8 -8 4059.42 382.655 44 -8 -8 6 1201.77 347.424 24 8 8 -6 1578.43 299.610 60 8 8 -6 977.186 402.998 56 -8 -8 6 1262.40 398.300 57 -8 -8 6 999.575 239.108 39 -8 8 6 1153.62 270.197 56 8 8 -6 945.385 299.005 55 -8 -8 6 1344.89 386.238 35 -8 8 6 1580.00 288.155 48 8 -8 -6 1345.21 244.558 45 -8 -8 6 1067.86 291.664 26 8 8 -6 1874.87 319.361 44 -8 -8 4 2882.32 378.299 24 8 8 -4 3028.51 359.762 60 -8 8 4 3186.56 363.004 56 8 8 -4 2833.01 444.865 56 8 8 -4 2791.26 361.354 55 -8 -8 4 2570.47 427.262 35 -8 -8 4 2879.64 376.661 57 -8 8 4 3484.66 345.788 48 8 -8 -4 3209.63 309.672 45 -8 -8 4 2370.64 356.647 26 8 8 -4 2704.94 351.078 44 8 8 -2 7727.80 503.059 60 -8 -8 2 5535.57 420.523 57 -8 8 2 6980.00 523.336 56 8 8 -2 7214.33 494.196 55 -8 8 2 8167.46 506.947 52 -8 8 2 7661.42 477.802 48 8 -8 -2 6556.48 440.641 45 -8 -8 2 6794.83 485.550 26 8 8 -2 6578.01 490.803 44 -8 -8 0 4624.14 394.752 24 8 8 0 6405.82 469.846 60 -8 8 0 5243.22 463.408 56 8 8 0 4713.48 454.484 56 -8 8 0 7563.18 493.438 52 -8 -8 0 5053.98 445.936 35 8 8 0 5631.41 489.135 50 -8 8 0 6152.68 437.851 48 8 -8 0 4863.09 393.897 45 -8 -8 0 4584.11 419.966 26 8 8 0 5618.66 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505.986 19 9 4 5 7010.46 668.707 34 9 4 5 9180.54 701.080 50 -9 4 -5 6974.47 651.902 49 -9 4 -5 9688.64 580.398 48 -9 4 -5 7134.81 596.774 30 9 4 5 8668.61 585.902 47 9 -4 5 7601.28 540.801 17 9 4 5 8230.56 667.649 46 -9 4 -5 7327.35 565.892 8 9 -4 5 9204.06 602.212 45 -9 -4 -5 7238.70 604.269 27 9 4 5 8701.49 585.623 44 9 4 5 8994.52 570.169 7 9 4 7 6739.48 536.404 7 9 4 7 7818.95 692.586 60 9 -4 7 7246.86 631.468 58 -9 -4 -7 5946.94 499.375 11 -9 -4 -7 6954.15 659.596 52 -9 4 -7 7313.21 581.120 52 9 -4 7 5834.74 448.837 19 9 4 7 6647.68 631.258 34 9 4 7 7528.77 663.343 50 -9 4 -7 5919.07 634.337 49 -9 4 -7 7917.10 549.672 48 -9 4 -7 5438.36 549.955 30 9 4 7 7077.70 541.523 47 9 4 7 7106.57 673.017 46 9 -4 7 6178.00 562.335 45 -9 -4 -7 6915.37 597.158 27 9 4 7 6973.09 548.958 44 9 -4 9 1855.56 497.406 58 -9 -4 -9 3456.88 374.499 11 -9 -4 -9 2913.07 509.560 52 -9 4 -9 2822.89 419.842 52 9 -4 9 2805.44 411.291 51 9 4 9 1379.66 499.942 50 -9 4 -9 2853.96 498.284 49 9 4 9 3016.11 611.650 60 9 4 9 3057.73 420.326 47 -9 4 -9 3290.59 437.469 30 9 4 9 2062.01 546.093 46 -9 -4 -9 2908.70 449.200 28 9 -4 9 2481.29 467.060 45 9 4 11 10798.3 782.500 60 9 -4 11 9982.95 733.237 58 -9 -4 -11 9515.59 668.460 52 -9 4 -11 10717.0 645.184 52 9 -4 11 11200.9 616.176 10 9 -4 11 9304.78 591.942 51 9 4 11 11077.8 778.911 50 -9 -4 -11 10660.7 743.238 49 -9 4 -11 11355.6 667.132 30 9 4 11 10323.8 659.025 47 -9 -4 -11 10781.1 673.308 28 9 -4 11 10635.1 677.730 45 9 4 13 6546.36 603.832 60 -9 -4 -13 8379.98 524.187 42 9 -4 13 7253.80 555.650 58 -9 -4 -13 6971.06 467.609 52 -9 4 -13 7320.10 480.729 52 9 4 13 7361.13 593.334 50 -9 -4 -13 8252.26 566.489 49 9 4 13 7171.22 539.453 47 -9 -4 -13 8781.81 513.010 28 9 -4 13 7991.79 509.494 45 -9 -4 -15 1988.38 253.062 42 9 -4 15 2071.85 312.401 58 9 4 15 1823.03 300.272 50 -9 -4 -15 1838.01 297.131 49 -9 4 -15 1882.21 306.903 49 9 4 15 1653.04 301.613 47 -9 4 -15 1709.18 245.976 30 -9 -4 -15 1881.96 253.842 28 9 -4 15 1804.64 236.973 45 -9 -5 22 1087.74 206.123 39 -9 -5 22 1447.88 279.253 51 -9 5 22 908.519 270.888 50 9 5 -22 1515.00 258.818 32 -9 5 22 715.569 170.129 48 9 -5 -22 1111.01 215.080 29 9 5 -22 1219.59 247.361 44 -9 -5 20 632.168 307.964 57 -9 -5 20 393.718 270.638 39 -9 5 20 452.228 279.001 53 -9 -5 20 456.748 314.200 51 -9 5 20 690.348 329.965 50 9 -5 -20 581.745 265.700 29 9 5 -20 1027.04 347.989 44 -9 -5 18 3323.81 470.717 57 9 -5 -18 3461.71 368.370 13 -9 -5 18 3800.16 410.691 39 9 5 -18 2767.18 359.458 54 -9 -5 18 3691.84 437.236 51 -9 5 18 3239.01 452.359 50 -9 5 18 4728.63 498.985 53 9 -5 -18 3247.31 360.400 15 9 5 -18 2475.09 470.351 44 9 -5 -16 7173.03 518.765 13 -9 -5 16 6883.51 615.027 57 -9 -5 16 7831.44 562.529 39 9 5 -16 6635.18 515.384 54 -9 5 16 7027.32 647.900 53 -9 -5 16 6231.02 551.120 51 -9 5 16 5826.86 552.588 50 9 5 -16 5898.22 541.177 46 9 -5 -16 7338.03 532.409 15 9 5 -16 6361.76 627.889 44 9 -5 -14 12202.5 699.598 13 -9 -5 14 10657.8 812.510 57 -9 5 14 12582.0 714.009 57 9 5 -14 12446.2 727.125 54 -9 5 14 13294.2 855.350 53 -9 -5 14 12177.6 722.816 51 9 5 -14 11906.7 793.521 32 9 5 -14 11088.5 758.767 46 9 -5 -14 12085.5 690.293 29 9 -5 -14 12625.6 701.247 15 9 5 -14 12492.8 830.634 44 -9 -5 12 1945.05 321.346 24 9 -5 -12 2436.17 325.978 13 -9 -5 12 1890.08 553.340 57 9 5 -12 1737.19 347.268 7 -9 5 12 2445.37 451.932 57 9 5 -12 1958.32 328.478 56 9 5 -12 2372.62 370.793 54 -9 5 12 2794.54 483.879 53 -9 -5 12 2120.99 353.143 35 9 5 -12 2203.57 432.039 32 9 -5 -12 1762.67 293.204 29 9 5 -12 2442.56 415.650 46 9 -5 -12 2057.10 317.270 15 -9 -5 10 1498.16 349.642 24 9 5 -10 1690.28 283.954 43 9 -5 -10 1536.51 308.910 23 -9 -5 10 2379.13 605.126 57 9 -5 -10 1723.48 286.271 13 9 5 -10 1595.48 326.653 7 -9 5 10 2057.99 494.254 57 -9 5 10 1379.39 260.959 56 9 5 -10 1683.51 366.262 56 -9 5 10 2839.08 461.171 53 -9 -5 10 1526.92 376.909 35 9 5 -10 1849.01 398.515 32 -9 5 10 1276.83 355.165 48 9 5 -10 1604.81 383.669 46 9 -5 -10 1741.73 294.902 15 -9 -5 8 523.805 370.551 24 9 5 -8 1327.93 263.606 43 9 -5 -8 249.330 276.836 23 -9 -5 8 895.278 512.099 57 9 5 -8 944.806 390.360 56 -9 5 8 91.7406 463.379 57 -9 -5 8 457.080 284.939 20 -9 -5 8 862.251 428.704 35 9 5 -8 71.1805 364.614 32 -9 5 8 476.504 289.039 48 9 5 -8 503.749 362.770 46 9 -5 -8 749.095 269.839 15 -9 -5 8 779.303 298.036 26 9 5 -8 694.722 378.245 44 9 5 -8 1110.82 329.068 7 -9 -5 6 26769.1 1285.74 24 9 5 -6 27046.6 1189.47 43 9 -5 -6 25819.8 1191.82 23 -9 -5 6 24969.9 1323.24 57 9 5 -6 25344.3 1304.07 56 9 5 -6 22491.4 1192.81 55 -9 -5 6 25580.3 1237.04 20 -9 5 6 23731.0 1181.86 52 -9 -5 6 27024.8 1331.65 35 9 5 -6 26723.8 1264.78 32 -9 5 6 24851.2 1379.95 57 9 5 -6 25575.4 1218.41 31 -9 5 6 23969.4 1224.18 48 9 5 -6 22941.8 1249.02 46 9 5 -6 29655.6 1253.01 7 9 -5 -6 28558.7 1214.27 15 -9 -5 6 27698.1 1242.67 26 9 5 -6 26580.2 1277.22 44 -9 -5 4 104528. 4074.34 24 9 5 -4 89099.4 3976.59 60 9 -5 -4 98708.1 3988.83 23 -9 -5 4 97867.9 4063.61 57 9 5 -4 100203. 4105.01 56 9 5 -4 89892.8 4009.54 55 -9 -5 4 102667. 4053.79 20 -9 5 4 87934.7 4006.83 52 -9 -5 4 107107. 4130.22 35 9 5 -4 100684. 4058.57 32 9 5 -4 93789.1 4023.89 31 9 -5 -4 102865. 4016.81 17 9 5 -4 94121.9 4063.96 46 9 5 -4 106100. 4056.42 7 -9 -5 4 103113. 4051.21 26 9 5 -4 95836.0 4068.31 44 9 5 -2 56590.4 2518.59 60 -9 -5 2 57002.9 2540.34 57 9 5 -2 59470.3 2541.60 55 -9 -5 2 60929.9 2559.79 20 -9 5 2 60539.0 2579.49 52 9 -5 -2 60053.6 2533.70 40 9 5 -2 59680.8 2567.73 32 -9 5 2 60148.6 2527.65 49 9 5 -2 57341.4 2557.04 31 -9 5 2 61727.4 2614.69 57 -9 5 2 57718.4 2495.87 30 9 -5 -2 61719.0 2531.03 17 9 5 -2 60097.6 2606.13 46 -9 -5 2 62499.5 2563.76 26 9 5 -2 63008.5 2556.36 7 9 5 -2 60293.8 2588.46 44 -9 -5 0 5969.27 526.469 24 9 5 0 6540.27 508.101 60 -9 5 0 6672.47 562.719 57 9 -5 0 6135.57 485.191 40 9 5 0 5816.45 544.744 56 9 5 0 5559.49 488.934 55 -9 -5 0 5216.24 499.390 20 -9 5 0 6423.46 586.897 52 -9 -5 0 5002.71 554.999 35 9 5 0 5268.69 513.487 34 -9 5 0 5950.83 480.033 49 9 5 0 5500.21 517.662 31 -9 5 0 6236.15 498.395 48 -9 5 0 6253.09 436.901 30 9 5 0 6112.47 576.941 46 -9 -5 0 5801.78 517.472 26 9 5 0 5523.96 514.924 44 -9 -5 -2 207.848 365.533 24 9 -5 2 708.581 394.741 58 9 -5 2 608.877 317.662 40 -9 5 -2 568.924 404.063 57 -9 -5 -2 606.107 356.348 20 -9 5 -2 656.760 455.731 52 -9 -5 -2 519.309 413.627 35 9 5 2 585.358 361.813 34 9 -5 2 495.224 316.550 19 -9 5 -2 680.041 354.788 49 9 5 2 948.438 406.058 60 -9 5 -2 425.860 339.063 48 -9 5 -2 766.149 308.729 30 9 -5 2 1021.47 331.040 17 9 5 2 470.769 467.044 46 -9 -5 -2-33.9085 353.311 27 -9 -5 -2 536.767 397.928 26 9 5 2 533.291 361.837 44 9 5 4 6866.05 629.713 60 -9 5 -4 7444.14 585.027 57 9 -5 4 7505.17 592.482 58 -9 -5 -4 6906.57 512.329 11 -9 -5 -4 5600.43 679.123 52 9 -5 4 7362.20 494.721 19 -9 -5 -4 6835.79 572.570 35 -9 5 -4 5824.86 600.731 49 -9 5 -4 7609.19 547.220 48 -9 5 -4 6713.63 546.737 30 9 -5 4 7274.96 519.797 17 9 5 4 6740.20 665.693 46 9 -5 4 7278.52 574.759 45 -9 -5 -4 5488.80 553.938 27 9 5 4 5911.40 535.168 44 9 5 6 45765.4 2056.91 60 9 -5 6 42737.9 1975.19 58 -9 -5 -6 42800.5 1947.51 11 -9 -5 -6 42634.0 2022.47 52 -9 5 -6 43200.8 1983.28 52 9 -5 6 45053.5 1892.10 19 9 5 6 44308.8 2068.20 50 -9 5 -6 39468.3 2016.35 49 -9 5 -6 49282.9 1965.76 48 -9 5 -6 38460.4 1961.87 30 9 5 6 45181.6 2072.03 46 9 -5 6 47935.2 1973.61 45 -9 -5 -6 44547.8 1980.01 27 -9 -5 -6 43587.1 1980.87 26 9 5 6 44125.2 1970.38 44 9 5 8 23755.9 1223.60 60 9 -5 8 19976.3 1098.37 58 -9 -5 -8 20178.9 1038.14 11 -9 -5 -8 21465.2 1134.70 52 -9 5 -8 21741.4 1071.73 52 9 -5 8 20023.1 985.552 19 9 5 8 19214.3 1170.33 50 -9 5 -8 23118.5 1148.05 49 -9 5 -8 19354.1 1072.16 30 9 -5 8 21538.6 1093.95 45 -9 -5 -8 23957.1 1105.26 27 9 -5 10 4783.71 482.748 58 -9 5 -10 3566.97 332.548 56 -9 -5 -10 4586.75 476.423 52 -9 5 -10 4748.47 435.423 52 9 -5 10 3798.09 417.910 51 9 5 10 4755.96 566.992 50 -9 5 -10 5090.20 493.663 49 -9 -5 -10 4850.24 559.336 49 -9 5 -10 4355.20 428.231 30 9 5 10 5026.82 605.501 60 -9 -5 -10 3526.84 428.215 28 9 -5 10 3470.91 451.163 45 9 5 12 1002.33 415.261 60 -9 -5 -12 304.673 292.766 42 -9 -5 -12 227.794 250.827 52 9 -5 12 393.351 280.953 58 -9 5 -12 331.297 255.222 52 9 -5 12 136.283 226.639 51 9 5 12 358.280 378.370 50 -9 -5 -12 102.592 354.773 49 -9 -5 -12 405.943 273.651 28 9 -5 12-113.175 294.187 45 -9 -5 -14 701.896 201.907 42 9 -5 14 195.678 187.388 58 9 5 14-299.905 298.398 60 -9 5 -14 63.5856 142.254 52 9 5 14 184.843 262.490 50 -9 -5 -14 371.632 243.683 49 -9 5 -14-6.31017 229.647 49 -9 5 -14 60.7446 167.168 30 -9 -5 -14 421.832 185.977 28 9 -5 14 106.093 196.087 45 -9 -6 21 116.210 154.035 51 9 6 -21 470.379 186.723 32 9 6 -21 122.765 161.142 44 -9 -6 19 1638.14 308.849 57 -9 -6 19 1205.02 276.724 39 -9 -6 19 1201.64 246.752 51 9 6 -19 1815.18 298.014 32 -9 6 19 1019.72 196.814 48 9 6 -19 1001.63 283.781 44 9 -6 -17 258.863 231.905 23 -9 -6 17 633.827 369.521 57 -9 -6 17 504.880 300.412 39 -9 -6 17 515.144 261.192 51 9 6 -17 246.593 337.117 32 -9 6 17 423.016 258.300 48 9 6 -17 144.911 332.907 44 9 -6 -15 371.018 250.474 23 9 6 -15 551.459 381.230 32 -9 6 15-11.9920 327.493 48 -9 -6 15 555.768 428.905 57 9 6 -15 499.649 382.824 44 9 6 -13 1773.99 296.892 43 9 -6 -13 1484.62 275.789 23 -9 -6 13 1249.05 521.690 57 -9 6 13 1862.68 365.519 57 -9 6 13 1420.69 359.470 48 9 -6 -13 1741.37 272.270 15 9 6 -13 1790.91 451.907 44 9 6 -11 3577.29 354.421 43 -9 -6 11 2773.06 365.814 24 9 -6 -11 2569.76 299.201 23 9 6 -11 3047.62 395.402 56 -9 -6 11 2684.94 410.583 35 -9 6 11 3022.77 487.564 57 -9 6 11 2885.09 405.357 48 9 -6 -11 2673.25 327.292 17 9 6 -11 2902.91 414.376 46 9 -6 -11 3163.91 310.437 15 9 6 -11 3390.39 462.227 44 -9 -6 9 10767.1 717.575 24 9 6 -9 13107.4 655.998 43 -9 -6 9 10976.9 853.339 57 -9 6 9 12302.5 861.786 57 -9 6 9 10118.1 604.525 56 9 6 -9 11990.7 735.715 56 -9 -6 9 12087.4 767.712 35 -9 6 9 10433.3 670.991 48 9 -6 -9 10378.0 623.172 17 9 6 -9 10800.6 703.396 46 9 -6 -9 10639.0 603.366 15 9 6 -9 11207.5 737.303 44 -9 -6 7 14239.7 865.982 24 -9 -6 7 16966.1 992.971 57 -9 6 7 17208.1 1039.78 57 -9 6 7 13816.2 774.280 56 9 6 -7 16661.3 926.148 56 9 6 -7 14188.2 806.608 55 -9 -6 7 12602.8 802.836 20 -9 6 7 15657.7 772.002 52 -9 -6 7 16002.4 943.894 35 9 6 -7 15270.9 862.258 32 -9 6 7 14693.1 816.220 48 9 -6 -7 13873.2 758.684 17 9 6 -7 14757.8 840.461 46 -9 -6 7 14495.2 825.160 26 -9 -6 5 15363.6 897.400 24 9 6 -5 15662.6 803.941 60 -9 -6 5 17569.5 940.440 57 9 -6 -5 14819.6 806.116 40 -9 6 5 18168.6 1032.19 57 9 6 -5 16238.7 956.270 56 9 6 -5 14924.4 827.742 55 -9 -6 5 14784.4 852.921 20 -9 6 5 14847.9 809.483 52 -9 -6 5 15827.9 966.774 35 9 6 -5 15516.1 882.509 32 -9 6 5 14340.9 828.335 48 9 -6 -5 13803.9 781.923 17 9 6 -5 15478.8 864.286 46 -9 -6 5 15113.3 863.369 26 -9 -6 3 10007.5 688.254 24 9 6 -3 10083.1 618.948 60 -9 -6 3 9695.84 671.372 57 9 -6 -3 9525.74 601.549 40 9 6 -3 9623.85 751.787 56 9 6 -3 10061.6 632.633 55 -9 -6 3 9814.09 654.904 20 -9 6 3 9112.45 640.979 52 -9 -6 3 10369.2 755.726 35 9 6 -3 10004.8 684.312 32 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135.095 310.388 30 -9 -6 -7 601.089 366.598 27 9 6 9 178.335 441.309 60 -9 6 -9 453.697 219.672 56 -9 -6 -9 521.089 351.256 52 -9 6 -9 168.954 294.229 52 9 -6 9 122.507 306.258 51 -9 -6 -9 220.206 392.228 49 -9 6 -9 254.040 342.612 49 -9 6 -9 329.324 240.456 30 -9 -6 -9-411.686 310.171 28 9 -6 9 8.81710 340.788 45 9 6 11 949.683 348.614 60 -9 -6 -11 505.029 210.876 52 -9 6 -11 149.314 215.796 52 9 -6 11 252.578 235.141 51 9 6 11 614.050 365.968 50 -9 -6 -11 822.284 309.664 49 -9 6 -11 528.840 266.040 49 -9 6 -11 616.783 202.028 30 -9 -6 -11 525.523 241.919 28 9 -6 11-13.1657 246.162 45 -9 -7 18 263.283 169.367 39 -9 -7 18 366.779 213.874 57 9 7 -18 123.580 170.638 32 9 7 -18 320.713 151.526 44 -9 -7 16 1044.66 332.308 57 9 7 -16 641.294 207.688 55 9 7 -16 567.339 260.297 32 9 7 -16 1234.82 265.977 44 -9 -7 14 226.930 360.904 57 -9 -7 14 61.1837 275.785 39 9 7 -14-105.670 256.296 55 9 7 -14 114.995 278.777 32 -9 7 14 155.446 224.499 48 9 7 -14 21.6519 298.158 44 9 7 -12 2500.66 288.220 43 9 7 -12 2279.72 345.672 55 -9 -7 12 2418.51 397.691 39 -9 -7 12 1773.78 298.274 35 9 7 -12 1589.20 365.153 32 -9 7 12 2351.08 325.910 48 9 7 -12 1862.34 375.821 44 -9 -7 10 2416.22 354.533 24 -9 -7 10 3336.27 570.035 57 9 7 -10 2788.06 391.138 56 9 7 -10 2833.69 366.664 55 -9 -7 10 2369.60 398.929 35 9 -7 -10 1811.00 295.051 19 9 7 -10 3180.26 402.832 32 -9 7 10 3725.94 369.028 48 9 7 -10 2526.30 403.113 44 -9 -7 8 96.7430 368.551 24 -9 -7 8-14.1705 479.178 57 -9 7 8 339.965 267.059 56 9 7 -8 162.558 397.885 56 9 7 -8 188.647 293.474 55 -9 -7 8-487.308 413.843 35 9 -7 -8-273.610 266.755 19 -9 7 8 783.592 282.526 48 9 -7 -8 267.130 207.809 17 -9 -7 8 311.926 286.422 26 9 7 -8-57.3058 329.335 44 -9 -7 6 503.805 362.576 24 9 7 -6 639.116 296.158 60 -9 -7 6 530.163 446.984 57 -9 -7 6 754.450 289.515 39 -9 7 6 510.995 291.450 56 9 7 -6 562.360 465.519 56 9 7 -6 723.598 319.743 55 -9 -7 6 1103.83 328.381 20 -9 7 6 934.238 269.618 52 -9 -7 6 670.928 480.496 35 9 7 -6 677.287 379.889 50 9 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20 -9 7 0 1440.85 421.186 52 -9 -7 0 1242.86 403.319 35 9 7 0 1853.28 442.192 50 -9 7 0 2140.08 399.344 48 -9 7 0 1528.23 255.954 30 9 7 0 1785.81 409.012 46 9 -7 0 1890.59 367.881 45 -9 -7 0 1460.56 390.041 26 9 7 2 103.651 369.951 44 9 7 2 475.140 395.656 60 -9 -7 -2-106.384 450.561 52 -9 7 -2-271.507 392.541 52 -9 -7 -2 47.2297 355.894 35 9 7 2-80.0866 422.927 50 9 -7 2 455.046 296.350 19 -9 7 -2-67.3199 326.790 48 -9 7 -2 357.552 242.964 30 9 7 2-164.189 397.955 46 9 -7 2 291.659 368.309 45 -9 -7 -2-213.409 329.222 27 -9 7 -2 162.040 363.332 56 -9 -7 -2 257.316 327.235 26 9 7 4 562.776 362.261 44 -9 7 -4 325.236 310.511 56 -9 -7 -4-10.8188 422.924 52 9 7 4 317.679 394.825 60 9 7 4 77.3793 403.107 50 -9 7 -4 784.901 272.122 30 9 -7 4 536.499 358.478 45 -9 -7 -4-82.0475 295.874 27 9 7 6 435.711 375.457 60 -9 7 -6 211.543 240.568 56 -9 -7 -6 388.919 376.631 52 -9 7 -6 204.940 311.164 52 9 -7 6 79.0690 347.105 51 9 7 6 427.096 384.144 50 -9 7 -6-84.7596 235.702 30 9 -7 6-8.68241 324.294 45 -9 -7 -6 585.041 293.311 27 9 7 8-186.408 324.634 60 -9 7 -8 132.855 171.606 56 -9 -7 -8 60.8769 262.960 52 -9 7 -8-148.958 237.445 52 9 -7 8-164.571 262.737 51 9 7 8-317.916 353.993 50 -9 -7 -8-114.825 318.290 49 -9 7 -8 98.3303 176.508 30 -9 -7 -8-196.557 224.719 28 9 -7 8-285.735 262.425 45 -9 -7 -8 458.272 230.052 27 -9 -8 13 449.466 192.440 39 9 8 -13 217.993 152.000 55 9 8 -13 43.1819 168.373 44 -9 -8 11 1988.05 263.049 39 9 8 -11 1759.60 244.172 55 -9 -8 11 2053.25 360.068 57 -9 8 11 1521.22 205.689 48 9 8 -11 1659.61 260.097 44 9 8 -9 3635.92 313.667 55 -9 -8 9 3587.23 441.005 57 -9 -8 9 3043.39 292.397 39 -9 -8 9 2929.47 349.685 35 -9 8 9 3528.09 306.379 48 9 8 -9 4021.39 351.974 44 -9 -8 7 1730.63 320.479 24 -9 -8 7 1072.88 349.002 57 -9 -8 7 1464.70 214.417 39 -9 8 7 1648.16 227.103 56 9 8 -7 1504.29 277.111 55 -9 -8 7 1581.70 358.501 35 -9 8 7 1841.14 277.038 48 9 -8 -7 1564.66 229.255 45 9 8 -7 1474.39 284.386 44 -9 -8 5 597.274 307.132 24 9 8 -5 452.584 267.368 60 -9 -8 5 186.714 281.087 57 -9 8 5 448.057 249.691 56 9 8 -5 505.591 257.107 55 -9 -8 5 587.195 369.860 35 -9 8 5 512.254 253.910 48 9 -8 -5 305.163 208.296 45 -9 -8 5 187.469 263.517 26 9 8 -5 259.514 251.901 44 9 8 -3 2046.15 309.821 44 9 8 -3 1966.42 321.695 60 -9 8 3 2312.46 336.931 56 -9 -8 3 1503.25 241.857 57 -9 8 3 2036.42 289.287 48 9 -8 -3 2193.04 264.078 45 -9 -8 3 1188.97 286.710 27 -9 -8 3 2196.35 315.663 26 9 8 -1 10273.7 586.326 60 -9 8 1 9740.38 596.530 56 -9 -8 1 7854.75 648.435 52 -9 8 1 11841.2 595.332 52 -9 -8 1 10146.4 609.000 35 9 8 -1 9664.42 612.283 50 -9 8 1 11286.7 567.930 48 9 -8 -1 8596.04 526.896 45 -9 -8 1 9412.02 559.312 27 -9 -8 1 9485.28 578.567 26 9 8 -1 9822.15 582.321 44 9 8 1 12801.2 696.540 60 9 8 1 12648.6 705.738 50 9 -8 1 11583.1 639.794 45 -9 -8 -1 12507.8 657.885 27 -9 -8 -1 12771.3 673.093 26 9 8 1 13614.9 703.042 44 9 8 3 5988.55 415.263 60 -9 8 -3 6099.05 382.263 56 -9 -8 -3 4649.99 426.284 52 -9 8 -3 6130.90 423.233 52 9 -8 3 4657.41 407.603 51 9 8 3 4851.65 405.606 50 9 -8 3 5352.87 365.887 45 -9 -8 -3 5634.24 369.952 27 -10 0 26 3701.22 395.007 53 10 0 -26 4522.94 405.775 46 10 0 -26 4366.49 312.130 29 -10 0 26 3958.59 364.426 45 10 0 -26 4708.38 379.534 44 10 0 -24 1037.10 384.964 46 10 0 -24 616.069 280.437 29 -10 0 24 968.674 364.277 45 10 0 -24 715.152 332.347 44 -10 0 22-442.824 426.900 51 10 0 -22 136.753 234.857 13 10 0 -22 643.786 346.134 29 -10 0 22 507.696 395.728 45 10 0 -22 645.840 387.192 44 10 0 -20 6995.89 508.124 13 10 0 -20 7290.41 588.026 29 -10 0 20 6995.42 485.146 39 -10 0 20 5513.69 597.492 45 10 0 -20 6194.04 594.442 44 10 0 -18 39484.0 1811.63 13 -10 0 18 40589.8 1910.67 59 -10 0 18 42470.7 1752.33 22 -10 0 18 43819.7 1806.94 39 -10 0 18 39428.3 1899.04 51 10 0 -18 40035.3 1922.19 46 10 0 -18 40913.2 1877.97 29 -10 0 18 38628.6 1864.26 45 10 0 -18 37216.2 1860.97 44 -10 0 18 38928.0 1801.40 57 10 0 -16 45889.0 1909.66 13 -10 0 16 42759.5 1851.80 22 -10 0 16 40316.4 1903.05 57 -10 0 16 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10 1 5 8016.58 588.795 60 10 -1 5 11689.0 699.363 58 10 1 5 9763.02 669.097 58 -10 -1 -5 9607.27 682.023 52 -10 1 -5 9194.04 645.871 52 -10 -1 -5 9174.05 591.594 36 -10 1 -5 8811.75 570.530 36 10 1 5 9663.87 625.492 34 -10 -1 -5 9852.27 651.073 49 -10 1 -5 9153.25 640.457 49 10 1 5 9534.34 616.650 31 10 -1 5 11055.4 616.246 18 10 -1 5 9485.07 635.894 47 10 1 5 8945.83 647.633 47 -10 1 -5 8196.95 527.500 5 10 1 5 10856.3 620.172 46 -10 -1 -5 9825.80 546.611 28 10 1 7 1007.29 371.523 60 -10 -1 -7 1854.11 277.614 42 10 -1 7 1136.27 498.689 58 10 1 7 1466.68 417.668 58 -10 -1 -7 1515.90 428.393 52 -10 1 -7 1335.95 383.653 52 -10 -1 -7 1225.73 319.120 36 10 -1 7 1007.60 359.404 34 10 1 7 1029.00 397.729 34 -10 -1 -7 1543.92 437.044 49 -10 1 -7 1125.49 411.412 49 10 -1 7 1016.06 349.203 18 10 1 7 121.029 431.144 18 -10 1 -7 1994.17 352.214 30 10 -1 7 936.694 475.740 47 10 1 7 560.781 462.966 47 10 1 7 1199.17 368.944 46 -10 -1 -7 1269.29 282.197 28 -10 1 -7 964.361 261.257 28 -10 -1 -9 2015.27 298.038 42 10 -1 9 1095.49 499.852 58 10 1 9 2026.45 489.661 58 -10 -1 -9 1442.76 434.318 52 -10 1 -9 2304.96 429.528 52 -10 -1 -9 2280.21 308.143 36 10 -1 9 1412.32 379.886 34 10 1 9 1312.06 447.475 34 10 1 9 1874.66 421.806 10 -10 -1 -9 2661.18 458.750 49 -10 1 -9 1883.32 434.244 49 10 -1 9 1250.44 392.312 18 10 1 9 1872.33 440.044 18 -10 1 -9 1940.09 359.963 30 10 -1 9 1676.50 536.562 47 10 1 9 1306.47 539.436 47 -10 1 -9 2297.23 327.208 8 -10 -1 -9 2102.19 309.358 28 -10 1 -9 1586.38 300.002 28 -10 -1 -11 8343.39 532.817 42 10 -1 11 9085.87 724.859 58 10 1 11 9750.53 694.387 58 -10 1 -11 8588.35 603.135 52 10 1 11 9825.02 626.360 10 10 1 11 8718.17 692.922 34 -10 -1 -11 9052.39 608.090 52 -10 1 -11 9397.05 611.167 30 10 -1 11 9925.69 748.813 47 -10 1 -11 9133.49 532.422 8 -10 -1 -11 8219.31 544.213 28 -10 1 -11 8281.79 540.960 28 -10 -1 -13 10428.5 601.221 42 10 -1 13 11194.6 763.911 58 10 1 13 10369.3 691.922 58 -10 -1 -13 9810.55 598.807 52 -10 1 -13 10175.7 609.867 52 10 -1 13 11874.0 670.610 10 10 1 13 11425.3 630.858 10 -10 -1 -13 10855.6 693.075 49 -10 1 -13 11209.2 692.023 49 10 -1 13 11291.7 737.571 47 -10 -1 -13 10630.9 603.309 28 -10 1 -13 10216.1 592.906 28 -10 1 -15 1714.25 236.310 43 10 1 15 2353.88 311.319 41 10 -1 15 1346.53 389.151 58 10 1 15 1764.48 355.972 58 -10 -1 -15 1222.79 247.829 42 -10 -1 -15 2006.14 355.041 49 -10 1 -15 1999.70 360.893 49 -10 -1 -15 2043.25 305.946 30 -10 1 -15 2026.17 303.327 30 10 -1 15 1724.14 366.965 47 10 1 15 1727.27 406.905 47 -10 -1 -15 1869.73 268.173 28 10 -1 17 614.391 220.270 41 10 -1 17 561.818 296.623 58 10 1 17 389.655 198.425 41 10 1 17-12.6123 243.451 58 -10 -1 -17 262.098 218.047 49 -10 1 -17 359.946 229.317 49 -10 -1 -17 226.444 184.585 30 -10 1 -17 98.5907 177.661 30 10 -1 17 534.830 230.191 47 10 1 17-97.6123 277.065 47 -10 -1 -17 168.304 155.484 28 -10 2 26 1065.13 236.298 53 10 -2 -26 1444.85 284.940 46 10 -2 -26 1169.53 227.280 29 10 2 -26 1286.58 230.368 46 -10 -2 26 983.171 231.500 45 -10 2 26 1100.41 243.698 45 10 -2 -26 1271.17 215.685 44 -10 2 24 1112.95 343.836 53 -10 -2 24 295.220 340.557 51 -10 2 24 502.620 425.479 50 10 -2 -24 1476.36 359.194 46 10 -2 -24 1412.99 302.072 29 10 2 -24 1020.02 341.053 46 -10 -2 24 633.000 302.402 45 -10 2 24 983.003 319.938 45 10 -2 -24 1000.98 291.204 44 10 2 -24 1172.80 349.236 44 10 -2 -22 776.470 273.083 14 10 -2 -22 1130.43 321.596 13 -10 -2 22 895.407 290.082 39 -10 2 22 697.447 426.308 53 -10 -2 22 688.767 417.687 51 -10 2 22 305.752 476.749 50 10 -2 -22 1030.78 374.849 29 10 -2 -22 1083.44 423.421 46 10 2 -22 971.051 429.310 46 -10 -2 22 644.887 366.798 45 -10 2 22 1288.94 452.132 45 10 -2 -22 837.326 336.090 44 10 2 -22 798.591 411.825 44 10 -2 -20 210.982 302.000 14 -10 -2 20 620.007 334.283 57 -10 -2 20 167.617 301.049 39 -10 2 20 123.432 249.416 39 -10 2 20 802.451 455.398 53 -10 -2 20 299.658 422.810 51 -10 2 20 158.739 512.340 50 10 -2 -20 365.215 430.647 46 10 2 -20 355.981 459.530 46 10 2 -20 53.0713 301.722 29 10 -2 -20 407.159 337.102 13 -10 -2 20 337.773 306.496 16 -10 -2 20-142.905 383.662 45 -10 2 20-134.414 465.662 45 10 -2 -20 132.410 348.858 44 10 2 -20 376.173 436.102 44 10 -2 -18 1455.32 328.590 14 10 -2 -18 1494.66 373.128 13 -10 -2 18 1914.97 295.692 22 -10 -2 18 1509.46 409.922 57 -10 -2 18 1859.70 372.064 39 -10 2 18 1359.00 320.403 39 -10 2 18 999.752 525.102 53 -10 -2 18 1649.19 459.969 51 -10 2 18 882.670 555.316 50 10 -2 -18 1586.55 473.763 46 10 2 -18 1563.31 494.801 46 10 2 -18 1583.34 369.257 29 -10 -2 18 2188.44 377.545 16 -10 -2 18 1185.14 400.571 45 10 -2 -18 1519.21 364.234 44 10 2 -18 1650.35 448.636 44 10 -2 -16 64.2101 268.366 14 -10 -2 16-25.0068 353.721 57 -10 2 16 368.844 333.941 57 -10 2 16-69.7095 239.990 22 -10 -2 16 146.091 358.769 39 -10 2 16-35.4600 348.927 39 -10 2 16 330.798 493.390 53 -10 -2 16 151.816 400.182 51 10 2 -16-225.480 292.983 33 -10 2 16 472.794 494.851 50 10 -2 -16 173.622 334.251 13 10 -2 -16 28.2046 408.566 46 10 2 -16 140.847 460.863 46 10 2 -16 166.353 339.556 29 -10 -2 16 90.1009 298.827 16 -10 -2 16 125.676 320.580 45 10 -2 -16-101.950 288.438 44 10 2 -16 323.395 387.735 44 10 -2 -14 319.612 226.418 14 -10 -2 14 587.881 417.463 57 -10 2 14 94.9139 376.227 57 -10 2 14 515.372 272.193 22 -10 -2 14 202.322 329.648 39 -10 2 14 241.777 375.392 39 -10 -2 14-94.4736 348.118 51 10 2 -14 192.300 285.413 33 -10 2 14 279.099 395.873 50 10 -2 -14-60.9746 348.055 29 10 -2 -14-11.9520 332.852 46 10 2 -14-109.876 389.283 46 10 2 -14 198.815 323.347 29 -10 -2 14 275.038 235.638 16 -10 -2 14 117.776 246.650 45 -10 2 14 44.2850 339.213 45 10 2 -14 138.731 343.882 44 -10 2 12 12544.2 702.217 22 -10 -2 12 10306.2 753.897 57 -10 2 12 11530.5 787.498 57 -10 2 12 10378.6 715.017 39 -10 2 12 10751.0 691.718 53 -10 -2 12 10635.3 627.407 51 10 2 -12 10200.8 609.880 33 -10 2 12 11123.2 659.955 50 10 -2 -12 10802.7 633.217 46 10 2 -12 9494.60 673.088 46 10 -2 -12 10483.8 645.491 29 10 2 -12 10745.9 645.556 29 -10 2 12 9591.24 626.083 45 10 2 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93.3850 180.767 32 10 2 -6 65.1223 213.628 47 -10 2 6-106.776 152.702 8 10 -2 -6-8.08400 223.889 29 10 2 -6-41.8968 292.694 46 10 -2 -6 25.0571 239.582 15 -10 -2 6 1499.93 271.689 26 10 2 -6 201.778 221.121 44 10 -2 -4 618.900 280.267 23 -10 2 4 111.055 274.873 57 -10 2 4 556.814 265.562 22 10 2 -4 486.171 214.925 7 -10 -2 4 473.809 201.046 39 -10 2 4 372.604 217.836 39 -10 2 4 364.611 296.079 36 10 -2 -4 449.345 265.370 33 10 2 -4 300.192 187.202 32 10 2 -4 453.968 224.222 47 -10 2 4 314.753 188.803 8 10 2 -4 438.904 287.234 46 -10 -2 4 318.337 296.651 26 10 2 -4 337.732 198.752 44 10 -2 -2 17129.5 865.421 23 -10 2 2 18059.5 859.972 22 -10 2 2 18079.1 895.851 57 -10 2 2 17318.2 852.411 39 -10 -2 2 18264.5 1025.25 52 -10 2 2 18331.8 934.247 52 -10 2 2 14972.1 901.561 36 10 -2 -2 18123.0 862.601 33 -10 -2 2 17057.4 812.876 39 10 -2 -2 17206.2 881.421 47 10 2 -2 17711.2 860.893 47 -10 2 2 18819.4 885.829 8 10 2 -2 17587.1 894.615 46 -10 -2 2 18296.6 897.303 27 10 2 -2 17751.5 837.918 7 10 2 -2 17754.1 838.684 44 -10 -2 2 20280.5 965.417 26 -10 2 0 20036.4 944.022 22 10 -2 0 20752.5 957.780 40 -10 2 0 20394.5 933.594 39 -10 -2 0 20208.4 1087.11 52 -10 2 0 18350.8 1033.36 52 10 -2 0 19689.9 938.390 33 10 2 0 20290.9 982.186 31 -10 2 0 19161.9 917.734 48 -10 2 0 19813.6 939.238 30 10 -2 0 20958.7 981.578 47 10 2 0 20880.2 976.891 47 -10 2 0 18205.7 977.413 8 10 -2 0 19681.6 911.784 17 10 2 0 19557.5 990.523 46 -10 -2 0 22247.0 1004.95 27 10 2 0 19315.6 924.773 7 -10 2 0 20521.2 980.469 57 -10 -2 -2 830.375 208.291 22 -10 2 -2 2066.26 316.126 57 -10 2 -2 597.840 237.408 22 10 2 2 783.573 229.953 7 -10 2 -2 936.574 220.809 39 -10 2 -2 2330.05 392.169 52 -10 -2 -2 1395.34 375.554 49 -10 2 -2 1324.21 328.423 49 10 -2 2 1219.66 308.702 40 10 2 2 1327.54 352.603 31 -10 2 -2 1042.60 232.294 48 10 2 2 1358.68 355.221 18 10 -2 2 1179.75 315.377 47 10 2 2 2035.79 356.398 47 -10 2 -2 1054.28 275.628 30 10 -2 2 909.841 234.174 17 -10 2 -2 1174.95 322.527 8 10 2 2 1367.01 323.909 46 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369.542 42 10 2 8 2938.43 469.934 60 10 2 8 4107.33 437.949 58 10 2 8 3299.33 379.361 7 -10 -2 -8 3887.26 534.713 52 -10 -2 -8 3513.75 385.065 36 -10 2 -8 3288.65 468.440 52 10 2 8 4692.61 419.737 10 10 2 8 2774.06 542.484 34 10 2 8 3563.67 481.490 50 -10 2 -8 4614.20 493.772 49 -10 -2 -8 3759.66 505.282 49 -10 2 -8 3952.11 441.884 30 10 -2 8 3162.24 403.522 18 10 2 8 3037.24 478.191 18 10 -2 8 2730.36 487.836 47 10 2 8 3444.03 576.975 47 -10 2 -8 3839.80 376.853 8 10 2 8 3377.18 512.475 46 -10 -2 -8 3486.44 389.478 28 10 -2 8 2987.24 375.463 45 -10 2 -8 3300.20 351.031 28 10 2 10 1071.71 433.858 60 -10 -2 -10 2422.97 329.464 42 10 2 10 1698.13 377.144 58 -10 -2 -10 1286.75 427.330 52 -10 2 -10 1635.42 396.311 52 10 -2 10 1544.55 427.354 10 10 2 10 1580.08 479.623 34 10 2 10 2757.75 371.664 10 10 2 10 1328.68 393.671 50 -10 2 -10 1781.71 428.034 49 10 -2 10 1127.04 466.553 47 -10 2 -10 1343.68 372.898 30 10 2 10 2123.28 516.775 47 -10 2 -10 2154.31 293.805 8 -10 -2 -10 2104.40 336.640 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922.686 461.846 46 -11 -4 -5 191.724 311.028 28 11 -4 5 724.649 365.789 45 -11 -4 -5 1465.45 357.943 27 11 4 7 2251.67 460.584 60 11 -4 7 2293.34 493.317 58 -11 -4 -7 2963.16 520.948 52 -11 4 -7 2052.22 413.798 52 11 4 7 1930.55 491.317 50 -11 -4 -7 2504.60 495.801 49 -11 4 -7 1961.83 447.287 49 11 4 7 2980.19 368.991 47 -11 4 -7 2407.97 376.965 30 11 4 7 1509.31 484.959 46 -11 -4 -7 1825.91 339.141 28 11 -4 7 2609.78 412.382 45 -11 -4 -9 3933.68 343.444 42 11 4 9 2873.21 460.676 60 11 -4 9 2935.47 480.381 58 -11 -4 -9 4203.67 465.982 52 -11 4 -9 3830.17 412.717 52 11 4 9 3164.99 475.472 50 -11 4 -9 5310.69 453.287 49 -11 -4 -9 4152.97 485.219 49 -11 4 -9 3727.74 381.607 30 11 4 9 2914.98 365.245 47 -11 -4 -9 4107.43 361.541 28 11 -4 9 2919.11 390.938 45 -11 -4 -11 2366.16 245.198 42 11 4 11 1084.39 339.010 60 11 -4 11 2009.42 388.327 58 -11 -4 -11 1916.45 301.721 52 -11 4 -11 2283.55 299.293 52 11 4 11 1848.23 352.620 50 -11 4 -11 2416.47 347.008 49 11 4 11 1857.96 294.186 47 -11 4 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795.678 274.118 15 11 5 -10 279.200 366.873 44 11 -5 -8 20369.7 983.911 23 -11 -5 8 21205.2 1172.05 57 -11 5 8 20563.6 1201.87 57 -11 -5 8 20536.2 1032.24 39 -11 -5 8 18612.0 1141.09 52 -11 -5 8 19629.3 1148.54 35 11 5 -8 19902.8 1031.43 32 11 5 -8 20124.5 1016.36 31 11 5 -8 20174.2 1062.19 46 11 5 -8 19363.0 1053.96 44 11 -5 -6 39895.1 1679.17 23 -11 -5 6 39219.9 1783.59 57 -11 -5 6 37216.2 1663.79 39 -11 -5 6 34185.2 1856.07 52 -11 5 6 36936.3 1668.10 52 -11 -5 6 36193.7 1830.33 35 11 5 -6 40867.2 1736.00 32 11 5 -6 37621.1 1712.48 31 -11 5 6 38121.1 1711.12 48 11 -5 -6 38527.5 1692.58 47 11 5 -6 38922.9 1756.86 46 -11 -5 6 34383.7 1735.74 26 11 5 -6 40345.7 1755.27 44 -11 -5 4 13662.4 774.838 57 -11 5 4 13555.1 850.140 57 11 -5 -4 12779.2 753.298 40 -11 -5 4 13360.3 940.845 52 -11 5 4 13555.8 752.701 52 -11 -5 4 13832.3 919.708 35 11 5 -4 12734.4 742.194 32 11 5 -4 11753.9 748.730 31 -11 5 4 12623.8 733.033 48 11 -5 -4 13610.2 715.351 47 11 5 -4 13284.2 818.145 46 -11 -5 4 9975.23 718.822 27 -11 -5 4 11340.5 783.061 26 11 5 -4 12417.5 766.112 44 -11 -5 2 382.273 318.617 57 11 -5 -2 428.961 342.706 40 -11 5 2 879.596 455.766 57 -11 -5 2 306.455 572.795 52 -11 5 2 1356.62 416.911 52 11 5 -2 293.556 370.990 31 -11 5 2 1034.71 337.299 48 11 -5 -2 621.418 313.849 17 11 5 -2 613.535 438.584 46 -11 -5 2 870.546 357.388 27 -11 -5 2 193.253 398.863 26 11 5 -2 374.195 348.481 44 11 5 0 192.185 366.995 60 11 -5 0 473.487 414.425 58 11 -5 0 457.219 342.561 40 -11 5 0 378.621 431.899 57 -11 -5 0 163.468 528.480 52 -11 5 0 659.601 430.054 52 11 5 0 179.747 348.219 34 11 -5 0 425.652 297.525 19 -11 5 0 581.336 296.672 49 -11 5 0 339.184 326.179 48 -11 5 0 763.130 245.351 30 11 -5 0 649.170 313.521 17 11 5 0 520.940 459.274 46 -11 -5 0 268.306 346.722 27 -11 -5 0 436.518 381.936 26 11 5 0 462.670 352.252 44 11 5 2 3817.40 433.502 44 11 5 2 3591.55 480.517 60 11 -5 2 3862.94 495.741 58 -11 5 -2 4401.69 484.077 57 -11 5 -2 2833.09 504.464 52 11 5 2 3642.25 450.604 34 11 -5 2 3758.77 376.346 19 -11 5 -2 3945.26 439.293 49 -11 5 -2 3921.78 423.364 48 -11 5 -2 3474.93 368.718 30 11 -5 2 3412.61 354.811 17 -11 -5 -2 3750.48 437.029 27 -11 -5 -2 3350.05 461.183 26 11 5 4 6718.87 603.380 60 11 -5 4 6662.00 589.960 58 -11 -5 -4 6859.74 676.206 52 11 -5 4 6993.66 447.336 19 11 5 4 8161.27 699.336 50 -11 5 -4 6107.96 566.193 49 -11 5 -4 7828.49 534.992 48 -11 5 -4 6154.71 497.242 30 11 -5 4 7171.81 545.345 45 -11 -5 -4 7125.99 529.118 27 11 5 4 5707.73 512.551 44 11 5 6 8777.09 608.834 60 11 -5 6 6173.33 579.489 58 -11 -5 -6 8819.63 656.506 52 -11 5 -6 8141.01 575.485 52 11 5 6 7848.63 666.403 50 -11 -5 -6 8159.50 638.077 49 -11 5 -6 7052.35 574.465 49 -11 5 -6 5994.37 509.929 30 11 5 6 6918.68 641.612 46 -11 -5 -6 7086.47 509.400 28 11 -5 6 7027.81 553.751 45 -11 -5 -6 7804.50 527.367 27 11 5 8 3241.15 423.902 60 11 -5 8 3024.68 434.411 58 -11 -5 -8 3365.49 441.316 52 -11 -5 -8 2419.33 267.247 36 -11 5 -8 3074.09 374.012 52 11 -5 8 2281.11 306.668 51 11 5 8 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5378.69 434.393 15 12 2 -10 3963.51 399.070 44 -12 -2 8 19840.7 1115.77 57 -12 -2 8 18981.9 985.020 39 -12 2 8 19725.2 1006.38 39 -12 2 8 17533.7 982.738 53 12 -2 -8 20571.4 1018.47 33 12 2 -8 18970.2 985.249 33 12 2 -8 18168.9 936.012 47 12 2 -8 18504.4 1039.02 46 12 -2 -8 19936.4 987.525 29 12 2 -8 21701.8 967.849 7 12 -2 -8 21515.7 996.533 15 12 2 -8 18919.3 954.960 44 -12 2 6 28910.5 1297.90 22 -12 -2 6 26536.6 1308.67 57 -12 2 6 25876.5 1312.90 57 -12 -2 6 24301.7 1206.74 39 -12 2 6 26404.1 1243.18 39 -12 2 6 29299.1 1275.34 53 -12 -2 6 26516.3 1383.67 52 -12 2 6 25338.0 1223.31 52 12 -2 -6 28992.4 1289.50 33 -12 2 6 23264.1 1196.97 48 12 -2 -6 28117.1 1316.11 47 12 2 -6 24226.9 1209.08 47 -12 2 6 27410.2 1190.73 8 12 2 -6 27470.6 1307.83 46 12 2 -6 29575.3 1232.17 7 12 2 -6 26296.3 1215.87 44 12 -2 -4 5395.17 477.627 23 -12 -2 4 4526.11 405.020 22 -12 2 4 4969.04 451.433 22 12 -2 -4 4887.85 465.704 40 -12 -2 4 4033.99 457.019 57 -12 2 4 4938.40 496.740 57 -12 -2 4 3999.62 367.217 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557.723 31 12 2 0 9087.03 584.125 18 -12 2 0 6867.13 461.279 30 12 -2 0 7031.63 569.487 47 12 2 0 7343.29 576.823 47 -12 2 0 6112.72 518.965 8 12 -2 0 7351.14 447.946 17 12 2 0 5694.38 547.426 46 12 2 0 8090.17 469.465 7 12 -2 2 27967.2 1340.72 58 -12 2 -2 26664.8 1244.00 57 12 -2 2 25995.0 1288.54 40 -12 -2 -2 28517.1 1394.38 52 -12 2 -2 30080.1 1375.68 52 -12 -2 -2 28579.6 1330.68 49 -12 2 -2 23081.3 1292.33 49 12 2 2 28151.7 1313.36 31 12 2 2 29593.3 1335.42 18 -12 2 -2 24937.4 1264.75 30 12 -2 2 27250.7 1303.96 47 12 2 2 27380.9 1350.61 47 -12 2 -2 27519.3 1286.71 8 12 -2 2 25841.4 1187.01 17 12 2 2 26474.2 1297.33 46 12 2 2 27470.2 1232.87 7 12 -2 4 2375.00 488.807 58 -12 -2 -4 2194.68 502.392 52 -12 -2 -4 2008.73 400.725 36 12 2 4 2751.82 353.979 10 12 2 4 2851.23 417.115 50 -12 -2 -4 2080.28 435.695 49 -12 2 -4 2102.66 409.407 49 12 2 4 2193.44 444.992 31 12 -2 4 2317.32 370.158 18 12 2 4 2153.66 414.836 18 12 -2 4 2431.65 454.101 47 12 2 4 1198.99 508.507 47 -12 2 -4 1601.08 349.407 30 -12 2 -4 2725.80 372.612 8 12 2 4 2686.70 436.343 46 12 -2 4 2425.82 321.593 45 12 -2 6-194.772 516.942 58 -12 -2 -6 481.772 494.160 52 -12 2 -6 301.793 400.194 52 -12 -2 -6 302.253 336.922 36 12 -2 6 45.4628 284.795 34 12 2 6 541.938 282.306 10 12 2 6 339.886 364.936 50 -12 -2 -6 628.679 391.034 49 -12 2 -6 864.538 409.292 49 12 -2 6 112.726 312.863 18 12 2 6 80.9181 435.318 18 12 -2 6-175.243 419.700 47 12 2 6-158.562 470.228 47 -12 2 -6 46.8511 335.760 30 -12 2 -6 38.5685 249.589 8 12 2 6 326.591 374.735 46 12 -2 8-726.415 544.504 58 -12 -2 -8 171.363 411.739 52 -12 2 -8 200.489 377.295 52 -12 -2 -8 98.6363 259.822 36 12 2 8-99.8521 408.167 34 12 2 8 610.947 261.410 10 -12 -2 -8 81.3857 363.167 49 -12 2 -8-33.2217 342.233 49 12 -2 8-166.333 276.078 18 12 -2 8-658.242 451.503 47 12 2 8 52.6764 453.353 47 -12 2 -8-81.3541 293.398 30 -12 2 -8 202.518 235.037 8 -12 -2 -8 136.127 213.859 28 12 -2 10 1564.13 492.592 58 -12 -2 -10 1304.62 366.421 52 -12 2 -10 1824.77 355.615 52 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4701.84 486.314 23 -12 -3 7 4059.63 401.899 39 -12 3 7 4027.72 460.435 39 -12 3 7 5316.60 502.679 53 -12 -3 7 3440.01 571.667 52 12 -3 -7 4145.24 461.239 33 12 3 -7 4051.03 380.490 32 -12 3 7 4084.53 407.056 48 12 3 -7 4176.33 511.718 46 12 3 -7 5117.62 411.717 7 12 3 -7 4528.27 430.957 44 -12 -3 7 4006.48 570.932 57 12 -3 -5 7605.50 540.804 23 -12 -3 5 5869.83 537.546 57 -12 3 5 6944.45 539.677 22 -12 3 5 6488.18 617.093 57 -12 -3 5 5622.36 444.936 39 -12 3 5 7248.15 516.496 39 -12 3 5 5341.55 478.373 52 -12 -3 5 6414.07 735.062 52 12 -3 -5 7794.22 521.516 33 12 3 -5 6950.55 471.218 32 12 3 -5 6749.36 564.609 31 -12 3 5 5710.65 461.906 48 12 -3 -5 6434.78 576.986 47 12 3 -5 7009.35 604.982 46 -12 3 5 7667.98 444.409 8 12 3 -5 6672.65 477.262 7 12 3 -5 6173.64 489.156 44 -12 -3 3 53749.2 2496.01 57 -12 3 3 59050.1 2513.90 22 -12 3 3 57407.7 2542.98 57 -12 3 3 60700.1 2506.10 39 -12 -3 3 59286.0 2684.67 52 -12 3 3 59888.4 2572.15 52 12 -3 -3 59141.7 2490.91 33 12 3 -3 60799.0 2549.61 31 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741.107 17 -12 3 -1 12465.0 804.815 8 12 3 1 16152.2 882.924 46 -12 -3 -1 15658.0 811.940 27 12 3 1 14828.0 770.222 7 12 -3 3 7966.40 659.756 58 -12 3 -3 6866.30 508.814 57 -12 3 -3 7848.04 640.108 52 12 3 3 7903.32 672.519 34 12 3 3 7560.48 621.365 50 -12 -3 -3 7073.26 613.473 49 -12 3 -3 6614.45 564.205 49 12 3 3 7505.34 645.880 31 12 -3 3 7588.28 481.382 18 -12 3 -3 8041.81 491.140 48 12 3 3 6851.53 607.102 18 -12 3 -3 5556.05 505.490 30 12 -3 3 7086.62 564.773 47 12 3 3 6372.97 584.102 47 12 -3 3 6978.15 456.014 17 -12 3 -3 7116.67 544.292 8 12 3 3 6484.09 594.872 46 12 -3 3 8113.19 520.463 45 12 3 5 434.991 335.731 60 12 -3 5 609.157 465.724 58 -12 -3 -5 379.136 490.227 52 12 3 5 139.973 494.726 34 12 3 5 739.884 406.750 50 -12 -3 -5 402.575 397.349 49 -12 3 -5 135.712 373.433 49 12 3 5 170.939 367.789 18 12 -3 5 442.775 385.878 47 12 3 5 364.508 400.786 47 -12 3 -5 170.677 312.185 30 12 3 5 699.648 418.868 46 -12 -3 -5 737.908 250.128 28 12 -3 5 344.296 318.321 45 12 3 7 599.859 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615.331 247.517 58 -12 3 -13 520.916 151.684 52 -12 3 -13 843.152 219.344 49 -12 -3 -13 693.920 185.352 30 12 3 13 546.193 222.950 47 -12 3 -13 529.414 165.828 30 -12 -4 22 1591.96 224.178 57 -12 -4 22 1381.54 236.062 39 -12 4 22 1571.23 293.296 53 -12 -4 22 1149.38 239.065 51 12 -4 -22 2288.51 287.229 33 12 4 -22 2115.05 263.177 32 12 -4 -22 1762.39 246.710 29 12 4 -22 1752.90 239.690 46 12 4 -22 2070.33 296.181 44 12 -4 -20 6235.58 468.991 23 -12 -4 20 6199.34 499.732 57 -12 -4 20 6900.35 487.298 39 -12 4 20 7261.71 577.887 53 -12 -4 20 6952.72 468.809 51 12 -4 -20 6620.60 512.534 33 12 4 -20 6995.30 508.627 32 12 4 -20 8051.30 526.999 46 12 -4 -20 7629.94 484.496 29 12 4 -20 6731.71 533.970 44 12 -4 -18 10519.5 661.487 23 -12 -4 18 9498.34 692.412 57 -12 -4 18 10890.6 652.576 39 -12 4 18 11649.5 601.402 39 -12 4 18 10895.9 779.640 53 -12 -4 18 9060.96 611.037 51 12 -4 -18 10595.9 679.913 33 12 4 -18 10972.4 683.838 32 12 4 -18 10011.5 704.023 46 12 -4 -18 10014.3 646.515 29 12 -4 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15477.9 804.102 7 12 4 -6 14582.7 828.001 44 -12 -4 4 1023.69 375.879 57 12 -4 -4 825.960 427.778 40 -12 4 4 1132.84 467.914 57 12 4 -4 360.643 265.926 7 -12 4 4 757.933 355.928 39 -12 -4 4 678.423 592.763 52 -12 4 4 521.649 345.872 52 12 4 -4 573.738 306.041 32 12 4 -4 747.591 386.762 31 -12 4 4 915.525 328.427 48 12 -4 -4 1155.36 401.277 47 12 -4 -4 486.203 322.933 17 12 4 -4 629.754 332.707 44 -12 -4 2 1104.01 335.945 57 12 -4 -2 948.867 403.215 40 -12 4 2 1264.74 449.315 57 -12 -4 2 916.211 583.550 52 -12 4 2 953.153 425.603 52 12 4 -2 826.147 349.445 34 12 4 -2 549.312 397.854 31 -12 4 2 938.426 309.928 48 12 -4 -2 867.671 361.102 47 12 -4 -2 782.659 284.325 17 -12 -4 2 963.975 359.546 27 12 4 -2 754.389 312.244 44 12 -4 0 877.185 406.297 40 12 -4 0 958.563 463.841 58 -12 4 0 454.967 382.311 57 -12 -4 0 1048.90 573.528 52 -12 4 0-370.757 472.730 52 12 4 0 571.936 393.019 34 -12 -4 0-339.019 439.000 49 -12 4 0 359.765 272.355 49 12 4 0-101.656 437.458 31 -12 4 0 436.311 292.971 48 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484.968 45 12 4 4 5399.85 453.842 44 12 4 6 5365.94 474.801 60 12 -4 6 4346.78 575.757 58 -12 4 -6 5248.35 493.290 52 -12 -4 -6 5177.70 435.722 36 -12 -4 -6 4955.33 563.900 52 12 4 6 4680.10 544.486 50 -12 -4 -6 5597.68 510.355 49 -12 4 -6 5328.42 496.269 49 -12 4 -6 4770.01 426.686 30 12 4 6 5418.46 418.919 47 -12 -4 -6 5513.78 383.054 28 12 4 6 4957.65 555.316 46 12 -4 6 5151.82 450.738 45 12 4 8 3572.66 404.870 60 12 -4 8 4239.67 513.784 58 -12 -4 -8 5113.77 478.333 52 -12 4 -8 4351.74 423.738 52 -12 -4 -8 4174.63 327.979 36 12 4 8 4260.75 481.828 50 -12 -4 -8 4948.83 457.747 49 -12 4 -8 5979.81 458.781 49 -12 4 -8 4881.92 392.574 30 12 4 8 4260.82 367.793 47 -12 -4 -8 5260.46 336.617 28 12 -4 8 4918.98 398.336 45 12 -4 10 1713.86 340.674 58 -12 -4 -10 1642.40 293.949 52 -12 4 -10 2117.31 276.683 52 12 4 10 1871.48 312.469 50 -12 -4 -10 2198.44 320.805 49 -12 4 -10 1857.42 303.092 49 12 4 10 1746.90 247.857 47 -12 4 -10 1660.05 242.808 30 -12 -4 -10 1838.15 198.253 28 12 -4 10 1815.90 225.376 45 -12 -5 21 368.906 180.283 57 -12 -5 21 211.596 175.391 39 12 5 -21 415.486 180.383 32 -12 5 21 75.5918 167.507 48 -12 -5 19 1250.27 329.380 57 -12 -5 19 1535.65 271.208 39 12 -5 -19 1522.15 261.540 33 12 5 -19 1374.66 298.423 32 -12 5 19 1500.60 310.478 48 12 -5 -19 1485.37 218.572 29 12 5 -19 1967.17 247.454 46 12 5 -19 1411.02 324.700 44 12 -5 -17 5613.73 425.064 23 -12 -5 17 5609.33 529.399 57 12 -5 -17 5594.27 427.040 33 12 5 -17 5939.28 478.641 32 -12 5 17 4976.07 502.468 48 12 5 -17 5811.56 464.433 46 12 5 -17 5427.99 500.961 44 12 -5 -15 4014.72 384.802 23 -12 5 15 4858.78 448.638 57 -12 -5 15 4712.53 555.971 57 -12 -5 15 5535.13 495.519 39 12 -5 -15 4200.93 396.682 33 12 5 -15 4163.01 433.131 32 -12 5 15 3089.40 456.781 48 12 5 -15 3893.36 474.049 46 12 5 -15 4842.38 488.733 44 12 -5 -13 808.393 287.282 23 -12 -5 13 899.931 381.567 39 -12 5 13 1122.94 458.514 57 12 -5 -13 753.248 275.672 33 12 5 -13 820.258 323.966 32 -12 5 13 749.150 366.400 48 12 5 -13 1127.49 415.324 46 12 -5 -13 1150.20 278.453 15 12 5 -13 1110.95 383.788 44 12 -5 -11-295.854 279.700 23 -12 -5 11 157.883 536.768 57 -12 5 11 191.254 505.393 57 -12 -5 11 279.045 362.205 39 12 -5 -11 32.1537 239.583 33 12 5 -11 243.035 303.340 32 12 5 -11 268.592 398.152 46 12 5 -11 438.476 374.181 44 12 -5 -9 8.89169 274.186 23 -12 -5 9 376.250 523.856 57 -12 5 9-183.234 533.925 57 -12 -5 9 111.723 324.469 39 -12 -5 9 206.569 420.584 52 12 5 -9 168.311 302.474 32 12 5 -9-86.0854 314.328 31 12 -5 -9 123.353 335.186 47 12 -5 -9-130.044 292.065 17 12 5 -9-62.9573 371.691 46 12 5 -9 35.3161 351.923 44 12 -5 -7 963.908 287.351 23 12 -5 -7 100.047 363.440 40 -12 -5 7 413.905 462.866 57 -12 5 7 721.313 539.198 57 -12 -5 7 439.273 276.570 39 -12 -5 7 632.637 504.671 52 -12 5 7 393.405 251.539 52 12 5 -7 609.120 316.706 32 12 5 -7 566.621 338.244 31 -12 5 7 327.833 317.385 48 12 -5 -7 489.837 327.013 47 12 5 -7 592.500 393.145 46 12 5 -7 46.8697 341.105 44 -12 -5 5 213.810 379.869 57 -12 5 5 574.323 497.171 57 12 -5 -5 296.666 341.834 40 -12 -5 5 161.382 548.422 52 -12 5 5 853.993 304.644 52 12 5 -5 663.458 312.020 32 12 5 -5 375.123 333.272 31 -12 5 5 331.934 312.648 48 12 -5 -5 817.500 322.574 47 12 -5 -5 529.044 305.647 17 12 5 -5 526.064 410.405 46 -12 -5 5 745.523 384.946 26 12 5 -5 343.455 359.000 44 12 -5 -3 1049.10 429.190 58 12 -5 -3 1356.75 355.372 40 -12 5 3 1282.64 462.556 57 -12 -5 3 533.946 316.119 57 -12 -5 3 1129.95 563.719 52 -12 5 3 1257.02 370.157 52 12 5 -3 772.319 370.851 31 -12 5 3 1061.86 360.080 48 12 -5 -3 1254.53 317.612 47 12 -5 -3 1368.09 327.191 17 12 5 -3 1632.18 444.711 46 -12 -5 3 1968.51 423.766 26 12 5 -3 1029.40 341.649 44 12 -5 -1 1212.82 430.547 58 12 -5 -1 808.571 365.408 40 -12 5 1 1099.59 420.706 57 -12 -5 1 1203.30 551.846 52 -12 5 1 1583.74 431.746 52 12 5 -1 803.564 343.823 34 12 -5 -1 822.112 299.581 19 -12 5 1 1334.05 347.443 48 12 -5 -1 978.005 308.112 17 12 5 -1 1215.30 458.790 46 -12 -5 1 1344.28 354.065 27 12 5 -1 972.215 339.524 44 12 5 1 234.398 306.865 44 12 -5 1 1029.65 415.531 58 -12 5 -1 114.393 366.179 57 -12 -5 -1 318.903 488.946 52 -12 5 -1 385.760 396.783 52 12 5 1-161.364 331.299 34 12 5 1 111.343 454.582 50 12 -5 1 50.5105 245.700 19 -12 -5 -1-455.170 438.659 49 -12 5 -1 297.062 286.992 49 -12 5 -1 143.198 310.336 48 -12 5 -1-185.799 215.511 30 12 -5 1 237.330 234.411 17 -12 -5 -1 953.487 314.367 27 12 5 3 563.757 300.877 44 12 5 3 528.447 347.375 60 12 -5 3 360.746 390.968 58 -12 5 -3 542.063 411.775 52 12 5 3 492.868 457.781 50 12 -5 3 403.542 217.791 19 -12 -5 -3 380.201 398.765 49 -12 5 -3 162.277 296.148 49 -12 5 -3 206.571 298.788 48 -12 5 -3 415.496 234.850 30 -12 -5 -3-47.1070 245.763 28 12 -5 3 314.171 329.275 45 -12 -5 -3 1209.94 303.920 27 12 5 5 955.713 322.531 60 12 -5 5 208.973 400.515 58 -12 -5 -5 1304.42 431.825 52 12 5 5 749.481 450.717 50 -12 -5 -5 956.918 382.791 49 -12 5 -5 557.032 304.447 49 -12 5 -5 246.186 229.849 30 12 5 5 608.943 423.095 46 -12 -5 -5 408.675 217.220 28 12 -5 5 300.985 335.739 45 12 5 7 1385.44 277.502 60 12 -5 7 446.316 342.061 58 -12 -5 -7 1705.61 362.873 52 -12 -5 -7 913.876 208.816 36 -12 5 -7 1378.62 302.237 52 12 -5 7 659.577 224.959 51 12 5 7 753.293 366.466 50 -12 -5 -7 1095.73 328.190 49 -12 5 -7 1259.02 302.608 49 -12 5 -7 550.125 231.570 30 -12 -5 -7 995.805 190.882 28 12 -5 7 694.336 280.887 45 12 -5 9 754.644 245.680 58 -12 5 -9 546.308 137.404 56 -12 -5 -9 483.589 237.514 52 -12 5 -9 611.070 214.199 52 12 5 9 952.663 294.108 50 -12 -5 -9 934.324 257.814 49 -12 5 -9 747.828 237.237 49 -12 5 -9 983.780 181.478 30 12 -5 9 586.150 199.866 45 -12 -6 18 1132.34 271.460 57 12 6 -18 1436.46 233.469 32 -12 6 18 1685.23 231.495 48 -12 -6 16 1674.52 355.117 57 -12 -6 16 1577.39 283.183 39 12 6 -16 1161.12 270.892 32 -12 6 16 1363.61 272.521 48 12 -6 -16 1165.25 236.952 47 -12 6 14 157.282 278.019 57 -12 -6 14 308.420 306.346 39 12 6 -14 274.808 280.184 32 -12 6 14-19.6749 268.680 48 12 -6 -14 12.9170 225.201 47 12 6 -14-157.005 245.899 46 12 6 -14-81.8183 315.142 44 -12 -6 12 640.485 461.601 57 -12 6 12 410.645 401.988 57 -12 -6 12 347.152 318.904 39 12 6 -12 446.927 293.073 32 -12 6 12 590.091 315.392 48 12 -6 -12 326.882 230.983 47 12 6 -12 563.004 309.751 46 12 6 -12 495.960 325.800 44 12 -6 -10 91.7859 279.082 40 -12 -6 10 13.1884 459.134 57 -12 6 10-247.920 489.981 57 -12 6 10 99.5664 195.907 56 -12 -6 10 240.643 283.489 39 12 6 -10 271.088 286.040 32 -12 6 10 826.572 327.812 48 12 6 -10 186.241 317.236 46 12 6 -10 381.980 325.151 44 12 -6 -8 4126.31 375.196 40 -12 -6 8 4120.17 531.757 57 -12 -6 8 4548.71 366.227 39 -12 6 8 5632.54 637.169 57 -12 6 8 3705.19 359.702 56 -12 -6 8 4217.62 534.623 52 12 6 -8 4696.59 421.460 32 -12 6 8 4779.54 427.641 48 12 6 -8 4770.98 458.825 46 12 6 -8 4098.69 423.646 44 -12 -6 6 4891.45 488.537 57 12 -6 -6 5359.38 414.286 40 -12 6 6 4809.47 442.189 56 -12 6 6 5462.59 388.702 52 -12 -6 6 4136.01 597.436 52 12 -6 -6 5373.72 375.847 17 12 6 -6 5370.34 484.363 46 12 6 -6 5270.70 465.223 44 12 -6 -4 409.952 320.383 58 -12 -6 4 486.529 298.008 57 12 -6 -4 495.153 277.553 40 -12 6 4 1066.68 448.655 57 -12 -6 4 426.419 516.199 52 -12 6 4 136.642 290.919 52 12 -6 -4 329.850 251.553 19 -12 6 4 261.055 308.107 48 12 -6 -4 572.178 263.147 17 12 6 -4 316.634 358.756 46 -12 -6 4 706.561 342.958 26 12 6 -4 787.982 319.267 44 12 6 -2 930.155 327.962 44 12 -6 -2 1389.29 348.649 58 12 -6 -2 1391.61 300.833 40 -12 6 2 1108.70 390.938 57 -12 -6 2 898.888 511.666 52 -12 6 2 722.019 335.644 52 12 6 -2 1123.53 439.279 50 12 -6 -2 1028.61 273.482 19 -12 6 2 1119.24 325.023 48 12 6 -2 1320.84 393.521 46 12 6 0 1393.06 325.832 44 12 -6 0 2100.64 355.320 58 -12 -6 0 1769.11 478.586 52 -12 6 0 1641.25 379.077 52 12 6 0 2368.05 466.332 50 -12 6 0 1939.16 332.958 48 12 6 0 2153.33 429.393 46 12 -6 0 1922.36 352.559 45 -12 -6 0 2509.31 309.100 27 12 6 2-81.7171 275.739 44 12 -6 2 185.493 309.999 58 -12 6 -2-216.514 346.951 52 -12 -6 -2 35.5270 337.963 49 -12 6 -2 205.298 272.725 48 12 6 2 107.861 386.580 46 12 -6 2 294.067 321.721 45 -12 -6 -2 641.950 236.599 27 12 6 4 1836.58 272.488 60 12 -6 4 1401.53 298.980 58 -12 6 -4 1224.26 248.651 56 -12 -6 -4 1985.72 383.498 52 -12 6 -4 1936.32 319.190 52 -12 -6 -4 1425.46 323.540 49 -12 6 -4 1284.68 198.142 30 12 6 4 1755.81 405.596 46 12 -6 4 1507.12 327.727 45 12 6 6 1675.53 219.896 60 12 -6 6 1178.71 215.247 58 -12 6 -6 2347.59 219.293 56 -12 6 -6 3054.83 293.582 52 -12 -6 -6 2729.00 323.999 52 12 -6 6 2130.91 232.845 51 12 6 6 2457.51 361.804 50 -12 -6 -6 2757.86 293.350 49 12 -6 6 2282.34 286.803 45 -12 -7 13 4062.04 400.333 57 12 7 -13 4774.52 337.561 32 -12 7 13 3867.60 323.516 48 -12 -7 11 3358.64 416.629 57 -12 -7 11 3733.61 275.056 39 12 7 -11 3543.85 287.941 50 -12 7 11 4181.21 327.256 48 12 -7 -9 528.941 184.284 58 -12 -7 9 1052.58 341.175 57 12 -7 -9 1001.77 173.780 40 -12 7 9 889.913 156.523 56 12 7 -9 1056.78 280.354 50 -12 7 9 1008.11 276.751 48 12 7 -9 703.659 236.269 46 12 7 -9 1153.73 263.079 44 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137.040 470.559 46 13 0 -17 29.0400 412.543 29 13 0 -17 178.446 248.868 15 -13 0 17 100.866 360.711 45 13 0 -17 289.947 295.474 44 13 0 -15-63.4711 324.549 23 -13 0 15 61.6621 335.580 22 -13 0 15-306.199 527.364 57 -13 0 15 717.418 447.529 39 -13 0 15-313.342 426.536 53 13 0 -15 79.4974 388.629 33 13 0 -15 56.2068 426.272 46 13 0 -15 269.497 260.931 15 -13 0 15 267.584 322.419 45 13 0 -13-190.836 324.797 23 -13 0 13 218.005 389.070 22 -13 0 13-18.4736 543.143 57 -13 0 13 92.6408 339.373 53 13 0 -13-161.189 372.407 33 13 0 -13 528.748 405.757 46 13 0 -13 27.5870 247.372 15 -13 0 13 142.041 278.927 45 -13 0 11-341.573 408.699 22 13 0 -11 262.610 313.676 23 -13 0 11-281.040 415.987 39 -13 0 11 10.2284 298.290 53 -13 0 11-79.0535 245.435 36 13 0 -11 23.5737 375.257 33 13 0 -11 218.495 364.292 46 13 0 -9-47.9648 284.983 23 -13 0 9 64.8845 515.008 57 -13 0 9 111.185 346.848 39 -13 0 9-150.297 297.206 53 -13 0 9 298.560 320.887 36 13 0 -9 34.5491 385.095 33 13 0 -9-180.873 354.667 47 13 0 -9 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396.109 58 -13 -3 -10 3381.55 313.146 52 -13 3 -10 2867.48 300.947 52 -13 -3 -10 3477.45 327.241 49 -13 3 -10 3529.33 320.034 49 -13 3 -10 3448.10 266.982 30 13 -3 10 3158.73 272.335 47 13 3 10 3259.86 320.328 47 -13 -4 21 31.6379 225.349 57 -13 -4 21-108.756 209.161 39 -13 -4 21 401.819 179.024 53 -13 4 21 215.681 298.126 53 13 -4 -21 131.578 238.502 33 13 4 -21 276.771 199.222 32 -13 4 21 157.865 231.405 48 13 -4 -21 160.024 191.338 29 13 4 -21 20.4304 226.530 46 13 4 -21 228.575 247.337 44 13 -4 -19 458.207 285.944 23 -13 -4 19 265.666 320.208 57 -13 -4 19 400.231 272.807 39 -13 4 19 115.893 388.887 53 13 -4 -19 601.775 312.386 33 13 4 -19 362.397 261.244 32 13 -4 -19 838.315 255.240 29 13 4 -19 368.132 316.445 46 13 4 -19 63.9823 304.469 44 13 -4 -17 61.0832 287.515 23 -13 -4 17 404.711 242.877 22 -13 -4 17 298.867 419.454 57 -13 4 17 282.285 290.176 57 -13 4 17 129.326 277.249 39 -13 4 17-272.353 454.451 53 13 -4 -17-42.5134 353.415 33 13 4 -17-130.793 297.960 32 13 -4 -17 18.8851 259.590 29 13 4 -17-380.113 393.856 46 13 4 -17 165.331 317.379 44 13 -4 -15 2635.00 383.306 23 -13 -4 15 1643.24 539.825 57 -13 4 15 2490.58 456.349 57 -13 -4 15 2722.93 447.636 39 -13 4 15 3442.59 462.361 39 13 -4 -15 2064.14 383.396 33 13 4 -15 2878.70 370.603 32 13 4 -15 2593.57 325.646 31 -13 4 15 874.050 415.008 48 13 -4 -15 2669.92 327.653 29 13 4 -15 2949.51 469.244 46 13 -4 -15 3303.11 365.702 15 13 4 -15 2602.14 404.566 44 13 -4 -13 8634.62 577.669 23 -13 4 13 10549.5 771.221 57 -13 -4 13 8399.97 634.718 39 -13 4 13 9250.26 690.999 39 -13 4 13 9609.00 706.761 53 13 -4 -13 7504.43 570.671 33 13 4 -13 8102.67 556.222 32 13 4 -13 7900.35 573.106 31 -13 4 13 8025.24 603.249 48 13 4 -13 9654.33 685.171 46 13 -4 -13 8345.74 517.131 29 13 -4 -13 8666.35 557.802 15 13 4 -13 7967.13 589.378 44 13 -4 -11 8025.35 553.441 23 -13 -4 11 7597.40 749.459 57 -13 4 11 8356.03 773.279 57 -13 -4 11 7516.38 614.765 39 -13 4 11 8266.69 669.598 39 -13 4 11 9267.18 657.672 53 13 -4 -11 8491.39 556.766 33 13 4 -11 8548.25 542.736 32 13 4 -11 7120.13 566.204 31 -13 4 11 7119.74 563.180 48 13 4 -11 7742.95 638.653 46 13 4 -11 7332.48 556.550 44 13 -4 -9 1136.80 346.512 23 -13 -4 9 1442.38 535.962 57 -13 4 9 1634.28 574.727 57 -13 -4 9 1289.35 347.277 39 -13 -4 9 1786.77 409.043 52 13 -4 -9 1397.64 314.866 33 13 4 -9 1001.50 298.952 32 13 4 -9 1213.29 368.482 31 -13 4 9 1020.18 355.205 48 13 -4 -9 485.052 388.419 47 13 4 -9 1400.63 446.579 46 13 4 -9 830.757 334.301 44 13 -4 -7 4971.68 448.901 23 13 -4 -7 3877.54 467.546 40 -13 -4 7 3963.95 535.685 57 -13 -4 7 3154.35 364.529 39 -13 4 7 4780.24 477.447 39 -13 4 7 3844.76 361.600 52 -13 -4 7 4249.85 600.448 52 13 -4 -7 4952.55 403.335 33 13 4 -7 4303.01 396.269 32 13 4 -7 3963.64 446.643 31 -13 4 7 4046.02 425.946 48 13 -4 -7 3919.07 479.302 47 13 -4 -7 4299.28 412.924 17 13 4 -7 3756.58 425.139 44 13 -4 -5 2652.37 449.822 40 -13 -4 5 2289.49 422.993 57 -13 4 5 2105.35 500.386 57 -13 -4 5 2084.16 595.566 52 -13 4 5 2317.93 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838.920 52 -14 -2 0 12699.2 794.166 36 -14 -2 0 12025.7 727.467 49 14 2 0 12963.8 801.344 31 14 2 0 14771.3 806.273 18 14 -2 0 13417.2 800.759 47 14 2 0 12881.1 806.842 47 -14 2 0 11584.3 737.175 8 14 2 0 12768.1 772.102 46 14 -2 2 5581.49 606.455 58 -14 -2 -2 5532.71 574.823 52 -14 2 -2 5813.51 568.076 52 -14 -2 -2 4044.37 459.936 36 14 2 2 5670.29 587.469 34 14 2 2 5559.73 483.821 50 -14 -2 -2 5479.21 471.654 49 -14 2 -2 4002.15 425.998 49 14 -2 2 5599.13 446.283 18 14 2 2 4941.97 528.325 31 14 2 2 5226.10 515.844 18 -14 2 -2 4177.41 379.010 30 14 -2 2 5669.98 560.038 47 14 2 2 4541.29 541.861 47 -14 2 -2 5378.19 436.912 8 14 2 2 5513.44 495.096 46 14 -2 4-114.188 496.198 58 -14 -2 -4 432.265 315.147 36 14 -2 4 241.423 272.608 34 14 2 4 430.451 319.304 50 -14 -2 -4 337.508 320.073 49 -14 2 -4-75.7812 300.074 49 14 -2 4 124.299 268.139 18 14 2 4-122.663 382.393 18 14 -2 4 276.272 408.910 47 14 2 4-262.272 446.086 47 -14 2 -4-285.875 242.652 30 14 2 4 10.7821 328.073 46 14 -2 6 971.992 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484.016 52 -16 -3 3 7511.56 524.208 36 16 3 -3 7864.28 527.859 34 16 -3 -3 8433.64 542.167 47 16 3 -3 7784.35 535.370 46 16 -3 -3 7202.64 417.487 45 16 -3 -1 5892.34 511.143 58 -16 3 1 4637.77 347.574 57 -16 -3 1 4685.14 459.415 52 -16 -3 1 4218.55 398.223 36 -16 3 1 4108.71 403.947 52 16 3 -1 4405.24 429.783 34 16 3 -1 5091.36 425.388 50 16 -3 -1 4896.83 443.142 47 16 3 -1 4946.46 427.565 46 16 -3 1 3905.27 436.672 58 -16 3 -1 3491.61 359.585 52 -16 -3 -1 3272.11 300.168 36 -16 -3 -1 3634.59 393.812 52 16 3 1 2889.49 354.552 34 16 3 1 3303.15 332.900 50 16 -3 1 3384.70 377.268 47 16 3 1 3450.94 351.220 46 16 -3 3 609.932 337.169 58 -16 -3 -3 744.030 265.220 52 -16 3 -3 945.359 241.810 52 -16 -3 -3 581.274 183.673 36 16 3 3 907.244 271.305 34 16 -3 3 683.442 254.193 47 16 -4 -16 617.088 209.513 40 -16 4 16 754.891 234.127 57 -16 -4 16 844.685 217.147 39 -16 4 16 855.998 224.092 48 16 -4 -16 1039.21 250.673 47 16 4 -16 509.883 237.132 46 16 -4 -14 461.167 228.823 40 -16 -4 14 499.252 342.156 57 -16 4 14 1197.19 354.760 57 -16 -4 14 667.086 241.827 39 16 -4 -14 694.523 188.130 33 -16 4 14 818.261 223.476 48 16 -4 -14 902.543 276.498 47 16 4 -14 932.326 300.638 46 16 -4 -12 1309.60 285.705 40 -16 -4 12 832.638 377.955 57 -16 4 12 1989.32 429.328 57 -16 -4 12 973.546 239.871 39 16 4 -12 1976.96 284.411 31 -16 4 12 1892.66 244.092 48 16 -4 -12 1984.99 303.749 47 16 -4 -10 4938.49 382.864 40 -16 -4 10 4115.37 447.041 57 -16 -4 10 4167.34 351.867 36 16 4 -10 5463.57 404.033 31 -16 4 10 4802.02 342.311 48 16 -4 -10 5374.86 396.938 47 16 4 -10 5133.81 424.821 46 -16 -4 8 10635.9 645.616 57 -16 4 8 14019.7 750.996 57 16 -4 -8 12585.6 639.422 40 -16 -4 8 12523.7 681.606 36 16 4 -8 13266.3 667.335 31 -16 4 8 10815.2 593.148 48 16 -4 -8 12000.4 635.628 47 16 4 -8 12150.7 685.789 46 -16 -4 6 5192.36 394.236 57 -16 4 6 7509.05 504.471 57 16 -4 -6 7071.14 457.344 40 -16 -4 6 5662.37 444.586 52 -16 -4 6 7365.08 511.470 36 16 4 -6 6105.34 435.469 34 16 4 -6 7143.78 472.797 31 -16 4 6 6689.41 385.974 48 16 -4 -6 7081.25 441.479 47 16 4 -6 7223.51 492.523 46 -16 4 4 5793.29 414.172 57 -16 -4 4 5024.78 444.920 52 -16 4 4 5344.48 357.264 52 -16 -4 4 6106.82 455.607 36 16 4 -4 4669.05 387.428 34 16 4 -4 5635.66 431.365 31 -16 4 4 5038.69 320.006 48 16 -4 -4 5438.61 394.180 47 16 4 -4 5904.02 453.670 46 -16 4 2 1866.42 249.624 57 -16 -4 2 1634.06 328.593 52 -16 4 2 1191.75 249.818 52 16 4 -2 1671.14 257.911 34 16 4 -2 2005.69 335.582 50 16 -4 -2 1635.91 260.433 47 16 4 -2 2086.39 324.597 46 16 -4 -2 1550.96 218.048 45 -16 -4 0 297.672 257.262 52 -16 -4 0 326.966 197.746 36 -16 4 0 158.267 211.940 52 16 4 0 227.007 251.570 50 16 -4 0 182.866 193.545 47 16 4 0 517.469 256.444 46 16 -5 -11 1645.90 270.772 58 16 -5 -11 1940.97 227.907 40 -16 -5 11 1377.97 263.713 57 -16 5 11 1927.97 346.030 57 -16 5 11 1292.38 205.879 48 16 -5 -11 1751.17 191.510 47 16 5 -11 1614.72 254.367 46 16 -5 -9 2538.85 277.891 58 16 -5 -9 2575.86 240.905 40 -16 -5 9 1659.90 243.234 57 -16 5 9 1493.28 156.147 56 -16 5 9 2378.96 219.867 48 16 -5 -9 2149.59 203.745 47 16 5 -9 2363.03 284.106 46 16 -5 -7 3743.56 316.277 58 -16 5 7 4446.49 373.739 57 16 -5 -7 3886.33 283.656 40 -16 5 7 2920.89 255.773 56 -16 -5 7 3283.63 316.166 36 -16 5 7 3593.95 257.491 48 16 -5 -5 1694.38 254.933 58 -16 5 5 1351.21 258.266 57 -16 -5 5 844.972 202.950 52 -16 -5 5 987.711 245.878 36 16 5 -5 1505.65 289.882 50 -16 5 5 1113.83 166.122 48 16 5 -5 1303.93 256.345 46 16 -5 -5 1291.44 193.977 45 -17 0 19-45.1485 227.459 57 -17 0 19-13.1194 203.021 39 -17 0 19 227.647 167.756 53 17 0 -19-76.2892 184.035 46 -17 0 17 316.467 328.109 57 17 0 -17-200.147 237.254 47 17 0 -17 433.790 235.270 46 -17 0 15 401.096 398.069 57 -17 0 15-253.594 316.098 39 17 0 -15 266.594 269.262 47 17 0 -15 445.269 242.883 46 -17 0 13-27.2818 446.102 57 -17 0 13 586.895 319.720 22 -17 0 13-225.582 338.670 39 17 0 -13 555.939 316.914 47 17 0 -13-80.9158 225.221 46 -17 0 11 192.288 433.725 57 -17 0 11 235.156 322.342 22 -17 0 11-178.657 281.835 39 17 0 -11 302.486 309.551 47 -17 0 9 108.784 394.889 57 -17 0 9-91.6288 297.184 22 -17 0 9 79.1313 246.373 39 17 0 -9 273.785 299.208 31 17 0 -9 272.423 327.834 47 -17 0 7-153.647 325.462 57 -17 0 7-126.297 232.327 22 -17 0 7 60.4337 197.520 39 17 0 -7 358.783 284.876 31 17 0 -7 485.548 338.429 47 -17 0 5-90.2731 274.952 57 -17 0 5 195.043 256.286 52 17 0 -5 87.6867 277.490 31 17 0 -5 185.239 351.510 47 -17 0 3-9.39119 281.695 52 17 0 -3 201.607 256.979 31 17 0 -3 391.438 362.379 47 -17 0 1 139.794 297.606 52 17 0 -1 389.137 303.445 34 17 0 -1-305.581 364.876 47 -17 0 -1-28.7994 273.108 52 17 0 1 221.680 281.076 34 17 0 1-107.387 320.331 47 -17 0 -3 88.7776 223.343 52 17 0 3 88.0565 210.727 34 17 0 3-37.0695 262.924 47 -17 -1 18 312.449 283.350 57 -17 1 18 129.489 253.116 57 -17 1 18 404.321 243.958 39 -17 1 18 394.199 216.823 53 17 -1 -18 29.7103 226.143 33 -17 1 18 217.842 140.188 48 17 -1 -18 177.268 240.464 47 17 1 -18 15.5950 245.640 46 -17 -1 16 2043.85 421.980 57 -17 1 16 1917.30 385.300 57 -17 -1 16 2168.72 345.551 39 -17 1 16 1827.66 267.907 53 17 -1 -16 2005.04 298.926 33 17 -1 -16 2218.10 345.054 47 17 1 -16 1934.12 312.961 46 -17 1 14 5606.50 572.723 57 -17 -1 14 6031.22 455.785 39 -17 1 14 6040.87 485.993 39 17 -1 -14 5889.38 461.057 47 17 1 -14 4947.31 381.523 47 17 1 -14 5432.80 430.577 46 17 -1 -12 1529.00 306.337 58 17 -1 -12 1380.37 235.856 40 -17 -1 12 1389.06 322.528 22 -17 -1 12 1449.66 452.953 57 -17 1 12 1447.58 471.585 57 -17 -1 12 1433.30 320.477 39 -17 1 12 1866.86 345.201 39 17 -1 -12 1647.18 368.790 47 17 1 -12 1895.38 301.126 47 17 1 -12 1539.82 306.954 46 17 -1 -10 1700.50 316.973 58 17 -1 -10 2162.64 259.691 40 -17 -1 10 2320.73 353.766 22 -17 -1 10 1592.26 422.201 57 -17 1 10 2084.16 449.988 57 -17 1 10 2342.89 373.885 22 -17 -1 10 1897.73 284.215 39 -17 1 10 2343.93 326.265 39 17 1 -10 1728.61 344.616 31 17 -1 -10 2599.54 401.525 47 17 1 -10 2326.88 329.052 47 17 1 -10 1658.09 298.771 46 17 -1 -8 6231.37 463.500 58 -17 -1 8 6972.86 465.305 22 -17 1 8 7113.62 476.868 22 -17 -1 8 6007.21 518.131 57 -17 1 8 6679.18 540.706 57 17 -1 -8 6434.36 419.232 40 -17 -1 8 6968.19 410.319 39 -17 1 8 6545.76 425.891 39 -17 -1 8 6726.14 491.491 36 17 -1 -8 6706.49 447.871 31 17 1 -8 7295.81 511.135 31 17 -1 -8 7669.91 539.097 47 17 1 -8 6855.44 480.083 47 17 1 -8 6584.80 449.933 46 17 -1 -6 4701.46 405.167 58 -17 1 6 3446.61 326.939 22 -17 1 6 4376.13 399.382 57 -17 -1 6 3488.82 371.599 57 -17 1 6 4307.86 303.911 39 -17 -1 6 3470.18 346.688 52 -17 1 6 3797.58 322.421 52 -17 -1 6 4277.04 417.036 36 17 -1 -6 3594.64 330.337 31 17 1 -6 4086.58 408.641 31 17 -1 -6 4124.35 436.666 47 17 1 -6 3942.54 401.204 47 17 1 -6 3382.31 330.815 46 17 -1 -4 1552.61 333.814 58 -17 -1 4 1127.63 249.369 57 -17 1 4 1316.78 283.893 57 -17 -1 4 1338.05 309.647 52 -17 1 4 1048.09 281.421 52 -17 -1 4 1391.11 347.012 36 17 1 -4 1237.27 312.522 31 17 -1 -4 1721.14 392.502 47 17 1 -4 1523.08 338.202 47 17 -1 -2 768.295 321.374 58 -17 -1 2 664.414 302.711 52 -17 1 2 311.370 280.571 52 17 -1 -2 947.738 297.467 34 17 1 -2 842.509 277.458 31 17 1 -2 532.276 331.124 47 -17 -1 0 5290.98 422.532 52 -17 1 0 5335.88 429.314 52 17 -1 0 6308.60 408.159 34 17 1 0 5581.95 447.271 34 17 1 0 5215.98 441.747 47 -17 -1 -2 10836.4 566.084 52 -17 1 -2 10184.4 557.079 52 17 1 2 11000.7 583.134 34 17 -1 2 10344.8 616.252 47 17 1 2 11265.2 586.167 47 -17 -2 17-66.9516 291.507 57 -17 2 17 118.836 256.774 57 -17 -2 17 441.551 253.704 39 -17 2 17 188.160 217.733 39 17 -2 -17 328.475 220.126 33 17 2 -17 185.541 219.429 31 -17 2 17 106.384 160.194 48 17 -2 -17-28.7467 251.485 47 17 2 -17-366.398 280.990 46 17 -2 -15 2573.90 270.900 40 -17 2 15 2709.55 415.146 57 -17 -2 15 2794.38 333.713 39 17 -2 -15 2972.26 322.574 33 17 2 -15 2750.47 336.072 31 -17 2 15 2347.64 240.021 48 17 -2 -15 3109.07 357.370 47 17 2 -15 2889.50 354.529 46 17 -2 -13 5332.43 362.052 40 -17 -2 13 4628.39 522.507 57 -17 -2 13 5128.79 393.022 39 -17 2 13 5505.99 432.510 39 17 2 -13 5039.27 407.743 31 -17 2 13 3785.42 296.903 48 17 -2 -13 5188.60 429.961 47 17 2 -13 5066.62 429.407 46 17 -2 -11 248.567 311.141 58 17 -2 -11 500.664 237.931 40 -17 -2 11 479.899 411.691 57 -17 2 11 543.646 408.104 57 -17 -2 11 625.567 236.769 39 -17 2 11 390.616 285.572 39 -17 -2 11 302.150 188.046 36 17 2 -11 511.757 312.229 31 17 -2 -11 522.504 320.634 47 17 2 -11 586.867 281.132 46 17 -2 -9 576.752 319.986 58 17 -2 -9 352.199 229.858 40 -17 -2 9-155.768 348.594 57 -17 2 9 31.7293 376.901 57 -17 -2 9 295.983 184.876 39 -17 2 9 406.378 242.174 39 -17 -2 9 325.879 246.138 36 17 2 -9 260.883 286.165 46 17 -2 -7 145.228 295.688 58 17 -2 -7 367.375 249.475 40 -17 -2 7-179.073 277.541 57 -17 2 7 335.018 318.021 57 -17 2 7-55.7628 202.688 39 -17 -2 7 98.4997 304.673 36 17 2 -7 413.127 283.910 31 17 2 -7 210.377 244.799 47 17 2 -7 137.823 263.093 46 17 -2 -5 4282.68 411.055 58 -17 -2 5 3437.88 321.768 57 -17 2 5 4074.32 377.748 57 -17 -2 5 3750.00 373.503 52 -17 2 5 4031.64 331.882 52 -17 -2 5 5693.65 451.796 36 17 2 -5 5330.49 426.376 34 17 2 -5 4770.18 405.731 31 17 -2 -5 5057.83 436.999 47 17 2 -5 3906.68 369.289 47 17 2 -5 4348.02 368.959 46 17 -2 -3 12596.8 667.417 58 -17 2 3 10695.0 577.488 57 -17 -2 3 10018.4 631.557 52 -17 2 3 9766.21 608.666 52 -17 -2 3 13792.8 669.985 36 17 2 -3 12943.2 670.061 34 17 2 -3 10733.1 585.932 50 17 2 -3 11967.8 650.962 31 17 -2 -3 13531.6 681.878 47 17 2 -3 9979.10 608.719 47 17 2 -3 11877.4 609.804 46 17 -2 -1 8830.34 567.862 58 -17 -2 1 9822.03 558.078 52 -17 2 1 8644.04 526.887 52 -17 -2 1 9216.73 512.392 36 17 -2 -1 8995.97 487.302 34 17 2 -1 8592.04 546.308 34 17 -2 -1 9890.58 592.802 47 17 2 -1 8779.78 518.401 47 17 -2 1 3208.66 363.718 58 -17 -2 -1 3697.81 331.511 52 -17 2 -1 4427.94 338.904 52 17 2 1 3917.70 302.043 47 17 -2 1 3530.86 381.667 47 -17 3 16 1373.04 267.408 57 -17 -3 16 1483.39 233.900 39 -17 3 16 1680.92 249.157 39 17 -3 -16 1407.41 214.073 33 -17 3 16 1097.63 189.496 48 17 3 -16 1419.89 276.149 46 17 -3 -14 2399.98 257.830 40 -17 -3 14 2269.91 371.265 57 -17 3 14 2847.50 393.676 57 -17 -3 14 2133.07 269.730 39 -17 3 14 2106.07 216.556 48 17 3 -14 1808.47 263.965 31 17 -3 -14 2308.36 322.515 47 17 3 -14 2367.69 308.875 46 17 -3 -12 2173.27 259.094 40 -17 -3 12 1587.57 373.234 57 -17 -3 12 1720.02 228.017 39 -17 3 12 2303.10 318.009 39 17 3 -12 1672.53 285.469 31 -17 3 12 1684.87 199.078 48 17 -3 -12 1984.53 299.267 47 17 3 -12 1647.37 315.220 46 17 -3 -10 2542.25 336.345 58 17 -3 -10 2826.38 286.837 40 -17 -3 10 1946.21 351.561 57 -17 3 10 2952.24 427.080 57 -17 -3 10 2375.95 257.335 36 17 3 -10 2646.44 290.400 34 17 3 -10 2700.45 319.794 31 -17 3 10 1671.60 200.404 48 17 -3 -10 3065.96 340.129 47 17 3 -10 2258.83 319.340 46 17 -3 -8 2608.34 342.461 58 17 -3 -8 2325.33 284.622 40 -17 -3 8 2000.77 304.694 57 -17 3 8 2586.53 374.985 57 -17 -3 8 2693.29 311.638 36 17 3 -8 2883.89 313.010 34 17 3 -8 2596.47 316.705 31 17 -3 -8 3369.24 350.964 47 17 3 -8 2418.17 331.384 46 17 -3 -6 1208.39 308.117 58 -17 -3 6 566.140 201.735 57 -17 3 6 837.451 292.078 57 -17 -3 6 559.173 221.377 52 -17 -3 6 804.089 275.409 36 17 3 -6 732.199 253.165 34 17 3 -6 785.412 268.685 31 17 -3 -6 1476.29 302.916 47 17 3 -6 951.506 279.481 46 17 -3 -4 799.603 301.888 58 -17 3 4 214.083 224.957 57 -17 -3 4 101.025 241.307 52 -17 -3 4 170.390 245.862 36 -17 3 4 382.095 188.292 52 17 3 -4 7.44470 232.563 34 17 3 -4 415.713 248.361 50 17 -3 -4 371.529 267.725 47 17 3 -4 534.462 242.418 46 17 -3 -2 228.400 298.743 58 -17 -3 2-183.122 248.061 52 -17 3 2 130.981 198.103 52 17 3 -2 253.775 243.591 34 17 3 -2 348.029 214.061 50 17 -3 -2-55.1417 253.539 47 17 3 -2 216.740 211.817 46 -17 -3 0 1298.05 243.613 52 -17 3 0 1347.97 218.998 52 -17 -3 0 1232.83 190.109 36 17 3 0 1510.56 240.067 34 17 -3 0 825.543 236.200 47 17 -4 -11 343.857 235.391 58 17 -4 -11 451.406 199.137 40 -17 -4 11 218.083 240.888 57 -17 4 11 168.364 138.401 48 17 -4 -11 663.116 203.227 47 17 4 -11 396.084 234.481 46 17 -4 -9 1507.71 267.395 58 17 -4 -9 1438.19 211.469 40 -17 -4 9 992.033 216.912 57 -17 4 9 1418.68 329.479 57 -17 4 9 1125.97 154.537 48 17 -4 -9 1491.57 220.439 47 17 4 -9 1382.14 247.910 46 17 -4 -7 1647.16 287.452 58 -17 4 7 1427.15 274.045 57 -17 -4 7 987.704 231.772 36 17 -4 -7 1022.12 206.045 47 17 4 -7 1426.27 262.496 46 -17 4 5 629.452 208.777 57 -17 -4 5 423.409 167.829 52 -17 -4 5 653.547 219.351 36 17 4 -5 938.546 242.697 50 17 -4 -5 430.243 183.986 47 17 4 -5 738.924 226.141 46 -18 0 16 969.116 290.825 57 -18 0 16 819.767 225.278 39 18 0 -16 870.993 178.473 47 -18 0 14 140.357 223.481 39 18 0 -14 387.357 219.736 47 -18 0 12 759.546 386.252 57 -18 0 12 683.198 225.972 39 18 0 -12 689.691 240.104 31 18 0 -12 725.321 260.897 47 -18 0 10 7646.48 542.018 57 -18 0 10 7830.86 444.304 39 18 0 -10 8674.35 487.717 31 18 0 -10 8613.21 506.962 47 -18 0 8 16199.9 840.437 57 18 0 -8 17557.9 825.761 31 18 0 -8 18797.5 861.787 47 -18 0 6 5851.10 383.547 57 18 0 -6 6398.00 397.945 31 18 0 -6 6708.92 453.993 47 -18 0 4 2008.86 238.245 52 18 0 -4 3042.24 321.951 34 18 0 -4 2385.10 331.943 47 -18 0 2 858.966 214.408 52 18 0 -2 1180.14 257.764 34 18 0 -2 541.377 290.906 47 -18 1 15 698.337 331.641 57 -18 -1 15 640.112 227.014 39 -18 1 15 1098.82 253.684 39 18 -1 -15 756.679 232.331 47 18 1 -15 885.129 202.214 46 -18 -1 13 989.371 357.688 57 -18 1 13 944.753 371.104 57 -18 -1 13 798.384 227.352 39 -18 1 13 1016.40 247.449 39 18 1 -13 1403.65 278.001 31 18 -1 -13 1590.08 286.550 47 18 1 -13 938.422 206.124 46 18 -1 -11 519.070 204.642 58 -18 -1 11 292.981 323.925 57 -18 1 11 459.394 334.194 57 -18 -1 11 373.131 184.823 39 -18 1 11 250.950 197.748 39 18 -1 -11 97.7021 190.287 31 18 1 -11 261.930 241.226 31 18 -1 -11 869.614 269.694 47 18 1 -11 260.795 215.595 47 18 1 -11 429.539 182.366 46 18 -1 -9 551.678 225.756 58 -18 -1 9 73.1693 275.004 57 -18 1 9 112.560 300.504 57 -18 1 9 118.835 171.516 39 18 -1 -9 276.017 181.783 31 18 1 -9 201.615 229.164 31 18 -1 -9 480.110 289.782 47 18 1 -9 155.275 234.367 47 18 -1 -7 351.888 225.366 58 -18 -1 7 80.1825 215.365 57 -18 1 7 380.804 252.409 57 18 1 -7 81.2919 229.173 31 18 -1 -7 222.120 292.539 47 18 1 -7 55.8115 242.106 47 18 -1 -5 1394.45 254.989 58 -18 1 5 1977.61 227.713 57 -18 -1 5 1561.15 214.945 52 18 1 -5 2056.90 306.367 34 18 1 -5 2024.18 270.742 31 18 -1 -5 2587.57 346.988 47 18 1 -5 1681.99 279.833 47 18 -1 -3 2340.28 270.565 58 -18 -1 3 3219.76 282.989 52 -18 1 3 3172.36 267.150 52 18 -1 -3 4752.27 325.790 34 18 -1 -3 4316.77 362.914 47 18 1 -3 3550.85 323.058 47 18 -2 -14 1259.29 211.222 58 -18 -2 14 1427.66 311.137 57 -18 2 14 1554.85 330.904 57 -18 2 14 1844.50 240.977 39 18 -2 -14 1925.15 271.157 47 18 2 -14 1777.01 235.983 46 18 -2 -12 77.3646 207.406 58 -18 -2 12 81.4148 303.707 57 -18 2 12 631.085 333.976 57 -18 2 12 181.442 198.752 39 18 2 -12 424.985 231.485 31 18 -2 -12 259.890 238.778 47 18 2 -12 316.180 198.175 46 18 -2 -10 3287.45 300.670 58 -18 -2 10 2660.53 330.789 57 -18 2 10 3226.18 386.438 57 -18 2 10 3849.90 279.212 39 18 -2 -10 3266.97 326.204 47 18 2 -10 3061.39 280.079 46 18 -2 -8 2997.15 305.173 58 -18 -2 8 2711.23 273.216 57 -18 2 8 2897.48 320.332 57 18 2 -8 3647.72 317.193 34 18 2 -8 3562.27 314.890 31 18 2 -8 2690.14 255.306 46 18 -2 -6 1107.47 261.008 58 -18 2 6 1409.72 226.931 57 -18 -2 6 1031.59 239.697 36 18 2 -6 1601.40 256.930 34 18 2 -6 1327.25 243.816 31 18 -2 -4 328.729 236.848 58 -18 2 4 436.910 142.470 57 -18 -2 4 334.147 170.797 52 -18 2 4 486.212 136.994 52 18 2 -4 509.635 229.030 34 18 -2 -4 541.565 246.983 47 0 0 0 0.00 0.00 0 TITL s4957r in I2/a REM I2/a (#15 in standard setting) CELL 1.54184 15.660138 8.154542 23.522272 90.0000 108.5072 90.0000 ZERR 12.00 0.000299 0.000128 0.000484 0.0000 0.0021 0.0000 LATT 2 SYMM -x+1/2, y,-z SFAC C H N O UNIT 132.00 120.00 12.00 12.00 TREF HKLF 4 END ; _shelx_hkl_checksum 40614 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.836 _oxdiff_exptl_absorpt_empirical_full_min 0.610 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mn1 Mn 0.250000 0.13699(9) 0.500000 0.0521(3) Uani 1 2 d S T P . . S2 S 0.42256(8) 0.21547(16) 0.52792(6) 0.0779(4) Uani 1 1 d . U . . . S1 S 0.29508(8) 0.34180(16) 0.58749(6) 0.0789(4) Uani 1 1 d . U . . . O1 O 0.4544(2) 0.4483(5) 0.6113(2) 0.1000(13) Uani 1 1 d . U . . . C1 C 0.3929(3) 0.3422(5) 0.5763(2) 0.0718(11) Uani 1 1 d . U . . . N006 N 0.2490(3) -0.0801(5) 0.4385(2) 0.0905(14) Uani 1 1 d . . . . . C2A C 0.5399(14) 0.468(2) 0.6051(9) 0.111(5) Uani 0.673(11) 1 d D U . A 2 H2AA H 0.535707 0.535851 0.570421 0.133 Uiso 0.673(11) 1 calc R . . A 2 H2AB H 0.564317 0.362408 0.599519 0.133 Uiso 0.673(11) 1 calc R . . A 2 C5 C 0.624(2) 0.816(2) 0.7050(15) 0.102(6) Uani 0.327(11) 1 d D U . A 1 H5A H 0.687499 0.818973 0.728265 0.122 Uiso 0.327(11) 1 calc R . . A 1 H5B H 0.619522 0.853272 0.664906 0.122 Uiso 0.327(11) 1 calc R . . A 1 C9 C 0.3151(5) -0.0589(11) 0.4061(4) 0.136(3) Uani 1 1 d . . . . . H9A H 0.299766 0.036465 0.381004 0.205 Uiso 1 1 calc GR . . . . H9B H 0.314255 -0.153853 0.381842 0.205 Uiso 1 1 calc GR . . . . H9C H 0.374148 -0.045527 0.434520 0.205 Uiso 1 1 calc GR . . . . C8 C 0.1585(5) -0.0963(11) 0.3936(4) 0.157(4) Uani 1 1 d . . . . . H8A H 0.115301 -0.121349 0.413531 0.235 Uiso 1 1 calc GR . . . . H8B H 0.159192 -0.182977 0.366084 0.235 Uiso 1 1 calc GR . . . . H8C H 0.142297 0.004836 0.371932 0.235 Uiso 1 1 calc GR . . . . C6A C 0.5757(8) 0.9948(13) 0.7104(4) 0.093(3) Uani 0.673(11) 1 d D U . A 2 H6AA H 0.569750 1.033241 0.670283 0.112 Uiso 0.673(11) 1 calc R . . A 2 H6AB H 0.516420 0.991551 0.715134 0.112 Uiso 0.673(11) 1 calc R . . A 2 C10 C 0.2743(6) -0.2253(7) 0.4778(5) 0.151(4) Uani 1 1 d . . . . . H10A H 0.259815 -0.324310 0.453818 0.182 Uiso 1 1 calc R . . . . H10B H 0.338644 -0.224338 0.498421 0.182 Uiso 1 1 calc R . . . . C7A C 0.6380(12) 1.1066(18) 0.7572(7) 0.113(5) Uani 0.673(11) 1 d D U . A 2 H7AA H 0.651466 1.057167 0.796038 0.170 Uiso 0.673(11) 1 calc GR . . A 2 H7AB H 0.609115 1.210490 0.757062 0.170 Uiso 0.673(11) 1 calc GR . . A 2 H7AC H 0.692873 1.122878 0.747873 0.170 Uiso 0.673(11) 1 calc GR . . A 2 C3A C 0.6018(6) 0.5511(10) 0.6625(5) 0.094(3) Uani 0.673(11) 1 d D U . A 2 H3AA H 0.602823 0.487856 0.697599 0.113 Uiso 0.673(11) 1 calc R . . A 2 H3AB H 0.662829 0.558728 0.660833 0.113 Uiso 0.673(11) 1 calc R . . A 2 C4A C 0.5633(5) 0.7240(10) 0.6654(5) 0.092(3) Uani 0.673(11) 1 d D U . A 2 H4AA H 0.502079 0.713475 0.666486 0.110 Uiso 0.673(11) 1 calc R . . A 2 H4AB H 0.560983 0.783630 0.629307 0.110 Uiso 0.673(11) 1 calc R . . A 2 C2 C 0.551(3) 0.458(4) 0.6082(18) 0.096(6) Uani 0.327(11) 1 d D U . A 1 H2A H 0.589980 0.375844 0.633369 0.115 Uiso 0.327(11) 1 calc R . . A 1 H2B H 0.552281 0.445332 0.567331 0.115 Uiso 0.327(11) 1 calc R . . A 1 C3 C 0.5806(12) 0.633(3) 0.6318(7) 0.088(5) Uani 0.327(11) 1 d D U . A 1 H3A H 0.534682 0.711431 0.611444 0.105 Uiso 0.327(11) 1 calc R . . A 1 H3B H 0.636262 0.662119 0.624531 0.105 Uiso 0.327(11) 1 calc R . . A 1 C4 C 0.5944(13) 0.635(2) 0.6998(7) 0.089(5) Uani 0.327(11) 1 d D U . A 1 H4A H 0.641367 0.560729 0.722553 0.107 Uiso 0.327(11) 1 calc R . . A 1 H4B H 0.539256 0.616556 0.709374 0.107 Uiso 0.327(11) 1 calc R . . A 1 C5A C 0.6194(10) 0.8249(12) 0.7210(6) 0.103(4) Uani 0.673(11) 1 d D U . A 2 H5AA H 0.615529 0.776998 0.757847 0.124 Uiso 0.673(11) 1 calc R . . A 2 H5AB H 0.682139 0.830492 0.722973 0.124 Uiso 0.673(11) 1 calc R . . A 2 C6 C 0.577(2) 0.944(3) 0.7319(14) 0.124(8) Uani 0.327(11) 1 d D U . A 1 H6A H 0.580479 0.905326 0.771501 0.148 Uiso 0.327(11) 1 calc R . . A 1 H6B H 0.513754 0.942005 0.708052 0.148 Uiso 0.327(11) 1 calc R . . A 1 C7 C 0.605(3) 1.125(4) 0.7388(19) 0.140(12) Uani 0.327(11) 1 d D U . A 1 H7A H 0.632792 1.149414 0.780453 0.211 Uiso 0.327(11) 1 calc GR . . A 1 H7B H 0.552862 1.192547 0.722675 0.211 Uiso 0.327(11) 1 calc GR . . A 1 H7C H 0.647078 1.144943 0.717457 0.211 Uiso 0.327(11) 1 calc GR . . A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Mn1 0.0501(5) 0.0360(4) 0.0632(5) 0.000 0.0079(4) 0.000 S2 0.0607(6) 0.0769(8) 0.0967(8) -0.0178(6) 0.0260(6) -0.0101(5) S1 0.0688(7) 0.0778(8) 0.0914(8) -0.0247(6) 0.0270(6) -0.0151(6) O1 0.0691(19) 0.103(3) 0.136(3) -0.060(2) 0.044(2) -0.0324(18) C1 0.081(2) 0.055(2) 0.079(3) -0.0139(18) 0.025(2) -0.0213(18) N006 0.072(2) 0.071(3) 0.122(4) -0.042(3) 0.021(2) 0.000(2) C2A 0.062(7) 0.108(8) 0.168(9) -0.057(8) 0.043(6) -0.036(7) C5 0.110(13) 0.097(9) 0.103(12) -0.010(8) 0.039(10) -0.015(9) C9 0.127(6) 0.144(7) 0.152(6) -0.070(6) 0.065(5) 0.004(5) C8 0.103(5) 0.152(7) 0.184(8) -0.121(7) 0.001(5) -0.013(5) C6A 0.095(6) 0.114(7) 0.073(6) -0.003(5) 0.029(5) -0.014(5) C10 0.159(8) 0.043(3) 0.254(12) -0.030(4) 0.068(7) 0.011(4) C7A 0.141(11) 0.086(7) 0.095(9) -0.005(6) 0.014(8) -0.004(7) C3A 0.057(4) 0.085(5) 0.130(8) -0.004(5) 0.014(5) -0.006(4) C4A 0.069(4) 0.084(5) 0.117(7) -0.015(5) 0.021(4) -0.012(4) C2 0.062(10) 0.103(12) 0.136(13) -0.049(11) 0.051(10) -0.009(9) C3 0.059(8) 0.104(11) 0.111(9) -0.028(8) 0.042(8) -0.030(8) C4 0.079(9) 0.089(9) 0.097(9) -0.012(8) 0.026(8) -0.004(8) C5A 0.091(6) 0.103(6) 0.121(9) -0.036(6) 0.040(6) -0.028(5) C6 0.142(15) 0.121(12) 0.110(16) -0.011(12) 0.043(13) 0.002(12) C7 0.20(3) 0.112(13) 0.11(2) 0.006(17) 0.04(2) 0.015(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn -0.5299 2.8052 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S2 Mn1 S2 152.04(7) . 2_556 ? S1 Mn1 S2 69.21(4) . . ? S1 Mn1 S2 92.34(5) 2_556 . ? S1 Mn1 S2 92.34(5) . 2_556 ? S1 Mn1 S2 69.20(4) 2_556 2_556 ? S1 Mn1 S1 98.90(7) . 2_556 ? N006 Mn1 S2 98.38(11) . . ? N006 Mn1 S2 103.23(11) . 2_556 ? N006 Mn1 S2 98.38(11) 2_556 2_556 ? N006 Mn1 S2 103.23(11) 2_556 . ? N006 Mn1 S1 163.04(12) 2_556 2_556 ? N006 Mn1 S1 163.05(12) . . ? N006 Mn1 S1 92.95(14) . 2_556 ? N006 Mn1 S1 92.95(14) 2_556 . ? N006 Mn1 N006 78.3(3) . 2_556 ? C1 S2 Mn1 80.75(17) . . ? C1 S1 Mn1 84.60(16) . . ? C1 O1 C2A 121.9(7) . . ? C1 O1 C2 121.5(9) . . ? S1 C1 S2 125.0(3) . . ? O1 C1 S2 119.8(4) . . ? O1 C1 S1 115.1(3) . . ? C9 N006 Mn1 111.8(4) . . ? C9 N006 C8 108.2(6) . . ? C9 N006 C10 108.9(5) . . ? C8 N006 Mn1 109.5(3) . . ? C10 N006 Mn1 106.1(4) . . ? C10 N006 C8 112.4(6) . . ? O1 C2A H2AA 110.0 . . ? O1 C2A H2AB 110.0 . . ? O1 C2A C3A 108.4(14) . . ? H2AA C2A H2AB 108.4 . . ? C3A C2A H2AA 110.0 . . ? C3A C2A H2AB 110.0 . . ? H5A C5 H5B 106.8 . . ? C4 C5 H5A 107.1 . . ? C4 C5 H5B 107.1 . . ? C6 C5 H5A 107.1 . . ? C6 C5 H5B 107.1 . . ? C6 C5 C4 121(2) . . ? N006 C9 H9A 109.5 . . ? N006 C9 H9B 109.5 . . ? N006 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? N006 C8 H8A 109.5 . . ? N006 C8 H8B 109.5 . . ? N006 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? H6AA C6A H6AB 108.7 . . ? C7A C6A H6AA 110.6 . . ? C7A C6A H6AB 110.6 . . ? C7A C6A C5A 105.9(9) . . ? C5A C6A H6AA 110.6 . . ? C5A C6A H6AB 110.6 . . ? N006 C10 H10A 109.6 . . ? N006 C10 H10B 109.6 . . ? C10 C10 N006 110.4(6) 2_556 . ? C10 C10 H10A 109.6 2_556 . ? C10 C10 H10B 109.6 2_556 . ? H10A C10 H10B 108.1 . . ? C6A C7A H7AA 109.5 . . ? C6A C7A H7AB 109.5 . . ? C6A C7A H7AC 109.5 . . ? H7AA C7A H7AB 109.5 . . ? H7AA C7A H7AC 109.5 . . ? H7AB C7A H7AC 109.5 . . ? C2A C3A H3AA 110.3 . . ? C2A C3A H3AB 110.3 . . ? H3AA C3A H3AB 108.6 . . ? C4A C3A C2A 107.0(11) . . ? C4A C3A H3AA 110.3 . . ? C4A C3A H3AB 110.3 . . ? C3A C4A H4AA 108.9 . . ? C3A C4A H4AB 108.9 . . ? C3A C4A C5A 113.3(8) . . ? H4AA C4A H4AB 107.7 . . ? C5A C4A H4AA 108.9 . . ? C5A C4A H4AB 108.9 . . ? O1 C2 H2A 111.3 . . ? O1 C2 H2B 111.3 . . ? H2A C2 H2B 109.2 . . ? C3 C2 O1 102(2) . . ? C3 C2 H2A 111.3 . . ? C3 C2 H2B 111.3 . . ? C2 C3 H3A 110.1 . . ? C2 C3 H3B 110.1 . . ? C2 C3 C4 108(2) . . ? H3A C3 H3B 108.4 . . ? C4 C3 H3A 110.1 . . ? C4 C3 H3B 110.1 . . ? C5 C4 H4A 113.3 . . ? C5 C4 H4B 113.3 . . ? C3 C4 C5 91.7(17) . . ? C3 C4 H4A 113.3 . . ? C3 C4 H4B 113.3 . . ? H4A C4 H4B 110.7 . . ? C6A C5A C4A 103.7(9) . . ? C6A C5A H5AA 111.0 . . ? C6A C5A H5AB 111.0 . . ? C4A C5A H5AA 111.0 . . ? C4A C5A H5AB 111.0 . . ? H5AA C5A H5AB 109.0 . . ? C5 C6 H6A 106.7 . . ? C5 C6 H6B 106.7 . . ? C5 C6 C7 123(2) . . ? H6A C6 H6B 106.6 . . ? C7 C6 H6A 106.7 . . ? C7 C6 H6B 106.7 . . ? C6 C7 H7A 109.5 . . ? C6 C7 H7B 109.5 . . ? C6 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Mn1 S2 2.6488(11) . ? Mn1 S2 2.6489(11) 2_556 ? Mn1 S1 2.5692(13) 2_556 ? Mn1 S1 2.5691(13) . ? Mn1 N006 2.283(4) . ? Mn1 N006 2.283(4) 2_556 ? S2 C1 1.708(5) . ? S1 C1 1.633(5) . ? O1 C1 1.361(5) . ? O1 C2A 1.40(2) . ? O1 C2 1.55(5) . ? N006 C9 1.476(8) . ? N006 C8 1.480(8) . ? N006 C10 1.478(10) . ? C2A H2AA 0.9700 . ? C2A H2AB 0.9700 . ? C2A C3A 1.545(10) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C5 C4 1.546(10) . ? C5 C6 1.527(10) . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C6A H6AA 0.9700 . ? C6A H6AB 0.9700 . ? C6A C7A 1.521(9) . ? C6A C5A 1.530(9) . ? C10 C10 1.472(16) 2_556 ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C7A H7AA 0.9600 . ? C7A H7AB 0.9600 . ? C7A H7AC 0.9600 . ? C3A H3AA 0.9700 . ? C3A H3AB 0.9700 . ? C3A C4A 1.544(8) . ? C4A H4AA 0.9700 . ? C4A H4AB 0.9700 . ? C4A C5A 1.558(9) . ? C2 H2A 0.9700 . ? C2 H2B 0.9700 . ? C2 C3 1.543(10) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C4 1.545(10) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C5A H5AA 0.9700 . ? C5A H5AB 0.9700 . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 C7 1.528(10) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ?